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Information card for entry 4308643
Preview
| Coordinates | 4308643.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | [Ni3salamo2(OAc)2(EtOH)2] |
|---|---|
| Formula | C42 H52 N4 Ni3 O15 |
| Calculated formula | C42 H52 N4 Ni3 O15 |
| Title of publication | Novel Thiosalamo Ligand as a Remarkably Stable N2S2 Salen-Type Chelate and Synthesis of a Nickel(II) Complex |
| Authors of publication | Shigehisa Akine; Tatsuya Nabeshima |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2005 |
| Journal volume | 44 |
| Pages of publication | 1205 - 1207 |
| a | 10.7606 ± 0.0017 Å |
| b | 12.4817 ± 0.0018 Å |
| c | 16.8606 ± 0.0019 Å |
| α | 89.042 ± 0.006° |
| β | 83.68 ± 0.006° |
| γ | 78.832 ± 0.003° |
| Cell volume | 2208.1 ± 0.5 Å3 |
| Cell temperature | 120 ± 2 K |
| Ambient diffraction temperature | 120 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1005 |
| Residual factor for significantly intense reflections | 0.0551 |
| Weighted residual factors for significantly intense reflections | 0.1156 |
| Weighted residual factors for all reflections included in the refinement | 0.1335 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.024 |
| Diffraction radiation wavelength | 0.71069 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
Version history
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