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Information card for entry 7112105
Preview
| Coordinates | 7112105.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C18 H23 Cl3 N2 Si |
|---|---|
| Calculated formula | C18 H23 Cl3 N2 Si |
| SMILES | Cl[Si]1(Cl)(Cl)[n]2ccccc2CN1c1c(cccc1C(C)C)C(C)C |
| Title of publication | Unusual formation of a N-heterocyclic germylene via homolytic cleavage of a C-C bond |
| Authors of publication | Yan Li; Kartik Chandra Mondal; Peter Stollberg; Hongping Zhu; Herbert W. Roesky; Regine Herbst-Irmer; Dietmar Stalke; Heike Fliegl |
| Journal of publication | Chem.Commun. |
| Year of publication | 2014 |
| Journal volume | 50 |
| Pages of publication | 3356 |
| a | 9.984 ± 0.002 Å |
| b | 13.987 ± 0.002 Å |
| c | 14.11 ± 0.002 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 1970.4 ± 0.6 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 19 |
| Hermann-Mauguin space group symbol | P 21 21 21 |
| Hall space group symbol | P 2ac 2ab |
| Residual factor for all reflections | 0.0334 |
| Residual factor for significantly intense reflections | 0.0322 |
| Weighted residual factors for significantly intense reflections | 0.0856 |
| Weighted residual factors for all reflections included in the refinement | 0.0864 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.08 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
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