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Information card for entry 4308668
Preview
| Coordinates | 4308668.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C65.5 H52 Cl Ge5 Ir3 O5 |
|---|---|
| Calculated formula | C65.5 H52 Cl Ge5 Ir3 O5 |
| Title of publication | High-Nuclearity Iridium Carbonyl Clusters Containing Phenylgermyl Ligands: Synthesis, Structures, and Reactivity |
| Authors of publication | Richard D. Adams; Burjor Captain; Jack L. Smith |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2005 |
| Journal volume | 44 |
| Pages of publication | 1413 - 1420 |
| a | 12.8208 ± 0.0008 Å |
| b | 21.496 ± 0.0014 Å |
| c | 23.5896 ± 0.0015 Å |
| α | 90° |
| β | 90.601 ± 0.001° |
| γ | 90° |
| Cell volume | 6500.8 ± 0.7 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0484 |
| Residual factor for significantly intense reflections | 0.0347 |
| Weighted residual factors for significantly intense reflections | 0.0961 |
| Weighted residual factors for all reflections included in the refinement | 0.1076 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.075 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
Version history
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Users of the data should acknowledge the original authors of the
structural data.