#------------------------------------------------------------------------------
#$Date: 2025-06-03 21:27:28 +0200 (Tue, 03 Jun 2025) $
#$Revision: 299938 $
#$URL: svn://www.crystallography.net/cod/cif/2/02/34/2023468.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2023468
loop_
_publ_author_name
'Palakshamurthy, B. S.'
'Anil Kumar, H.'
'Devarajegowda, H. C.'
'Srinivasa, H. T.'
'Harish Kumar, M.'
_publ_section_title
;
Synthesis and structure of 4-bromo-2-chloro-phenyl
4'-meth-oxy-[1,1'-biphen-yl]-4-carboxyl-ate featuring short
halogen⋯oxygen contacts.
;
_journal_coeditor_code HB8126
_journal_issue 'Pt 5'
_journal_name_full
'Acta crystallographica. Section E, Crystallographic communications'
_journal_page_first 364
_journal_page_last 367
_journal_paper_doi 10.1107/S2056989025002658
_journal_volume 81
_journal_year 2025
_chemical_absolute_configuration ad
_chemical_formula_iupac 'C20 H14 Br Cl O3'
_chemical_formula_moiety 'C20 H14 Br Cl O3'
_chemical_formula_sum 'C20 H14 Br Cl O3'
_chemical_formula_weight 417.67
_chemical_name_systematic
;
4-Bromo-2-chlorophenyl 4'-methoxy-[1,1'-biphenyl]-4-carboxylate
;
_space_group_crystal_system orthorhombic
_space_group_IT_number 19
_space_group_name_Hall 'P 2ac 2ab'
_space_group_name_H-M_alt 'P 21 21 21'
_atom_sites_solution_hydrogens geom
_atom_sites_solution_primary dual
_atom_sites_solution_secondary difmap
_audit_creation_method SHELXL-2019/3
_cell_angle_alpha 90
_cell_angle_beta 90
_cell_angle_gamma 90
_cell_formula_units_Z 4
_cell_length_a 8.8347(4)
_cell_length_b 9.4124(5)
_cell_length_c 20.5526(11)
_cell_measurement_reflns_used 4264
_cell_measurement_temperature 296(2)
_cell_measurement_theta_max 28.5
_cell_measurement_theta_min 2.5
_cell_volume 1709.07(15)
_computing_cell_refinement
;
SAINT (Bruker, 2017)
;
_computing_data_collection
;
APEX2 and SAINT (Bruker, 2017)
;
_computing_data_reduction
;
SHELXL2018/3 (Sheldrick, 2015b)
;
_computing_molecular_graphics
;
Mercury (Macrae et al., 2020)
;
_computing_structure_refinement
;
SHELXL2019/2 (Sheldrick, 20b15)
;
_computing_structure_solution
;
SHELXT 2018/2 (Sheldrick, 2015a)
;
_diffrn_ambient_temperature 296(2)
_diffrn_detector_area_resol_mean 1.02
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type 'Bruker SMART APEXII CCD'
_diffrn_measurement_method \w
_diffrn_radiation_monochromator Graphite
_diffrn_radiation_type MoK\a
_diffrn_radiation_wavelength 0.71073
_diffrn_reflns_av_R_equivalents 0.0526
_diffrn_reflns_av_unetI/netI 0.0370
_diffrn_reflns_limit_h_max 11
_diffrn_reflns_limit_h_min -11
_diffrn_reflns_limit_k_max 11
_diffrn_reflns_limit_k_min -12
_diffrn_reflns_limit_l_max 27
_diffrn_reflns_limit_l_min -27
_diffrn_reflns_number 28805
_diffrn_reflns_theta_full 25.242
_diffrn_reflns_theta_max 28.349
_diffrn_reflns_theta_min 1.982
_diffrn_source 'fine-focus sealed tube'
_exptl_absorpt_coefficient_mu 2.578
_exptl_absorpt_correction_T_max 0.475
_exptl_absorpt_correction_T_min 0.371
_exptl_absorpt_correction_type multi-scan
_exptl_absorpt_process_details
;
(SADABS; Krause et al., 2015)
;
_exptl_crystal_colour colourless
_exptl_crystal_density_diffrn 1.623
_exptl_crystal_description prism
_exptl_crystal_F_000 840
_exptl_crystal_size_max 0.400
_exptl_crystal_size_mid 0.350
_exptl_crystal_size_min 0.290
_refine_diff_density_max 0.269
_refine_diff_density_min -0.231
_refine_ls_abs_structure_details 'Flack parameter'
_refine_ls_abs_structure_Flack 0.011(8)
_refine_ls_extinction_method none
_refine_ls_goodness_of_fit_ref 1.038
_refine_ls_hydrogen_treatment constr
_refine_ls_matrix_type full
_refine_ls_number_constraints 0
_refine_ls_number_parameters 228
_refine_ls_number_reflns 4264
_refine_ls_number_restraints 0
_refine_ls_restrained_S_all 1.038
_refine_ls_R_factor_all 0.0268
_refine_ls_R_factor_gt 0.0234
_refine_ls_shift/su_max 0.005
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0209P)^2^+0.2511P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.0525
_refine_ls_wR_factor_ref 0.0536
_reflns_number_gt 4012
_reflns_number_total 4264
_reflns_threshold_expression 'I > 2\s(I)'
_cod_data_source_file hb8126.cif
_cod_data_source_block I
_cod_depositor_comments 'Adding full bibliography for 2023468.cif.'
_cod_database_code 2023468
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min 0.425
_shelx_estimated_absorpt_t_max 0.522
_shelx_hkl_file
;
-1 0 0 1.40 0.40
-1 0 0 0.60 0.40
-1 0 0 -0.30 0.40
1 0 0 0.40 0.30
1 0 0 1.20 0.50
1 0 0 1.00 0.40
1 0 0 0.40 0.50
-2 0 0 1865.21 132.19
-2 0 0 2078.39 132.59
-2 0 0 2141.89 131.99
-2 0 0 2123.99 132.09
2 0 0 2105.69 132.69
2 0 0 2096.29 131.99
2 0 0 2107.69 132.39
-3 0 0 -0.10 1.50
-3 0 0 1.70 1.10
-3 0 0 1.70 1.50
-3 0 0 -0.60 0.90
3 0 0 1.50 1.10
3 0 0 -0.20 1.40
3 0 0 0.00 1.60
-4 0 0 224.38 16.00
-4 0 0 243.78 17.30
-4 0 0 217.48 16.50
-4 0 0 246.18 16.10
4 0 0 215.68 16.70
4 0 0 246.78 17.60
-5 0 0 9.20 2.40
-5 0 0 -0.20 2.90
-5 0 0 3.40 2.70
-5 0 0 -0.30 2.00
5 0 0 1.90 2.50
-6 0 0 257.57 17.30
-6 0 0 233.58 17.10
-6 0 0 250.57 18.90
6 0 0 208.18 18.20
-7 0 0 -3.00 4.00
-7 0 0 0.20 3.20
-7 0 0 4.80 2.80
7 0 0 -6.00 3.70
-8 0 0 754.52 49.90
-8 0 0 692.53 47.00
8 0 0 658.33 48.90
-9 0 0 -4.40 6.00
-9 0 0 -0.10 4.10
9 0 0 1.60 5.70
-10 0 0 6.00 6.50
-10 0 0 12.00 5.30
10 0 0 14.20 7.90
-11 0 0 0.50 8.20
-11 0 0 6.20 5.60
11 0 0 6.90 9.10
11 -1 0 25.00 9.60
-11 1 0 -1.50 7.70
10 -1 0 210.88 19.30
-10 1 0 189.18 19.20
-10 1 0 172.98 14.60
9 -1 0 105.59 12.50
-9 1 0 103.59 14.00
-9 1 0 113.39 9.90
-9 1 0 103.89 10.40
8 -1 0 78.39 10.30
-8 1 0 70.89 7.70
-8 1 0 94.99 8.60
-8 1 0 83.99 11.10
7 -1 0 45.70 7.30
-7 1 0 41.80 5.20
-7 1 0 38.70 7.20
-7 1 0 44.50 5.50
6 -1 0 337.37 25.50
-6 1 0 340.37 24.00
-6 1 0 375.66 26.30
-6 1 0 369.26 24.10
5 -1 0 1434.46 94.19
5 -1 0 1507.65 95.09
-5 1 0 1477.75 93.09
-5 1 0 1488.35 93.09
-5 1 0 1473.35 94.79
-5 1 0 1320.07 94.09
4 -1 0 481.85 31.90
4 -1 0 476.55 31.40
-4 1 0 462.95 31.60
-4 1 0 427.06 31.20
-4 1 0 470.55 30.30
-4 1 0 466.25 30.30
3 -1 0 197.78 14.20
3 -1 0 188.08 13.90
3 -1 0 196.58 13.00
-3 1 0 202.28 14.10
-3 1 0 194.68 13.00
-3 1 0 196.48 13.00
2 -1 0 14.70 1.30
2 -1 0 13.90 2.20
2 -1 0 15.80 2.30
-2 1 0 17.00 2.20
-2 1 0 16.80 1.40
-2 1 0 14.70 2.10
1 -1 0 5.10 1.00
1 -1 0 5.00 0.60
1 -1 0 5.40 0.90
-1 1 0 5.50 1.00
-1 1 0 5.30 0.80
-1 1 0 4.30 0.60
0 -1 0 0.00 0.40
0 -1 0 0.00 0.40
0 -1 0 0.00 0.50
0 -1 0 0.20 0.30
0 -1 0 -0.10 0.30
0 1 0 0.20 0.40
0 1 0 0.60 0.50
0 1 0 0.20 0.40
0 1 0 0.30 0.30
-1 -1 0 5.80 1.10
-1 -1 0 4.70 1.00
-1 -1 0 5.40 1.20
-1 -1 0 6.40 1.20
1 1 0 5.10 1.10
1 1 0 6.60 1.30
1 1 0 4.90 1.10
-2 -1 0 14.60 2.50
-2 -1 0 17.20 2.30
-2 -1 0 13.50 2.10
-2 -1 0 12.30 1.90
2 1 0 16.80 2.30
2 1 0 16.50 2.60
2 1 0 12.90 2.10
2 1 0 15.90 2.70
-3 -1 0 182.88 13.40
-3 -1 0 173.48 13.40
-3 -1 0 189.78 14.20
-3 -1 0 191.78 13.50
3 1 0 188.38 14.30
3 1 0 209.18 13.70
3 1 0 193.58 13.90
-4 -1 0 470.15 32.40
-4 -1 0 476.65 31.50
-4 -1 0 457.75 31.30
-4 -1 0 446.06 31.50
4 1 0 457.45 32.60
4 1 0 501.35 32.20
-5 -1 0 1529.05 96.39
-5 -1 0 1454.15 96.59
-5 -1 0 1475.25 97.69
-5 -1 0 1479.15 96.39
5 1 0 1509.15 97.39
-6 -1 0 355.26 26.10
-6 -1 0 344.07 24.40
-6 -1 0 346.57 24.40
6 1 0 338.37 25.60
-7 -1 0 51.99 6.70
-7 -1 0 54.89 8.90
7 1 0 40.70 7.90
-8 -1 0 95.39 11.90
-8 -1 0 87.09 9.50
8 1 0 81.59 11.70
-9 -1 0 110.29 14.20
-9 -1 0 111.59 11.60
9 1 0 98.29 13.20
-10 -1 0 196.98 17.10
10 1 0 185.98 19.80
-11 -1 0 -10.30 8.00
-11 -1 0 -1.40 6.20
11 1 0 -5.30 8.30
11 -2 0 6.90 8.60
-11 2 0 -0.20 8.80
10 -2 0 37.20 9.00
-10 2 0 30.80 4.10
-10 2 0 50.09 10.70
9 -2 0 29.20 7.80
-9 2 0 37.50 4.40
-9 2 0 31.20 4.60
-9 2 0 50.09 9.30
8 -2 0 8.60 5.00
-8 2 0 10.10 3.10
-8 2 0 2.10 4.90
-8 2 0 3.20 2.40
7 -2 0 460.95 32.10
-7 2 0 472.55 32.80
-7 2 0 457.65 29.60
-7 2 0 415.06 29.50
6 -2 0 76.39 8.10
-6 2 0 85.69 8.80
-6 2 0 68.09 5.90
-6 2 0 78.39 6.10
5 -2 0 513.05 33.40
5 -2 0 463.95 32.70
-5 2 0 462.75 32.70
-5 2 0 492.55 33.10
-5 2 0 469.75 30.90
-5 2 0 467.05 30.90
4 -2 0 1839.52 117.19
4 -2 0 1896.91 117.09
-4 2 0 1882.41 117.19
-4 2 0 1815.72 115.39
-4 2 0 1776.42 115.29
-4 2 0 1683.23 116.79
3 -2 0 213.28 14.20
3 -2 0 198.88 14.30
-3 2 0 175.48 14.10
-3 2 0 206.48 14.20
0 -2 0 1968.40 129.69
0 -2 0 2030.90 129.49
0 -2 0 2150.48 129.59
0 -2 0 2107.79 130.09
0 -2 0 2099.19 130.19
0 2 0 1964.80 129.49
0 2 0 1919.11 129.69
0 2 0 2050.09 130.09
0 2 0 2018.50 130.09
2 2 0 9999.00 634.84
-3 -2 0 189.58 14.10
-3 -2 0 193.08 14.00
-3 -2 0 197.08 14.70
-3 -2 0 195.38 14.20
3 2 0 205.78 14.80
3 2 0 200.68 14.30
3 2 0 170.58 14.50
-4 -2 0 1897.51 116.79
-4 -2 0 1818.22 116.79
-4 -2 0 1802.12 117.59
-4 -2 0 1822.92 116.89
4 2 0 1770.42 117.49
4 2 0 1728.13 117.79
4 2 0 1825.22 116.99
-5 -2 0 480.45 33.30
-5 -2 0 469.45 34.40
-5 -2 0 506.95 33.60
5 2 0 490.15 34.40
-6 -2 0 75.39 8.00
-6 -2 0 79.69 9.70
6 2 0 70.09 9.70
-7 -2 0 447.96 33.70
-7 -2 0 478.45 32.50
7 2 0 439.56 33.90
-8 -2 0 7.00 6.00
-8 -2 0 4.70 4.30
8 2 0 3.30 6.00
-9 -2 0 50.09 9.80
-9 -2 0 42.30 7.50
9 2 0 30.40 9.20
-10 -2 0 63.19 11.60
-10 -2 0 37.50 7.90
10 2 0 46.70 11.00
-11 -2 0 2.10 9.40
-11 -2 0 12.90 7.00
11 2 0 1.10 10.20
11 -3 0 -2.20 8.90
-11 3 0 9.10 9.20
10 -3 0 0.20 6.40
-10 3 0 3.90 7.50
9 -3 0 501.75 37.60
-9 3 0 530.55 38.40
8 -3 0 39.00 7.20
-8 3 0 49.40 8.60
7 -3 0 75.59 9.20
-7 3 0 77.49 9.70
6 -3 0 317.87 23.80
-6 3 0 324.57 23.80
5 -3 0 1260.77 78.29
5 -3 0 1206.18 78.29
-5 3 0 1256.37 78.29
-5 3 0 1045.50 77.99
4 -3 0 475.25 32.60
4 -3 0 487.85 32.20
-4 3 0 489.25 32.30
-4 3 0 452.15 32.60
3 -3 0 379.66 24.70
3 -3 0 374.26 23.00
3 -3 0 369.46 24.00
-3 3 0 332.87 22.90
-3 3 0 334.77 24.70
-3 3 0 352.46 24.00
2 -3 0 92.19 7.90
2 -3 0 90.59 6.70
2 -3 0 100.49 7.00
-2 3 0 93.99 6.80
-2 3 0 96.39 7.10
-2 3 0 95.19 8.20
1 -3 0 396.96 23.90
1 -3 0 375.26 25.00
1 -3 0 369.06 23.80
1 -3 0 357.96 24.00
-1 3 0 342.57 24.00
-1 3 0 321.17 24.70
-1 3 0 371.06 23.80
0 -3 0 1.00 1.10
0 -3 0 3.10 1.40
0 -3 0 -0.60 1.50
0 -3 0 -0.30 1.40
0 -3 0 -0.40 1.10
0 -3 0 0.10 1.00
0 3 0 0.80 1.00
0 3 0 -0.60 1.50
0 3 0 -0.30 1.30
0 3 0 0.30 1.40
-1 -3 0 333.87 24.30
-1 -3 0 353.26 23.90
-1 -3 0 370.96 24.70
-1 -3 0 375.96 24.20
-1 -3 0 340.27 23.80
1 3 0 355.26 24.50
1 3 0 340.27 23.80
1 3 0 358.76 24.10
-2 -3 0 90.59 7.90
-2 -3 0 95.09 8.10
-2 -3 0 97.49 8.20
-2 -3 0 98.49 8.20
2 3 0 93.89 8.20
2 3 0 81.49 8.00
2 3 0 99.69 8.50
-3 -3 0 360.76 25.40
-3 -3 0 361.26 24.90
-3 -3 0 352.06 25.00
-3 -3 0 345.47 24.90
3 3 0 355.06 25.50
3 3 0 349.47 25.10
3 3 0 378.56 25.70
-4 -3 0 487.85 33.00
-4 -3 0 478.25 33.50
4 3 0 461.45 33.70
-5 -3 0 1237.78 79.89
-5 -3 0 1179.08 80.59
5 3 0 1218.98 80.99
-6 -3 0 354.36 25.10
-6 -3 0 314.07 25.70
6 3 0 340.67 26.30
-7 -3 0 80.99 10.40
-7 -3 0 82.29 10.30
7 3 0 84.39 12.30
-8 -3 0 50.29 8.30
-8 -3 0 44.40 8.70
8 3 0 34.80 9.70
-9 -3 0 468.05 34.70
-9 -3 0 476.35 36.50
9 3 0 461.45 37.50
-10 -3 0 12.80 7.00
-10 -3 0 2.30 8.80
10 3 0 -5.90 8.80
-11 -3 0 16.40 11.40
-11 -3 0 9.40 7.90
11 3 0 8.10 11.40
11 -4 0 36.80 10.80
-11 4 0 52.79 12.40
10 -4 0 21.90 8.30
-10 4 0 11.20 8.60
9 -4 0 25.50 7.40
-9 4 0 31.80 8.50
8 -4 0 26.10 6.90
-8 4 0 21.70 6.50
7 -4 0 137.49 13.30
-7 4 0 136.19 13.10
6 -4 0 123.49 11.90
6 -4 0 123.59 11.90
-6 4 0 123.69 11.60
5 -4 0 967.50 65.19
5 -4 0 987.40 64.49
-5 4 0 982.90 64.49
4 -4 0 1743.73 112.09
4 -4 0 1755.52 111.19
-4 4 0 1799.62 111.39
-4 4 0 1604.44 112.29
3 -4 0 3169.88 199.38
3 -4 0 3166.38 198.98
3 -4 0 3145.99 198.98
3 -4 0 3356.76 200.88
-3 4 0 2973.30 198.88
-3 4 0 3118.79 199.58
-3 4 0 2981.80 200.88
2 -4 0 857.51 54.39
2 -4 0 825.32 55.79
2 -4 0 868.51 54.49
2 -4 0 892.11 54.29
-2 4 0 881.61 54.39
-2 4 0 812.12 55.79
-2 4 0 747.83 54.29
1 -4 0 13.70 2.20
1 -4 0 10.60 3.20
1 -4 0 16.30 2.40
1 -4 0 9.80 3.20
1 -4 0 15.60 2.70
1 -4 0 13.50 2.50
-1 4 0 12.40 3.20
-1 4 0 11.20 2.40
-1 4 0 13.90 2.20
0 -4 0 13.50 2.60
0 -4 0 13.60 3.60
0 -4 0 13.70 2.90
0 -4 0 16.60 2.90
0 -4 0 12.80 3.60
0 -4 0 9.00 2.20
0 4 0 11.10 2.30
0 4 0 21.50 3.40
0 4 0 19.90 3.60
-1 -4 0 11.60 3.00
-1 -4 0 17.60 3.50
-1 -4 0 15.80 3.10
-1 -4 0 11.30 3.00
-1 -4 0 12.50 3.60
-1 -4 0 13.00 2.80
1 4 0 15.00 3.50
1 4 0 14.00 3.00
1 4 0 9.90 2.70
-2 -4 0 814.22 54.69
-2 -4 0 883.91 55.89
-2 -4 0 822.82 54.99
-2 -4 0 829.82 54.89
-2 -4 0 865.01 55.19
2 4 0 808.12 55.49
2 4 0 810.02 54.79
2 4 0 788.42 54.79
-3 -4 0 3013.00 187.08
-3 -4 0 2893.11 187.08
3 4 0 2815.62 187.18
3 4 0 2903.31 187.58
-4 -4 0 1716.43 112.49
-4 -4 0 1737.53 112.99
4 4 0 1719.33 113.49
-5 -4 0 918.41 63.89
-5 -4 0 948.61 63.39
5 4 0 961.00 64.69
-6 -4 0 102.09 11.20
-6 -4 0 107.29 11.80
6 4 0 112.69 12.70
-7 -4 0 131.79 14.90
-7 -4 0 167.88 14.80
7 4 0 174.98 17.50
-8 -4 0 23.40 7.70
-8 -4 0 25.20 6.60
8 4 0 28.40 9.00
-9 -4 0 17.50 7.10
-9 -4 0 24.80 9.20
9 4 0 22.40 10.30
-10 -4 0 13.00 8.60
-10 -4 0 27.00 8.10
10 4 0 27.90 11.50
-11 -4 0 42.30 9.60
-11 -4 0 31.00 12.40
11 4 0 27.20 13.30
10 -5 0 55.79 11.60
-10 5 0 92.39 13.40
9 -5 0 11.10 6.60
-9 5 0 -8.30 6.90
8 -5 0 410.96 32.30
-8 5 0 452.45 32.50
7 -5 0 37.90 7.60
-7 5 0 32.30 6.50
6 -5 0 393.56 27.10
6 -5 0 354.86 28.00
-6 5 0 382.06 27.20
5 -5 0 207.48 16.10
5 -5 0 176.68 14.60
-5 5 0 196.38 14.80
4 -5 0 290.87 19.00
4 -5 0 289.07 19.00
4 -5 0 284.47 21.60
4 -5 0 279.97 20.00
-4 5 0 301.27 20.30
3 -5 0 206.08 16.20
3 -5 0 205.98 14.20
3 -5 0 218.48 14.30
-3 5 0 197.48 14.30
-3 5 0 192.48 14.20
2 -5 0 1365.76 88.09
2 -5 0 1424.16 87.79
2 -5 0 1390.86 87.79
2 -5 0 1359.26 89.69
2 -5 0 1336.37 88.09
-2 5 0 1303.67 88.09
-2 5 0 1383.56 87.79
1 -5 0 25.10 3.30
1 -5 0 27.50 5.10
1 -5 0 28.80 3.70
1 -5 0 29.00 5.50
1 -5 0 25.00 3.90
1 -5 0 23.00 3.90
-1 5 0 24.90 5.40
-1 5 0 19.10 3.70
0 -5 0 3.00 2.80
0 -5 0 0.10 2.20
0 -5 0 1.00 2.00
0 -5 0 1.70 2.10
0 -5 0 2.30 2.10
0 5 0 1.60 2.40
-1 -5 0 24.20 5.20
-1 -5 0 27.00 4.80
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1 3 -9 107.49 9.40
1 3 -9 111.09 9.40
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1 2 -9 329.87 22.00
1 2 -9 326.57 23.30
1 2 -9 306.67 22.00
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1 -2 9 314.77 20.90
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-8 2 -9 277.07 19.80
-8 2 -9 274.27 19.20
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8 -2 9 281.77 19.80
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3 1 -9 1096.49 71.09
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1 2 -10 366.46 28.30
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3 -1 -10 537.05 38.20
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1 1 10 2170.58 137.09
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4 -3 -24 61.79 12.70
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4 -1 -25 418.36 36.20
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3 -1 -25 178.18 20.70
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2 -3 -25 80.09 13.50
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1 -3 -25 290.37 27.30
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3 -4 -25 5.00 10.70
3 -4 -25 -1.80 8.90
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1 -5 -25 30.50 11.90
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3 1 -26 15.00 10.40
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0 -1 -27 73.39 13.90
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1 -2 -27 27.50 12.10
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0 0 0 0.00 0.00
_computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)'
;
_shelx_hkl_checksum 33053
_shelx_res_file
;
TITL S1_0m_a.res in P2(1)2(1)2(1)
shelx.res
created by SHELXL-2019/3 at 19:05:25 on 10-Feb-2025
CELL 0.71073 8.8347 9.4124 20.5526 90.000 90.000 90.000
ZERR 4.00 0.0004 0.0005 0.0011 0.000 0.000 0.000
LATT -1
SYMM 1/2 - X, - Y, 1/2 + Z
SYMM - X, 1/2 + Y, 1/2 - Z
SYMM 1/2 + X, 1/2 - Y, - Z
SFAC C H BR O CL
UNIT 80 56 4 12 4
SIZE 0.40 0.35 0.29
MERG 2
FMAP 2
PLAN 20
BOND $H
EQIV $1 x,y,z
HTAB C13 O1_$1
ACTA
TWIN -1 0 0 0 -1 0 0 0 -1 2
CONF
LIST 4
L.S. 20
TEMP 23.00
WGHT 0.020900 0.251100
BASF 0.01086
FVAR 0.43595
BR1 3 0.362936 0.654153 1.079771 11.00000 0.03127 0.02241 =
0.01170 -0.00150 0.00389 -0.00941
CL1 5 0.272064 0.775862 0.820226 11.00000 0.02318 0.02671 =
0.01943 0.00659 -0.00483 0.00056
O1 4 0.517801 0.573241 0.796145 11.00000 0.02786 0.02275 =
0.01074 0.00016 0.00376 -0.00504
O2 4 0.682851 0.756164 0.795105 11.00000 0.02361 0.03208 =
0.01528 -0.00339 0.00122 -0.00819
O3 4 0.558491 0.621319 0.282401 11.00000 0.02477 0.02311 =
0.01200 0.00157 -0.00192 -0.00391
C1 1 0.489175 0.597122 0.862196 11.00000 0.01596 0.02218 =
0.01278 -0.00145 0.00302 -0.00355
C2 1 0.373285 0.687974 0.879782 11.00000 0.01604 0.01771 =
0.01473 0.00346 -0.00457 -0.00267
C3 1 0.336704 0.706587 0.944750 11.00000 0.01800 0.01736 =
0.01822 -0.00032 0.00226 -0.00069
AFIX 43
H3 2 0.260073 0.768730 0.957100 11.00000 -1.20000
AFIX 0
C4 1 0.417367 0.630089 0.991007 11.00000 0.01901 0.01956 =
0.01036 0.00077 0.00234 -0.00759
C5 1 0.532996 0.539546 0.974134 11.00000 0.01815 0.02427 =
0.01519 0.00574 -0.00150 -0.00120
AFIX 43
H5 2 0.586627 0.490548 1.005954 11.00000 -1.20000
AFIX 0
C6 1 0.568530 0.522414 0.908402 11.00000 0.01731 0.02308 =
0.01972 0.00102 0.00329 0.00296
AFIX 43
H6 2 0.645518 0.460749 0.895960 11.00000 -1.20000
AFIX 0
C7 1 0.609003 0.671216 0.765691 11.00000 0.01504 0.02096 =
0.01601 0.00024 0.00214 -0.00022
C8 1 0.602376 0.655576 0.694017 11.00000 0.01610 0.01910 =
0.01340 -0.00291 0.00150 0.00034
C9 1 0.705208 0.732279 0.656709 11.00000 0.01785 0.02583 =
0.01419 -0.00412 0.00009 -0.00769
AFIX 43
H9 2 0.776532 0.789750 0.677077 11.00000 -1.20000
AFIX 0
C10 1 0.702159 0.723684 0.589363 11.00000 0.01915 0.02496 =
0.01568 0.00003 0.00340 -0.00673
AFIX 43
H10 2 0.772926 0.773917 0.565012 11.00000 -1.20000
AFIX 0
C11 1 0.593611 0.640134 0.557583 11.00000 0.01435 0.01413 =
0.01270 -0.00102 -0.00033 0.00146
C12 1 0.491769 0.563763 0.595881 11.00000 0.01630 0.02040 =
0.01770 -0.00199 -0.00135 -0.00284
AFIX 43
H12 2 0.419557 0.507014 0.575668 11.00000 -1.20000
AFIX 0
C13 1 0.495272 0.570162 0.663343 11.00000 0.01630 0.01932 =
0.01577 0.00174 0.00309 -0.00411
AFIX 43
H13 2 0.426611 0.517802 0.687867 11.00000 -1.20000
AFIX 0
C14 1 0.584591 0.632657 0.485439 11.00000 0.01237 0.01601 =
0.01277 0.00112 -0.00083 0.00359
C15 1 0.638892 0.743488 0.445822 11.00000 0.01669 0.01440 =
0.01793 -0.00186 -0.00138 0.00078
AFIX 43
H15 2 0.682792 0.822772 0.465137 11.00000 -1.20000
AFIX 0
C16 1 0.628296 0.736870 0.378859 11.00000 0.01726 0.01760 =
0.01676 0.00449 0.00035 -0.00116
AFIX 43
H16 2 0.664628 0.811468 0.353630 11.00000 -1.20000
AFIX 0
C17 1 0.563412 0.618914 0.348978 11.00000 0.01507 0.02141 =
0.01143 -0.00084 -0.00024 0.00302
C18 1 0.508329 0.508453 0.386850 11.00000 0.01768 0.01515 =
0.01617 -0.00181 -0.00371 -0.00050
AFIX 43
H18 2 0.464090 0.429602 0.367308 11.00000 -1.20000
AFIX 0
C19 1 0.519689 0.516388 0.454237 11.00000 0.01613 0.01603 =
0.01536 0.00290 -0.00037 0.00097
AFIX 43
H19 2 0.482771 0.441679 0.479239 11.00000 -1.20000
AFIX 0
C20 1 0.494453 0.500539 0.250317 11.00000 0.02867 0.02835 =
0.01430 -0.00350 -0.00309 -0.00211
AFIX 137
H20A 2 0.509264 0.509222 0.204215 11.00000 -1.50000
H20B 2 0.388077 0.495699 0.259587 11.00000 -1.50000
H20C 2 0.543054 0.415659 0.265624 11.00000 -1.50000
AFIX 0
HKLF 4
REM S1_0m_a.res in P2(1)2(1)2(1)
REM wR2 = 0.0536, GooF = S = 1.038, Restrained GooF = 1.038 for all data
REM R1 = 0.0234 for 4012 Fo > 4sig(Fo) and 0.0268 for all 4264 data
REM 228 parameters refined using 0 restraints
END
WGHT 0.0209 0.2563
REM Highest difference peak 0.269, deepest hole -0.231, 1-sigma level 0.054
Q1 1 0.6320 0.7162 0.6733 11.00000 0.05 0.27
Q2 1 0.6074 0.6636 0.7273 11.00000 0.05 0.27
Q3 1 0.3329 0.5768 1.1072 11.00000 0.05 0.27
Q4 1 0.6499 0.6751 0.4737 11.00000 0.05 0.23
Q5 1 0.6229 0.6091 0.5248 11.00000 0.05 0.22
Q6 1 0.3595 0.7343 1.1107 11.00000 0.05 0.22
Q7 1 0.5635 0.5830 0.5771 11.00000 0.05 0.22
Q8 1 0.6263 0.6991 0.5724 11.00000 0.05 0.22
Q9 1 0.6265 0.6623 0.3639 11.00000 0.05 0.22
Q10 1 0.4786 0.6638 1.0730 11.00000 0.05 0.22
Q11 1 0.6418 0.6672 0.5714 11.00000 0.05 0.21
Q12 1 0.4395 0.6524 0.8701 11.00000 0.05 0.21
Q13 1 0.2078 0.8441 0.8140 11.00000 0.05 0.21
Q14 1 0.2978 0.5944 1.0570 11.00000 0.05 0.21
Q15 1 0.6730 0.6609 0.6822 11.00000 0.05 0.21
Q16 1 0.4768 0.5310 0.4214 11.00000 0.05 0.20
Q17 1 0.3547 0.6523 0.9144 11.00000 0.05 0.20
Q18 1 0.6044 0.6793 0.4654 11.00000 0.05 0.20
Q19 1 0.6275 0.3849 0.3628 11.00000 0.05 0.20
Q20 1 0.6371 0.4338 0.8721 11.00000 0.05 0.20
;
_shelx_res_checksum 94036
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-x, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Br Br1 0.36294(3) 0.65415(3) 1.07977(2) 0.02179(8) Uani d 1 . .
Cl Cl1 0.27206(8) 0.77586(8) 0.82023(3) 0.02310(15) Uani d 1 . .
O O1 0.5178(2) 0.5732(2) 0.79614(9) 0.0205(4) Uani d 1 . .
O O2 0.6829(2) 0.7562(2) 0.79511(9) 0.0237(4) Uani d 1 . .
O O3 0.5585(2) 0.6213(2) 0.28240(9) 0.0200(4) Uani d 1 . .
C C1 0.4892(3) 0.5971(3) 0.86220(13) 0.0170(5) Uani d 1 . .
C C2 0.3733(3) 0.6880(3) 0.87978(12) 0.0162(5) Uani d 1 . .
C C3 0.3367(3) 0.7066(3) 0.94475(13) 0.0179(5) Uani d 1 . .
H H3 0.260073 0.768730 0.957100 0.021 Uiso calc 1 . .
C C4 0.4174(3) 0.6301(3) 0.99101(12) 0.0163(5) Uani d 1 . .
C C5 0.5330(3) 0.5395(3) 0.97413(13) 0.0192(6) Uani d 1 . .
H H5 0.586627 0.490548 1.005954 0.023 Uiso calc 1 . .
C C6 0.5685(3) 0.5224(3) 0.90840(13) 0.0200(6) Uani d 1 . .
H H6 0.645518 0.460749 0.895960 0.024 Uiso calc 1 . .
C C7 0.6090(3) 0.6712(3) 0.76569(12) 0.0173(5) Uani d 1 . .
C C8 0.6024(3) 0.6556(3) 0.69402(12) 0.0162(5) Uani d 1 . .
C C9 0.7052(3) 0.7323(3) 0.65671(13) 0.0193(5) Uani d 1 . .
H H9 0.776532 0.789750 0.677077 0.023 Uiso calc 1 . .
C C10 0.7022(3) 0.7237(3) 0.58936(13) 0.0199(5) Uani d 1 . .
H H10 0.772926 0.773917 0.565012 0.024 Uiso calc 1 . .
C C11 0.5936(3) 0.6401(3) 0.55758(12) 0.0137(5) Uani d 1 . .
C C12 0.4918(3) 0.5638(3) 0.59588(12) 0.0181(6) Uani d 1 . .
H H12 0.419557 0.507014 0.575668 0.022 Uiso calc 1 . .
C C13 0.4953(3) 0.5702(3) 0.66334(13) 0.0171(5) Uani d 1 . .
H H13 0.426611 0.517802 0.687867 0.021 Uiso calc 1 . .
C C14 0.5846(3) 0.6327(3) 0.48544(12) 0.0137(5) Uani d 1 . .
C C15 0.6389(3) 0.7435(3) 0.44582(12) 0.0163(5) Uani d 1 . .
H H15 0.682792 0.822772 0.465137 0.020 Uiso calc 1 . .
C C16 0.6283(3) 0.7369(3) 0.37886(12) 0.0172(5) Uani d 1 . .
H H16 0.664628 0.811468 0.353630 0.021 Uiso calc 1 . .
C C17 0.5634(3) 0.6189(3) 0.34898(12) 0.0160(5) Uani d 1 . .
C C18 0.5083(3) 0.5085(3) 0.38685(12) 0.0163(5) Uani d 1 . .
H H18 0.464090 0.429602 0.367308 0.020 Uiso calc 1 . .
C C19 0.5197(3) 0.5164(3) 0.45424(13) 0.0158(5) Uani d 1 . .
H H19 0.482771 0.441679 0.479239 0.019 Uiso calc 1 . .
C C20 0.4945(4) 0.5005(3) 0.25032(13) 0.0238(6) Uani d 1 . .
H H20A 0.509264 0.509222 0.204215 0.036 Uiso calc 1 . .
H H20B 0.388077 0.495699 0.259587 0.036 Uiso calc 1 . .
H H20C 0.543054 0.415659 0.265624 0.036 Uiso calc 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Br1 0.03127(14) 0.02241(13) 0.01170(11) -0.00941(12) 0.00389(11) -0.00150(11)
Cl1 0.0232(3) 0.0267(3) 0.0194(3) 0.0006(3) -0.0048(3) 0.0066(3)
O1 0.0279(10) 0.0228(10) 0.0107(9) -0.0050(8) 0.0038(8) 0.0002(8)
O2 0.0236(10) 0.0321(11) 0.0153(9) -0.0082(9) 0.0012(8) -0.0034(8)
O3 0.0248(10) 0.0231(11) 0.0120(9) -0.0039(8) -0.0019(8) 0.0016(7)
C1 0.0160(12) 0.0222(13) 0.0128(12) -0.0036(11) 0.0030(10) -0.0014(10)
C2 0.0160(11) 0.0177(13) 0.0147(11) -0.0027(10) -0.0046(10) 0.0035(9)
C3 0.0180(13) 0.0174(12) 0.0182(12) -0.0007(10) 0.0023(10) -0.0003(10)
C4 0.0190(12) 0.0196(14) 0.0104(11) -0.0076(11) 0.0023(9) 0.0008(10)
C5 0.0181(13) 0.0243(14) 0.0152(13) -0.0012(12) -0.0015(10) 0.0057(11)
C6 0.0173(12) 0.0231(14) 0.0197(14) 0.0030(11) 0.0033(11) 0.0010(11)
C7 0.0150(12) 0.0210(13) 0.0160(11) -0.0002(11) 0.0021(10) 0.0002(10)
C8 0.0161(12) 0.0191(12) 0.0134(11) 0.0003(11) 0.0015(9) -0.0029(11)
C9 0.0179(12) 0.0258(14) 0.0142(12) -0.0077(12) 0.0001(10) -0.0041(11)
C10 0.0192(12) 0.0250(13) 0.0157(14) -0.0067(11) 0.0034(11) 0.0000(11)
C11 0.0143(11) 0.0141(12) 0.0127(11) 0.0015(10) -0.0003(9) -0.0010(10)
C12 0.0163(12) 0.0204(13) 0.0177(13) -0.0028(11) -0.0014(10) -0.0020(10)
C13 0.0163(12) 0.0193(13) 0.0158(13) -0.0041(11) 0.0031(10) 0.0017(10)
C14 0.0124(11) 0.0160(13) 0.0128(11) 0.0036(10) -0.0008(9) 0.0011(10)
C15 0.0167(11) 0.0144(12) 0.0179(12) 0.0008(11) -0.0014(11) -0.0019(9)
C16 0.0173(11) 0.0176(12) 0.0168(12) -0.0012(12) 0.0004(11) 0.0045(9)
C17 0.0151(12) 0.0214(14) 0.0114(12) 0.0030(10) -0.0002(10) -0.0008(9)
C18 0.0177(12) 0.0152(13) 0.0162(13) -0.0005(10) -0.0037(10) -0.0018(10)
C19 0.0161(12) 0.0160(13) 0.0154(12) 0.0010(11) -0.0004(10) 0.0029(10)
C20 0.0287(14) 0.0283(16) 0.0143(13) -0.0021(13) -0.0031(11) -0.0035(11)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
C7 O1 C1 . . 116.1(2) ?
C17 O3 C20 . . 117.4(2) ?
C6 C1 C2 . . 120.9(2) ?
C6 C1 O1 . 1 119.7(2) ?
C2 C1 O1 . 1 119.1(2) ?
C6 C1 O1 . . 119.7(2) ?
C2 C1 O1 . . 119.1(2) ?
C1 C2 C3 . . 120.2(2) ?
C1 C2 Cl1 . . 119.6(2) ?
C3 C2 Cl1 . . 120.1(2) ?
C2 C3 C4 . . 118.3(2) ?
C2 C3 H3 . . 120.8 ?
C4 C3 H3 . . 120.8 ?
C5 C4 C3 . . 122.0(2) ?
C5 C4 Br1 . . 120.3(2) ?
C3 C4 Br1 . . 117.7(2) ?
C4 C5 C6 . . 118.9(3) ?
C4 C5 H5 . . 120.6 ?
C6 C5 H5 . . 120.6 ?
C1 C6 C5 . . 119.7(3) ?
C1 C6 H6 . . 120.2 ?
C5 C6 H6 . . 120.2 ?
O2 C7 O1 . 1 122.5(2) ?
O2 C7 O1 . . 122.5(2) ?
O2 C7 C8 . . 126.2(2) ?
O1 C7 C8 1 . 111.3(2) ?
O1 C7 C8 . . 111.3(2) ?
C9 C8 C13 . . 119.6(2) ?
C9 C8 C7 . . 118.1(2) ?
C13 C8 C7 . . 122.3(2) ?
C10 C9 C8 . . 120.5(2) ?
C10 C9 H9 . . 119.8 ?
C8 C9 H9 . . 119.8 ?
C9 C10 C11 . . 120.7(2) ?
C9 C10 H10 . . 119.6 ?
C11 C10 H10 . . 119.6 ?
C12 C11 C10 . . 117.9(2) ?
C12 C11 C14 . . 120.3(2) ?
C10 C11 C14 . . 121.9(2) ?
C13 C12 C11 . . 121.8(2) ?
C13 C12 H12 . . 119.1 ?
C11 C12 H12 . . 119.1 ?
C12 C13 C8 . . 119.5(2) ?
C12 C13 H13 . . 120.3 ?
C8 C13 H13 . . 120.3 ?
C19 C14 C15 . . 117.2(2) ?
C19 C14 C11 . . 121.3(2) ?
C15 C14 C11 . . 121.6(2) ?
C16 C15 C14 . . 121.3(2) ?
C16 C15 H15 . . 119.3 ?
C14 C15 H15 . . 119.3 ?
C15 C16 C17 . . 120.2(2) ?
C15 C16 H16 . . 119.9 ?
C17 C16 H16 . . 119.9 ?
O3 C17 C18 . . 124.2(2) ?
O3 C17 C16 . . 116.1(2) ?
C18 C17 C16 . . 119.6(2) ?
C17 C18 C19 . . 119.6(2) ?
C17 C18 H18 . . 120.2 ?
C19 C18 H18 . . 120.2 ?
C18 C19 C14 . . 122.1(3) ?
C18 C19 H19 . . 119.0 ?
C14 C19 H19 . . 119.0 ?
O3 C20 H20A . . 109.5 ?
O3 C20 H20B . . 109.5 ?
H20A C20 H20B . . 109.5 ?
O3 C20 H20C . . 109.5 ?
H20A C20 H20C . . 109.5 ?
H20B C20 H20C . . 109.5 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Br1 C4 . 1.900(2) ?
Cl1 C2 . 1.727(3) ?
O1 C7 . 1.375(3) ?
O1 C1 . 1.399(3) ?
O2 C7 . 1.196(3) ?
O3 C17 . 1.369(3) ?
O3 C20 . 1.431(3) ?
C1 C6 . 1.374(4) ?
C1 C2 . 1.382(4) ?
C2 C3 . 1.385(4) ?
C3 C4 . 1.389(4) ?
C3 H3 . 0.9300 ?
C4 C5 . 1.375(4) ?
C5 C6 . 1.396(4) ?
C5 H5 . 0.9300 ?
C6 H6 . 0.9300 ?
C7 C8 . 1.482(3) ?
C8 C9 . 1.391(4) ?
C8 C13 . 1.393(4) ?
C9 C10 . 1.387(4) ?
C9 H9 . 0.9300 ?
C10 C11 . 1.402(4) ?
C10 H10 . 0.9300 ?
C11 C12 . 1.395(4) ?
C11 C14 . 1.487(3) ?
C12 C13 . 1.388(4) ?
C12 H12 . 0.9300 ?
C13 H13 . 0.9300 ?
C14 C19 . 1.392(4) ?
C14 C15 . 1.408(3) ?
C15 C16 . 1.381(3) ?
C15 H15 . 0.9300 ?
C16 C17 . 1.392(4) ?
C16 H16 . 0.9300 ?
C17 C18 . 1.387(4) ?
C18 C19 . 1.391(3) ?
C18 H18 . 0.9300 ?
C19 H19 . 0.9300 ?
C20 H20A . 0.9600 ?
C20 H20B . 0.9600 ?
C20 H20C . 0.9600 ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
C6 H6 Cg3 2_665 0.93 2.65 3.459(3) 147
C10 H10 Cg3 3_566 0.93 2.85 3.577(3) 136
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
O1 O1 C1 C6 1 . . . 0.0(6) ?
C7 O1 C1 C6 . . . . -100.4(3) ?
O1 O1 C1 C2 1 . . . 0.0(6) ?
C7 O1 C1 C2 . . . . 84.4(3) ?
C7 O1 C1 O1 . . . 1 0E1(3) ?
C6 C1 C2 C3 . . . . 0.9(4) ?
O1 C1 C2 C3 1 . . . 176.0(2) ?
O1 C1 C2 C3 . . . . 176.0(2) ?
C6 C1 C2 Cl1 . . . . -178.0(2) ?
O1 C1 C2 Cl1 1 . . . -2.8(3) ?
O1 C1 C2 Cl1 . . . . -2.8(3) ?
C1 C2 C3 C4 . . . . -1.1(4) ?
Cl1 C2 C3 C4 . . . . 177.7(2) ?
C2 C3 C4 C5 . . . . 1.2(4) ?
C2 C3 C4 Br1 . . . . -178.8(2) ?
C3 C4 C5 C6 . . . . -1.1(4) ?
Br1 C4 C5 C6 . . . . 178.9(2) ?
C2 C1 C6 C5 . . . . -0.7(4) ?
O1 C1 C6 C5 1 . . . -175.8(2) ?
O1 C1 C6 C5 . . . . -175.8(2) ?
C4 C5 C6 C1 . . . . 0.8(4) ?
O1 O1 C7 O2 1 . . . 0.0(5) ?
C1 O1 C7 O2 . . . . 13.6(4) ?
C1 O1 C7 O1 . . . 1 0E1(7) ?
O1 O1 C7 C8 1 . . . 0.0(4) ?
C1 O1 C7 C8 . . . . -166.6(2) ?
O2 C7 C8 C9 . . . . 9.3(4) ?
O1 C7 C8 C9 1 . . . -170.5(2) ?
O1 C7 C8 C9 . . . . -170.5(2) ?
O2 C7 C8 C13 . . . . -169.1(3) ?
O1 C7 C8 C13 1 . . . 11.1(4) ?
O1 C7 C8 C13 . . . . 11.1(4) ?
C13 C8 C9 C10 . . . . -0.3(4) ?
C7 C8 C9 C10 . . . . -178.8(3) ?
C8 C9 C10 C11 . . . . 1.4(4) ?
C9 C10 C11 C12 . . . . -1.5(4) ?
C9 C10 C11 C14 . . . . 178.0(2) ?
C10 C11 C12 C13 . . . . 0.6(4) ?
C14 C11 C12 C13 . . . . -178.9(2) ?
C11 C12 C13 C8 . . . . 0.4(4) ?
C9 C8 C13 C12 . . . . -0.6(4) ?
C7 C8 C13 C12 . . . . 177.8(2) ?
C12 C11 C14 C19 . . . . -24.4(4) ?
C10 C11 C14 C19 . . . . 156.1(3) ?
C12 C11 C14 C15 . . . . 154.5(3) ?
C10 C11 C14 C15 . . . . -25.0(4) ?
C19 C14 C15 C16 . . . . -0.1(4) ?
C11 C14 C15 C16 . . . . -179.1(3) ?
C14 C15 C16 C17 . . . . -0.2(4) ?
C20 O3 C17 C18 . . . . -1.1(4) ?
C20 O3 C17 C16 . . . . 179.1(2) ?
C15 C16 C17 O3 . . . . -179.7(3) ?
C15 C16 C17 C18 . . . . 0.5(4) ?
O3 C17 C18 C19 . . . . 179.7(3) ?
C16 C17 C18 C19 . . . . -0.5(4) ?
C17 C18 C19 C14 . . . . 0.2(4) ?
C15 C14 C19 C18 . . . . 0.1(4) ?
C11 C14 C19 C18 . . . . 179.1(2) ?