Crystallography Open Database

Information card for entry 2022924

2022923 << 2022924 >> 2022925

Preview

Coordinates	2022924.cif
Original IUCr paper	HTML

Structure parameters

Chemical name	Bis(9-mesityl-9,10-dihydro-10-aza-9-borabenzo[<i>h</i>]quinolinato-κ^2^<i>N</i>^1^,<i>N</i>^10^)zinc(II)
Formula	C40 H36 B2 N4 Zn
Calculated formula	C40 H36 B2 N4 Zn
Title of publication	Synthesis and crystal structure of bis-(9-mesityl-9,10-di-hydro-10-aza-9-borabenzo[<i>h</i>]quinolinato-κ<sup>2</sup><i>N</i><sup>1</sup>,<i>N</i><sup>10</sup>)zinc(II).
Authors of publication	Appiarius, Yannik; Puylaert, Pim; Staubitz, Anne
Journal of publication	Acta crystallographica. Section E, Crystallographic communications
Year of publication	2023
Journal volume	79
Journal issue	Pt 11
Pages of publication	1063 - 1066
a	20.0425 ± 0.0014 Å
b	9.8589 ± 0.0006 Å
c	17.1167 ± 0.0009 Å
α	90°
β	105.172 ± 0.004°
γ	90°
Cell volume	3264.3 ± 0.4 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.05
Residual factor for significantly intense reflections	0.0363
Weighted residual factors for significantly intense reflections	0.0891
Weighted residual factors for all reflections included in the refinement	0.0974
Goodness-of-fit parameter for all reflections included in the refinement	1.057
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
288150 (current)	2023-12-07	cif/ Updating files of 2022924 Original log message: Adding full bibliography for 2022924.cif.	2022924.cif
287108	2023-10-25	cif/ hkl/ Adding structures of 2022924 via cif-deposit CGI script.	2022924.cif