#------------------------------------------------------------------------------ #$Date: 2023-12-07 12:52:00 +0100 (Thu, 07 Dec 2023) $ #$Revision: 288150 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/29/2022924.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022924 loop_ _publ_author_name 'Appiarius, Yannik' 'Puylaert, Pim' 'Staubitz, Anne' _publ_section_title ; Synthesis and crystal structure of bis-(9-mesityl-9,10-di-hydro-10-aza-9-borabenzo[h]quinolinato-κ2N1,N10)zinc(II). ; _journal_coeditor_code DJ2071 _journal_issue 'Pt 11' _journal_name_full 'Acta crystallographica. Section E, Crystallographic communications' _journal_page_first 1063 _journal_page_last 1066 _journal_paper_doi 10.1107/S2056989023009192 _journal_volume 79 _journal_year 2023 _chemical_formula_iupac '[Zn (C20 H18 B1 N2)2]' _chemical_formula_moiety 'C40 H36 B2 N4 Zn' _chemical_formula_sum 'C40 H36 B2 N4 Zn' _chemical_formula_weight 659.72 _chemical_name_systematic Bis(9-mesityl-9,10-dihydro-10-aza-9-borabenzo[h]quinolinato-\k^2^N^1^,N^10^)zinc(II) _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_method ; Olex2 1.5 (compiled 2021.08.20 svn.r13c46975 for OlexSys, GUI svn.r6396) ; _cell_angle_alpha 90 _cell_angle_beta 105.172(4) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 20.0425(14) _cell_length_b 9.8589(6) _cell_length_c 17.1167(9) _cell_measurement_reflns_used 9897 _cell_measurement_temperature 100.00 _cell_measurement_theta_max 33.35 _cell_measurement_theta_min 2.75 _cell_volume 3264.3(4) _computing_cell_refinement ; SAINT (Bruker, 2016) ; _computing_data_collection ; APEX2 (Bruker, 2016) ; _computing_data_reduction ; SAINT (Bruker, 2016) ; _computing_molecular_graphics ; Olex2 1.5 (Dolomanov et al., 2009), ORTEP-3 for Windows (Farrugia, 2012) ; _computing_publication_material ; publCIF (Westrip, 2010) ; _computing_structure_refinement ; SHELXL2018/3 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2018/2 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 100.00 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device_type 'Bruker APEXII CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0835 _diffrn_reflns_av_unetI/netI 0.0321 _diffrn_reflns_limit_h_max 31 _diffrn_reflns_limit_h_min -31 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_limit_l_min -26 _diffrn_reflns_number 95271 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 33.865 _diffrn_reflns_theta_min 2.753 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.788 _exptl_absorpt_correction_T_max 0.7467 _exptl_absorpt_correction_T_min 0.6767 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_crystal_colour 'light yellow' _exptl_crystal_density_diffrn 1.342 _exptl_crystal_description irregular _exptl_crystal_F_000 1376 _exptl_crystal_size_max 0.24 _exptl_crystal_size_mid 0.12 _exptl_crystal_size_min 0.09 _refine_diff_density_max 0.518 _refine_diff_density_min -0.402 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.057 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 216 _refine_ls_number_reflns 6577 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.057 _refine_ls_R_factor_all 0.0500 _refine_ls_R_factor_gt 0.0363 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0416P)^2^+3.4887P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0891 _refine_ls_wR_factor_ref 0.0974 _reflns_number_gt 5466 _reflns_number_total 6577 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file dj2071sup1.cif _cod_data_source_block I _cod_depositor_comments 'Adding full bibliography for 2022924.cif.' _cod_database_code 2022924 _cod_database_fobs_code 2022924 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.833 _shelx_estimated_absorpt_t_max 0.932 _shelx_hkl_file ; -2 0 0 0.20 0.20 -2 0 0 0.10 0.10 -2 0 0 0.10 0.20 4 0 0 193.68 9.80 4 0 0 179.48 10.20 4 0 0 170.18 9.50 4 0 0 167.38 10.10 -4 0 0 164.98 9.60 -4 0 0 187.88 9.80 -4 0 0 195.18 10.30 -4 0 0 167.58 10.20 6 0 0 5.30 1.80 6 0 0 6.30 1.10 -6 0 0 6.20 1.00 -6 0 0 6.70 1.80 6 0 0 6.70 1.60 -6 0 0 7.30 1.80 -6 0 0 4.80 1.20 -8 0 0 340.67 17.70 -8 0 0 280.27 18.20 -8 0 0 328.77 16.60 -8 0 0 315.57 17.30 -8 0 0 344.97 16.90 -8 0 0 330.37 18.70 8 0 0 331.57 18.50 8 0 0 283.57 17.50 8 0 0 340.27 18.60 8 0 0 312.67 16.40 8 0 0 322.97 17.20 8 0 0 323.77 16.60 10 0 0 127.09 7.10 10 0 0 139.39 9.10 10 0 0 132.39 8.40 10 0 0 125.09 6.90 -10 0 0 112.39 8.90 10 0 0 126.99 9.00 10 0 0 117.29 7.60 -10 0 0 117.49 8.00 -10 0 0 125.99 6.90 -10 0 0 123.89 7.20 -12 0 0 94.39 5.70 -12 0 0 72.99 6.40 12 0 0 78.89 7.50 12 0 0 90.59 6.10 12 0 0 92.39 5.30 -12 0 0 90.89 7.80 -12 0 0 94.69 5.40 12 0 0 92.49 7.60 12 0 0 95.99 7.00 12 0 0 88.79 5.00 14 0 0 370.96 22.50 -14 0 0 373.96 19.20 14 0 0 349.57 19.00 -14 0 0 403.76 19.70 -14 0 0 383.06 21.00 -14 0 0 365.96 22.50 14 0 0 360.96 20.00 14 0 0 324.97 20.80 14 0 0 350.46 18.70 14 0 0 322.77 21.60 16 0 0 93.49 5.50 16 0 0 104.39 9.40 -16 0 0 96.19 7.60 16 0 0 83.19 5.70 16 0 0 97.09 8.10 -16 0 0 90.99 6.30 -16 0 0 91.09 9.10 -16 0 0 96.39 6.00 18 0 0 39.80 3.40 -18 0 0 42.80 5.80 -18 0 0 49.80 7.40 18 0 0 38.00 3.00 18 0 0 38.70 4.20 -18 0 0 45.60 3.70 -18 0 0 46.60 4.20 18 0 0 46.20 7.50 18 0 0 54.19 7.20 20 0 0 104.59 7.70 20 0 0 103.89 9.50 20 0 0 100.99 6.10 20 0 0 91.59 6.40 20 0 0 95.59 9.40 -20 0 0 105.29 7.40 -20 0 0 98.09 13.60 -20 0 0 111.79 10.80 20 0 0 91.09 10.10 -20 0 0 102.39 6.80 22 0 0 85.39 13.50 -22 0 0 101.79 6.80 22 0 0 92.99 10.70 22 0 0 88.59 6.70 22 0 0 91.09 6.30 22 0 0 90.59 7.20 -22 0 0 97.39 11.10 22 0 0 102.09 9.90 -24 0 0 31.30 7.70 -24 0 0 30.10 4.80 24 0 0 30.70 3.70 24 0 0 27.50 4.90 24 0 0 35.40 3.00 -24 0 0 28.70 4.10 24 0 0 43.50 7.20 24 0 0 42.60 8.20 26 0 0 -0.20 4.00 26 0 0 3.30 1.90 -26 0 0 7.20 4.80 -26 0 0 6.20 2.90 26 0 0 -4.20 2.60 -26 0 0 -0.90 2.70 26 0 0 -6.50 2.80 26 0 0 5.20 1.60 28 0 0 22.10 5.90 -28 0 0 16.70 7.20 28 0 0 23.70 3.30 28 0 0 29.00 2.70 -28 0 0 25.90 4.70 28 0 0 28.90 5.00 28 0 0 25.40 7.10 -28 0 0 21.90 5.00 -30 0 0 15.70 8.00 30 0 0 9.90 5.20 -30 0 0 16.40 4.30 30 0 0 13.60 5.40 30 0 0 3.00 6.00 -30 0 0 8.60 4.40 -1 -1 0 0.20 0.30 -1 -1 0 0.20 0.20 -1 1 0 -0.10 0.20 3 -1 0 270.67 15.20 -3 -1 0 288.07 15.00 -3 -1 0 268.27 15.30 3 -1 0 285.67 15.00 3 -1 0 302.97 15.80 3 1 0 305.47 15.40 -3 1 0 313.87 15.40 3 1 0 276.87 14.50 -3 1 0 296.07 14.90 3 1 0 254.27 14.90 -5 -1 0 488.15 25.80 -5 -1 0 474.15 25.70 -5 -1 0 444.96 26.80 -5 -1 0 523.95 26.40 5 -1 0 491.75 26.30 5 -1 0 517.95 26.30 5 1 0 546.05 27.10 -5 1 0 498.45 26.40 5 1 0 544.35 26.50 -5 1 0 478.55 25.80 -5 1 0 563.74 26.40 -5 1 0 525.55 27.00 -5 1 0 490.05 25.70 7 -1 0 6.00 1.90 7 -1 0 5.40 0.70 7 -1 0 6.00 1.30 -7 -1 0 6.10 1.50 7 -1 0 5.60 2.00 -7 -1 0 5.00 1.00 7 -1 0 7.00 1.60 -7 -1 0 6.40 1.90 7 -1 0 4.60 0.80 -7 -1 0 7.10 1.40 -7 1 0 5.60 1.40 -7 1 0 3.00 1.40 7 1 0 7.20 1.10 -7 1 0 4.50 2.20 7 1 0 4.90 1.90 7 1 0 6.70 1.60 -7 1 0 3.90 1.00 7 1 0 3.70 1.00 -7 1 0 2.40 1.60 -7 1 0 6.60 1.00 7 1 0 6.30 0.90 7 1 0 7.60 1.60 -9 -1 0 126.89 9.00 -9 -1 0 124.09 8.10 -9 -1 0 126.69 7.20 9 -1 0 122.79 8.80 9 -1 0 123.89 7.80 9 -1 0 131.29 6.70 9 -1 0 120.09 6.90 9 -1 0 113.69 8.90 -9 -1 0 124.59 6.90 9 -1 0 109.79 8.00 9 1 0 133.89 8.60 9 1 0 141.79 9.20 -9 1 0 124.29 7.00 -9 1 0 128.99 7.20 -9 1 0 119.89 7.90 9 1 0 136.09 8.30 -9 1 0 139.79 8.10 -9 1 0 111.89 9.20 -9 1 0 135.49 9.10 9 1 0 128.19 7.50 11 -1 0 4.80 2.30 -11 -1 0 3.70 1.30 11 -1 0 3.70 0.80 11 -1 0 4.30 1.90 -11 -1 0 3.50 1.70 11 -1 0 1.80 0.80 11 -1 0 5.30 1.50 11 -1 0 4.40 2.20 -11 -1 0 1.40 2.00 -11 -1 0 2.90 1.10 11 1 0 0.60 1.40 -11 1 0 1.80 1.00 11 1 0 4.80 1.30 -11 1 0 3.90 2.30 11 1 0 3.20 1.70 11 1 0 3.70 0.90 11 1 0 3.00 1.00 -11 1 0 0.20 1.70 -11 1 0 2.80 1.50 11 1 0 1.60 1.50 -11 1 0 2.60 1.00 -11 1 0 0.70 1.30 -13 -1 0 34.90 5.70 -13 -1 0 30.60 4.20 13 -1 0 32.50 2.20 13 -1 0 28.20 3.20 -13 -1 0 32.10 2.60 13 -1 0 30.20 2.40 13 -1 0 36.00 4.50 -13 -1 0 34.40 3.00 13 -1 0 43.10 5.80 13 -1 0 32.00 5.50 -13 1 0 36.70 5.60 13 1 0 22.90 3.80 -13 1 0 33.10 5.70 13 1 0 32.70 4.80 -13 1 0 33.40 3.80 -13 1 0 30.50 2.80 13 1 0 30.80 3.00 13 1 0 47.90 5.50 13 1 0 32.40 2.30 13 1 0 35.40 2.70 -13 1 0 30.10 4.00 -13 1 0 31.60 3.80 15 -1 0 135.19 7.70 15 -1 0 144.19 11.30 -15 -1 0 136.29 8.10 15 -1 0 149.29 9.30 15 -1 0 131.29 7.90 15 -1 0 152.18 10.30 -15 -1 0 141.79 9.90 -15 -1 0 133.99 8.50 15 -1 0 126.59 10.80 -15 -1 0 131.09 11.30 15 1 0 141.39 10.40 -15 1 0 140.79 9.70 15 1 0 144.19 10.30 15 1 0 131.69 10.90 15 1 0 139.89 7.80 15 1 0 143.99 8.20 -15 1 0 143.39 8.60 -15 1 0 139.99 8.20 15 1 0 136.09 8.70 -15 1 0 153.38 11.40 17 -1 0 52.89 5.10 17 -1 0 63.69 6.70 -17 -1 0 55.69 4.60 -17 -1 0 65.49 6.20 17 -1 0 53.29 3.70 -17 -1 0 43.60 7.30 -17 -1 0 49.99 4.10 17 -1 0 57.29 4.00 17 -1 0 55.99 8.00 17 -1 0 44.70 7.30 -17 1 0 57.09 4.30 17 1 0 56.99 3.80 -17 1 0 69.99 6.10 -17 1 0 59.19 4.80 17 1 0 64.19 7.50 -17 1 0 56.39 8.30 17 1 0 52.69 7.00 17 1 0 64.59 6.60 17 1 0 55.99 4.10 17 1 0 55.09 4.70 -19 -1 0 60.29 4.90 -19 -1 0 72.69 7.00 -19 -1 0 57.79 9.00 19 -1 0 61.09 8.60 19 -1 0 64.09 9.20 -19 -1 0 66.19 5.50 19 -1 0 69.39 4.70 19 -1 0 71.39 4.40 19 -1 0 73.79 6.10 19 -1 0 78.99 7.80 -19 1 0 69.69 9.70 -19 1 0 63.59 5.50 19 1 0 76.19 5.00 19 1 0 75.29 5.80 19 1 0 72.39 7.60 19 1 0 54.19 8.70 19 1 0 61.79 4.40 -19 1 0 60.59 4.90 19 1 0 71.79 8.40 -21 -1 0 68.39 7.70 21 -1 0 85.49 7.10 21 -1 0 94.89 11.00 21 -1 0 63.19 9.90 -21 -1 0 88.19 9.70 21 -1 0 100.39 9.20 -21 -1 0 83.09 6.60 -21 -1 0 86.19 6.00 21 -1 0 83.19 5.60 21 -1 0 84.59 5.20 21 1 0 68.29 8.70 21 1 0 109.69 9.50 21 1 0 86.89 5.40 -21 1 0 74.79 5.90 21 1 0 83.69 9.40 21 1 0 75.09 6.30 -21 1 0 77.39 6.60 21 1 0 76.89 5.70 -21 1 0 66.39 10.10 23 -1 0 26.50 8.80 23 -1 0 47.30 5.80 23 -1 0 43.60 7.20 -23 -1 0 43.30 6.10 -23 -1 0 36.00 7.60 -23 -1 0 48.50 4.80 23 -1 0 46.90 3.50 23 -1 0 43.70 3.90 23 -1 0 36.00 7.20 -23 1 0 49.60 9.30 23 1 0 35.10 6.70 23 1 0 46.00 3.60 23 1 0 44.90 4.90 23 1 0 44.40 7.30 23 1 0 53.49 7.50 23 1 0 48.30 4.10 23 1 0 45.20 4.70 -25 -1 0 10.90 3.10 25 -1 0 25.60 2.40 25 -1 0 17.90 5.70 -25 -1 0 19.70 4.20 -25 -1 0 22.10 7.10 25 -1 0 20.00 3.00 -25 1 0 18.40 3.70 25 1 0 20.00 3.90 25 1 0 22.60 2.70 -25 1 0 13.50 4.00 -25 1 0 16.90 6.10 25 1 0 11.10 3.00 25 1 0 18.00 5.50 25 1 0 19.50 3.20 25 1 0 17.10 4.80 25 1 0 14.80 4.50 -27 -1 0 10.60 3.70 27 -1 0 9.00 4.90 -27 -1 0 4.10 2.70 27 -1 0 10.60 1.80 -27 -1 0 2.10 4.80 27 -1 0 7.20 2.10 27 1 0 9.00 1.80 27 1 0 6.80 2.20 27 1 0 7.00 3.70 -27 1 0 10.40 3.70 27 1 0 3.70 2.60 -27 1 0 -1.50 5.10 -27 1 0 7.20 3.00 27 1 0 6.70 5.30 -29 -1 0 3.60 3.10 29 -1 0 -2.60 4.80 -29 -1 0 1.40 3.40 -29 -1 0 -0.20 5.30 -29 1 0 1.40 2.60 29 1 0 -0.60 2.80 29 1 0 -0.10 2.20 -29 1 0 0.60 3.10 -29 1 0 1.40 6.40 29 1 0 -5.30 5.30 0 -2 0 330.97 18.60 0 -2 0 383.06 18.60 0 -2 0 361.76 18.60 0 2 0 361.36 18.80 0 2 0 367.06 18.70 -2 -2 0 200.68 10.30 -2 -2 0 203.58 10.90 2 -2 0 198.08 10.50 2 -2 0 207.28 10.70 -2 -2 0 206.68 10.70 2 -2 0 199.08 10.80 -2 -2 0 179.48 10.60 2 -2 0 218.78 11.70 2 2 0 188.38 10.30 -2 2 0 205.08 11.70 -2 2 0 200.08 10.80 2 2 0 194.38 10.40 2 2 0 197.98 10.70 2 2 0 188.18 10.20 -2 2 0 182.18 10.80 -2 2 0 203.18 10.40 4 -2 0 1403.16 68.79 4 -2 0 1345.97 68.49 -4 -2 0 1437.66 68.99 -4 2 0 1330.57 68.59 4 2 0 1323.17 67.79 -4 2 0 1236.18 68.79 4 2 0 1352.26 68.99 -6 -2 0 297.77 15.30 6 -2 0 288.47 17.50 6 -2 0 296.97 16.30 -6 -2 0 284.17 15.50 6 -2 0 294.17 15.20 -6 -2 0 335.07 16.50 -6 -2 0 286.67 16.90 6 -2 0 328.87 15.40 6 -2 0 305.87 16.80 6 -2 0 290.77 16.20 6 2 0 303.57 15.50 6 2 0 295.27 16.30 6 2 0 314.37 17.10 6 2 0 302.47 15.70 -6 2 0 314.37 15.60 -6 2 0 284.67 16.40 -6 2 0 304.67 16.10 6 2 0 298.27 15.40 6 2 0 295.07 15.90 -6 2 0 280.77 15.40 -6 2 0 266.97 16.70 -8 -2 0 74.39 4.50 -8 -2 0 81.79 5.70 8 -2 0 76.29 6.70 -8 -2 0 69.79 6.20 -8 -2 0 75.79 4.70 8 -2 0 88.09 5.80 8 -2 0 80.89 4.50 8 -2 0 81.99 5.60 8 -2 0 70.49 6.10 8 -2 0 80.89 4.40 8 2 0 76.79 4.60 -8 2 0 72.19 5.60 8 2 0 78.69 4.60 -8 2 0 85.69 6.50 -8 2 0 84.59 4.90 8 2 0 82.29 4.80 8 2 0 77.09 5.60 -8 2 0 93.79 5.60 8 2 0 88.49 5.90 8 2 0 77.29 6.40 8 2 0 74.59 4.80 -8 2 0 73.99 7.00 -8 2 0 81.89 4.60 8 2 0 80.59 5.30 -10 -2 0 2.20 0.90 -10 -2 0 4.50 1.20 10 -2 0 1.10 1.30 10 -2 0 1.80 1.60 10 -2 0 1.60 0.70 -10 -2 0 1.60 1.80 10 -2 0 2.10 1.90 10 -2 0 4.10 1.60 -10 -2 0 2.50 1.50 10 -2 0 2.20 0.80 -10 2 0 -1.10 1.70 10 2 0 3.50 1.70 10 2 0 3.80 0.90 10 2 0 2.80 1.00 -10 2 0 1.40 0.90 -10 2 0 1.10 1.30 -10 2 0 4.60 2.50 10 2 0 0.90 1.10 10 2 0 3.10 1.20 10 2 0 2.30 1.70 10 2 0 2.40 1.30 -10 2 0 1.20 1.40 -10 2 0 3.70 1.30 10 2 0 1.80 0.90 -12 -2 0 11.00 1.60 12 -2 0 9.20 2.90 12 -2 0 8.50 1.20 12 -2 0 7.50 3.40 -12 -2 0 6.80 1.60 -12 -2 0 11.00 2.50 -12 -2 0 8.00 2.90 12 -2 0 9.10 1.40 12 -2 0 2.20 1.80 12 -2 0 6.60 2.30 -12 2 0 4.80 2.10 -12 2 0 5.30 2.60 -12 2 0 5.90 1.40 12 2 0 4.20 1.80 12 2 0 5.90 1.30 12 2 0 6.00 2.70 12 2 0 5.60 2.10 12 2 0 7.20 1.50 -12 2 0 9.60 3.80 12 2 0 9.30 1.70 12 2 0 9.30 1.40 -12 2 0 9.50 1.90 -12 2 0 7.80 2.10 12 2 0 5.70 1.90 -14 -2 0 16.10 4.30 14 -2 0 14.40 2.80 14 -2 0 12.00 3.70 14 -2 0 18.50 2.10 -14 -2 0 17.90 2.20 14 -2 0 13.60 1.40 14 -2 0 16.60 3.50 -14 -2 0 16.10 3.30 -14 -2 0 15.30 2.40 14 -2 0 17.30 3.80 -14 2 0 10.20 2.70 14 2 0 12.60 2.20 14 2 0 16.30 3.40 14 2 0 16.10 2.30 -14 2 0 16.80 2.60 -14 2 0 10.40 3.70 -14 2 0 21.00 2.40 14 2 0 19.40 2.10 14 2 0 16.70 2.30 14 2 0 17.50 3.40 14 2 0 18.40 3.40 14 2 0 19.00 4.20 -16 -2 0 34.10 3.80 16 -2 0 25.30 5.50 16 -2 0 27.70 2.10 -16 -2 0 25.80 4.50 16 -2 0 27.80 2.40 16 -2 0 21.90 4.20 -16 -2 0 29.10 5.80 -16 -2 0 29.10 2.70 16 -2 0 23.40 4.90 16 -2 0 36.60 4.50 -16 2 0 27.40 2.80 16 2 0 24.40 2.30 -16 2 0 31.20 5.80 -16 2 0 20.00 5.50 16 2 0 28.30 3.30 16 2 0 21.30 4.00 16 2 0 23.40 5.60 16 2 0 22.30 4.00 -16 2 0 23.60 4.20 16 2 0 23.80 4.60 16 2 0 20.10 2.80 -16 2 0 28.60 4.70 -16 2 0 28.60 3.70 16 2 0 27.20 3.20 -18 -2 0 12.30 4.60 18 -2 0 7.70 2.70 18 -2 0 2.60 2.80 18 -2 0 9.00 1.80 18 -2 0 6.90 1.40 18 -2 0 5.30 3.10 -18 -2 0 7.60 2.70 18 -2 0 3.80 3.50 -18 -2 0 8.20 2.00 -18 -2 0 5.30 2.20 -18 2 0 9.00 4.10 -18 2 0 10.70 3.10 18 2 0 3.10 1.40 18 2 0 8.00 2.10 18 2 0 6.60 3.60 -18 2 0 5.00 2.10 18 2 0 5.80 2.60 18 2 0 3.90 2.60 -18 2 0 7.50 1.90 18 2 0 10.10 3.50 18 2 0 3.70 1.70 18 2 0 5.90 1.50 20 -2 0 1.60 2.90 20 -2 0 -4.00 2.00 20 -2 0 -1.20 2.70 -20 -2 0 2.30 1.70 20 -2 0 -0.50 1.10 -20 -2 0 1.20 3.90 -20 -2 0 0.20 1.80 -20 -2 0 -0.80 2.20 20 -2 0 -0.20 1.20 20 -2 0 0.70 1.60 -20 2 0 -2.10 1.90 20 2 0 0.30 1.20 20 2 0 -0.10 1.50 -20 2 0 -0.50 1.60 -20 2 0 -1.00 2.40 20 2 0 -1.60 3.00 -20 2 0 4.20 2.90 20 2 0 -0.60 2.10 20 2 0 1.90 2.30 20 2 0 -0.50 1.40 -22 -2 0 4.50 4.50 22 -2 0 7.80 4.40 -22 -2 0 1.90 2.20 22 -2 0 5.00 2.70 22 -2 0 1.00 3.20 22 -2 0 -1.30 3.70 -22 -2 0 4.00 3.20 -22 -2 0 6.70 2.20 22 2 0 2.80 1.90 -22 2 0 0.80 1.90 22 2 0 4.00 2.60 22 2 0 -1.80 3.00 -22 2 0 0.50 3.30 -22 2 0 3.80 2.60 22 2 0 3.50 1.60 22 2 0 0.70 1.90 22 2 0 10.40 4.40 24 -2 0 13.70 2.00 -24 -2 0 7.60 2.70 -24 -2 0 19.90 5.60 24 -2 0 9.90 2.30 -24 -2 0 13.20 3.60 24 2 0 15.10 4.10 -24 2 0 11.70 3.40 24 2 0 18.10 3.10 24 2 0 9.60 4.60 24 2 0 10.80 2.80 24 2 0 5.90 2.50 24 2 0 22.20 8.40 24 2 0 13.90 2.30 -24 2 0 13.80 3.00 -24 2 0 6.80 4.50 24 2 0 4.00 2.90 -26 -2 0 3.70 4.10 -26 -2 0 0.70 2.80 26 -2 0 2.50 1.40 -26 -2 0 4.80 2.70 26 -2 0 2.30 1.70 26 -2 0 3.10 4.00 -26 2 0 -3.50 4.30 26 2 0 -1.30 2.40 -26 2 0 6.00 3.40 26 2 0 1.00 1.80 -26 2 0 2.50 2.60 26 2 0 2.40 2.00 26 2 0 -5.00 2.30 26 2 0 2.30 2.70 26 2 0 2.10 4.20 26 2 0 1.20 1.60 -28 -2 0 0.50 3.00 -28 -2 0 -1.40 2.60 -28 -2 0 4.50 6.20 28 -2 0 -5.80 4.10 -28 2 0 1.90 5.10 28 2 0 0.90 1.90 28 2 0 9.90 6.30 -28 2 0 0.90 2.70 28 2 0 -0.80 1.70 28 2 0 3.50 1.60 -28 2 0 2.70 3.10 28 2 0 1.10 1.40 -30 -2 0 0.00 3.40 -30 2 0 1.70 3.30 1 -3 0 60.39 4.00 -1 -3 0 61.59 3.60 1 -3 0 62.79 4.70 -1 -3 0 51.39 4.10 -1 -3 0 54.19 3.80 1 -3 0 56.89 3.80 1 -3 0 56.59 3.60 -1 3 0 55.69 3.50 -1 3 0 54.59 3.90 -1 3 0 56.39 3.80 -1 3 0 55.99 3.60 1 3 0 53.69 3.60 -1 3 0 59.19 3.40 -1 3 0 59.29 4.80 1 3 0 61.39 4.40 1 3 0 52.99 3.90 3 -3 0 292.17 15.60 3 -3 0 286.57 15.80 3 -3 0 304.67 15.40 -3 -3 0 282.87 15.00 -3 -3 0 283.07 15.90 3 -3 0 299.37 16.90 -3 -3 0 311.07 15.60 -3 -3 0 265.97 15.50 -3 3 0 291.57 15.70 3 3 0 276.67 15.00 -3 3 0 306.57 15.90 3 3 0 285.67 15.20 3 3 0 282.27 15.00 3 3 0 286.57 15.60 -3 3 0 305.27 17.10 -3 3 0 270.67 15.20 -5 -3 0 433.66 24.00 -5 -3 0 443.76 23.20 -5 -3 0 476.35 23.30 5 -3 0 455.55 23.90 5 -3 0 481.75 25.70 5 -3 0 454.45 24.10 -5 -3 0 472.85 24.70 -5 -3 0 442.16 23.10 -5 -3 0 465.25 23.70 5 -3 0 457.25 24.40 -5 3 0 451.75 25.90 -5 3 0 475.45 24.40 5 3 0 490.15 23.20 5 3 0 425.96 24.60 -5 3 0 420.76 23.00 -5 3 0 461.65 24.60 -5 3 0 414.06 23.60 -5 3 0 455.85 23.20 5 3 0 431.46 23.20 5 3 0 455.65 23.50 7 -3 0 72.59 5.00 7 -3 0 69.09 3.90 7 -3 0 61.69 5.20 7 -3 0 62.09 3.70 -7 -3 0 69.79 5.00 -7 -3 0 70.09 5.70 7 -3 0 74.99 6.50 7 -3 0 74.99 5.10 7 3 0 61.79 3.80 7 3 0 66.89 4.30 -7 3 0 68.19 4.10 -7 3 0 68.09 3.90 7 3 0 66.19 4.00 7 3 0 52.79 5.30 -7 3 0 61.49 5.10 7 3 0 64.49 4.30 -7 3 0 71.19 6.70 -7 3 0 69.69 4.70 7 3 0 59.29 4.80 -7 3 0 55.39 5.20 9 -3 0 146.29 10.20 9 -3 0 155.88 9.60 9 -3 0 162.28 8.30 -9 -3 0 150.18 10.50 9 -3 0 150.98 11.20 9 -3 0 156.88 9.50 -9 -3 0 150.28 8.40 -9 -3 0 151.38 8.20 -9 -3 0 148.99 9.60 9 -3 0 146.09 8.00 -9 3 0 165.28 10.60 9 3 0 145.79 8.20 9 3 0 154.88 8.70 -9 3 0 142.09 11.50 9 3 0 146.89 9.60 9 3 0 127.09 10.00 -9 3 0 155.68 8.30 -9 3 0 157.38 8.60 -9 3 0 150.98 9.20 9 3 0 154.88 8.90 9 3 0 153.18 8.30 -9 3 0 144.19 9.70 11 -3 0 73.39 5.90 -11 -3 0 83.19 7.10 -11 -3 0 80.09 6.30 11 -3 0 79.59 4.40 -11 -3 0 79.89 4.90 11 -3 0 77.49 4.60 11 -3 0 82.99 7.80 11 -3 0 81.49 7.70 11 -3 0 88.69 6.50 -11 -3 0 76.39 4.60 -11 3 0 67.09 6.80 -11 3 0 79.29 6.40 11 3 0 62.39 6.80 11 3 0 79.89 4.70 11 3 0 73.69 5.70 -11 3 0 79.89 5.10 11 3 0 71.09 4.80 11 3 0 75.79 4.70 -11 3 0 78.69 5.80 11 3 0 76.09 5.00 11 3 0 76.99 5.40 11 3 0 73.39 6.20 -11 3 0 80.09 9.80 -11 3 0 78.99 4.80 13 -3 0 48.30 4.70 -13 -3 0 46.10 5.00 -13 -3 0 56.69 3.70 13 -3 0 54.39 3.30 13 -3 0 55.19 3.60 -13 -3 0 54.19 3.90 13 -3 0 51.39 7.40 -13 -3 0 54.09 6.30 13 -3 0 49.80 5.70 13 3 0 51.39 6.10 -13 3 0 52.19 7.00 13 3 0 51.59 3.60 -13 3 0 52.59 5.30 -13 3 0 51.59 4.10 13 3 0 42.40 5.00 13 3 0 55.19 4.80 13 3 0 55.39 3.60 13 3 0 58.19 4.10 -13 3 0 42.80 7.60 13 3 0 47.10 4.40 -13 3 0 41.10 3.60 13 3 0 55.69 3.80 -13 3 0 60.09 4.90 15 -3 0 48.60 6.60 15 -3 0 34.10 2.50 -15 -3 0 38.50 5.20 15 -3 0 32.30 2.80 -15 -3 0 35.80 3.00 -15 -3 0 33.50 3.30 -15 -3 0 37.00 6.30 15 -3 0 32.10 4.40 15 -3 0 45.20 5.70 15 -3 0 42.40 7.00 -15 3 0 37.40 3.50 15 3 0 42.80 4.20 15 3 0 34.50 3.10 15 3 0 42.10 4.90 15 3 0 36.00 3.00 -15 3 0 33.70 3.10 -15 3 0 43.90 7.90 -15 3 0 35.70 6.10 15 3 0 36.20 2.90 15 3 0 35.20 3.20 -15 3 0 33.80 4.10 15 3 0 31.90 4.90 -15 3 0 30.80 5.00 15 3 0 34.30 6.00 17 -3 0 10.90 4.30 17 -3 0 1.10 2.40 17 -3 0 13.00 4.10 17 -3 0 6.00 1.40 -17 -3 0 7.10 1.90 -17 -3 0 5.40 3.80 -17 -3 0 7.80 2.30 17 -3 0 11.90 3.00 -17 -3 0 9.20 3.00 17 -3 0 10.60 1.90 -17 3 0 6.80 3.30 17 3 0 5.60 2.30 17 3 0 9.60 2.60 -17 3 0 8.10 2.90 17 3 0 4.70 2.80 -17 3 0 10.20 2.10 -17 3 0 8.10 2.30 -17 3 0 4.60 2.60 17 3 0 4.30 3.10 17 3 0 10.10 1.80 -17 3 0 3.70 3.70 17 3 0 7.20 1.70 17 3 0 7.30 2.00 17 3 0 7.20 2.40 -19 -3 0 2.20 2.50 19 -3 0 6.50 3.30 -19 -3 0 1.90 1.80 -19 -3 0 7.50 2.60 19 -3 0 1.90 1.20 -19 -3 0 3.40 2.60 19 -3 0 0.40 1.20 -19 3 0 1.20 2.10 19 3 0 0.30 1.60 19 3 0 0.70 1.30 -19 3 0 1.50 2.00 19 3 0 -1.60 3.40 19 3 0 3.70 1.50 -19 3 0 3.10 1.90 19 3 0 3.20 1.90 19 3 0 2.80 2.10 19 3 0 4.30 1.30 -19 3 0 1.60 2.60 19 3 0 2.80 2.80 -21 -3 0 19.70 4.60 21 -3 0 17.00 3.90 21 -3 0 13.20 5.00 -21 -3 0 31.40 6.80 21 -3 0 25.40 5.50 -21 -3 0 20.00 3.70 -21 -3 0 18.60 3.10 21 -3 0 20.60 3.20 21 -3 0 19.20 3.70 21 3 0 17.30 3.80 21 3 0 19.20 2.70 -21 3 0 24.30 4.00 -21 3 0 16.10 4.90 -21 3 0 18.00 3.10 21 3 0 19.20 6.40 21 3 0 17.20 3.70 21 3 0 17.60 2.70 21 3 0 15.80 2.60 21 3 0 18.80 3.10 21 3 0 12.70 4.30 23 -3 0 18.80 2.50 23 -3 0 27.10 5.60 23 -3 0 19.30 2.90 -23 -3 0 23.40 6.20 23 3 0 14.10 2.50 23 3 0 24.40 6.50 23 3 0 26.30 3.10 -23 3 0 25.70 6.70 -23 3 0 16.30 3.90 23 3 0 11.20 5.30 23 3 0 20.60 3.40 23 3 0 13.40 3.40 -23 3 0 16.60 3.30 25 -3 0 54.09 3.80 -25 -3 0 49.90 6.40 25 -3 0 47.90 7.80 25 -3 0 49.99 4.30 -25 -3 0 32.20 8.50 -25 -3 0 54.69 5.20 -25 3 0 47.00 6.50 25 3 0 53.49 6.40 25 3 0 49.00 4.40 25 3 0 45.20 5.10 25 3 0 37.30 10.40 25 3 0 52.69 8.40 -25 3 0 54.99 5.20 -25 3 0 54.19 10.00 25 3 0 50.49 4.20 27 -3 0 55.49 3.80 27 -3 0 43.50 8.50 27 -3 0 43.20 4.10 -27 -3 0 42.00 9.30 -27 -3 0 54.29 5.50 -27 -3 0 37.00 6.20 -27 3 0 35.80 6.10 -27 3 0 58.69 5.70 27 3 0 52.79 8.80 27 3 0 56.29 4.10 -27 3 0 35.30 9.00 27 3 0 51.69 4.70 -29 -3 0 1.80 3.30 -29 -3 0 2.70 3.20 -29 -3 0 -1.60 5.70 29 -3 0 0.70 4.50 -29 3 0 5.00 5.70 -29 3 0 -1.20 2.50 29 3 0 -1.80 6.40 29 3 0 2.20 2.30 29 3 0 -0.70 1.60 -29 3 0 2.90 3.40 0 -4 0 305.37 16.70 0 -4 0 313.67 17.60 0 -4 0 285.97 16.50 0 -4 0 310.17 16.50 0 4 0 316.97 16.50 0 4 0 315.77 17.00 0 4 0 287.37 16.60 0 4 0 328.47 17.10 0 4 0 328.07 18.10 0 4 0 314.97 16.20 2 -4 0 39.10 4.70 2 -4 0 30.70 2.60 -2 -4 0 31.30 3.00 -2 -4 0 30.50 2.70 -2 -4 0 27.50 2.30 2 -4 0 30.20 2.70 2 -4 0 31.10 2.90 -2 -4 0 26.50 3.20 2 4 0 31.20 2.50 2 4 0 27.70 3.60 2 4 0 28.80 2.20 -2 4 0 32.10 3.10 -2 4 0 20.40 3.70 2 4 0 27.20 2.30 -2 4 0 27.20 2.20 2 4 0 22.00 2.40 -2 4 0 33.60 3.00 4 -4 0 77.89 5.20 -4 -4 0 77.69 5.30 4 -4 0 80.79 5.40 -4 -4 0 75.89 5.80 4 -4 0 68.59 5.40 4 -4 0 79.19 6.60 -4 -4 0 76.69 4.60 4 4 0 78.79 4.70 4 4 0 79.79 6.60 -4 4 0 73.19 4.80 -4 4 0 83.99 5.70 -4 4 0 92.79 7.40 4 4 0 75.39 4.90 4 4 0 76.19 5.40 4 4 0 80.49 4.70 -4 4 0 82.29 5.80 -6 -4 0 127.79 8.20 6 -4 0 121.39 9.10 -6 -4 0 132.49 7.70 6 -4 0 102.99 7.30 -6 -4 0 111.29 6.20 6 -4 0 101.79 7.60 6 -4 0 114.59 7.30 -6 -4 0 109.89 6.10 -6 -4 0 113.79 7.10 -6 -4 0 113.69 6.40 -6 4 0 115.89 7.80 -6 4 0 117.19 7.00 6 4 0 116.19 6.90 -6 4 0 117.09 6.70 -6 4 0 116.59 8.10 6 4 0 123.19 6.50 -6 4 0 115.89 6.40 6 4 0 114.29 7.10 6 4 0 93.99 7.80 6 4 0 117.89 6.50 -6 4 0 99.29 9.20 8 -4 0 154.78 8.30 -8 -4 0 137.99 10.10 8 -4 0 130.99 9.20 -8 -4 0 136.29 8.10 -8 -4 0 150.08 8.20 8 -4 0 159.08 10.10 -8 -4 0 142.69 8.00 -8 -4 0 165.08 9.70 8 -4 0 147.19 8.00 -8 -4 0 154.48 8.90 -8 4 0 148.79 8.20 -8 4 0 140.69 10.10 8 4 0 145.09 8.70 8 4 0 152.98 8.40 -8 4 0 157.78 12.10 8 4 0 145.79 8.70 8 4 0 173.08 9.70 -8 4 0 151.58 9.90 -8 4 0 136.09 8.30 8 4 0 164.38 8.20 8 4 0 170.08 10.70 -10 -4 0 125.39 10.10 10 -4 0 152.18 11.60 10 -4 0 140.59 9.30 -10 -4 0 145.39 7.80 10 -4 0 153.98 10.30 -10 -4 0 122.79 9.30 -10 -4 0 148.19 8.10 10 -4 0 149.79 8.00 10 -4 0 147.99 7.70 10 -4 0 147.59 9.50 10 4 0 142.89 10.50 10 4 0 144.39 8.50 10 4 0 134.19 7.80 10 4 0 143.49 8.10 -10 4 0 143.69 8.00 -10 4 0 134.69 8.30 10 4 0 149.59 9.60 -10 4 0 138.59 8.90 -10 4 0 156.08 10.60 10 4 0 140.79 8.50 -12 -4 0 98.09 8.30 12 -4 0 90.39 5.10 -12 -4 0 92.09 5.30 12 -4 0 89.09 7.70 -12 -4 0 73.79 6.70 12 -4 0 94.09 5.40 -12 -4 0 92.69 5.60 12 -4 0 87.09 8.70 12 -4 0 75.49 6.80 12 -4 0 85.79 6.80 12 4 0 86.29 5.90 -12 4 0 78.39 5.40 12 4 0 93.79 5.20 12 4 0 87.99 8.20 12 4 0 80.89 6.20 12 4 0 97.19 5.60 -12 4 0 87.79 11.30 -12 4 0 81.39 7.80 -12 4 0 82.09 6.40 12 4 0 83.69 5.80 -12 4 0 103.99 7.70 12 4 0 102.59 7.40 -12 4 0 91.59 5.90 12 4 0 86.99 5.40 14 -4 0 132.89 9.30 14 -4 0 101.49 10.40 14 -4 0 128.19 8.80 14 -4 0 115.79 7.00 -14 -4 0 101.09 9.80 -14 -4 0 110.59 7.30 -14 -4 0 136.29 9.30 -14 -4 0 120.79 7.00 14 -4 0 114.79 6.70 14 -4 0 143.89 10.40 14 4 0 116.19 7.00 -14 4 0 114.19 7.60 -14 4 0 111.09 13.50 -14 4 0 106.79 9.10 14 4 0 115.29 8.00 14 4 0 127.39 9.30 14 4 0 109.69 7.60 14 4 0 125.69 6.90 -14 4 0 109.89 10.00 -14 4 0 128.69 7.20 14 4 0 113.29 10.20 -14 4 0 117.29 8.40 16 -4 0 81.89 6.90 16 -4 0 108.09 11.90 16 -4 0 80.69 8.10 -16 -4 0 88.39 5.90 16 -4 0 82.49 7.60 16 -4 0 79.49 5.30 16 -4 0 79.29 4.90 -16 -4 0 88.79 9.00 -16 -4 0 86.69 5.40 -16 4 0 96.29 9.20 16 4 0 85.09 5.30 -16 4 0 82.99 6.00 16 4 0 83.79 7.70 16 4 0 74.89 5.90 16 4 0 75.69 5.00 16 4 0 80.79 5.90 16 4 0 90.49 9.10 16 4 0 75.09 5.30 -16 4 0 74.19 11.40 -16 4 0 80.99 5.50 -16 4 0 74.99 7.60 16 4 0 81.89 6.30 -18 -4 0 87.89 6.60 -18 -4 0 98.09 10.10 18 -4 0 95.69 8.70 18 -4 0 97.69 8.00 18 -4 0 87.39 11.50 18 -4 0 102.69 5.90 -18 -4 0 89.49 6.10 18 -4 0 85.49 9.30 -18 -4 0 90.09 8.30 18 -4 0 93.69 6.30 18 4 0 96.79 8.90 -18 4 0 89.09 6.80 -18 4 0 98.29 6.30 18 4 0 88.09 5.80 18 4 0 86.49 6.80 -18 4 0 78.99 8.00 -18 4 0 111.19 14.50 18 4 0 96.09 6.00 18 4 0 85.49 6.60 18 4 0 103.79 5.80 18 4 0 95.69 9.80 18 4 0 93.29 6.50 -18 4 0 73.39 8.70 -18 4 0 90.59 8.70 -20 -4 0 24.90 3.40 20 -4 0 28.70 3.30 -20 -4 0 24.70 6.50 -20 -4 0 20.50 4.60 -20 -4 0 29.10 4.10 20 -4 0 25.70 2.40 20 -4 0 24.80 5.10 -20 4 0 20.10 3.80 20 4 0 24.00 5.90 20 4 0 23.20 2.40 -20 4 0 17.60 6.90 -20 4 0 16.70 5.70 20 4 0 24.20 2.40 20 4 0 20.30 2.90 20 4 0 19.20 3.20 20 4 0 22.40 3.30 -20 4 0 17.10 3.10 20 4 0 22.40 3.50 20 4 0 29.80 5.40 -20 4 0 20.50 5.30 -22 -4 0 25.00 6.60 22 -4 0 27.90 6.00 -22 -4 0 32.00 4.50 22 -4 0 31.20 2.70 -22 -4 0 28.20 3.90 -22 -4 0 29.30 5.60 22 -4 0 38.10 3.80 22 4 0 25.60 5.50 22 4 0 22.40 2.50 22 4 0 31.60 4.30 -22 4 0 24.20 6.30 22 4 0 25.30 2.60 22 4 0 23.40 3.50 -22 4 0 29.60 4.80 22 4 0 27.50 7.30 -22 4 0 27.50 4.00 22 4 0 31.60 4.00 22 4 0 29.60 3.50 24 -4 0 9.80 2.30 24 -4 0 14.80 2.20 -24 -4 0 14.60 3.70 24 -4 0 11.20 4.80 -24 -4 0 10.20 5.40 -24 -4 0 15.20 3.10 24 4 0 12.00 1.80 -24 4 0 9.40 5.10 24 4 0 7.70 2.20 24 4 0 -5.90 5.80 24 4 0 13.90 3.20 24 4 0 9.50 2.40 -24 4 0 11.90 3.60 24 4 0 15.50 5.30 24 4 0 11.20 2.50 -24 4 0 12.30 3.00 24 4 0 8.70 1.60 26 -4 0 24.70 6.50 -26 -4 0 30.60 5.30 -26 -4 0 20.50 4.10 26 -4 0 21.30 2.60 -26 -4 0 27.00 7.30 26 -4 0 22.30 3.20 26 4 0 23.10 3.30 -26 4 0 25.20 7.90 26 4 0 23.40 3.80 -26 4 0 13.20 4.20 26 4 0 22.40 6.70 -26 4 0 22.60 4.10 28 -4 0 20.00 6.70 -28 -4 0 13.40 7.60 -28 -4 0 20.20 4.70 -28 -4 0 31.30 4.90 -28 4 0 19.20 5.10 28 4 0 28.00 4.00 -28 4 0 26.90 8.60 28 4 0 28.80 3.40 -28 4 0 19.80 4.30 1 -5 0 205.58 11.20 1 -5 0 206.48 12.60 1 -5 0 201.78 11.30 1 -5 0 203.28 11.20 -1 -5 0 189.18 10.90 -1 -5 0 179.98 11.20 -1 -5 0 170.38 11.00 -1 -5 0 195.58 12.10 1 5 0 210.78 10.60 1 5 0 186.18 11.10 1 5 0 201.48 12.50 -1 5 0 185.88 11.60 1 5 0 192.68 10.90 1 5 0 202.28 11.70 -1 5 0 198.98 13.00 -1 5 0 196.78 11.40 1 5 0 185.28 11.60 -3 -5 0 120.89 7.30 3 -5 0 98.39 8.00 -3 -5 0 105.39 6.80 3 -5 0 101.19 6.50 -3 -5 0 105.09 7.10 -3 -5 0 98.79 6.10 3 -5 0 109.69 7.10 3 -5 0 106.19 6.70 3 5 0 95.49 7.00 -3 5 0 104.29 7.10 -3 5 0 97.09 6.90 3 5 0 99.59 6.40 3 5 0 106.89 6.30 -3 5 0 87.69 5.90 3 5 0 96.79 5.90 3 5 0 94.39 7.20 3 5 0 100.69 6.30 -3 5 0 98.39 8.50 -5 -5 0 33.00 2.50 5 -5 0 34.30 5.30 -5 -5 0 34.30 3.30 5 -5 0 29.00 3.10 5 -5 0 32.10 3.60 -5 -5 0 31.30 3.60 5 -5 0 30.10 3.20 -5 -5 0 35.40 3.40 -5 5 0 32.50 3.80 5 5 0 34.00 2.70 5 5 0 30.30 2.50 5 5 0 34.60 3.20 -5 5 0 30.10 3.00 -5 5 0 30.70 2.10 -5 5 0 27.30 5.10 -5 5 0 33.80 3.70 5 5 0 36.80 3.50 5 5 0 28.50 2.80 -5 5 0 32.40 2.30 7 -5 0 212.48 12.50 7 -5 0 213.98 13.00 -7 -5 0 208.18 12.50 -7 -5 0 199.08 10.80 -7 -5 0 195.78 13.10 7 -5 0 217.38 14.60 -7 -5 0 210.28 11.20 -7 -5 0 211.78 12.10 -7 -5 0 204.18 11.00 7 -5 0 213.38 12.30 -7 5 0 204.28 11.00 -7 5 0 194.98 15.00 -7 5 0 211.28 13.00 7 5 0 236.38 12.30 7 5 0 196.38 11.30 -7 5 0 206.48 11.20 -7 5 0 197.98 11.70 7 5 0 196.68 11.70 -7 5 0 190.88 12.90 7 5 0 218.78 13.50 7 5 0 210.68 11.20 -9 -5 0 204.28 10.90 9 -5 0 211.38 11.00 9 -5 0 204.28 13.20 9 -5 0 210.88 15.00 9 -5 0 219.88 11.30 -9 -5 0 211.58 11.20 9 -5 0 200.88 12.70 -9 -5 0 201.68 11.10 -9 -5 0 187.88 11.90 9 -5 0 224.38 12.80 -9 -5 0 179.38 12.60 -9 -5 0 210.28 13.70 -9 5 0 220.58 13.40 9 5 0 210.08 13.90 9 5 0 209.58 12.00 9 5 0 220.78 12.00 9 5 0 208.88 11.20 -9 5 0 217.58 11.20 9 5 0 201.88 11.40 -9 5 0 200.88 15.70 -9 5 0 214.78 11.50 -9 5 0 198.48 11.90 -9 5 0 182.88 13.30 11 -5 0 189.28 12.30 11 -5 0 181.98 14.40 11 -5 0 204.28 10.80 11 -5 0 198.68 12.40 -11 -5 0 191.88 10.50 11 -5 0 212.88 13.40 -11 -5 0 206.58 12.70 -11 -5 0 198.08 13.70 -11 -5 0 190.78 10.80 11 -5 0 197.58 10.40 -11 5 0 180.48 15.60 -11 5 0 192.98 13.50 11 5 0 217.18 12.70 -11 5 0 189.58 10.70 -11 5 0 190.88 11.10 11 5 0 168.18 13.30 -11 5 0 182.78 12.90 11 5 0 185.08 11.20 11 5 0 204.88 11.30 -11 5 0 191.18 11.70 11 5 0 208.08 10.50 11 5 0 175.48 11.80 13 -5 0 164.78 9.10 13 -5 0 179.48 13.80 -13 -5 0 171.68 9.40 -13 -5 0 160.98 11.20 13 -5 0 157.38 8.80 -13 -5 0 178.98 12.60 -13 -5 0 156.18 8.90 13 -5 0 170.48 11.00 13 -5 0 152.78 11.00 -13 5 0 159.78 9.60 13 5 0 159.88 12.40 -13 5 0 147.99 14.10 13 5 0 144.79 9.80 -13 5 0 173.28 11.80 -13 5 0 153.18 9.10 -13 5 0 152.68 10.20 13 5 0 159.18 9.80 13 5 0 156.88 9.20 13 5 0 159.28 9.40 13 5 0 161.58 11.10 13 5 0 163.18 8.70 13 5 0 151.58 8.90 15 -5 0 30.10 5.40 15 -5 0 33.60 4.20 -15 -5 0 30.00 4.80 15 -5 0 24.50 4.00 -15 -5 0 20.80 2.60 -15 -5 0 21.50 3.00 15 -5 0 26.60 4.50 15 -5 0 34.30 6.90 -15 -5 0 21.90 5.20 -15 5 0 31.40 7.70 15 5 0 19.50 2.00 15 5 0 26.20 3.60 -15 5 0 22.10 4.60 15 5 0 21.40 2.90 15 5 0 24.10 2.80 15 5 0 24.80 3.00 15 5 0 23.30 5.20 -15 5 0 22.50 3.60 -15 5 0 24.20 3.50 -15 5 0 28.30 5.50 15 5 0 21.60 4.30 -15 5 0 22.90 2.90 15 5 0 25.20 2.00 17 -5 0 15.60 3.70 -17 -5 0 20.30 3.20 17 -5 0 19.60 5.40 17 -5 0 21.10 2.30 -17 -5 0 30.80 6.30 -17 -5 0 19.20 2.70 -17 -5 0 22.70 4.60 17 -5 0 18.30 4.20 17 -5 0 16.50 4.80 17 -5 0 20.70 2.70 17 5 0 20.00 2.50 -17 5 0 17.80 3.30 -17 5 0 13.50 2.60 17 5 0 27.00 5.80 17 5 0 17.20 1.70 17 5 0 17.30 2.50 -17 5 0 20.40 7.20 -17 5 0 20.70 5.50 17 5 0 15.10 2.70 17 5 0 18.60 1.80 -17 5 0 11.20 4.00 17 5 0 22.40 3.40 17 5 0 16.10 4.00 -19 -5 0 13.30 4.40 -19 -5 0 21.40 3.10 -19 -5 0 32.70 4.10 19 -5 0 24.50 2.40 -19 -5 0 13.00 4.10 19 -5 0 18.20 4.70 19 -5 0 24.50 3.10 19 5 0 25.20 3.80 -19 5 0 25.80 5.40 19 5 0 20.50 1.90 19 5 0 23.90 1.90 -19 5 0 23.70 3.90 -19 5 0 24.70 7.60 -19 5 0 28.20 6.30 19 5 0 25.20 3.10 19 5 0 21.90 2.50 -19 5 0 27.00 3.50 19 5 0 28.70 6.20 19 5 0 25.10 2.40 19 5 0 27.60 5.20 21 -5 0 38.30 3.60 21 -5 0 44.10 6.80 -21 -5 0 48.00 8.50 -21 -5 0 42.70 6.80 -21 -5 0 41.70 4.00 21 -5 0 37.60 3.20 -21 -5 0 48.50 5.50 21 5 0 47.00 5.20 -21 5 0 31.30 7.50 21 5 0 36.60 3.30 21 5 0 30.60 7.80 -21 5 0 37.90 4.00 21 5 0 35.70 3.70 -21 5 0 29.00 6.20 -21 5 0 34.10 5.10 -21 5 0 36.30 9.10 21 5 0 33.70 6.30 -23 -5 0 27.20 5.00 -23 -5 0 20.30 6.10 23 -5 0 27.40 3.00 23 -5 0 27.60 6.20 23 -5 0 31.60 3.60 -23 -5 0 20.40 4.10 23 5 0 27.30 4.30 23 5 0 22.90 5.50 -23 5 0 36.00 5.40 23 5 0 16.60 3.00 23 5 0 14.50 6.90 -23 5 0 24.00 4.00 -23 5 0 14.60 6.10 -25 -5 0 5.40 5.90 -25 -5 0 4.40 2.80 25 -5 0 -3.60 3.20 25 -5 0 8.70 1.90 25 -5 0 3.60 1.90 -25 -5 0 4.50 3.10 25 5 0 -3.90 3.30 25 5 0 5.20 2.80 25 5 0 6.40 2.40 25 5 0 -2.00 9.40 -25 5 0 2.50 2.60 -25 5 0 7.90 3.50 -25 5 0 4.00 4.70 27 -5 0 3.70 4.70 -27 -5 0 2.90 3.10 -27 -5 0 10.60 6.90 27 -5 0 6.30 2.20 -27 -5 0 2.10 2.80 27 -5 0 7.40 1.80 27 5 0 5.20 2.30 -27 5 0 2.90 3.40 -27 5 0 6.60 3.20 27 5 0 -1.00 2.20 -27 5 0 5.00 5.60 27 5 0 1.50 5.70 0 -6 0 215.08 13.00 0 -6 0 206.68 11.50 0 -6 0 190.88 11.20 0 -6 0 167.78 11.30 0 6 0 188.48 11.90 0 6 0 198.68 13.40 0 6 0 207.38 11.70 0 6 0 191.98 12.00 -2 -6 0 76.09 6.60 2 -6 0 80.09 5.90 -2 -6 0 89.59 5.60 -2 -6 0 85.89 6.10 2 -6 0 85.99 6.00 -2 -6 0 86.79 6.00 2 -6 0 82.59 7.30 2 6 0 87.29 5.30 -2 6 0 86.49 6.50 2 6 0 92.49 7.40 2 6 0 80.29 6.40 -2 6 0 83.79 7.90 -2 6 0 82.69 6.30 2 6 0 85.49 5.90 2 6 0 87.99 6.60 2 6 0 83.59 5.70 -4 -6 0 56.49 5.20 -4 -6 0 51.79 4.00 4 -6 0 67.99 7.70 -4 -6 0 61.29 4.90 -4 -6 0 53.59 4.90 4 -6 0 64.49 5.20 4 -6 0 53.29 4.70 4 6 0 63.69 4.60 4 6 0 60.39 4.40 4 6 0 58.39 4.50 -4 6 0 59.49 5.20 4 6 0 59.99 4.00 -4 6 0 71.79 8.50 4 6 0 51.49 5.30 4 6 0 51.19 5.10 -6 -6 0 30.40 2.10 -6 -6 0 36.90 3.90 -6 -6 0 29.70 2.00 -6 -6 0 39.40 4.30 6 -6 0 34.70 4.50 6 -6 0 39.70 6.30 6 -6 0 34.00 3.70 -6 -6 0 29.60 3.90 6 -6 0 39.50 3.80 -6 -6 0 35.70 2.80 6 6 0 29.50 3.70 6 6 0 33.40 2.90 -6 6 0 29.70 4.20 6 6 0 35.50 4.50 -6 6 0 27.70 5.70 6 6 0 37.80 3.00 -6 6 0 35.70 4.80 -6 6 0 34.60 3.00 6 6 0 36.00 3.60 8 -6 0 149.69 11.40 -8 -6 0 118.69 7.00 8 -6 0 117.69 9.00 -8 -6 0 122.69 6.90 -8 -6 0 130.59 7.40 -8 -6 0 133.99 9.60 8 -6 0 131.79 8.80 8 -6 0 109.49 8.40 -8 -6 0 142.09 9.10 -8 -6 0 114.89 8.20 -8 6 0 120.09 9.40 8 6 0 127.49 9.90 -8 6 0 116.39 9.20 -8 6 0 134.19 7.10 8 6 0 132.59 8.70 -8 6 0 136.39 7.50 8 6 0 124.29 7.40 8 6 0 125.99 7.60 8 6 0 123.19 8.50 8 6 0 136.89 8.20 -8 6 0 131.79 7.90 -8 6 0 128.99 11.90 -10 -6 0 56.79 3.90 -10 -6 0 60.49 3.70 10 -6 0 72.39 9.30 -10 -6 0 51.89 5.40 -10 -6 0 59.29 4.80 10 -6 0 62.19 5.40 -10 -6 0 65.69 6.60 10 -6 0 63.49 5.60 -10 -6 0 57.99 3.90 10 -6 0 53.99 5.70 10 6 0 59.99 6.60 10 6 0 60.69 4.80 -10 6 0 65.09 6.70 -10 6 0 58.39 4.70 -10 6 0 67.59 10.40 -10 6 0 59.09 6.10 10 6 0 59.19 3.90 10 6 0 53.89 4.70 -10 6 0 53.49 4.20 -10 6 0 55.69 3.90 10 6 0 62.49 4.30 12 -6 0 4.10 2.20 12 -6 0 4.50 1.30 12 -6 0 3.40 2.40 -12 -6 0 3.50 2.20 12 -6 0 3.00 1.40 -12 -6 0 5.30 2.60 -12 -6 0 2.70 1.40 -12 -6 0 2.30 1.10 12 -6 0 5.20 2.40 12 -6 0 3.10 3.20 12 6 0 5.60 2.00 12 6 0 0.70 2.70 12 6 0 4.20 1.30 12 6 0 3.80 1.60 -12 6 0 2.60 1.40 -12 6 0 3.90 2.60 -12 6 0 5.00 2.00 -12 6 0 -0.90 3.20 12 6 0 2.10 1.60 -12 6 0 4.30 2.60 -12 6 0 5.50 1.50 12 6 0 2.30 0.90 14 -6 0 2.00 1.60 14 -6 0 0.50 1.10 14 -6 0 -0.10 2.20 -14 -6 0 0.50 2.10 14 -6 0 0.30 3.10 14 -6 0 -0.10 1.90 -14 -6 0 0.30 1.40 -14 -6 0 -0.90 1.00 -14 -6 0 1.90 2.70 -14 6 0 -5.10 2.60 14 6 0 0.40 1.80 14 6 0 2.10 1.70 -14 6 0 -1.90 2.10 -14 6 0 -1.20 1.30 14 6 0 0.20 0.90 14 6 0 1.60 0.70 -14 6 0 -0.80 1.50 -14 6 0 0.90 2.40 -14 6 0 0.30 1.30 14 6 0 1.30 1.10 14 6 0 0.40 1.80 14 6 0 0.80 2.30 14 6 0 0.40 0.70 -16 -6 0 -1.50 2.60 -16 -6 0 3.20 2.60 -16 -6 0 1.30 1.40 16 -6 0 1.40 3.00 -16 -6 0 3.80 1.80 16 -6 0 0.50 1.20 16 -6 0 0.30 1.40 16 -6 0 1.40 2.60 -16 6 0 2.30 3.10 -16 6 0 0.70 3.90 16 6 0 1.20 1.60 16 6 0 0.60 0.60 -16 6 0 -1.00 2.30 16 6 0 0.40 0.50 -16 6 0 0.70 1.50 16 6 0 0.30 0.40 16 6 0 1.90 2.50 -16 6 0 0.30 1.70 16 6 0 0.30 0.70 16 6 0 0.60 2.80 16 6 0 -1.00 1.60 18 -6 0 4.70 1.60 -18 -6 0 6.60 1.90 18 -6 0 5.90 1.90 18 -6 0 2.90 3.10 -18 -6 0 3.30 3.00 -18 -6 0 8.00 2.50 -18 -6 0 0.90 3.70 18 6 0 0.00 3.60 -18 6 0 6.70 2.20 18 6 0 8.60 3.20 -18 6 0 4.60 3.70 -18 6 0 2.70 3.40 18 6 0 7.70 2.70 -18 6 0 1.90 4.30 18 6 0 3.70 1.90 -18 6 0 6.70 2.70 -20 -6 0 20.40 3.70 -20 -6 0 27.00 3.60 20 -6 0 26.60 5.40 20 -6 0 19.50 3.00 -20 -6 0 23.90 5.20 20 -6 0 28.50 3.00 -20 -6 0 20.60 5.80 20 6 0 19.60 5.80 20 6 0 25.00 4.00 -20 6 0 25.40 8.20 -20 6 0 27.50 4.50 -20 6 0 22.50 5.70 20 6 0 37.20 6.00 -20 6 0 24.30 3.60 -20 6 0 25.90 6.10 20 6 0 24.20 3.40 -22 -6 0 2.50 2.40 -22 -6 0 2.70 2.20 22 -6 0 2.90 1.80 22 -6 0 -1.30 1.40 -22 -6 0 1.70 4.20 22 6 0 -0.90 2.00 -22 6 0 3.40 4.60 -22 6 0 -5.60 2.70 -22 6 0 0.10 4.70 -22 6 0 2.00 2.70 -22 6 0 -1.50 1.90 22 6 0 0.20 5.80 22 6 0 -4.80 3.00 22 6 0 -0.50 1.90 24 -6 0 11.50 2.70 24 -6 0 14.50 2.40 -24 -6 0 15.30 3.40 -24 -6 0 13.70 3.80 24 -6 0 12.40 4.70 -24 -6 0 11.40 5.80 24 6 0 13.40 2.90 24 6 0 7.40 3.20 -24 6 0 6.00 3.30 -24 6 0 12.70 3.20 -24 6 0 7.70 5.30 24 6 0 10.50 8.10 -26 -6 0 -3.20 5.40 26 -6 0 0.60 1.90 26 -6 0 -2.00 4.20 26 -6 0 1.00 1.50 -26 -6 0 -1.60 2.50 -26 -6 0 6.80 3.10 26 6 0 0.80 2.40 26 6 0 2.10 2.90 -26 6 0 1.90 2.70 -26 6 0 -1.10 3.00 26 6 0 -4.80 4.70 -26 6 0 8.20 5.40 1 -7 0 25.80 3.40 -1 -7 0 19.70 3.00 1 -7 0 15.80 2.70 -1 -7 0 18.70 2.70 1 -7 0 13.00 3.50 -1 -7 0 21.70 3.20 -1 -7 0 18.60 4.30 1 -7 0 24.00 3.20 -1 7 0 18.90 4.60 -1 7 0 19.60 3.50 1 7 0 15.70 3.20 1 7 0 16.80 4.10 1 7 0 23.50 2.60 -1 7 0 21.80 3.60 1 7 0 18.30 3.00 1 7 0 21.40 3.60 -1 7 0 16.80 3.20 1 7 0 20.60 3.10 3 -7 0 6.80 2.80 -3 -7 0 8.40 2.60 -3 -7 0 7.00 2.00 3 -7 0 10.90 2.30 3 -7 0 6.00 2.00 -3 -7 0 8.10 2.20 -3 -7 0 10.10 1.90 -3 7 0 4.60 1.90 -3 7 0 8.10 3.70 3 7 0 7.60 2.90 -3 7 0 7.70 2.50 3 7 0 5.70 2.50 3 7 0 10.30 2.80 3 7 0 9.20 2.40 3 7 0 7.40 1.90 3 7 0 5.40 1.90 -5 -7 0 -0.80 1.50 -5 -7 0 2.20 1.20 -5 -7 0 0.80 1.90 5 -7 0 5.80 1.90 -5 -7 0 1.30 1.50 5 -7 0 1.70 1.80 5 -7 0 2.10 2.00 5 -7 0 2.80 1.60 -5 7 0 0.90 0.70 -5 7 0 1.40 2.90 5 7 0 3.30 1.50 5 7 0 0.90 2.10 5 7 0 3.50 1.60 -5 7 0 3.70 2.30 -5 7 0 1.70 1.90 -5 7 0 2.00 0.70 5 7 0 7.00 2.70 5 7 0 1.90 1.70 -7 -7 0 16.30 3.20 -7 -7 0 15.60 3.10 -7 -7 0 14.30 1.40 7 -7 0 12.50 4.10 -7 -7 0 16.10 3.60 7 -7 0 14.80 3.00 -7 -7 0 21.40 2.40 -7 -7 0 15.80 1.30 7 -7 0 22.50 3.70 7 -7 0 14.50 2.90 7 7 0 18.30 3.00 7 7 0 19.00 2.50 -7 7 0 20.60 2.20 -7 7 0 15.00 1.60 -7 7 0 19.50 5.50 -7 7 0 12.90 3.30 -7 7 0 19.40 2.20 7 7 0 18.80 3.50 7 7 0 19.60 3.20 7 7 0 20.60 2.80 -7 7 0 11.60 3.00 9 -7 0 25.90 3.90 -9 -7 0 22.10 3.50 9 -7 0 29.80 6.10 -9 -7 0 22.60 1.90 -9 -7 0 29.00 2.50 -9 -7 0 24.10 4.10 9 -7 0 27.70 4.30 9 -7 0 25.70 2.30 9 -7 0 35.50 4.70 9 -7 0 26.10 3.10 -9 -7 0 22.40 2.10 -9 -7 0 21.80 4.30 -9 7 0 21.40 4.50 9 7 0 24.80 3.70 -9 7 0 21.30 2.10 -9 7 0 26.40 4.70 9 7 0 25.80 5.70 -9 7 0 28.80 2.90 -9 7 0 27.30 2.90 -9 7 0 24.30 6.60 9 7 0 32.50 4.10 9 7 0 28.80 3.40 9 7 0 25.80 3.90 9 7 0 25.80 2.70 -11 -7 0 2.40 1.20 11 -7 0 5.00 1.70 -11 -7 0 -2.00 2.20 -11 -7 0 3.60 1.60 11 -7 0 1.80 2.00 -11 -7 0 0.40 1.90 11 -7 0 6.00 3.40 -11 -7 0 2.80 1.00 11 -7 0 5.20 1.40 -11 -7 0 3.20 1.10 11 7 0 4.30 1.90 -11 7 0 -0.40 3.60 11 7 0 1.90 2.80 11 7 0 4.80 2.20 -11 7 0 4.40 1.70 11 7 0 5.40 2.30 -11 7 0 3.60 1.40 -11 7 0 0.80 2.50 -11 7 0 2.80 2.50 11 7 0 2.60 1.60 11 7 0 2.20 1.10 13 -7 0 7.90 3.10 13 -7 0 14.30 2.40 -13 -7 0 13.40 2.30 13 -7 0 8.70 1.80 13 -7 0 18.60 5.70 -13 -7 0 10.30 3.30 -13 -7 0 14.30 4.10 13 -7 0 12.50 3.40 13 -7 0 9.30 3.50 -13 -7 0 17.30 2.10 13 7 0 10.70 1.50 -13 7 0 9.80 4.60 13 7 0 7.90 3.80 -13 7 0 9.20 3.60 -13 7 0 8.20 1.80 13 7 0 12.90 2.90 -13 7 0 6.30 3.30 13 7 0 10.00 2.10 -13 7 0 13.20 2.50 13 7 0 12.60 2.50 -13 7 0 8.70 2.10 -15 -7 0 4.30 1.50 15 -7 0 3.70 3.00 15 -7 0 6.70 1.70 -15 -7 0 1.00 2.80 -15 -7 0 7.00 2.10 15 -7 0 6.00 2.00 -15 -7 0 7.00 3.00 15 7 0 5.90 2.20 -15 7 0 10.10 2.70 15 7 0 1.40 1.40 -15 7 0 3.20 3.30 15 7 0 4.70 0.70 15 7 0 4.00 0.90 15 7 0 7.20 2.60 -15 7 0 10.80 3.80 -15 7 0 -0.60 3.70 -15 7 0 1.40 1.60 15 7 0 6.40 3.70 -17 -7 0 3.30 1.90 17 -7 0 0.80 1.40 -17 -7 0 1.30 2.90 -17 -7 0 1.10 1.50 -17 -7 0 1.00 3.70 17 -7 0 -0.30 2.80 17 -7 0 -0.80 1.50 -17 7 0 -0.70 1.80 17 7 0 1.10 1.80 -17 7 0 0.70 3.80 17 7 0 -0.40 1.90 -17 7 0 2.90 1.80 17 7 0 4.50 2.60 -17 7 0 2.90 3.40 17 7 0 -1.40 3.50 -17 7 0 0.10 2.80 -19 -7 0 0.80 1.80 -19 -7 0 1.60 1.90 19 -7 0 1.60 1.60 19 -7 0 1.90 2.80 -19 -7 0 -3.00 2.60 -19 -7 0 -0.90 2.70 19 -7 0 1.10 1.70 19 7 0 0.90 3.90 -19 7 0 0.80 2.40 19 7 0 4.40 2.20 -19 7 0 0.60 1.80 -19 7 0 -0.10 4.10 19 7 0 -1.10 2.50 19 7 0 0.10 2.20 -21 -7 0 -0.20 1.90 21 -7 0 -0.80 3.10 21 -7 0 0.10 1.70 -21 -7 0 0.70 4.40 -21 -7 0 2.90 2.20 -21 -7 0 1.80 3.80 21 -7 0 0.00 1.50 -21 7 0 -0.10 2.10 21 7 0 1.10 2.10 21 7 0 -2.00 3.00 -21 7 0 4.20 5.20 21 7 0 -0.80 2.20 21 7 0 -4.20 5.10 -21 7 0 3.70 2.90 -21 7 0 4.50 3.20 -21 7 0 -3.20 3.30 23 -7 0 24.70 3.10 23 -7 0 25.20 3.60 23 -7 0 22.80 6.00 -23 -7 0 17.90 4.00 -23 -7 0 9.50 7.10 -23 -7 0 25.60 3.90 -23 7 0 20.90 6.60 -23 7 0 27.00 4.20 -23 7 0 19.50 4.50 23 7 0 15.60 8.70 -25 -7 0 27.20 8.30 -25 -7 0 26.90 4.40 25 -7 0 40.60 4.40 25 -7 0 32.40 3.50 25 -7 0 33.70 7.00 -25 -7 0 26.80 4.90 -25 7 0 30.90 7.70 25 7 0 27.70 4.90 -25 7 0 26.00 5.20 -25 7 0 23.60 4.40 25 7 0 26.10 4.10 0 -8 0 89.79 7.00 0 -8 0 101.89 8.60 0 -8 0 107.39 7.40 0 -8 0 95.49 6.70 0 8 0 95.09 7.80 0 8 0 84.99 7.50 0 8 0 85.09 7.20 0 8 0 92.39 10.70 -2 -8 0 65.29 5.50 -2 -8 0 60.19 7.20 2 -8 0 62.69 8.10 2 -8 0 69.19 5.60 -2 -8 0 70.89 5.80 2 -8 0 56.89 5.10 -2 -8 0 61.79 5.00 2 -8 0 60.69 5.50 2 8 0 67.99 5.70 2 8 0 64.19 6.30 -2 8 0 64.99 9.20 -2 8 0 69.69 6.30 2 8 0 74.39 9.00 -2 8 0 53.79 5.70 2 8 0 50.49 6.00 -2 8 0 57.79 5.80 4 -8 0 60.59 5.40 4 -8 0 76.79 9.20 -4 -8 0 59.99 5.60 4 -8 0 55.89 5.40 -4 -8 0 53.89 5.40 -4 8 0 42.20 7.70 4 8 0 58.99 6.10 4 8 0 64.79 5.30 4 8 0 66.49 5.20 4 8 0 56.99 7.40 4 8 0 59.69 6.20 4 8 0 59.99 4.60 -4 8 0 66.89 6.20 -4 8 0 67.39 6.30 -6 -8 0 30.10 4.30 6 -8 0 33.60 6.50 -6 -8 0 44.30 4.70 6 -8 0 35.70 4.20 -6 -8 0 38.00 5.20 6 -8 0 27.80 4.50 -6 -8 0 28.00 3.00 6 -8 0 29.60 4.40 -6 8 0 23.50 2.20 6 8 0 38.10 5.40 -6 8 0 22.90 4.50 6 8 0 29.90 4.90 -6 8 0 38.00 5.50 -6 8 0 28.10 6.90 6 8 0 32.60 5.30 6 8 0 31.70 3.60 6 8 0 29.00 3.70 6 8 0 36.40 4.40 -6 8 0 29.10 2.10 8 -8 0 19.30 6.10 -8 -8 0 14.80 1.70 -8 -8 0 16.80 2.40 8 -8 0 16.30 3.80 -8 -8 0 20.10 3.70 -8 -8 0 18.10 3.70 -8 -8 0 14.20 1.30 8 -8 0 16.00 3.30 -8 8 0 13.50 3.50 8 8 0 14.70 3.50 -8 8 0 17.10 1.70 8 8 0 12.20 3.00 8 8 0 19.00 2.70 -8 8 0 12.30 2.10 -8 8 0 16.60 5.50 8 8 0 15.00 2.80 -8 8 0 21.50 4.20 8 8 0 17.80 2.90 -8 8 0 19.50 2.30 -10 -8 0 4.40 2.80 10 -8 0 -0.20 1.40 -10 -8 0 4.20 1.80 -10 -8 0 1.70 2.00 -10 -8 0 1.20 1.00 -10 -8 0 0.60 0.80 10 -8 0 2.00 1.40 10 -8 0 -3.30 1.60 10 -8 0 -0.40 1.90 10 -8 0 2.10 3.10 10 -8 0 1.40 2.10 -10 -8 0 0.30 0.90 -10 8 0 1.20 1.20 -10 8 0 -4.60 2.50 -10 8 0 6.90 3.20 10 8 0 1.40 2.10 10 8 0 3.60 2.00 -10 8 0 0.80 1.20 10 8 0 -1.70 1.30 10 8 0 0.10 1.80 -10 8 0 -0.20 2.60 -10 8 0 -1.00 0.90 10 8 0 0.10 1.00 -12 -8 0 10.10 3.60 -12 -8 0 10.90 2.00 12 -8 0 6.10 2.80 -12 -8 0 9.40 1.50 -12 -8 0 13.90 3.60 12 -8 0 9.40 2.30 12 -8 0 15.50 2.20 -12 8 0 10.50 4.30 12 8 0 11.50 1.90 -12 8 0 11.30 2.00 12 8 0 7.00 3.30 12 8 0 10.70 2.50 12 8 0 10.40 2.50 -12 8 0 8.80 2.20 -12 8 0 9.40 3.60 -12 8 0 6.60 4.80 12 8 0 7.30 2.80 12 8 0 14.10 3.30 -14 -8 0 69.99 4.70 -14 -8 0 72.89 8.20 14 -8 0 72.89 5.30 14 -8 0 69.19 4.80 -14 -8 0 64.99 7.20 14 -8 0 87.59 7.80 -14 -8 0 68.39 5.00 14 8 0 61.89 5.90 14 8 0 69.09 8.40 -14 8 0 79.59 5.20 14 8 0 69.59 4.90 -14 8 0 79.39 8.70 14 8 0 65.79 6.70 -14 8 0 66.39 5.40 -14 8 0 81.79 8.50 -14 8 0 54.69 11.00 14 8 0 68.59 4.30 14 8 0 73.89 5.50 -16 -8 0 21.20 3.20 -16 -8 0 20.70 5.50 -16 -8 0 22.10 2.90 16 -8 0 28.10 3.60 -16 -8 0 19.70 4.80 16 -8 0 27.60 5.20 16 -8 0 31.60 3.20 -16 8 0 17.30 7.10 16 8 0 24.90 4.40 16 8 0 23.20 6.10 -16 8 0 18.30 5.40 -16 8 0 14.70 4.70 16 8 0 21.10 3.50 16 8 0 24.20 4.20 -16 8 0 23.40 3.30 -16 8 0 18.50 3.40 18 -8 0 14.40 2.50 -18 -8 0 17.50 2.80 -18 -8 0 17.10 3.30 -18 -8 0 18.30 4.80 -18 -8 0 9.10 4.20 18 -8 0 14.60 2.90 -18 8 0 10.90 4.40 -18 8 0 8.70 5.90 -18 8 0 12.90 2.80 18 8 0 10.00 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12.30 3.40 -1 9 0 12.50 4.80 -1 9 0 8.00 3.10 1 9 0 10.20 4.20 -1 9 0 7.40 2.90 -3 -9 0 99.39 7.90 -3 -9 0 91.49 7.90 3 -9 0 105.59 7.80 -3 -9 0 91.49 7.00 3 -9 0 105.39 9.90 3 -9 0 104.19 8.00 3 -9 0 106.99 7.80 -3 -9 0 103.39 8.90 3 9 0 97.09 7.70 -3 9 0 95.49 8.30 3 9 0 99.09 8.70 3 9 0 114.59 10.30 3 9 0 105.09 8.70 -3 9 0 104.69 12.80 -3 9 0 105.79 8.60 -3 9 0 96.69 8.30 5 -9 0 166.18 11.60 5 -9 0 145.89 11.10 5 -9 0 164.48 12.10 5 -9 0 177.68 15.70 -5 -9 0 183.48 11.90 -5 -9 0 185.58 12.50 -5 -9 0 183.48 10.60 5 9 0 161.08 12.40 5 9 0 163.98 12.20 -5 9 0 179.78 15.70 -5 9 0 178.48 12.30 -5 9 0 173.98 12.40 5 9 0 172.08 10.30 5 9 0 170.98 11.00 7 -9 0 75.09 10.10 7 -9 0 77.49 6.70 -7 -9 0 58.39 6.40 -7 -9 0 78.89 6.90 -7 -9 0 72.59 5.70 -7 -9 0 71.09 8.40 7 -9 0 71.29 6.50 7 -9 0 63.19 6.60 7 9 0 66.59 6.00 -7 9 0 62.69 10.80 7 9 0 86.19 8.10 -7 9 0 64.19 7.30 7 9 0 68.29 5.80 -7 9 0 69.49 7.30 7 9 0 76.89 8.90 7 9 0 73.49 7.50 7 9 0 71.29 5.40 9 -9 0 5.80 2.60 -9 -9 0 6.30 1.60 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47.40 11.40 -21 9 0 39.60 7.90 -21 9 0 49.99 6.50 21 9 0 42.30 6.30 23 -9 0 20.10 5.90 -23 -9 0 22.80 4.30 23 -9 0 18.80 3.80 -23 -9 0 32.00 4.30 -23 -9 0 15.00 7.50 -23 9 0 30.90 10.60 -23 9 0 14.40 5.60 -23 9 0 27.00 7.00 23 9 0 23.50 4.90 -23 9 0 28.50 4.40 23 9 0 22.90 4.10 -23 9 0 26.30 5.20 0 -10 0 181.88 13.10 0 -10 0 193.28 12.50 0 -10 0 222.58 13.40 0 -10 0 193.88 14.90 0 10 0 205.38 13.80 0 10 0 189.48 13.90 0 10 0 190.38 16.30 0 10 0 201.78 13.60 -2 -10 0 92.69 7.10 2 -10 0 94.09 7.80 -2 -10 0 102.39 8.10 -2 -10 0 100.09 8.20 2 -10 0 105.09 8.30 -2 -10 0 88.19 8.90 2 10 0 94.59 7.80 2 10 0 77.79 8.00 2 10 0 102.89 12.30 -2 10 0 102.39 8.50 2 10 0 98.99 8.80 -2 10 0 101.09 8.50 -2 10 0 77.19 7.90 -2 10 0 82.59 12.10 4 -10 0 12.80 3.10 -4 -10 0 13.90 3.80 4 -10 0 8.30 3.00 4 -10 0 13.80 4.80 -4 -10 0 18.80 3.80 -4 -10 0 20.50 4.10 -4 -10 0 12.40 2.80 4 -10 0 13.60 3.50 -4 10 0 21.20 6.30 4 10 0 19.20 5.10 -4 10 0 10.80 3.70 4 10 0 11.80 3.80 4 10 0 15.10 3.40 4 10 0 13.10 4.00 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7.70 2.50 -12 -10 0 12.20 3.80 12 -10 0 7.00 2.20 -12 -10 0 4.30 1.20 12 10 0 7.50 3.30 12 10 0 9.10 2.80 12 10 0 5.90 2.60 12 10 0 8.90 2.80 12 10 0 9.90 1.90 -14 -10 0 7.40 3.90 14 -10 0 7.60 2.30 -14 -10 0 11.10 2.10 -14 -10 0 6.70 3.60 14 -10 0 9.00 2.70 14 -10 0 6.80 3.60 -14 -10 0 10.40 1.80 14 10 0 9.60 4.50 14 10 0 11.00 3.00 -14 10 0 11.70 2.70 14 10 0 6.30 3.30 -14 10 0 9.10 4.50 -14 10 0 15.50 4.80 -14 10 0 9.10 2.10 -14 10 0 3.50 5.30 14 10 0 7.90 1.70 14 10 0 8.90 1.40 14 10 0 17.30 4.00 -16 -10 0 22.00 2.80 -16 -10 0 28.90 6.60 16 -10 0 27.00 4.00 16 -10 0 33.50 3.80 -16 -10 0 21.90 3.20 16 -10 0 23.30 5.20 -16 10 0 31.40 4.30 -16 10 0 29.00 6.90 16 10 0 28.10 4.30 -16 10 0 15.70 8.00 16 10 0 28.30 5.00 -16 10 0 23.40 6.20 16 10 0 17.10 4.60 -16 10 0 23.70 3.30 16 10 0 16.50 6.40 -18 -10 0 5.80 5.00 18 -10 0 11.70 4.40 -18 -10 0 12.00 2.40 -18 -10 0 15.60 5.70 -18 -10 0 11.60 2.70 18 10 0 10.60 4.70 -18 10 0 8.70 2.60 18 10 0 -3.00 5.10 -18 10 0 13.30 3.40 -18 10 0 18.20 5.80 -18 10 0 6.00 4.90 18 10 0 10.90 3.30 -18 10 0 6.20 5.90 18 10 0 14.00 4.10 20 -10 0 104.09 7.90 -20 -10 0 90.09 13.40 -20 -10 0 109.29 8.00 20 -10 0 122.49 11.80 -20 -10 0 122.39 7.60 20 -10 0 120.69 7.60 -20 10 0 103.59 8.90 20 10 0 121.69 9.60 20 10 0 117.49 8.50 -20 10 0 93.49 16.80 -20 10 0 114.59 10.00 22 -10 0 34.10 7.50 22 -10 0 36.40 4.20 -22 -10 0 29.50 5.00 22 -10 0 34.00 4.60 -22 -10 0 37.20 6.10 -22 10 0 39.40 5.80 22 10 0 40.30 5.30 -22 10 0 35.20 4.90 -22 10 0 16.60 8.60 22 10 0 39.20 6.20 -22 10 0 23.70 7.40 1 -11 0 1.10 2.20 -1 -11 0 3.50 2.70 1 -11 0 6.40 2.90 -1 -11 0 6.80 2.80 -1 -11 0 8.50 3.80 -1 -11 0 4.90 2.40 1 -11 0 1.00 2.60 1 -11 0 5.60 2.90 -1 11 0 6.90 3.30 1 11 0 1.30 2.80 1 11 0 12.80 4.90 -1 11 0 5.90 4.60 1 11 0 5.20 3.60 1 11 0 6.60 3.30 -1 11 0 5.50 2.70 -1 11 0 3.30 2.80 -3 -11 0 11.40 2.80 -3 -11 0 4.60 3.30 -3 -11 0 4.70 2.90 3 -11 0 7.70 2.80 -3 -11 0 10.20 3.50 3 -11 0 13.10 3.40 3 11 0 9.60 3.50 -3 11 0 6.10 3.20 3 11 0 9.10 3.00 -3 11 0 7.80 3.50 3 11 0 9.00 3.20 3 11 0 10.50 4.70 -3 11 0 8.80 5.40 -3 11 0 9.30 3.50 5 -11 0 78.89 7.70 -5 -11 0 66.99 8.90 -5 -11 0 84.99 8.00 -5 -11 0 79.79 6.40 5 -11 0 81.19 7.60 -5 -11 0 75.39 10.90 5 11 0 78.89 7.10 -5 11 0 84.19 8.30 5 11 0 72.79 8.00 5 11 0 51.69 9.10 -5 11 0 76.29 8.00 -5 11 0 91.19 9.00 5 11 0 84.69 8.70 -5 11 0 88.39 13.30 7 -11 0 1.60 2.60 -7 -11 0 0.50 2.50 7 -11 0 5.30 2.90 -7 -11 0 5.00 3.20 -7 -11 0 6.40 3.20 -7 -11 0 3.50 2.00 7 11 0 1.40 3.10 7 11 0 7.70 3.60 7 11 0 -0.50 3.20 7 11 0 1.80 2.30 -7 11 0 1.80 3.10 -7 11 0 -0.10 2.70 -7 11 0 4.30 3.40 -7 11 0 1.00 4.50 9 -11 0 -0.60 2.30 -9 -11 0 1.90 2.30 -9 -11 0 -0.10 3.00 9 -11 0 2.50 2.60 -9 -11 0 4.00 2.70 -9 -11 0 1.50 1.80 -9 11 0 -3.60 2.50 9 11 0 1.90 2.80 9 11 0 0.70 1.90 9 11 0 -1.90 3.00 9 11 0 4.80 3.90 11 -11 0 6.40 3.30 -11 -11 0 2.80 3.20 -11 -11 0 1.20 3.10 11 11 0 0.90 1.70 -11 11 0 3.10 4.00 -11 11 0 1.00 3.10 11 11 0 -0.30 3.10 -11 11 0 2.30 4.80 11 11 0 5.10 4.30 11 11 0 5.20 3.00 -11 11 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2.70 2.80 6 -12 0 34.70 5.70 -6 -12 0 42.20 8.10 -6 -12 0 36.00 5.40 -6 -12 0 39.30 6.20 -6 -12 0 38.40 6.30 6 -12 0 42.90 6.30 -6 12 0 41.10 10.30 6 12 0 47.80 8.50 -6 12 0 45.90 7.00 6 12 0 44.00 6.00 6 12 0 54.49 7.90 -6 12 0 37.80 6.50 -6 12 0 42.00 7.20 6 12 0 48.90 7.80 -8 -12 0 16.40 4.70 -8 -12 0 28.70 5.80 -8 -12 0 19.00 3.30 -8 -12 0 22.50 5.10 8 -12 0 17.80 4.60 8 -12 0 19.20 4.60 -8 12 0 21.90 5.20 -8 12 0 31.30 6.60 8 12 0 20.10 5.80 8 12 0 31.50 6.40 -8 12 0 30.90 9.00 8 12 0 24.90 4.20 8 12 0 27.80 6.10 -8 12 0 26.10 5.50 -10 -12 0 -1.40 1.70 -10 -12 0 0.80 3.20 10 -12 0 2.50 2.40 -10 -12 0 -1.10 3.00 -10 -12 0 -2.20 1.60 10 -12 0 3.10 3.40 10 -12 0 6.10 2.90 10 -12 0 -0.70 2.80 -10 12 0 -4.30 4.30 10 12 0 -0.20 3.60 10 12 0 3.30 4.50 -10 12 0 3.60 3.30 10 12 0 1.40 2.00 -10 12 0 -2.10 3.40 -10 12 0 -2.40 2.90 10 12 0 -0.50 2.30 12 -12 0 -1.20 2.30 12 -12 0 -1.70 2.50 -12 -12 0 0.30 3.30 12 -12 0 2.20 2.20 -12 -12 0 3.30 3.50 -12 12 0 5.20 4.10 12 12 0 0.90 2.00 -12 12 0 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16.80 5.40 3 13 0 22.80 5.50 5 -13 0 112.69 9.90 -5 -13 0 121.39 10.40 -5 -13 0 91.69 9.90 5 -13 0 102.79 9.60 5 13 0 91.19 13.40 -5 13 0 83.89 14.60 5 13 0 101.49 9.40 5 13 0 96.89 10.10 -5 13 0 94.09 10.60 -7 -13 0 35.40 5.00 7 -13 0 36.20 6.30 -7 -13 0 41.70 7.30 -7 -13 0 52.19 7.40 -7 -13 0 36.80 6.20 7 -13 0 36.50 6.20 7 13 0 46.40 8.70 7 13 0 41.80 7.80 7 13 0 39.50 6.00 -7 13 0 29.10 6.70 -7 13 0 38.60 10.40 -7 13 0 33.00 6.20 9 -13 0 7.50 4.00 -9 -13 0 18.10 4.50 9 -13 0 12.40 3.70 9 -13 0 19.10 3.60 9 -13 0 18.80 4.70 -9 -13 0 18.30 5.00 -9 13 0 26.30 9.20 -9 13 0 20.50 5.00 9 13 0 17.90 3.90 9 13 0 17.30 5.30 9 13 0 12.80 5.10 -9 13 0 8.30 4.70 -9 13 0 16.10 5.90 11 -13 0 14.10 5.00 -11 -13 0 31.20 6.10 11 -13 0 24.30 3.90 11 -13 0 23.20 5.40 11 -13 0 24.30 4.40 -11 13 0 23.20 6.30 -11 13 0 22.80 9.60 11 13 0 31.20 6.60 -11 13 0 23.10 5.60 13 -13 0 6.50 3.20 13 -13 0 14.80 3.40 -13 -13 0 20.00 4.90 13 -13 0 15.10 4.50 13 13 0 18.60 5.60 -13 13 0 12.30 4.60 -13 13 0 1.50 6.20 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35.90 10.40 21 -3 -4 45.00 7.80 -21 -3 4 32.40 3.30 -21 -3 4 29.70 4.20 21 -3 -4 29.00 5.80 -21 -3 4 23.40 5.10 21 -3 -4 28.30 2.90 -21 3 4 30.60 3.70 -21 3 4 21.90 6.70 -21 3 4 27.40 4.90 21 3 -4 28.60 5.00 21 3 -4 33.30 4.40 -21 3 4 28.70 5.70 21 3 -4 25.70 3.40 21 3 -4 24.10 6.70 -21 3 4 20.50 5.90 -21 3 4 23.40 3.90 19 -3 -4 17.50 4.90 19 -3 -4 16.60 4.80 19 -3 -4 17.30 4.60 19 -3 -4 16.70 2.80 19 -3 -4 18.00 2.50 -19 -3 4 21.60 3.30 -19 -3 4 21.90 2.80 19 -3 -4 16.30 3.30 -19 -3 4 13.00 4.60 -19 3 4 15.60 5.50 19 3 -4 15.50 3.10 -19 3 4 18.50 4.50 -19 3 4 17.30 5.00 -19 3 4 23.70 3.00 19 3 -4 23.10 5.40 19 3 -4 13.20 3.60 -19 3 4 17.80 4.00 -19 3 4 16.00 3.00 19 3 -4 16.50 2.70 -17 -3 4 8.00 2.20 17 -3 -4 11.20 3.60 -17 -3 4 3.80 3.10 17 -3 -4 7.80 3.20 17 -3 -4 8.80 1.80 17 -3 -4 4.80 3.10 -17 -3 4 5.20 2.70 -17 -3 4 11.60 2.00 17 -3 -4 5.80 2.20 17 -3 -4 4.70 1.90 17 3 -4 5.10 2.70 17 3 -4 9.10 2.10 -17 3 4 7.00 2.10 17 3 -4 13.00 4.20 -17 3 4 7.00 2.80 -17 3 4 13.60 4.40 17 3 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4 17.00 2.70 -1 3 -4 21.40 2.20 1 3 4 24.20 2.30 1 3 4 18.30 2.50 1 3 4 22.50 3.40 -1 3 -4 20.60 1.50 -3 -3 -4 24.50 2.40 -3 -3 -4 26.90 3.00 -3 -3 -4 26.00 1.90 3 -3 4 24.60 3.20 3 -3 4 24.60 4.30 -3 -3 -4 31.80 3.30 -3 -3 -4 24.90 3.00 -3 -3 -4 25.00 1.80 3 -3 4 26.60 2.30 3 -3 4 24.50 1.90 -3 -3 -4 27.30 3.90 -3 3 -4 24.70 2.40 -3 3 -4 25.00 1.90 -3 3 -4 26.70 5.00 -3 3 -4 25.60 1.90 3 3 4 23.90 3.20 -3 3 -4 24.80 2.20 3 3 4 25.90 3.60 -3 3 -4 25.70 3.50 -3 3 -4 25.10 1.70 3 3 4 25.60 2.50 3 3 4 27.50 3.70 -5 -3 -4 35.20 3.50 5 -3 4 34.20 2.80 5 -3 4 31.60 3.50 -5 -3 -4 33.90 3.00 -5 -3 -4 34.40 2.80 -5 -3 -4 42.10 4.40 -5 -3 -4 33.10 2.50 5 -3 4 32.90 5.50 -5 -3 -4 40.00 4.80 5 -3 4 34.70 3.20 -5 -3 -4 35.40 3.60 -5 3 -4 33.40 2.00 5 3 4 30.10 2.80 -5 3 -4 35.40 3.30 5 3 4 37.40 3.70 -5 3 -4 36.70 4.40 -5 3 -4 28.80 5.30 5 3 4 35.90 4.60 5 3 4 30.20 4.20 -5 3 -4 29.70 2.60 -5 3 -4 31.90 2.40 -7 -3 -4 305.37 17.80 7 -3 4 328.27 16.60 -7 -3 -4 283.37 16.20 -7 -3 -4 312.17 15.90 -7 -3 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76.39 5.00 -4 4 -10 69.39 5.70 -4 4 -10 76.39 5.10 4 4 10 86.69 7.20 4 4 10 82.19 6.40 -4 4 -10 76.89 4.50 4 4 10 81.99 7.60 4 4 10 70.19 7.40 4 4 10 76.09 9.20 -4 4 -10 71.09 5.20 -4 4 -10 75.39 4.80 -6 -4 -10 102.49 9.20 6 -4 10 122.49 14.20 -6 -4 -10 92.89 7.80 -6 -4 -10 95.69 5.60 -6 -4 -10 97.59 7.50 6 -4 10 91.89 8.20 6 -4 10 96.09 6.80 6 -4 10 104.89 6.80 -6 -4 -10 84.29 7.10 -6 -4 -10 99.79 7.90 -6 -4 -10 99.39 5.90 -6 -4 -10 91.59 9.50 -6 -4 -10 90.09 6.60 -6 4 -10 108.09 6.70 -6 4 -10 97.69 7.10 -6 4 -10 99.49 6.90 -6 4 -10 100.79 5.40 6 4 10 102.89 9.10 6 4 10 91.49 7.40 -6 4 -10 95.09 5.70 6 4 10 102.69 9.70 8 -4 10 349.37 26.90 -8 -4 -10 314.57 18.60 -8 -4 -10 269.17 19.50 8 -4 10 282.67 23.60 -8 -4 -10 313.87 16.70 -8 -4 -10 301.77 15.80 -8 -4 -10 306.97 16.00 8 -4 10 285.27 17.40 -8 -4 -10 318.37 17.30 -8 -4 -10 300.67 18.60 -8 4 -10 299.87 17.70 -8 4 -10 291.07 17.80 8 4 10 301.17 20.30 8 4 10 320.77 18.20 -8 4 -10 304.27 17.00 8 4 10 298.17 20.70 8 4 10 306.67 19.20 10 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14 36.80 6.60 -7 5 14 37.20 5.60 7 5 -14 39.20 3.90 7 5 -14 42.30 3.80 -7 5 14 48.50 5.90 5 -5 -14 45.70 7.90 5 -5 -14 42.20 5.70 5 -5 -14 37.70 3.50 5 -5 -14 42.30 3.60 5 -5 -14 46.50 4.90 -5 -5 14 33.40 5.10 -5 -5 14 38.80 6.70 5 -5 -14 49.60 4.20 -5 -5 14 43.20 5.20 -5 -5 14 40.20 7.50 5 -5 -14 40.10 5.50 5 -5 -14 49.10 5.50 -5 -5 14 41.20 3.40 -5 5 14 52.29 5.40 5 5 -14 48.20 4.10 -5 5 14 32.20 6.90 5 5 -14 39.00 3.60 5 5 -14 40.30 5.20 -5 5 14 38.50 5.70 -5 5 14 49.30 7.60 5 5 -14 39.60 4.90 -5 5 14 36.30 6.40 -3 -5 14 119.09 11.40 3 -5 -14 130.19 7.70 3 -5 -14 122.39 8.40 -3 -5 14 139.59 13.00 -3 -5 14 129.09 9.30 -3 -5 14 124.29 7.80 3 -5 -14 127.99 7.90 3 -5 -14 132.89 9.60 3 -5 -14 140.29 10.10 3 -5 -14 111.09 11.70 3 -5 -14 102.39 9.50 -3 -5 14 128.89 10.00 3 -5 -14 126.99 8.20 -3 5 14 121.49 11.30 -3 5 14 143.29 11.40 -3 5 14 138.79 12.40 3 5 -14 116.49 8.80 3 5 -14 129.09 8.40 -3 5 14 130.29 9.70 3 5 -14 126.89 7.80 3 5 -14 138.69 8.50 -3 5 14 143.09 11.50 1 -5 -14 64.19 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-0.50 4.30 4 -4 -25 3.20 2.70 4 -4 -25 6.20 3.50 4 -4 -25 6.40 2.60 -4 -4 25 -5.60 3.20 4 -4 -25 5.40 3.90 4 4 -25 6.40 2.50 -4 4 25 -2.50 4.20 -4 4 25 1.50 3.90 4 4 -25 4.20 2.70 4 4 -25 4.00 3.90 4 4 -25 6.40 3.60 2 -4 -25 0.50 2.00 2 -4 -25 -1.10 3.20 2 -4 -25 0.50 2.50 -2 -4 25 -0.30 4.80 2 -4 -25 1.90 3.50 -2 4 25 3.00 4.20 2 4 -25 -0.70 3.00 2 4 -25 -2.00 3.70 2 4 -25 3.00 2.70 -2 4 25 -4.80 4.00 2 4 -25 4.60 2.40 0 -4 -25 12.70 4.90 0 4 -25 7.30 5.30 11 -5 -25 6.00 3.20 11 -5 -25 2.30 3.50 -11 -5 25 -5.40 2.70 -11 -5 25 8.60 4.70 -11 -5 25 -4.70 3.00 11 5 -25 -0.70 3.00 11 5 -25 -4.10 2.40 -11 5 25 -4.10 3.40 -11 5 25 2.70 4.90 -9 -5 25 4.30 2.80 -9 -5 25 3.20 4.10 9 -5 -25 1.40 2.80 -9 -5 25 3.20 3.40 9 -5 -25 -0.40 2.90 9 5 -25 -2.30 3.30 -9 5 25 -1.50 3.70 9 5 -25 0.30 2.60 -9 5 25 1.30 4.50 9 5 -25 -3.40 2.40 9 5 -25 -0.30 3.80 7 -5 -25 -0.60 2.40 7 -5 -25 -0.10 3.20 -7 -5 25 2.50 2.70 -7 -5 25 3.40 4.40 7 -5 -25 2.60 3.20 7 -5 -25 4.20 3.50 -7 -5 25 2.60 3.60 -7 5 25 1.90 5.30 7 5 -25 5.60 4.00 -7 5 25 -2.00 3.70 7 5 -25 2.50 2.80 7 5 -25 4.00 4.40 7 5 -25 4.50 3.50 5 -5 -25 6.00 3.80 5 -5 -25 6.30 3.40 -5 -5 25 3.10 3.80 -5 -5 25 5.90 5.30 5 -5 -25 3.80 3.50 5 -5 -25 2.30 2.70 -5 5 25 6.10 5.90 5 5 -25 3.20 4.20 -5 5 25 11.10 4.60 5 5 -25 5.40 2.60 5 5 -25 1.60 3.70 5 5 -25 8.60 3.30 3 -5 -25 2.70 3.50 3 5 -25 4.80 2.40 3 5 -25 9.00 3.10 3 5 -25 1.10 3.90 -14 0 26 15.00 4.50 14 0 -26 11.20 4.50 14 0 -26 17.50 4.20 -14 0 26 21.20 7.10 -12 0 26 14.80 4.50 12 0 -26 6.50 3.30 -12 0 26 13.60 6.30 12 0 -26 11.20 4.00 10 0 -26 38.10 5.80 10 0 -26 33.10 5.60 -10 0 26 36.00 8.80 10 0 -26 34.60 6.80 -10 0 26 46.30 7.40 10 0 -26 29.40 4.80 8 0 -26 22.20 4.50 8 0 -26 21.70 3.80 -8 0 26 10.30 4.50 8 0 -26 21.60 5.00 8 0 -26 25.80 6.10 -8 0 26 29.80 8.20 6 0 -26 14.30 3.90 6 0 -26 12.20 5.10 6 0 -26 17.50 4.90 -6 0 26 17.10 7.00 6 0 -26 14.40 3.10 -6 0 26 9.70 4.60 4 0 -26 4.00 4.40 4 0 -26 6.70 4.10 4 0 -26 10.50 2.60 4 0 -26 14.80 3.70 -2 0 26 49.50 10.90 2 0 -26 39.90 6.50 2 0 -26 34.50 7.00 15 -1 -26 -0.70 3.30 15 1 -26 3.30 3.90 13 -1 -26 16.40 4.90 -13 -1 26 13.10 4.50 -13 -1 26 12.70 5.60 13 -1 -26 23.80 4.70 13 1 -26 15.00 4.00 13 1 -26 26.60 5.50 -13 1 26 15.30 6.50 -13 1 26 20.40 5.00 -11 -1 26 5.80 5.00 -11 -1 26 8.70 4.10 11 -1 -26 17.60 4.00 11 -1 -26 23.30 5.10 -11 1 26 9.10 5.90 -11 1 26 6.70 4.40 11 1 -26 10.80 4.20 11 1 -26 14.70 5.00 11 1 -26 11.20 4.40 11 1 -26 12.50 3.60 9 -1 -26 28.70 6.50 9 -1 -26 38.10 6.10 -9 -1 26 22.20 7.10 -9 -1 26 28.90 5.90 9 -1 -26 31.80 5.60 9 -1 -26 39.70 5.20 9 1 -26 28.10 6.10 9 1 -26 25.90 5.20 9 1 -26 26.50 4.40 -9 1 26 27.90 6.20 -9 1 26 21.20 7.40 9 1 -26 27.30 5.30 -7 -1 26 23.10 7.60 -7 -1 26 33.50 6.50 7 -1 -26 33.70 5.60 7 -1 -26 41.80 6.50 7 -1 -26 32.60 4.70 7 -1 -26 44.00 7.60 7 1 -26 36.60 5.50 7 1 -26 38.80 6.00 -7 1 26 31.70 9.30 -7 1 26 26.40 5.80 7 1 -26 22.10 5.70 7 1 -26 35.30 4.70 5 -1 -26 4.20 4.00 5 -1 -26 7.90 4.00 5 -1 -26 9.20 2.90 -5 -1 26 7.40 4.60 -5 -1 26 18.60 7.80 5 -1 -26 12.50 3.60 5 1 -26 12.00 3.50 5 1 -26 9.80 2.90 5 1 -26 8.30 4.40 5 1 -26 9.10 3.80 -3 -1 26 9.40 5.50 3 -1 -26 18.80 3.10 3 -1 -26 10.60 4.60 3 -1 -26 21.10 3.70 -3 -1 26 11.00 7.70 3 -1 -26 18.30 4.80 3 1 -26 19.60 3.80 3 1 -26 19.30 3.10 -3 1 26 14.00 5.00 -3 1 26 23.90 8.10 3 1 -26 13.30 5.20 3 1 -26 15.50 4.60 1 -1 -26 17.00 5.40 1 1 -26 14.40 5.30 14 -2 -26 -1.10 3.40 14 -2 -26 0.30 3.00 14 2 -26 4.90 3.80 14 2 -26 3.60 3.20 -12 -2 26 2.30 3.40 12 -2 -26 -4.00 2.70 12 -2 -26 2.50 3.00 -12 -2 26 3.00 4.50 12 2 -26 4.00 3.60 -12 2 26 8.50 4.40 -12 2 26 6.50 5.90 12 2 -26 5.60 3.30 -10 -2 26 0.20 3.80 10 -2 -26 -1.20 3.10 -10 -2 26 -2.50 3.00 10 -2 -26 1.10 2.70 10 -2 -26 -0.60 3.00 10 2 -26 2.50 2.80 10 2 -26 0.00 2.80 10 2 -26 8.10 3.80 10 2 -26 1.80 3.80 -10 2 26 4.80 4.30 -10 2 26 -7.00 3.20 8 -2 -26 -0.60 2.40 -8 -2 26 -4.10 3.00 8 -2 -26 1.30 3.60 8 -2 -26 1.90 3.60 8 -2 -26 -1.40 2.50 -8 -2 26 0.70 3.60 8 2 -26 -2.00 3.00 8 2 -26 -0.50 2.80 8 2 -26 3.10 4.10 8 2 -26 0.40 2.50 6 -2 -26 3.80 3.00 6 -2 -26 3.10 3.60 -6 -2 26 -1.40 4.70 -6 -2 26 0.70 3.70 6 -2 -26 8.20 2.90 6 -2 -26 -0.80 3.40 -6 2 26 4.80 7.00 -6 2 26 2.30 7.10 6 2 -26 1.70 2.60 6 2 -26 2.80 3.90 6 2 -26 1.80 3.40 6 2 -26 5.60 2.50 4 -2 -26 8.10 2.80 4 -2 -26 18.80 4.70 4 -2 -26 17.40 5.00 4 -2 -26 8.60 3.20 -4 2 26 4.60 5.70 4 2 -26 2.60 4.00 4 2 -26 11.60 3.20 -4 2 26 4.30 4.20 4 2 -26 8.00 3.60 4 2 -26 13.50 2.70 2 -2 -26 3.90 3.80 -2 -2 26 13.10 6.40 2 -2 -26 0.50 3.70 2 -2 -26 7.40 2.20 2 -2 -26 2.70 2.30 2 2 -26 2.30 3.40 2 2 -26 2.20 4.20 -2 2 26 5.90 5.80 2 2 -26 2.30 1.90 2 2 -26 3.50 1.50 11 -3 -26 6.50 3.80 11 -3 -26 9.30 3.60 -11 -3 26 3.90 3.40 -11 -3 26 6.80 5.20 -11 3 26 12.40 7.10 11 3 -26 6.30 3.80 11 3 -26 4.10 4.10 11 3 -26 8.40 3.50 11 3 -26 8.80 3.90 -11 3 26 8.00 4.70 9 -3 -26 14.20 4.40 9 -3 -26 7.10 4.40 9 -3 -26 6.10 2.80 -9 -3 26 10.00 5.90 9 -3 -26 7.40 3.50 -9 -3 26 5.10 4.00 9 3 -26 3.20 2.80 9 3 -26 8.00 3.80 9 3 -26 8.50 3.70 9 3 -26 7.00 4.40 -9 3 26 12.40 4.80 -9 3 26 7.70 5.60 7 -3 -26 7.70 3.00 -7 -3 26 -0.30 4.00 -7 -3 26 5.10 3.80 7 -3 -26 3.80 3.10 7 -3 -26 5.10 3.90 7 -3 -26 5.10 4.00 -7 3 26 10.10 4.40 7 3 -26 13.00 5.00 -7 3 26 3.60 5.40 7 3 -26 9.60 3.80 7 3 -26 10.00 3.00 7 3 -26 15.80 4.00 -5 -3 26 0.30 6.50 -5 -3 26 -0.60 5.30 5 -3 -26 -0.90 2.00 5 -3 -26 -0.30 3.30 5 -3 -26 2.00 2.60 5 -3 -26 3.10 3.80 -5 3 26 0.80 4.70 -5 3 26 4.20 4.80 5 3 -26 2.90 2.60 5 3 -26 -0.90 3.90 5 3 -26 6.40 2.50 5 3 -26 0.20 3.20 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 56289 _shelx_res_file ; TITL appiariusy230601_0m_a.res in C2/c appiariusy230601_0m.res created by SHELXL-2018/3 at 15:54:28 on 29-Jun-2023 REM Old TITL AppiariusY230601_0m in C2/c REM SHELXT solution in C2/c: R1 0.092, Rweak 0.005, Alpha 0.033 REM 0.290 for 202 systematic absences, Orientation as input REM Formula found by SHELXT: C42 N4 Zn CELL 0.71073 20.0425 9.8589 17.1167 90 105.172 90 ZERR 4 0.0014 0.0006 0.0009 0 0.004 0 LATT 7 SYMM -X,+Y,0.5-Z SFAC C H B N Zn UNIT 160 144 8 16 4 L.S. 40 PLAN 10 SIZE 0.12 0.24 0.09 TEMP -173.15 CONF list 4 MORE -1 BOND $H fmap 2 53 acta OMIT -1 1 1 OMIT 2 0 0 OMIT 1 1 0 OMIT 0 0 2 REM REM REM WGHT 0.041600 3.488700 FVAR 0.18239 ZN1 5 0.500000 0.389776 0.750000 10.50000 0.01813 0.01939 = 0.01154 0.00000 0.00488 0.00000 N1 4 0.456358 0.288370 0.651324 11.00000 0.01600 0.01859 = 0.01333 0.00000 0.00554 -0.00001 N2 4 0.556103 0.480626 0.679880 11.00000 0.01979 0.02089 = 0.01474 0.00095 0.00416 -0.00224 C16 1 0.332353 0.143649 0.830740 11.00000 0.02200 0.03032 = 0.01878 0.00095 0.00889 -0.00550 AFIX 43 H16 2 0.341124 0.087836 0.877572 11.00000 -1.20000 AFIX 0 C9 1 0.484436 0.221244 0.527015 11.00000 0.02028 0.01925 = 0.01492 -0.00016 0.00658 0.00149 C1 1 0.494083 0.302370 0.596466 11.00000 0.01621 0.01785 = 0.01287 0.00158 0.00498 0.00228 C2 1 0.545758 0.407714 0.609866 11.00000 0.01669 0.01896 = 0.01392 0.00224 0.00477 0.00089 C8 1 0.524938 0.246881 0.471252 11.00000 0.02875 0.02466 = 0.01774 -0.00075 0.01154 0.00246 AFIX 43 H8 2 0.519116 0.190173 0.425081 11.00000 -1.20000 AFIX 0 C10 1 0.432851 0.117314 0.514020 11.00000 0.02744 0.02119 = 0.01711 -0.00340 0.00697 -0.00156 AFIX 43 H10 2 0.427219 0.059047 0.468550 11.00000 -1.20000 AFIX 0 C7 1 0.571651 0.350080 0.482188 11.00000 0.02662 0.02746 = 0.01936 0.00215 0.01273 0.00176 AFIX 43 H7 2 0.596684 0.366128 0.443013 11.00000 -1.20000 AFIX 0 C6 1 0.583097 0.434100 0.552245 11.00000 0.02019 0.02273 = 0.01872 0.00455 0.00838 0.00059 C12 1 0.356160 0.199675 0.702579 11.00000 0.01517 0.02261 = 0.01686 -0.00045 0.00489 -0.00338 C15 1 0.285176 0.249561 0.822893 11.00000 0.02072 0.03140 = 0.02172 -0.00499 0.01046 -0.00644 C17 1 0.367144 0.117280 0.771538 11.00000 0.01743 0.02370 = 0.01920 0.00146 0.00639 -0.00379 C11 1 0.391513 0.099624 0.565188 11.00000 0.02330 0.02255 = 0.02028 -0.00258 0.00628 -0.00490 AFIX 43 H11 2 0.356957 0.031157 0.554933 11.00000 -1.20000 AFIX 0 C20 1 0.418026 0.000896 0.783959 11.00000 0.02542 0.02558 = 0.02577 0.00592 0.00978 0.00069 AFIX 137 H20A 2 0.463242 0.031778 0.816536 11.00000 -1.50000 H20B 2 0.422293 -0.031172 0.731288 11.00000 -1.50000 H20C 2 0.401508 -0.073317 0.812099 11.00000 -1.50000 AFIX 0 C14 1 0.272874 0.329462 0.753491 11.00000 0.01835 0.02822 = 0.02649 -0.00295 0.00941 -0.00103 AFIX 43 H14 2 0.240393 0.401532 0.746658 11.00000 -1.20000 AFIX 0 C19 1 0.248122 0.277441 0.887368 11.00000 0.03122 0.04307 = 0.03068 -0.00663 0.01915 -0.00538 AFIX 137 H19A 2 0.204988 0.225380 0.875753 11.00000 -1.50000 H19B 2 0.237646 0.374471 0.887957 11.00000 -1.50000 H19C 2 0.277652 0.250591 0.940294 11.00000 -1.50000 AFIX 0 C13 1 0.307290 0.305684 0.693945 11.00000 0.01787 0.02596 = 0.02093 0.00160 0.00735 -0.00041 C4 1 0.640057 0.615772 0.638588 11.00000 0.02641 0.02913 = 0.02601 0.00405 0.00678 -0.00835 AFIX 43 H4 2 0.672060 0.688821 0.649815 11.00000 -1.20000 AFIX 0 C3 1 0.602260 0.580832 0.693533 11.00000 0.02659 0.02448 = 0.01947 0.00061 0.00370 -0.00644 AFIX 43 H3 2 0.609776 0.630540 0.742618 11.00000 -1.20000 AFIX 0 C18 1 0.292271 0.394852 0.619863 11.00000 0.02936 0.03954 = 0.03094 0.01216 0.01368 0.01229 AFIX 137 H18A 2 0.333702 0.447143 0.619199 11.00000 -1.50000 H18B 2 0.254432 0.457120 0.621039 11.00000 -1.50000 H18C 2 0.278912 0.338272 0.571181 11.00000 -1.50000 AFIX 0 C5 1 0.630284 0.542973 0.568073 11.00000 0.02383 0.02927 = 0.02438 0.00589 0.00997 -0.00356 AFIX 43 H5 2 0.655364 0.566043 0.529928 11.00000 -1.20000 AFIX 0 B1 3 0.401713 0.191865 0.639375 11.00000 0.01670 0.01971 = 0.01517 0.00041 0.00451 -0.00038 HKLF 4 REM appiariusy230601_0m_a.res in C2/c REM wR2 = 0.0974, GooF = S = 1.057, Restrained GooF = 1.057 for all data REM R1 = 0.0363 for 5466 Fo > 4sig(Fo) and 0.0500 for all 6577 data REM 216 parameters refined using 0 restraints END WGHT 0.0416 3.4889 REM Highest difference peak 0.518, deepest hole -0.402, 1-sigma level 0.071 Q1 1 0.5980 0.6592 0.7605 11.00000 0.05 0.52 Q2 1 0.5194 0.3600 0.6009 11.00000 0.05 0.50 Q3 1 0.3861 0.1467 0.6025 11.00000 0.05 0.47 Q4 1 0.4606 0.1684 0.5221 11.00000 0.05 0.44 Q5 1 0.5783 0.3824 0.5206 11.00000 0.05 0.43 Q6 1 0.6125 0.4788 0.5628 11.00000 0.05 0.43 Q7 1 0.5376 0.7195 0.7628 11.00000 0.05 0.42 Q8 1 0.3619 0.1647 0.7388 11.00000 0.05 0.42 Q9 1 0.5392 0.3181 0.4680 11.00000 0.05 0.41 Q10 1 0.2838 0.3209 0.7183 11.00000 0.05 0.39 ; _shelx_res_checksum 73644 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Zn Zn1 0.500000 0.38978(2) 0.750000 0.01617(6) Uani d 1 . . N N1 0.45636(5) 0.28837(11) 0.65132(6) 0.01565(17) Uani d 1 . . N N2 0.55610(6) 0.48063(11) 0.67988(6) 0.01854(19) Uani d 1 . . C C16 0.33235(7) 0.14365(15) 0.83074(8) 0.0230(2) Uani d 1 . . H H16 0.341124 0.087836 0.877572 0.028 Uiso calc 1 . . C C9 0.48444(6) 0.22124(13) 0.52702(7) 0.0178(2) Uani d 1 . . C C1 0.49408(6) 0.30237(12) 0.59647(7) 0.01542(19) Uani d 1 . . C C2 0.54576(6) 0.40771(12) 0.60987(7) 0.0164(2) Uani d 1 . . C C8 0.52494(7) 0.24688(14) 0.47125(8) 0.0227(2) Uani d 1 . . H H8 0.519116 0.190173 0.425081 0.027 Uiso calc 1 . . C C10 0.43285(7) 0.11731(14) 0.51402(8) 0.0217(2) Uani d 1 . . H H10 0.427219 0.059047 0.468550 0.026 Uiso calc 1 . . C C7 0.57165(7) 0.35008(15) 0.48219(8) 0.0232(2) Uani d 1 . . H H7 0.596684 0.366128 0.443013 0.028 Uiso calc 1 . . C C6 0.58310(7) 0.43410(14) 0.55225(8) 0.0199(2) Uani d 1 . . C C12 0.35616(6) 0.19967(13) 0.70258(7) 0.0181(2) Uani d 1 . . C C15 0.28518(7) 0.24956(15) 0.82289(8) 0.0237(2) Uani d 1 . . C C17 0.36714(6) 0.11728(14) 0.77154(8) 0.0198(2) Uani d 1 . . C C11 0.39151(7) 0.09962(14) 0.56519(8) 0.0219(2) Uani d 1 . . H H11 0.356957 0.031157 0.554933 0.026 Uiso calc 1 . . C C20 0.41803(7) 0.00090(15) 0.78396(9) 0.0250(3) Uani d 1 . . H H20A 0.463242 0.031778 0.816536 0.038 Uiso calc 1 . . H H20B 0.422293 -0.031172 0.731288 0.038 Uiso calc 1 . . H H20C 0.401508 -0.073317 0.812099 0.038 Uiso calc 1 . . C C14 0.27287(7) 0.32946(15) 0.75349(8) 0.0237(2) Uani d 1 . . H H14 0.240393 0.401532 0.746658 0.028 Uiso calc 1 . . C C19 0.24812(8) 0.27744(19) 0.88737(10) 0.0329(3) Uani d 1 . . H H19A 0.204988 0.225380 0.875753 0.049 Uiso calc 1 . . H H19B 0.237646 0.374471 0.887957 0.049 Uiso calc 1 . . H H19C 0.277652 0.250591 0.940294 0.049 Uiso calc 1 . . C C13 0.30729(6) 0.30568(14) 0.69395(8) 0.0212(2) Uani d 1 . . C C4 0.64006(8) 0.61577(16) 0.63859(9) 0.0272(3) Uani d 1 . . H H4 0.672060 0.688821 0.649815 0.033 Uiso calc 1 . . C C3 0.60226(7) 0.58083(14) 0.69353(8) 0.0240(2) Uani d 1 . . H H3 0.609776 0.630540 0.742618 0.029 Uiso calc 1 . . C C18 0.29227(8) 0.39485(18) 0.61986(10) 0.0322(3) Uani d 1 . . H H18A 0.333702 0.447143 0.619199 0.048 Uiso calc 1 . . H H18B 0.254432 0.457120 0.621039 0.048 Uiso calc 1 . . H H18C 0.278912 0.338272 0.571181 0.048 Uiso calc 1 . . C C5 0.63028(7) 0.54297(15) 0.56807(9) 0.0251(3) Uani d 1 . . H H5 0.655364 0.566043 0.529928 0.030 Uiso calc 1 . . B B1 0.40171(7) 0.19187(14) 0.63937(8) 0.0171(2) Uani d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Zn1 0.01813(9) 0.01939(10) 0.01154(8) 0.000 0.00488(6) 0.000 N1 0.0160(4) 0.0186(4) 0.0133(4) 0.0000(3) 0.0055(3) 0.0000(3) N2 0.0198(5) 0.0209(5) 0.0147(4) -0.0022(4) 0.0042(4) 0.0009(3) C16 0.0220(6) 0.0303(7) 0.0188(5) -0.0055(5) 0.0089(4) 0.0010(5) C9 0.0203(5) 0.0193(5) 0.0149(5) 0.0015(4) 0.0066(4) -0.0002(4) C1 0.0162(5) 0.0178(5) 0.0129(4) 0.0023(4) 0.0050(4) 0.0016(4) C2 0.0167(5) 0.0190(5) 0.0139(4) 0.0009(4) 0.0048(4) 0.0022(4) C8 0.0288(6) 0.0247(6) 0.0177(5) 0.0025(5) 0.0115(5) -0.0008(4) C10 0.0274(6) 0.0212(6) 0.0171(5) -0.0016(5) 0.0070(4) -0.0034(4) C7 0.0266(6) 0.0275(6) 0.0194(5) 0.0018(5) 0.0127(5) 0.0021(5) C6 0.0202(5) 0.0227(5) 0.0187(5) 0.0006(4) 0.0084(4) 0.0046(4) C12 0.0152(5) 0.0226(6) 0.0169(5) -0.0034(4) 0.0049(4) -0.0004(4) C15 0.0207(5) 0.0314(7) 0.0217(6) -0.0064(5) 0.0105(5) -0.0050(5) C17 0.0174(5) 0.0237(6) 0.0192(5) -0.0038(4) 0.0064(4) 0.0015(4) C11 0.0233(6) 0.0226(6) 0.0203(5) -0.0049(4) 0.0063(4) -0.0026(4) C20 0.0254(6) 0.0256(6) 0.0258(6) 0.0007(5) 0.0098(5) 0.0059(5) C14 0.0183(5) 0.0282(7) 0.0265(6) -0.0010(5) 0.0094(5) -0.0030(5) C19 0.0312(7) 0.0431(9) 0.0307(7) -0.0054(6) 0.0191(6) -0.0066(6) C13 0.0179(5) 0.0260(6) 0.0209(5) -0.0004(4) 0.0073(4) 0.0016(4) C4 0.0264(6) 0.0291(7) 0.0260(6) -0.0084(5) 0.0068(5) 0.0041(5) C3 0.0266(6) 0.0245(6) 0.0195(5) -0.0064(5) 0.0037(5) 0.0006(4) C18 0.0294(7) 0.0395(8) 0.0309(7) 0.0123(6) 0.0137(6) 0.0122(6) C5 0.0238(6) 0.0293(7) 0.0244(6) -0.0036(5) 0.0100(5) 0.0059(5) B1 0.0167(5) 0.0197(6) 0.0152(5) -0.0004(4) 0.0045(4) 0.0004(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag N1 Zn1 N1 2_656 . 118.68(6) y N1 Zn1 N2 2_656 2_656 84.72(4) ? N1 Zn1 N2 2_656 . 122.48(4) y N1 Zn1 N2 . 2_656 122.48(4) ? N1 Zn1 N2 . . 84.72(4) y N2 Zn1 N2 . 2_656 128.26(6) y C1 N1 Zn1 . . 109.89(8) ? C1 N1 B1 . . 120.99(10) ? B1 N1 Zn1 . . 128.11(8) ? C2 N2 Zn1 . . 107.62(8) ? C3 N2 Zn1 . . 133.06(9) ? C3 N2 C2 . . 118.90(11) ? C15 C16 H16 . . 119.2 ? C15 C16 C17 . . 121.69(12) ? C17 C16 H16 . . 119.2 ? C1 C9 C8 . . 119.26(11) ? C1 C9 C10 . . 118.26(11) ? C8 C9 C10 . . 122.46(11) ? N1 C1 C9 . . 123.33(11) ? N1 C1 C2 . . 118.03(10) ? C9 C1 C2 . . 118.63(10) ? N2 C2 C1 . . 117.15(10) ? N2 C2 C6 . . 122.03(11) ? C6 C2 C1 . . 120.82(11) ? C9 C8 H8 . . 119.0 ? C7 C8 C9 . . 122.07(12) ? C7 C8 H8 . . 119.0 ? C9 C10 H10 . . 119.1 ? C11 C10 C9 . . 121.79(12) ? C11 C10 H10 . . 119.1 ? C8 C7 H7 . . 119.9 ? C8 C7 C6 . . 120.21(11) ? C6 C7 H7 . . 119.9 ? C2 C6 C7 . . 118.90(12) ? C5 C6 C2 . . 117.29(12) ? C5 C6 C7 . . 123.81(12) ? C17 C12 C13 . . 117.92(11) ? C17 C12 B1 . . 123.59(11) ? C13 C12 B1 . . 118.06(11) ? C16 C15 C14 . . 118.10(12) ? C16 C15 C19 . . 121.23(13) ? C14 C15 C19 . . 120.67(14) ? C16 C17 C12 . . 120.32(12) ? C16 C17 C20 . . 119.04(12) ? C12 C17 C20 . . 120.62(11) ? C10 C11 H11 . . 120.5 ? C10 C11 B1 . . 118.97(12) ? B1 C11 H11 . . 120.5 ? C17 C20 H20A . . 109.5 ? C17 C20 H20B . . 109.5 ? C17 C20 H20C . . 109.5 ? H20A C20 H20B . . 109.5 ? H20A C20 H20C . . 109.5 ? H20B C20 H20C . . 109.5 ? C15 C14 H14 . . 119.4 ? C13 C14 C15 . . 121.22(13) ? C13 C14 H14 . . 119.4 ? C15 C19 H19A . . 109.5 ? C15 C19 H19B . . 109.5 ? C15 C19 H19C . . 109.5 ? H19A C19 H19B . . 109.5 ? H19A C19 H19C . . 109.5 ? H19B C19 H19C . . 109.5 ? C12 C13 C18 . . 119.97(11) ? C14 C13 C12 . . 120.70(12) ? C14 C13 C18 . . 119.32(12) ? C3 C4 H4 . . 120.5 ? C5 C4 H4 . . 120.5 ? C5 C4 C3 . . 119.03(13) ? N2 C3 C4 . . 122.63(13) ? N2 C3 H3 . . 118.7 ? C4 C3 H3 . . 118.7 ? C13 C18 H18A . . 109.5 ? C13 C18 H18B . . 109.5 ? C13 C18 H18C . . 109.5 ? H18A C18 H18B . . 109.5 ? H18A C18 H18C . . 109.5 ? H18B C18 H18C . . 109.5 ? C6 C5 H5 . . 120.0 ? C4 C5 C6 . . 120.08(12) ? C4 C5 H5 . . 120.0 ? N1 B1 C12 . . 115.27(11) ? N1 B1 C11 . . 116.51(11) ? C11 B1 C12 . . 128.12(11) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Zn1 N1 2_656 1.9606(10) ? Zn1 N1 . 1.9606(10) y Zn1 N2 . 2.0527(10) y Zn1 N2 2_656 2.0527(10) ? N1 C1 . 1.3580(14) y N1 B1 . 1.4245(17) y N2 C2 . 1.3660(16) y N2 C3 . 1.3316(17) y C16 H16 . 0.9500 ? C16 C15 . 1.391(2) ? C16 C17 . 1.3966(18) ? C9 C1 . 1.4035(16) ? C9 C8 . 1.4281(17) ? C9 C10 . 1.4310(18) ? C1 C2 . 1.4421(17) ? C2 C6 . 1.4095(16) ? C8 H8 . 0.9500 ? C8 C7 . 1.362(2) ? C10 H10 . 0.9500 ? C10 C11 . 1.3652(18) ? C7 H7 . 0.9500 ? C7 C6 . 1.4257(19) ? C6 C5 . 1.4092(19) ? C12 C17 . 1.4020(17) ? C12 C13 . 1.4134(18) ? C12 B1 . 1.5896(18) y C15 C14 . 1.393(2) ? C15 C19 . 1.5080(19) ? C17 C20 . 1.5127(19) ? C11 H11 . 0.9500 ? C11 B1 . 1.5315(19) y C20 H20A . 0.9800 ? C20 H20B . 0.9800 ? C20 H20C . 0.9800 ? C14 H14 . 0.9500 ? C14 C13 . 1.3920(18) ? C19 H19A . 0.9800 ? C19 H19B . 0.9800 ? C19 H19C . 0.9800 ? C13 C18 . 1.507(2) ? C4 H4 . 0.9500 ? C4 C3 . 1.3964(19) ? C4 C5 . 1.374(2) ? C3 H3 . 0.9500 ? C18 H18A . 0.9800 ? C18 H18B . 0.9800 ? C18 H18C . 0.9800 ? C5 H5 . 0.9500 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag Zn1 N1 C1 C9 . . . . 166.76(9) y Zn1 N1 C1 C2 . . . . -14.38(13) y Zn1 N1 B1 C12 . . . . 20.10(16) y Zn1 N1 B1 C11 . . . . -163.25(9) y Zn1 N2 C2 C1 . . . . 7.93(13) ? Zn1 N2 C2 C6 . . . . -172.71(10) ? Zn1 N2 C3 C4 . . . . 172.48(11) ? N1 C1 C2 N2 . . . . 4.08(16) ? N1 C1 C2 C6 . . . . -175.29(11) ? N2 C2 C6 C7 . . . . 177.35(12) ? N2 C2 C6 C5 . . . . -2.32(19) ? C16 C15 C14 C13 . . . . -0.8(2) ? C9 C1 C2 N2 . . . . -177.01(11) ? C9 C1 C2 C6 . . . . 3.63(17) ? C9 C8 C7 C6 . . . . 2.0(2) ? C9 C10 C11 B1 . . . . -1.2(2) ? C1 N1 B1 C12 . . . . -172.61(11) ? C1 N1 B1 C11 . . . . 4.04(17) ? C1 C9 C8 C7 . . . . -1.7(2) ? C1 C9 C10 C11 . . . . 2.81(19) ? C1 C2 C6 C7 . . . . -3.32(18) ? C1 C2 C6 C5 . . . . 177.02(12) ? C2 N2 C3 C4 . . . . 0.8(2) ? C2 C6 C5 C4 . . . . 2.1(2) ? C8 C9 C1 N1 . . . . 177.72(11) ? C8 C9 C1 C2 . . . . -1.14(17) ? C8 C9 C10 C11 . . . . -175.75(13) ? C8 C7 C6 C2 . . . . 0.5(2) ? C8 C7 C6 C5 . . . . -179.86(14) ? C10 C9 C1 N1 . . . . -0.89(18) ? C10 C9 C1 C2 . . . . -179.75(11) ? C10 C9 C8 C7 . . . . 176.87(13) ? C10 C11 B1 N1 . . . . -2.14(19) ? C10 C11 B1 C12 . . . . 174.00(13) ? C7 C6 C5 C4 . . . . -177.57(14) ? C15 C16 C17 C12 . . . . 1.2(2) ? C15 C16 C17 C20 . . . . 179.74(13) ? C15 C14 C13 C12 . . . . -0.3(2) ? C15 C14 C13 C18 . . . . 180.00(14) ? C17 C16 C15 C14 . . . . 0.4(2) ? C17 C16 C15 C19 . . . . -179.75(13) ? C17 C12 C13 C14 . . . . 1.89(19) ? C17 C12 C13 C18 . . . . -178.44(13) ? C17 C12 B1 N1 . . . . -96.44(15) ? C17 C12 B1 C11 . . . . 87.37(17) ? C19 C15 C14 C13 . . . . 179.30(13) ? C13 C12 C17 C16 . . . . -2.33(18) ? C13 C12 C17 C20 . . . . 179.19(12) ? C13 C12 B1 N1 . . . . 75.93(15) ? C13 C12 B1 C11 . . . . -100.25(16) ? C3 N2 C2 C1 . . . . -178.47(11) ? C3 N2 C2 C6 . . . . 0.89(18) ? C3 C4 C5 C6 . . . . -0.5(2) ? C5 C4 C3 N2 . . . . -1.0(2) ? B1 N1 C1 C9 . . . . -2.63(18) ? B1 N1 C1 C2 . . . . 176.23(11) ? B1 C12 C17 C16 . . . . 170.06(12) ? B1 C12 C17 C20 . . . . -8.42(19) ? B1 C12 C13 C14 . . . . -170.92(12) ? B1 C12 C13 C18 . . . . 8.75(19) ?