#------------------------------------------------------------------------------ #$Date: 2025-06-03 21:26:11 +0200 (Tue, 03 Jun 2025) $ #$Revision: 299930 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/34/2023476.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023476 loop_ _publ_author_name 'Lenz, Tabea' 'Hebenbrock, Marian' _publ_section_title ; Crystal structure of bis-(diiso-propyl-amino)-fluoro-borane. ; _journal_coeditor_code JY2057 _journal_issue 'Pt 5' _journal_name_full 'Acta crystallographica. Section E, Crystallographic communications' _journal_page_first 401 _journal_page_last 404 _journal_paper_doi 10.1107/S2056989025003160 _journal_volume 81 _journal_year 2025 _chemical_formula_iupac 'C12 H28 B F N2' _chemical_formula_moiety 'C12 H28 B F N2' _chemical_formula_sum 'C12 H28 B F N2' _chemical_formula_weight 230.17 _chemical_name_systematic ; Bis(diisopropylamino)fluoroborane ; _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary 'intrinsic phasing' _audit_creation_method SHELXL-2019/3 _cell_angle_alpha 84.3340(10) _cell_angle_beta 84.8200(10) _cell_angle_gamma 67.5180(10) _cell_formula_units_Z 2 _cell_length_a 6.3603(2) _cell_length_b 7.6440(3) _cell_length_c 16.4098(6) _cell_measurement_reflns_used 9941 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 29.57 _cell_measurement_theta_min 2.50 _cell_volume 732.38(5) _computing_cell_refinement ; SAINT-Plus (Bruker, 2021) ; _computing_data_collection ; APEX4 (Bruker, 2021) ; _computing_data_reduction ; SAINT-Plus (Bruker, 2021) ; _computing_molecular_graphics ; SHELXTL (Sheldrick, 2008) ; _computing_publication_material ; APEX4 (Bruker, 2021) and publCIF (Westrip, 2010) ; _computing_structure_refinement ; SHELXL2019 (L\"ubben et al., 2019; Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2018 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device_type 'Bruker D8 VENTURE with a PHOTON III CMOS detector' _diffrn_measurement_method 'f\ and w\ scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0425 _diffrn_reflns_av_unetI/netI 0.0268 _diffrn_reflns_limit_h_max 8 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_number 44165 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 29.585 _diffrn_reflns_theta_min 2.499 _diffrn_source microsource _exptl_absorpt_coefficient_mu 0.069 _exptl_absorpt_correction_T_max 0.7459 _exptl_absorpt_correction_T_min 0.5139 _exptl_absorpt_correction_type empirical _exptl_absorpt_process_details ; (SADABS; Bruker, 2021) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.044 _exptl_crystal_description plate _exptl_crystal_F_000 256 _exptl_crystal_size_max 0.500 _exptl_crystal_size_mid 0.500 _exptl_crystal_size_min 0.100 _refine_diff_density_max 0.505 _refine_diff_density_min -0.266 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.084 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 153 _refine_ls_number_reflns 4103 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.084 _refine_ls_R_factor_all 0.0450 _refine_ls_R_factor_gt 0.0420 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0628P)^2^+0.1203P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1071 _refine_ls_wR_factor_ref 0.1096 _reflns_number_gt 3776 _reflns_number_total 4103 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file jy2057.cif _cod_data_source_block I _cod_depositor_comments 'Adding full bibliography for 2023476.cif.' _cod_database_code 2023476 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.966 _shelx_estimated_absorpt_t_max 0.993 _shelx_hkl_file ; -1 0 0 1800.92 99.19 1 0 0 1685.33 97.29 1 0 0 1683.53 102.79 -2 0 0 723.43 20.10 2 0 0 704.03 20.00 -3 0 0 39.70 2.50 -3 0 0 42.90 1.70 -3 0 0 37.50 3.30 -3 0 0 40.20 2.00 -3 0 0 43.20 1.40 -3 0 0 37.50 2.80 -3 0 0 40.70 2.60 -3 0 0 35.30 3.80 -3 0 0 40.40 2.40 -3 0 0 32.30 3.30 -3 0 0 42.70 1.30 -3 0 0 40.00 4.10 3 0 0 32.90 3.20 3 0 0 34.40 4.20 3 0 0 41.30 1.70 3 0 0 36.70 2.60 3 0 0 38.10 3.50 3 0 0 38.00 2.90 3 0 0 38.80 2.40 3 0 0 42.70 1.60 3 0 0 42.00 2.10 -4 0 0 -0.50 1.20 -4 0 0 0.90 0.30 -4 0 0 0.60 0.30 -4 0 0 0.80 1.40 -4 0 0 2.10 1.20 -4 0 0 1.70 0.90 -4 0 0 1.70 0.60 -4 0 0 -0.30 1.60 -4 0 0 3.30 2.10 -4 0 0 0.40 2.20 -4 0 0 1.60 0.70 -4 0 0 1.70 2.50 4 0 0 1.50 0.70 4 0 0 3.30 2.50 4 0 0 2.70 1.30 4 0 0 1.30 0.80 4 0 0 0.30 0.30 4 0 0 1.20 1.40 4 0 0 0.20 0.80 4 0 0 -0.30 1.80 -5 0 0 177.18 6.60 -5 0 0 174.88 10.40 -5 0 0 184.98 8.20 -5 0 0 191.08 9.00 -5 0 0 193.18 6.10 -5 0 0 191.58 8.40 -5 0 0 191.88 5.20 -5 0 0 170.88 6.20 5 0 0 179.38 6.50 5 0 0 171.68 6.20 5 0 0 173.98 8.70 5 0 0 183.98 7.10 5 0 0 189.78 9.40 -6 0 0 16.00 3.00 -6 0 0 14.90 2.00 -6 0 0 14.50 3.20 -6 0 0 15.90 3.80 -6 0 0 12.30 0.90 -6 0 0 14.10 1.80 -6 0 0 15.10 4.80 6 0 0 11.30 1.80 6 0 0 11.10 3.10 6 0 0 12.50 1.90 6 0 0 13.00 4.00 6 0 0 16.70 2.00 -7 0 0 13.20 1.30 -7 0 0 14.10 2.80 -7 0 0 14.60 4.60 -7 0 0 20.60 4.10 -7 0 0 17.50 3.50 -7 0 0 17.00 2.20 -7 0 0 17.90 2.30 7 0 0 16.70 3.80 7 0 0 13.20 4.20 7 0 0 19.60 2.00 -8 0 0 3.20 3.20 -8 0 0 2.20 2.10 -8 0 0 -3.40 2.20 -8 0 0 0.10 1.20 8 0 0 1.30 0.90 8 0 0 -4.20 3.30 7 -1 0 89.49 7.40 7 -1 0 98.39 5.00 7 -1 0 98.29 8.50 -7 1 0 89.59 4.80 -7 1 0 88.69 7.70 -7 1 0 97.09 6.50 -7 1 0 111.29 7.20 -7 1 0 95.49 8.90 6 -1 0 14.60 4.20 6 -1 0 20.30 3.00 6 -1 0 19.30 3.90 6 -1 0 22.00 2.20 -6 1 0 25.20 5.10 -6 1 0 24.90 3.90 -6 1 0 19.40 2.20 -6 1 0 16.80 3.00 -6 1 0 14.80 3.70 -6 1 0 16.00 2.10 5 -1 0 252.37 8.70 5 -1 0 243.18 7.50 5 -1 0 227.58 11.00 5 -1 0 259.97 11.50 5 -1 0 254.67 11.90 -5 1 0 253.47 8.10 -5 1 0 249.78 7.20 -5 1 0 244.98 12.60 -5 1 0 237.18 10.00 -5 1 0 249.78 7.80 -5 1 0 256.77 11.50 -5 1 0 240.48 9.10 4 -1 0 10.80 0.90 4 -1 0 18.10 3.70 4 -1 0 7.00 2.70 4 -1 0 10.20 2.60 4 -1 0 12.10 1.30 4 -1 0 9.10 1.50 4 -1 0 10.60 0.90 -4 1 0 11.40 2.20 -4 1 0 10.10 0.90 -4 1 0 12.60 2.40 -4 1 0 9.40 3.30 -4 1 0 11.10 3.40 -4 1 0 11.80 2.90 -4 1 0 13.50 1.50 -4 1 0 10.30 2.30 -4 1 0 11.60 3.10 -4 1 0 11.90 1.40 3 -1 0 75.99 5.30 3 -1 0 64.59 3.20 3 -1 0 69.59 2.10 3 -1 0 62.29 3.80 3 -1 0 72.09 2.50 3 -1 0 66.29 4.60 3 -1 0 71.79 2.40 3 -1 0 60.29 4.20 -3 1 0 72.39 2.20 -3 1 0 63.39 3.80 -3 1 0 69.49 2.70 -3 1 0 74.89 5.10 -3 1 0 69.19 4.10 -3 1 0 72.89 4.00 -3 1 0 71.79 2.70 -3 1 0 69.79 5.00 -3 1 0 68.39 5.20 -3 1 0 61.99 3.70 -3 1 0 64.59 5.20 2 -1 0 94.39 3.00 2 -1 0 91.19 4.70 2 -1 0 99.29 5.20 2 -1 0 88.39 4.80 2 -1 0 92.29 3.70 2 -1 0 97.09 2.70 2 -1 0 94.19 4.10 -2 1 0 91.39 3.10 -2 1 0 103.39 5.20 -2 1 0 97.19 3.20 -2 1 0 86.49 4.90 -2 1 0 92.69 4.50 -2 1 0 86.09 5.00 -2 1 0 94.89 2.80 -2 1 0 97.19 4.60 -2 1 0 102.69 5.30 -2 1 0 101.09 4.10 -2 1 0 91.49 4.00 1 -1 0 140.89 4.60 1 -1 0 133.69 4.60 1 -1 0 141.89 5.60 1 -1 0 138.39 4.00 1 -1 0 137.09 5.40 1 -1 0 132.59 5.50 1 -1 0 140.69 5.50 -1 1 0 138.49 5.50 -1 1 0 131.49 4.50 -1 1 0 130.09 5.40 -1 1 0 140.99 4.20 -1 1 0 136.69 4.60 -1 1 0 129.89 4.00 -1 1 0 138.89 5.40 -1 1 0 140.09 5.50 -1 1 0 143.09 5.30 -1 1 0 130.09 5.20 0 -1 0 472.95 53.79 0 -1 0 439.66 55.39 0 -1 0 543.35 28.50 0 1 0 450.45 55.99 0 1 0 538.65 28.70 -2 -1 0 1485.15 66.69 -2 -1 0 1486.85 70.59 2 1 0 1053.09 73.39 2 1 0 1048.30 69.59 -3 -1 0 209.38 7.10 -3 -1 0 220.68 8.60 -3 -1 0 215.18 6.50 -3 -1 0 218.98 6.10 -3 -1 0 198.68 7.30 -3 -1 0 200.98 6.60 -3 -1 0 222.08 7.00 -3 -1 0 214.48 7.00 -3 -1 0 213.78 6.90 3 1 0 206.88 9.10 3 1 0 218.08 6.80 3 1 0 210.28 7.10 3 1 0 217.68 6.70 -4 -1 0 271.17 7.80 -4 -1 0 271.47 9.10 -4 -1 0 282.77 9.50 -4 -1 0 274.67 9.60 -4 -1 0 277.27 13.10 -4 -1 0 270.87 7.90 -4 -1 0 256.87 8.80 -4 -1 0 267.17 8.80 4 1 0 263.77 7.30 4 1 0 258.87 9.40 4 1 0 268.57 8.60 4 1 0 283.67 9.50 4 1 0 264.37 7.70 4 1 0 279.37 7.90 4 1 0 255.77 11.90 -5 -1 0 183.88 7.20 -5 -1 0 191.38 5.60 -5 -1 0 193.08 5.90 -5 -1 0 186.58 8.10 -5 -1 0 187.88 8.20 -5 -1 0 189.28 5.20 -5 -1 0 191.58 5.90 -5 -1 0 184.88 10.40 -5 -1 0 189.38 7.60 -5 -1 0 184.88 7.40 5 1 0 183.48 6.80 5 1 0 191.18 8.50 5 1 0 193.38 5.80 5 1 0 186.68 6.30 5 1 0 176.88 8.00 5 1 0 186.48 10.90 5 1 0 181.18 5.80 -6 -1 0 62.09 2.30 -6 -1 0 61.69 3.50 -6 -1 0 65.19 3.00 -6 -1 0 60.39 5.00 -6 -1 0 68.89 4.20 -6 -1 0 62.19 4.30 -6 -1 0 62.69 2.20 -6 -1 0 55.09 7.20 -6 -1 0 60.59 4.80 6 1 0 65.69 3.20 6 1 0 70.79 5.90 6 1 0 62.79 5.00 -7 -1 0 129.19 6.10 -7 -1 0 115.09 7.20 -7 -1 0 128.29 5.10 -7 -1 0 114.99 7.10 -7 -1 0 118.29 9.80 -7 -1 0 111.49 3.80 -7 -1 0 130.19 6.20 7 1 0 124.79 8.20 7 1 0 116.89 7.00 7 1 0 124.79 5.40 -8 -1 0 19.40 4.20 -8 -1 0 21.10 5.90 -8 -1 0 20.60 2.50 -8 -1 0 16.50 1.30 8 1 0 22.60 3.80 8 1 0 24.40 2.10 7 -2 0 87.89 9.30 -7 2 0 84.69 4.90 -7 2 0 93.99 8.60 -7 2 0 93.19 9.40 6 -2 0 45.80 3.40 6 -2 0 51.19 7.00 6 -2 0 46.20 6.20 6 -2 0 41.20 4.50 -6 2 0 56.59 6.40 -6 2 0 41.10 3.80 -6 2 0 54.49 4.50 -6 2 0 48.40 6.50 -6 2 0 56.19 5.60 -6 2 0 47.80 3.40 5 -2 0 83.49 4.40 5 -2 0 74.29 6.60 5 -2 0 79.89 3.00 5 -2 0 75.09 7.20 5 -2 0 72.09 5.80 -5 2 0 77.99 4.00 -5 2 0 76.89 5.20 -5 2 0 72.79 6.90 -5 2 0 72.39 5.00 -5 2 0 85.19 6.60 -5 2 0 80.79 3.70 -5 2 0 78.59 6.90 4 -2 0 34.40 1.40 4 -2 0 35.30 1.70 4 -2 0 31.40 4.20 4 -2 0 36.90 4.80 4 -2 0 29.80 4.90 4 -2 0 29.50 2.60 -4 2 0 34.90 4.10 -4 2 0 38.20 5.10 -4 2 0 28.80 4.70 -4 2 0 32.20 2.40 -4 2 0 31.00 3.60 -4 2 0 32.50 2.20 -4 2 0 35.20 2.40 -4 2 0 31.00 4.40 3 -2 0 504.05 15.30 3 -2 0 525.75 17.50 3 -2 0 511.05 16.00 3 -2 0 479.95 17.40 3 -2 0 509.15 18.00 -3 2 0 514.85 17.70 -3 2 0 484.75 15.50 -3 2 0 484.85 17.60 -3 2 0 495.85 17.60 -3 2 0 510.35 15.80 -3 2 0 512.85 14.20 -3 2 0 496.85 17.60 -3 2 0 512.15 14.50 -3 2 0 520.35 17.10 -3 2 0 519.75 14.60 -3 2 0 516.35 16.90 2 -2 0 205.58 8.80 2 -2 0 188.78 5.40 2 -2 0 195.08 7.00 2 -2 0 179.88 8.00 2 -2 0 191.78 5.70 2 -2 0 191.78 8.30 2 -2 0 192.18 6.90 -2 2 0 188.78 6.90 -2 2 0 200.08 9.00 -2 2 0 180.88 8.10 -2 2 0 179.08 6.60 -2 2 0 194.08 8.60 -2 2 0 183.48 8.40 -2 2 0 187.88 6.00 -2 2 0 182.48 6.00 -2 2 0 178.68 8.00 -2 2 0 190.38 6.20 -2 2 0 183.08 7.90 1 -2 0 31.50 1.50 1 -2 0 27.50 3.00 1 -2 0 31.00 1.90 1 -2 0 23.90 3.00 1 -2 0 31.60 3.50 1 -2 0 30.70 1.50 1 -2 0 31.30 1.80 1 -2 0 30.10 2.20 1 -2 0 32.70 3.30 -1 2 0 26.00 1.90 -1 2 0 26.60 1.60 -1 2 0 33.20 3.50 -1 2 0 34.70 3.20 -1 2 0 29.40 2.10 -1 2 0 27.10 1.70 -1 2 0 26.70 2.30 -1 2 0 30.40 3.30 -1 2 0 26.40 2.10 -1 2 0 30.50 2.90 -1 2 0 30.10 3.40 -1 -2 0 57.79 2.90 -1 -2 0 59.29 2.50 -1 -2 0 49.30 2.80 -1 -2 0 55.09 2.70 -1 -2 0 54.09 1.90 -1 -2 0 55.29 2.00 -1 -2 0 48.20 2.70 -1 -2 0 55.39 1.80 -1 -2 0 55.19 2.00 1 2 0 52.69 2.80 1 2 0 53.89 2.00 1 2 0 54.09 2.80 1 2 0 56.49 2.40 1 2 0 52.59 2.80 1 2 0 51.89 1.60 1 2 0 52.39 2.80 1 2 0 51.99 1.70 1 2 0 56.09 2.20 1 2 0 55.49 2.20 -2 -2 0 12.80 1.70 -2 -2 0 10.00 0.70 -2 -2 0 13.10 0.90 -2 -2 0 10.80 0.70 -2 -2 0 11.30 0.60 -2 -2 0 11.80 1.60 -2 -2 0 9.20 1.50 -2 -2 0 10.80 0.60 -2 -2 0 11.60 0.60 -2 -2 0 13.50 1.60 2 2 0 10.20 1.80 2 2 0 10.20 0.90 2 2 0 9.30 1.40 2 2 0 10.70 0.70 -3 -2 0 999.10 33.00 -4 -2 0 85.69 3.10 -4 -2 0 85.19 3.20 -4 -2 0 90.29 3.00 -4 -2 0 84.89 3.70 -4 -2 0 84.29 3.50 -4 -2 0 84.59 5.60 -4 -2 0 81.69 4.60 -4 -2 0 88.79 3.30 -4 -2 0 87.89 3.80 -4 -2 0 91.09 4.30 -4 -2 0 83.39 4.40 -4 -2 0 91.79 3.80 4 2 0 86.19 6.50 4 2 0 90.69 3.50 4 2 0 86.19 3.00 -5 -2 0 87.79 3.60 -5 -2 0 86.09 3.00 -5 -2 0 84.69 3.20 -5 -2 0 78.49 4.90 -5 -2 0 85.09 3.60 -5 -2 0 88.09 4.50 -5 -2 0 69.69 4.60 -5 -2 0 82.09 3.10 -5 -2 0 89.49 4.70 5 2 0 87.39 3.30 5 2 0 83.79 4.40 5 2 0 87.89 4.70 5 2 0 83.19 7.40 -6 -2 0 15.50 2.40 -6 -2 0 15.30 0.90 -6 -2 0 15.80 3.00 -6 -2 0 11.10 2.70 -6 -2 0 15.70 1.80 -6 -2 0 15.10 2.70 -6 -2 0 13.20 1.30 -6 -2 0 15.60 4.40 -6 -2 0 15.80 1.30 6 2 0 14.80 1.30 6 2 0 14.60 2.50 6 2 0 16.60 3.20 -7 -2 0 14.70 1.90 -7 -2 0 11.90 1.90 -7 -2 0 15.20 0.80 -7 -2 0 15.40 2.30 -7 -2 0 14.70 1.20 -7 -2 0 16.80 5.00 -7 -2 0 12.60 2.70 -7 -2 0 12.60 2.50 -7 -2 0 9.90 3.00 7 2 0 16.50 3.50 7 2 0 11.30 2.50 7 2 0 14.00 1.40 -8 -2 0 90.59 5.70 -8 -2 0 87.19 4.10 -8 -2 0 86.39 6.80 -8 -2 0 88.89 3.10 -8 -2 0 92.79 4.40 -8 -2 0 96.49 9.60 8 2 0 74.79 6.70 8 2 0 93.99 4.10 8 2 0 89.09 5.20 6 -3 0 358.46 17.30 -6 3 0 359.46 14.00 -6 3 0 357.26 17.10 -6 3 0 382.76 12.70 -6 3 0 372.56 16.90 5 -3 0 7.10 1.80 5 -3 0 3.20 3.00 5 -3 0 6.40 3.00 5 -3 0 7.60 0.90 -5 3 0 5.20 3.30 -5 3 0 5.90 3.80 -5 3 0 5.70 1.90 -5 3 0 6.90 1.90 -5 3 0 2.00 2.30 -5 3 0 4.80 1.70 -5 3 0 14.40 3.70 4 -3 0 1.10 1.20 4 -3 0 2.10 0.50 4 -3 0 2.30 0.40 4 -3 0 0.80 2.50 4 -3 0 6.80 3.40 4 -3 0 1.20 2.50 -4 3 0 4.00 2.50 -4 3 0 3.30 2.80 -4 3 0 3.30 1.60 -4 3 0 3.10 2.30 -4 3 0 2.40 1.20 -4 3 0 -0.90 1.80 -4 3 0 1.70 1.20 -4 3 0 1.40 1.30 3 -3 0 3.90 0.40 3 -3 0 3.10 2.60 3 -3 0 3.00 2.60 3 -3 0 2.70 2.90 3 -3 0 3.50 0.50 3 -3 0 4.50 2.90 3 -3 0 2.50 0.70 3 -3 0 3.30 1.60 -3 3 0 1.80 1.20 -3 3 0 5.40 1.60 -3 3 0 2.80 1.50 -3 3 0 4.80 2.90 -3 3 0 4.40 2.60 -3 3 0 -0.30 1.90 -3 3 0 3.40 1.20 -3 3 0 4.80 3.10 -3 3 0 3.00 2.70 -3 3 0 2.70 2.30 2 -3 0 10.90 2.90 2 -3 0 13.40 1.40 2 -3 0 11.70 2.10 2 -3 0 16.30 3.40 2 -3 0 10.20 0.90 2 -3 0 12.70 1.10 2 -3 0 8.70 2.00 2 -3 0 10.80 3.00 2 -3 0 10.00 3.20 -2 3 0 12.50 3.30 -2 3 0 13.00 3.30 -2 3 0 19.30 4.50 -2 3 0 12.00 1.90 -2 3 0 8.50 2.20 -2 3 0 9.70 2.80 -2 3 0 6.80 2.10 -2 3 0 12.50 2.00 -2 3 0 11.80 1.80 -2 3 0 13.60 3.00 -2 3 0 12.30 1.70 1 -3 0 12.70 1.20 1 -3 0 20.50 3.20 1 -3 0 13.40 2.70 1 -3 0 15.90 1.80 1 -3 0 10.70 2.80 1 -3 0 15.30 2.90 1 -3 0 17.00 2.20 1 -3 0 15.70 1.80 1 -3 0 17.60 1.90 -1 3 0 15.60 2.00 -1 3 0 10.20 2.40 -1 3 0 14.70 2.80 -1 3 0 12.80 2.40 -1 3 0 17.40 2.20 -1 3 0 17.20 3.10 -1 3 0 12.10 1.20 -1 3 0 16.10 1.70 -1 3 0 14.80 2.00 -1 3 0 15.50 2.00 0 -3 0 198.08 5.90 0 -3 0 195.48 6.00 0 -3 0 192.78 6.70 0 -3 0 193.58 6.50 0 -3 0 200.28 6.20 0 -3 0 195.88 7.80 0 -3 0 187.98 8.00 0 -3 0 188.88 7.70 0 -3 0 181.38 6.60 0 -3 0 187.88 7.40 0 3 0 191.08 8.00 0 3 0 184.68 6.00 0 3 0 190.68 6.90 0 3 0 182.38 7.50 0 3 0 183.58 7.90 0 3 0 185.98 5.50 0 3 0 193.18 7.90 0 3 0 194.98 5.50 0 3 0 195.18 6.40 0 3 0 183.78 7.00 -1 -3 0 1263.37 133.49 -1 -3 0 1395.36 148.09 -1 -3 0 1531.05 74.19 1 3 0 1620.94 75.59 -2 -3 0 465.85 14.50 -2 -3 0 478.75 14.30 -2 -3 0 493.35 14.50 2 3 0 484.15 13.90 2 3 0 470.15 14.30 2 3 0 472.85 13.80 2 3 0 445.86 14.30 2 3 0 475.35 13.30 -3 -3 0 6.90 1.50 -3 -3 0 4.20 1.60 -3 -3 0 3.70 1.30 -3 -3 0 9.60 1.80 3 3 0 3.60 1.70 -4 -3 0 1044.00 29.90 -5 -3 0 511.95 14.70 -5 -3 0 492.35 14.70 -5 -3 0 501.95 16.00 -5 -3 0 498.05 14.30 -5 -3 0 497.95 16.20 -5 -3 0 503.35 15.30 -5 -3 0 590.14 22.80 5 3 0 494.65 19.20 -6 -3 0 2.20 0.60 -6 -3 0 3.50 0.50 -6 -3 0 1.60 0.90 -6 -3 0 -2.20 2.40 -6 -3 0 0.90 1.60 -6 -3 0 0.60 1.60 -6 -3 0 -1.10 1.30 -6 -3 0 2.00 0.70 6 3 0 0.60 3.20 6 3 0 3.30 0.70 -7 -3 0 0.90 0.70 -7 -3 0 0.40 0.60 -7 -3 0 0.70 0.40 -7 -3 0 0.00 1.30 -7 -3 0 1.10 1.70 -7 -3 0 0.20 1.90 -7 -3 0 -3.00 2.40 7 3 0 -1.40 2.00 7 3 0 0.80 0.60 -8 -3 0 213.98 6.40 -8 -3 0 214.58 6.80 -8 -3 0 202.98 7.90 -8 -3 0 216.98 13.70 -8 -3 0 205.18 7.40 -8 -3 0 219.98 8.30 -8 -3 0 189.98 10.30 8 3 0 215.38 7.30 8 3 0 211.88 9.60 8 3 0 216.48 7.00 6 -4 0 4.00 1.60 6 -4 0 -4.00 4.00 -6 4 0 -3.20 3.00 -6 4 0 3.00 1.60 -6 4 0 2.30 1.40 5 -4 0 111.79 6.00 5 -4 0 105.99 9.20 5 -4 0 97.89 8.00 5 -4 0 127.09 9.20 -5 4 0 105.89 5.60 -5 4 0 126.49 8.90 -5 4 0 118.59 5.80 -5 4 0 98.49 7.40 -5 4 0 113.39 9.30 -5 4 0 93.29 7.40 -5 4 0 110.69 6.10 4 -4 0 -0.70 2.40 4 -4 0 1.60 2.40 4 -4 0 4.80 3.80 4 -4 0 0.50 1.30 -4 4 0 -4.20 1.70 -4 4 0 -3.40 2.30 -4 4 0 0.80 1.10 -4 4 0 1.10 1.10 -4 4 0 -0.20 1.70 -4 4 0 2.60 2.90 -4 4 0 -0.80 1.50 3 -4 0 12.10 3.80 3 -4 0 11.30 1.00 3 -4 0 14.70 3.70 3 -4 0 12.10 4.00 3 -4 0 12.60 2.50 3 -4 0 11.80 0.70 -3 4 0 9.50 3.70 -3 4 0 12.00 2.50 -3 4 0 11.00 3.40 -3 4 0 9.60 2.60 -3 4 0 9.20 3.60 -3 4 0 8.80 4.80 -3 4 0 10.00 1.90 -3 4 0 12.50 2.00 -3 4 0 9.90 2.10 2 -4 0 67.89 6.10 2 -4 0 68.19 2.60 2 -4 0 64.79 3.00 2 -4 0 68.09 3.30 2 -4 0 68.99 6.20 2 -4 0 65.39 4.50 2 -4 0 67.79 6.10 2 -4 0 66.29 4.10 2 -4 0 76.99 6.70 -2 4 0 58.09 5.90 -2 4 0 66.59 4.30 -2 4 0 71.79 4.40 -2 4 0 68.29 6.00 -2 4 0 65.69 6.40 -2 4 0 65.49 3.40 -2 4 0 63.79 5.60 -2 4 0 55.19 4.10 -2 4 0 57.39 6.20 -2 4 0 64.99 3.50 1 -4 0 6.00 2.80 1 -4 0 0.90 1.30 1 -4 0 -0.20 2.10 1 -4 0 2.70 1.20 1 -4 0 3.00 2.30 1 -4 0 1.70 1.10 1 -4 0 5.60 2.50 1 -4 0 2.70 1.70 -1 4 0 3.00 0.80 -1 4 0 1.00 1.70 -1 4 0 1.50 2.10 -1 4 0 1.70 1.60 -1 4 0 5.30 2.30 -1 4 0 2.20 2.60 -1 4 0 2.60 0.90 -1 4 0 2.40 2.30 -1 4 0 5.60 1.90 -1 4 0 4.20 2.70 -1 4 0 1.00 0.80 0 -4 0 432.16 13.30 0 -4 0 431.66 13.20 0 -4 0 440.76 14.50 0 -4 0 447.96 12.90 0 -4 0 430.56 15.40 0 -4 0 428.46 14.90 0 -4 0 448.66 12.60 0 -4 0 425.76 14.90 0 -4 0 425.56 13.40 0 -4 0 449.36 12.50 0 4 0 420.56 14.80 0 4 0 450.05 15.40 0 4 0 413.96 15.30 0 4 0 404.16 13.90 0 4 0 416.66 12.60 0 4 0 436.56 13.90 0 4 0 417.26 15.20 0 4 0 435.46 13.00 -1 -4 0 58.69 3.70 -1 -4 0 56.29 4.00 -1 -4 0 59.39 2.70 -1 -4 0 61.39 4.60 -1 -4 0 58.59 2.30 -1 -4 0 59.89 3.20 -1 -4 0 58.69 3.20 -1 -4 0 58.99 2.10 -1 -4 0 59.59 3.70 -1 -4 0 60.39 4.20 1 4 0 58.99 2.70 1 4 0 61.79 4.50 1 4 0 55.39 4.30 1 4 0 55.09 3.80 1 4 0 64.29 2.00 1 4 0 53.69 4.30 1 4 0 57.49 2.00 1 4 0 60.59 4.10 1 4 0 60.29 2.60 2 4 0 1042.70 28.60 2 4 0 1013.70 29.20 -3 -4 0 4.70 0.60 -3 -4 0 3.70 1.10 -3 -4 0 3.10 0.60 -3 -4 0 2.90 1.70 -3 -4 0 5.00 1.20 -3 -4 0 4.60 1.70 -3 -4 0 4.30 0.90 -3 -4 0 3.40 1.70 -3 -4 0 4.40 0.50 -3 -4 0 4.00 1.60 3 4 0 4.70 1.00 3 4 0 4.50 0.90 3 4 0 2.60 0.60 3 4 0 4.30 1.80 3 4 0 2.90 2.40 -4 -4 0 91.49 3.30 -4 -4 0 88.89 5.50 -4 -4 0 92.29 3.70 -4 -4 0 81.19 5.50 -4 -4 0 99.99 3.50 -4 -4 0 98.49 3.00 -4 -4 0 91.19 5.00 -4 -4 0 98.99 3.20 -4 -4 0 90.09 4.80 -4 -4 0 89.19 3.30 -4 -4 0 102.39 5.30 4 4 0 95.09 3.40 4 4 0 85.89 6.10 4 4 0 104.99 4.30 -5 -4 0 570.24 19.10 -5 -4 0 577.94 17.40 -5 -4 0 598.14 18.60 -5 -4 0 579.64 17.90 -5 -4 0 535.55 18.90 -5 -4 0 569.44 16.30 5 4 0 608.34 17.80 5 4 0 588.04 20.90 -6 -4 0 69.69 3.00 -6 -4 0 71.29 5.00 -6 -4 0 66.29 4.80 -6 -4 0 72.89 3.00 -6 -4 0 69.49 4.10 -6 -4 0 67.09 3.40 -6 -4 0 70.79 3.60 6 4 0 78.79 7.60 -7 -4 0 10.10 1.70 -7 -4 0 9.30 2.70 -7 -4 0 9.80 2.50 -7 -4 0 8.20 1.20 -7 -4 0 8.50 4.10 7 4 0 7.40 1.00 -8 -4 0 3.60 1.10 -8 -4 0 1.30 3.60 -8 -4 0 4.20 2.60 -8 -4 0 2.90 1.90 -8 -4 0 1.60 0.90 -8 -4 0 2.40 0.80 8 4 0 2.90 0.90 5 -5 0 2.40 1.30 5 -5 0 -4.80 3.20 5 -5 0 1.10 0.50 -5 5 0 2.90 1.70 -5 5 0 -2.20 3.20 -5 5 0 1.00 1.30 -5 5 0 0.50 1.10 4 -5 0 45.40 6.70 4 -5 0 47.30 2.00 4 -5 0 46.60 6.90 4 -5 0 49.90 7.00 4 -5 0 51.59 4.20 -4 5 0 60.49 6.70 -4 5 0 51.99 3.80 -4 5 0 44.30 3.60 -4 5 0 47.60 6.60 -4 5 0 50.79 4.70 -4 5 0 48.40 5.30 -4 5 0 49.30 7.20 -4 5 0 56.99 3.10 3 -5 0 195.08 11.20 3 -5 0 180.48 5.30 3 -5 0 192.48 6.00 3 -5 0 195.08 10.70 3 -5 0 182.48 10.90 3 -5 0 161.78 10.30 -3 5 0 188.58 7.40 -3 5 0 170.98 8.20 -3 5 0 181.48 10.90 -3 5 0 169.58 10.80 -3 5 0 203.78 10.90 -3 5 0 183.88 8.50 -3 5 0 178.78 7.50 -3 5 0 190.48 7.50 2 -5 0 661.23 24.00 2 -5 0 648.14 23.50 2 -5 0 665.03 21.20 2 -5 0 691.93 19.40 2 -5 0 689.93 18.60 2 -5 0 648.64 23.40 -2 5 0 661.63 19.90 -2 5 0 681.13 20.40 -2 5 0 672.73 19.50 -2 5 0 649.74 23.90 -2 5 0 623.94 20.90 -2 5 0 667.13 24.40 -2 5 0 649.43 23.90 -2 5 0 725.73 20.90 -2 5 0 756.62 24.50 1 -5 0 2.70 1.60 1 -5 0 4.80 1.40 1 -5 0 3.40 2.60 1 -5 0 3.90 2.00 1 -5 0 5.70 2.60 1 -5 0 6.40 3.30 1 -5 0 4.00 1.40 1 -5 0 3.40 2.30 -1 5 0 3.70 1.30 -1 5 0 4.60 2.20 -1 5 0 6.60 3.00 -1 5 0 2.30 3.20 -1 5 0 3.80 2.10 -1 5 0 5.30 1.10 -1 5 0 4.40 2.50 -1 5 0 5.20 1.10 -1 5 0 3.60 3.30 -1 5 0 5.40 2.70 0 -5 0 4.10 1.10 0 -5 0 2.40 2.20 0 -5 0 3.50 1.70 0 -5 0 3.70 2.50 0 -5 0 0.70 1.60 0 -5 0 2.40 1.60 0 -5 0 5.10 2.10 0 -5 0 1.70 2.50 0 -5 0 3.40 1.00 0 5 0 3.90 1.10 0 5 0 2.90 2.10 0 5 0 3.50 0.80 0 5 0 5.60 2.70 0 5 0 3.80 1.50 0 5 0 1.50 1.60 0 5 0 4.00 0.50 0 5 0 4.20 2.70 0 5 0 3.40 2.10 -1 -5 0 62.59 3.80 -1 -5 0 57.09 4.20 -1 -5 0 61.29 2.60 -1 -5 0 65.39 5.60 -1 -5 0 58.09 2.60 -1 -5 0 69.29 5.20 -1 -5 0 67.99 7.60 -1 -5 0 60.19 3.00 -1 -5 0 59.49 4.30 -1 -5 0 56.49 3.60 1 5 0 63.39 2.10 1 5 0 57.59 2.80 1 5 0 53.39 4.40 1 5 0 59.59 5.50 1 5 0 59.69 4.60 1 5 0 59.59 3.00 1 5 0 56.69 4.00 1 5 0 63.89 2.20 1 5 0 56.49 5.10 1 5 0 60.19 6.00 -2 -5 0 488.85 16.00 -2 -5 0 485.05 14.20 -2 -5 0 470.25 14.90 -2 -5 0 471.75 15.60 -2 -5 0 506.45 15.90 -2 -5 0 479.45 14.00 -2 -5 0 489.85 13.80 -2 -5 0 474.65 15.70 2 5 0 470.65 16.10 2 5 0 494.55 15.50 2 5 0 440.56 15.50 2 5 0 487.35 14.40 2 5 0 478.85 13.70 2 5 0 457.85 16.00 2 5 0 444.76 15.90 2 5 0 464.95 13.70 -3 -5 0 87.59 2.80 -3 -5 0 80.19 5.10 -3 -5 0 87.59 3.00 -3 -5 0 79.09 5.20 -3 -5 0 86.99 4.70 -3 -5 0 80.69 3.70 -3 -5 0 82.69 4.50 -3 -5 0 83.69 5.40 -3 -5 0 88.09 3.60 3 5 0 90.69 5.40 3 5 0 83.69 3.40 3 5 0 92.59 5.00 3 5 0 87.49 4.70 3 5 0 82.89 4.80 3 5 0 88.29 3.30 3 5 0 89.49 3.00 3 5 0 83.59 3.90 3 5 0 84.89 3.00 -4 -5 0 0.00 1.60 -4 -5 0 2.20 0.80 -4 -5 0 0.70 1.90 -4 -5 0 2.90 1.30 -4 -5 0 2.90 0.70 -4 -5 0 2.80 1.30 -4 -5 0 2.20 1.70 -4 -5 0 2.60 0.50 -4 -5 0 1.90 0.50 4 5 0 3.80 1.10 4 5 0 3.40 1.10 4 5 0 3.80 2.40 4 5 0 2.20 0.60 4 5 0 2.30 1.20 -5 -5 0 585.64 18.80 -5 -5 0 565.84 16.20 -5 -5 0 584.74 18.40 -5 -5 0 619.94 19.40 5 5 0 587.94 17.70 5 5 0 561.14 20.50 -6 -5 0 0.00 0.40 -6 -5 0 -0.10 1.30 -6 -5 0 -0.70 1.00 -6 -5 0 -0.20 1.80 -6 -5 0 -0.30 0.40 6 5 0 0.00 2.80 6 5 0 -3.00 0.90 -7 -5 0 7.70 1.20 -7 -5 0 8.40 2.60 -7 -5 0 7.90 2.40 -7 -5 0 5.90 3.60 -7 -5 0 10.40 2.00 -7 -5 0 7.20 1.10 7 5 0 7.90 4.60 -8 -5 0 14.70 1.40 -8 -5 0 12.30 4.60 -8 -5 0 11.90 2.00 -8 -5 0 16.80 3.10 -8 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5.40 0 -6 0 130.39 6.20 0 -6 0 131.39 6.60 0 -6 0 127.19 8.80 0 6 0 114.49 8.90 0 6 0 135.99 3.90 0 6 0 122.19 7.20 0 6 0 107.79 9.30 0 6 0 117.69 6.20 0 6 0 135.09 4.40 0 6 0 130.29 5.60 0 6 0 131.19 8.70 0 6 0 124.89 7.70 -1 -6 0 15.70 2.90 -1 -6 0 16.70 2.60 -1 -6 0 18.00 3.80 -1 -6 0 16.20 3.90 -1 -6 0 17.80 1.90 -1 -6 0 20.80 2.90 -1 -6 0 19.90 3.10 -1 -6 0 17.40 1.60 1 6 0 16.60 2.70 1 6 0 16.10 1.10 1 6 0 16.10 4.00 1 6 0 14.40 3.20 1 6 0 16.00 1.00 1 6 0 20.30 4.00 1 6 0 21.00 1.90 1 6 0 15.60 1.80 -2 -6 0 399.16 12.80 -2 -6 0 399.56 14.10 -2 -6 0 380.16 11.80 -2 -6 0 409.06 14.80 -2 -6 0 406.76 12.40 -2 -6 0 406.16 11.10 -2 -6 0 390.26 14.80 2 6 0 376.16 11.40 2 6 0 404.96 11.70 2 6 0 402.36 13.10 2 6 0 388.86 14.70 2 6 0 408.86 12.20 2 6 0 406.16 15.20 -3 -6 0 180.78 5.40 -3 -6 0 177.38 5.00 -3 -6 0 181.78 8.00 -3 -6 0 182.78 6.90 -3 -6 0 162.48 8.20 -3 -6 0 174.38 8.10 -3 -6 0 176.48 5.50 3 6 0 171.98 8.60 3 6 0 166.28 8.10 3 6 0 182.68 5.70 3 6 0 180.58 6.20 3 6 0 179.58 5.60 3 6 0 167.28 8.60 3 6 0 173.18 7.00 3 6 0 173.38 5.90 -4 -6 0 246.88 9.60 -4 -6 0 247.38 10.70 -4 -6 0 249.68 8.80 -4 -6 0 260.67 8.40 -4 -6 0 257.87 7.40 -4 -6 0 255.37 7.50 -4 -6 0 244.98 10.60 -4 -6 0 264.77 7.80 4 6 0 262.67 10.10 4 6 0 249.18 10.30 4 6 0 253.17 9.40 4 6 0 269.57 8.50 4 6 0 260.77 8.20 -5 -6 0 104.59 3.80 -5 -6 0 103.89 6.30 -5 -6 0 90.39 4.80 -5 -6 0 97.59 4.70 -5 -6 0 87.79 6.20 -5 -6 0 106.09 4.10 -5 -6 0 106.59 3.70 5 6 0 103.99 4.20 5 6 0 103.09 4.00 5 6 0 92.09 6.90 5 6 0 102.49 4.90 5 6 0 106.99 5.30 -6 -6 0 5.30 2.50 -6 -6 0 5.20 2.00 -6 -6 0 3.50 0.90 -6 -6 0 3.60 1.00 6 6 0 2.90 3.20 6 6 0 3.70 1.60 -7 -6 0 2.30 1.80 -7 -6 0 -0.20 1.10 -7 -6 0 2.50 2.10 -8 -6 0 8.60 1.90 -8 -6 0 10.90 3.00 -8 -6 0 7.70 1.30 -8 -6 0 6.60 1.20 -8 -6 0 8.20 2.90 -8 -6 0 9.70 4.20 3 -7 0 17.10 3.20 3 -7 0 13.50 1.80 3 -7 0 8.70 5.20 3 -7 0 4.40 3.60 -3 7 0 13.50 2.00 -3 7 0 3.20 3.50 -3 7 0 21.20 2.80 -3 7 0 12.90 2.00 -3 7 0 13.60 2.70 -3 7 0 7.50 4.40 2 -7 0 18.20 2.40 2 -7 0 11.20 4.10 2 -7 0 19.00 3.50 2 -7 0 13.90 5.00 -2 7 0 21.60 1.80 -2 7 0 18.80 1.80 -2 7 0 12.40 4.50 -2 7 0 18.20 2.80 -2 7 0 10.40 3.90 -2 7 0 20.80 3.40 1 -7 0 41.20 3.90 1 -7 0 46.00 5.80 1 -7 0 39.80 5.90 1 -7 0 52.99 7.60 1 -7 0 43.90 5.00 -1 7 0 36.90 5.90 -1 7 0 46.90 6.90 -1 7 0 48.50 6.70 -1 7 0 43.90 2.10 -1 7 0 39.40 4.60 -1 7 0 38.50 4.40 -1 7 0 39.30 3.30 -1 7 0 39.70 2.40 0 -7 0 7.50 3.60 0 -7 0 10.60 2.60 0 -7 0 11.80 2.70 0 -7 0 13.10 3.00 0 -7 0 9.00 3.80 0 7 0 9.20 1.10 0 7 0 8.60 1.80 0 7 0 12.30 3.00 0 7 0 5.70 3.40 0 7 0 9.10 0.70 0 7 0 4.80 3.90 0 7 0 3.70 2.30 0 7 0 6.80 2.40 -1 -7 0 1.30 2.40 -1 -7 0 0.30 1.40 -1 -7 0 -0.90 1.50 -1 -7 0 0.40 2.60 -1 -7 0 1.50 1.80 1 7 0 1.40 0.50 1 7 0 2.00 2.10 1 7 0 0.30 3.10 1 7 0 -1.20 1.60 1 7 0 1.00 0.90 1 7 0 0.90 2.60 1 7 0 0.20 1.20 1 7 0 0.90 0.70 -2 -7 0 36.80 2.80 -2 -7 0 38.50 5.30 -2 -7 0 32.10 4.50 -2 -7 0 36.30 3.40 -2 -7 0 40.20 4.60 2 7 0 36.00 2.60 2 7 0 31.60 5.10 2 7 0 39.60 3.30 2 7 0 33.30 4.50 2 7 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4.80 2.90 2 -5 4 6.20 2.30 2 -5 4 5.50 1.30 2 -5 4 8.30 3.60 2 -5 4 5.90 1.80 -3 5 -4 28.10 4.50 -3 5 -4 29.40 2.80 -3 5 -4 28.00 2.50 -3 5 -4 27.40 5.40 -3 5 -4 30.00 4.90 -3 5 -4 28.20 2.90 3 -5 4 21.90 3.70 3 -5 4 26.30 4.10 3 -5 4 32.00 3.10 3 -5 4 30.20 5.30 3 -5 4 31.20 1.80 -4 5 -4 -1.60 1.60 -4 5 -4 -1.10 0.80 -4 5 -4 0.50 1.20 -4 5 -4 1.30 1.10 -4 5 -4 -4.40 2.70 -4 5 -4 -1.30 3.30 4 -5 4 -1.70 1.90 4 -5 4 2.00 1.40 4 -5 4 -0.50 5.10 4 -5 4 2.10 3.60 4 -5 4 0.10 0.40 -5 5 -4 57.09 4.90 -5 5 -4 58.69 4.30 -5 5 -4 43.40 6.30 5 -5 4 36.30 5.60 5 -5 4 49.70 2.40 8 4 -4 31.90 4.30 8 4 -4 28.80 1.50 8 4 -4 23.60 6.80 -8 -4 4 23.20 4.10 -8 -4 4 28.30 2.30 -8 -4 4 28.10 1.80 -8 -4 4 27.60 1.70 -8 -4 4 24.60 2.40 -8 -4 4 23.30 3.50 -8 -4 4 31.50 2.20 7 4 -4 25.20 2.60 7 4 -4 20.90 1.20 7 4 -4 21.80 5.60 -7 -4 4 21.40 2.90 -7 -4 4 27.60 2.90 -7 -4 4 26.20 4.00 -7 -4 4 23.60 1.90 -7 -4 4 22.30 1.40 -7 -4 4 19.30 2.30 -7 -4 4 21.70 1.40 -7 -4 4 20.20 2.80 6 4 -4 0.30 0.70 6 4 -4 0.00 0.30 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0 -4 4 146.89 5.30 0 -4 4 148.79 5.60 0 -4 4 156.28 7.20 0 -4 4 146.69 5.90 0 -4 4 151.88 6.20 -1 4 -4 306.27 9.40 -1 4 -4 299.47 11.70 -1 4 -4 306.17 11.00 -1 4 -4 320.97 9.60 -1 4 -4 310.07 9.90 -1 4 -4 305.67 13.60 -1 4 -4 291.57 13.00 -1 4 -4 304.57 11.90 1 -4 4 325.17 9.90 1 -4 4 323.27 11.30 1 -4 4 300.67 9.80 1 -4 4 311.77 9.50 1 -4 4 323.87 10.10 1 -4 4 321.57 12.50 1 -4 4 309.97 10.10 1 -4 4 317.37 10.40 1 -4 4 325.77 11.10 1 -4 4 318.27 12.50 -2 4 -4 279.07 13.70 -2 4 -4 309.17 12.30 -2 4 -4 302.47 14.30 -2 4 -4 301.67 10.00 -2 4 -4 316.97 10.70 -2 4 -4 307.97 10.20 -2 4 -4 304.57 11.20 2 -4 4 298.87 13.00 2 -4 4 335.17 12.50 2 -4 4 304.97 13.10 2 -4 4 306.77 10.60 2 -4 4 321.97 9.30 2 -4 4 314.57 12.20 2 -4 4 319.07 9.50 2 -4 4 308.67 9.30 2 -4 4 322.47 13.60 -3 4 -4 141.59 10.20 -3 4 -4 149.29 8.70 -3 4 -4 160.28 6.50 -3 4 -4 149.88 6.30 -3 4 -4 158.98 8.20 -3 4 -4 149.99 7.30 3 -4 4 145.79 9.10 3 -4 4 154.78 8.30 3 -4 4 156.08 5.00 3 -4 4 158.08 8.20 3 -4 4 157.88 6.70 -4 4 -4 20.10 4.60 -4 4 -4 15.60 3.60 -4 4 -4 16.00 4.60 -4 4 -4 18.00 2.50 -4 4 -4 15.70 2.90 -4 4 -4 20.40 2.70 4 -4 4 14.90 4.10 4 -4 4 20.70 1.30 4 -4 4 19.70 3.90 4 -4 4 21.00 3.70 4 -4 4 19.60 2.60 -5 4 -4 37.40 4.20 -5 4 -4 31.60 5.20 -5 4 -4 30.20 4.10 -5 4 -4 23.70 3.20 -5 4 -4 37.10 3.20 5 -4 4 31.50 1.80 5 -4 4 33.70 9.50 5 -4 4 27.10 4.60 5 -4 4 23.70 3.10 -6 4 -4 4.00 3.00 -6 4 -4 7.40 1.90 -6 4 -4 12.50 2.80 -6 4 -4 7.70 2.10 6 -4 4 7.10 3.60 6 -4 4 7.80 1.30 6 -4 4 9.20 1.90 8 3 -4 87.59 3.50 8 3 -4 95.49 7.30 8 3 -4 105.19 11.40 8 3 -4 96.99 3.70 -8 -3 4 87.59 6.90 -8 -3 4 87.89 4.20 -8 -3 4 90.79 3.70 -8 -3 4 64.49 9.40 -8 -3 4 77.69 6.10 -8 -3 4 93.99 3.60 7 3 -4 25.10 3.50 7 3 -4 23.20 1.50 7 3 -4 14.10 5.20 7 3 -4 24.90 1.60 -7 -3 4 20.30 3.60 -7 -3 4 23.10 1.90 -7 -3 4 24.70 1.50 -7 -3 4 19.90 3.30 -7 -3 4 24.70 1.80 6 3 -4 75.29 7.80 6 3 -4 58.29 2.50 6 3 -4 64.59 2.60 6 3 -4 62.59 3.60 -6 -3 4 57.69 3.70 -6 -3 4 59.79 3.30 -6 -3 4 64.39 2.90 -6 -3 4 58.79 4.50 -6 -3 4 64.09 2.50 -6 -3 4 60.69 3.10 -6 -3 4 61.49 2.70 -6 -3 4 63.69 4.00 5 3 -4 43.40 2.20 5 3 -4 45.90 1.70 5 3 -4 46.10 3.60 5 3 -4 51.79 5.70 5 3 -4 44.50 1.80 -5 -3 4 41.10 2.70 -5 -3 4 48.10 3.10 -5 -3 4 48.10 2.80 -5 -3 4 49.70 2.00 -5 -3 4 45.10 2.70 -5 -3 4 47.50 2.30 -5 -3 4 43.70 2.50 4 3 -4 109.99 4.90 4 3 -4 103.49 3.30 4 3 -4 118.59 7.00 4 3 -4 106.49 4.00 4 3 -4 110.79 4.20 4 3 -4 113.89 3.50 -4 -3 4 103.19 3.60 -4 -3 4 110.99 5.60 -4 -3 4 115.39 4.90 -4 -3 4 107.49 3.80 -4 -3 4 100.29 4.50 -4 -3 4 114.79 5.50 -4 -3 4 98.29 4.70 -4 -3 4 105.49 3.90 -4 -3 4 112.29 3.70 -4 -3 4 106.99 4.00 -4 -3 4 111.29 3.30 -4 -3 4 109.39 3.80 3 3 -4 6.50 0.70 3 3 -4 7.70 0.70 3 3 -4 10.40 2.00 3 3 -4 7.60 1.30 3 3 -4 6.50 0.70 3 3 -4 7.00 0.60 3 3 -4 7.00 1.20 3 3 -4 7.70 1.90 3 3 -4 10.10 2.30 -3 -3 4 5.90 1.50 -3 -3 4 11.70 2.00 -3 -3 4 8.70 1.30 -3 -3 4 8.10 1.40 -3 -3 4 8.90 1.30 -3 -3 4 6.60 0.50 -3 -3 4 7.10 1.50 -3 -3 4 7.00 0.90 -3 -3 4 6.50 0.70 -3 -3 4 7.60 0.70 -3 -3 4 5.50 0.50 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2.70 -4 -6 5 82.49 3.70 -4 -6 5 79.89 3.00 -4 -6 5 88.59 5.40 -4 -6 5 82.49 5.10 3 6 -5 150.28 5.30 3 6 -5 152.08 4.50 3 6 -5 138.79 5.40 3 6 -5 155.58 7.40 3 6 -5 154.78 7.10 3 6 -5 154.38 5.30 3 6 -5 156.88 6.70 -3 -6 5 154.38 7.20 -3 -6 5 143.19 4.90 -3 -6 5 142.89 7.00 -3 -6 5 149.99 6.20 -3 -6 5 146.79 7.20 -3 -6 5 148.79 5.60 -3 -6 5 155.68 4.70 2 6 -5 0.10 0.60 2 6 -5 2.60 1.30 2 6 -5 -0.30 0.90 2 6 -5 1.30 0.70 2 6 -5 0.80 0.50 2 6 -5 1.20 0.60 2 6 -5 1.60 2.00 -2 -6 5 2.70 1.60 -2 -6 5 1.30 1.20 -2 -6 5 1.20 0.50 -2 -6 5 1.70 1.40 -2 -6 5 0.80 0.50 -2 -6 5 -0.50 1.70 -2 -6 5 2.70 1.60 1 6 -5 230.98 9.20 1 6 -5 238.68 7.20 1 6 -5 218.98 8.80 1 6 -5 245.28 10.60 1 6 -5 244.08 8.30 1 6 -5 253.37 7.60 -1 -6 5 242.58 8.80 -1 -6 5 252.47 10.00 -1 -6 5 244.68 9.40 -1 -6 5 242.28 10.90 -1 -6 5 234.48 9.40 -1 -6 5 232.98 8.30 0 6 -5 0.20 0.40 0 6 -5 0.80 1.70 0 6 -5 -0.70 0.60 0 6 -5 0.30 0.50 0 6 -5 -1.30 2.80 0 6 -5 2.00 1.40 0 -6 5 1.40 1.10 0 -6 5 1.60 1.70 0 -6 5 0.70 1.40 0 -6 5 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4.00 -3 -5 5 135.49 5.00 -3 -5 5 140.49 4.80 2 5 -5 5.50 1.40 2 5 -5 3.00 1.30 2 5 -5 3.50 0.60 2 5 -5 4.20 0.70 2 5 -5 0.80 1.20 2 5 -5 3.00 0.80 2 5 -5 3.20 0.80 -2 -5 5 3.60 1.30 -2 -5 5 4.40 1.60 -2 -5 5 3.80 0.70 -2 -5 5 3.20 0.70 -2 -5 5 7.00 2.10 -2 -5 5 2.80 0.60 -2 -5 5 3.00 1.20 -2 -5 5 4.20 1.80 -2 -5 5 3.60 1.50 1 5 -5 1.40 1.10 1 5 -5 2.10 2.90 1 5 -5 1.20 1.20 1 5 -5 0.30 0.50 1 5 -5 0.30 0.80 1 5 -5 1.30 0.70 1 5 -5 0.20 1.70 -1 -5 5 0.70 1.50 -1 -5 5 0.00 1.00 -1 -5 5 0.50 1.40 -1 -5 5 0.00 0.40 -1 -5 5 0.30 0.60 -1 -5 5 0.30 1.20 -1 -5 5 -0.50 1.10 -1 -5 5 0.00 0.40 -1 -5 5 1.30 1.70 -1 -5 5 -0.10 0.60 -1 -5 5 -1.60 1.70 0 5 -5 140.69 5.50 0 5 -5 153.88 7.00 0 5 -5 140.19 8.60 0 5 -5 144.69 8.60 0 5 -5 137.89 9.20 0 5 -5 142.19 4.80 0 -5 5 149.79 6.10 0 -5 5 148.89 8.00 0 -5 5 142.99 6.20 0 -5 5 148.89 6.20 0 -5 5 151.08 5.60 0 -5 5 143.19 7.10 0 -5 5 152.48 6.70 0 -5 5 143.49 8.10 0 -5 5 148.89 6.10 0 -5 5 142.99 6.30 -1 5 -5 37.70 5.90 -1 5 -5 32.80 5.70 -1 5 -5 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6 -8 8.70 1.50 0 6 -8 4.70 3.80 0 -6 8 6.80 2.00 0 -6 8 8.30 1.50 0 -6 8 10.40 2.40 0 -6 8 4.80 3.00 0 -6 8 10.70 1.80 0 -6 8 11.10 1.90 -1 6 -8 1.90 0.70 -1 6 -8 0.60 0.90 -1 6 -8 0.70 0.60 -1 6 -8 -0.30 1.00 -1 6 -8 2.80 1.70 1 -6 8 1.10 1.30 1 -6 8 0.60 0.80 1 -6 8 0.00 1.40 1 -6 8 2.10 1.20 1 -6 8 1.50 0.80 -2 6 -8 78.69 4.90 -2 6 -8 73.59 5.80 -2 6 -8 77.19 6.10 -2 6 -8 76.29 3.90 -2 6 -8 77.59 4.40 2 -6 8 79.09 5.40 2 -6 8 75.69 2.90 2 -6 8 72.69 5.50 2 -6 8 80.69 4.50 2 -6 8 66.19 3.90 2 -6 8 70.59 3.40 -3 6 -8 14.30 3.20 -3 6 -8 16.00 2.20 -3 6 -8 14.20 3.60 -3 6 -8 13.90 2.30 -3 6 -8 11.30 1.90 3 -6 8 15.60 1.40 3 -6 8 8.10 2.40 3 -6 8 11.50 2.10 -4 6 -8 43.60 3.60 -4 6 -8 48.00 3.80 -4 6 -8 43.20 3.50 -4 6 -8 40.10 5.90 4 -6 8 44.60 4.90 4 -6 8 42.30 2.40 4 -6 8 51.59 3.90 7 5 -8 87.69 6.20 7 5 -8 87.89 4.40 7 5 -8 90.19 4.00 7 5 -8 94.49 9.50 -7 -5 8 89.79 4.00 -7 -5 8 90.29 4.20 -7 -5 8 91.19 4.80 -7 -5 8 90.99 4.40 -7 -5 8 83.19 4.40 6 5 -8 6.20 3.40 6 5 -8 4.30 1.00 6 5 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6.60 4 4 -8 93.49 4.00 4 4 -8 95.39 3.60 -4 -4 8 93.19 3.70 -4 -4 8 91.49 4.40 -4 -4 8 100.59 4.30 -4 -4 8 93.79 4.40 -4 -4 8 97.49 4.10 -4 -4 8 99.99 3.70 3 4 -8 35.90 2.10 3 4 -8 36.30 3.80 3 4 -8 38.60 2.00 3 4 -8 34.10 3.80 3 4 -8 32.80 2.20 3 4 -8 40.20 2.10 -3 -4 8 38.70 2.90 -3 -4 8 41.10 2.70 -3 -4 8 37.00 2.60 -3 -4 8 41.10 2.10 -3 -4 8 35.80 1.90 2 4 -8 109.49 5.00 2 4 -8 107.39 4.50 2 4 -8 111.09 4.00 2 4 -8 110.69 6.50 2 4 -8 112.49 4.00 2 4 -8 104.39 4.90 2 4 -8 93.29 5.60 -2 -4 8 103.79 4.20 -2 -4 8 103.19 5.00 -2 -4 8 107.09 3.90 -2 -4 8 114.39 4.80 -2 -4 8 112.89 4.70 -2 -4 8 106.09 4.20 -2 -4 8 109.49 3.70 1 4 -8 16.40 1.30 1 4 -8 18.40 1.50 1 4 -8 16.00 1.80 1 4 -8 16.80 2.40 1 4 -8 13.70 2.90 1 4 -8 17.50 1.70 1 4 -8 15.20 1.10 1 4 -8 15.50 1.50 -1 -4 8 13.50 1.30 -1 -4 8 17.20 1.70 -1 -4 8 15.60 2.00 -1 -4 8 18.40 2.50 -1 -4 8 14.90 1.10 -1 -4 8 19.60 2.80 -1 -4 8 13.40 2.20 -1 -4 8 13.70 1.60 -1 -4 8 16.20 1.50 -1 -4 8 16.00 1.30 0 4 -8 9.60 0.90 0 4 -8 10.50 1.20 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1.50 4 3 -8 1.80 1.60 4 3 -8 4.40 1.50 -4 -3 8 3.00 0.80 -4 -3 8 3.40 1.40 -4 -3 8 3.50 1.00 -4 -3 8 3.80 0.90 -4 -3 8 2.90 0.90 -4 -3 8 2.50 0.70 3 3 -8 1.40 1.90 3 3 -8 0.10 1.40 3 3 -8 1.90 0.60 3 3 -8 1.20 0.80 3 3 -8 0.60 0.40 -3 -3 8 0.70 0.50 -3 -3 8 1.10 0.70 -3 -3 8 0.80 0.50 -3 -3 8 0.40 0.50 -3 -3 8 0.90 0.70 -3 -3 8 0.80 0.40 -3 -3 8 1.10 0.70 -3 -3 8 1.90 0.90 2 3 -8 30.30 3.00 2 3 -8 33.80 1.70 2 3 -8 36.90 2.90 2 3 -8 33.80 2.10 2 3 -8 30.50 2.90 2 3 -8 30.30 2.60 2 3 -8 32.50 1.90 2 3 -8 35.40 1.90 -2 -3 8 34.00 1.70 -2 -3 8 31.40 1.60 -2 -3 8 32.80 2.10 -2 -3 8 35.70 2.30 -2 -3 8 32.10 1.50 -2 -3 8 34.40 2.60 -2 -3 8 34.40 2.50 1 3 -8 257.37 7.50 1 3 -8 262.37 8.10 1 3 -8 256.77 8.40 1 3 -8 261.67 8.90 1 3 -8 261.77 7.60 1 3 -8 255.87 9.50 1 3 -8 254.77 7.60 1 3 -8 265.37 9.30 -1 -3 8 260.77 8.00 -1 -3 8 257.37 8.20 -1 -3 8 278.77 9.50 -1 -3 8 252.77 7.60 -1 -3 8 263.57 7.70 -1 -3 8 254.17 7.90 -1 -3 8 267.47 7.10 -1 -3 8 254.27 7.90 -1 -3 8 264.57 8.10 0 3 -8 0.60 0.30 0 3 -8 3.50 1.60 0 3 -8 2.10 1.30 0 3 -8 0.90 1.00 0 3 -8 1.30 0.50 0 3 -8 4.20 1.40 0 3 -8 1.50 0.70 0 3 -8 1.00 0.60 0 3 -8 1.20 0.40 0 3 -8 0.80 1.50 0 -3 8 -0.40 1.00 0 -3 8 0.80 0.60 0 -3 8 1.50 0.60 0 -3 8 1.30 0.50 0 -3 8 1.00 0.90 0 -3 8 1.20 0.50 0 -3 8 0.50 0.40 0 -3 8 0.90 0.60 0 -3 8 1.00 0.50 -1 3 -8 205.28 7.70 -1 3 -8 205.18 6.40 -1 3 -8 205.78 7.70 -1 3 -8 197.08 7.70 -1 3 -8 212.88 6.80 -1 3 -8 201.68 9.00 -1 3 -8 201.08 6.50 -1 3 -8 201.88 9.50 -1 3 -8 187.08 7.80 1 -3 8 211.28 6.40 1 -3 8 201.58 7.50 1 -3 8 209.28 8.00 1 -3 8 217.58 7.20 1 -3 8 207.48 7.40 1 -3 8 217.28 8.80 1 -3 8 184.48 7.00 1 -3 8 204.68 6.70 1 -3 8 207.18 6.50 1 -3 8 217.08 6.10 1 -3 8 207.18 8.80 -2 3 -8 190.08 7.80 -2 3 -8 150.68 9.00 -2 3 -8 175.38 7.20 -2 3 -8 188.48 6.40 -2 3 -8 173.68 9.70 -2 3 -8 186.98 6.00 -2 3 -8 182.88 6.80 -2 3 -8 171.38 7.60 2 -3 8 172.28 8.60 2 -3 8 172.78 8.60 2 -3 8 179.38 5.70 2 -3 8 185.08 5.00 2 -3 8 181.08 7.30 2 -3 8 172.68 7.10 2 -3 8 176.98 5.60 2 -3 8 179.08 6.40 -3 3 -8 122.69 5.30 -3 3 -8 123.09 5.80 -3 3 -8 123.99 5.90 -3 3 -8 127.69 6.10 -3 3 -8 121.19 6.60 -3 3 -8 121.09 9.00 3 -3 8 120.89 4.10 3 -3 8 124.59 6.20 3 -3 8 124.09 7.70 3 -3 8 114.29 4.10 3 -3 8 115.19 5.10 3 -3 8 129.09 5.90 -4 3 -8 5.80 2.00 -4 3 -8 3.90 4.00 -4 3 -8 4.80 2.70 -4 3 -8 6.20 1.40 -4 3 -8 6.40 1.60 -4 3 -8 5.60 1.50 4 -3 8 5.50 0.90 4 -3 8 6.20 0.90 4 -3 8 4.20 1.70 4 -3 8 5.50 1.60 4 -3 8 6.50 1.50 4 -3 8 6.10 3.00 -5 3 -8 1.10 1.10 -5 3 -8 -5.50 3.40 -5 3 -8 0.70 1.60 -5 3 -8 1.80 1.40 -5 3 -8 0.00 0.70 -5 3 -8 0.70 1.00 5 -3 8 0.60 0.90 5 -3 8 0.00 0.80 5 -3 8 -2.10 3.00 5 -3 8 -1.10 1.10 5 -3 8 -0.10 0.60 -6 3 -8 7.10 2.20 -6 3 -8 5.50 1.60 -6 3 -8 6.20 2.50 6 -3 8 2.00 1.90 6 -3 8 5.50 1.60 6 -3 8 3.80 1.20 7 2 -8 35.20 2.20 7 2 -8 24.20 4.20 7 2 -8 25.30 6.50 7 2 -8 30.90 1.70 -7 -2 8 30.50 1.90 -7 -2 8 29.50 4.30 -7 -2 8 27.70 4.40 -7 -2 8 31.00 2.10 -7 -2 8 29.70 2.40 6 2 -8 4.20 0.90 6 2 -8 4.30 1.80 6 2 -8 0.70 2.10 6 2 -8 2.60 3.30 6 2 -8 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212.88 6.90 0 -4 9 209.78 7.30 0 -4 9 213.18 6.80 0 -4 9 220.48 9.60 0 -4 9 227.98 7.10 0 -4 9 214.88 9.20 -1 4 -9 2.70 2.60 -1 4 -9 2.80 0.80 -1 4 -9 1.30 2.80 -1 4 -9 2.40 1.10 -1 4 -9 1.60 0.80 -1 4 -9 1.90 1.10 -1 4 -9 3.10 1.70 -1 4 -9 2.90 0.80 1 -4 9 1.70 0.80 1 -4 9 2.60 2.00 1 -4 9 1.90 0.60 1 -4 9 1.20 1.00 1 -4 9 4.60 1.60 1 -4 9 2.50 1.00 1 -4 9 2.80 0.80 1 -4 9 1.00 2.10 -2 4 -9 148.19 10.30 -2 4 -9 158.98 7.60 -2 4 -9 157.68 5.70 -2 4 -9 148.69 6.00 -2 4 -9 153.78 5.80 -2 4 -9 150.28 7.10 2 -4 9 158.28 6.00 2 -4 9 156.48 4.50 2 -4 9 151.58 6.80 2 -4 9 143.59 5.30 2 -4 9 152.58 5.90 2 -4 9 155.98 5.20 2 -4 9 150.38 6.90 2 -4 9 137.49 8.60 -3 4 -9 23.70 2.20 -3 4 -9 21.00 2.00 -3 4 -9 18.60 5.60 -3 4 -9 22.90 3.00 -3 4 -9 20.10 2.80 -3 4 -9 20.40 3.40 3 -4 9 20.70 3.00 3 -4 9 19.10 2.40 3 -4 9 20.00 1.40 3 -4 9 20.30 1.60 3 -4 9 19.90 2.80 3 -4 9 15.10 4.20 -4 4 -9 91.79 6.60 -4 4 -9 98.59 5.20 -4 4 -9 93.69 5.80 -4 4 -9 88.59 5.40 -4 4 -9 97.19 10.40 -4 4 -9 106.29 4.90 4 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3 -9 1.90 0.70 3 3 -9 2.20 0.90 3 3 -9 1.80 2.00 3 3 -9 1.70 0.60 3 3 -9 1.90 0.70 3 3 -9 2.20 1.60 -3 -3 9 2.00 0.60 -3 -3 9 1.50 0.60 -3 -3 9 1.60 0.70 -3 -3 9 1.80 0.60 -3 -3 9 1.60 0.80 -3 -3 9 1.10 0.70 2 3 -9 921.11 27.30 2 3 -9 988.40 28.00 2 3 -9 953.60 26.50 2 3 -9 944.01 28.90 -2 -3 9 979.10 27.40 -2 -3 9 979.00 26.00 1 3 -9 1.00 0.80 1 3 -9 0.40 0.40 1 3 -9 0.00 0.40 1 3 -9 0.90 0.70 1 3 -9 0.60 0.40 1 3 -9 0.00 1.30 1 3 -9 1.20 1.20 1 3 -9 0.80 1.10 1 3 -9 0.40 0.30 1 3 -9 1.20 0.60 -1 -3 9 0.50 1.00 -1 -3 9 0.40 0.50 -1 -3 9 0.10 0.50 -1 -3 9 0.70 0.50 -1 -3 9 0.50 0.30 -1 -3 9 0.10 0.30 -1 -3 9 0.40 0.60 -1 -3 9 1.00 0.50 -1 -3 9 1.20 0.30 -1 -3 9 0.30 0.60 0 3 -9 63.09 3.50 0 3 -9 75.59 3.60 0 3 -9 68.19 4.00 0 3 -9 70.29 3.50 0 3 -9 69.79 4.30 0 3 -9 74.79 2.80 0 3 -9 63.79 4.20 0 3 -9 68.49 2.90 0 3 -9 63.39 4.60 0 3 -9 70.19 2.70 0 -3 9 72.19 3.50 0 -3 9 74.99 2.70 0 -3 9 77.39 4.60 0 -3 9 76.49 2.90 0 -3 9 76.39 3.20 0 -3 9 73.69 3.00 0 -3 9 75.49 4.30 0 -3 9 73.69 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-10 18.40 2.70 2 7 -10 20.70 1.80 2 7 -10 20.80 1.40 2 7 -10 20.00 2.90 2 7 -10 17.10 4.60 -2 -7 10 20.30 1.60 -2 -7 10 19.40 2.60 -2 -7 10 21.20 2.40 -2 -7 10 15.50 3.80 -2 -7 10 23.40 1.50 -2 -7 10 18.50 2.50 1 7 -10 4.20 1.40 1 7 -10 3.30 1.10 1 7 -10 4.70 1.40 1 7 -10 3.20 0.90 1 7 -10 -6.10 3.30 1 7 -10 4.90 1.80 -1 -7 10 3.00 1.40 -1 -7 10 5.10 1.50 -1 -7 10 5.10 1.00 -1 -7 10 3.40 0.90 -1 -7 10 4.70 2.90 0 7 -10 5.50 1.20 0 7 -10 3.80 0.90 0 7 -10 4.10 1.50 0 7 -10 3.10 1.80 0 7 -10 4.80 1.30 0 -7 10 3.70 1.60 0 -7 10 4.00 1.20 0 -7 10 5.30 1.30 0 -7 10 4.20 1.30 0 -7 10 4.80 1.20 -1 7 -10 7.70 2.40 -1 7 -10 11.60 2.00 -1 7 -10 9.70 2.40 -1 7 -10 10.40 1.50 -1 7 -10 8.10 1.30 1 -7 10 9.20 2.00 1 -7 10 8.90 1.40 1 -7 10 10.00 1.30 1 -7 10 11.20 1.90 1 -7 10 13.20 2.90 -2 7 -10 0.20 1.60 -2 7 -10 3.00 1.90 -2 7 -10 1.30 1.10 -2 7 -10 2.00 0.90 -2 7 -10 0.90 0.90 2 -7 10 1.40 1.40 2 -7 10 3.50 1.20 2 -7 10 1.00 1.60 2 -7 10 1.50 0.50 2 -7 10 1.60 0.70 7 6 -10 11.80 1.70 7 6 -10 9.50 2.80 7 6 -10 8.70 4.90 -7 -6 10 8.60 1.50 -7 -6 10 11.60 1.80 -7 -6 10 10.40 1.80 -7 -6 10 9.20 1.80 6 6 -10 62.69 4.20 6 6 -10 65.59 3.30 6 6 -10 71.29 5.10 6 6 -10 60.69 7.70 -6 -6 10 63.89 3.40 -6 -6 10 54.29 4.10 -6 -6 10 62.69 3.90 -6 -6 10 63.59 3.40 5 6 -10 15.90 4.10 5 6 -10 17.10 1.60 5 6 -10 18.50 2.80 5 6 -10 14.70 2.40 -5 -6 10 14.30 2.60 -5 -6 10 16.70 3.50 -5 -6 10 17.50 1.60 -5 -6 10 17.00 1.90 -5 -6 10 12.80 2.10 4 6 -10 20.10 2.50 4 6 -10 22.30 2.00 4 6 -10 25.70 1.80 4 6 -10 21.40 1.80 -4 -6 10 27.40 1.80 -4 -6 10 23.70 3.60 -4 -6 10 24.30 2.50 -4 -6 10 21.00 1.80 -4 -6 10 23.10 1.80 -4 -6 10 22.10 3.10 3 6 -10 16.80 3.20 3 6 -10 12.00 1.40 3 6 -10 14.50 2.00 3 6 -10 14.40 1.90 3 6 -10 12.90 2.80 -3 -6 10 13.70 2.70 -3 -6 10 14.50 1.20 -3 -6 10 14.90 2.20 -3 -6 10 16.30 3.00 2 6 -10 8.50 1.70 2 6 -10 6.80 0.80 2 6 -10 7.20 1.40 2 6 -10 4.40 2.30 2 6 -10 6.40 1.90 2 6 -10 7.00 1.20 2 6 -10 7.80 1.30 -2 -6 10 7.50 1.00 -2 -6 10 6.50 2.20 -2 -6 10 7.80 1.70 -2 -6 10 6.30 1.40 -2 -6 10 8.50 0.80 -2 -6 10 9.40 1.80 1 6 -10 529.45 17.30 1 6 -10 490.15 15.30 1 6 -10 529.25 15.40 1 6 -10 508.35 16.40 1 6 -10 502.35 19.60 1 6 -10 511.95 14.80 1 6 -10 543.05 15.70 -1 -6 10 492.65 15.10 -1 -6 10 521.55 19.10 -1 -6 10 541.15 16.70 -1 -6 10 526.15 15.80 -1 -6 10 521.65 15.30 -1 -6 10 524.35 15.80 0 6 -10 127.69 4.90 0 6 -10 125.39 4.60 0 6 -10 105.29 9.10 0 6 -10 128.09 5.20 0 6 -10 122.09 6.80 0 6 -10 132.19 6.50 0 -6 10 127.29 5.10 0 -6 10 126.29 6.40 0 -6 10 117.89 5.00 0 -6 10 131.59 5.30 0 -6 10 128.09 5.60 0 -6 10 126.19 8.70 -1 6 -10 0.10 0.60 -1 6 -10 -1.20 0.90 -1 6 -10 0.10 0.80 -1 6 -10 1.40 1.30 1 -6 10 0.60 0.90 1 -6 10 0.30 0.60 1 -6 10 1.10 0.60 1 -6 10 -0.90 1.00 1 -6 10 -0.40 0.70 -2 6 -10 65.19 3.50 -2 6 -10 67.49 3.90 -2 6 -10 65.79 3.60 -2 6 -10 69.79 5.60 -2 6 -10 66.79 5.30 2 -6 10 65.99 3.20 2 -6 10 63.19 4.60 2 -6 10 61.49 4.90 2 -6 10 66.09 3.90 -3 6 -10 19.10 3.90 -3 6 -10 20.50 2.60 -3 6 -10 17.20 3.20 -3 6 -10 21.30 3.80 -3 6 -10 21.60 2.40 3 -6 10 15.90 3.00 3 -6 10 16.60 2.40 3 -6 10 21.70 3.70 3 -6 10 19.90 1.60 7 5 -10 0.90 0.80 7 5 -10 1.80 5.20 7 5 -10 -0.30 1.60 -7 -5 10 1.40 1.20 -7 -5 10 2.50 1.30 -7 -5 10 1.90 1.00 -7 -5 10 0.80 0.90 6 5 -10 -2.00 1.10 6 5 -10 0.70 0.60 6 5 -10 0.70 0.70 6 5 -10 2.90 3.30 -6 -5 10 2.10 0.70 -6 -5 10 1.20 0.90 -6 -5 10 1.20 0.80 -6 -5 10 1.00 0.70 -6 -5 10 0.70 0.80 5 5 -10 6.50 1.40 5 5 -10 6.40 1.10 5 5 -10 5.80 1.80 5 5 -10 8.60 3.50 -5 -5 10 7.80 1.20 -5 -5 10 7.80 1.50 -5 -5 10 7.10 1.60 -5 -5 10 6.10 1.10 -5 -5 10 7.80 1.70 -5 -5 10 6.60 1.40 4 5 -10 34.20 2.80 4 5 -10 38.90 5.20 4 5 -10 37.50 2.30 4 5 -10 31.80 2.40 -4 -5 10 38.00 2.40 -4 -5 10 34.90 2.70 -4 -5 10 32.30 2.70 -4 -5 10 36.70 2.30 -4 -5 10 28.20 2.40 -4 -5 10 33.00 2.90 3 5 -10 61.49 3.30 3 5 -10 62.59 4.90 3 5 -10 61.59 4.10 3 5 -10 56.39 2.80 3 5 -10 59.79 3.20 3 5 -10 60.89 3.00 -3 -5 10 62.19 3.50 -3 -5 10 60.49 2.70 -3 -5 10 55.49 4.00 -3 -5 10 58.39 3.40 2 5 -10 100.29 4.00 2 5 -10 99.59 4.40 2 5 -10 106.09 5.30 2 5 -10 104.59 4.10 2 5 -10 99.49 4.70 2 5 -10 102.89 5.90 -2 -5 10 105.39 4.70 -2 -5 10 110.79 6.00 -2 -5 10 108.69 4.60 -2 -5 10 102.79 4.70 -2 -5 10 99.39 3.80 1 5 -10 31.60 1.80 1 5 -10 26.00 1.80 1 5 -10 29.60 2.40 1 5 -10 26.70 2.20 1 5 -10 26.80 3.80 1 5 -10 27.40 2.50 1 5 -10 30.40 2.20 -1 -5 10 30.70 2.30 -1 -5 10 26.70 2.20 -1 -5 10 27.10 3.60 -1 -5 10 32.10 1.70 -1 -5 10 28.40 2.40 -1 -5 10 30.70 1.90 0 5 -10 188.88 10.30 0 5 -10 207.18 6.80 0 5 -10 205.18 8.50 0 5 -10 199.68 6.50 0 5 -10 200.18 7.70 0 5 -10 208.38 7.00 0 5 -10 208.58 8.20 0 -5 10 203.08 9.90 0 -5 10 202.28 7.00 0 -5 10 216.98 6.90 0 -5 10 214.68 8.30 0 -5 10 205.98 6.90 0 -5 10 197.48 7.30 -1 5 -10 51.59 4.00 -1 5 -10 49.20 2.80 -1 5 -10 52.09 2.80 -1 5 -10 49.40 4.00 -1 5 -10 47.40 2.60 1 -5 10 49.50 3.70 1 -5 10 52.09 3.50 1 -5 10 50.59 2.30 1 -5 10 47.70 6.30 1 -5 10 51.19 3.80 1 -5 10 45.10 3.70 1 -5 10 49.20 2.90 -2 5 -10 -4.80 4.00 -2 5 -10 4.40 1.70 -2 5 -10 3.80 1.70 -2 5 -10 5.20 1.20 -2 5 -10 4.80 1.80 -2 5 -10 4.50 1.10 2 -5 10 4.10 1.70 2 -5 10 5.30 0.60 2 -5 10 3.10 1.10 2 -5 10 3.40 1.40 2 -5 10 3.20 0.80 2 -5 10 3.80 1.50 -3 5 -10 18.00 2.30 -3 5 -10 14.60 2.70 -3 5 -10 10.80 2.70 -3 5 -10 5.10 5.10 -3 5 -10 12.90 1.90 -3 5 -10 15.30 2.20 3 -5 10 13.30 2.10 3 -5 10 13.30 1.30 3 -5 10 12.80 2.50 3 -5 10 15.30 2.80 -4 5 -10 26.50 2.60 -4 5 -10 21.30 3.80 -4 5 -10 20.30 3.00 -4 5 -10 18.90 3.10 4 -5 10 27.30 3.80 4 -5 10 20.00 1.70 4 -5 10 19.70 2.70 7 4 -10 13.80 5.60 7 4 -10 17.40 1.90 -7 -4 10 21.20 1.90 6 4 -10 2.90 3.10 6 4 -10 5.50 1.30 6 4 -10 5.30 2.10 6 4 -10 6.00 1.10 -6 -4 10 5.90 1.50 -6 -4 10 5.30 1.20 -6 -4 10 5.80 1.20 -6 -4 10 3.40 1.00 -6 -4 10 6.90 0.90 -6 -4 10 2.10 1.60 5 4 -10 17.90 4.20 5 4 -10 14.70 2.50 5 4 -10 17.40 2.80 5 4 -10 20.30 2.30 5 4 -10 16.80 1.60 5 4 -10 15.60 1.50 -5 -4 10 12.50 1.70 -5 -4 10 15.20 1.70 -5 -4 10 14.80 1.60 -5 -4 10 15.70 1.50 -5 -4 10 16.70 1.50 4 4 -10 113.69 4.30 4 4 -10 103.99 7.30 4 4 -10 112.59 4.80 4 4 -10 108.19 5.20 -4 -4 10 114.89 4.40 -4 -4 10 106.79 4.30 -4 -4 10 112.79 4.70 -4 -4 10 110.39 5.00 -4 -4 10 107.79 4.20 -4 -4 10 112.29 4.80 3 4 -10 16.50 1.50 3 4 -10 14.30 1.90 3 4 -10 16.90 1.90 3 4 -10 15.40 3.00 -3 -4 10 16.70 1.30 -3 -4 10 17.20 1.50 -3 -4 10 16.40 2.10 -3 -4 10 14.60 1.30 -3 -4 10 15.70 1.90 -3 -4 10 16.30 1.80 2 4 -10 66.79 4.00 2 4 -10 58.39 2.90 2 4 -10 64.99 2.70 2 4 -10 58.39 3.10 2 4 -10 62.09 3.80 2 4 -10 63.29 2.90 -2 -4 10 60.09 3.10 -2 -4 10 61.39 3.80 -2 -4 10 65.09 2.60 -2 -4 10 59.39 3.10 1 4 -10 23.40 2.00 1 4 -10 22.90 1.50 1 4 -10 21.80 2.80 1 4 -10 28.40 5.30 1 4 -10 25.80 2.00 1 4 -10 22.20 1.90 1 4 -10 21.70 1.90 1 4 -10 24.40 1.50 -1 -4 10 24.00 2.70 -1 -4 10 24.50 1.80 -1 -4 10 19.80 1.70 -1 -4 10 24.50 1.80 -1 -4 10 24.40 1.60 -1 -4 10 23.60 1.10 -1 -4 10 22.20 1.90 0 4 -10 65.19 2.80 0 4 -10 62.99 2.70 0 4 -10 62.59 3.70 0 4 -10 65.09 4.40 0 4 -10 63.09 5.80 0 4 -10 70.09 3.80 0 4 -10 67.09 5.00 0 4 -10 69.59 3.00 0 -4 10 67.89 3.60 0 -4 10 65.09 3.20 0 -4 10 64.79 2.80 0 -4 10 67.19 4.20 0 -4 10 86.89 6.00 0 -4 10 66.59 2.90 0 -4 10 67.29 3.10 0 -4 10 69.19 3.10 0 -4 10 64.39 5.20 -1 4 -10 5.00 1.90 -1 4 -10 3.60 1.20 -1 4 -10 8.30 1.70 -1 4 -10 4.20 0.90 -1 4 -10 6.20 1.00 -1 4 -10 5.10 2.70 -1 4 -10 3.30 3.10 -1 4 -10 3.90 0.90 1 -4 10 4.80 1.20 1 -4 10 3.10 2.30 1 -4 10 4.40 1.10 1 -4 10 4.40 0.80 1 -4 10 4.60 1.30 1 -4 10 7.80 1.80 1 -4 10 4.50 2.10 1 -4 10 5.30 1.10 -2 4 -10 3.40 3.70 -2 4 -10 4.40 1.10 -2 4 -10 3.10 1.20 -2 4 -10 2.20 1.30 -2 4 -10 3.20 1.00 -2 4 -10 4.00 1.00 2 -4 10 4.40 0.80 2 -4 10 4.30 1.00 2 -4 10 4.00 1.10 2 -4 10 3.60 0.50 2 -4 10 6.20 1.50 2 -4 10 2.30 2.60 2 -4 10 4.20 1.40 2 -4 10 3.30 1.30 -3 4 -10 52.49 3.90 -3 4 -10 52.79 4.50 -3 4 -10 62.49 4.00 -3 4 -10 48.40 7.40 -3 4 -10 64.19 3.60 -3 4 -10 54.89 3.10 3 -4 10 57.59 6.80 3 -4 10 54.09 2.60 3 -4 10 53.39 2.60 3 -4 10 54.59 3.80 3 -4 10 60.69 4.10 3 -4 10 54.29 4.10 -4 4 -10 0.10 1.00 -4 4 -10 0.10 0.90 -4 4 -10 -0.40 0.80 -4 4 -10 -0.40 1.00 -4 4 -10 0.50 0.90 4 -4 10 0.10 0.50 4 -4 10 -0.70 3.60 4 -4 10 -1.10 0.80 4 -4 10 0.60 0.80 4 -4 10 -0.80 1.00 -5 4 -10 16.00 3.10 -5 4 -10 11.50 2.50 -5 4 -10 13.50 3.10 -5 4 -10 18.00 2.30 5 -4 10 18.70 1.80 5 -4 10 19.40 3.20 7 3 -10 53.99 8.70 7 3 -10 63.39 5.40 -7 -3 10 76.19 6.30 -7 -3 10 65.19 6.00 -7 -3 10 67.19 3.50 -7 -3 10 66.69 4.50 -7 -3 10 60.79 3.10 6 3 -10 19.10 2.60 6 3 -10 15.70 4.70 6 3 -10 23.90 3.60 6 3 -10 15.90 1.40 6 3 -10 19.90 3.10 -6 -3 10 22.00 2.90 -6 -3 10 18.30 1.70 -6 -3 10 19.90 1.80 -6 -3 10 19.00 1.70 5 3 -10 55.19 4.10 5 3 -10 57.39 3.30 5 3 -10 56.39 6.30 5 3 -10 59.79 3.80 5 3 -10 56.09 4.20 -5 -3 10 59.49 2.90 -5 -3 10 57.89 2.90 -5 -3 10 56.79 3.40 -5 -3 10 52.09 3.90 -5 -3 10 56.19 3.00 -5 -3 10 56.59 2.20 4 3 -10 118.19 5.30 4 3 -10 118.59 4.50 4 3 -10 112.69 5.70 4 3 -10 112.99 5.50 4 3 -10 126.59 7.90 -4 -3 10 115.39 4.70 -4 -3 10 114.79 4.50 -4 -3 10 122.49 6.00 -4 -3 10 116.79 4.30 -4 -3 10 115.79 4.00 -4 -3 10 114.29 4.70 3 3 -10 115.99 4.60 3 3 -10 108.29 5.60 3 3 -10 117.29 4.90 3 3 -10 111.39 4.40 3 3 -10 123.49 6.90 3 3 -10 115.09 4.30 -3 -3 10 114.79 4.10 -3 -3 10 118.19 4.80 -3 -3 10 113.59 4.10 -3 -3 10 114.29 4.40 -3 -3 10 118.39 4.40 -3 -3 10 111.49 4.60 2 3 -10 53.79 2.60 2 3 -10 49.50 3.80 2 3 -10 55.19 3.70 2 3 -10 55.29 3.90 2 3 -10 53.69 2.60 2 3 -10 52.89 2.90 -2 -3 10 52.59 2.40 -2 -3 10 51.49 2.50 -2 -3 10 54.19 2.50 -2 -3 10 50.39 2.20 -2 -3 10 53.99 3.10 -2 -3 10 49.50 2.50 -2 -3 10 52.39 2.50 1 3 -10 24.00 1.40 1 3 -10 24.60 1.40 1 3 -10 22.80 1.80 1 3 -10 24.00 1.80 1 3 -10 27.40 2.30 1 3 -10 21.10 2.80 1 3 -10 27.50 2.70 1 3 -10 23.40 1.70 1 3 -10 24.40 1.80 1 3 -10 23.10 2.90 -1 -3 10 23.00 1.50 -1 -3 10 26.00 1.80 -1 -3 10 21.90 1.60 -1 -3 10 27.00 2.60 -1 -3 10 20.70 1.50 -1 -3 10 22.60 1.40 -1 -3 10 24.80 2.30 -1 -3 10 23.50 0.90 -1 -3 10 27.00 2.60 0 3 -10 2.90 0.60 0 3 -10 3.40 1.40 0 3 -10 1.60 0.50 0 3 -10 1.90 0.70 0 3 -10 0.10 1.20 0 3 -10 1.00 1.10 0 3 -10 1.00 0.60 0 3 -10 1.50 0.60 0 3 -10 0.90 1.50 0 -3 10 1.20 0.70 0 -3 10 4.30 0.80 0 -3 10 2.80 1.50 0 -3 10 1.60 0.60 0 -3 10 2.00 0.50 0 -3 10 3.10 1.30 0 -3 10 2.40 0.70 0 -3 10 2.00 0.60 -1 3 -10 6.00 1.00 -1 3 -10 6.30 1.30 -1 3 -10 6.00 0.90 -1 3 -10 3.10 1.80 -1 3 -10 5.00 1.20 -1 3 -10 4.10 3.20 -1 3 -10 6.70 1.70 -1 3 -10 4.70 0.80 -1 3 -10 3.90 2.40 1 -3 10 6.60 1.80 1 -3 10 5.20 2.00 1 -3 10 4.90 1.20 1 -3 10 7.20 1.20 1 -3 10 6.10 0.90 1 -3 10 5.60 1.10 1 -3 10 5.80 0.70 1 -3 10 5.70 0.90 -2 3 -10 17.60 2.00 -2 3 -10 18.00 1.80 -2 3 -10 20.00 1.40 -2 3 -10 20.60 1.70 -2 3 -10 19.40 2.50 -2 3 -10 17.80 4.10 2 -3 10 20.00 1.70 2 -3 10 23.10 2.10 2 -3 10 18.30 2.00 2 -3 10 29.50 4.10 2 -3 10 19.80 1.40 2 -3 10 18.00 1.30 2 -3 10 18.50 2.00 2 -3 10 18.40 0.90 -3 3 -10 154.18 6.70 -3 3 -10 161.98 7.60 -3 3 -10 147.79 10.20 -3 3 -10 171.78 5.70 -3 3 -10 164.88 7.10 -3 3 -10 153.08 6.30 3 -3 10 155.98 5.10 3 -3 10 179.98 7.30 3 -3 10 161.88 5.30 3 -3 10 167.68 6.20 3 -3 10 158.28 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5 -14 9.10 2.70 6 5 -14 12.20 1.90 -6 -5 14 7.10 1.40 -6 -5 14 11.20 1.80 -6 -5 14 11.20 2.00 5 5 -14 0.90 1.50 5 5 -14 2.10 0.90 5 5 -14 5.90 3.70 -5 -5 14 2.60 0.80 -5 -5 14 2.50 1.00 -5 -5 14 1.10 0.80 -5 -5 14 2.30 1.00 4 5 -14 19.30 3.30 4 5 -14 13.30 1.80 4 5 -14 16.00 2.60 4 5 -14 16.20 2.70 4 5 -14 13.20 4.00 -4 -5 14 15.40 1.70 -4 -5 14 17.60 3.10 -4 -5 14 14.80 1.70 -4 -5 14 16.30 1.50 -4 -5 14 13.40 1.80 3 5 -14 3.50 1.40 3 5 -14 3.50 1.70 3 5 -14 2.30 2.40 3 5 -14 3.90 1.10 -3 -5 14 3.50 0.90 -3 -5 14 3.40 0.90 -3 -5 14 4.70 1.20 -3 -5 14 5.30 1.00 -3 -5 14 4.40 1.10 2 5 -14 149.99 8.20 2 5 -14 156.38 6.10 2 5 -14 153.48 7.70 2 5 -14 147.69 6.20 -2 -5 14 160.98 5.70 -2 -5 14 160.28 5.50 -2 -5 14 156.48 5.80 -2 -5 14 165.08 5.70 -2 -5 14 153.48 6.10 -2 -5 14 158.38 8.30 1 5 -14 19.10 1.70 1 5 -14 15.20 1.90 1 5 -14 19.40 2.10 1 5 -14 17.70 2.00 1 5 -14 17.50 1.50 1 5 -14 17.50 2.40 1 5 -14 13.30 3.40 -1 -5 14 18.00 1.50 -1 -5 14 19.60 3.80 -1 -5 14 19.30 1.60 -1 -5 14 17.40 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27.90 2.50 1 -1 21 25.00 4.30 1 -1 21 22.20 2.60 -2 1 -21 10.30 1.50 -2 1 -21 13.50 2.20 -2 1 -21 14.00 1.60 -2 1 -21 11.70 2.10 2 -1 21 11.70 1.70 2 -1 21 11.90 2.10 2 -1 21 9.00 2.30 2 0 -21 0.40 1.60 -2 0 21 2.30 1.60 -2 0 21 6.40 2.50 -2 0 21 3.90 1.60 -2 0 21 1.60 1.10 -2 0 21 0.90 1.30 1 0 -21 4.70 2.20 1 0 -21 13.40 2.60 1 0 -21 14.90 2.60 1 0 -21 6.90 1.90 1 0 -21 6.50 3.00 -1 0 21 12.90 2.70 -1 0 21 6.90 1.70 -1 0 21 7.70 1.40 -1 0 21 6.90 1.90 -1 0 21 11.40 2.50 0 0 -21 6.80 1.50 0 0 -21 10.70 2.00 0 0 -21 13.10 2.60 0 0 -21 5.50 2.30 0 0 -21 4.60 1.60 0 0 21 8.20 2.00 0 0 21 12.60 2.30 0 0 21 7.90 1.80 0 0 21 9.40 1.30 0 0 21 15.10 2.50 -1 0 -21 1.50 1.40 -1 0 -21 3.50 1.20 -1 0 -21 3.00 1.00 -1 0 -21 8.20 1.50 -1 0 -21 5.10 1.60 1 0 21 3.30 1.50 1 0 21 1.00 1.70 1 0 21 3.70 1.50 -2 0 -21 12.60 2.10 -2 0 -21 12.30 1.70 -2 0 -21 17.10 2.70 -2 0 -21 12.10 1.50 2 0 21 12.00 2.60 2 0 21 14.10 2.40 -3 0 -21 19.60 1.60 -3 0 -21 14.80 2.10 -3 0 -21 16.40 2.40 -3 0 -21 14.90 1.90 3 0 21 12.10 2.30 3 0 21 10.00 2.80 3 0 21 21.80 2.10 2 -1 -21 23.60 4.30 2 -1 -21 18.30 5.20 2 -1 -21 23.80 3.40 2 -1 -21 18.40 2.70 -2 1 21 13.80 2.50 -2 1 21 21.10 4.10 -2 1 21 26.90 4.30 -2 1 21 18.00 2.70 -2 1 21 17.60 2.20 1 -1 -21 40.20 5.70 1 -1 -21 60.19 5.30 1 -1 -21 66.39 5.40 1 -1 -21 58.19 4.10 1 -1 -21 54.99 4.50 -1 1 21 57.09 3.30 -1 1 21 47.30 4.00 -1 1 21 59.09 5.40 -1 1 21 64.49 5.20 -1 1 21 56.09 4.30 0 -1 -21 5.60 1.80 0 -1 -21 2.60 1.40 0 -1 -21 -0.70 1.90 0 -1 -21 0.00 1.80 0 -1 -21 9.80 2.00 0 1 21 3.60 1.90 0 1 21 5.30 1.80 0 1 21 3.20 1.60 0 1 21 4.40 1.10 0 1 21 2.10 1.90 -1 -1 -21 7.40 2.10 -1 -1 -21 9.40 1.60 -1 -1 -21 8.70 1.70 -1 -1 -21 13.50 2.50 1 1 21 4.60 2.10 1 1 21 10.40 2.10 1 1 21 15.10 2.40 1 1 21 10.50 2.20 -2 -1 -21 43.90 2.90 -2 -1 -21 49.40 3.90 -2 -1 -21 36.80 3.20 -2 -1 -21 42.00 2.40 2 1 21 46.40 3.50 2 1 21 49.80 5.60 2 1 21 38.10 4.30 2 1 21 36.40 3.60 -3 -1 -21 59.29 4.10 -3 -1 -21 49.80 3.50 -3 -1 -21 50.59 3.30 -3 -1 -21 55.99 2.60 3 1 21 59.09 5.90 3 1 21 65.79 3.90 3 1 21 51.79 4.80 2 -2 -21 8.80 4.00 -2 2 21 -2.20 1.70 -2 2 21 -0.20 2.00 -2 2 21 -1.30 1.10 -2 2 21 -0.90 1.50 1 -2 -21 28.20 5.20 -1 2 21 27.60 3.20 -1 2 21 41.90 4.80 -1 2 21 27.80 4.00 -1 2 21 32.70 3.70 -1 2 21 30.00 4.70 0 -2 -21 60.39 3.80 0 -2 -21 57.69 4.90 0 -2 -21 73.39 6.20 0 2 21 75.69 5.90 0 2 21 71.29 4.90 0 2 21 75.39 5.80 0 2 21 66.99 5.20 0 2 21 67.09 3.40 -1 -2 -21 11.60 2.80 -1 -2 -21 9.80 2.50 -1 -2 -21 6.40 1.50 -1 -2 -21 7.90 2.00 1 2 21 13.80 2.80 1 2 21 2.90 2.30 1 2 21 9.30 2.40 1 2 21 9.60 1.10 1 2 21 10.20 2.40 -2 -2 -21 342.67 11.80 -2 -2 -21 320.67 12.10 -2 -2 -21 354.56 13.60 -2 -2 -21 397.86 12.60 2 2 21 363.96 13.10 2 2 21 349.77 13.10 2 2 21 352.56 13.50 -3 -2 -21 22.80 2.30 -3 -2 -21 30.10 3.10 -3 -2 -21 23.10 1.60 -3 -2 -21 16.30 2.20 3 2 21 20.00 3.70 3 2 21 28.50 2.70 -4 -2 -21 47.10 4.00 -4 -2 -21 48.80 4.80 -4 -2 -21 43.80 4.60 4 2 21 40.60 4.80 4 2 21 34.40 4.30 1 -3 -21 3.30 3.40 1 -3 -21 6.40 2.60 -1 3 21 5.20 1.50 -1 3 21 3.10 2.50 -1 3 21 1.60 2.20 -1 3 21 7.90 2.80 -1 3 21 8.90 3.50 0 -3 -21 9.30 2.90 0 -3 -21 -0.90 2.60 0 -3 -21 12.40 5.00 0 -3 -21 2.90 2.90 0 3 21 8.70 2.80 0 3 21 7.10 1.40 0 3 21 9.30 3.10 0 3 21 8.20 2.60 -1 -3 -21 121.59 6.60 -1 -3 -21 127.79 7.50 -1 -3 -21 147.39 8.70 1 3 21 136.39 7.90 1 3 21 130.59 4.70 1 3 21 118.89 7.00 1 3 21 147.09 8.40 1 3 21 128.69 8.90 -2 -3 -21 12.60 2.30 -2 -3 -21 16.10 2.70 -2 -3 -21 17.60 3.30 2 3 21 13.20 3.40 2 3 21 21.30 3.20 2 3 21 15.50 3.10 -3 -3 -21 38.10 3.80 -3 -3 -21 27.00 2.70 -3 -3 -21 25.60 2.60 3 3 21 31.40 3.30 3 3 21 39.60 7.20 3 3 21 27.30 4.40 -4 -3 -21 59.89 4.50 -4 -3 -21 57.09 5.50 -4 -3 -21 50.69 3.40 4 3 21 58.09 5.30 4 3 21 58.79 4.10 4 3 21 42.70 5.30 0 -4 -21 1.20 2.70 0 -4 -21 1.50 2.80 0 -4 -21 -0.80 2.80 0 4 21 5.20 2.90 0 4 21 5.00 2.90 0 4 21 -2.60 2.10 0 4 21 2.30 1.50 -1 -4 -21 3.00 2.70 -1 -4 -21 3.80 2.40 -1 -4 -21 0.30 2.50 1 4 21 4.60 2.60 1 4 21 1.30 2.70 1 4 21 -0.90 2.10 1 4 21 6.00 1.20 -2 -4 -21 223.28 9.60 -2 -4 -21 219.88 9.40 -2 -4 -21 221.88 11.40 2 4 21 218.38 10.70 2 4 21 224.48 10.50 2 4 21 213.98 10.90 -3 -4 -21 48.40 3.70 -3 -4 -21 56.79 5.10 -3 -4 -21 47.70 3.80 3 4 21 43.80 5.60 3 4 21 49.50 6.10 3 4 21 52.89 4.60 -2 -5 -21 20.20 3.60 -2 -5 -21 27.50 4.60 2 5 21 20.70 4.50 2 5 21 23.20 4.90 2 5 21 29.20 4.60 1 1 -22 87.99 5.70 1 1 -22 72.89 6.90 1 1 -22 84.29 5.30 1 1 -22 75.79 4.60 -1 -1 22 89.49 5.60 -1 -1 22 74.99 4.60 -1 -1 22 66.49 4.10 -1 -1 22 72.59 3.50 0 1 -22 -1.10 1.20 0 1 -22 0.90 1.20 0 1 -22 1.40 2.20 0 -1 22 0.50 1.00 0 -1 22 -0.80 1.30 -1 1 -22 8.10 2.40 -1 1 -22 14.90 2.40 -1 1 -22 12.50 1.90 1 -1 22 9.40 2.20 1 -1 22 8.90 1.80 1 0 -22 10.30 2.20 1 0 -22 11.50 4.00 1 0 -22 8.20 2.40 -1 0 22 11.00 2.40 -1 0 22 15.60 2.80 -1 0 22 16.70 2.60 -1 0 22 9.70 1.60 -1 0 22 10.70 2.10 0 0 -22 1.00 1.10 0 0 22 2.30 1.40 0 0 22 4.70 1.90 0 0 22 0.50 0.90 -1 0 -22 5.00 1.70 -1 0 -22 1.70 2.50 -1 0 -22 6.00 1.70 1 0 22 8.70 1.90 1 0 22 7.10 1.60 -2 0 -22 146.29 7.10 -2 0 -22 136.39 5.40 -2 0 -22 136.39 5.80 -2 0 -22 133.39 6.70 2 0 22 146.19 7.40 2 0 22 161.08 6.80 1 -1 -22 21.80 3.00 1 -1 -22 19.50 3.20 -1 1 22 21.50 3.40 -1 1 22 19.90 3.70 -1 1 22 21.10 2.50 -1 1 22 15.30 2.80 -1 1 22 18.90 2.90 0 -1 -22 22.90 4.20 0 -1 -22 20.00 2.50 0 -1 -22 15.60 3.40 0 1 22 31.40 3.50 0 1 22 20.60 3.00 0 1 22 28.50 5.90 0 1 22 20.70 1.90 -1 -1 -22 -0.60 1.10 -1 -1 -22 -0.80 1.00 -1 -1 -22 -1.00 1.60 1 1 22 2.20 1.30 1 1 22 -1.40 1.30 1 1 22 -0.40 1.90 -2 -1 -22 37.50 2.90 -2 -1 -22 32.40 3.50 -2 -1 -22 38.20 2.40 -2 -1 -22 41.60 3.70 2 1 22 29.90 4.00 2 1 22 41.80 3.40 2 1 22 33.30 4.60 0 -2 -22 2.30 2.80 0 -2 -22 -2.50 2.30 0 -2 -22 2.40 1.60 0 2 22 7.50 2.20 0 2 22 -0.60 2.10 0 2 22 4.90 2.30 0 2 22 5.80 1.40 0 2 22 1.70 1.90 -1 -2 -22 57.09 4.40 -1 -2 -22 65.29 5.40 -1 -2 -22 58.19 4.10 -1 -2 -22 74.99 5.70 1 2 22 70.19 5.40 1 2 22 68.79 5.00 1 2 22 55.29 5.20 -2 -2 -22 27.80 3.40 -2 -2 -22 41.00 3.90 -2 -2 -22 29.50 2.90 2 2 22 37.60 3.60 2 2 22 25.30 4.20 -3 -2 -22 48.80 4.40 -3 -2 -22 50.89 4.20 -3 -2 -22 48.20 3.40 3 2 22 41.70 5.00 3 2 22 48.80 4.70 0 -3 -22 115.19 7.50 0 -3 -22 125.29 8.70 0 -3 -22 114.19 8.60 0 3 22 110.79 7.50 0 3 22 127.39 5.20 0 3 22 122.39 7.10 0 3 22 119.99 8.40 -1 -3 -22 47.70 5.20 -1 -3 -22 41.50 4.40 1 3 22 45.10 5.30 1 3 22 55.49 5.30 1 3 22 41.10 4.70 -2 -3 -22 24.90 3.10 -2 -3 -22 23.20 3.30 2 3 22 21.70 4.80 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 44442 _shelx_res_file ; TITL sad_a.res in P-1 sad_a.res created by SHELXL-2019/3 at 18:20:56 on 24-Jan-2025 REM Old TITL sad in P-1 REM SHELXT solution in P-1: R1 0.143, Rweak 0.005, Alpha 0.030 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C13 F N2 CELL 0.71073 6.3603 7.6440 16.4098 84.334 84.820 67.518 ZERR 2.000 0.0002 0.0003 0.0006 0.001 0.001 0.001 LATT 1 SFAC C H B F N UNIT 24 56 2 2 4 ACTA LIST 4 TEMP -173.150 SIZE 0.10 0.50 0.50 L.S. 10 BOND $H CONF HTAB REM LIST 6 FMAP 2 PLAN 20 WGHT 0.062800 0.120300 FVAR 1.30599 F1 4 0.939037 0.042671 0.716230 11.00000 0.03428 0.01511 = 0.02074 -0.00367 -0.00725 -0.00216 N1 5 0.886673 0.251058 0.819252 11.00000 0.01761 0.01275 = 0.01516 0.00024 -0.00353 -0.00442 N2 5 0.727166 0.364320 0.677048 11.00000 0.01775 0.01536 = 0.01358 -0.00161 -0.00212 -0.00396 C1 1 0.946820 0.091070 0.882554 11.00000 0.01782 0.01496 = 0.01645 0.00154 -0.00363 -0.00498 AFIX 13 H1 2 0.948918 0.145510 0.935300 11.00000 -1.20000 AFIX 0 C2 1 1.183852 -0.061194 0.867680 11.00000 0.02024 0.01884 = 0.02468 0.00112 -0.00481 -0.00126 AFIX 137 H2A 2 1.224662 -0.148577 0.916731 11.00000 -1.50000 H2B 2 1.295300 -0.000875 0.855770 11.00000 -1.50000 H2C 2 1.183618 -0.131787 0.821000 11.00000 -1.50000 AFIX 0 C3 1 0.764178 0.005440 0.895276 11.00000 0.02489 0.02375 = 0.02700 0.00466 -0.00481 -0.01305 AFIX 137 H3A 2 0.803276 -0.093603 0.940334 11.00000 -1.50000 H3B 2 0.755731 -0.049951 0.844889 11.00000 -1.50000 H3C 2 0.616325 0.104925 0.908771 11.00000 -1.50000 AFIX 0 C4 1 0.880505 0.430689 0.845971 11.00000 0.01697 0.01502 = 0.01685 -0.00033 -0.00350 -0.00638 AFIX 13 H4 2 0.845794 0.524505 0.797241 11.00000 -1.20000 AFIX 0 C5 1 0.691368 0.511099 0.912192 11.00000 0.02101 0.01869 = 0.02061 -0.00455 -0.00136 -0.00507 AFIX 137 H5A 2 0.679720 0.638557 0.922731 11.00000 -1.50000 H5B 2 0.726963 0.428370 0.962753 11.00000 -1.50000 H5C 2 0.546150 0.517926 0.893549 11.00000 -1.50000 AFIX 0 C6 1 1.110673 0.413713 0.874674 11.00000 0.02077 0.02437 = 0.02328 0.00159 -0.00617 -0.01200 AFIX 137 H6A 2 1.103194 0.539362 0.886261 11.00000 -1.50000 H6B 2 1.229965 0.362372 0.831561 11.00000 -1.50000 H6C 2 1.146032 0.328549 0.924554 11.00000 -1.50000 AFIX 0 C7 1 0.546395 0.547208 0.695651 11.00000 0.01618 0.01565 = 0.01606 -0.00075 -0.00250 -0.00396 AFIX 13 H7 2 0.528695 0.550183 0.756731 11.00000 -1.20000 AFIX 0 C8 1 0.605638 0.718001 0.662294 11.00000 0.02449 0.01736 = 0.02296 0.00150 -0.00447 -0.00737 AFIX 137 H8A 2 0.486698 0.834686 0.681208 11.00000 -1.50000 H8B 2 0.615843 0.724314 0.602201 11.00000 -1.50000 H8C 2 0.752295 0.704329 0.682121 11.00000 -1.50000 AFIX 0 C9 1 0.315325 0.567698 0.666257 11.00000 0.01731 0.02495 = 0.02102 -0.00118 -0.00335 -0.00634 AFIX 137 H9A 2 0.197235 0.685037 0.684966 11.00000 -1.50000 H9B 2 0.277831 0.458913 0.688826 11.00000 -1.50000 H9C 2 0.323321 0.572230 0.606207 11.00000 -1.50000 AFIX 0 C10 1 0.766730 0.323759 0.589344 11.00000 0.02036 0.01953 = 0.01373 -0.00171 -0.00217 -0.00652 AFIX 13 H10 2 0.680044 0.444801 0.557470 11.00000 -1.20000 AFIX 0 C11 1 1.017435 0.269921 0.560976 11.00000 0.02244 0.02848 = 0.02172 -0.00467 0.00262 -0.00832 AFIX 137 H11A 2 1.036191 0.253792 0.501909 11.00000 -1.50000 H11B 2 1.108985 0.150774 0.590426 11.00000 -1.50000 H11C 2 1.068066 0.370637 0.572384 11.00000 -1.50000 AFIX 0 C12 1 0.675856 0.176098 0.568236 11.00000 0.02959 0.02608 = 0.02060 -0.00491 -0.00462 -0.01247 AFIX 137 H12A 2 0.687330 0.168847 0.508612 11.00000 -1.50000 H12B 2 0.516015 0.212989 0.588332 11.00000 -1.50000 H12C 2 0.766010 0.051867 0.594240 11.00000 -1.50000 AFIX 0 B1 3 0.847424 0.225729 0.738037 11.00000 0.01790 0.01510 = 0.01658 -0.00149 -0.00220 -0.00475 HKLF 4 REM sad_a.res in P-1 REM wR2 = 0.1096, GooF = S = 1.084, Restrained GooF = 1.084 for all data REM R1 = 0.0420 for 3776 Fo > 4sig(Fo) and 0.0450 for all 4103 data REM 153 parameters refined using 0 restraints END WGHT 0.0628 0.1203 REM Instructions for potential hydrogen bonds HTAB C2 F1 HTAB C3 F1 HTAB C11 F1 HTAB C12 F1 REM Highest difference peak 0.505, deepest hole -0.266, 1-sigma level 0.076 Q1 1 0.4365 0.5633 0.6789 11.00000 0.05 0.50 Q2 1 0.7878 0.4680 0.8784 11.00000 0.05 0.45 Q3 1 0.5800 0.6253 0.6734 11.00000 0.05 0.44 Q4 1 0.9920 0.4153 0.8600 11.00000 0.05 0.42 Q5 1 0.7114 0.2635 0.5798 11.00000 0.05 0.39 Q6 1 0.7798 0.2982 0.7040 11.00000 0.05 0.38 Q7 1 0.6319 0.4556 0.6823 11.00000 0.05 0.37 Q8 1 0.8799 0.3397 0.8337 11.00000 0.05 0.33 Q9 1 0.9164 0.1783 0.8488 11.00000 0.05 0.32 Q10 1 0.8890 0.2977 0.5723 11.00000 0.05 0.32 Q11 1 1.0670 0.0227 0.8699 11.00000 0.05 0.31 Q12 1 0.7518 0.3442 0.6344 11.00000 0.05 0.25 Q13 1 0.8588 0.2435 0.7821 11.00000 0.05 0.24 Q14 1 0.5156 0.5578 0.7270 11.00000 0.05 0.22 Q15 1 1.2449 -0.1198 0.8196 11.00000 0.05 0.22 Q16 1 0.8560 0.0498 0.8864 11.00000 0.05 0.21 Q17 1 0.4031 0.8214 0.6701 11.00000 0.05 0.21 Q18 1 0.2524 0.7258 0.6706 11.00000 0.05 0.21 Q19 1 0.1523 0.8344 0.6962 11.00000 0.05 0.20 Q20 1 0.5082 0.8031 0.6610 11.00000 0.05 0.20 ; _shelx_res_checksum 2603 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group F F1 0.93904(9) 0.04267(7) 0.71623(3) 0.02497(13) Uani d 1 . . N N1 0.88667(11) 0.25106(9) 0.81925(4) 0.01548(13) Uani d 1 . . N N2 0.72717(11) 0.36432(9) 0.67705(4) 0.01613(14) Uani d 1 . . C C1 0.94682(13) 0.09107(10) 0.88255(4) 0.01678(15) Uani d 1 . . H H1 0.948918 0.145510 0.935300 0.020 Uiso calc 1 . . C C2 1.18385(14) -0.06119(12) 0.86768(5) 0.02304(17) Uani d 1 . . H H2A 1.224662 -0.148577 0.916731 0.035 Uiso calc 1 . . H H2B 1.295300 -0.000875 0.855770 0.035 Uiso calc 1 . . H H2C 1.183618 -0.131787 0.821000 0.035 Uiso calc 1 . . C C3 0.76418(15) 0.00544(12) 0.89528(5) 0.02429(17) Uani d 1 . . H H3A 0.803276 -0.093603 0.940334 0.036 Uiso calc 1 . . H H3B 0.755731 -0.049951 0.844889 0.036 Uiso calc 1 . . H H3C 0.616325 0.104925 0.908771 0.036 Uiso calc 1 . . C C4 0.88051(12) 0.43069(10) 0.84597(4) 0.01606(15) Uani d 1 . . H H4 0.845794 0.524505 0.797241 0.019 Uiso calc 1 . . C C5 0.69137(14) 0.51110(11) 0.91219(5) 0.02059(16) Uani d 1 . . H H5A 0.679720 0.638557 0.922731 0.031 Uiso calc 1 . . H H5B 0.726963 0.428370 0.962753 0.031 Uiso calc 1 . . H H5C 0.546150 0.517926 0.893549 0.031 Uiso calc 1 . . C C6 1.11067(14) 0.41371(12) 0.87467(5) 0.02167(16) Uani d 1 . . H H6A 1.103194 0.539362 0.886261 0.033 Uiso calc 1 . . H H6B 1.229965 0.362372 0.831561 0.033 Uiso calc 1 . . H H6C 1.146032 0.328549 0.924554 0.033 Uiso calc 1 . . C C7 0.54639(12) 0.54721(10) 0.69565(4) 0.01650(15) Uani d 1 . . H H7 0.528695 0.550183 0.756731 0.020 Uiso calc 1 . . C C8 0.60564(14) 0.71800(11) 0.66229(5) 0.02176(16) Uani d 1 . . H H8A 0.486698 0.834686 0.681208 0.033 Uiso calc 1 . . H H8B 0.615843 0.724314 0.602201 0.033 Uiso calc 1 . . H H8C 0.752295 0.704329 0.682121 0.033 Uiso calc 1 . . C C9 0.31532(13) 0.56770(12) 0.66626(5) 0.02146(16) Uani d 1 . . H H9A 0.197235 0.685037 0.684966 0.032 Uiso calc 1 . . H H9B 0.277831 0.458913 0.688826 0.032 Uiso calc 1 . . H H9C 0.323321 0.572230 0.606207 0.032 Uiso calc 1 . . C C10 0.76673(13) 0.32376(11) 0.58934(4) 0.01805(15) Uani d 1 . . H H10 0.680044 0.444801 0.557470 0.022 Uiso calc 1 . . C C11 1.01744(15) 0.26992(13) 0.56098(5) 0.02464(17) Uani d 1 . . H H11A 1.036191 0.253792 0.501909 0.037 Uiso calc 1 . . H H11B 1.108985 0.150774 0.590426 0.037 Uiso calc 1 . . H H11C 1.068066 0.370637 0.572384 0.037 Uiso calc 1 . . C C12 0.67586(15) 0.17610(13) 0.56824(5) 0.02438(17) Uani d 1 . . H H12A 0.687330 0.168847 0.508612 0.037 Uiso calc 1 . . H H12B 0.516015 0.212989 0.588332 0.037 Uiso calc 1 . . H H12C 0.766010 0.051867 0.594240 0.037 Uiso calc 1 . . B B1 0.84742(14) 0.22573(12) 0.73804(5) 0.01686(16) Uani d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 F1 0.0343(3) 0.0151(2) 0.0207(2) -0.0022(2) -0.00725(19) -0.00367(17) N1 0.0176(3) 0.0128(3) 0.0152(3) -0.0044(2) -0.0035(2) 0.0002(2) N2 0.0178(3) 0.0154(3) 0.0136(3) -0.0040(2) -0.0021(2) -0.0016(2) C1 0.0178(3) 0.0150(3) 0.0164(3) -0.0050(3) -0.0036(2) 0.0015(2) C2 0.0202(4) 0.0188(4) 0.0247(4) -0.0013(3) -0.0048(3) 0.0011(3) C3 0.0249(4) 0.0237(4) 0.0270(4) -0.0130(3) -0.0048(3) 0.0047(3) C4 0.0170(3) 0.0150(3) 0.0168(3) -0.0064(3) -0.0035(2) -0.0003(2) C5 0.0210(4) 0.0187(3) 0.0206(3) -0.0051(3) -0.0014(3) -0.0046(3) C6 0.0208(4) 0.0244(4) 0.0233(4) -0.0120(3) -0.0062(3) 0.0016(3) C7 0.0162(3) 0.0157(3) 0.0161(3) -0.0040(3) -0.0025(2) -0.0007(2) C8 0.0245(4) 0.0174(3) 0.0230(4) -0.0074(3) -0.0045(3) 0.0015(3) C9 0.0173(3) 0.0250(4) 0.0210(3) -0.0063(3) -0.0034(3) -0.0012(3) C10 0.0204(3) 0.0195(3) 0.0137(3) -0.0065(3) -0.0022(2) -0.0017(2) C11 0.0224(4) 0.0285(4) 0.0217(4) -0.0083(3) 0.0026(3) -0.0047(3) C12 0.0296(4) 0.0261(4) 0.0206(4) -0.0125(3) -0.0046(3) -0.0049(3) B1 0.0179(4) 0.0151(4) 0.0166(3) -0.0048(3) -0.0022(3) -0.0015(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag B1 N1 C4 . . 123.84(6) ? B1 N1 C1 . . 121.01(6) ? C4 N1 C1 . . 115.11(6) ? B1 N2 C7 . . 123.64(6) ? B1 N2 C10 . . 120.53(6) ? C7 N2 C10 . . 115.66(6) ? N1 C1 C3 . . 111.48(6) ? N1 C1 C2 . . 113.89(6) ? C3 C1 C2 . . 111.49(7) ? N1 C1 H1 . . 106.5 ? C3 C1 H1 . . 106.5 ? C2 C1 H1 . . 106.5 ? C1 C2 H2A . . 109.5 ? C1 C2 H2B . . 109.5 ? H2A C2 H2B . . 109.5 ? C1 C2 H2C . . 109.5 ? H2A C2 H2C . . 109.5 ? H2B C2 H2C . . 109.5 ? C1 C3 H3A . . 109.5 ? C1 C3 H3B . . 109.5 ? H3A C3 H3B . . 109.5 ? C1 C3 H3C . . 109.5 ? H3A C3 H3C . . 109.5 ? H3B C3 H3C . . 109.5 ? N1 C4 C5 . . 112.25(6) ? N1 C4 C6 . . 112.37(6) ? C5 C4 C6 . . 110.44(6) ? N1 C4 H4 . . 107.2 ? C5 C4 H4 . . 107.2 ? C6 C4 H4 . . 107.2 ? C4 C5 H5A . . 109.5 ? C4 C5 H5B . . 109.5 ? H5A C5 H5B . . 109.5 ? C4 C5 H5C . . 109.5 ? H5A C5 H5C . . 109.5 ? H5B C5 H5C . . 109.5 ? C4 C6 H6A . . 109.5 ? C4 C6 H6B . . 109.5 ? H6A C6 H6B . . 109.5 ? C4 C6 H6C . . 109.5 ? H6A C6 H6C . . 109.5 ? H6B C6 H6C . . 109.5 ? N2 C7 C8 . . 113.11(6) ? N2 C7 C9 . . 112.27(6) ? C8 C7 C9 . . 110.19(6) ? N2 C7 H7 . . 107.0 ? C8 C7 H7 . . 107.0 ? C9 C7 H7 . . 107.0 ? C7 C8 H8A . . 109.5 ? C7 C8 H8B . . 109.5 ? H8A C8 H8B . . 109.5 ? C7 C8 H8C . . 109.5 ? H8A C8 H8C . . 109.5 ? H8B C8 H8C . . 109.5 ? C7 C9 H9A . . 109.5 ? C7 C9 H9B . . 109.5 ? H9A C9 H9B . . 109.5 ? C7 C9 H9C . . 109.5 ? H9A C9 H9C . . 109.5 ? H9B C9 H9C . . 109.5 ? N2 C10 C11 . . 111.40(6) ? N2 C10 C12 . . 113.43(6) ? C11 C10 C12 . . 111.42(7) ? N2 C10 H10 . . 106.7 ? C11 C10 H10 . . 106.7 ? C12 C10 H10 . . 106.7 ? C10 C11 H11A . . 109.5 ? C10 C11 H11B . . 109.5 ? H11A C11 H11B . . 109.5 ? C10 C11 H11C . . 109.5 ? H11A C11 H11C . . 109.5 ? H11B C11 H11C . . 109.5 ? C10 C12 H12A . . 109.5 ? C10 C12 H12B . . 109.5 ? H12A C12 H12B . . 109.5 ? C10 C12 H12C . . 109.5 ? H12A C12 H12C . . 109.5 ? H12B C12 H12C . . 109.5 ? F1 B1 N2 . . 116.05(7) ? F1 B1 N1 . . 115.03(6) ? N2 B1 N1 . . 128.91(7) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag F1 B1 . 1.3650(9) ? N1 B1 . 1.4227(10) ? N1 C4 . 1.4676(9) ? N1 C1 . 1.4779(9) ? N2 B1 . 1.4206(10) ? N2 C7 . 1.4701(9) ? N2 C10 . 1.4812(9) ? C1 C3 . 1.5272(11) ? C1 C2 . 1.5280(11) ? C1 H1 . 1.0000 ? C2 H2A . 0.9800 ? C2 H2B . 0.9800 ? C2 H2C . 0.9800 ? C3 H3A . 0.9800 ? C3 H3B . 0.9800 ? C3 H3C . 0.9800 ? C4 C5 . 1.5284(11) ? C4 C6 . 1.5326(10) ? C4 H4 . 1.0000 ? C5 H5A . 0.9800 ? C5 H5B . 0.9800 ? C5 H5C . 0.9800 ? C6 H6A . 0.9800 ? C6 H6B . 0.9800 ? C6 H6C . 0.9800 ? C7 C8 . 1.5310(11) ? C7 C9 . 1.5343(10) ? C7 H7 . 1.0000 ? C8 H8A . 0.9800 ? C8 H8B . 0.9800 ? C8 H8C . 0.9800 ? C9 H9A . 0.9800 ? C9 H9B . 0.9800 ? C9 H9C . 0.9800 ? C10 C11 . 1.5266(11) ? C10 C12 . 1.5298(11) ? C10 H10 . 1.0000 ? C11 H11A . 0.9800 ? C11 H11B . 0.9800 ? C11 H11C . 0.9800 ? C12 H12A . 0.9800 ? C12 H12B . 0.9800 ? C12 H12C . 0.9800 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag B1 N1 C1 C3 . . . . -58.17(9) ? C4 N1 C1 C3 . . . . 124.16(7) ? B1 N1 C1 C2 . . . . 69.05(9) ? C4 N1 C1 C2 . . . . -108.62(7) ? B1 N1 C4 C5 . . . . 117.02(8) ? C1 N1 C4 C5 . . . . -65.38(8) ? B1 N1 C4 C6 . . . . -117.78(8) ? C1 N1 C4 C6 . . . . 59.82(8) ? B1 N2 C7 C8 . . . . 117.08(8) ? C10 N2 C7 C8 . . . . -67.68(8) ? B1 N2 C7 C9 . . . . -117.45(8) ? C10 N2 C7 C9 . . . . 57.79(8) ? B1 N2 C10 C11 . . . . -57.08(9) ? C7 N2 C10 C11 . . . . 127.52(7) ? B1 N2 C10 C12 . . . . 69.60(9) ? C7 N2 C10 C12 . . . . -105.80(8) ? C7 N2 B1 F1 . . . . 154.87(7) ? C10 N2 B1 F1 . . . . -20.15(10) ? C7 N2 B1 N1 . . . . -25.31(12) ? C10 N2 B1 N1 . . . . 159.67(8) ? C4 N1 B1 F1 . . . . 156.92(7) ? C1 N1 B1 F1 . . . . -20.55(10) ? C4 N1 B1 N2 . . . . -22.91(12) ? C1 N1 B1 N2 . . . . 159.63(7) ?