Crystallography Open Database

Information card for entry 4308181

Preview

Coordinates	4308181.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H39 Cl4 N8 O17.5 Zn
Calculated formula	C22 H32.5 Cl4 N8 O17.5 Zn
Title of publication	A New Branched Phenanthroline Derivative Ligand: Synthesis, Solution Chemistry, and Crystal Structures of Copper(II) and Zinc(II) Complexes
Authors of publication	Gianluca Ambrosi; Mauro Formica; Vieri Fusi; Luca Giorgi; Annalisa Guerri; Mauro Micheloni; Paola Paoli; Roberto Pontellini; Patrizia Rossi
Journal of publication	Inorganic Chemistry
Year of publication	2007
Journal volume	46
Pages of publication	4737 - 4748
a	10.225 ± 0.006 Å
b	15.88 ± 0.001 Å
c	24.179 ± 0.002 Å
α	102.033 ± 0.007°
β	100.026 ± 0.006°
γ	105.365 ± 0.007°
Cell volume	3591 ± 2 Å³
Cell temperature	298 K
Ambient diffraction temperature	298 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.2131
Residual factor for significantly intense reflections	0.08
Weighted residual factors for significantly intense reflections	0.184
Weighted residual factors for all reflections included in the refinement	0.2263
Goodness-of-fit parameter for all reflections included in the refinement	0.849
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179119 (current)	2016-03-22	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/81.	4308181.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4308181.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4308181.cif
1194	2010-06-06	cif/4/ Adding data from Inorg-Chem-2007_01-13/ processing directory.	4308181.cif