#------------------------------------------------------------------------------ #$Date: 2026-08-29 15:26:25 +0200 (Sat, 29 Aug 2026) $ #$Revision: 306769 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/35/2023544.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023544 loop_ _publ_author_name 'Naeem, Marilyn' 'Chadeayne, Andrew R.' 'Golen, James A.' 'Manke, David R.' _publ_section_title ; Syntheses and structures of two norpsilocin derivatives: N-ethyl-4-hydroxytryptamine (4-HO-NET) and 4-hydroxy-N-propyltryptamine (4-HO-NPT) ; _journal_coeditor_code HB8250 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E Crystallographic Communications' _journal_page_first 1082 _journal_page_last 1086 _journal_paper_doi 10.1107/S2056989026008571 _journal_volume 82 _journal_year 2026 _chemical_formula_iupac 'C13 H18 N2 O' _chemical_formula_moiety 'C13 H18 N2 O' _chemical_formula_sum 'C13 H18 N2 O' _chemical_formula_weight 218.29 _chemical_name_common ; 4-Hydroxy-N-propyltryptamine ; _chemical_name_systematic ; 3-[2-(Propylamino)ethyl]-1H-indol-4-ol ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_method ; Olex2 1.5 (compiled 2023.08.24 svn.re1ec1418 for OlexSys, GUI svn.r6817) ; _cell_angle_alpha 90 _cell_angle_beta 91.523(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 9.0478(6) _cell_length_b 11.6680(8) _cell_length_c 11.3885(7) _cell_measurement_reflns_used 8762 _cell_measurement_temperature 300(2) _cell_measurement_theta_max 26.37 _cell_measurement_theta_min 2.84 _cell_volume 1201.86(14) _computing_cell_refinement ; SAINT (Bruker, 2021) ; _computing_data_collection ; APEX3 (Bruker, 2021) ; _computing_data_reduction ; SAINT (Bruker, 2021) ; _computing_molecular_graphics ; OLEX2 (Dolomanov et al., 2009) ; _computing_publication_material ; publCIF (Westrip, 2010) ; _computing_structure_refinement ; SHELXL2018 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2014 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 300.15 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device_type 'Bruker D8 Venture CMOS' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0398 _diffrn_reflns_av_unetI/netI 0.0151 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 14 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 34791 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.428 _diffrn_reflns_theta_min 2.839 _diffrn_source_current 30.0 _diffrn_source_power 1.5 _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.077 _exptl_absorpt_correction_T_max 0.745 _exptl_absorpt_correction_T_min 0.705 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.206 _exptl_crystal_description block _exptl_crystal_F_000 472 _exptl_crystal_size_max 0.24 _exptl_crystal_size_mid 0.22 _exptl_crystal_size_min 0.21 _refine_diff_density_max 0.136 _refine_diff_density_min -0.111 _refine_ls_extinction_coef 0.010(2) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method ; SHELXL2018 (Sheldrick, 2015b) ; _refine_ls_goodness_of_fit_ref 1.010 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 159 _refine_ls_number_reflns 2472 _refine_ls_number_restraints 3 _refine_ls_restrained_S_all 1.010 _refine_ls_R_factor_all 0.0522 _refine_ls_R_factor_gt 0.0383 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0476P)^2^+0.2229P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0967 _refine_ls_wR_factor_ref 0.1071 _reflns_number_gt 1941 _reflns_number_total 2472 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file hb8250.cif _cod_data_source_block 4-HO-NPT _cod_database_code 2023544 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.982 _shelx_estimated_absorpt_t_max 0.984 _shelx_hkl_file ; -2 0 0 1035.00 16.60 -2 0 0 1098.39 17.40 -3 0 0 0.00 0.80 -3 0 0 -1.40 0.70 3 0 0 -0.60 0.60 -3 0 0 0.00 0.90 3 0 0 1.00 0.70 -3 0 0 -0.70 0.70 -3 0 0 0.80 1.00 3 0 0 -0.40 0.60 3 0 0 0.90 0.90 4 0 0 807.52 13.80 4 0 0 847.52 13.70 4 0 0 820.22 14.20 -4 0 0 841.52 13.70 -4 0 0 821.52 13.70 -4 0 0 837.52 15.10 -4 0 0 802.72 13.80 4 0 0 822.32 13.40 -4 0 0 845.32 14.30 -5 0 0 -0.70 0.90 -5 0 0 -0.20 0.90 5 0 0 -0.50 0.90 -5 0 0 1.40 1.10 5 0 0 -0.10 0.80 5 0 0 0.10 0.70 5 0 0 -0.20 1.00 -5 0 0 0.60 1.00 -5 0 0 1.90 1.30 6 0 0 197.88 5.30 -6 0 0 198.28 5.30 6 0 0 188.38 4.80 -6 0 0 191.48 5.40 -6 0 0 185.58 6.10 -6 0 0 183.88 4.60 -6 0 0 188.88 4.80 6 0 0 180.98 4.00 6 0 0 186.38 4.00 7 0 0 0.20 0.80 7 0 0 1.20 1.30 -7 0 0 2.00 1.50 7 0 0 0.00 1.10 -7 0 0 -2.00 1.40 -7 0 0 -1.00 1.20 -7 0 0 -1.20 1.20 -7 0 0 -0.20 1.20 7 0 0 -0.60 0.80 -8 0 0 32.90 3.50 -8 0 0 35.10 2.60 8 0 0 32.00 2.90 8 0 0 31.90 1.40 -8 0 0 32.00 2.50 -8 0 0 32.10 2.90 -8 0 0 33.90 2.50 -9 0 0 -3.00 1.70 9 0 0 -1.40 1.30 -9 0 0 -1.00 1.30 -9 0 0 -0.30 1.50 -9 0 0 0.00 1.70 -9 0 0 -1.80 1.50 -10 0 0 6.30 2.30 -10 0 0 0.70 2.20 -10 0 0 5.60 1.90 -10 0 0 4.60 1.70 -10 0 0 5.60 2.00 10 0 0 4.50 1.90 11 0 0 -2.30 1.60 -11 0 0 1.20 1.50 -11 0 0 -0.70 2.30 -11 0 0 1.30 1.60 -11 0 0 2.70 2.00 -11 0 0 1.40 2.10 -1 -1 0 409.96 6.60 1 -1 0 414.96 7.00 -1 -1 0 410.76 6.60 -1 -1 0 407.16 6.90 -1 -1 0 406.36 6.50 1 -1 0 386.16 6.70 1 1 0 408.86 6.80 -1 1 0 398.36 6.40 -1 1 0 378.86 6.50 -1 1 0 408.46 6.50 2 -1 0 117.99 3.60 -2 -1 0 116.89 2.80 2 -1 0 118.19 2.40 -2 -1 0 112.29 2.60 2 -1 0 118.29 2.40 2 -1 0 119.39 2.60 -2 -1 0 113.99 2.50 -2 -1 0 115.09 2.60 2 1 0 115.49 2.50 2 1 0 116.49 2.50 -2 1 0 119.39 2.60 2 1 0 113.69 3.30 -2 1 0 114.19 2.60 -2 1 0 115.19 2.50 2 1 0 114.89 2.60 -2 1 0 113.59 2.50 -2 1 0 114.99 3.10 3 -1 0 96.99 2.20 3 -1 0 97.69 2.30 3 -1 0 94.09 3.20 -3 -1 0 94.99 2.60 -3 -1 0 91.79 2.40 3 -1 0 92.99 2.60 -3 -1 0 94.79 2.80 -3 1 0 96.19 2.60 -3 1 0 92.79 2.50 3 1 0 94.29 2.30 -3 1 0 94.59 3.20 -3 1 0 93.29 2.50 -3 1 0 95.49 2.40 3 1 0 95.59 2.80 3 1 0 94.19 2.60 3 1 0 96.99 2.30 -4 -1 0 -0.20 0.90 -4 -1 0 0.20 0.90 -4 -1 0 0.20 1.10 4 -1 0 -1.10 0.90 4 -1 0 -0.70 1.20 -4 1 0 -0.30 1.10 -4 1 0 -0.30 0.90 4 1 0 0.50 0.80 -4 1 0 -1.70 0.80 4 1 0 -0.10 0.80 -4 1 0 -0.60 0.90 -4 1 0 1.10 0.90 4 1 0 -0.20 0.90 4 1 0 1.40 1.20 -5 -1 0 0.10 0.90 -5 -1 0 1.50 1.00 -5 -1 0 0.20 1.20 -5 -1 0 1.10 1.00 5 -1 0 0.60 1.00 -5 -1 0 1.20 1.20 5 -1 0 1.70 0.80 5 -1 0 0.50 0.80 5 1 0 0.50 0.80 -5 1 0 1.00 1.10 -5 1 0 0.70 1.30 -5 1 0 0.90 1.00 5 1 0 0.50 0.80 5 1 0 0.60 1.00 -5 1 0 0.40 1.00 -5 1 0 0.80 0.90 5 1 0 0.70 1.20 -6 -1 0 737.43 13.70 -6 -1 0 712.13 12.80 6 -1 0 714.23 11.80 -6 -1 0 693.63 12.70 -6 -1 0 705.93 13.80 6 -1 0 709.23 11.80 -6 -1 0 736.53 14.70 6 -1 0 726.63 13.30 6 1 0 716.33 12.90 6 1 0 709.13 12.00 -6 1 0 678.53 13.50 -6 1 0 720.33 14.60 -6 1 0 696.63 12.60 -6 1 0 723.83 13.30 -6 1 0 727.33 12.80 6 1 0 694.13 11.90 6 1 0 722.73 13.60 -7 -1 0 59.49 4.00 -7 -1 0 61.99 3.30 7 -1 0 62.69 2.00 -7 -1 0 63.99 2.90 7 -1 0 61.09 2.00 -7 -1 0 63.39 2.90 7 -1 0 66.29 3.30 -7 -1 0 65.39 3.00 -7 1 0 62.39 2.90 7 1 0 58.59 2.10 -7 1 0 61.69 3.30 -7 1 0 58.39 2.90 -7 1 0 56.99 2.90 7 1 0 60.89 2.90 -7 1 0 60.09 3.90 7 1 0 60.09 2.20 7 1 0 67.79 5.50 8 -1 0 23.90 1.20 -8 -1 0 19.70 2.90 -8 -1 0 29.10 2.60 -8 -1 0 22.40 2.60 8 -1 0 24.10 2.50 -8 -1 0 22.50 2.30 -8 -1 0 20.10 2.10 8 1 0 23.20 2.00 8 1 0 26.60 2.80 8 1 0 24.30 2.30 -8 1 0 26.00 2.40 -8 1 0 23.00 2.60 -8 1 0 19.90 2.90 -8 1 0 24.50 2.30 8 1 0 21.80 1.40 -8 1 0 15.90 1.90 9 -1 0 15.00 2.30 -9 -1 0 20.20 2.50 -9 -1 0 15.60 2.60 -9 -1 0 17.70 3.00 -9 -1 0 13.50 2.00 -9 -1 0 14.70 2.20 -9 1 0 15.70 2.20 -9 1 0 12.80 2.70 -9 1 0 14.70 2.00 9 1 0 16.10 2.40 -9 1 0 16.90 2.50 -9 1 0 15.40 2.20 -10 -1 0 -1.10 1.80 -10 -1 0 2.90 1.80 -10 -1 0 -0.50 1.80 -10 -1 0 3.90 2.40 10 -1 0 4.20 1.90 -10 1 0 3.80 2.10 -10 1 0 0.80 2.20 -10 1 0 1.40 1.60 -10 1 0 0.60 1.70 -10 1 0 2.50 1.80 10 1 0 -0.70 1.60 -11 -1 0 1.70 1.70 -11 -1 0 -0.70 2.30 11 -1 0 1.70 1.90 -11 -1 0 2.20 2.00 -11 -1 0 1.30 2.00 -11 1 0 0.20 1.50 -11 1 0 5.00 2.20 -11 1 0 0.50 1.60 -11 1 0 -1.50 2.30 -11 1 0 1.00 2.00 11 1 0 1.60 2.00 0 -2 0 1196.68 30.00 0 2 0 1235.78 30.20 -1 -2 0 47.80 1.70 1 -2 0 50.29 1.70 -1 -2 0 48.60 1.60 1 -2 0 48.60 1.90 -1 -2 0 48.40 1.90 1 -2 0 50.79 1.60 -1 -2 0 48.80 1.60 -1 -2 0 49.50 1.70 1 2 0 47.40 1.60 -1 2 0 50.39 1.70 -1 2 0 49.30 1.90 -1 2 0 47.80 2.20 1 2 0 46.10 1.70 -1 2 0 49.20 1.60 -1 2 0 48.70 1.60 1 2 0 48.50 1.70 1 2 0 49.90 1.70 1 2 0 46.00 1.80 -2 -2 0 2667.93 58.39 -2 2 0 2858.01 73.89 -3 -2 0 87.49 2.80 3 -2 0 86.99 2.50 -3 -2 0 82.29 2.50 3 -2 0 88.39 3.20 3 -2 0 83.89 2.40 -3 -2 0 82.89 2.60 -3 -2 0 85.69 2.50 -3 -2 0 83.89 3.30 3 -2 0 84.59 2.30 -3 2 0 87.79 3.30 3 2 0 85.99 2.60 -3 2 0 86.19 2.40 3 2 0 86.89 2.40 3 2 0 87.19 2.40 3 2 0 86.49 2.90 -3 2 0 86.49 2.40 -3 2 0 81.39 2.40 -4 -2 0 108.89 3.50 4 -2 0 114.49 2.80 -4 -2 0 109.39 3.10 -4 -2 0 105.59 3.50 -4 -2 0 112.29 3.20 4 -2 0 112.29 2.80 4 -2 0 104.69 3.10 4 -2 0 114.79 4.00 -4 2 0 116.29 4.00 4 2 0 109.79 2.90 -4 2 0 111.59 3.10 -4 2 0 108.09 3.40 4 2 0 112.19 3.60 4 2 0 112.99 2.90 4 2 0 113.89 3.20 -4 2 0 113.09 3.00 5 -2 0 10.20 1.40 5 -2 0 11.60 1.80 5 -2 0 12.40 1.20 -5 -2 0 12.10 1.50 -5 -2 0 8.30 1.40 -5 -2 0 9.60 1.60 5 -2 0 12.90 1.20 5 2 0 13.50 1.80 -5 2 0 12.30 1.40 -5 2 0 10.60 1.80 5 2 0 13.70 1.50 -5 2 0 10.70 1.40 5 2 0 14.00 1.30 -5 2 0 11.20 1.50 -5 2 0 11.90 1.40 5 2 0 11.80 1.20 6 -2 0 108.09 3.70 -6 -2 0 100.09 4.10 -6 -2 0 109.29 3.60 -6 -2 0 105.29 3.50 6 -2 0 114.19 4.60 -6 -2 0 105.59 3.50 6 -2 0 110.39 2.80 6 -2 0 103.09 2.80 -6 -2 0 102.79 4.70 6 2 0 103.19 3.00 -6 2 0 109.19 3.70 6 2 0 108.49 3.60 6 2 0 109.29 4.10 -6 2 0 101.29 4.10 -6 2 0 108.69 3.40 6 2 0 108.09 3.00 -6 2 0 106.59 3.40 -6 2 0 102.89 4.60 7 -2 0 3.30 0.90 7 -2 0 2.70 0.90 -7 -2 0 4.00 1.50 -7 -2 0 4.50 1.50 -7 -2 0 1.80 1.30 7 -2 0 3.90 1.50 -7 -2 0 2.80 1.70 -7 -2 0 3.50 1.60 7 2 0 4.30 1.40 -7 2 0 4.40 1.80 -7 2 0 1.60 1.30 7 2 0 2.70 1.00 7 2 0 2.70 1.50 -7 2 0 2.30 1.40 7 2 0 4.10 1.60 -7 2 0 2.90 1.40 -7 2 0 1.50 1.20 -8 -2 0 -0.70 1.50 -8 -2 0 -2.50 1.60 -8 -2 0 3.30 1.90 8 -2 0 -0.10 1.50 8 -2 0 0.60 0.70 -8 -2 0 -1.00 1.40 -8 -2 0 1.30 1.40 8 2 0 -0.10 1.50 -8 2 0 0.00 1.30 8 2 0 -2.60 1.40 -8 2 0 0.80 1.30 8 2 0 0.30 0.90 8 2 0 0.20 0.90 -8 2 0 5.10 1.60 -8 2 0 1.50 2.00 -8 2 0 1.50 1.60 -9 -2 0 1.90 2.00 -9 -2 0 2.30 1.60 -9 -2 0 1.20 1.60 9 -2 0 1.70 1.60 -9 -2 0 0.50 1.80 -9 -2 0 4.30 1.80 -9 2 0 0.40 2.00 9 2 0 1.20 0.70 -9 2 0 1.30 1.70 9 2 0 2.50 1.50 -9 2 0 0.30 1.30 -9 2 0 1.40 1.60 -9 2 0 0.30 1.60 -10 -2 0 4.30 2.00 -10 -2 0 5.40 2.20 -10 -2 0 5.40 2.90 -10 -2 0 4.80 1.70 -10 -2 0 7.30 2.00 -10 -2 0 4.10 2.30 -10 2 0 7.50 1.90 -10 2 0 6.90 2.00 10 2 0 7.90 2.90 -10 2 0 4.30 2.50 10 2 0 4.60 1.60 -10 2 0 7.50 2.20 -10 2 0 6.10 2.00 11 -2 0 2.50 2.00 -11 -2 0 1.30 2.20 -11 -2 0 3.70 1.80 -11 -2 0 1.90 2.00 -11 -2 0 3.50 1.70 -11 -2 0 1.10 3.00 -11 2 0 3.40 1.70 -11 2 0 -1.20 2.20 -11 2 0 3.30 2.00 -11 2 0 4.00 1.90 -11 2 0 3.40 2.00 0 -3 0 0.70 0.90 0 -3 0 1.70 1.10 0 -3 0 -1.70 1.00 0 -3 0 -0.80 1.10 0 3 0 -1.10 0.90 0 3 0 0.30 1.00 0 3 0 1.00 0.90 0 3 0 0.20 1.00 0 3 0 -0.50 0.90 -1 -3 0 69.99 2.30 1 -3 0 68.89 2.30 -1 -3 0 72.09 2.30 1 -3 0 72.99 2.20 1 -3 0 71.59 2.80 -1 -3 0 72.09 2.20 1 -3 0 73.39 2.60 1 -3 0 75.39 2.30 -1 -3 0 74.59 2.70 -1 -3 0 75.39 2.50 -1 3 0 71.99 2.30 -1 3 0 74.39 2.20 -1 3 0 73.59 2.90 -1 3 0 72.19 2.20 1 3 0 74.39 2.40 1 3 0 69.09 2.20 1 3 0 71.99 2.30 1 3 0 70.89 2.60 -1 3 0 75.99 2.70 -2 -3 0 7.10 1.40 -2 -3 0 5.90 1.10 2 -3 0 4.70 1.00 2 -3 0 4.70 0.70 -2 -3 0 5.10 1.20 2 -3 0 5.40 1.00 -2 -3 0 5.90 1.20 -2 -3 0 2.70 1.00 2 -3 0 2.10 1.10 -2 3 0 1.90 1.10 -2 3 0 3.80 1.00 -2 3 0 4.80 1.00 2 3 0 4.80 1.10 2 3 0 5.30 1.10 -2 3 0 4.30 1.00 -2 3 0 4.50 1.20 2 3 0 4.60 1.10 2 3 0 3.40 1.10 2 3 0 3.10 1.10 -3 -3 0 170.58 4.80 3 -3 0 171.58 4.70 -3 -3 0 167.78 4.00 3 -3 0 173.98 3.70 3 -3 0 176.38 3.70 3 -3 0 172.18 3.80 -3 -3 0 172.28 4.30 3 3 0 168.88 4.30 3 3 0 171.08 4.20 3 3 0 168.98 3.90 -3 3 0 167.78 3.70 3 3 0 167.38 3.90 -3 3 0 171.58 3.90 -3 3 0 176.18 4.80 -3 3 0 171.68 4.00 -4 -3 0 180.38 4.50 -4 -3 0 187.88 4.90 -4 -3 0 187.48 4.50 4 -3 0 181.98 4.20 -4 -3 0 179.18 4.30 4 -3 0 186.88 5.40 -4 -3 0 197.58 5.80 4 -3 0 181.28 4.00 4 -3 0 179.48 4.00 4 3 0 181.58 4.10 4 3 0 179.78 4.50 -4 3 0 180.08 4.30 -4 3 0 186.08 5.40 4 3 0 173.58 4.50 -4 3 0 182.18 4.30 4 3 0 183.98 4.80 -4 3 0 189.18 4.40 -5 -3 0 12.60 2.10 -5 -3 0 14.30 1.60 5 -3 0 14.40 1.30 5 -3 0 10.10 1.40 -5 -3 0 12.60 1.60 -5 -3 0 12.70 1.70 5 -3 0 14.50 1.30 5 -3 0 11.50 1.90 -5 -3 0 10.40 1.50 -5 3 0 12.20 1.50 5 3 0 12.90 1.40 5 3 0 12.80 1.40 5 3 0 11.00 1.50 -5 3 0 14.10 1.60 -5 3 0 10.80 1.90 5 3 0 15.30 1.90 -5 3 0 10.20 1.40 -5 3 0 9.10 1.60 6 -3 0 21.40 2.50 -6 -3 0 27.80 2.50 6 -3 0 25.00 1.60 6 -3 0 26.50 2.10 6 -3 0 25.40 1.60 -6 -3 0 22.90 2.10 -6 -3 0 24.50 2.10 -6 -3 0 27.70 3.40 -6 -3 0 26.00 2.20 6 3 0 21.60 1.70 -6 3 0 25.70 2.80 6 3 0 27.10 2.60 -6 3 0 24.30 2.10 -6 3 0 28.40 2.10 6 3 0 25.40 2.20 -6 3 0 22.50 2.10 6 3 0 26.30 1.90 -6 3 0 25.70 2.00 7 -3 0 4.70 1.00 7 -3 0 4.50 1.90 -7 -3 0 3.80 1.50 7 -3 0 5.60 1.10 -7 -3 0 1.60 2.10 7 -3 0 5.50 1.50 -7 -3 0 9.10 2.00 -7 -3 0 4.80 1.50 -7 -3 0 2.20 1.50 -7 3 0 1.60 1.40 7 3 0 6.10 1.20 7 3 0 6.20 1.80 -7 3 0 4.60 1.40 -7 3 0 5.20 1.50 -7 3 0 4.50 1.50 7 3 0 4.70 1.20 -7 3 0 3.10 1.90 -8 -3 0 15.90 2.20 -8 -3 0 14.10 2.70 8 -3 0 15.90 2.70 -8 -3 0 12.00 3.00 8 -3 0 17.60 1.30 -8 -3 0 15.50 2.10 -8 -3 0 23.90 2.90 -8 3 0 15.40 2.10 8 3 0 17.50 1.80 -8 3 0 18.70 2.20 8 3 0 13.40 2.00 -8 3 0 15.40 2.70 -8 3 0 19.10 2.20 8 3 0 14.60 2.50 -8 3 0 15.20 2.10 -9 -3 0 0.50 2.00 -9 -3 0 -3.20 2.10 -9 -3 0 -1.10 1.60 -9 -3 0 2.40 2.10 9 -3 0 0.60 1.50 -9 -3 0 2.40 1.60 -9 3 0 2.00 1.70 9 3 0 2.30 0.90 -9 3 0 2.70 2.20 9 3 0 0.90 1.90 -9 3 0 -0.40 1.60 9 3 0 1.10 0.90 -9 3 0 0.60 1.50 9 3 0 0.70 1.40 -10 -3 0 7.40 1.90 -10 -3 0 3.60 2.00 -10 -3 0 6.00 2.50 -10 -3 0 2.90 2.30 -10 -3 0 1.70 2.60 -10 -3 0 4.10 1.90 10 3 0 2.30 2.00 -10 3 0 4.80 2.00 -10 3 0 5.40 2.50 -10 3 0 4.20 1.70 10 3 0 4.30 1.60 -10 3 0 5.50 2.00 -10 3 0 2.70 1.80 -11 -3 0 1.30 2.30 -11 -3 0 -1.40 2.00 -11 -3 0 -2.40 2.40 -11 -3 0 -1.20 2.00 11 -3 0 -2.40 2.50 -11 -3 0 2.50 1.70 -11 3 0 2.40 1.60 -11 3 0 -2.30 1.50 -11 3 0 0.50 1.50 11 3 0 0.30 1.40 -11 3 0 3.80 2.50 0 -4 0 2133.39 55.19 0 4 0 2127.19 55.39 1 -4 0 996.70 15.90 -1 -4 0 923.71 16.40 -1 -4 0 971.70 15.80 1 -4 0 972.40 16.50 1 -4 0 957.50 16.90 -1 -4 0 946.71 16.10 -1 -4 0 943.21 16.50 -1 -4 0 958.80 15.90 1 -4 0 961.40 15.80 1 -4 0 936.41 16.00 1 4 0 940.41 16.40 -1 4 0 993.40 17.00 1 4 0 961.10 15.90 -1 4 0 1012.40 18.80 1 4 0 952.30 16.10 -1 4 0 962.60 16.60 1 4 0 929.71 16.50 -1 4 0 936.71 15.80 2 -4 0 1.50 0.70 -2 -4 0 3.40 1.00 -2 -4 0 1.10 1.20 -2 -4 0 2.00 1.10 2 -4 0 2.10 1.00 2 -4 0 1.10 1.10 2 -4 0 0.20 1.00 -2 -4 0 0.00 1.00 -2 -4 0 2.10 1.10 2 4 0 1.30 1.00 2 4 0 1.70 1.10 -2 4 0 0.70 1.00 2 4 0 0.60 1.20 -2 4 0 2.00 1.10 2 4 0 0.00 1.10 -2 4 0 1.70 1.20 -2 4 0 2.50 1.10 2 4 0 1.20 1.00 -2 4 0 2.10 1.20 3 -4 0 28.00 2.10 -3 -4 0 27.90 1.90 3 -4 0 30.60 2.40 3 -4 0 29.30 1.60 3 -4 0 28.20 1.70 -3 -4 0 29.70 2.10 -3 -4 0 27.40 2.10 -3 -4 0 32.80 2.10 -3 4 0 31.10 2.00 3 4 0 30.40 1.90 -3 4 0 27.70 2.00 -3 4 0 31.50 2.80 -3 4 0 31.80 2.50 3 4 0 28.10 2.10 3 4 0 30.50 2.10 3 4 0 31.10 1.90 -3 4 0 29.50 1.90 -4 -4 0 51.29 2.70 -4 -4 0 42.90 3.40 -4 -4 0 53.29 2.40 -4 -4 0 52.59 2.50 -4 -4 0 50.59 2.50 4 -4 0 51.99 2.10 4 -4 0 52.19 3.00 4 -4 0 49.90 2.10 4 4 0 52.89 2.70 -4 4 0 49.60 2.20 -4 4 0 49.80 2.40 -4 4 0 53.39 2.40 4 4 0 53.19 2.30 4 4 0 49.90 2.50 -4 4 0 46.10 2.90 4 4 0 51.59 2.30 -5 -4 0 187.18 4.80 5 -4 0 183.98 4.60 -5 -4 0 190.38 4.90 5 -4 0 186.78 5.80 -5 -4 0 181.58 5.00 -5 -4 0 180.58 6.00 -5 -4 0 189.58 5.40 5 -4 0 181.38 4.30 5 -4 0 183.98 4.60 -5 4 0 183.58 4.70 -5 4 0 181.48 4.70 5 4 0 190.98 5.90 5 4 0 192.08 5.40 5 4 0 184.58 4.50 -5 4 0 184.18 5.90 5 4 0 190.38 4.50 -5 4 0 178.38 4.80 -5 4 0 187.28 4.60 6 -4 0 17.70 1.60 6 -4 0 18.60 2.20 -6 -4 0 14.40 2.30 -6 -4 0 18.90 2.10 -6 -4 0 21.10 2.10 -6 -4 0 21.90 2.20 -6 -4 0 22.80 2.40 6 -4 0 22.70 2.00 -6 4 0 15.80 2.40 -6 4 0 19.70 1.90 -6 4 0 14.90 1.80 -6 4 0 19.80 2.00 6 4 0 19.80 3.40 6 4 0 19.50 2.10 6 4 0 18.70 1.90 6 4 0 20.00 1.70 -6 4 0 13.10 1.80 7 -4 0 9.50 1.70 -7 -4 0 9.90 1.80 7 -4 0 6.90 2.10 -7 -4 0 8.40 1.90 -7 -4 0 7.00 2.40 -7 -4 0 8.60 2.20 -7 4 0 9.00 1.70 -7 4 0 9.10 1.80 -7 4 0 7.00 1.50 -7 4 0 10.00 1.80 7 4 0 10.90 1.50 -7 4 0 5.70 2.10 7 4 0 9.00 2.10 7 4 0 6.80 1.70 7 4 0 10.20 1.50 -8 -4 0 12.00 2.80 8 -4 0 18.30 1.50 8 -4 0 13.40 1.20 -8 -4 0 14.50 2.20 -8 -4 0 19.90 2.50 8 -4 0 15.50 2.40 -8 -4 0 18.80 2.30 -8 -4 0 17.50 2.70 -8 4 0 14.10 2.80 8 4 0 15.80 1.70 -8 4 0 18.30 3.30 -8 4 0 12.10 1.90 8 4 0 14.80 2.10 -8 4 0 15.50 2.20 -8 4 0 15.50 2.10 8 4 0 15.30 1.60 -9 -4 0 0.00 2.00 -9 -4 0 3.20 1.80 -9 -4 0 -3.60 1.70 -9 -4 0 -0.10 1.50 -9 -4 0 1.10 1.80 9 -4 0 1.00 1.30 -9 -4 0 3.10 1.70 -9 4 0 0.30 1.40 -9 4 0 -2.10 1.50 9 4 0 -0.50 1.40 -9 4 0 -2.70 1.40 9 4 0 -0.50 1.00 -9 4 0 2.80 2.30 -9 4 0 -0.20 2.40 9 4 0 -0.40 1.80 -10 -4 0 1.90 1.90 -10 -4 0 5.80 2.50 -10 -4 0 2.30 2.00 -10 -4 0 2.90 1.80 -10 -4 0 -0.80 2.20 -10 -4 0 0.50 2.20 -10 4 0 7.80 2.00 10 4 0 3.30 2.10 -10 4 0 3.40 1.80 -10 4 0 5.50 2.60 -10 4 0 5.60 1.80 10 4 0 3.10 1.70 -10 4 0 1.50 1.80 0 -5 0 0.10 1.10 0 -5 0 0.50 1.10 0 -5 0 -1.20 1.20 0 -5 0 0.50 1.10 0 -5 0 -0.60 1.00 0 5 0 0.70 1.20 0 5 0 -0.70 1.80 0 5 0 -1.40 1.00 0 5 0 -1.20 1.20 0 5 0 0.30 1.10 -1 -5 0 14.10 1.60 1 -5 0 18.20 1.70 -1 -5 0 17.40 1.80 1 -5 0 16.60 1.80 -1 -5 0 15.10 1.80 1 -5 0 16.80 1.70 1 -5 0 13.60 1.80 -1 -5 0 15.00 2.00 1 -5 0 16.70 1.70 -1 -5 0 14.20 1.70 -1 5 0 14.30 1.80 -1 5 0 16.00 1.80 -1 5 0 15.60 1.70 -1 5 0 17.30 1.60 1 5 0 14.50 1.60 1 5 0 16.60 1.70 1 5 0 16.40 1.60 1 5 0 15.50 2.00 -1 5 0 15.50 1.60 -2 -5 0 553.04 10.70 -2 -5 0 522.45 9.90 2 -5 0 525.05 9.70 2 -5 0 552.54 10.90 2 -5 0 519.45 9.70 -2 -5 0 520.85 9.90 -2 -5 0 527.65 10.10 -2 -5 0 520.25 9.90 -2 5 0 537.85 10.10 2 5 0 538.05 10.20 -2 5 0 536.15 9.90 -2 5 0 566.84 10.90 2 5 0 514.25 9.80 -2 5 0 551.54 11.40 -2 5 0 520.65 9.90 2 5 0 522.15 9.90 -3 -5 0 272.57 6.20 3 -5 0 266.27 6.80 3 -5 0 266.17 5.70 -3 -5 0 265.07 6.20 -3 -5 0 270.97 6.80 3 -5 0 267.17 5.70 3 -5 0 268.57 5.30 -3 -5 0 261.97 6.10 -3 -5 0 275.17 6.10 -3 5 0 264.57 5.90 3 5 0 262.07 5.80 -3 5 0 263.67 5.90 -3 5 0 274.57 7.50 3 5 0 260.57 5.80 3 5 0 279.17 7.00 3 5 0 273.17 6.30 3 5 0 265.47 6.20 -3 5 0 255.97 6.00 -3 5 0 267.17 6.90 -4 -5 0 13.40 1.80 4 -5 0 10.70 1.80 4 -5 0 14.60 1.50 -4 -5 0 13.70 1.70 4 -5 0 16.60 1.70 -4 -5 0 13.50 1.90 4 -5 0 13.80 1.30 -4 -5 0 16.80 1.90 -4 -5 0 13.70 1.80 4 5 0 15.40 1.70 -4 5 0 17.40 1.90 -4 5 0 15.60 1.80 4 5 0 13.90 1.50 -4 5 0 17.50 1.70 4 5 0 18.10 2.00 4 5 0 17.10 2.00 -4 5 0 12.90 2.00 -4 5 0 11.60 2.00 5 -5 0 38.30 2.00 -5 -5 0 36.80 2.60 5 -5 0 40.50 2.20 -5 -5 0 38.10 2.60 5 -5 0 40.70 2.10 5 -5 0 36.20 3.00 -5 -5 0 37.70 2.60 -5 -5 0 36.60 3.40 -5 -5 0 39.10 2.80 -5 5 0 34.70 2.40 -5 5 0 40.70 2.60 5 5 0 38.20 2.70 5 5 0 40.30 2.30 5 5 0 34.70 2.20 5 5 0 39.30 2.60 -5 5 0 35.40 3.10 -6 -5 0 -0.40 1.40 6 -5 0 2.60 1.10 -6 -5 0 2.00 1.60 -6 -5 0 2.80 1.50 -6 -5 0 0.80 2.00 6 -5 0 0.80 1.60 -6 -5 0 2.70 1.50 6 -5 0 0.70 1.00 6 -5 0 -0.60 1.00 -6 5 0 3.30 1.20 6 5 0 1.40 1.20 -6 5 0 1.50 1.50 -6 5 0 4.10 1.60 6 5 0 3.00 1.40 -6 5 0 2.00 1.40 -6 5 0 1.00 1.70 6 5 0 0.00 1.20 6 5 0 0.40 1.40 7 -5 0 4.60 2.00 -7 -5 0 2.80 1.90 7 -5 0 5.60 1.20 -7 -5 0 5.60 1.70 7 -5 0 4.40 1.20 -7 -5 0 2.80 1.80 7 -5 0 3.50 1.40 -7 -5 0 0.40 3.40 -7 -5 0 3.30 1.60 7 5 0 4.30 1.40 7 5 0 8.30 1.90 7 5 0 3.80 1.50 -7 5 0 3.80 2.00 -7 5 0 1.60 1.30 -7 5 0 2.70 1.60 -7 5 0 0.90 1.50 -7 5 0 9.60 1.90 -8 -5 0 2.40 2.00 -8 -5 0 -3.10 1.70 -8 -5 0 -0.20 1.60 -8 -5 0 -4.30 2.00 8 -5 0 -1.80 1.20 8 5 0 -0.90 1.50 -8 5 0 0.80 1.30 -8 5 0 -1.80 1.80 8 5 0 -0.20 1.20 8 5 0 -1.20 1.30 -8 5 0 0.00 1.60 -8 5 0 -0.90 1.40 -8 5 0 -0.10 1.50 -9 -5 0 -2.40 2.00 9 -5 0 0.00 1.40 -9 -5 0 0.70 1.70 -9 -5 0 0.70 1.70 -9 -5 0 -1.20 1.80 -9 -5 0 5.30 2.40 9 -5 0 1.00 0.90 9 -5 0 0.70 2.30 -9 -5 0 1.10 2.10 9 5 0 -0.70 1.10 -9 5 0 -1.80 1.30 -9 5 0 0.70 1.60 9 5 0 1.50 2.40 -9 5 0 0.90 1.60 -9 5 0 -1.70 1.80 9 5 0 0.40 1.50 -9 5 0 0.30 1.60 9 5 0 1.10 1.10 -10 -5 0 1.90 3.20 10 -5 0 -0.80 1.10 -10 -5 0 -1.00 1.70 -10 -5 0 -1.70 1.90 -10 -5 0 2.40 1.90 10 5 0 1.90 1.00 -10 5 0 3.20 1.70 10 5 0 1.30 1.60 -10 5 0 2.50 1.80 -10 5 0 -0.50 1.60 -10 5 0 3.00 3.80 -10 5 0 2.90 1.90 0 -6 0 156.48 5.00 0 -6 0 158.28 4.30 0 -6 0 146.89 4.20 0 -6 0 156.18 4.90 0 -6 0 155.88 4.50 0 6 0 162.38 4.50 0 6 0 157.08 4.40 0 6 0 158.98 4.40 0 6 0 159.48 5.00 0 6 0 150.28 4.90 -1 -6 0 18.60 2.20 -1 -6 0 18.00 1.70 1 -6 0 20.10 1.80 -1 -6 0 19.00 1.80 -1 -6 0 21.00 2.30 1 -6 0 18.00 1.80 -1 -6 0 17.20 1.90 1 -6 0 15.90 2.00 1 -6 0 18.30 2.40 1 -6 0 18.40 1.90 -1 -6 0 22.70 2.10 1 6 0 19.10 1.80 1 6 0 21.40 2.10 -1 6 0 22.40 2.10 -1 6 0 19.10 2.00 -1 6 0 13.90 1.80 -1 6 0 20.20 1.90 -1 6 0 17.50 2.00 1 6 0 18.20 1.90 1 6 0 21.00 2.40 2 -6 0 44.40 2.40 -2 -6 0 45.60 3.40 2 -6 0 47.20 2.30 -2 -6 0 45.90 3.00 -2 -6 0 49.30 2.50 -2 -6 0 46.10 2.50 -2 -6 0 44.80 2.70 2 -6 0 44.80 2.90 -2 -6 0 46.80 2.70 -2 6 0 55.59 3.40 -2 6 0 51.39 2.60 2 6 0 48.50 2.60 -2 6 0 52.09 2.60 2 6 0 45.50 2.40 -2 6 0 45.50 3.30 -2 6 0 46.80 2.40 2 6 0 41.60 2.50 -3 -6 0 9.70 1.70 -3 -6 0 11.80 1.70 3 -6 0 10.40 1.80 -3 -6 0 9.60 1.60 -3 -6 0 9.80 1.60 3 -6 0 12.10 1.20 -3 -6 0 7.10 1.50 3 -6 0 11.90 1.60 3 -6 0 12.90 1.60 3 6 0 10.90 1.70 -3 6 0 11.70 1.70 3 6 0 10.00 1.80 -3 6 0 10.70 1.60 -3 6 0 11.70 2.00 3 6 0 12.70 1.90 -3 6 0 8.10 1.80 -3 6 0 11.20 1.60 4 -6 0 221.28 4.90 4 -6 0 218.68 5.30 4 -6 0 221.78 6.60 -4 -6 0 232.78 5.90 -4 -6 0 221.68 6.00 -4 -6 0 222.58 6.60 4 -6 0 220.38 5.30 -4 -6 0 234.88 5.90 -4 -6 0 217.08 5.90 4 6 0 223.68 6.70 -4 6 0 225.08 5.70 -4 6 0 222.08 5.80 -4 6 0 224.98 5.70 -4 6 0 228.68 7.40 4 6 0 226.18 6.10 4 6 0 220.58 5.90 -4 6 0 220.08 6.60 4 6 0 229.48 5.60 4 6 0 223.58 5.50 -5 -6 0 165.68 5.10 5 -6 0 168.78 7.00 5 -6 0 170.98 4.30 5 -6 0 173.38 4.50 -5 -6 0 164.88 6.00 5 -6 0 160.78 4.40 -5 -6 0 162.38 5.10 -5 -6 0 167.98 5.40 -5 -6 0 163.98 5.10 -5 6 0 176.58 5.00 -5 6 0 169.38 5.00 -5 6 0 158.28 6.60 5 6 0 168.98 4.70 -5 6 0 170.38 6.10 5 6 0 170.08 4.70 5 6 0 141.19 7.10 -5 6 0 170.58 5.00 5 6 0 162.68 5.10 6 -6 0 49.70 2.60 -6 -6 0 49.40 3.20 -6 -6 0 59.59 3.80 6 -6 0 54.59 2.60 -6 -6 0 45.90 4.00 -6 -6 0 51.89 3.40 -6 -6 0 51.19 3.30 6 -6 0 50.29 3.70 6 -6 0 48.50 2.50 -6 6 0 54.59 3.10 -6 6 0 50.59 3.10 6 6 0 49.90 3.30 -6 6 0 55.29 4.00 6 6 0 53.59 2.80 -6 6 0 51.69 4.60 6 6 0 48.00 2.80 6 6 0 56.79 3.50 -6 6 0 48.30 3.10 7 -6 0 1.00 1.20 7 -6 0 1.50 1.70 -7 -6 0 1.50 1.80 -7 -6 0 0.40 1.50 7 -6 0 0.80 1.20 -7 -6 0 -0.30 1.80 -7 -6 0 -4.10 2.10 -7 -6 0 0.80 1.50 7 -6 0 0.90 1.20 -7 6 0 -0.90 1.80 7 6 0 1.10 1.30 -7 6 0 -0.60 1.50 -7 6 0 0.50 1.50 -7 6 0 0.90 1.80 -7 6 0 -0.10 1.50 -7 6 0 2.50 2.20 7 6 0 -1.30 1.40 7 6 0 0.30 1.50 -8 -6 0 1.90 1.80 -8 -6 0 3.30 1.80 -8 -6 0 2.20 1.90 8 -6 0 2.10 1.00 -8 -6 0 0.50 1.70 8 -6 0 1.30 1.90 8 -6 0 -0.30 1.30 -8 -6 0 -2.10 1.90 8 -6 0 2.00 1.10 8 6 0 0.90 1.30 -8 6 0 2.30 1.90 -8 6 0 2.00 1.50 -8 6 0 1.00 2.00 8 6 0 -1.00 1.60 -8 6 0 1.10 1.70 -8 6 0 3.10 1.40 -8 6 0 2.80 2.20 -8 6 0 1.00 1.50 8 6 0 2.70 1.50 9 -6 0 9.10 1.70 -9 -6 0 7.40 2.00 -9 -6 0 11.20 2.60 -9 -6 0 5.20 2.20 -9 -6 0 4.10 2.50 9 -6 0 8.70 2.60 9 -6 0 9.10 0.90 -9 -6 0 8.10 2.50 9 6 0 15.10 2.50 -9 6 0 4.80 2.60 9 6 0 8.00 1.50 -9 6 0 8.80 1.90 -9 6 0 6.90 2.10 -9 6 0 7.50 2.60 9 6 0 4.40 2.30 -9 6 0 8.30 1.90 -9 6 0 7.60 2.10 9 6 0 5.20 1.40 -9 6 0 10.00 2.30 -10 -6 0 2.20 2.50 -10 -6 0 3.50 1.80 -10 -6 0 1.70 2.30 10 -6 0 1.50 1.30 -10 -6 0 4.60 2.20 -10 -6 0 -6.10 4.30 -10 -6 0 0.40 1.80 -10 6 0 1.60 2.30 -10 6 0 1.10 1.60 10 6 0 3.30 1.70 -10 6 0 6.50 2.00 -10 6 0 0.70 1.90 -10 6 0 4.40 1.70 -10 6 0 3.10 2.70 -10 6 0 0.50 1.70 10 6 0 1.90 1.70 10 6 0 2.90 1.00 0 -7 0 0.10 1.20 0 -7 0 -0.20 1.30 0 -7 0 -0.30 1.20 0 -7 0 1.00 1.30 0 -7 0 1.20 1.20 0 -7 0 0.60 0.90 0 7 0 -0.70 1.20 0 7 0 1.70 1.30 0 7 0 -1.00 1.30 0 7 0 2.50 1.20 1 -7 0 65.09 3.20 -1 -7 0 67.29 3.60 1 -7 0 64.49 2.90 -1 -7 0 67.29 3.20 -1 -7 0 59.09 3.40 -1 -7 0 66.39 2.70 -1 -7 0 63.59 3.00 1 -7 0 70.39 3.80 -1 -7 0 63.99 2.90 1 -7 0 72.79 3.00 1 -7 0 62.79 3.30 -1 7 0 67.29 3.00 -1 7 0 68.09 3.70 -1 7 0 65.79 3.10 -1 7 0 63.99 3.70 1 7 0 62.99 3.00 1 7 0 58.49 2.90 1 7 0 69.19 3.20 1 7 0 67.39 3.60 -1 7 0 66.89 3.10 2 -7 0 150.88 4.50 -2 -7 0 152.58 4.60 -2 -7 0 148.79 5.40 -2 -7 0 151.38 4.60 2 -7 0 157.58 5.30 2 -7 0 150.38 4.40 -2 -7 0 157.08 5.20 -2 -7 0 152.38 4.50 -2 -7 0 144.89 4.80 2 7 0 148.69 5.20 2 7 0 151.38 4.80 -2 7 0 154.48 4.50 -2 7 0 150.88 4.70 -2 7 0 147.49 5.20 2 7 0 150.88 4.50 2 7 0 160.58 4.70 -2 7 0 159.68 4.70 -2 7 0 150.48 5.70 -3 -7 0 0.10 1.30 3 -7 0 0.20 1.40 -3 -7 0 -1.30 1.40 3 -7 0 -1.20 1.20 3 -7 0 -1.10 0.80 3 -7 0 0.20 1.30 -3 -7 0 0.40 1.40 -3 -7 0 0.70 1.30 -3 -7 0 -0.70 1.40 -3 7 0 -0.40 1.30 3 7 0 0.90 1.40 -3 7 0 -1.30 1.40 -3 7 0 1.70 1.60 -3 7 0 -1.10 1.40 3 7 0 -0.40 1.40 3 7 0 -0.40 1.50 3 7 0 0.90 1.50 -3 7 0 -0.80 1.20 -4 -7 0 15.20 2.10 -4 -7 0 15.50 2.10 4 -7 0 15.70 1.60 -4 -7 0 20.60 2.40 4 -7 0 19.40 2.00 -4 -7 0 17.70 2.20 4 -7 0 16.80 3.90 -4 -7 0 13.60 2.10 4 -7 0 16.70 1.90 -4 7 0 22.80 2.40 -4 7 0 14.90 2.40 -4 7 0 17.00 2.20 -4 7 0 16.90 2.70 4 7 0 14.60 2.10 4 7 0 16.10 2.10 -4 7 0 18.20 2.30 4 7 0 19.70 2.00 4 7 0 15.70 2.30 -5 -7 0 44.20 3.00 -5 -7 0 49.90 3.80 5 -7 0 52.29 2.40 -5 -7 0 48.10 3.20 -5 -7 0 51.09 3.30 -5 -7 0 51.19 3.10 5 -7 0 49.00 3.60 5 -7 0 48.10 2.80 5 -7 0 46.30 2.60 5 7 0 48.00 3.20 -5 7 0 46.00 3.20 5 7 0 51.69 3.00 -5 7 0 45.20 3.10 5 7 0 58.29 3.10 -5 7 0 52.09 3.00 -5 7 0 48.10 3.80 5 7 0 46.80 3.30 -5 7 0 47.60 4.40 -6 -7 0 18.00 2.40 6 -7 0 18.50 2.70 -6 -7 0 17.20 2.50 -6 -7 0 12.00 2.50 6 -7 0 19.70 1.90 -6 -7 0 20.40 2.70 6 -7 0 19.80 2.00 -6 -7 0 18.00 2.50 6 -7 0 22.40 2.10 -6 7 0 20.00 2.30 6 7 0 22.20 2.90 6 7 0 16.90 2.10 -6 7 0 14.80 2.80 -6 7 0 18.60 2.80 6 7 0 19.50 2.20 -6 7 0 18.50 2.40 6 7 0 21.00 2.60 -6 7 0 15.70 3.00 7 -7 0 8.50 1.60 -7 -7 0 14.10 2.50 -7 -7 0 8.50 2.80 7 -7 0 9.70 1.60 -7 -7 0 7.80 2.20 -7 -7 0 8.50 2.30 -7 -7 0 7.70 2.00 7 -7 0 11.10 1.60 -7 7 0 9.10 2.10 7 7 0 8.90 2.20 -7 7 0 10.10 2.10 7 7 0 9.70 1.90 -7 7 0 6.50 2.40 7 7 0 11.20 1.90 -7 7 0 10.40 2.80 -7 7 0 8.80 2.10 7 7 0 7.40 2.00 8 -7 0 1.10 1.20 8 -7 0 3.00 1.20 -8 -7 0 3.20 2.00 -8 -7 0 2.60 2.40 -8 -7 0 3.80 2.00 -8 -7 0 5.00 2.20 8 -7 0 6.10 2.70 -8 -7 0 0.50 1.70 8 -7 0 3.20 1.40 -8 7 0 1.80 1.80 8 7 0 3.60 1.90 8 7 0 3.50 1.60 -8 7 0 1.50 2.20 -8 7 0 1.00 2.10 8 7 0 1.20 1.60 -8 7 0 6.00 2.10 -8 7 0 2.90 1.70 -8 7 0 5.30 1.70 -9 -7 0 3.00 2.30 9 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0.90 1.60 2 8 0 -0.10 1.30 -2 8 0 1.00 1.50 -2 8 0 0.80 1.50 -2 8 0 0.30 1.60 -2 8 0 2.10 1.40 2 8 0 -1.30 1.30 3 -8 0 141.99 4.60 -3 -8 0 152.18 5.70 -3 -8 0 141.19 4.80 -3 -8 0 142.09 5.50 3 -8 0 145.09 4.60 -3 -8 0 145.59 4.80 -3 -8 0 141.79 5.70 3 -8 0 141.69 3.70 -3 -8 0 144.39 5.10 3 -8 0 147.49 5.70 -3 8 0 141.99 6.00 3 8 0 141.09 5.60 3 8 0 142.69 4.70 -3 8 0 132.69 5.50 3 8 0 141.39 4.70 -3 8 0 145.09 5.00 3 8 0 153.88 5.20 -3 8 0 139.59 4.90 -3 8 0 136.89 4.70 -4 -8 0 23.50 2.60 -4 -8 0 22.70 2.50 4 -8 0 20.80 2.20 -4 -8 0 18.60 2.50 4 -8 0 18.10 2.10 -4 -8 0 20.10 2.60 -4 -8 0 19.80 2.50 4 -8 0 16.80 1.70 4 8 0 17.40 2.40 -4 8 0 18.20 2.30 -4 8 0 19.70 2.40 -4 8 0 16.00 2.20 4 8 0 22.30 2.50 -4 8 0 13.00 2.50 4 8 0 24.20 2.50 4 8 0 16.70 2.60 -4 8 0 18.90 2.90 5 -8 0 237.98 6.10 -5 -8 0 245.18 7.90 5 -8 0 237.28 5.50 5 -8 0 242.18 6.20 5 -8 0 233.08 7.80 -5 -8 0 259.07 8.30 -5 -8 0 235.68 6.90 -5 -8 0 244.48 7.00 -5 -8 0 240.28 7.60 -5 8 0 237.68 6.60 5 8 0 236.88 6.40 -5 8 0 235.98 6.70 5 8 0 253.37 7.10 -5 8 0 229.28 6.90 -5 8 0 232.88 12.80 -5 8 0 243.48 8.30 -6 -8 0 44.20 3.50 -6 -8 0 38.10 3.20 -6 -8 0 44.10 3.60 -6 -8 0 39.50 3.50 -6 -8 0 36.90 4.30 6 -8 0 39.30 2.70 6 -8 0 39.40 2.40 6 -8 0 41.00 2.80 -6 8 0 38.10 4.00 -6 8 0 42.80 3.30 -6 8 0 41.20 3.20 6 8 0 40.10 2.90 -6 8 0 36.40 3.50 6 8 0 47.70 3.10 6 8 0 41.40 3.30 -6 8 0 41.80 4.80 -7 -8 0 5.10 2.00 7 -8 0 6.40 1.60 7 -8 0 5.00 2.30 -7 -8 0 1.10 2.00 7 -8 0 4.70 1.60 -7 -8 0 2.90 2.20 -7 -8 0 7.30 2.20 -7 -8 0 9.40 2.30 7 -8 0 4.60 1.40 7 8 0 6.00 1.80 -7 8 0 10.20 2.20 -7 8 0 4.80 2.00 -7 8 0 3.80 2.40 7 8 0 9.90 2.00 -7 8 0 3.40 2.30 -7 8 0 5.80 2.20 7 8 0 2.70 2.00 -8 -8 0 9.10 2.50 -8 -8 0 11.70 2.60 -8 -8 0 4.30 2.20 -8 -8 0 8.30 2.40 8 -8 0 8.20 1.50 8 -8 0 8.20 2.50 8 -8 0 5.60 1.40 -8 -8 0 6.60 2.60 8 -8 0 8.40 1.60 8 8 0 8.20 1.80 -8 8 0 12.30 2.30 -8 8 0 5.80 2.60 -8 8 0 8.00 2.00 -8 8 0 7.60 2.20 -8 8 0 11.80 2.40 -8 8 0 5.50 2.60 8 8 0 9.00 2.20 8 8 0 8.30 1.80 9 -8 0 0.60 1.20 -9 -8 0 3.30 2.20 -9 -8 0 -3.50 2.10 -9 -8 0 0.70 2.10 -9 -8 0 2.30 2.40 -9 8 0 -0.40 1.70 9 8 0 1.00 1.40 -9 8 0 2.60 1.80 -9 8 0 -0.60 2.20 -9 8 0 2.80 2.60 9 8 0 6.00 2.10 -9 8 0 4.00 2.00 0 -9 0 -0.90 1.00 0 -9 0 -2.90 1.30 0 -9 0 0.40 1.50 0 -9 0 -0.30 1.50 0 -9 0 3.60 1.80 0 9 0 -0.20 1.50 0 9 0 0.70 1.60 0 9 0 -1.40 1.40 0 9 0 0.50 1.30 -1 -9 0 1.20 1.60 -1 -9 0 1.30 1.60 1 -9 0 0.10 1.50 1 -9 0 0.00 1.70 -1 -9 0 -0.90 1.10 -1 -9 0 2.00 1.40 1 -9 0 -0.60 1.50 1 -9 0 0.30 1.60 -1 -9 0 0.20 1.40 1 -9 0 0.00 1.70 -1 9 0 -0.60 1.50 -1 9 0 1.30 1.50 -1 9 0 -2.70 1.40 -1 9 0 -0.20 1.90 -1 9 0 -0.10 1.60 1 9 0 -2.10 1.50 1 9 0 1.60 1.70 1 9 0 1.40 1.60 2 -9 0 0.40 1.60 -2 -9 0 5.00 2.40 2 -9 0 -1.60 1.30 -2 -9 0 1.30 1.50 -2 -9 0 -0.40 1.50 2 -9 0 3.40 1.80 -2 -9 0 0.10 1.50 -2 -9 0 0.90 1.60 -2 -9 0 0.50 1.30 2 9 0 1.00 1.50 -2 9 0 5.30 2.20 -2 9 0 1.80 1.70 2 9 0 -0.80 1.60 -2 9 0 -0.10 1.70 2 9 0 0.40 1.60 2 9 0 0.60 2.10 -2 9 0 -0.20 1.50 -2 9 0 0.50 1.70 3 -9 0 180.68 4.60 3 -9 0 187.18 5.60 3 -9 0 204.18 6.70 3 -9 0 187.88 6.60 -3 -9 0 194.38 6.10 -3 -9 0 193.98 5.80 -3 -9 0 193.28 7.10 -3 -9 0 190.68 5.90 -3 -9 0 194.48 6.30 -3 -9 0 179.18 6.50 -3 9 0 178.88 5.60 -3 9 0 191.88 7.00 3 9 0 182.08 6.10 3 9 0 182.18 5.60 -3 9 0 193.18 5.90 3 9 0 185.68 5.70 3 9 0 189.08 6.90 -3 9 0 184.78 7.30 -3 9 0 189.28 6.10 -4 -9 0 9.10 2.20 4 -9 0 6.90 2.20 -4 -9 0 10.30 2.30 4 -9 0 9.30 2.00 -4 -9 0 11.60 2.50 4 -9 0 9.70 2.30 -4 -9 0 9.80 2.00 -4 -9 0 8.10 2.20 4 -9 0 7.60 1.40 -4 -9 0 12.00 2.60 4 9 0 9.00 2.40 -4 9 0 4.70 2.30 4 9 0 7.70 2.30 4 9 0 11.10 2.20 -4 9 0 7.50 2.10 -4 9 0 9.00 2.90 4 9 0 8.70 2.20 -4 9 0 9.40 2.20 5 -9 0 0.70 2.40 5 -9 0 -0.10 1.30 -5 -9 0 2.00 2.00 5 -9 0 0.80 1.00 -5 -9 0 1.50 2.10 -5 -9 0 0.00 1.80 5 -9 0 2.20 1.60 -5 -9 0 0.50 1.60 -5 -9 0 0.10 2.20 -5 9 0 1.20 2.20 5 9 0 0.80 1.70 5 9 0 0.00 1.70 -5 9 0 -0.30 1.80 -5 9 0 3.70 1.80 5 9 0 1.70 1.90 -5 9 0 -0.70 1.60 -5 9 0 -0.60 2.00 6 -9 0 2.20 1.50 -6 -9 0 5.00 3.00 -6 -9 0 4.10 2.00 6 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96.49 3.80 1 -10 0 95.89 5.00 1 -10 0 96.39 4.20 1 -10 0 93.49 4.00 -1 -10 0 96.99 5.10 1 -10 0 95.89 3.50 -1 -10 0 85.69 4.10 -1 -10 0 91.39 6.60 -1 -10 0 90.29 4.50 1 -10 0 94.79 5.40 1 -10 0 95.99 4.40 1 10 0 91.19 6.70 1 10 0 91.49 4.40 1 10 0 89.59 4.10 1 10 0 98.49 5.50 -1 10 0 97.39 5.50 -1 10 0 107.79 8.30 -1 10 0 105.99 5.60 -2 -10 0 14.50 2.90 -2 -10 0 15.80 2.60 2 -10 0 15.10 2.60 2 -10 0 15.80 2.20 -2 -10 0 18.30 2.20 2 -10 0 17.00 2.50 -2 -10 0 19.60 2.60 -2 -10 0 15.50 2.50 -2 10 0 21.90 2.70 -2 10 0 13.00 2.90 -2 10 0 17.60 2.50 -2 10 0 21.90 2.70 -2 10 0 14.60 2.60 2 10 0 17.90 2.90 2 10 0 19.80 2.80 2 10 0 21.10 2.60 3 -10 0 128.99 3.90 -3 -10 0 127.39 4.90 -3 -10 0 131.09 5.80 3 -10 0 127.89 5.90 3 -10 0 129.49 4.70 -3 -10 0 125.59 5.30 3 -10 0 128.19 4.90 -3 -10 0 121.39 5.30 -3 10 0 135.39 5.10 3 10 0 125.39 5.30 3 10 0 118.29 5.90 -3 10 0 118.79 4.80 -3 10 0 125.09 5.30 -3 10 0 127.39 6.10 3 10 0 130.39 5.00 -3 10 0 144.99 8.10 -4 -10 0 27.50 3.10 4 -10 0 24.90 2.50 -4 -10 0 24.90 3.00 -4 -10 0 25.90 4.70 4 -10 0 31.40 2.90 4 -10 0 23.70 2.00 -4 -10 0 26.80 2.90 -4 -10 0 28.30 3.20 -4 10 0 28.20 3.20 4 10 0 26.60 2.80 -4 10 0 23.50 3.40 -4 10 0 27.00 3.00 4 10 0 22.80 3.00 -4 10 0 24.10 3.50 4 10 0 27.10 3.50 -4 10 0 25.10 3.10 4 10 0 27.00 3.00 -5 -10 0 4.30 2.20 -5 -10 0 0.20 2.20 5 -10 0 2.10 1.70 5 -10 0 2.70 1.70 -5 -10 0 -1.10 1.70 -5 -10 0 4.20 2.20 5 -10 0 2.00 2.10 -5 -10 0 2.10 2.00 -5 -10 0 2.10 2.00 -5 10 0 3.30 2.00 -5 10 0 2.30 2.30 -5 10 0 -0.90 1.80 5 10 0 -0.50 1.50 5 10 0 -0.10 1.80 -5 10 0 2.00 1.80 5 10 0 3.10 2.20 -5 10 0 0.60 2.20 5 10 0 3.50 1.90 -6 -10 0 4.20 2.20 6 -10 0 1.70 3.30 -6 -10 0 8.70 2.40 -6 -10 0 6.30 2.30 6 -10 0 5.70 1.70 6 -10 0 3.70 1.10 6 -10 0 7.40 1.90 -6 -10 0 7.90 2.40 -6 -10 0 12.40 2.60 6 10 0 6.10 2.10 -6 10 0 4.00 2.60 -6 10 0 3.40 2.10 -6 10 0 4.70 2.50 6 10 0 4.60 1.80 -6 10 0 3.80 2.10 6 10 0 8.00 2.10 -6 10 0 3.00 1.90 7 -10 0 1.30 2.10 -7 -10 0 -0.30 2.10 7 -10 0 -1.00 1.00 -7 -10 0 2.80 2.10 -7 -10 0 -2.90 1.70 -7 -10 0 -3.10 1.80 -7 -10 0 -2.00 1.70 7 -10 0 2.20 1.60 7 -10 0 1.90 1.40 -7 10 0 0.30 2.40 7 10 0 -1.20 2.20 -7 10 0 -1.30 2.00 -7 10 0 -1.60 1.60 7 10 0 0.20 1.70 7 10 0 0.80 1.50 -7 10 0 0.50 2.30 -8 -10 0 -3.60 2.00 -8 -10 0 -0.30 2.10 8 -10 0 1.30 1.50 8 -10 0 0.60 1.00 8 -10 0 4.20 2.30 -8 -10 0 3.20 2.10 -8 10 0 -1.10 1.70 -8 10 0 2.70 2.20 -8 10 0 4.40 2.00 8 10 0 1.60 2.50 -8 10 0 2.60 2.70 -8 10 0 -0.20 2.10 8 10 0 2.40 1.80 8 10 0 0.30 1.90 -8 10 0 -1.40 2.40 0 -11 0 -1.60 1.40 0 -11 0 -1.40 1.20 0 -11 0 -0.10 1.60 0 -11 0 -1.20 1.10 0 -11 0 -0.20 1.80 0 -11 0 -2.00 1.50 0 11 0 -2.10 1.60 0 11 0 -1.60 1.80 0 11 0 1.90 2.10 -1 -11 0 13.00 2.50 1 -11 0 15.00 1.90 -1 -11 0 17.10 2.70 1 -11 0 11.50 2.60 -1 -11 0 14.10 2.60 1 -11 0 8.30 2.00 1 -11 0 9.80 2.20 -1 -11 0 11.40 1.90 -1 11 0 12.40 2.40 1 11 0 16.20 2.50 -1 11 0 12.90 2.70 1 11 0 9.50 2.50 -1 11 0 15.60 2.60 1 11 0 12.70 2.60 -2 -11 0 13.30 2.20 2 -11 0 17.80 1.90 2 -11 0 15.90 2.50 -2 -11 0 20.70 2.90 2 -11 0 14.50 2.40 -2 -11 0 20.00 2.80 -2 -11 0 15.30 2.80 -2 11 0 14.00 2.60 2 11 0 17.70 2.60 -2 11 0 16.40 3.20 2 11 0 20.20 3.00 -2 11 0 17.60 2.70 2 11 0 13.60 2.80 -2 11 0 16.10 2.60 -2 11 0 13.60 3.10 3 -11 0 4.10 1.30 3 -11 0 4.70 1.80 -3 -11 0 2.60 3.20 -3 -11 0 4.70 3.00 -3 -11 0 4.20 2.00 3 -11 0 0.10 1.60 -3 -11 0 1.90 2.10 -3 -11 0 7.20 2.30 -3 11 0 3.70 2.20 -3 11 0 3.20 2.00 3 11 0 1.70 2.10 -3 11 0 2.90 2.00 3 11 0 1.80 2.00 -3 11 0 1.20 1.90 -3 11 0 0.60 2.30 3 11 0 5.60 2.50 4 -11 0 0.40 1.80 -4 -11 0 -0.40 1.70 4 -11 0 1.60 1.90 4 -11 0 -0.50 1.60 4 -11 0 1.30 1.10 -4 -11 0 0.10 1.90 -4 -11 0 -1.50 2.30 -4 -11 0 8.20 2.10 -4 -11 0 -3.40 1.70 -4 -11 0 -0.10 1.90 -4 11 0 -1.60 1.90 4 11 0 1.90 1.80 -4 11 0 3.00 2.10 -4 11 0 -2.00 1.60 -4 11 0 -1.70 2.10 4 11 0 2.00 2.30 4 11 0 2.40 2.10 -4 11 0 3.00 2.20 -5 -11 0 6.90 3.30 -5 -11 0 18.60 3.00 -5 -11 0 16.30 2.90 5 -11 0 16.40 2.40 -5 -11 0 10.60 2.40 -5 -11 0 6.50 4.00 5 -11 0 11.30 1.50 -5 -11 0 11.10 2.40 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7.20 5 -5 -4 271.77 11.00 -5 -5 4 287.87 7.30 -5 -5 4 266.57 7.00 5 -5 -4 265.27 6.90 5 5 -4 274.17 8.30 5 5 -4 266.37 6.90 -5 5 4 259.67 6.90 -5 5 4 268.27 7.00 5 5 -4 276.17 7.50 -5 5 4 274.27 7.40 -5 5 4 272.37 7.80 5 5 -4 278.47 9.50 -4 -5 4 46.10 2.90 -4 -5 4 49.80 4.20 4 -5 -4 48.80 3.20 -4 -5 4 42.50 2.70 4 -5 -4 44.50 2.90 4 -5 -4 48.20 2.80 -4 -5 4 46.30 3.10 4 -5 -4 42.60 2.80 -4 -5 4 48.70 2.80 -4 5 4 48.60 3.30 -4 5 4 50.39 2.80 4 5 -4 44.50 4.70 -4 5 4 47.20 2.90 4 5 -4 49.50 2.90 -4 5 4 41.00 3.00 4 5 -4 44.20 3.00 4 5 -4 46.80 2.70 4 5 -4 48.00 2.90 -3 -5 4 5.30 1.60 -3 -5 4 4.50 1.80 3 -5 -4 4.30 1.50 -3 -5 4 7.10 1.60 3 -5 -4 5.70 1.50 -3 -5 4 5.50 1.60 3 -5 -4 4.40 1.40 3 -5 -4 5.40 1.60 -3 -5 4 7.10 1.40 3 5 -4 6.50 2.10 3 5 -4 4.80 1.40 3 5 -4 3.70 1.50 -3 5 4 4.40 1.50 3 5 -4 8.50 1.80 3 5 -4 5.40 1.40 -3 5 4 6.60 1.60 -3 5 4 6.70 1.60 -2 -5 4 39.40 2.40 2 -5 -4 38.90 2.40 -2 -5 4 38.80 2.40 -2 -5 4 43.80 2.70 -2 -5 4 35.80 3.20 2 -5 -4 39.30 2.30 -2 -5 4 41.30 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63.69 4.40 -2 -3 8 65.99 3.40 -2 3 8 67.89 3.10 2 3 -8 66.89 3.50 2 3 -8 70.29 3.20 2 3 -8 68.39 3.40 -2 3 8 67.19 4.00 2 3 -8 71.09 4.70 -2 3 8 69.59 3.30 -2 3 8 60.49 3.00 2 3 -8 66.29 3.50 -2 3 8 67.39 3.50 1 -3 -8 7.10 1.70 -1 -3 8 5.60 1.90 1 -3 -8 3.80 1.50 -1 -3 8 5.00 1.40 -1 -3 8 8.50 1.50 1 -3 -8 5.60 1.20 -1 3 8 6.60 1.60 1 3 -8 2.90 1.90 1 3 -8 7.00 1.70 1 3 -8 6.60 1.70 1 3 -8 5.00 1.70 -1 3 8 10.00 1.70 1 3 -8 8.20 1.50 -1 3 8 6.30 1.30 -1 3 8 7.20 1.50 0 -3 -8 160.68 4.20 0 -3 8 165.08 4.00 0 -3 -8 164.48 4.80 0 -3 8 168.68 4.10 0 -3 8 169.78 4.80 0 -3 8 154.58 6.00 0 -3 -8 168.88 4.80 0 3 8 167.98 4.90 0 3 8 166.88 4.30 0 3 8 160.48 4.20 0 3 8 158.88 4.30 0 3 -8 166.28 6.30 0 3 -8 171.58 4.70 0 3 -8 157.68 4.70 0 3 -8 163.48 4.70 0 3 -8 166.28 4.40 -1 -3 -8 2.20 1.30 1 -3 8 0.50 1.40 1 -3 8 0.00 0.60 1 -3 8 -1.00 0.90 -1 -3 -8 1.70 1.30 -1 -3 -8 -0.60 0.80 1 3 8 0.20 0.80 -1 3 -8 0.10 1.60 -1 3 -8 0.60 1.00 1 3 8 -0.60 1.00 1 3 8 0.20 0.60 -1 3 -8 -0.30 1.10 -1 3 -8 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2.20 4 4 -8 0.20 1.70 -4 4 8 2.80 2.20 -4 4 8 -0.50 1.70 -4 4 8 3.30 1.60 4 4 -8 0.90 1.50 3 -4 -8 1.60 1.60 -3 -4 8 -0.80 0.90 -3 -4 8 -1.30 1.70 3 -4 -8 1.60 1.30 3 -4 -8 1.90 1.70 -3 -4 8 -0.50 1.40 -3 -4 8 -0.10 1.30 -3 -4 8 2.50 2.10 3 -4 -8 0.70 1.70 -3 -4 8 -2.10 1.50 -3 4 8 0.60 1.90 -3 4 8 -0.20 1.60 3 4 -8 -3.30 1.40 -3 4 8 2.10 1.40 3 4 -8 0.80 1.60 3 4 -8 1.50 2.30 -3 4 8 0.10 1.50 3 4 -8 0.20 1.30 3 4 -8 -1.30 1.80 -3 4 8 0.70 1.50 -2 -4 8 0.00 0.90 2 -4 -8 0.70 1.50 -2 -4 8 -0.30 1.50 -2 -4 8 2.00 1.60 2 -4 -8 -0.40 1.20 2 -4 -8 1.90 1.80 2 -4 -8 -0.80 1.70 -2 -4 8 0.80 1.50 -2 -4 8 0.50 1.80 -2 4 8 1.50 1.50 -2 4 8 0.40 1.40 2 4 -8 -0.70 1.50 2 4 -8 -2.10 2.00 -2 4 8 -0.80 1.30 -2 4 8 -1.90 1.20 2 4 -8 3.20 1.70 -2 4 8 1.00 1.30 2 4 -8 1.90 1.70 2 4 -8 1.00 1.20 -1 -4 8 179.48 10.10 -1 -4 8 173.18 3.70 1 -4 -8 173.88 4.90 1 -4 -8 173.88 5.30 1 -4 -8 173.08 5.20 -1 -4 8 184.88 4.90 -1 -4 8 175.78 5.30 -1 -4 8 177.48 4.80 1 4 -8 175.78 5.30 -1 4 8 185.48 5.60 -1 4 8 176.08 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0.50 1.40 -2 -2 -9 0.20 1.20 -2 -2 -9 1.10 0.90 -2 -2 -9 0.30 0.80 2 -2 9 -1.00 0.90 -2 -2 -9 -1.10 1.10 -2 2 -9 0.50 1.10 -2 2 -9 0.90 0.90 2 2 9 0.30 0.80 -2 2 -9 0.50 1.20 -2 2 -9 -0.70 1.60 -2 2 -9 0.60 1.10 2 2 9 -0.20 1.00 3 -2 9 41.60 1.80 -3 -2 -9 42.60 2.30 3 -2 9 43.90 3.60 -3 -2 -9 42.50 2.40 -3 -2 -9 43.50 2.30 -3 -2 -9 42.00 2.30 -3 2 -9 38.50 1.50 -3 2 -9 41.70 2.20 3 2 9 45.20 2.10 -3 2 -9 40.20 2.20 -3 2 -9 43.10 3.70 -4 -2 -9 174.38 4.30 -4 -2 -9 169.68 4.60 -4 -2 -9 172.68 4.30 -4 -2 -9 176.78 5.00 4 2 9 168.18 3.60 -4 2 -9 178.88 6.60 -4 2 -9 175.18 4.00 -4 2 -9 175.38 4.10 4 2 9 171.58 3.60 -4 2 -9 180.08 5.20 -4 2 -9 175.28 4.80 -5 -2 -9 8.50 1.80 -5 -2 -9 11.20 1.80 -5 -2 -9 12.80 3.40 -5 -2 -9 9.90 1.30 -5 -2 -9 11.00 1.30 -5 2 -9 8.00 1.40 -5 2 -9 11.40 1.60 -5 2 -9 6.20 1.80 -5 2 -9 10.20 1.10 -6 -2 -9 -0.70 0.80 -6 -2 -9 0.60 1.60 -6 -2 -9 0.70 0.90 -6 -2 -9 0.40 1.10 -6 -2 -9 -0.10 1.20 -6 2 -9 -0.30 0.60 -6 2 -9 1.70 0.60 -6 2 -9 -1.20 1.50 -6 2 -9 -0.40 1.10 -6 2 -9 1.60 1.20 -7 -2 -9 15.30 1.30 -7 -2 -9 10.70 2.00 -7 -2 -9 13.80 1.20 -7 -2 -9 11.80 1.90 -7 -2 -9 11.30 2.20 -7 2 -9 10.20 2.30 -7 2 -9 11.10 0.70 -7 2 -9 8.40 1.80 -7 2 -9 7.50 1.60 -7 2 -9 11.50 0.70 -8 -2 -9 0.90 1.50 -8 -2 -9 2.10 0.80 -8 -2 -9 0.40 0.80 -8 -2 -9 1.70 1.70 -8 -2 -9 2.30 1.50 -8 2 -9 0.60 1.40 -8 2 -9 -0.20 1.00 -8 2 -9 -0.40 1.40 -8 -3 9 0.90 2.00 8 -3 -9 -1.10 3.50 -8 -3 9 -2.90 2.50 8 -3 -9 -1.30 2.00 -8 -3 9 -1.50 3.50 -8 -3 9 0.70 1.80 8 3 -9 0.40 2.10 -8 3 9 -7.50 3.00 -8 3 9 -1.80 2.10 8 3 -9 0.10 2.20 -8 3 9 -3.20 2.40 -8 3 9 -1.20 1.90 7 -3 -9 3.20 2.20 -7 -3 9 0.70 2.80 -7 -3 9 1.70 3.30 7 -3 -9 0.40 2.00 -7 -3 9 -1.00 1.80 7 -3 -9 4.90 2.40 -7 -3 9 -0.90 2.00 -7 -3 9 -2.40 2.20 -7 3 9 0.10 1.80 7 3 -9 1.40 2.10 -7 3 9 0.60 2.20 7 3 -9 -0.50 1.90 7 3 -9 0.90 2.20 -7 3 9 -0.10 1.90 -7 3 9 -2.30 3.00 7 3 -9 0.20 2.00 6 -3 -9 3.50 2.60 -6 -3 9 2.10 2.00 -6 -3 9 1.80 2.20 -6 -3 9 3.50 2.10 -6 -3 9 3.80 1.60 6 -3 -9 4.00 2.00 -6 -3 9 2.00 2.80 -6 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2 -3 -9 -1.20 1.60 -2 -3 9 0.20 0.50 2 -3 -9 -0.60 1.60 -2 -3 9 -0.60 1.40 -2 -3 9 1.60 2.20 -2 -3 9 1.20 1.50 2 -3 -9 -0.20 1.00 -2 -3 9 0.10 1.50 2 3 -9 0.50 2.30 2 3 -9 2.20 1.50 -2 3 9 -2.80 1.50 -2 3 9 -0.40 1.50 2 3 -9 4.20 1.90 2 3 -9 -0.40 1.60 -2 3 9 -0.60 1.50 2 3 -9 -1.50 1.90 -1 -3 9 24.80 2.30 1 -3 -9 22.90 2.60 -1 -3 9 21.40 2.10 1 -3 -9 26.10 2.80 -1 -3 9 24.70 2.50 1 -3 -9 27.40 3.10 1 -3 -9 18.30 1.90 -1 3 9 19.20 2.00 1 3 -9 24.60 2.60 -1 3 9 25.90 2.60 1 3 -9 21.60 2.40 -1 3 9 26.20 2.80 1 3 -9 17.60 2.00 -1 3 9 22.10 2.20 0 -3 9 6.40 1.30 0 -3 9 6.00 1.50 0 -3 -9 4.30 1.60 0 -3 -9 3.00 1.00 0 -3 -9 8.10 1.70 0 -3 9 5.30 1.90 0 -3 9 3.70 1.10 0 3 9 6.90 1.60 0 3 -9 3.60 1.30 0 3 9 6.60 1.40 0 3 9 5.20 1.30 0 3 -9 5.20 1.60 0 3 9 5.20 1.20 0 3 -9 6.60 1.60 0 3 -9 5.70 1.50 -1 -3 -9 -0.60 1.30 1 -3 9 0.80 0.60 1 -3 9 0.50 0.50 -1 -3 -9 -0.70 0.80 1 -3 9 1.00 1.60 -1 -3 -9 0.90 1.30 -1 3 -9 -1.20 1.10 -1 3 -9 -1.00 1.20 1 3 9 0.00 1.10 -1 3 -9 0.20 1.30 -1 3 -9 -1.60 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-9 5.20 2.10 2 -4 -9 2.70 1.60 -2 -4 9 5.10 2.10 -2 -4 9 3.70 1.70 -2 -4 9 3.50 0.80 -2 -4 9 3.00 0.90 2 -4 -9 2.90 1.30 -2 4 9 6.40 1.70 2 4 -9 4.30 2.50 -2 4 9 3.60 1.50 2 4 -9 4.60 1.90 2 4 -9 7.00 1.70 -2 4 9 3.90 1.70 2 4 -9 5.20 1.80 2 4 -9 4.10 1.90 -2 4 9 4.30 1.80 -1 -4 9 159.68 4.70 -1 -4 9 159.88 5.30 -1 -4 9 166.38 6.80 1 -4 -9 155.18 5.20 1 -4 -9 168.98 5.40 -1 -4 9 162.58 4.60 1 -4 -9 159.78 4.80 1 4 -9 166.28 7.40 1 4 -9 156.78 5.00 -1 4 9 163.58 5.10 1 4 -9 169.48 5.40 1 4 -9 167.98 6.40 -1 4 9 156.78 5.40 1 4 -9 160.38 4.70 -1 4 9 162.18 4.90 -1 4 9 165.08 4.90 0 -4 9 6.50 2.10 0 -4 9 7.30 1.40 0 -4 -9 6.10 1.30 0 -4 9 6.50 1.60 0 -4 9 7.10 1.40 0 -4 -9 8.30 1.80 0 4 -9 6.30 1.70 0 4 -9 8.50 1.40 0 4 -9 7.20 1.70 0 4 9 8.20 1.20 0 4 -9 5.90 2.40 0 4 9 7.20 1.50 0 4 -9 7.70 1.80 0 4 9 8.10 1.60 0 4 9 10.10 1.80 -1 -4 -9 44.50 2.60 1 -4 9 39.10 2.60 -1 -4 -9 44.70 2.90 1 -4 9 42.90 3.90 1 -4 9 40.70 1.60 -1 -4 -9 37.70 2.70 -1 4 -9 47.60 2.80 1 4 9 40.70 2.20 -1 4 -9 45.20 2.70 -1 4 -9 45.20 2.60 1 4 9 41.20 2.10 -1 4 -9 41.60 4.40 -1 4 -9 42.10 2.30 1 4 9 42.90 2.70 -2 -4 -9 219.78 5.80 2 -4 9 193.18 7.30 -2 -4 -9 220.68 5.80 2 -4 9 211.58 7.60 -2 -4 -9 218.88 5.70 2 4 9 215.98 5.60 -2 4 -9 215.58 5.50 -2 4 -9 220.58 5.00 -2 4 -9 224.38 7.90 -2 4 -9 216.48 5.40 2 4 9 216.88 5.60 -2 4 -9 222.28 5.50 -3 -4 -9 6.00 1.70 3 -4 9 2.70 1.00 -3 -4 -9 4.30 1.40 3 -4 9 1.90 1.70 -3 -4 -9 3.70 1.50 -3 4 -9 3.10 1.30 3 4 9 4.30 1.20 -3 4 -9 4.90 1.00 -3 4 -9 4.70 1.10 -3 4 -9 1.90 2.10 3 4 9 3.90 1.20 -3 4 -9 2.90 1.30 4 -4 9 31.50 3.60 -4 -4 -9 33.30 2.30 -4 -4 -9 30.70 2.30 -4 -4 -9 27.50 2.90 4 -4 9 32.70 1.50 -4 4 -9 30.70 1.50 -4 4 -9 30.80 3.80 -4 4 -9 33.70 2.10 -4 4 -9 27.60 2.10 -4 4 -9 32.50 1.80 -4 4 -9 34.70 2.10 -4 4 -9 29.30 1.80 -5 -4 -9 38.50 2.30 -5 -4 -9 37.10 2.40 -5 -4 -9 36.60 3.30 -5 4 -9 36.70 2.60 -5 4 -9 40.00 2.10 5 4 9 37.20 1.80 5 4 9 37.20 1.70 -5 4 -9 37.90 2.00 -5 4 -9 41.10 4.30 -5 4 -9 36.60 1.90 -6 -4 -9 3.40 1.20 -6 -4 -9 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2 10 44.50 3.10 4 2 -10 40.20 3.70 -4 2 10 43.70 5.00 4 2 -10 39.70 3.70 4 2 -10 39.60 3.20 4 2 -10 36.00 3.40 -4 2 10 33.70 3.40 -4 2 10 35.50 3.20 3 -2 -10 19.70 2.80 -3 -2 10 23.40 2.60 3 -2 -10 25.50 2.90 -3 -2 10 19.90 2.50 3 -2 -10 20.80 2.80 -3 -2 10 19.00 1.40 -3 -2 10 18.90 3.10 3 2 -10 20.10 2.70 3 2 -10 22.80 2.50 -3 2 10 17.30 2.30 -3 2 10 26.30 2.50 3 2 -10 19.90 2.70 -3 2 10 21.40 2.60 3 2 -10 25.60 3.00 2 -2 -10 -1.00 1.70 -2 -2 10 0.60 1.50 2 -2 -10 -1.50 2.00 -2 -2 10 -1.00 1.40 2 -2 -10 -2.30 1.80 -2 -2 10 -0.90 1.50 2 -2 -10 1.30 0.80 -2 -2 10 6.10 2.40 -2 2 10 5.70 2.10 2 2 -10 1.50 2.30 2 2 -10 2.90 1.80 -2 2 10 4.40 1.80 -2 2 10 0.20 1.60 2 2 -10 -3.40 1.30 -2 2 10 2.50 1.20 2 2 -10 -1.80 1.60 1 -2 -10 0.60 1.80 1 -2 -10 0.10 0.80 1 -2 -10 -0.60 1.60 -1 -2 10 0.40 1.30 -1 -2 10 1.90 2.10 1 -2 -10 -1.50 1.70 -1 -2 10 0.20 1.30 -1 -2 10 1.30 1.30 -1 2 10 -2.90 1.20 -1 2 10 1.60 1.50 1 2 -10 -0.30 1.50 -1 2 10 3.80 1.60 1 2 -10 0.40 1.60 1 2 -10 -0.60 1.80 1 2 -10 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-13 4.10 1.70 3 1 13 0.60 0.90 -3 1 -13 0.40 1.40 -3 1 -13 -2.60 1.50 -4 -1 -13 10.70 1.90 -4 -1 -13 7.60 1.70 -4 1 -13 8.50 1.70 -4 1 -13 7.60 2.30 -4 -2 13 0.10 1.90 4 -2 -13 -1.20 2.00 -4 -2 13 -0.80 1.80 -4 -2 13 -1.90 2.50 4 2 -13 1.00 2.10 -4 2 13 -2.10 4.00 4 2 -13 1.60 2.20 4 2 -13 0.90 1.90 -4 2 13 -0.70 1.80 -3 -2 13 1.50 1.70 3 -2 -13 -0.50 2.20 -3 -2 13 -2.20 2.20 3 -2 -13 -4.40 2.10 3 -2 -13 -2.10 2.10 3 2 -13 -1.70 2.20 3 2 -13 4.70 2.40 3 2 -13 -0.90 1.80 -3 2 13 0.90 2.10 -3 2 13 1.90 1.80 2 -2 -13 9.90 2.60 -2 -2 13 6.20 2.30 -2 -2 13 12.60 2.10 -2 -2 13 4.50 2.80 2 -2 -13 11.60 2.60 2 -2 -13 9.20 2.40 -2 -2 13 9.60 1.80 -2 2 13 5.10 2.00 -2 2 13 10.40 1.90 2 2 -13 8.40 2.50 2 2 -13 10.80 2.30 -2 2 13 14.00 2.70 2 2 -13 8.50 2.10 2 2 -13 8.30 2.40 -2 2 13 9.80 2.10 -1 -2 13 9.10 1.60 1 -2 -13 10.70 2.60 1 -2 -13 7.70 2.40 1 -2 -13 5.70 2.10 -1 -2 13 9.40 2.40 -1 2 13 3.60 1.70 -1 2 13 8.40 1.60 -1 2 13 3.70 1.50 1 2 -13 3.20 2.20 1 2 -13 6.00 2.50 1 2 -13 5.40 2.00 1 2 -13 3.90 2.00 1 2 -13 6.60 2.10 -1 2 13 5.30 2.30 0 -2 -13 6.20 2.00 0 -2 -13 6.20 2.20 0 -2 -13 8.60 2.60 0 -2 13 5.90 2.00 0 -2 13 6.80 3.30 0 2 -13 4.70 2.10 0 2 -13 6.80 2.00 0 2 13 9.50 1.00 0 2 13 6.80 1.60 0 2 13 12.30 2.50 0 2 -13 5.90 2.10 0 2 -13 4.90 2.40 -1 -2 -13 0.50 1.80 -1 -2 -13 1.60 1.70 1 -2 13 -1.00 1.50 -1 2 -13 0.50 1.90 -1 2 -13 0.80 1.60 -1 2 -13 -0.50 1.40 -1 2 -13 0.90 1.60 1 2 13 0.60 1.00 1 2 13 2.20 1.60 2 -2 13 4.30 2.00 -2 -2 -13 6.60 1.80 -2 -2 -13 3.70 1.70 2 2 13 6.70 1.70 -2 2 -13 6.90 1.80 -2 2 -13 4.30 1.70 -2 2 -13 5.30 1.80 3 -2 13 6.20 1.10 -3 -2 -13 4.90 1.50 3 -2 13 1.90 1.70 -3 -2 -13 3.30 1.70 -3 2 -13 -1.30 1.80 -3 2 -13 1.00 1.40 -3 2 -13 4.60 1.60 3 2 13 2.50 1.50 -3 2 -13 4.30 1.90 -4 -2 -13 10.00 1.70 -4 2 -13 6.50 1.90 4 2 13 6.40 0.80 -4 2 -13 8.00 1.70 4 2 13 7.70 0.80 -4 2 -13 7.90 1.70 4 -3 -13 5.60 2.60 -4 -3 13 0.70 3.80 -4 -3 13 2.00 2.80 -4 -3 13 7.40 2.20 -4 3 13 6.40 2.50 -4 3 13 7.60 2.40 4 3 -13 3.50 2.50 -4 3 13 3.80 1.60 4 3 -13 1.70 2.10 4 3 -13 6.00 2.10 -3 -3 13 2.00 2.60 -3 -3 13 0.20 1.60 -3 3 13 -1.80 2.00 -3 3 13 3.20 1.80 3 3 -13 0.50 1.70 3 3 -13 0.70 2.00 2 -3 -13 2.50 2.20 -2 -3 13 4.10 2.60 2 -3 -13 0.90 2.00 -2 -3 13 1.10 1.50 -2 -3 13 5.60 1.50 -2 -3 13 -0.20 2.00 2 -3 -13 -1.30 2.00 -2 3 13 3.80 2.70 -2 3 13 5.50 1.80 2 3 -13 0.60 2.30 2 3 -13 3.60 2.30 2 3 -13 6.20 2.10 2 3 -13 1.60 2.00 2 3 -13 2.10 1.80 -2 3 13 4.60 3.80 1 -3 -13 8.80 2.60 1 -3 -13 8.50 2.40 -1 -3 13 7.60 1.60 -1 -3 13 10.30 2.40 -1 -3 13 7.20 2.50 -1 -3 13 11.40 1.60 -1 3 13 9.50 1.90 1 3 -13 9.60 2.10 1 3 -13 10.00 2.30 -1 3 13 9.40 1.70 1 3 -13 12.00 2.80 1 3 -13 10.00 2.20 -1 3 13 11.10 2.00 1 3 -13 4.40 2.50 -1 3 13 14.40 2.70 0 -3 -13 0.90 1.60 0 -3 -13 0.10 1.80 0 -3 -13 3.50 2.10 0 3 -13 -1.70 2.00 0 3 13 1.00 1.00 0 3 13 -0.60 0.80 0 3 -13 1.70 1.60 0 3 13 1.00 1.70 0 3 -13 0.00 1.80 0 3 -13 3.70 2.00 0 3 -13 1.70 1.60 -1 -3 -13 -3.30 1.70 1 -3 13 -1.40 1.50 -1 -3 -13 0.80 1.70 -1 -3 -13 2.00 1.80 1 3 13 -0.30 2.80 -1 3 -13 1.70 2.20 -1 3 -13 0.70 1.60 -1 3 -13 1.40 1.50 -1 3 -13 0.20 1.60 2 -3 13 13.10 2.00 -2 -3 -13 13.70 2.20 -2 3 -13 21.40 2.40 -2 3 -13 12.40 1.90 2 3 13 18.90 2.10 2 3 13 17.30 2.20 -2 3 -13 8.00 2.60 -3 -3 -13 4.10 1.70 -3 -3 -13 5.70 1.70 3 -3 13 0.30 0.80 -3 3 -13 -2.60 1.80 -3 3 -13 2.50 1.80 -3 3 -13 1.90 1.40 3 -4 -13 7.00 2.60 -3 -4 13 6.10 2.80 -3 -4 13 6.90 2.10 -3 4 13 8.20 2.10 -3 4 13 9.20 2.20 -3 4 13 4.90 2.20 3 4 -13 7.70 3.90 3 4 -13 6.80 2.20 3 4 -13 5.20 1.90 -2 -4 13 7.20 2.60 2 -4 -13 5.00 2.50 -2 -4 13 9.30 1.90 2 -4 -13 10.80 2.70 -2 4 13 10.80 2.10 2 4 -13 6.10 2.20 2 4 -13 8.60 2.00 -2 4 13 5.60 1.80 2 4 -13 7.50 3.10 2 4 -13 11.90 2.70 -2 4 13 6.60 1.90 1 -4 -13 5.10 2.10 -1 -4 13 2.90 2.60 -1 -4 13 1.80 1.30 -1 -4 13 0.50 1.80 1 -4 -13 0.40 2.90 1 -4 -13 -1.10 1.80 1 4 -13 3.20 2.00 -1 4 13 2.20 1.40 1 4 -13 4.40 1.80 -1 4 13 1.00 1.40 1 4 -13 1.80 2.50 1 4 -13 0.10 1.60 1 4 -13 -1.80 2.10 -1 4 13 1.50 1.10 -1 4 13 0.50 2.30 0 -4 -13 2.00 1.90 0 -4 13 2.20 1.80 0 -4 -13 -0.50 2.20 0 -4 13 2.30 2.00 0 -4 -13 0.50 2.10 0 4 13 1.10 0.70 0 4 -13 0.10 1.30 0 4 -13 -0.50 1.50 0 4 -13 -1.40 2.20 0 4 13 2.50 2.00 0 4 13 1.10 0.90 0 4 -13 2.90 2.00 0 4 -13 0.00 1.80 0 4 13 2.40 1.10 -1 -4 -13 -1.00 1.70 1 -4 13 3.60 1.90 1 -4 13 -0.50 1.80 -1 -4 -13 0.00 1.80 -1 4 -13 -1.10 1.20 -1 4 -13 -0.80 1.30 1 4 13 1.20 1.70 -1 4 -13 -1.10 1.50 -1 4 -13 -0.10 1.60 -1 4 -13 -3.30 1.90 -2 -4 -13 1.40 1.70 -2 -4 -13 2.10 0.60 2 -4 13 -0.10 1.80 -2 -4 -13 -1.00 1.70 2 -4 13 0.20 1.30 -2 4 -13 -0.70 1.10 -2 4 -13 3.20 1.60 2 4 13 3.50 2.30 -2 4 -13 0.90 1.70 2 4 13 2.30 1.30 -2 4 -13 1.30 1.30 -3 -4 -13 0.80 0.80 -3 -4 -13 2.10 1.70 3 -4 13 0.80 1.80 -3 -4 -13 0.30 1.50 -3 4 -13 -0.30 1.40 -3 4 -13 1.50 1.30 3 4 13 2.60 1.40 3 4 13 0.30 1.00 -3 4 -13 0.40 1.10 2 -5 -13 0.70 1.00 -2 -5 13 1.10 1.40 -2 -5 13 7.70 2.70 -2 -5 13 3.00 1.90 -2 5 13 0.90 1.30 2 5 -13 -1.70 2.60 2 5 -13 1.10 2.40 2 5 -13 -2.80 2.60 2 5 -13 3.50 1.50 2 5 -13 1.80 1.90 -2 5 13 3.10 1.80 -1 -5 13 0.70 1.30 1 -5 -13 0.00 2.10 1 -5 -13 -0.30 0.90 1 -5 -13 0.20 2.00 -1 -5 13 -0.60 2.10 -1 -5 13 -0.90 1.00 1 5 -13 -0.70 1.30 1 5 -13 -1.00 1.70 1 5 -13 -3.30 2.60 1 5 -13 1.90 1.80 -1 5 13 -1.10 0.80 -1 5 13 0.40 1.40 -1 5 13 -1.60 1.20 0 -5 -13 1.00 2.00 0 -5 13 1.90 2.20 0 -5 -13 0.00 0.90 0 -5 13 0.50 0.60 0 -5 13 2.50 1.90 0 -5 -13 -0.90 1.90 0 5 13 -0.70 1.00 0 5 -13 -1.70 1.20 0 5 -13 3.20 1.70 0 5 -13 1.90 1.90 0 5 13 6.80 3.60 0 5 13 1.90 1.10 0 5 -13 -1.90 2.30 1 -5 13 6.20 2.40 -1 -5 -13 2.50 1.00 -1 -5 -13 3.40 1.90 1 -5 13 3.70 1.80 -1 5 -13 1.80 1.80 -1 5 -13 5.40 2.00 -1 5 -13 2.90 1.50 1 5 13 3.10 1.50 1 5 13 2.70 1.80 -1 5 -13 0.40 2.30 -1 5 -13 1.60 1.70 2 -5 13 0.10 2.00 2 -5 13 2.60 2.70 -2 -5 -13 2.40 1.10 -2 -5 -13 2.00 1.70 -2 -5 -13 -4.20 1.70 2 5 13 2.00 1.60 -2 5 -13 -2.90 1.90 -2 5 -13 0.20 1.10 -2 5 -13 1.10 1.10 -2 5 -13 2.70 1.70 -2 5 -13 0.10 1.80 2 5 13 -0.90 1.60 0 -6 13 7.40 2.70 -2 0 14 6.90 1.80 -2 0 14 9.70 1.70 2 0 -14 7.40 2.40 -1 0 14 2.00 1.00 1 0 -14 1.60 1.80 1 0 -14 2.90 2.10 1 0 -14 1.90 2.10 -1 0 14 -0.50 1.70 -1 0 14 0.50 1.00 0 0 -14 2.60 1.80 0 0 -14 -0.10 1.80 0 0 14 2.50 1.60 0 0 14 2.00 1.80 -1 0 -14 -4.40 2.20 -1 0 -14 1.40 1.70 1 0 14 0.10 1.50 1 0 14 0.80 1.30 -1 0 -14 2.10 1.50 -2 -1 14 2.90 1.40 -2 -1 14 0.60 1.60 -2 -1 14 0.90 2.10 -2 1 14 0.60 1.80 2 1 -14 5.80 3.20 2 1 -14 -0.20 1.90 -2 1 14 2.30 1.60 1 -1 -14 -1.20 1.70 -1 -1 14 2.10 1.10 1 -1 -14 -0.70 1.80 1 -1 -14 -3.70 1.80 -1 -1 14 1.80 0.90 1 1 -14 -1.30 1.70 1 1 -14 1.30 1.70 -1 1 14 2.10 1.10 -1 1 14 1.70 1.50 -1 1 14 2.60 1.00 1 1 -14 1.60 1.90 0 -1 14 5.40 1.90 0 -1 14 13.10 2.40 0 -1 -14 5.90 2.40 0 -1 -14 2.30 1.80 0 1 -14 9.80 4.00 0 1 -14 0.90 2.20 0 1 14 5.30 1.80 0 1 -14 4.70 1.80 -1 -1 -14 0.20 1.90 -1 -1 -14 -2.20 1.50 1 -1 14 1.70 1.60 1 -1 14 1.70 1.60 -1 -1 -14 5.80 2.00 -1 1 -14 1.60 1.80 -1 1 -14 0.50 1.70 -1 1 -14 -1.80 1.70 1 1 14 1.40 1.20 1 1 14 3.50 1.90 -1 1 -14 3.20 1.70 1 -2 -14 4.00 2.30 -1 -2 14 1.20 0.90 -1 -2 14 1.70 1.10 -1 -2 14 -1.00 1.80 1 -2 -14 0.10 1.90 1 2 -14 -1.40 1.50 -1 2 14 -1.40 1.00 -1 2 14 0.60 1.40 1 2 -14 -0.50 3.00 -1 2 14 -1.30 1.10 1 2 -14 -0.40 2.00 0 -2 -14 5.10 2.10 0 -2 -14 -2.10 1.80 0 -2 -14 3.00 2.10 0 -2 14 4.30 2.00 0 2 -14 1.80 1.80 0 2 14 3.20 1.30 0 2 -14 1.60 1.60 0 2 -14 -1.00 2.00 0 2 14 4.00 2.30 -1 -2 -14 3.00 2.30 -1 -2 -14 -0.20 1.60 -1 -2 -14 2.30 1.80 -1 2 -14 4.00 1.90 1 2 14 2.00 1.10 1 2 14 3.40 1.80 -1 2 -14 0.10 1.60 -1 2 -14 2.00 1.50 -1 2 -14 -1.20 1.80 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 61080 _shelx_res_file ; TITL UMD2852D_a.res in P2(1)/n umd2852d_a.res created by SHELXL-2018/3 at 15:53:39 on 01-Mar-2023 REM Old TITL UMD2852D in P2(1)/n REM SHELXT solution in P2(1)/n: R1 0.192, Rweak 0.012, Alpha 0.022 REM 0.403 for 131 systematic absences, Orientation as input REM Formula found by SHELXT: C14 N O CELL 0.71073 9.0478 11.668 11.3885 90 91.523 90 ZERR 4 0.0006 0.0008 0.0007 0 0.002 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H N O UNIT 52 72 8 4 EQIV $1 -0.5+X,1.5-Y,-0.5+Z EQIV $2 1-X,1-Y,1-Z DFIX 0.87 0.01 N1 H1a DFIX 0.9 0.01 N2 H2 DFIX 1 0.01 O1 H1 L.S. 10 PLAN 2 SIZE 0.21 0.22 0.24 TEMP 27 CONF HTAB O1 N2 HTAB N1 O1_$1 HTAB N2 O1_$2 BOND $h LIST 4 HTAB 2 fmap 2 acta MORE -1 REM REM REM WGHT 0.047600 0.222900 EXTI 0.009572 FVAR 0.82817 O1 4 0.672893 0.653186 0.466308 11.00000 0.07402 0.05416 = 0.05774 -0.00681 -0.02875 0.00536 N1 3 0.376154 0.737037 0.137022 11.00000 0.08335 0.07058 = 0.06721 0.00813 -0.03730 -0.00350 N2 3 0.653727 0.439348 0.406640 11.00000 0.05278 0.05039 = 0.07078 -0.00201 -0.00537 -0.00001 C1 1 0.462602 0.645128 0.113224 11.00000 0.09614 0.06867 = 0.05166 -0.00372 -0.02594 -0.00931 AFIX 43 H1B 2 0.459562 0.605365 0.042428 11.00000 -1.20000 AFIX 0 C2 1 0.410027 0.774754 0.248046 11.00000 0.05189 0.05572 = 0.05811 0.01045 -0.01375 -0.00982 C3 1 0.352372 0.866582 0.309445 11.00000 0.05684 0.05707 = 0.08489 0.01474 -0.00738 0.00283 AFIX 43 H3 2 0.279287 0.913394 0.276289 11.00000 -1.20000 AFIX 0 C4 1 0.407602 0.885237 0.420671 11.00000 0.07623 0.05308 = 0.07587 -0.00051 0.00566 0.00608 AFIX 43 H4 2 0.372585 0.946906 0.463557 11.00000 -1.20000 AFIX 0 C5 1 0.515428 0.813792 0.471379 11.00000 0.07823 0.05246 = 0.05186 -0.00354 -0.00442 -0.00146 AFIX 43 H5 2 0.549839 0.828481 0.547572 11.00000 -1.20000 AFIX 0 C6 1 0.571921 0.722136 0.411149 11.00000 0.04949 0.04532 = 0.04688 0.00205 -0.00821 -0.00734 C7 1 0.521035 0.701445 0.295193 11.00000 0.04342 0.04782 = 0.04599 0.00383 -0.00606 -0.01044 C8 1 0.554277 0.618538 0.206072 11.00000 0.05983 0.05816 = 0.04620 -0.00182 -0.00918 -0.01027 C9 1 0.664695 0.522720 0.206902 11.00000 0.06794 0.07822 = 0.05480 -0.01821 -0.00531 0.00171 AFIX 23 H9A 2 0.759008 0.552462 0.235646 11.00000 -1.20000 H9B 2 0.677518 0.497638 0.126609 11.00000 -1.20000 AFIX 0 C10 1 0.625562 0.419499 0.280170 11.00000 0.07369 0.05488 = 0.08100 -0.01751 -0.02345 0.00468 AFIX 23 H10A 2 0.521883 0.401214 0.266863 11.00000 -1.20000 H10B 2 0.683237 0.354207 0.255279 11.00000 -1.20000 AFIX 0 C11 1 0.791919 0.386314 0.452049 11.00000 0.05562 0.05164 = 0.07412 0.00345 -0.00534 0.00368 AFIX 23 H11A 2 0.873537 0.411109 0.404706 11.00000 -1.20000 H11B 2 0.784125 0.303640 0.445430 11.00000 -1.20000 AFIX 0 C12 1 0.823277 0.417981 0.578047 11.00000 0.06394 0.06553 = 0.06607 0.01208 -0.00097 -0.00317 AFIX 23 H12A 2 0.733916 0.407145 0.621928 11.00000 -1.20000 H12B 2 0.848746 0.498669 0.581958 11.00000 -1.20000 AFIX 0 C13 1 0.946385 0.349631 0.636072 11.00000 0.07509 0.08958 = 0.08186 0.02243 -0.01553 -0.00248 AFIX 137 H13A 2 0.960198 0.374269 0.716039 11.00000 -1.50000 H13B 2 1.036130 0.361400 0.594605 11.00000 -1.50000 H13C 2 0.921194 0.269711 0.634508 11.00000 -1.50000 AFIX 0 H1 2 0.663723 0.571531 0.438843 11.00000 0.10916 H1A 2 0.313968 0.770585 0.088231 11.00000 0.09655 H2 2 0.580731 0.406979 0.447647 11.00000 0.08939 HKLF 4 REM UMD2852D_a.res in P2(1)/n REM wR2 = 0.1071, GooF = S = 1.010, Restrained GooF = 1.010 for all data REM R1 = 0.0383 for 1941 Fo > 4sig(Fo) and 0.0522 for all 2472 data REM 159 parameters refined using 3 restraints END WGHT 0.0476 0.2229 REM Instructions for potential hydrogen bonds HTAB O1 N2 HTAB N1 O1_$1 HTAB N2 O1_$2 REM Highest difference peak 0.136, deepest hole -0.111, 1-sigma level 0.025 Q1 1 0.5525 0.6624 0.2557 11.00000 0.05 0.14 Q2 1 0.4708 0.7426 0.2775 11.00000 0.05 0.14 ; _shelx_res_checksum 39710 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O O1 0.67289(11) 0.65319(8) 0.46631(9) 0.0625(3) Uani d 1 . . N N1 0.37615(16) 0.73704(13) 0.13702(12) 0.0744(4) Uani d 1 . . N N2 0.65373(13) 0.43935(10) 0.40664(11) 0.0581(3) Uani d 1 . . C C1 0.4626(2) 0.64513(15) 0.11322(13) 0.0727(5) Uani d 1 . . H H1B 0.459562 0.605365 0.042428 0.087 Uiso calc 1 . . C C2 0.41003(15) 0.77475(12) 0.24805(12) 0.0555(4) Uani d 1 . . C C3 0.35237(17) 0.86658(14) 0.30944(15) 0.0664(4) Uani d 1 . . H H3 0.279287 0.913394 0.276289 0.080 Uiso calc 1 . . C C4 0.40760(18) 0.88524(13) 0.42067(15) 0.0683(4) Uani d 1 . . H H4 0.372585 0.946906 0.463557 0.082 Uiso calc 1 . . C C5 0.51543(17) 0.81379(12) 0.47138(13) 0.0610(4) Uani d 1 . . H H5 0.549839 0.828481 0.547572 0.073 Uiso calc 1 . . C C6 0.57192(14) 0.72214(11) 0.41115(11) 0.0474(3) Uani d 1 . . C C7 0.52103(13) 0.70145(11) 0.29519(11) 0.0459(3) Uani d 1 . . C C8 0.55428(15) 0.61854(12) 0.20607(11) 0.0549(3) Uani d 1 . . C C9 0.66469(18) 0.52272(14) 0.20690(13) 0.0671(4) Uani d 1 . . H H9A 0.759008 0.552462 0.235646 0.081 Uiso calc 1 . . H H9B 0.677518 0.497638 0.126609 0.081 Uiso calc 1 . . C C10 0.62556(19) 0.41950(13) 0.28017(15) 0.0703(4) Uani d 1 . . H H10A 0.521883 0.401214 0.266863 0.084 Uiso calc 1 . . H H10B 0.683237 0.354207 0.255279 0.084 Uiso calc 1 . . C C11 0.79192(15) 0.38631(13) 0.45205(14) 0.0606(4) Uani d 1 . . H H11A 0.873537 0.411109 0.404706 0.073 Uiso calc 1 . . H H11B 0.784125 0.303640 0.445430 0.073 Uiso calc 1 . . C C12 0.82328(17) 0.41798(14) 0.57805(14) 0.0652(4) Uani d 1 . . H H12A 0.733916 0.407145 0.621928 0.078 Uiso calc 1 . . H H12B 0.848746 0.498669 0.581958 0.078 Uiso calc 1 . . C C13 0.9464(2) 0.34963(17) 0.63607(16) 0.0825(5) Uani d 1 . . H H13A 0.960198 0.374269 0.716039 0.124 Uiso calc 1 . . H H13B 1.036130 0.361400 0.594605 0.124 Uiso calc 1 . . H H13C 0.921194 0.269711 0.634508 0.124 Uiso calc 1 . . H H1 0.664(2) 0.5715(10) 0.4388(17) 0.109(7) Uiso d 1 . . H H1A 0.3140(18) 0.7706(16) 0.0882(14) 0.097(6) Uiso d 1 . . H H2 0.5807(16) 0.4070(15) 0.4476(15) 0.089(6) Uiso d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.0740(6) 0.0542(6) 0.0577(6) 0.0054(5) -0.0287(5) -0.0068(4) N1 0.0834(9) 0.0706(9) 0.0672(8) -0.0035(7) -0.0373(7) 0.0081(7) N2 0.0528(7) 0.0504(7) 0.0708(8) 0.0000(5) -0.0054(6) -0.0020(6) C1 0.0961(12) 0.0687(10) 0.0517(8) -0.0093(9) -0.0259(8) -0.0037(7) C2 0.0519(7) 0.0557(8) 0.0581(8) -0.0098(6) -0.0138(6) 0.0105(6) C3 0.0568(8) 0.0571(9) 0.0849(11) 0.0028(7) -0.0074(7) 0.0147(8) C4 0.0762(10) 0.0531(8) 0.0759(10) 0.0061(7) 0.0057(8) -0.0005(7) C5 0.0782(10) 0.0525(8) 0.0519(8) -0.0015(7) -0.0044(7) -0.0035(6) C6 0.0495(7) 0.0453(7) 0.0469(7) -0.0073(5) -0.0082(5) 0.0020(5) C7 0.0434(6) 0.0478(7) 0.0460(7) -0.0104(5) -0.0061(5) 0.0038(5) C8 0.0598(8) 0.0582(8) 0.0462(7) -0.0103(6) -0.0092(6) -0.0018(6) C9 0.0679(9) 0.0782(11) 0.0548(8) 0.0017(8) -0.0053(7) -0.0182(7) C10 0.0737(10) 0.0549(9) 0.0810(11) 0.0047(7) -0.0234(8) -0.0175(8) C11 0.0556(8) 0.0516(8) 0.0741(10) 0.0037(6) -0.0053(7) 0.0035(7) C12 0.0639(9) 0.0655(9) 0.0661(9) -0.0032(7) -0.0010(7) 0.0121(7) C13 0.0751(11) 0.0896(13) 0.0819(11) -0.0025(9) -0.0155(9) 0.0224(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C6 O1 H1 . . 111.6(12) ? C1 N1 C2 . . 108.83(12) ? C1 N1 H1A . . 126.3(13) ? C2 N1 H1A . . 124.7(13) ? C10 N2 C11 . . 113.53(12) ? C10 N2 H2 . . 109.3(12) ? C11 N2 H2 . . 105.6(12) ? N1 C1 H1B . . 124.2 ? N1 C1 C8 . . 111.52(14) ? C8 C1 H1B . . 124.2 ? N1 C2 C3 . . 129.54(13) ? N1 C2 C7 . . 107.23(13) ? C3 C2 C7 . . 123.23(13) ? C2 C3 H3 . . 121.4 ? C4 C3 C2 . . 117.17(14) ? C4 C3 H3 . . 121.4 ? C3 C4 H4 . . 119.3 ? C3 C4 C5 . . 121.49(15) ? C5 C4 H4 . . 119.3 ? C4 C5 H5 . . 119.3 ? C6 C5 C4 . . 121.49(13) ? C6 C5 H5 . . 119.3 ? O1 C6 C5 . . 118.93(11) ? O1 C6 C7 . . 122.09(12) ? C5 C6 C7 . . 118.96(12) ? C2 C7 C8 . . 107.36(11) ? C6 C7 C2 . . 117.62(12) ? C6 C7 C8 . . 135.02(12) ? C1 C8 C7 . . 105.06(13) ? C1 C8 C9 . . 124.52(14) ? C7 C8 C9 . . 130.41(12) ? C8 C9 H9A . . 108.4 ? C8 C9 H9B . . 108.4 ? C8 C9 C10 . . 115.57(13) ? H9A C9 H9B . . 107.4 ? C10 C9 H9A . . 108.4 ? C10 C9 H9B . . 108.4 ? N2 C10 C9 . . 112.14(12) ? N2 C10 H10A . . 109.2 ? N2 C10 H10B . . 109.2 ? C9 C10 H10A . . 109.2 ? C9 C10 H10B . . 109.2 ? H10A C10 H10B . . 107.9 ? N2 C11 H11A . . 109.3 ? N2 C11 H11B . . 109.3 ? N2 C11 C12 . . 111.62(13) ? H11A C11 H11B . . 108.0 ? C12 C11 H11A . . 109.3 ? C12 C11 H11B . . 109.3 ? C11 C12 H12A . . 108.7 ? C11 C12 H12B . . 108.7 ? C11 C12 C13 . . 114.03(14) ? H12A C12 H12B . . 107.6 ? C13 C12 H12A . . 108.7 ? C13 C12 H12B . . 108.7 ? C12 C13 H13A . . 109.5 ? C12 C13 H13B . . 109.5 ? C12 C13 H13C . . 109.5 ? H13A C13 H13B . . 109.5 ? H13A C13 H13C . . 109.5 ? H13B C13 H13C . . 109.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag O1 C6 . 1.3587(15) ? O1 H1 . 1.006(9) ? N1 C1 . 1.359(2) ? N1 C2 . 1.3659(19) ? N1 H1A . 0.873(9) ? N2 C10 . 1.474(2) ? N2 C11 . 1.4762(18) ? N2 H2 . 0.902(9) ? C1 H1B . 0.9300 ? C1 C8 . 1.3623(19) ? C2 C3 . 1.389(2) ? C2 C7 . 1.4142(18) ? C3 H3 . 0.9300 ? C3 C4 . 1.367(2) ? C4 H4 . 0.9300 ? C4 C5 . 1.397(2) ? C5 H5 . 0.9300 ? C5 C6 . 1.3763(19) ? C6 C7 . 1.4078(16) ? C7 C8 . 1.4397(19) ? C8 C9 . 1.499(2) ? C9 H9A . 0.9700 ? C9 H9B . 0.9700 ? C9 C10 . 1.513(2) ? C10 H10A . 0.9700 ? C10 H10B . 0.9700 ? C11 H11A . 0.9700 ? C11 H11B . 0.9700 ? C11 C12 . 1.501(2) ? C12 H12A . 0.9700 ? C12 H12B . 0.9700 ? C12 C13 . 1.508(2) ? C13 H13A . 0.9600 ? C13 H13B . 0.9600 ? C13 H13C . 0.9600 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag O1 H1 N2 . 1.006(9) 1.587(10) 2.5905(15) 175.0(19) yes N1 H1A O1 4_575 0.873(9) 2.063(10) 2.9347(16) 177.2(19) yes N2 H2 O1 3_666 0.902(9) 2.615(10) 3.4957(17) 165.6(16) yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag O1 C6 C7 C2 . . . . 176.68(11) ? O1 C6 C7 C8 . . . . -2.7(2) ? N1 C1 C8 C7 . . . . 0.13(18) ? N1 C1 C8 C9 . . . . -179.06(14) ? N1 C2 C3 C4 . . . . -179.79(15) ? N1 C2 C7 C6 . . . . -178.60(12) ? N1 C2 C7 C8 . . . . 0.94(15) ? N2 C11 C12 C13 . . . . 169.17(13) ? C1 N1 C2 C3 . . . . 179.00(15) ? C1 N1 C2 C7 . . . . -0.87(17) ? C1 C8 C9 C10 . . . . -107.09(17) ? C2 N1 C1 C8 . . . . 0.5(2) ? C2 C3 C4 C5 . . . . -1.2(2) ? C2 C7 C8 C1 . . . . -0.65(15) ? C2 C7 C8 C9 . . . . 178.47(15) ? C3 C2 C7 C6 . . . . 1.52(19) ? C3 C2 C7 C8 . . . . -178.94(13) ? C3 C4 C5 C6 . . . . 0.7(2) ? C4 C5 C6 O1 . . . . -177.74(13) ? C4 C5 C6 C7 . . . . 1.0(2) ? C5 C6 C7 C2 . . . . -2.00(18) ? C5 C6 C7 C8 . . . . 178.62(14) ? C6 C7 C8 C1 . . . . 178.77(15) ? C6 C7 C8 C9 . . . . -2.1(3) ? C7 C2 C3 C4 . . . . 0.1(2) ? C7 C8 C9 C10 . . . . 73.94(19) ? C8 C9 C10 N2 . . . . -77.85(16) ? C10 N2 C11 C12 . . . . 174.61(13) ? C11 N2 C10 C9 . . . . -101.41(15) ?