#------------------------------------------------------------------------------
#$Date: 2025-05-03 21:22:23 +0200 (Sat, 03 May 2025) $
#$Revision: 299529 $
#$URL: svn://www.crystallography.net/cod/cif/2/02/34/2023452.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2023452
loop_
_publ_author_name
'Ummer, Muhammed Rafi'
'NizamMohideen, M.'
'Noorulla, Mohammed Nazrudeen'
'Moolan Khaja, Abubacker Sidhik'
_publ_section_title
;
Synthesis, crystal structure, and in silico mol-ecular docking
studies of 4-hy-droxy-3,5-di-meth-oxy-benzaldehyde
(6-chloro-pyridazin-3-yl)hydrazone monohydrate.
;
_journal_coeditor_code YZ2065
_journal_issue 'Pt 4'
_journal_name_full
'Acta crystallographica. Section E, Crystallographic communications'
_journal_page_first 336
_journal_page_last 340
_journal_paper_doi 10.1107/S205698902500252X
_journal_volume 81
_journal_year 2025
_chemical_formula_iupac 'C13 H13 Cl N4 O3, H2 O'
_chemical_formula_moiety 'C13 H13 Cl N4 O3, H2 O'
_chemical_formula_sum 'C13 H15 Cl N4 O4'
_chemical_formula_weight 326.74
_chemical_name_common
;
4-{[2-(6-Chloropyridazin-3-yl)hydrazin-1-ylidene]methyl}-2,6-dimethoxyphenol
monohydrate
;
_chemical_name_systematic
;
4-Hydroxy-3,5-dimethoxybenzaldehyde (6-chloropyridazin-3-yl)hydrazone
monohydrate
;
_space_group_crystal_system monoclinic
_space_group_IT_number 15
_space_group_name_Hall '-C 2yc'
_space_group_name_H-M_alt 'C 1 2/c 1'
_atom_sites_solution_hydrogens mixed
_atom_sites_solution_primary dual
_audit_creation_method SHELXL-2019/3
_cell_angle_alpha 90
_cell_angle_beta 127.495(2)
_cell_angle_gamma 90
_cell_formula_units_Z 8
_cell_length_a 32.1977(19)
_cell_length_b 4.6431(3)
_cell_length_c 26.400(2)
_cell_measurement_reflns_used 9970
_cell_measurement_temperature 298(2)
_cell_measurement_theta_max 28.22
_cell_measurement_theta_min 2.53
_cell_volume 3131.4(4)
_computing_cell_refinement
;
APEX3/SAINT (Bruker, 2016)
;
_computing_data_collection
;
APEX3 (Bruker, 2016)
;
_computing_data_reduction
;
SAINT/XPREP (Bruker, 2016)
;
_computing_molecular_graphics
;
ORTEP-3 for Windows (Farrugia, 2012), PLATON (Spek, 2009)
;
_computing_publication_material
;
WinGX (Farrugia, 2012), publCIF (Westrip, 2010) and PLATON
(Spek, 2009)
;
_computing_structure_refinement
;
SHELXL2019/3 (Sheldrick, 2015b)
;
_computing_structure_solution
;
SHELXT2018/2 (Sheldrick, 2015a)
;
_diffrn_ambient_temperature 298(2)
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type
'Bruker D8 VENTURE diffractometer equipped with PHOTON II detector'
_diffrn_measurement_method '\w and \f scan'
_diffrn_radiation_source 'fine-focus sealed tube'
_diffrn_radiation_type MoK\a
_diffrn_radiation_wavelength 0.71073
_diffrn_reflns_av_R_equivalents 0.0515
_diffrn_reflns_av_unetI/netI 0.0259
_diffrn_reflns_limit_h_max 42
_diffrn_reflns_limit_h_min -42
_diffrn_reflns_limit_k_max 4
_diffrn_reflns_limit_k_min -6
_diffrn_reflns_limit_l_max 35
_diffrn_reflns_limit_l_min -35
_diffrn_reflns_number 32222
_diffrn_reflns_theta_full 25.242
_diffrn_reflns_theta_max 28.268
_diffrn_reflns_theta_min 3.179
_exptl_absorpt_coefficient_mu 0.267
_exptl_absorpt_correction_T_max 0.7457
_exptl_absorpt_correction_T_min 0.5803
_exptl_absorpt_correction_type multi-scan
_exptl_absorpt_process_details
;
(SADABS; Krause et al., 2015)
;
_exptl_crystal_colour Brown
_exptl_crystal_density_diffrn 1.386
_exptl_crystal_description Block
_exptl_crystal_F_000 1360
_exptl_crystal_size_max 0.445
_exptl_crystal_size_mid 0.254
_exptl_crystal_size_min 0.103
_refine_diff_density_max 0.320
_refine_diff_density_min -0.270
_refine_ls_extinction_method none
_refine_ls_goodness_of_fit_ref 1.068
_refine_ls_hydrogen_treatment mixed
_refine_ls_matrix_type full
_refine_ls_number_parameters 215
_refine_ls_number_reflns 3867
_refine_ls_number_restraints 0
_refine_ls_restrained_S_all 1.068
_refine_ls_R_factor_all 0.0581
_refine_ls_R_factor_gt 0.0492
_refine_ls_shift/su_max 0.001
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0564P)^2^+2.0701P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.1253
_refine_ls_wR_factor_ref 0.1324
_reflns_number_gt 3259
_reflns_number_total 3867
_reflns_threshold_expression 'I > 2\s(I)'
_cod_data_source_file yz2065.cif
_cod_data_source_block I
_cod_depositor_comments 'Adding full bibliography for 2023452.cif.'
_cod_original_sg_symbol_H-M 'C 2/c'
_cod_database_code 2023452
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min 0.890
_shelx_estimated_absorpt_t_max 0.973
_shelx_hkl_file
;
-4 0 4 2660.33 162.18
6 0 -6 132.99 9.10
-6 0 6 145.19 9.10
-6 0 6 143.49 9.20
6 0 -6 143.39 9.00
6 0 -6 147.39 9.20
6 0 -6 135.59 9.20
8 0 -8 1432.46 96.09
8 0 -8 1554.74 96.09
8 0 -8 1656.63 96.09
-8 0 8 1569.04 96.19
8 0 -8 1646.64 95.99
8 0 -8 1615.34 96.19
-8 0 8 1663.43 95.99
-8 0 8 1623.14 96.09
-8 0 8 1496.15 96.09
-8 0 8 1431.96 96.09
-10 0 10 1376.06 81.59
-10 0 10 1356.76 82.09
10 0 -10 1188.88 81.69
-10 0 10 1402.86 81.69
-10 0 10 1311.17 81.69
10 0 -10 1200.28 81.59
-10 0 10 1218.38 81.69
10 0 -10 1412.46 81.79
10 0 -10 1435.76 81.69
10 0 -10 1397.96 81.59
-12 0 12 111.39 8.70
-12 0 12 123.09 8.70
12 0 -12 109.69 8.70
12 0 -12 134.89 8.60
12 0 -12 131.19 8.50
-12 0 12 133.09 8.60
-12 0 12 128.39 8.80
14 0 -14 650.03 39.70
14 0 -14 631.44 39.80
-14 0 14 636.04 39.70
-14 0 14 629.04 39.60
14 0 -14 638.84 39.60
-14 0 14 624.54 39.90
-16 0 16 74.39 5.80
16 0 -16 69.69 5.30
16 0 -16 62.79 5.40
-16 0 16 72.29 5.50
-16 0 16 54.49 5.50
-16 0 16 63.99 5.30
16 0 -16 52.29 5.50
16 0 -16 67.89 5.50
16 0 -16 68.59 5.50
-16 0 16 60.39 5.70
18 0 -18 1.10 2.00
-18 0 18 -1.60 2.10
-18 0 18 0.90 2.40
18 0 -18 -1.10 1.70
-18 0 18 0.30 2.20
-18 0 18 1.10 1.90
18 0 -18 3.00 1.90
-20 0 20 106.09 9.00
20 0 -20 116.19 8.80
-20 0 20 116.69 9.00
-20 0 20 118.59 8.70
20 0 -20 112.49 8.40
20 0 -20 102.39 8.60
-20 0 20 114.69 8.90
20 0 -20 104.99 8.30
22 0 -22 91.49 7.60
-22 0 22 87.99 8.20
22 0 -22 80.69 7.60
-22 0 22 102.19 8.20
24 0 -24 475.55 31.80
-24 0 24 463.05 32.30
-24 0 24 497.95 32.10
24 0 -24 527.75 31.70
26 0 -26 458.25 30.30
-26 0 26 463.95 30.50
-26 0 26 432.86 30.70
26 0 -26 489.75 30.10
28 0 -28 5.80 2.90
-28 0 28 6.50 3.30
-28 0 28 3.50 3.30
28 0 -28 5.90 2.90
30 0 -30 17.20 3.60
-30 0 30 12.70 4.20
30 0 -30 9.20 3.20
-30 0 30 13.30 4.40
32 0 -32 16.00 4.10
32 0 -32 23.70 4.30
-32 0 32 11.40 5.00
-32 0 32 15.60 4.70
-34 0 34 28.90 6.50
-1 1 1 9.50 1.20
1 -1 -1 11.50 1.30
-1 -1 1 11.40 1.40
-1 -1 1 10.60 1.30
5 1 -5 3386.06 198.08
-5 1 5 3255.97 198.08
-5 1 5 3261.47 198.48
-5 1 5 3276.17 198.08
-5 1 5 3238.58 198.18
5 1 -5 3332.07 198.08
5 1 -5 3252.47 198.28
-5 -1 5 3219.98 198.38
-5 -1 5 3421.46 198.18
-5 -1 5 3111.89 198.08
5 -1 -5 3369.06 198.38
5 -1 -5 3130.49 198.38
5 -1 -5 3466.45 198.18
5 -1 -5 3072.79 198.48
5 -1 -5 2951.50 198.18
-7 1 7 2072.09 125.99
-7 1 7 2028.90 125.99
-7 1 7 2130.49 126.39
7 1 -7 2055.69 125.99
-7 1 7 2078.79 126.19
7 1 -7 2204.48 125.99
7 1 -7 2081.29 126.19
7 -1 -7 2164.98 126.29
7 -1 -7 1896.21 126.09
7 -1 -7 2215.98 126.09
7 -1 -7 2050.99 126.39
7 -1 -7 1872.51 126.19
-7 -1 7 1979.20 126.09
-7 -1 7 1906.31 126.19
-7 -1 7 2211.58 126.09
9 1 -9 114.89 7.20
9 1 -9 111.49 7.70
-9 1 9 105.49 7.60
-9 1 9 99.79 7.20
-9 1 9 106.29 7.20
9 1 -9 104.29 7.10
9 1 -9 114.29 6.70
-9 1 9 99.49 7.40
-9 1 9 110.19 7.30
9 -1 -9 121.79 7.60
-9 -1 9 117.79 7.40
9 -1 -9 111.09 7.50
-9 -1 9 94.99 7.20
9 -1 -9 103.99 7.40
-9 -1 9 89.89 7.30
9 -1 -9 104.39 7.60
9 -1 -9 96.19 7.20
-11 1 11 1151.48 75.79
11 1 -11 1262.77 75.49
-11 1 11 1251.67 75.59
11 1 -11 1251.67 75.79
11 1 -11 1257.67 75.19
-11 1 11 1256.27 75.59
11 1 -11 1253.47 75.49
-11 1 11 1253.17 75.79
-11 1 11 1266.47 75.89
11 -1 -11 1254.07 75.79
11 -1 -11 1285.37 75.69
-11 -1 11 1038.90 75.69
11 -1 -11 1258.67 75.99
-11 -1 11 1246.98 75.19
11 -1 -11 1093.09 75.69
-11 -1 11 1337.47 75.69
-11 -1 11 1096.99 75.59
-11 -1 11 1317.17 76.09
-13 1 13 78.29 6.00
13 1 -13 66.49 5.40
-13 1 13 72.79 5.60
13 1 -13 68.59 5.40
-13 1 13 72.59 5.50
-13 1 13 71.89 5.70
13 1 -13 70.49 4.90
13 1 -13 74.39 5.70
13 -1 -13 76.19 6.00
-13 -1 13 59.69 5.60
-13 -1 13 65.29 5.70
-13 -1 13 81.59 6.20
13 -1 -13 73.19 5.70
13 -1 -13 60.29 5.50
-13 -1 13 72.39 5.00
13 -1 -13 81.99 5.90
-15 1 15 13.60 2.40
-15 1 15 14.40 3.00
15 1 -15 14.30 1.90
-15 1 15 11.00 2.30
15 1 -15 14.00 2.20
15 1 -15 17.80 2.70
-15 1 15 17.10 2.70
-15 -1 15 9.10 2.50
15 -1 -15 14.10 2.80
15 -1 -15 12.40 2.50
-15 -1 15 14.00 2.50
15 -1 -15 14.40 2.80
15 -1 -15 19.80 3.20
-15 -1 15 10.40 2.40
-15 -1 15 16.30 3.10
15 -1 -15 16.70 2.70
17 1 -17 20.50 2.40
-17 1 17 20.10 3.40
-17 1 17 19.80 2.90
17 1 -17 18.50 2.80
17 1 -17 21.40 3.30
-17 1 17 19.40 3.10
-17 1 17 24.00 3.30
17 1 -17 18.20 2.70
17 -1 -17 23.40 3.70
17 -1 -17 25.80 4.00
17 -1 -17 18.30 3.50
-17 -1 17 26.60 4.00
-17 -1 17 16.90 3.10
17 -1 -17 25.00 3.70
-17 -1 17 21.10 3.60
-17 -1 17 23.40 5.20
17 -1 -17 16.80 3.00
-19 1 19 21.00 4.00
19 1 -19 27.40 3.50
-19 1 19 23.80 3.40
-19 1 19 26.10 3.60
19 1 -19 24.00 2.90
19 1 -19 30.00 3.90
-19 -1 19 14.10 3.30
-19 -1 19 26.70 3.80
19 -1 -19 27.60 4.10
19 -1 -19 18.10 3.40
19 -1 -19 29.80 3.80
19 -1 -19 26.60 4.20
-19 -1 19 25.70 4.20
-19 -1 19 26.50 4.10
19 -1 -19 28.40 3.80
-21 1 21 2.60 3.00
21 1 -21 3.20 1.90
-21 1 21 -1.20 2.20
21 1 -21 -0.50 1.80
-21 1 21 0.90 2.50
21 1 -21 -0.70 2.10
-21 -1 21 -1.80 2.20
21 -1 -21 2.70 2.20
-21 -1 21 0.60 3.00
21 -1 -21 -2.60 2.70
21 -1 -21 4.40 2.70
23 1 -23 25.00 3.10
-23 1 23 19.70 4.40
23 1 -23 26.50 3.80
-23 1 23 23.40 4.00
-23 -1 23 23.00 4.60
23 -1 -23 22.70 3.80
23 -1 -23 20.80 4.10
-23 -1 23 18.30 3.90
23 -1 -23 22.70 4.20
-25 1 25 134.29 11.20
25 1 -25 137.59 10.40
25 1 -25 126.29 9.50
25 -1 -25 154.98 11.10
-25 -1 25 125.79 10.90
25 -1 -25 123.39 10.60
-25 -1 25 133.69 11.40
27 1 -27 14.50 2.80
27 1 -27 12.10 3.30
-27 1 27 13.20 4.10
-27 1 27 13.80 3.80
-27 -1 27 12.10 3.80
27 -1 -27 14.30 3.80
27 -1 -27 14.10 4.00
-27 -1 27 13.60 4.50
-29 1 29 38.90 6.00
-29 1 29 33.70 5.30
29 1 -29 38.90 5.30
29 1 -29 43.60 4.40
29 -1 -29 34.90 5.40
29 -1 -29 47.90 6.30
-29 -1 29 32.40 5.70
-29 -1 29 42.70 6.70
31 1 -31 6.60 2.40
31 1 -31 0.10 2.70
-31 1 31 5.30 3.50
-31 1 31 9.40 4.60
-31 -1 31 4.40 3.70
-31 -1 31 3.60 4.10
31 -1 -31 9.90 3.70
31 -1 -31 7.60 3.60
-33 1 33 27.70 6.10
33 1 -33 33.70 4.60
33 1 -33 30.60 5.30
33 -1 -33 32.30 5.80
-33 -1 33 39.40 7.10
33 -1 -33 32.30 5.60
-33 -1 33 26.40 5.60
0 -2 0 783.22 52.69
0 -2 0 892.01 52.79
0 -2 0 890.31 52.89
2 -2 -2 4339.37 274.17
-2 -2 2 4851.01 274.37
-2 -2 2 4219.08 274.07
2 -2 -2 4567.14 274.47
4 2 -4 421.66 24.20
-4 2 4 412.06 24.00
4 -2 -4 356.36 24.30
4 -2 -4 341.27 23.90
-4 -2 4 351.56 23.80
4 -2 -4 435.26 23.60
-4 -2 4 397.86 24.20
4 -2 -4 346.67 23.60
6 2 -6 1231.38 73.39
-6 2 6 1244.88 73.19
-6 -2 6 1335.47 72.99
6 -2 -6 1068.19 73.19
6 -2 -6 1377.66 73.09
-6 -2 6 1095.19 72.89
6 -2 -6 1208.78 73.79
-6 -2 6 1093.29 72.89
6 -2 -6 1068.69 72.99
-6 -2 6 1200.68 73.49
-8 2 8 542.65 32.90
-8 2 8 558.34 32.50
8 2 -8 524.35 33.00
-8 2 8 542.45 32.50
8 -2 -8 499.55 33.50
-8 -2 8 485.15 33.10
8 -2 -8 486.05 33.00
-8 -2 8 468.45 32.70
-8 -2 8 591.34 32.80
8 -2 -8 579.04 33.20
8 -2 -8 456.35 32.70
8 -2 -8 606.44 33.40
10 2 -10 55.79 3.90
10 2 -10 55.19 4.70
-10 2 10 53.19 4.20
-10 2 10 50.99 4.20
10 2 -10 59.69 4.00
10 -2 -10 66.59 5.10
-10 -2 10 62.49 4.70
10 -2 -10 56.79 5.60
10 -2 -10 58.89 4.70
-10 -2 10 58.59 5.00
10 -2 -10 59.09 4.80
-10 -2 10 48.70 4.50
12 2 -12 116.19 7.70
12 2 -12 123.89 8.50
-12 2 12 121.29 8.00
-12 2 12 119.79 8.00
-12 2 12 112.59 8.30
12 2 -12 115.09 7.70
12 -2 -12 130.09 8.80
12 -2 -12 124.79 8.40
12 -2 -12 119.29 9.10
-12 -2 12 135.29 9.20
12 -2 -12 114.59 8.50
-12 -2 12 94.89 8.10
-12 -2 12 110.39 9.30
12 -2 -12 101.99 8.20
-12 -2 12 127.79 8.40
14 2 -14 77.79 6.30
14 2 -14 80.09 5.70
-14 2 14 80.29 6.30
14 2 -14 77.79 5.80
-14 2 14 76.39 5.90
-14 2 14 85.39 6.00
-14 -2 14 70.99 6.70
14 -2 -14 88.79 6.80
14 -2 -14 78.19 6.20
14 -2 -14 71.99 6.30
-14 -2 14 76.39 6.60
14 -2 -14 82.59 6.30
14 -2 -14 79.39 7.00
16 2 -16 175.88 11.70
16 2 -16 177.38 11.70
-16 2 16 182.98 11.90
-16 2 16 180.78 12.00
-16 2 16 173.48 12.30
-16 -2 16 152.48 12.50
16 -2 -16 180.78 12.50
16 -2 -16 164.48 13.00
-16 -2 16 200.88 13.30
16 -2 -16 198.08 13.00
16 -2 -16 163.18 12.20
16 -2 -16 192.08 12.70
-16 -2 16 163.08 12.20
18 2 -18 105.19 7.60
18 2 -18 98.59 8.20
-18 2 18 101.79 7.60
-18 2 18 102.19 8.10
18 2 -18 100.89 7.50
-18 2 18 106.69 7.90
18 -2 -18 111.59 8.30
-18 -2 18 113.89 8.50
-18 -2 18 105.29 8.90
18 -2 -18 98.99 8.40
18 -2 -18 114.49 9.30
-18 -2 18 106.29 8.40
18 -2 -18 97.49 8.20
20 2 -20 317.57 19.80
-20 2 20 318.27 20.20
-20 2 20 306.87 20.50
-20 2 20 302.27 20.00
20 2 -20 322.37 19.90
20 -2 -20 327.57 21.30
-20 -2 20 270.67 20.90
20 -2 -20 290.57 20.50
-20 -2 20 310.77 20.60
20 -2 -20 297.87 20.70
22 2 -22 90.19 7.10
-22 2 22 93.79 8.50
22 2 -22 91.39 7.00
-22 2 22 98.09 7.60
-22 -2 22 90.39 8.10
22 -2 -22 77.09 7.80
22 -2 -22 94.69 8.60
22 -2 -22 78.29 7.90
-22 -2 22 89.49 8.60
24 2 -24 216.78 16.10
24 2 -24 227.38 15.50
-24 2 24 242.98 16.00
-24 -2 24 231.48 17.10
24 -2 -24 256.67 17.20
24 -2 -24 205.48 16.40
24 -2 -24 223.58 16.40
-24 -2 24 231.08 16.60
-26 2 26 17.60 4.20
26 2 -26 21.20 3.60
26 -2 -26 26.10 4.70
26 -2 -26 24.70 4.50
26 -2 -26 27.20 5.20
-26 -2 26 22.00 5.20
-26 -2 26 24.60 4.70
-28 2 28 11.90 3.50
28 -2 -28 19.90 4.90
-28 -2 28 11.20 4.90
-28 -2 28 19.40 4.50
28 -2 -28 18.60 4.30
-30 2 30 27.30 4.40
30 2 -30 20.00 4.10
-30 -2 30 21.20 4.90
30 -2 -30 27.40 5.80
30 -2 -30 29.60 5.00
-30 -2 30 23.30 6.20
32 2 -32 0.30 2.70
-32 2 32 -0.40 3.10
32 -2 -32 -1.10 3.90
-32 -2 32 7.50 5.30
32 -2 -32 -6.00 3.00
-32 -2 32 3.30 4.30
1 -3 -1 2.30 1.80
-1 -3 1 5.00 1.90
-1 -3 1 3.50 1.80
1 -3 -1 2.90 1.90
-1 -3 1 1.00 1.90
1 -3 -1 2.70 1.70
-3 -3 3 6.40 2.10
-3 -3 3 7.10 1.80
3 -3 -3 7.80 1.90
-3 -3 3 7.90 2.20
3 -3 -3 4.60 2.70
-5 -3 5 185.38 13.00
5 -3 -5 217.58 12.20
5 -3 -5 187.78 12.10
-5 -3 5 178.28 12.50
5 -3 -5 190.68 12.80
5 -3 -5 180.88 13.40
-7 3 7 37.60 3.80
7 3 -7 43.60 4.00
-7 -3 7 40.30 3.20
7 -3 -7 39.20 3.40
7 -3 -7 42.70 4.10
7 -3 -7 29.50 4.70
7 -3 -7 42.40 3.50
-7 -3 7 38.80 3.20
-7 -3 7 42.50 3.50
-9 3 9 3.90 1.70
9 3 -9 4.20 2.00
9 -3 -9 4.80 2.20
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9 -1 -8 2503.35 150.18
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-7 -1 6 5037.40 318.57
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1 -1 1 1766.72 103.19
1 1 -3 6898.11 406.36
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1 1 2 1257.77 76.29
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1 -1 2 1277.77 76.09
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1 -1 2 1291.07 75.99
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1 -1 -4 58.69 3.70
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7 -1 -10 799.32 48.70
7 -1 -10 876.01 48.50
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9 1 -12 1199.28 73.39
9 1 -12 1169.38 72.59
-9 1 12 1227.28 73.19
9 1 -12 1218.48 73.09
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9 -1 -12 1315.97 73.29
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9 -1 -12 1031.00 73.19
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9 -1 -12 1219.58 73.49
-11 1 14 6.40 1.80
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11 -1 -14 10.70 2.10
11 -1 -14 5.20 2.10
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11 -1 -14 6.10 2.30
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13 -1 -16 671.63 39.10
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13 -1 -16 513.65 38.80
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13 -1 -16 693.63 38.90
13 -1 -16 649.93 38.90
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15 -1 -18 520.55 32.80
15 -1 -18 436.76 32.60
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19 -1 -22 532.15 36.10
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-31 -1 34 10.70 4.60
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34 -2 -31 19.30 5.30
34 -2 -31 8.20 4.30
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32 -2 -29 81.49 8.90
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18 -2 -15 0.80 1.80
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18 -2 -15 -0.90 1.60
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16 2 -13 171.98 10.70
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-16 2 13 164.08 12.30
-16 2 13 168.88 10.90
16 -2 -13 171.58 11.30
-16 -2 13 137.59 11.80
16 -2 -13 161.28 11.10
-16 -2 13 161.68 11.20
-16 -2 13 150.38 11.40
16 -2 -13 165.88 12.00
16 -2 -13 150.68 11.20
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-14 2 11 3.40 1.60
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14 -2 -11 4.80 2.40
14 -2 -11 4.80 1.50
-14 -2 11 3.70 1.80
14 -2 -11 6.40 2.20
14 -2 -11 -0.90 1.60
14 -2 -11 7.20 1.90
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12 2 -9 84.69 5.40
-12 2 9 78.39 5.80
-12 2 9 88.69 5.90
-12 2 9 82.39 6.70
-12 2 9 78.69 5.80
-12 -2 9 94.89 5.70
12 -2 -9 65.59 6.10
-12 -2 9 76.99 6.30
-12 -2 9 89.89 6.10
12 -2 -9 73.99 5.90
12 -2 -9 85.19 6.90
-12 -2 9 67.69 5.90
12 -2 -9 89.79 6.20
12 -2 -9 96.49 6.70
-10 2 7 67.49 5.40
-10 2 7 61.19 4.40
-10 2 7 68.69 4.50
-10 2 7 52.29 4.30
10 -2 -7 70.59 4.70
-10 -2 7 70.59 4.60
10 -2 -7 61.09 5.10
10 -2 -7 50.89 4.80
-10 -2 7 62.49 4.90
-10 -2 7 51.69 4.60
10 -2 -7 62.99 5.70
-10 -2 7 71.49 4.70
8 2 -5 1447.66 84.79
-8 2 5 1441.46 84.59
-8 2 5 1416.36 85.19
8 -2 -5 1226.48 84.69
8 -2 -5 1320.97 84.59
8 -2 -5 1337.67 85.29
-8 -2 5 1326.77 84.59
-8 -2 5 1218.68 84.79
-8 -2 5 1534.25 84.79
-8 -2 5 1559.94 84.59
6 2 -3 280.57 16.10
-6 2 3 274.77 16.40
6 -2 -3 244.98 15.80
-6 -2 3 234.68 16.00
6 -2 -3 242.58 15.80
6 -2 -3 241.88 16.50
4 -2 -1 89.99 6.00
-4 -2 1 90.89 6.80
-4 -2 1 88.29 6.20
4 -2 -1 89.99 6.60
4 -2 -1 91.59 5.80
-2 2 -1 16.00 2.20
2 -2 1 15.60 2.40
-2 -2 -1 14.50 2.00
2 -2 1 16.10 2.20
-2 -2 -1 16.90 2.50
0 2 3 1491.35 83.69
0 2 -3 1476.45 83.39
0 -2 3 1174.88 83.29
0 -2 -3 1426.96 83.79
0 -2 3 1233.48 83.69
2 2 -5 2.20 1.50
-2 2 5 4.70 1.80
2 -2 -5 1.20 0.90
2 -2 -5 2.10 1.60
-2 -2 5 4.80 1.00
-2 -2 5 1.80 1.10
-2 -2 5 2.90 1.70
-2 -2 5 2.10 0.90
2 -2 -5 0.10 1.60
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4 -2 -7 161.48 9.60
-4 -2 7 130.69 10.10
4 -2 -7 133.79 10.20
-4 -2 7 169.28 9.60
-4 -2 7 156.88 10.10
4 -2 -7 150.88 10.20
4 -2 -7 127.79 9.50
-4 -2 7 127.59 9.50
4 -2 -7 165.58 10.00
-6 2 9 342.87 22.60
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-6 2 9 349.67 22.00
-6 2 9 359.96 22.00
-6 -2 9 400.16 23.00
6 -2 -9 338.97 22.80
6 -2 -9 384.16 22.50
-6 -2 9 307.87 22.30
6 -2 -9 380.66 22.70
-6 -2 9 398.66 22.50
6 -2 -9 357.56 25.10
-6 -2 9 305.97 22.70
8 2 -11 10.90 1.30
-8 2 11 9.50 1.50
-8 2 11 7.90 1.60
8 2 -11 11.30 2.40
8 2 -11 8.20 1.30
-8 2 11 9.90 2.20
-8 -2 11 6.60 2.70
-8 -2 11 11.30 2.00
8 -2 -11 10.80 2.30
8 -2 -11 6.90 1.80
8 -2 -11 8.30 2.00
-8 -2 11 11.20 2.50
8 -2 -11 8.50 2.60
-8 -2 11 7.70 1.80
8 -2 -11 7.70 2.40
-10 2 13 454.85 28.60
-10 2 13 464.75 28.10
10 2 -13 439.66 28.60
10 2 -13 441.46 27.90
10 2 -13 442.06 27.90
-10 2 13 458.05 28.10
-10 -2 13 500.15 29.20
10 -2 -13 467.45 28.70
-10 -2 13 408.56 28.80
10 -2 -13 409.86 28.80
10 -2 -13 485.15 28.50
-10 -2 13 406.46 28.30
10 -2 -13 447.46 29.10
-10 -2 13 498.55 28.60
10 -2 -13 424.06 28.80
-12 2 15 65.99 5.80
12 2 -15 71.99 5.10
-12 2 15 68.79 5.30
12 2 -15 70.19 5.10
12 2 -15 66.19 6.00
-12 2 15 69.39 5.40
12 -2 -15 71.99 6.70
12 -2 -15 70.99 5.80
12 -2 -15 61.49 5.60
-12 -2 15 64.09 5.80
12 -2 -15 80.89 6.20
-12 -2 15 63.69 5.90
-12 -2 15 58.89 6.20
12 -2 -15 58.39 6.10
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-14 2 17 13.80 3.10
14 2 -17 10.00 2.10
14 2 -17 13.40 2.20
14 2 -17 14.30 3.00
-14 2 17 10.70 2.40
14 -2 -17 10.70 3.10
14 -2 -17 13.60 3.20
14 -2 -17 12.40 2.70
14 -2 -17 14.10 3.80
-14 -2 17 13.60 3.70
-14 -2 17 10.00 2.80
-14 -2 17 14.30 3.60
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-16 2 19 234.88 16.60
16 2 -19 240.98 15.80
16 2 -19 232.68 15.80
-16 2 19 258.67 16.10
-16 -2 19 246.98 16.60
-16 -2 19 234.48 17.10
-16 -2 19 254.77 16.60
16 -2 -19 231.98 16.50
16 -2 -19 222.78 16.70
16 -2 -19 263.97 17.30
-18 2 21 2.60 2.30
-18 2 21 6.60 2.20
18 2 -21 1.40 1.70
18 2 -21 3.30 2.10
-18 2 21 8.50 2.80
-18 -2 21 2.60 2.70
-18 -2 21 5.50 3.40
18 -2 -21 1.70 2.70
18 -2 -21 -1.10 3.00
18 -2 -21 0.80 2.40
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20 2 -23 38.40 4.30
20 -2 -23 49.20 6.30
-20 -2 23 41.30 6.30
20 -2 -23 37.70 5.20
-20 -2 23 44.40 5.80
20 -2 -23 45.30 5.90
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22 -2 -25 84.99 8.30
-22 -2 25 81.99 8.30
-22 -2 25 88.79 8.50
22 -2 -25 89.49 8.60
22 -2 -25 87.29 8.10
-24 2 27 16.00 3.50
24 2 -27 20.80 3.60
24 -2 -27 11.90 4.30
-24 -2 27 18.30 5.20
-24 -2 27 14.90 4.10
24 -2 -27 22.60 4.30
24 -2 -27 19.10 4.30
-26 2 29 15.20 3.70
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-26 -2 29 7.20 3.80
26 -2 -29 13.20 4.60
-26 -2 29 1.00 4.30
26 -2 -29 3.60 3.70
26 -2 -29 7.80 3.40
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-28 2 31 45.10 5.80
-28 -2 31 42.20 7.60
28 -2 -31 46.70 8.40
28 -2 -31 40.40 6.90
-28 -2 31 48.20 6.80
28 -2 -31 46.50 6.90
-31 3 28 22.30 3.80
31 3 -28 22.80 3.30
-31 -3 28 27.80 5.00
-31 -3 28 20.20 5.60
31 -3 -28 20.50 7.10
31 -3 -28 20.40 6.70
29 3 -26 14.40 2.60
-29 3 26 10.80 3.20
-29 -3 26 15.20 4.10
-29 -3 26 19.20 5.60
29 -3 -26 22.80 5.40
29 -3 -26 20.30 4.40
-27 3 24 12.00 2.90
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27 3 -24 12.60 2.10
27 -3 -24 12.00 3.50
27 -3 -24 12.70 4.20
-27 -3 24 5.60 3.20
-27 -3 24 23.90 5.10
25 3 -22 22.00 2.80
-25 3 22 19.00 2.80
-25 3 22 17.20 3.40
25 3 -22 25.40 2.80
-25 3 22 19.50 3.20
25 -3 -22 19.30 4.70
25 -3 -22 20.30 4.10
-25 -3 22 20.70 7.50
-25 -3 22 14.40 4.00
-23 3 20 144.49 9.80
-23 3 20 136.59 9.60
-23 3 20 131.29 10.80
23 -3 -20 139.89 10.60
-23 -3 20 137.29 10.70
23 -3 -20 132.09 11.60
-23 -3 20 145.89 11.40
23 -3 -20 132.39 11.40
-21 3 18 65.89 5.50
-21 3 18 69.49 5.50
-21 3 18 74.29 6.10
21 -3 -18 67.59 7.40
-21 -3 18 72.29 7.00
21 -3 -18 64.39 6.60
-21 -3 18 62.49 6.50
21 -3 -18 71.59 6.30
-19 3 16 27.40 3.20
-19 3 16 28.60 3.70
-19 3 16 24.50 3.10
19 3 -16 31.10 3.90
19 -3 -16 30.20 4.30
19 -3 -16 32.20 4.10
-19 -3 16 33.00 4.30
-19 -3 16 31.00 4.60
-19 -3 16 22.80 3.70
19 -3 -16 28.10 5.10
-17 3 14 24.50 2.90
-17 3 14 15.00 2.20
-17 3 14 16.20 2.00
17 -3 -14 16.30 4.10
17 -3 -14 23.50 3.00
17 -3 -14 10.40 2.90
17 -3 -14 17.90 2.90
-17 -3 14 19.60 3.50
-17 -3 14 18.40 3.10
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15 -3 -12 118.89 8.70
15 -3 -12 119.69 8.30
-15 -3 12 105.49 8.30
15 -3 -12 120.19 9.80
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15 -3 -12 116.59 8.50
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13 -3 -10 16.10 3.30
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13 -3 -10 11.60 2.20
-13 -3 10 15.00 2.00
13 -3 -10 9.70 3.20
13 -3 -10 14.10 2.50
13 -3 -10 16.20 2.40
-13 -3 10 17.00 2.10
-13 -3 10 16.50 3.10
-13 -3 10 10.90 2.20
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-11 -3 8 308.97 19.70
11 -3 -8 316.27 19.80
11 -3 -8 341.07 20.00
11 -3 -8 325.67 20.00
-11 -3 8 301.57 19.70
-11 -3 8 291.57 20.20
11 -3 -8 307.37 21.00
-11 -3 8 319.77 19.80
9 3 -6 22.40 2.80
-9 3 6 21.30 3.10
-9 -3 6 19.80 2.80
-9 -3 6 15.70 1.90
9 -3 -6 15.30 2.20
-9 -3 6 15.50 2.30
-9 -3 6 17.80 2.00
9 -3 -6 18.10 2.40
9 -3 -6 15.70 3.50
9 -3 -6 18.40 2.40
7 -3 -4 11.10 3.00
-7 -3 4 11.50 3.10
7 -3 -4 14.30 1.90
7 -3 -4 14.40 2.20
-7 -3 4 13.70 2.40
7 -3 -4 13.30 1.90
-7 -3 4 18.20 2.50
5 -3 -2 548.55 32.60
5 -3 -2 499.95 32.20
5 -3 -2 584.94 35.80
-5 -3 2 472.05 32.70
5 -3 -2 566.64 32.20
-5 -3 2 475.85 32.80
-3 -3 0 35.90 4.10
3 -3 0 41.50 4.10
3 -3 0 38.00 4.10
-3 -3 0 38.00 3.60
-3 -3 0 36.00 4.10
3 -3 0 33.60 3.50
-1 -3 -2 16.10 2.40
-1 -3 -2 11.60 3.50
1 -3 2 13.70 2.60
1 -3 2 16.20 2.50
1 -3 2 16.50 2.90
-1 -3 -2 17.10 3.00
1 -3 -4 259.77 18.00
-1 -3 4 264.47 17.40
1 -3 -4 289.57 18.00
-1 -3 4 264.17 17.90
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-3 -3 6 630.64 36.50
-3 -3 6 564.94 36.50
-3 -3 6 614.14 37.60
-3 -3 6 569.04 36.80
3 -3 -6 587.84 37.40
3 -3 -6 554.54 37.70
3 -3 -6 636.14 36.60
3 -3 -6 573.24 36.50
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5 3 -8 30.60 3.80
5 -3 -8 28.20 3.00
5 -3 -8 35.20 3.80
-5 -3 8 29.60 4.00
5 -3 -8 33.60 4.20
-5 -3 8 33.50 3.10
-5 -3 8 29.00 2.80
-5 -3 8 35.00 4.50
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5 -3 -8 32.80 4.60
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7 -3 -10 149.69 11.20
7 -3 -10 143.59 11.60
-7 -3 10 157.58 10.40
-7 -3 10 172.08 11.50
7 -3 -10 156.78 10.50
7 -3 -10 166.28 10.50
-7 -3 10 166.68 10.50
7 -3 -10 146.89 10.90
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9 3 -12 1099.59 71.09
9 -3 -12 1098.69 71.09
-9 -3 12 1152.58 70.59
9 -3 -12 1171.58 71.39
-9 -3 12 1254.27 70.79
9 -3 -12 1060.19 70.79
9 -3 -12 1135.79 71.79
9 -3 -12 1183.18 70.69
-9 -3 12 1164.78 71.59
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11 -3 -14 248.88 16.80
11 -3 -14 224.38 15.50
-11 -3 14 247.68 15.60
11 -3 -14 228.68 16.10
11 -3 -14 225.98 15.60
11 -3 -14 220.88 15.90
-11 -3 14 238.58 16.50
-11 -3 14 217.78 15.40
-11 -3 14 273.37 16.90
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-13 3 16 332.07 21.00
-13 3 16 309.97 22.00
13 -3 -16 365.66 22.10
13 -3 -16 324.67 22.40
13 -3 -16 324.67 23.10
-13 -3 16 335.77 22.50
13 -3 -16 368.96 23.20
-13 -3 16 323.57 22.00
-13 -3 16 329.27 22.80
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-15 3 18 58.19 6.00
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15 -3 -18 61.49 6.60
15 -3 -18 76.89 6.40
-15 -3 18 63.39 7.40
15 -3 -18 71.79 7.60
-15 -3 18 65.09 6.20
-15 -3 18 82.19 6.60
17 3 -20 25.80 2.70
-17 3 20 27.90 3.80
-17 3 20 32.10 4.30
17 3 -20 23.50 2.60
-17 3 20 26.90 3.10
-17 -3 20 22.50 4.10
17 -3 -20 34.00 4.80
17 -3 -20 31.80 5.70
-17 -3 20 31.80 5.30
17 -3 -20 29.30 4.20
19 3 -22 67.79 5.20
-19 3 22 70.89 5.70
-19 3 22 78.29 5.90
19 3 -22 68.99 5.30
19 -3 -22 65.39 7.90
-19 -3 22 69.49 8.00
19 -3 -22 67.09 7.20
-19 -3 22 72.89 7.30
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-21 3 24 14.20 2.50
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21 3 -24 8.00 2.00
21 -3 -24 14.20 4.30
21 -3 -24 10.60 3.40
-21 -3 24 12.10 4.60
-21 -3 24 11.30 3.20
21 -3 -24 10.90 3.40
23 3 -26 2.90 1.90
-23 3 26 5.60 2.40
23 3 -26 5.30 1.80
-23 -3 26 9.40 3.70
23 -3 -26 5.60 3.90
-23 -3 26 5.70 4.60
23 -3 -26 3.10 3.40
23 -3 -26 6.00 3.00
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25 3 -28 3.70 2.10
25 -3 -28 3.80 3.30
25 -3 -28 2.10 4.00
25 -3 -28 2.70 3.90
-25 -3 28 6.30 4.90
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27 -3 -30 23.30 5.80
27 -3 -30 26.30 5.30
27 -3 -30 28.70 5.50
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28 -4 -25 7.70 5.30
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14 -4 -11 76.79 6.00
-14 -4 11 59.39 5.50
14 -4 -11 70.99 9.10
14 -4 -11 66.59 5.60
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-1 -1 -3 1930.11 110.69
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7 -1 -11 15.60 2.60
7 -1 -11 12.70 2.10
-7 -1 11 14.90 2.20
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27 1 -22 14.00 2.70
27 -1 -22 11.30 4.40
-27 -1 22 10.30 3.40
-27 -1 22 10.10 2.60
27 -1 -22 14.10 3.70
-27 -1 22 20.30 4.30
25 1 -20 320.77 20.50
-25 1 20 298.77 20.10
25 1 -20 310.77 20.00
-25 1 20 337.77 20.30
25 1 -20 310.47 19.70
-25 -1 20 280.67 20.50
25 -1 -20 313.87 20.50
25 -1 -20 288.27 20.20
-25 -1 20 262.87 19.50
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23 1 -18 144.59 10.50
23 1 -18 145.49 10.20
-23 1 18 151.28 10.50
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23 -1 -18 136.79 10.60
-23 -1 18 129.49 10.00
23 -1 -18 156.78 11.00
-23 -1 18 133.49 10.60
-23 -1 18 133.59 10.70
21 1 -16 291.57 18.10
-21 1 16 278.07 18.40
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21 1 -16 268.47 18.10
21 1 -16 288.07 18.50
-21 1 16 287.97 18.40
21 1 -16 257.67 18.20
21 -1 -16 281.57 18.40
21 -1 -16 297.97 18.80
-21 -1 16 318.67 18.70
-21 -1 16 257.07 18.60
-21 -1 16 254.97 18.40
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21 -1 -16 278.57 18.60
21 -1 -16 260.77 18.50
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19 1 -14 159.98 10.90
19 1 -14 165.28 11.20
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19 1 -14 176.98 10.90
19 1 -14 166.18 11.00
19 -1 -14 169.48 11.60
19 -1 -14 162.28 11.40
-19 -1 14 175.38 11.40
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19 -1 -14 141.59 11.10
19 -1 -14 165.78 11.20
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17 -1 -12 1387.56 81.89
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15 1 -10 1085.79 64.69
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15 1 -10 1068.59 64.59
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15 -1 -10 1125.89 64.79
15 -1 -10 1110.39 65.09
15 -1 -10 927.91 64.79
15 -1 -10 1013.10 64.99
-15 -1 10 888.21 64.69
13 1 -8 1819.02 111.69
13 1 -8 1853.81 111.69
13 1 -8 1861.71 111.69
-13 1 8 1849.31 111.79
-13 1 8 1796.92 111.99
-13 1 8 1820.62 111.79
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13 -1 -8 1888.11 112.09
-13 -1 8 1884.41 111.69
-13 -1 8 1611.14 111.69
13 -1 -8 1882.81 111.89
13 -1 -8 1727.13 112.09
-13 -1 8 1976.10 111.89
11 1 -6 8.20 1.50
-11 1 6 7.20 1.50
-11 1 6 6.50 1.60
11 1 -6 8.20 1.50
11 1 -6 7.20 1.30
-11 1 6 5.80 1.90
11 1 -6 5.40 1.40
-11 1 6 9.30 1.40
-11 -1 6 5.10 1.50
-11 -1 6 7.00 1.60
-11 -1 6 6.20 1.40
-11 -1 6 10.90 1.70
11 -1 -6 5.30 1.50
7 1 -2 1854.91 115.09
-7 1 2 1929.11 115.19
-7 1 2 1923.21 115.19
7 1 -2 1919.01 115.09
-7 1 2 1797.62 115.49
7 1 -2 1888.41 115.09
-7 -1 2 1761.92 115.09
-7 -1 2 1676.23 115.19
-7 -1 2 2010.20 115.39
-7 -1 2 2084.89 115.29
7 -1 -2 1867.71 115.29
7 -1 -2 1762.72 115.49
7 -1 -2 2054.89 115.39
-5 1 0 5755.62 353.46
-5 1 0 5439.36 353.66
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5 -1 0 6175.98 353.56
-5 -1 0 5837.22 353.76
5 -1 0 5450.55 353.66
-5 -1 0 6160.08 353.46
-3 1 -2 3373.16 201.18
-3 1 -2 3448.46 201.18
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3 1 2 3276.57 201.08
-3 1 -2 3242.08 201.08
3 1 2 3382.66 201.08
-3 1 -2 3252.87 201.28
3 -1 2 3091.39 201.38
3 -1 2 3130.79 201.48
3 -1 2 3343.17 201.08
3 -1 2 3120.49 201.28
3 -1 2 3549.45 201.28
-3 -1 -2 3093.59 201.18
-3 -1 -2 3540.15 201.18
-1 1 -4 1080.19 66.29
1 1 4 1153.98 66.29
1 1 4 1050.59 66.69
1 1 4 1066.29 66.29
-1 1 -4 1148.39 66.29
1 1 4 1111.89 66.29
-1 1 -4 1065.99 66.59
-1 1 -4 1058.09 66.39
-1 1 -4 1082.89 66.29
1 -1 4 1152.88 66.39
1 -1 4 1000.40 66.39
-1 -1 -4 1062.09 66.69
-1 -1 -4 1231.58 66.39
-1 -1 -4 1100.69 66.29
-1 -1 -4 1034.60 66.39
1 -1 4 981.90 66.39
1 -1 4 1097.69 66.49
1 -1 4 1032.00 66.59
1 1 -6 2044.00 122.59
-1 1 6 2076.89 122.69
1 1 -6 2054.69 122.69
1 1 -6 1990.00 122.89
-1 1 6 1985.10 122.69
-1 1 6 1964.10 122.99
1 1 -6 2115.09 122.69
1 1 -6 1987.20 122.89
-1 1 6 2085.59 122.69
1 -1 -6 1866.21 122.99
-1 -1 6 2133.29 122.79
-1 -1 6 2005.70 122.89
-1 -1 6 1863.91 122.99
1 -1 -6 1903.71 122.69
1 -1 -6 2103.19 122.79
-1 -1 6 1911.51 122.79
1 -1 -6 2052.09 122.69
3 1 -8 6507.85 398.86
3 1 -8 6592.64 399.36
3 1 -8 6458.85 399.36
-3 1 8 6555.34 399.16
-3 1 8 6718.23 399.06
-3 1 8 6957.60 399.16
3 1 -8 6746.52 399.06
3 1 -8 6637.64 399.06
3 -1 -8 6181.08 399.16
-3 -1 8 6795.82 399.16
3 -1 -8 7073.19 399.26
-3 -1 8 6629.04 399.36
-3 -1 8 6121.49 399.16
-3 -1 8 6159.48 399.36
3 -1 -8 6500.85 399.16
3 -1 -8 6135.89 399.46
5 1 -10 38.80 3.70
-5 1 10 38.10 3.60
5 1 -10 38.30 3.70
-5 1 10 41.10 3.80
5 1 -10 39.80 3.50
5 1 -10 39.60 2.90
-5 1 10 42.50 3.40
-5 -1 10 34.50 3.50
5 -1 -10 40.90 3.80
-5 -1 10 40.00 3.60
-5 -1 10 44.80 3.90
5 -1 -10 45.20 3.60
5 -1 -10 33.30 3.80
-5 -1 10 34.80 3.70
5 -1 -10 33.00 3.40
7 1 -12 927.81 54.19
-7 1 12 911.21 54.29
-7 1 12 903.31 54.29
7 1 -12 880.01 53.79
-7 1 12 881.71 54.39
7 1 -12 893.31 54.19
-7 1 12 883.71 54.59
7 1 -12 808.92 54.49
7 1 -12 877.51 54.49
7 -1 -12 925.11 54.49
-7 -1 12 774.82 54.29
7 -1 -12 996.00 54.49
7 -1 -12 770.92 54.59
-7 -1 12 937.71 54.69
-7 -1 12 844.62 54.59
-7 -1 12 947.51 54.39
7 -1 -12 745.73 54.19
7 -1 -12 893.61 54.59
-9 1 14 1527.65 94.99
9 1 -14 1420.26 95.09
-9 1 14 1582.64 94.69
9 1 -14 1535.95 94.19
9 1 -14 1595.54 94.69
9 1 -14 1579.24 94.69
9 1 -14 1509.85 94.99
-9 1 14 1520.45 94.69
-9 1 14 1550.24 94.99
-9 -1 14 1582.74 95.19
-9 -1 14 1340.47 95.39
-9 -1 14 1448.06 95.09
9 -1 -14 1586.94 94.89
9 -1 -14 1706.93 94.89
9 -1 -14 1541.85 95.19
-9 -1 14 1617.24 94.79
-11 1 16 12.10 2.50
11 1 -16 14.50 2.60
11 1 -16 13.60 1.80
11 1 -16 7.90 2.40
11 1 -16 9.00 2.00
-11 1 16 7.20 2.10
11 1 -16 8.20 2.00
-11 1 16 9.50 2.10
-11 1 16 13.10 2.80
-11 -1 16 15.60 3.00
11 -1 -16 12.50 2.90
-11 -1 16 7.60 2.30
11 -1 -16 10.60 2.70
11 -1 -16 15.10 2.60
-11 -1 16 8.90 2.20
11 -1 -16 8.40 2.20
-11 -1 16 7.20 2.40
11 -1 -16 12.70 2.50
13 1 -18 93.09 7.10
13 1 -18 86.39 7.50
-13 1 18 107.59 7.60
-13 1 18 93.89 7.30
13 1 -18 88.79 6.30
-13 1 18 94.49 7.60
13 1 -18 82.19 6.90
-13 1 18 93.39 7.00
13 1 -18 92.49 7.00
-13 -1 18 103.59 7.80
-13 -1 18 73.39 7.10
13 -1 -18 94.69 7.50
-13 -1 18 96.79 7.80
-13 -1 18 87.29 7.40
13 -1 -18 79.89 7.40
13 -1 -18 105.19 7.30
13 -1 -18 70.39 6.90
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15 1 -20 219.38 14.80
15 1 -20 220.48 14.90
15 1 -20 227.28 15.80
-15 1 20 226.78 14.90
-15 1 20 231.68 15.10
-15 1 20 213.68 15.20
15 1 -20 209.78 14.10
15 -1 -20 239.18 15.20
15 -1 -20 200.28 15.40
-15 -1 20 223.28 16.40
15 -1 -20 190.38 14.90
-15 -1 20 234.18 15.20
-15 -1 20 197.48 15.10
15 -1 -20 236.18 15.20
-15 -1 20 207.68 15.40
15 -1 -20 224.98 15.40
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17 1 -22 658.13 38.50
-17 1 22 647.94 38.60
17 1 -22 615.74 38.30
-17 1 22 604.74 38.80
17 -1 -22 562.24 38.50
17 -1 -22 580.94 39.00
17 -1 -22 656.33 38.80
-17 -1 22 567.94 38.90
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19 1 -24 37.80 4.70
-19 1 24 36.50 4.80
19 1 -24 36.80 3.80
19 -1 -24 37.00 5.70
-19 -1 24 45.60 6.10
19 -1 -24 34.00 4.80
-19 -1 24 35.00 5.00
19 -1 -24 38.70 5.40
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21 1 -26 67.79 5.40
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21 -1 -26 77.29 7.10
-21 -1 26 65.39 7.20
21 -1 -26 55.29 6.70
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-23 -1 28 15.10 4.30
23 -1 -28 13.10 4.10
23 -1 -28 17.10 4.10
23 -1 -28 14.60 3.70
-23 -1 28 5.70 3.40
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25 1 -30 59.89 5.20
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25 -1 -30 55.79 6.90
25 -1 -30 61.19 7.50
25 -1 -30 62.69 6.90
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-27 -1 32 3.00 4.10
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27 -1 -32 0.00 2.90
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29 1 -34 -2.60 2.20
29 1 -34 -0.50 2.70
29 -1 -34 2.40 3.40
29 -1 -34 -3.50 2.90
-29 -1 34 3.80 4.30
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34 2 -29 21.00 3.70
34 -2 -29 23.80 5.60
-34 -2 29 20.80 5.60
-34 -2 29 13.50 5.00
32 2 -27 51.49 4.90
32 2 -27 56.79 5.90
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32 -2 -27 57.79 7.10
32 -2 -27 64.29 7.90
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30 2 -25 1.30 1.70
30 2 -25 2.40 2.20
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30 -2 -25 4.40 3.40
30 -2 -25 1.80 2.90
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28 -2 -23 15.00 4.20
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26 2 -21 10.40 2.60
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24 2 -19 141.29 9.40
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24 -2 -19 136.19 10.70
24 -2 -19 138.99 11.20
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-12 -2 17 938.11 52.89
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3 1 3 103.69 6.70
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1 1 5 223.78 13.50
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1 1 5 212.58 13.50
1 1 5 220.48 14.00
1 1 5 217.38 13.50
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1 -1 5 235.68 13.80
1 -1 5 226.98 13.70
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1 -1 5 191.68 13.50
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1 -1 5 196.28 13.60
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1 -1 5 212.08 13.90
-1 -1 -5 200.18 13.60
1 1 -7 3098.59 188.58
1 1 -7 3216.68 188.28
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1 1 -7 2977.30 188.38
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1 1 -7 3105.39 188.08
1 1 -7 3104.69 188.18
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1 -1 -7 3455.95 188.38
1 -1 -7 3194.48 188.28
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1 -1 -7 2948.80 188.28
1 -1 -7 2793.62 188.58
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3 1 -9 207.08 14.00
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3 1 -9 205.88 13.40
3 -1 -9 233.58 13.90
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-3 -1 9 202.18 14.00
3 -1 -9 220.58 13.80
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3 -1 -9 195.18 13.80
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5 -1 -11 3675.43 259.77
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7 -1 -13 2417.66 176.88
7 -1 -13 2460.95 176.58
-7 -1 13 3040.40 176.68
7 -1 -13 2947.71 176.78
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9 1 -15 744.63 46.10
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9 -1 -15 624.44 46.20
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9 -1 -15 649.43 45.90
9 -1 -15 757.72 46.00
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9 -1 -15 785.92 46.40
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11 1 -17 48.00 3.90
11 1 -17 48.90 4.60
11 1 -17 48.10 4.50
-11 1 17 55.59 4.90
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11 -1 -17 54.19 4.80
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11 -1 -17 51.79 5.20
11 -1 -17 44.90 4.70
11 -1 -17 50.69 4.90
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13 1 -19 9.80 2.50
-13 1 19 7.40 2.60
13 1 -19 12.80 3.20
-13 1 19 10.90 3.20
13 1 -19 14.70 2.60
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13 1 -19 9.60 2.70
13 -1 -19 12.70 3.20
13 -1 -19 12.00 3.20
13 -1 -19 12.20 2.60
13 -1 -19 10.30 2.70
-13 -1 19 7.80 2.50
-13 -1 19 11.70 3.10
-13 -1 19 13.10 3.40
-13 -1 19 13.00 2.80
13 -1 -19 16.80 3.10
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15 1 -21 680.93 41.80
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15 -1 -21 727.53 42.90
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19 -1 -25 -1.90 2.70
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21 -1 -27 9.90 3.60
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25 -1 -31 20.40 4.60
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27 -1 -33 22.00 4.80
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34 2 -28 10.70 2.50
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-11 1 4 39.30 3.10
11 1 -4 34.40 3.20
11 1 -4 32.10 2.70
-11 1 4 36.30 3.10
11 -1 -4 31.50 3.10
-11 -1 4 25.50 2.60
11 -1 -4 34.00 3.20
-11 -1 4 38.30 3.10
-11 -1 4 32.20 3.00
11 -1 -4 32.50 3.50
-9 1 2 3562.94 204.28
9 1 -2 3391.36 203.98
9 1 -2 3267.07 204.18
-9 1 2 3306.57 204.28
9 1 -2 3369.46 204.18
9 1 -2 3335.27 204.48
-9 -1 2 3667.03 204.38
9 -1 -2 3570.34 204.38
9 -1 -2 3000.90 204.48
9 -1 -2 3272.17 204.38
-9 -1 2 3036.80 204.28
-9 -1 2 3517.45 204.48
-9 -1 2 3224.88 204.68
7 1 0 57.99 4.30
-7 1 0 65.79 4.60
-7 1 0 68.09 4.90
-7 1 0 63.59 4.50
7 1 0 60.69 4.30
-7 -1 0 68.69 4.90
7 -1 0 73.99 4.70
-7 -1 0 53.79 4.40
7 -1 0 57.99 4.80
-7 -1 0 68.89 4.60
7 -1 0 60.69 4.60
5 1 2 4295.37 257.47
5 1 2 4230.08 256.97
-5 1 -2 4252.37 256.87
5 1 2 4271.67 256.97
-5 1 -2 4115.59 257.17
-5 1 -2 4382.06 257.07
-5 1 -2 4312.97 256.97
-5 -1 -2 4344.57 257.37
-5 -1 -2 3747.62 256.97
5 -1 2 4590.54 257.17
-5 -1 -2 4680.33 257.07
5 -1 2 3961.90 257.07
5 -1 2 4172.88 257.37
5 -1 2 3995.20 257.17
5 -1 2 4156.38 256.87
-5 -1 -2 3938.71 257.37
3 1 4 166.68 10.60
-3 1 -4 170.88 10.70
3 1 4 167.08 11.10
-3 1 -4 169.08 10.70
3 1 4 171.08 10.60
-3 1 -4 173.18 11.00
3 1 4 169.68 10.40
-3 1 -4 161.38 10.70
-3 1 -4 167.98 10.70
-3 -1 -4 158.08 10.70
3 -1 4 150.28 10.80
-3 -1 -4 156.78 10.40
3 -1 4 187.98 10.80
-3 -1 -4 160.88 11.20
3 -1 4 168.68 10.70
3 -1 4 160.88 10.70
3 -1 4 162.98 11.00
-3 -1 -4 178.68 10.80
1 1 6 28.30 3.30
-1 1 -6 23.10 2.60
-1 1 -6 24.00 2.30
1 1 6 20.70 2.30
1 1 6 22.10 2.10
-1 1 -6 26.80 2.20
1 1 6 20.20 2.30
-1 1 -6 19.70 2.30
-1 1 -6 22.60 2.40
-1 -1 -6 19.90 2.50
1 -1 6 20.90 2.20
-1 -1 -6 26.70 2.20
1 -1 6 28.50 2.60
1 -1 6 21.60 2.50
1 -1 6 21.00 2.70
-1 -1 -6 22.40 2.50
1 -1 6 17.40 2.40
-1 -1 -6 20.80 2.80
-1 1 8 712.23 43.70
-1 1 8 720.43 43.30
1 1 -8 720.73 43.30
1 1 -8 700.93 43.10
-1 1 8 684.33 43.20
1 1 -8 692.43 43.60
1 1 -8 707.03 43.30
1 1 -8 672.73 43.40
-1 1 8 732.93 43.30
-1 -1 8 789.82 43.80
1 -1 -8 652.53 43.70
-1 -1 8 641.74 43.30
-1 -1 8 719.93 43.60
1 -1 -8 730.43 43.30
-1 -1 8 664.13 43.60
1 -1 -8 675.23 43.40
-3 1 10 212.48 13.40
-3 1 10 209.68 13.30
3 1 -10 201.58 13.00
-3 1 10 220.58 13.80
-3 1 10 202.48 13.30
3 1 -10 196.78 13.50
3 1 -10 214.18 13.40
3 1 -10 199.28 13.60
3 1 -10 212.08 13.30
-3 -1 10 177.58 13.40
-3 -1 10 222.88 13.70
-3 -1 10 216.98 13.50
3 -1 -10 176.68 13.40
3 -1 -10 227.38 13.50
3 -1 -10 193.78 13.80
-3 -1 10 210.68 13.70
5 1 -12 1347.27 86.29
-5 1 12 1405.56 86.09
-5 1 12 1380.46 86.39
-5 1 12 1462.45 86.09
5 1 -12 1485.05 86.09
5 1 -12 1402.76 85.69
-5 1 12 1446.96 85.99
5 1 -12 1385.66 86.29
5 1 -12 1496.15 86.09
5 -1 -12 1420.76 86.19
5 -1 -12 1191.28 85.99
5 -1 -12 1293.57 86.49
-5 -1 12 1532.35 86.19
-5 -1 12 1312.17 86.39
5 -1 -12 1542.95 86.19
-5 -1 12 1243.98 86.09
-5 -1 12 1448.26 86.39
-7 1 14 844.32 51.79
7 1 -14 863.71 51.39
-7 1 14 862.21 51.59
7 1 -14 808.62 51.79
7 1 -14 843.12 50.89
7 1 -14 823.92 51.59
7 1 -14 865.61 51.39
-7 1 14 843.62 51.39
-7 1 14 860.61 51.39
-7 -1 14 799.32 51.69
7 -1 -14 915.01 51.59
-7 -1 14 884.71 51.49
7 -1 -14 697.93 51.39
7 -1 -14 708.23 51.69
-7 -1 14 853.31 51.79
7 -1 -14 840.02 51.49
-7 -1 14 756.22 51.89
9 1 -16 662.63 42.70
-9 1 16 693.43 42.50
-9 1 16 666.83 42.60
9 1 -16 732.93 42.50
-9 1 16 686.33 42.90
9 1 -16 697.23 42.00
-9 1 16 701.43 42.50
9 1 -16 702.43 42.40
9 1 -16 654.53 42.90
9 -1 -16 725.33 42.70
9 -1 -16 743.73 42.80
-9 -1 16 702.63 42.60
9 -1 -16 609.04 42.60
-9 -1 16 664.43 42.90
-9 -1 16 696.13 43.00
9 -1 -16 603.94 42.90
9 -1 -16 692.43 42.90
-9 -1 16 593.94 42.50
-11 1 18 440.26 27.80
11 1 -18 440.06 27.40
11 1 -18 432.36 27.80
-11 1 18 444.26 27.60
11 1 -18 446.66 27.00
11 1 -18 424.66 27.40
-11 1 18 449.95 27.50
11 1 -18 407.86 27.90
-11 1 18 439.96 28.90
-11 -1 18 377.96 27.60
-11 -1 18 472.25 27.70
11 -1 -18 466.05 27.70
-11 -1 18 409.06 27.90
-11 -1 18 450.95 28.10
11 -1 -18 355.56 27.50
11 -1 -18 431.36 27.90
11 -1 -18 389.06 28.00
11 -1 -18 471.85 28.50
13 1 -20 524.65 32.60
13 1 -20 541.65 35.20
13 1 -20 512.95 31.90
13 1 -20 499.45 32.40
-13 1 20 486.95 32.90
13 1 -20 495.35 33.10
-13 1 20 523.75 33.00
-13 1 20 513.35 32.50
-13 1 20 533.75 32.70
-13 -1 20 506.65 33.10
13 -1 -20 436.16 33.00
-13 -1 20 476.05 32.70
-13 -1 20 535.15 34.10
-13 -1 20 530.65 32.80
13 -1 -20 549.95 33.10
13 -1 -20 542.25 33.40
13 -1 -20 479.25 32.70
13 -1 -20 521.75 32.90
15 1 -22 795.52 54.49
15 1 -22 879.31 53.29
15 1 -22 865.71 53.89
-15 1 22 879.41 54.39
-15 1 22 933.41 54.19
15 1 -22 915.31 53.99
-15 -1 22 857.71 54.59
-15 -1 22 756.62 54.09
15 -1 -22 774.72 54.49
15 -1 -22 941.81 54.49
17 1 -24 19.80 3.70
-17 1 24 23.20 4.40
-17 1 24 27.00 4.20
17 1 -24 22.60 3.10
17 -1 -24 25.30 4.00
-17 -1 24 21.50 4.50
-17 -1 24 15.20 3.70
17 -1 -24 23.70 4.60
17 -1 -24 26.00 4.60
19 1 -26 21.10 2.90
19 1 -26 19.50 3.90
-19 1 26 16.30 3.90
19 -1 -26 22.10 4.20
19 -1 -26 17.40 3.80
19 -1 -26 20.60 5.40
-19 -1 26 22.90 4.70
-19 -1 26 10.00 3.50
-21 1 28 -0.50 2.40
21 1 -28 -2.70 2.10
21 1 -28 -1.80 2.40
-21 1 28 -3.90 2.30
21 -1 -28 -0.40 2.80
-21 -1 28 -0.80 3.00
-21 -1 28 0.40 3.30
21 -1 -28 -2.00 2.50
21 -1 -28 -1.20 2.90
23 1 -30 3.00 2.90
23 1 -30 7.90 2.20
-23 1 30 8.00 3.30
-23 1 30 7.30 3.40
23 -1 -30 3.20 3.20
23 -1 -30 10.50 4.10
-23 -1 30 7.50 3.70
-23 -1 30 7.20 4.30
23 -1 -30 2.90 3.20
25 1 -32 3.00 2.70
-25 1 32 3.40 3.20
-25 1 32 8.60 3.90
25 1 -32 5.00 2.10
-25 -1 32 6.00 4.40
-25 -1 32 2.30 3.80
25 -1 -32 5.20 3.70
25 -1 -32 0.00 3.60
25 -1 -32 -0.80 3.20
27 1 -34 0.10 2.10
27 1 -34 -0.60 2.70
-27 1 34 6.90 4.20
-27 1 34 12.40 7.10
27 -1 -34 3.40 3.40
-27 -1 34 0.70 4.10
27 -1 -34 1.30 3.70
-27 -1 34 -1.40 3.90
-36 2 29 6.20 3.20
36 2 -29 13.10 3.20
-36 -2 29 8.90 4.60
36 -2 -29 6.10 4.20
-36 -2 29 3.40 4.70
36 -2 -29 9.70 3.80
34 2 -27 25.50 3.90
-34 2 27 17.50 4.00
34 -2 -27 26.50 5.10
34 -2 -27 36.50 6.20
-34 -2 27 14.50 4.70
-34 -2 27 29.30 5.60
-32 2 25 1.00 2.50
32 2 -25 0.10 2.10
32 2 -25 2.30 2.30
-32 -2 25 4.70 2.40
-32 -2 25 -0.70 3.30
32 -2 -25 5.20 3.20
-32 -2 25 1.60 3.40
32 -2 -25 3.50 3.60
30 2 -23 0.50 1.80
30 2 -23 2.00 2.10
-30 -2 23 1.20 2.00
30 -2 -23 7.50 2.90
-30 -2 23 -2.60 3.10
30 -2 -23 3.90 3.40
-28 2 21 57.89 6.20
28 2 -21 59.49 5.10
28 2 -21 66.09 5.70
28 2 -21 60.49 5.30
-28 -2 21 55.79 5.20
28 -2 -21 63.89 6.80
-28 -2 21 62.99 9.30
-28 -2 21 68.39 7.10
28 -2 -21 65.09 7.20
26 2 -19 4.90 2.10
-26 2 19 2.20 2.20
-26 2 19 3.00 2.40
26 2 -19 5.40 1.90
26 -2 -19 7.00 2.80
-26 -2 19 5.00 2.80
-26 -2 19 6.30 2.00
-26 -2 19 6.70 3.10
26 -2 -19 0.50 2.60
-24 2 17 118.29 9.10
24 2 -17 125.39 8.80
-24 2 17 118.49 8.80
24 2 -17 114.79 8.50
24 2 -17 129.09 9.00
-24 2 17 122.19 8.90
24 2 -17 128.09 8.50
-24 -2 17 103.19 8.40
-24 -2 17 133.69 9.70
24 -2 -17 118.09 9.50
24 -2 -17 127.29 10.10
-24 -2 17 109.39 9.50
-22 2 15 24.50 3.50
-22 2 15 36.30 3.50
22 2 -15 29.80 3.20
22 2 -15 37.30 3.60
22 2 -15 24.40 3.00
-22 2 15 26.30 3.50
22 -2 -15 26.60 4.30
-22 -2 15 33.40 4.40
-22 -2 15 20.20 3.60
22 -2 -15 25.50 3.80
-22 -2 15 25.10 3.70
22 -2 -15 23.80 4.30
-22 -2 15 23.50 3.10
20 2 -13 39.00 3.60
-20 2 13 28.80 3.70
-20 2 13 34.50 3.40
20 2 -13 31.50 3.30
-20 2 13 41.50 4.50
20 2 -13 32.40 3.20
-20 2 13 29.60 3.50
20 2 -13 24.50 3.30
20 -2 -13 28.70 4.00
-20 -2 13 32.20 4.00
20 -2 -13 38.30 4.40
-20 -2 13 35.40 4.10
20 -2 -13 40.40 4.90
-20 -2 13 34.80 3.90
-20 -2 13 28.80 3.90
20 -2 -13 33.80 4.00
18 2 -11 5.40 1.60
-18 2 11 10.90 1.80
-18 2 11 5.40 1.90
-18 2 11 11.10 2.70
-18 2 11 6.60 1.70
18 2 -11 10.10 2.10
18 2 -11 12.80 2.50
18 -2 -11 9.70 2.50
-18 -2 11 8.50 2.10
18 -2 -11 8.10 2.10
18 -2 -11 9.70 2.80
-18 -2 11 5.10 2.00
18 -2 -11 4.40 2.10
-18 -2 11 10.00 2.40
-16 2 9 389.96 24.80
16 2 -9 388.36 24.10
-16 2 9 400.26 23.80
16 2 -9 389.66 23.80
-16 2 9 371.06 24.00
-16 2 9 379.16 24.10
16 2 -9 369.86 23.70
-16 -2 9 343.37 24.20
-16 -2 9 388.66 24.30
-16 -2 9 348.07 24.10
16 -2 -9 384.16 24.40
16 -2 -9 436.46 25.10
16 -2 -9 342.87 24.70
-16 -2 9 410.96 24.70
14 2 -7 1411.56 84.79
14 2 -7 1417.86 84.79
14 2 -7 1377.96 85.09
-14 2 7 1407.96 85.69
-14 2 7 1433.46 85.09
14 -2 -7 1205.18 85.69
-14 -2 7 1473.95 85.79
-14 -2 7 1282.67 85.19
-14 -2 7 1542.35 85.29
14 -2 -7 1522.65 85.49
14 -2 -7 1297.57 85.39
-14 -2 7 1269.07 85.09
-12 2 5 2642.84 158.18
12 2 -5 2596.64 157.48
-12 2 5 2704.33 157.48
12 -2 -5 2978.70 157.88
-12 -2 5 2398.56 157.58
-12 -2 5 2625.94 157.58
12 -2 -5 2255.87 158.68
12 -2 -5 2423.36 157.78
10 2 -3 1201.28 73.79
-10 2 3 1191.08 74.39
-10 2 3 1183.38 73.79
-10 2 3 1237.58 73.79
10 -2 -3 1091.59 74.09
-10 -2 3 1371.86 74.49
-10 -2 3 1355.16 73.99
-10 -2 3 1176.98 74.89
10 -2 -3 1381.66 74.29
-10 -2 3 1169.08 73.79
-10 -2 3 1064.39 73.89
10 -2 -3 1048.60 74.49
-8 2 1 753.62 47.20
-8 2 1 814.92 46.60
-8 2 1 785.02 46.60
-8 -2 1 693.33 46.70
-8 -2 1 874.61 47.40
-8 -2 1 877.11 46.80
8 -2 -1 690.03 46.90
-8 -2 1 723.93 47.70
8 -2 -1 674.83 47.30
-8 -2 1 714.53 46.60
-6 2 -1 290.77 17.80
6 -2 1 275.27 18.20
6 -2 1 253.37 17.50
-6 -2 -1 266.57 18.40
-6 -2 -1 325.87 17.50
6 -2 1 277.17 17.90
-6 -2 -1 255.47 17.40
4 2 3 592.44 34.50
-4 2 -3 558.64 34.10
-4 -2 -3 493.45 34.50
4 -2 3 603.54 33.80
-4 -2 -3 563.84 33.60
-4 -2 -3 521.85 33.70
-4 -2 -3 617.14 33.80
4 -2 3 492.35 33.80
4 -2 3 482.35 34.00
4 -2 3 535.85 34.50
-2 2 -5 39.60 3.30
2 2 5 38.60 3.90
-2 -2 -5 50.09 3.40
2 -2 5 35.20 4.10
2 -2 5 37.20 3.40
2 -2 5 35.40 3.30
2 -2 5 47.60 3.50
-2 -2 -5 37.20 3.20
-2 -2 -5 38.50 4.30
-2 -2 -5 39.40 3.20
2 -2 5 40.00 3.50
0 2 7 49.60 4.50
0 2 -7 46.70 3.30
0 2 -7 46.50 3.30
0 2 -7 41.70 4.50
0 2 -7 47.00 3.60
0 -2 -7 48.10 4.80
0 -2 -7 52.39 3.90
0 -2 7 40.40 3.90
0 -2 -7 36.60 3.70
0 -2 -7 52.79 3.90
0 -2 7 45.80 5.40
0 -2 7 45.50 3.70
0 -2 7 54.79 4.60
2 2 -9 1023.50 61.99
2 2 -9 1046.10 62.79
-2 2 9 1027.20 61.89
-2 2 9 1029.00 62.79
2 2 -9 1002.50 61.89
2 2 -9 1042.00 61.99
-2 2 9 1018.70 61.89
2 -2 -9 918.41 62.89
-2 -2 9 865.21 62.79
-2 -2 9 1085.29 62.39
2 -2 -9 937.31 62.29
-2 -2 9 1119.49 62.69
2 -2 -9 1146.49 62.39
-2 -2 9 918.41 62.29
-2 -2 9 983.90 61.99
-4 2 11 154.98 9.80
4 2 -11 160.18 10.60
4 2 -11 152.08 9.70
4 2 -11 147.59 9.70
-4 2 11 149.99 10.60
-4 2 11 157.08 9.80
-4 -2 11 156.48 10.60
-4 -2 11 131.09 10.60
4 -2 -11 146.99 11.40
4 -2 -11 134.99 10.20
-4 -2 11 136.09 10.20
-4 -2 11 158.28 10.20
4 -2 -11 149.49 10.20
4 -2 -11 157.98 10.20
-6 2 13 891.51 56.19
-6 2 13 915.91 55.49
-6 2 13 951.50 55.99
-6 2 13 913.41 55.49
6 2 -13 922.61 55.49
6 2 -13 916.71 55.49
6 2 -13 889.01 56.09
-6 -2 13 947.91 55.89
-6 -2 13 856.31 56.29
6 -2 -13 947.91 55.89
-6 -2 13 851.41 56.39
-6 -2 13 903.81 56.29
6 -2 -13 904.01 56.49
6 -2 -13 790.82 56.29
6 -2 -13 888.81 55.89
8 2 -15 4.60 2.20
-8 2 15 2.90 1.60
8 2 -15 2.60 1.50
8 2 -15 1.20 1.50
-8 2 15 2.90 1.60
-8 2 15 9.30 2.60
-8 2 15 4.60 2.10
8 -2 -15 2.40 2.60
-8 -2 15 1.90 1.90
-8 -2 15 4.00 2.10
8 -2 -15 6.50 2.70
-8 -2 15 4.80 2.70
8 -2 -15 5.40 2.00
-8 -2 15 5.70 2.60
8 -2 -15 1.60 1.80
8 -2 -15 3.40 2.00
-10 2 17 313.37 19.50
10 2 -17 292.07 19.90
-10 2 17 286.57 19.80
-10 2 17 304.07 19.40
10 2 -17 296.77 19.30
-10 2 17 301.57 20.30
10 2 -17 284.37 20.60
-10 -2 17 292.97 20.30
-10 -2 17 361.66 20.80
10 -2 -17 340.37 20.00
10 -2 -17 313.07 20.60
-10 -2 17 319.47 20.60
10 -2 -17 271.97 19.80
10 -2 -17 284.67 20.40
-10 -2 17 282.67 19.90
10 -2 -17 286.07 20.40
-12 2 19 294.17 20.60
-12 2 19 308.97 20.60
12 2 -19 293.37 19.80
-12 2 19 308.67 20.00
-12 2 19 307.37 20.10
12 2 -19 302.97 19.90
12 -2 -19 316.97 20.70
-12 -2 19 274.37 21.00
12 -2 -19 293.17 21.10
12 -2 -19 309.27 20.70
12 -2 -19 330.17 21.40
12 -2 -19 335.17 21.40
-12 -2 19 297.67 20.50
-12 -2 19 350.26 20.70
-14 2 21 -1.60 1.80
14 2 -21 2.30 1.80
14 2 -21 0.80 1.90
-14 2 21 -2.00 2.00
-14 2 21 -0.70 2.70
14 -2 -21 -2.10 3.00
-14 -2 21 3.10 3.30
14 -2 -21 -1.80 2.30
14 -2 -21 2.10 3.00
-14 -2 21 1.50 2.80
-16 2 23 12.00 3.70
-16 2 23 14.90 3.00
16 2 -23 17.40 2.80
16 2 -23 15.70 2.70
16 -2 -23 15.70 4.20
-16 -2 23 13.60 3.50
16 -2 -23 17.30 4.30
18 2 -25 23.40 3.50
-18 2 25 28.60 4.00
-18 2 25 25.90 4.70
-18 -2 25 22.70 4.60
18 -2 -25 23.20 5.00
18 -2 -25 26.10 4.30
-18 -2 25 19.40 4.80
-20 2 27 18.00 4.20
20 2 -27 19.80 3.20
20 -2 -27 23.90 4.70
20 -2 -27 13.30 3.80
-20 -2 27 19.00 4.30
20 -2 -27 26.40 4.90
-20 -2 27 12.70 4.70
-22 2 29 5.80 2.90
22 2 -29 4.70 2.70
-22 2 29 7.30 3.90
-22 -2 29 4.60 3.70
22 -2 -29 4.20 3.80
-22 -2 29 9.20 4.80
22 -2 -29 7.10 3.80
22 -2 -29 3.10 3.20
-24 2 31 3.30 3.40
24 2 -31 2.80 2.60
-24 2 31 -3.40 2.90
24 -2 -31 9.90 4.40
24 -2 -31 1.20 3.50
-24 -2 31 2.00 4.00
24 -2 -31 -0.60 3.80
-24 -2 31 2.50 4.70
26 2 -33 24.30 4.40
-26 2 33 16.90 4.30
-26 2 33 26.20 5.60
26 -2 -33 27.70 5.80
-26 -2 33 27.00 5.60
26 -2 -33 23.50 5.30
-26 -2 33 24.50 6.90
26 -2 -33 41.20 6.90
33 3 -26 1.30 2.00
-33 3 26 3.40 2.60
-33 -3 26 10.00 4.40
33 -3 -26 0.30 6.20
33 -3 -26 4.10 6.90
-33 -3 26 -0.40 3.50
-31 3 24 63.09 6.30
31 3 -24 60.49 5.30
31 -3 -24 72.19 8.60
31 -3 -24 67.89 7.70
-31 -3 24 58.09 7.40
-31 -3 24 62.39 7.60
29 3 -22 2.50 1.60
-29 3 22 2.80 2.30
-29 3 22 0.70 2.90
-29 -3 22 0.00 2.70
29 -3 -22 -0.70 3.20
29 -3 -22 1.10 2.50
-27 3 20 9.30 2.30
27 3 -20 10.50 1.70
-27 3 20 8.90 2.70
-27 3 20 13.20 2.80
27 3 -20 7.30 1.70
27 -3 -20 11.70 3.50
-27 -3 20 14.50 4.00
27 -3 -20 9.10 3.90
-25 3 18 -2.50 1.70
-25 3 18 1.40 1.70
-25 3 18 2.90 1.90
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1 1 7 431.36 26.70
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1 -1 7 427.46 26.50
1 1 -9 16.70 2.20
1 1 -9 15.20 2.50
1 1 -9 16.60 2.40
1 1 -9 16.80 2.10
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1 -1 -9 13.90 2.20
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1 -1 -9 16.30 2.70
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-1 1 -8 236.28 15.30
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1 1 8 242.98 15.10
1 1 8 236.28 15.60
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1 -1 8 270.07 15.30
1 -1 8 195.08 15.00
1 1 -10 2205.68 136.79
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1 1 -10 2189.08 136.59
1 1 -10 2315.47 136.79
1 1 -10 2201.08 137.09
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1 1 -10 2239.58 136.99
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1 -1 -10 1997.90 136.89
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1 -1 -10 2231.58 136.79
1 -1 -10 2066.29 137.29
-1 -1 10 2410.36 136.99
1 -1 -10 2476.95 136.99
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3 1 -12 25.90 3.20
3 1 -12 25.40 3.40
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7 1 -16 9.10 2.00
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7 1 -16 10.30 1.70
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7 -1 -16 10.20 2.80
7 -1 -16 6.10 2.00
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11 -1 -20 150.78 12.20
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11 -1 -20 143.29 11.70
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19 -1 -28 -0.60 2.50
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36 -2 -27 -1.40 3.90
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12 -2 -3 1775.02 115.19
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12 -2 -3 1613.04 115.99
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10 -2 -1 2.60 2.00
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2 -2 7 180.18 10.80
2 -2 7 168.38 10.80
0 2 -9 70.69 5.30
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0 2 -9 74.29 5.30
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21 1 -11 3.90 2.00
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21 -1 -11 4.60 2.00
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17 -1 -7 572.04 33.40
17 -1 -7 496.85 33.60
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15 -1 -5 24.40 3.20
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13 -1 -3 38.90 3.70
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11 -1 -1 946.01 53.49
11 -1 -1 802.72 53.59
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1 1 9 412.06 25.70
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1 1 9 403.06 26.30
-1 1 -9 418.06 25.90
1 1 9 419.76 25.90
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1 1 9 420.36 25.80
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1 -1 9 416.26 26.10
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-1 -1 -9 450.05 26.00
-1 -1 -9 441.96 25.80
1 -1 9 338.57 25.90
1 -1 9 402.26 26.20
1 -1 9 439.86 26.00
1 1 -11 365.36 22.50
1 1 -11 357.36 22.70
1 1 -11 355.46 22.70
-1 1 11 338.17 22.90
1 1 -11 367.56 22.50
1 1 -11 357.46 22.30
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1 -1 -11 389.86 22.70
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1 -1 -11 303.87 22.50
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1 -1 -11 366.76 22.50
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3 1 -13 624.54 38.50
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3 1 -13 609.94 38.10
3 1 -13 629.14 38.40
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3 -1 -13 646.84 38.50
3 -1 -13 682.63 38.70
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5 1 -15 27.70 3.40
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5 1 -15 25.90 2.80
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5 -1 -15 23.30 3.40
5 -1 -15 29.90 3.50
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7 1 -17 38.30 4.50
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7 -1 -17 40.00 4.20
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7 -1 -17 31.40 4.10
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9 1 -19 141.39 9.60
9 1 -19 146.69 10.30
9 1 -19 145.99 10.20
9 1 -19 147.79 11.00
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11 -1 -21 631.84 38.00
11 -1 -21 603.74 37.80
11 -1 -21 495.25 38.00
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13 1 -23 385.86 23.90
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13 -1 -23 316.77 24.40
13 -1 -23 365.66 24.10
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13 -1 -23 396.06 24.40
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15 1 -25 129.49 9.00
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17 -1 -27 104.79 8.90
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19 1 -29 -0.50 1.60
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21 -1 -31 6.80 3.70
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36 -2 -26 44.60 7.00
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34 -2 -24 -2.40 2.70
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-14 0 3 3.00 1.70
-12 0 1 4.20 1.40
-12 0 1 1.10 1.30
-12 0 1 0.10 1.30
12 0 -1 -0.20 1.30
12 0 -1 -1.40 1.10
-12 0 1 0.20 1.40
-10 0 -1 -0.10 1.10
10 0 1 -1.10 1.30
10 0 1 1.60 1.50
10 0 1 0.90 1.20
-10 0 -1 3.20 1.40
-10 0 -1 -0.80 1.10
10 0 1 0.00 1.10
10 0 1 1.10 1.20
-10 0 -1 -1.70 1.30
8 0 3 1.40 1.20
8 0 3 1.50 1.40
-8 0 -3 1.90 1.50
-8 0 -3 1.90 1.40
-8 0 -3 0.20 1.10
-8 0 -3 1.60 1.20
8 0 3 0.10 1.40
8 0 3 -0.50 1.10
8 0 3 0.10 1.10
6 0 5 4.40 1.80
6 0 5 0.60 1.20
-6 0 -5 0.80 1.20
6 0 5 2.80 1.30
6 0 5 0.00 1.20
6 0 5 1.20 1.30
-6 0 -5 0.40 1.40
-6 0 -5 1.50 1.20
-6 0 -5 0.60 1.30
-6 0 -5 1.10 1.30
4 0 7 -0.30 1.30
-4 0 -7 -1.40 1.30
4 0 7 0.80 1.30
-4 0 -7 0.50 1.20
-4 0 -7 -0.10 1.50
4 0 7 -1.80 1.10
-4 0 -7 1.10 1.30
4 0 7 1.80 1.30
-4 0 -7 3.00 1.40
2 0 9 0.90 1.60
-2 0 -9 6.80 1.70
2 0 9 -3.10 1.40
2 0 9 3.60 1.60
-2 0 -9 0.40 1.70
-2 0 -9 0.70 1.40
-2 0 13 1.30 1.50
-2 0 13 3.10 1.80
2 0 -13 -0.10 1.80
-2 0 13 0.00 1.40
2 0 -13 -1.30 1.50
-2 0 13 3.00 1.80
2 0 -13 1.00 1.40
2 0 -13 -2.40 1.30
4 0 -15 3.70 2.00
4 0 -15 -2.80 1.30
-4 0 15 -2.60 1.40
4 0 -15 0.00 1.50
4 0 -15 -0.70 1.40
-4 0 15 0.20 1.60
-4 0 15 -0.30 1.80
-4 0 15 0.80 1.80
-6 0 17 -0.20 1.80
6 0 -17 2.90 2.20
6 0 -17 -2.20 1.60
6 0 -17 1.10 1.80
-6 0 17 -0.10 1.90
-8 0 19 -2.70 1.90
8 0 -19 1.40 2.00
8 0 -19 -2.80 2.00
8 0 -19 1.00 1.80
-8 0 19 0.40 1.80
8 0 -19 -0.50 1.80
-8 0 19 2.50 2.30
-8 0 19 -0.60 1.90
10 0 -21 2.00 2.70
-10 0 21 0.70 2.50
10 0 -21 -0.20 2.20
-10 0 21 -0.90 2.50
12 0 -23 1.50 2.40
12 0 -23 1.20 2.20
-12 0 23 -1.80 2.50
12 0 -23 1.80 2.80
-12 0 23 2.60 2.70
14 0 -25 -1.60 2.20
-14 0 25 -8.00 4.10
-14 0 25 1.60 2.80
-16 0 27 4.40 3.20
16 0 -27 -2.50 2.10
-16 0 27 -1.20 2.90
16 0 -27 2.50 3.10
16 0 -27 1.30 2.40
-18 0 29 4.10 3.00
18 0 -29 1.60 2.80
18 0 -29 1.20 2.90
-18 0 29 -1.50 2.70
18 0 -29 -1.00 2.20
-20 0 31 -2.40 2.80
20 0 -31 2.10 2.70
-20 0 31 -1.20 3.40
20 0 -31 -0.90 2.50
20 0 -31 4.70 3.60
22 0 -33 1.30 3.00
22 0 -33 1.30 4.30
-22 0 33 -1.60 3.50
22 0 -33 3.30 2.90
-22 0 33 -4.30 3.30
24 0 -35 8.50 3.80
24 0 -35 5.80 4.10
-24 0 35 6.80 4.70
-24 0 35 8.60 4.10
24 0 -35 0.40 3.30
39 1 -28 2.70 3.30
39 1 -28 1.60 2.80
-39 1 28 6.60 6.20
39 -1 -28 0.90 3.70
-39 -1 28 7.80 3.80
39 -1 -28 3.70 3.30
-37 1 26 3.40 3.40
37 1 -26 5.30 2.80
37 1 -26 7.30 3.10
37 -1 -26 15.60 4.60
37 -1 -26 10.70 3.80
-37 -1 26 8.20 4.60
-37 -1 26 6.00 3.60
35 1 -24 0.90 2.40
-35 1 24 -3.20 2.50
35 -1 -24 2.70 2.60
-35 -1 24 5.00 3.80
35 -1 -24 2.50 3.20
-35 -1 24 -0.20 3.20
33 1 -22 33.30 4.40
-33 1 22 27.40 4.50
33 1 -22 37.70 4.90
-33 -1 22 24.30 4.80
33 -1 -22 28.60 4.70
33 -1 -22 37.30 5.60
31 1 -20 31.20 4.20
-31 1 20 24.50 4.80
31 1 -20 24.60 3.80
-31 1 20 26.90 4.90
31 -1 -20 21.00 4.20
31 -1 -20 31.90 4.90
-31 -1 20 25.50 4.70
-31 -1 20 32.70 4.40
-31 -1 20 19.60 4.60
-29 1 18 41.50 4.80
-29 1 18 32.00 4.70
29 1 -18 38.00 4.40
29 1 -18 32.00 4.40
29 -1 -18 32.20 5.10
-29 -1 18 24.00 4.80
-29 -1 18 50.69 5.70
29 -1 -18 52.99 5.70
-29 -1 18 44.00 5.20
27 1 -16 2.10 1.70
27 1 -16 2.90 2.30
27 1 -16 6.60 2.20
-27 1 16 1.80 2.40
-27 1 16 4.70 2.20
27 1 -16 2.60 2.20
-27 -1 16 -1.00 2.40
27 -1 -16 3.50 2.80
-27 -1 16 3.10 2.50
-27 -1 16 2.50 2.10
27 -1 -16 -0.70 2.20
25 1 -14 886.81 56.69
25 1 -14 940.61 56.79
25 1 -14 858.31 56.49
-25 1 14 902.21 56.59
-25 1 14 974.40 56.99
25 1 -14 979.90 56.79
-25 1 14 928.71 56.89
-25 1 14 928.31 57.29
25 -1 -14 956.80 57.29
-25 -1 14 1033.30 59.49
25 -1 -14 912.31 56.99
25 -1 -14 935.21 57.29
-25 -1 14 774.42 56.79
-25 -1 14 853.61 56.79
-25 -1 14 805.82 56.69
23 1 -12 135.49 9.40
-23 1 12 126.19 9.40
-23 1 12 132.89 9.10
-23 1 12 140.09 9.90
-23 1 12 127.39 9.30
23 1 -12 120.39 8.90
23 1 -12 122.69 9.20
23 1 -12 131.09 9.10
-23 -1 12 115.59 9.20
-23 -1 12 118.29 9.60
23 -1 -12 142.09 9.90
23 -1 -12 126.89 9.30
-23 -1 12 134.79 9.60
-23 -1 12 118.19 9.70
23 -1 -12 109.69 9.40
23 -1 -12 125.09 9.50
-21 1 10 625.14 39.80
-21 1 10 652.13 40.90
21 1 -10 644.64 39.70
21 1 -10 651.53 39.70
-21 1 10 680.03 39.90
21 1 -10 661.33 39.80
-21 1 10 644.74 39.60
-21 -1 10 538.55 39.80
-21 -1 10 559.94 39.60
21 -1 -10 674.03 40.20
-21 -1 10 634.54 39.90
-21 -1 10 704.53 40.10
21 -1 -10 596.14 40.00
21 -1 -10 623.64 40.20
-19 1 8 288.47 19.00
19 1 -8 299.07 19.10
19 1 -8 297.67 18.80
19 1 -8 291.97 18.70
-19 1 8 294.77 19.00
19 1 -8 304.57 19.40
-19 1 8 284.57 19.30
-19 -1 8 264.07 19.00
19 -1 -8 304.77 19.30
19 -1 -8 322.17 19.20
-19 -1 8 296.17 19.20
-19 -1 8 330.57 19.20
19 -1 -8 285.07 19.40
19 -1 -8 246.88 19.00
-17 1 6 70.09 5.80
17 1 -6 68.29 5.00
-17 1 6 69.09 5.50
17 1 -6 69.49 5.40
17 1 -6 70.99 5.20
-17 1 6 64.59 5.80
17 1 -6 72.59 5.60
-17 -1 6 58.09 5.70
-17 -1 6 74.99 5.70
-17 -1 6 74.39 5.70
17 -1 -6 57.69 5.50
17 -1 -6 65.89 5.80
17 -1 -6 73.49 5.60
15 1 -4 346.57 20.90
-15 1 4 324.77 20.90
-15 1 4 333.97 20.60
15 1 -4 319.77 20.80
15 1 -4 336.87 21.20
-15 1 4 337.57 21.30
-15 1 4 314.67 20.90
15 1 -4 344.37 20.50
-15 -1 4 356.26 21.20
15 -1 -4 344.97 21.10
15 -1 -4 292.67 21.00
-15 -1 4 334.07 21.00
-15 -1 4 338.27 21.50
-15 -1 4 278.77 20.90
13 1 -2 532.05 33.20
-13 1 2 560.54 33.80
13 1 -2 529.85 33.60
13 1 -2 526.75 33.90
13 1 -2 555.04 33.70
-13 1 2 527.05 33.40
-13 1 2 518.75 33.70
-13 1 2 550.64 34.10
-13 -1 2 579.54 33.90
13 -1 -2 496.05 34.00
-13 -1 2 572.94 34.10
13 -1 -2 593.94 34.00
-13 -1 2 544.05 34.30
13 -1 -2 484.85 33.80
11 1 0 170.38 11.40
-11 1 0 168.18 11.30
-11 1 0 167.38 10.70
11 1 0 165.58 11.00
-11 1 0 176.58 11.10
-11 -1 0 179.38 11.40
-11 -1 0 171.68 11.60
11 -1 0 186.68 11.30
11 -1 0 140.19 11.10
-11 -1 0 183.18 11.20
11 -1 0 157.58 11.40
-11 -1 0 148.29 11.00
9 1 2 6.40 1.50
9 1 2 2.40 1.80
-9 1 -2 2.10 1.20
-9 1 -2 -0.30 1.20
-9 1 -2 2.80 1.50
-9 1 -2 -0.30 1.30
9 -1 2 -0.10 1.40
9 -1 2 0.70 1.50
9 -1 2 0.70 1.80
9 -1 2 3.80 1.50
-9 -1 -2 -1.00 1.20
9 -1 2 5.30 1.40
-9 -1 -2 0.40 1.40
-9 -1 -2 4.10 1.70
-9 -1 -2 8.70 2.30
-7 1 -4 1807.02 110.09
-7 1 -4 1809.42 110.19
7 1 4 1782.52 109.79
-7 1 -4 1841.12 110.19
7 1 4 1810.12 110.69
-7 1 -4 1761.22 110.39
7 1 4 1761.92 110.09
-7 -1 -4 1744.03 109.79
7 -1 4 1926.11 110.59
-7 -1 -4 1504.05 110.19
-7 -1 -4 1949.41 110.29
-7 -1 -4 1921.21 110.69
7 -1 4 1977.30 110.39
-7 -1 -4 1812.02 110.79
7 -1 4 1836.02 110.19
7 -1 4 1545.65 110.19
5 1 6 7430.96 457.65
-5 1 -6 7630.94 458.05
5 1 6 7543.35 457.95
5 1 6 7489.95 458.45
5 1 6 7643.04 457.95
-5 1 -6 7656.23 458.05
-5 1 -6 7474.55 458.15
-5 1 -6 7523.45 458.05
-5 1 -6 7515.45 458.25
5 -1 6 7586.44 458.15
-5 -1 -6 7464.75 457.75
5 -1 6 6838.52 458.15
-5 -1 -6 8076.59 458.15
-5 -1 -6 7144.89 458.55
5 -1 6 7522.35 458.35
-5 -1 -6 6428.16 458.05
5 -1 6 8250.08 458.25
-5 -1 -6 8024.40 458.55
3 1 8 390.66 25.40
-3 1 -8 417.66 25.30
-3 1 -8 400.06 25.00
-3 1 -8 415.96 25.20
-3 1 -8 405.76 25.00
3 1 8 408.46 25.00
3 1 8 396.86 24.70
3 1 8 403.86 24.90
-3 -1 -8 422.36 24.80
-3 -1 -8 348.67 25.00
3 -1 8 415.46 25.20
3 -1 8 420.46 25.20
-3 -1 -8 379.56 25.50
3 -1 8 390.96 25.30
-3 -1 -8 438.86 25.20
3 -1 8 337.37 25.00
3 -1 8 353.46 25.00
-1 1 -10 1480.95 90.99
-1 1 -10 1487.95 90.69
1 1 10 1500.25 90.69
1 1 10 1451.15 90.49
1 1 10 1458.15 91.09
-1 1 -10 1506.55 90.99
1 1 10 1520.35 90.69
-1 1 -10 1533.15 90.79
-1 -1 -10 1267.27 90.69
1 -1 10 1407.36 91.09
1 -1 10 1252.87 90.69
1 -1 10 1644.04 90.89
1 -1 10 1470.45 90.99
-1 -1 -10 1525.85 90.69
-1 -1 -10 1634.34 90.89
1 1 -12 733.33 46.60
-1 1 12 734.33 46.20
-1 1 12 745.93 46.30
1 1 -12 757.32 46.60
-1 1 12 776.02 46.30
1 1 -12 745.23 46.30
1 1 -12 766.02 46.30
-1 1 12 732.53 46.70
-1 -1 12 725.53 46.60
1 -1 -12 814.42 46.50
1 -1 -12 767.12 46.30
1 -1 -12 685.83 46.80
1 -1 -12 661.23 46.40
-1 -1 12 798.22 46.50
-1 -1 12 717.83 46.50
-3 1 14 914.41 54.89
-3 1 14 937.71 54.89
3 1 -14 884.51 55.09
3 1 -14 949.51 54.99
-3 1 14 871.01 55.29
-3 1 14 893.41 54.89
3 1 -14 867.61 55.19
3 1 -14 920.31 54.89
-3 -1 14 894.71 55.19
3 -1 -14 871.61 54.89
-3 -1 14 946.91 55.09
3 -1 -14 841.82 55.49
-3 -1 14 866.61 55.19
3 -1 -14 756.12 54.89
-3 -1 14 738.33 54.89
3 -1 -14 985.20 55.09
5 1 -16 145.09 10.50
-5 1 16 147.09 10.20
5 1 -16 142.59 9.70
-5 1 16 153.88 10.30
5 1 -16 141.49 10.00
-5 1 16 144.89 10.10
5 1 -16 174.98 10.40
5 -1 -16 123.09 10.20
-5 -1 16 155.68 10.70
5 -1 -16 142.89 10.20
-5 -1 16 142.49 10.60
5 -1 -16 137.49 10.80
-5 -1 16 121.89 10.20
7 1 -18 45.70 4.60
-7 1 18 31.00 4.30
7 1 -18 38.40 4.40
-7 1 18 36.60 4.60
-7 1 18 45.60 4.60
7 1 -18 36.30 3.50
7 1 -18 37.30 4.70
7 -1 -18 32.10 4.30
7 -1 -18 36.10 5.00
-7 -1 18 41.60 5.00
7 -1 -18 32.40 4.30
-7 -1 18 33.90 4.40
-7 -1 18 41.80 4.90
7 -1 -18 41.70 4.60
-7 -1 18 36.60 4.50
9 1 -20 24.80 3.10
-9 1 20 31.90 4.40
9 1 -20 23.00 3.50
-9 1 20 24.00 3.70
9 1 -20 26.40 3.80
9 1 -20 36.50 4.90
-9 1 20 20.30 3.40
9 -1 -20 22.70 3.80
9 -1 -20 23.30 3.90
-9 -1 20 36.10 4.30
-9 -1 20 27.40 4.50
9 -1 -20 30.40 4.80
11 1 -22 50.19 5.90
11 1 -22 49.60 4.30
-11 1 22 44.70 5.60
11 1 -22 45.40 4.50
-11 1 22 53.99 5.70
11 -1 -22 42.40 5.90
11 -1 -22 43.10 5.60
11 -1 -22 45.40 5.90
-11 -1 22 40.20 5.50
-11 -1 22 46.90 6.00
13 1 -24 2.00 2.50
13 1 -24 1.30 1.80
-13 1 24 0.90 2.70
13 1 -24 -1.00 2.90
13 1 -24 -1.00 2.10
-13 1 24 3.50 3.00
-13 -1 24 1.20 3.50
13 -1 -24 0.40 2.90
13 -1 -24 -0.80 2.70
-13 -1 24 2.50 3.00
13 -1 -24 2.10 2.60
-15 1 26 9.10 5.20
15 1 -26 10.90 3.70
15 1 -26 6.90 3.50
-15 1 26 7.80 4.30
15 1 -26 6.90 2.70
15 1 -26 6.60 2.10
-15 -1 26 4.50 3.50
15 -1 -26 10.40 3.20
-15 -1 26 8.10 3.50
15 -1 -26 8.70 3.60
15 -1 -26 7.40 3.90
17 1 -28 16.40 3.00
17 1 -28 21.10 4.50
-17 1 28 10.30 3.80
17 1 -28 16.10 3.60
17 1 -28 18.10 2.80
-17 1 28 17.00 3.70
17 -1 -28 20.50 4.80
17 -1 -28 12.70 3.50
17 -1 -28 16.00 4.10
-17 -1 28 19.10 4.50
-17 -1 28 7.60 3.50
-19 1 30 23.50 5.00
19 1 -30 36.10 5.10
-19 1 30 28.20 4.90
19 1 -30 29.70 3.80
-19 -1 30 24.50 5.20
-19 -1 30 24.00 4.50
19 -1 -30 21.50 4.50
19 -1 -30 19.60 5.30
19 -1 -30 34.00 5.40
21 1 -32 -0.30 3.00
-21 1 32 0.10 3.50
21 1 -32 2.80 2.20
-21 1 32 0.30 2.90
-21 -1 32 4.10 4.00
21 -1 -32 2.70 3.30
-21 -1 32 -2.40 3.70
21 -1 -32 2.30 3.70
21 -1 -32 3.60 3.70
-23 1 34 8.10 4.80
23 1 -34 2.70 3.10
23 1 -34 0.40 2.30
-23 1 34 10.20 4.60
-23 -1 34 1.40 4.00
23 -1 -34 0.30 3.40
23 -1 -34 -0.10 4.20
23 -1 -34 3.00 3.50
-23 -1 34 8.10 5.20
-38 2 27 12.70 3.80
38 2 -27 6.30 2.90
38 2 -27 4.10 2.90
-38 -2 27 7.60 4.50
38 -2 -27 4.20 3.70
-38 -2 27 11.90 4.80
-36 2 25 25.00 4.60
36 2 -25 30.40 4.10
36 2 -25 28.80 4.30
-36 -2 25 24.00 5.20
-36 -2 25 34.00 5.90
36 -2 -25 34.20 5.70
36 -2 -25 27.30 5.70
-34 2 23 6.50 3.10
34 2 -23 10.00 2.70
34 2 -23 9.90 2.80
34 -2 -23 8.50 3.60
-34 -2 23 4.70 4.30
-34 -2 23 5.50 3.60
-34 -2 23 13.40 4.00
34 -2 -23 9.80 4.30
-32 2 21 17.70 3.40
32 2 -21 13.10 3.00
-32 2 21 14.00 3.40
32 2 -21 12.40 2.90
-32 -2 21 18.20 3.20
32 -2 -21 20.20 4.60
-32 -2 21 13.70 4.30
32 -2 -21 5.90 3.60
-32 -2 21 4.90 3.60
-30 2 19 27.00 3.70
30 2 -19 18.90 3.10
-30 2 19 23.80 3.90
30 2 -19 21.40 3.40
30 2 -19 25.50 3.70
-30 -2 19 24.70 4.60
30 -2 -19 21.80 4.40
-30 -2 19 21.00 4.30
30 -2 -19 31.50 5.10
-30 -2 19 31.00 4.00
-28 2 17 3.80 2.40
28 2 -17 6.50 2.20
28 2 -17 0.60 2.00
28 2 -17 6.30 1.90
-28 2 17 4.10 2.30
28 2 -17 5.50 2.40
28 -2 -17 -1.40 3.20
-28 -2 17 8.00 2.90
-28 -2 17 -2.10 2.60
-28 -2 17 4.50 2.10
-26 2 15 5.00 2.60
26 2 -15 8.50 2.10
26 2 -15 11.00 2.50
26 2 -15 13.60 2.70
26 2 -15 12.40 2.60
-26 2 15 11.50 2.50
-26 -2 15 9.80 3.30
26 -2 -15 7.50 3.50
-26 -2 15 10.80 2.50
-26 -2 15 11.70 3.10
26 -2 -15 11.60 3.20
24 2 -13 494.05 31.70
-24 2 13 520.75 31.90
-24 2 13 494.35 32.00
24 2 -13 526.15 31.60
24 2 -13 492.05 31.40
-24 2 13 510.55 31.40
-24 -2 13 437.06 31.70
-24 -2 13 507.45 32.30
24 -2 -13 499.85 32.40
-24 -2 13 536.35 32.30
-24 -2 13 485.35 31.90
24 -2 -13 505.55 32.80
22 2 -11 285.57 18.90
-22 2 11 277.37 18.40
22 2 -11 268.37 18.00
-22 2 11 287.87 18.40
22 2 -11 278.37 18.20
-22 2 11 285.17 17.90
22 2 -11 278.77 18.10
22 -2 -11 309.07 19.00
22 -2 -11 304.97 19.60
-22 -2 11 248.08 18.60
-22 -2 11 314.97 18.90
-22 -2 11 286.17 18.50
-22 -2 11 245.28 18.40
22 -2 -11 282.37 18.90
20 2 -9 28.90 3.20
20 2 -9 34.30 3.60
-20 2 9 28.40 3.50
20 2 -9 27.50 3.00
20 2 -9 30.50 3.30
-20 2 9 27.80 3.40
-20 2 9 32.00 4.30
20 -2 -9 27.70 3.80
-20 -2 9 28.50 3.80
-20 -2 9 26.50 3.50
-20 -2 9 30.60 3.70
-20 -2 9 28.20 3.70
20 -2 -9 33.00 4.10
20 -2 -9 32.70 4.70
18 2 -7 57.39 4.50
-18 2 7 59.89 4.90
-18 2 7 61.39 5.10
-18 2 7 63.89 5.80
18 2 -7 61.99 4.70
-18 -2 7 56.59 5.20
18 -2 -7 57.89 5.90
18 -2 -7 57.89 5.40
-18 -2 7 52.69 4.60
-18 -2 7 66.89 5.50
18 -2 -7 71.69 5.50
-18 -2 7 59.59 5.40
-16 2 5 69.59 5.30
16 2 -5 74.39 5.00
16 2 -5 73.09 5.00
-16 2 5 74.69 5.50
-16 2 5 72.89 6.30
16 2 -5 71.89 4.80
-16 -2 5 63.19 4.90
-16 -2 5 60.69 5.60
-16 -2 5 72.09 5.70
-16 -2 5 73.99 6.00
16 -2 -5 57.09 6.20
-16 -2 5 70.99 7.00
16 -2 -5 76.69 5.80
16 -2 -5 61.39 5.80
-14 2 3 591.24 37.80
-14 2 3 631.14 37.20
-14 2 3 604.34 37.20
14 2 -3 588.74 36.90
14 2 -3 623.94 36.90
-14 -2 3 595.84 38.40
-14 -2 3 656.33 37.50
-14 -2 3 532.25 37.30
-14 -2 3 638.64 37.80
14 -2 -3 670.33 37.70
14 -2 -3 520.75 37.90
14 -2 -3 535.85 37.60
-12 2 1 4.50 1.90
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17 -1 -29 31.20 5.90
17 -1 -29 31.10 5.10
17 -1 -29 40.60 6.40
-17 -1 29 29.00 5.50
-17 -1 29 36.30 5.20
19 1 -31 6.50 2.50
19 1 -31 1.70 2.90
19 1 -31 2.50 2.40
-19 1 31 5.60 3.30
-19 1 31 8.80 4.10
-19 -1 31 6.70 3.60
19 -1 -31 -1.90 3.50
19 -1 -31 1.80 3.00
19 -1 -31 8.90 4.20
-19 -1 31 -4.50 3.80
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21 1 -33 15.30 2.90
21 1 -33 14.90 4.00
-21 1 33 14.70 4.00
21 -1 -33 15.40 4.70
21 -1 -33 17.90 7.00
-21 -1 33 6.60 7.70
-21 -1 33 18.10 6.20
21 -1 -33 22.50 7.10
38 2 -26 4.80 3.00
38 2 -26 2.60 2.60
-38 2 26 4.20 3.20
-38 -2 26 0.50 4.20
38 -2 -26 2.60 3.30
38 -2 -26 3.00 4.60
-38 -2 26 9.90 4.20
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36 2 -24 11.30 3.10
36 2 -24 10.70 2.90
-36 -2 24 19.50 4.60
36 -2 -24 9.70 3.60
36 -2 -24 5.00 4.30
-36 -2 24 14.00 4.20
-36 -2 24 1.70 3.80
-34 2 22 -0.10 3.20
34 2 -22 2.30 2.30
34 2 -22 0.10 2.20
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-34 -2 22 3.20 2.60
34 -2 -22 1.90 3.00
-34 -2 22 4.00 3.50
34 -2 -22 1.60 3.40
32 2 -20 5.70 2.70
-32 2 20 5.30 2.80
-32 2 20 0.10 3.90
32 2 -20 5.10 2.50
32 -2 -20 6.00 3.60
-32 -2 20 5.40 3.40
32 -2 -20 2.60 3.10
-32 -2 20 10.80 4.60
-32 -2 20 7.60 3.50
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30 2 -18 55.29 8.00
-30 2 18 51.99 5.80
30 2 -18 57.39 5.20
30 2 -18 43.10 4.80
30 2 -18 48.30 5.20
-30 -2 18 43.60 6.20
30 -2 -18 48.20 6.20
30 -2 -18 51.19 6.50
-30 -2 18 54.19 5.40
-30 -2 18 56.89 6.30
28 2 -16 15.10 2.80
-28 2 16 6.90 2.60
28 2 -16 5.30 2.30
-28 2 16 10.30 2.60
28 2 -16 6.30 2.30
28 2 -16 7.30 2.50
-28 -2 16 8.80 2.90
-28 -2 16 6.20 2.80
-28 -2 16 8.90 3.30
28 -2 -16 4.70 3.10
26 2 -14 40.70 4.40
-26 2 14 45.80 4.50
-26 2 14 50.69 5.30
26 2 -14 48.70 4.80
-26 2 14 49.80 4.90
26 2 -14 53.19 4.80
26 2 -14 48.80 5.00
-26 -2 14 46.20 5.40
-26 -2 14 45.50 5.90
-26 -2 14 49.50 5.00
26 -2 -14 45.50 5.80
26 -2 -14 52.79 6.20
24 2 -12 67.69 5.70
-24 2 12 73.29 6.00
-24 2 12 71.39 6.30
-24 2 12 63.39 6.40
24 2 -12 58.69 5.40
24 2 -12 74.79 6.20
24 2 -12 70.19 5.80
24 -2 -12 60.99 6.70
-24 -2 12 66.79 6.00
24 -2 -12 82.79 7.70
-24 -2 12 62.99 6.60
-24 -2 12 58.69 6.40
-24 -2 12 65.49 7.00
-22 2 10 238.88 16.10
-22 2 10 231.38 16.00
22 2 -10 242.68 15.60
22 2 -10 230.48 15.70
22 2 -10 242.68 16.10
22 2 -10 244.18 15.80
-22 2 10 252.27 15.40
-22 -2 10 258.17 16.40
-22 -2 10 242.78 15.90
-22 -2 10 211.08 16.20
22 -2 -10 257.17 17.10
-22 -2 10 233.48 16.20
22 -2 -10 255.07 16.50
22 -2 -10 244.08 16.60
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-20 2 8 419.76 27.90
20 2 -8 422.46 26.80
20 2 -8 392.76 27.00
20 2 -8 443.36 27.00
-20 2 8 432.16 27.20
-20 -2 8 412.16 27.00
-20 -2 8 443.56 27.60
20 -2 -8 501.05 27.90
20 -2 -8 430.36 28.20
20 -2 -8 404.96 27.60
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-20 -2 8 430.96 27.50
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18 2 -6 210.78 14.00
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-18 2 6 197.48 14.60
18 2 -6 214.88 13.70
-18 -2 6 215.78 14.40
-18 -2 6 217.48 14.30
18 -2 -6 202.48 14.90
-18 -2 6 227.58 15.40
18 -2 -6 250.97 14.60
-18 -2 6 193.78 14.20
18 -2 -6 189.98 14.30
-16 2 4 30.00 3.70
-16 2 4 26.10 3.00
16 2 -4 20.70 2.60
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16 2 -4 24.30 2.50
16 -2 -4 27.10 3.50
16 -2 -4 23.60 3.30
16 -2 -4 28.80 4.00
-16 -2 4 26.80 3.60
-16 -2 4 27.30 4.40
-16 -2 4 23.40 3.10
-16 -2 4 28.10 3.30
-14 2 2 631.94 38.20
-14 2 2 631.34 38.20
14 2 -2 621.04 37.90
14 2 -2 624.64 37.90
-14 2 2 616.44 38.80
-14 -2 2 684.13 38.50
-14 -2 2 608.64 38.80
-14 -2 2 555.14 38.30
14 -2 -2 633.44 38.60
-14 -2 2 649.34 39.50
14 -2 -2 558.14 39.20
14 -2 -2 559.14 38.90
-12 2 0 11.00 1.80
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-12 2 0 12.00 1.80
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12 -2 0 10.30 2.20
12 -2 0 8.80 2.50
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12 -2 0 11.90 2.20
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-10 2 -2 131.09 9.20
-10 2 -2 140.79 8.80
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-10 2 -2 129.19 8.70
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10 -2 2 113.99 9.70
-10 -2 -2 107.69 8.80
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-10 -2 -2 157.08 9.70
-10 -2 -2 125.49 10.00
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8 2 4 996.60 61.09
-8 2 -4 1000.70 61.19
-8 2 -4 1001.00 62.29
8 2 4 1004.00 61.19
-8 2 -4 994.20 61.79
8 -2 4 1108.49 61.79
8 -2 4 879.81 61.59
8 -2 4 1018.80 61.29
-8 -2 -4 855.61 62.29
-8 -2 -4 1127.49 61.69
8 -2 4 907.41 61.89
-8 -2 -4 839.62 61.49
-8 -2 -4 1156.88 62.39
8 -2 4 1008.10 62.29
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-6 2 -6 3.30 1.60
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6 -2 6 4.00 1.60
6 -2 6 6.20 1.90
-6 -2 -6 3.30 1.70
6 -2 6 5.40 2.50
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4 2 8 107.79 7.20
-4 2 -8 113.19 7.50
-4 2 -8 111.69 7.60
-4 2 -8 117.69 8.20
4 -2 8 108.69 7.80
4 -2 8 95.39 8.30
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4 -2 8 111.69 7.80
4 -2 8 124.99 8.60
4 -2 8 94.09 7.70
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-4 -2 -8 94.99 7.70
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-2 2 -10 137.99 9.60
2 2 10 143.79 9.50
-2 2 -10 141.19 9.60
2 2 10 142.19 9.60
2 2 10 144.19 9.50
2 -2 10 147.69 10.10
2 -2 10 149.09 10.10
-2 -2 -10 142.29 9.90
2 -2 10 127.39 9.70
2 -2 10 127.89 10.00
-2 -2 -10 152.18 9.60
-2 -2 -10 123.79 10.70
2 -2 10 152.38 10.80
0 2 -12 401.16 24.40
0 2 -12 410.66 24.50
0 2 12 384.66 25.80
0 2 12 397.66 24.40
0 2 -12 375.56 24.70
0 2 -12 391.06 25.20
0 2 12 418.46 24.50
0 2 12 390.16 24.30
0 -2 -12 403.06 24.50
0 -2 12 388.06 24.80
0 -2 -12 350.66 25.50
0 -2 12 407.56 25.50
0 -2 12 380.26 24.90
0 -2 -12 385.06 24.90
0 -2 12 332.07 24.30
0 -2 12 374.86 24.90
0 -2 -12 378.86 24.70
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2 2 -14 -0.10 2.00
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2 2 -14 -0.40 1.40
-2 2 14 -2.00 1.60
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2 2 -14 1.80 1.30
2 2 -14 -0.70 1.40
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2 -2 -14 -0.10 2.50
2 -2 -14 -0.70 1.90
-2 -2 14 0.20 2.00
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-2 -2 14 -0.60 2.60
2 -2 -14 2.50 1.80
2 -2 -14 1.60 1.50
-4 2 16 131.79 9.90
4 2 -16 149.39 9.40
-4 2 16 143.09 10.10
4 2 -16 147.49 10.70
-4 2 16 134.49 9.80
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4 2 -16 131.49 9.80
-4 -2 16 134.09 10.50
4 -2 -16 156.68 10.60
4 -2 -16 148.49 11.40
-4 -2 16 157.98 11.30
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4 -2 -16 138.19 10.10
-4 -2 16 123.69 10.60
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-6 2 18 823.42 49.70
-6 2 18 805.92 49.99
6 2 -18 792.22 49.10
6 2 -18 787.42 50.39
6 2 -18 839.72 49.80
6 2 -18 788.12 49.60
6 -2 -18 802.02 50.29
6 -2 -18 784.62 50.99
-6 -2 18 795.82 50.29
-6 -2 18 812.52 50.59
6 -2 -18 698.53 49.90
-6 -2 18 809.32 50.79
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8 2 -20 134.19 10.70
-8 2 20 129.49 9.70
-8 2 20 133.49 9.90
8 2 -20 144.49 9.90
8 -2 -20 153.28 10.40
-8 -2 20 136.19 10.70
-8 -2 20 134.59 11.20
8 -2 -20 128.39 11.40
8 -2 -20 129.39 10.50
8 -2 -20 127.69 11.00
10 2 -22 178.68 12.70
10 2 -22 181.48 12.90
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10 -2 -22 192.58 14.20
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10 -2 -22 186.08 14.40
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12 -2 -24 50.89 6.10
-12 -2 24 49.30 6.70
12 -2 -24 46.00 6.80
-12 -2 24 48.10 6.20
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14 -2 -26 41.40 5.90
14 -2 -26 40.20 6.50
-14 -2 26 37.60 6.10
-14 -2 26 31.60 5.20
14 -2 -26 34.10 5.30
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16 -2 -28 20.40 4.80
-16 -2 28 10.90 4.60
16 -2 -28 4.70 3.70
-16 -2 28 7.90 3.70
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18 2 -30 10.70 3.20
18 -2 -30 12.20 4.00
-18 -2 30 11.60 4.20
18 -2 -30 14.00 5.00
18 -2 -30 16.60 4.50
-18 -2 30 14.60 5.20
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20 -2 -32 4.50 3.90
20 -2 -32 0.90 3.50
20 -2 -32 4.10 5.00
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35 -3 -23 3.50 4.20
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35 -3 -23 5.90 6.50
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-33 -3 21 -2.10 3.10
33 -3 -21 -1.80 3.20
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31 -3 -19 2.40 3.20
-31 -3 19 6.10 3.40
31 -3 -19 7.80 4.10
-31 -3 19 6.50 2.50
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29 3 -17 2.30 2.30
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29 -3 -17 12.00 3.70
29 -3 -17 10.10 4.00
-29 -3 17 9.00 3.20
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27 3 -15 1.70 2.00
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27 -3 -15 1.90 3.40
-27 -3 15 0.30 2.70
-27 -3 15 -0.90 1.90
-27 -3 15 2.40 2.90
27 -3 -15 6.40 3.10
-25 3 13 8.90 2.10
-25 3 13 9.10 2.10
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-25 -3 13 8.40 2.60
25 -3 -13 9.00 3.00
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-23 -3 11 62.69 6.40
-23 -3 11 67.29 5.90
-23 -3 11 58.99 5.80
-23 -3 11 55.89 6.10
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21 -3 -9 595.54 40.70
-21 -3 9 656.63 39.70
-21 -3 9 633.44 39.80
-21 -3 9 658.53 39.70
-21 -3 9 619.54 39.10
21 -3 -9 674.83 40.10
-21 -3 9 626.74 41.10
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19 3 -7 124.99 9.20
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19 -3 -7 162.88 10.60
-19 -3 7 129.29 10.00
19 -3 -7 159.08 10.70
19 -3 -7 122.39 11.30
-19 -3 7 131.19 10.40
-19 -3 7 141.29 9.50
-19 -3 7 158.38 10.50
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-17 -3 5 91.39 7.50
17 -3 -5 93.89 8.00
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15 -3 -3 68.49 6.20
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13 -3 -1 299.97 19.40
-13 -3 1 277.87 19.80
13 -3 -1 297.77 20.20
13 -3 -1 286.27 19.30
-13 -3 1 273.87 20.60
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9 -3 3 44.30 5.60
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-7 -3 -5 13.00 2.30
-7 -3 -5 16.90 2.60
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7 -3 5 19.30 2.60
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3 -3 9 0.00 2.90
3 -3 9 2.90 1.80
3 -3 9 -0.30 2.00
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1 -3 11 75.69 7.30
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1 -3 11 62.29 5.60
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1 -3 -13 74.19 6.30
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-1 -3 13 79.49 6.90
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1 -3 -13 84.09 6.80
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3 -3 -15 26.50 3.90
3 -3 -15 23.10 3.80
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-3 -3 15 20.80 4.80
-3 -3 15 24.60 4.10
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3 -3 -15 37.10 5.80
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5 -3 -17 24.40 4.00
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7 -3 -19 7.50 3.50
7 -3 -19 3.20 3.60
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9 -3 -21 33.10 5.90
9 -3 -21 46.20 7.20
9 -3 -21 35.10 5.00
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11 3 -23 43.80 4.30
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11 -3 -23 53.89 6.30
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15 -3 -27 33.50 6.00
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-20 -4 8 73.99 6.50
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11 -1 -24 402.06 31.30
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1 -1 -15 15.50 2.90
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1 -1 -15 15.90 2.60
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13 -1 3 32.30 4.10
13 -1 3 43.60 4.20
-13 -1 -3 34.10 3.90
-13 -1 -3 41.20 4.10
-11 1 -5 -0.80 1.40
-11 1 -5 -2.70 1.30
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11 1 5 -0.40 1.70
-11 1 -5 0.90 1.60
11 -1 5 -0.40 1.70
-11 -1 -5 -1.80 1.40
11 -1 5 -2.40 1.40
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-11 -1 -5 -0.20 2.00
11 -1 5 0.40 1.70
11 -1 5 -0.80 1.60
11 -1 5 -1.30 1.80
-11 -1 -5 -3.00 1.60
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9 1 7 497.45 30.80
9 1 7 501.65 31.30
-9 1 -7 517.05 31.40
-9 1 -7 482.25 31.50
9 1 7 483.65 31.20
-9 1 -7 508.25 31.40
-9 1 -7 500.85 31.30
9 -1 7 532.45 31.60
9 -1 7 525.85 31.70
9 -1 7 496.15 31.50
9 -1 7 409.66 31.40
9 -1 7 414.96 31.50
-9 -1 -7 545.95 31.60
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-9 -1 -7 497.05 32.00
-7 1 -9 248.68 15.90
7 1 9 236.58 15.40
-7 1 -9 237.78 16.00
-7 1 -9 235.48 16.10
7 1 9 243.68 15.80
7 1 9 242.78 16.50
-7 1 -9 249.18 16.00
-7 1 -9 234.68 16.00
7 1 9 246.98 15.90
7 -1 9 259.37 16.20
7 -1 9 226.88 16.00
7 -1 9 253.37 16.30
-7 -1 -9 241.08 16.60
-7 -1 -9 266.67 16.20
-7 -1 -9 236.68 15.50
-7 -1 -9 207.48 15.90
-7 -1 -9 267.47 16.50
7 -1 9 213.08 16.10
5 1 11 217.08 13.80
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-5 1 -11 217.88 14.30
-5 1 -11 225.78 14.50
5 1 11 220.18 14.10
-5 1 -11 214.38 14.20
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5 1 11 211.18 14.20
5 -1 11 208.28 14.50
-5 -1 -11 228.38 15.10
-5 -1 -11 206.28 13.90
5 -1 11 230.28 14.70
5 -1 11 191.08 14.30
-5 -1 -11 181.68 14.20
-5 -1 -11 205.88 15.00
-3 1 -13 21.90 3.60
-3 1 -13 22.80 3.00
3 1 13 18.40 2.70
3 1 13 17.40 2.90
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3 1 13 19.50 3.00
-3 1 -13 13.90 2.70
3 1 13 20.40 3.40
-3 -1 -13 24.00 3.70
-3 -1 -13 18.80 3.20
3 -1 13 15.30 2.90
-3 -1 -13 25.90 4.30
-3 -1 -13 23.50 3.00
-3 -1 -13 18.80 2.90
3 -1 13 19.40 3.00
3 -1 13 17.40 3.20
3 -1 13 20.50 3.60
-1 1 -15 160.48 11.50
1 1 15 160.58 12.00
1 1 15 167.38 11.50
-1 1 -15 163.18 11.40
-1 1 -15 173.78 12.10
-1 1 -15 152.98 11.20
1 1 15 172.98 12.00
-1 1 -15 157.98 11.70
-1 -1 -15 186.38 11.80
-1 -1 -15 153.58 11.30
-1 -1 -15 147.49 12.10
-1 -1 -15 149.88 11.60
1 -1 15 156.18 11.70
-1 -1 -15 159.88 11.80
1 -1 15 173.88 11.70
1 -1 15 165.18 11.90
-1 1 17 304.87 19.80
1 1 -17 300.87 19.50
1 1 -17 306.17 19.90
-1 1 17 308.17 19.80
-1 1 17 298.47 19.70
1 1 -17 295.77 20.30
1 1 -17 299.97 20.20
1 1 -17 296.87 19.70
1 -1 -17 313.17 20.80
-1 -1 17 286.57 20.30
1 -1 -17 271.57 19.60
1 -1 -17 301.97 20.20
-1 -1 17 283.87 20.10
-1 -1 17 321.17 20.40
3 1 -19 8.60 2.80
3 1 -19 7.90 2.20
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3 1 -19 2.70 2.80
-3 1 19 8.50 2.90
3 -1 -19 4.80 2.70
3 -1 -19 5.70 3.30
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3 -1 -19 4.00 2.40
-3 -1 19 4.80 3.10
5 1 -21 41.00 5.50
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5 1 -21 32.10 3.80
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5 1 -21 34.20 4.60
-5 -1 21 25.90 4.30
5 -1 -21 30.60 4.60
5 -1 -21 40.80 5.90
-5 -1 21 35.60 5.40
5 -1 -21 41.20 4.70
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7 1 -23 66.99 5.70
7 1 -23 83.09 7.90
7 1 -23 62.99 6.50
-7 1 23 60.49 6.40
-7 -1 23 79.59 10.00
7 -1 -23 54.49 7.00
7 -1 -23 47.20 6.60
-7 -1 23 54.69 7.10
9 1 -25 13.20 2.60
-9 1 25 10.10 3.30
-9 1 25 19.20 4.10
9 1 -25 15.20 3.20
9 1 -25 15.30 3.70
-9 -1 25 11.60 3.40
9 -1 -25 12.30 3.50
9 -1 -25 17.20 4.20
-9 -1 25 14.70 4.00
-11 1 27 3.90 3.40
11 1 -27 11.40 2.70
11 1 -27 7.00 3.40
11 1 -27 9.40 3.00
-11 1 27 2.80 2.80
-11 -1 27 5.10 3.20
11 -1 -27 9.90 3.50
-11 -1 27 3.90 3.40
11 -1 -27 6.90 4.00
11 -1 -27 10.10 3.30
13 1 -29 1.60 2.70
13 1 -29 0.60 2.30
-13 1 29 6.50 3.50
-13 1 29 5.40 3.00
13 1 -29 0.10 2.70
13 1 -29 1.60 2.70
-13 -1 29 1.30 3.30
13 -1 -29 -1.40 2.80
-13 -1 29 -1.90 3.00
13 -1 -29 7.80 3.50
13 -1 -29 3.90 3.40
15 1 -31 29.10 4.90
15 1 -31 22.10 4.60
-15 1 31 22.50 4.50
15 1 -31 25.60 3.80
-15 1 31 30.20 5.70
-15 -1 31 23.90 5.50
15 -1 -31 30.40 5.30
-15 -1 31 25.80 5.50
15 -1 -31 31.80 6.20
17 1 -33 8.10 4.30
17 1 -33 12.10 3.80
17 1 -33 9.90 3.20
-17 1 33 10.20 3.60
-17 1 33 8.20 4.20
17 -1 -33 23.50 5.90
-17 -1 33 14.90 5.10
17 -1 -33 8.00 4.10
17 -1 -33 10.00 4.10
-17 -1 33 13.70 4.60
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40 2 -24 2.60 3.20
40 2 -24 -2.70 2.50
-40 -2 24 -3.70 3.80
40 -2 -24 3.10 3.80
40 -2 -24 6.00 3.60
38 2 -22 3.40 3.00
38 2 -22 -0.10 2.60
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-38 -2 22 -3.60 3.60
38 -2 -22 -2.30 3.70
38 -2 -22 2.50 4.40
-36 2 20 22.70 4.30
36 2 -20 23.00 4.20
-36 2 20 26.80 4.10
36 -2 -20 18.20 4.50
-36 -2 20 20.50 4.80
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34 2 -18 26.50 3.90
34 2 -18 27.10 4.30
34 -2 -18 26.60 5.20
34 -2 -18 28.40 4.90
-34 -2 18 25.70 4.70
32 2 -16 56.79 5.50
32 2 -16 54.69 5.40
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32 2 -16 56.69 6.00
32 -2 -16 49.10 6.90
32 -2 -16 53.09 6.70
-30 2 14 230.58 15.70
-30 2 14 217.18 14.80
30 2 -14 229.48 15.70
30 2 -14 215.38 15.00
30 2 -14 212.98 15.00
-30 2 14 213.98 14.80
30 2 -14 233.48 15.20
30 -2 -14 228.48 16.20
-30 -2 14 234.98 16.00
30 -2 -14 223.88 16.70
-28 2 12 163.98 11.40
28 2 -12 178.48 11.80
28 2 -12 158.08 11.60
-28 2 12 170.08 11.40
-28 2 12 179.38 12.20
28 2 -12 169.98 12.30
-28 -2 12 160.18 12.70
28 -2 -12 157.28 13.90
-28 -2 12 188.18 12.80
28 -2 -12 158.88 13.00
26 2 -10 72.09 6.60
-26 2 10 70.49 6.20
26 2 -10 65.39 5.50
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-26 2 10 66.19 5.20
-26 2 10 59.49 5.10
26 2 -10 63.09 5.40
26 2 -10 68.69 5.80
-26 -2 10 71.69 6.90
26 -2 -10 74.89 6.90
-26 -2 10 69.39 6.80
-26 -2 10 77.29 8.10
26 -2 -10 65.59 7.30
24 2 -8 815.22 49.70
-24 2 8 806.42 49.99
24 2 -8 786.02 49.60
-24 2 8 836.32 50.09
24 2 -8 767.32 50.19
-24 -2 8 816.32 50.59
24 -2 -8 732.83 50.39
24 -2 -8 778.02 50.99
-24 -2 8 813.82 50.39
-24 -2 8 837.02 51.49
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22 2 -6 170.88 10.90
22 2 -6 168.68 11.30
-22 2 6 157.78 12.20
-22 -2 6 158.88 12.20
22 -2 -6 163.68 12.90
-22 -2 6 160.28 13.40
22 -2 -6 167.98 12.40
-22 -2 6 170.78 12.40
-22 -2 6 185.98 12.40
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20 2 -4 326.87 21.40
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20 -2 -4 319.27 22.20
20 -2 -4 395.66 22.50
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-20 -2 4 366.06 22.20
-20 -2 4 331.97 23.10
20 -2 -4 310.47 22.60
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-18 2 2 655.33 40.60
-18 2 2 656.83 40.60
18 2 -2 642.44 40.30
18 2 -2 675.23 40.40
-18 -2 2 736.03 41.70
18 -2 -2 576.44 40.90
-18 -2 2 656.33 41.00
-18 -2 2 680.93 42.00
18 -2 -2 562.64 41.30
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16 2 0 210.08 14.50
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-16 2 0 212.68 14.70
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16 -2 0 225.68 15.60
-16 -2 0 244.78 15.80
16 -2 0 255.57 15.50
-16 -2 0 227.08 15.10
16 -2 0 210.78 15.60
-16 -2 0 217.38 15.10
16 -2 0 213.18 15.20
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-14 2 -2 78.19 7.20
14 2 2 73.49 5.70
-14 2 -2 85.39 6.10
-14 2 -2 82.19 6.10
14 -2 2 75.29 7.00
-14 -2 -2 79.39 7.50
-14 -2 -2 68.19 6.30
-14 -2 -2 79.29 6.30
-14 -2 -2 83.69 7.00
14 -2 2 64.89 6.30
14 -2 2 71.59 6.80
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-12 2 -4 104.49 7.70
-12 2 -4 101.29 6.80
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12 -2 4 90.99 7.90
12 -2 4 95.19 8.30
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12 -2 4 97.39 6.90
12 -2 4 121.39 8.70
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10 2 6 32.30 4.50
-10 2 -6 32.40 4.70
-10 2 -6 31.60 4.00
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-10 -2 -6 39.30 4.40
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10 -2 6 38.40 6.00
-10 -2 -6 31.50 3.70
-10 -2 -6 25.90 3.60
-10 -2 -6 33.20 4.90
10 -2 6 35.40 4.50
-8 2 -8 368.16 22.80
-8 2 -8 353.06 22.70
8 2 8 353.46 22.50
-8 2 -8 367.66 22.80
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-8 2 -8 357.16 23.00
8 -2 8 337.27 22.80
-8 -2 -8 338.47 23.00
8 -2 8 329.07 23.10
-8 -2 -8 408.76 24.00
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-8 -2 -8 366.86 24.10
8 -2 8 324.27 23.10
8 -2 8 370.46 23.70
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-6 2 -10 18.20 2.70
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6 -2 10 18.60 3.70
-6 -2 -10 20.60 4.40
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4 2 12 1706.53 104.79
-4 2 -12 1673.13 104.99
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2 2 14 457.75 28.70
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2 -2 14 415.96 29.20
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2 -2 14 433.36 29.40
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2 -2 14 485.45 29.50
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2 -2 14 462.15 30.00
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0 2 -16 165.28 12.40
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0 2 -16 183.68 12.70
0 2 -16 175.78 12.10
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2 2 -18 72.09 6.00
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2 2 -18 69.49 6.50
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2 2 -18 67.79 5.50
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2 -2 -18 65.99 5.90
2 -2 -18 52.69 7.20
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2 -2 -18 66.79 6.90
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4 2 -20 214.88 15.10
4 2 -20 210.08 15.80
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4 -2 -20 258.37 15.70
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4 -2 -20 227.58 15.90
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10 -2 -26 8.10 4.20
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31 -3 -15 4.20 3.20
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-1 1 -16 245.98 16.90
1 1 16 249.08 17.00
-1 1 -16 271.27 17.60
-1 1 -16 256.07 17.30
-1 1 -16 239.18 16.70
-1 1 -16 268.97 17.10
1 1 16 266.17 17.00
1 -1 16 231.48 17.30
-1 -1 -16 279.77 17.70
-1 -1 -16 239.08 17.20
-1 -1 -16 229.78 16.70
-1 -1 -16 251.27 17.90
1 -1 16 273.17 17.60
1 -1 16 236.48 17.30
1 1 -18 373.76 23.70
1 1 -18 339.17 23.20
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1 1 -18 355.46 24.00
-1 1 18 363.66 23.60
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1 -1 -18 360.36 23.90
1 -1 -18 382.96 24.70
-1 -1 18 337.97 23.80
1 -1 -18 311.67 23.30
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3 -1 -20 258.07 19.00
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34 -2 -17 6.50 3.10
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26 -2 -9 70.59 7.90
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22 -2 -5 464.75 30.70
-22 -2 5 500.55 30.70
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22 -2 -5 451.85 31.10
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18 -2 -1 323.17 19.10
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-18 -2 -14 5.10 4.00
16 2 16 4.20 3.00
-16 2 -16 5.30 2.90
-16 2 -16 4.90 3.40
16 -2 16 5.40 4.10
-16 -2 -16 9.60 4.90
16 -2 16 3.60 4.50
-16 -2 -16 1.00 3.50
36 0 -3 -0.90 3.10
-36 0 3 -1.30 3.60
-36 0 3 -2.90 3.10
36 0 -3 0.90 4.00
36 0 -3 3.00 3.60
34 0 -1 5.40 3.40
-34 0 1 -5.00 3.40
-34 0 1 0.80 3.10
34 0 -1 4.80 4.20
32 0 1 -1.70 3.90
-32 0 -1 0.60 3.40
-32 0 -1 0.40 3.40
32 0 1 -1.20 3.00
32 0 1 -0.20 3.10
30 0 3 -4.80 2.70
-30 0 -3 3.50 3.60
30 0 3 0.00 3.30
28 0 5 4.40 3.80
28 0 5 3.40 3.40
-28 0 -5 -0.70 2.70
-28 0 -5 -1.00 3.20
28 0 5 3.00 2.80
-26 0 -7 2.20 3.10
26 0 7 -1.80 3.20
-26 0 -7 4.70 3.90
26 0 7 -1.20 2.40
24 0 9 0.10 2.50
-24 0 -9 -3.90 2.80
24 0 9 -3.90 2.80
-24 0 -9 2.90 3.30
-22 0 -11 -1.80 3.10
-22 0 -11 -0.90 3.40
22 0 11 1.00 2.80
22 0 11 -1.10 3.00
-20 0 -13 -1.20 3.40
20 0 13 1.10 2.80
-20 0 -13 -3.20 3.30
20 0 13 4.00 3.40
18 0 15 2.80 3.60
18 0 15 -2.10 3.40
-18 0 -15 4.70 4.20
-16 0 -17 3.50 3.60
16 0 17 2.80 3.10
-16 0 -17 1.70 4.00
14 0 19 1.90 3.60
-14 0 -19 2.90 3.50
14 0 19 4.40 3.30
-14 0 -19 6.50 4.40
-35 1 2 28.90 5.20
-35 -1 2 16.10 5.60
35 -1 -2 34.10 6.80
35 -1 -2 38.20 6.10
-33 1 0 13.50 4.10
33 1 0 7.30 3.60
-33 -1 0 12.00 4.00
33 -1 0 6.60 3.90
33 -1 0 13.20 4.80
33 -1 0 4.50 3.90
-33 -1 0 6.40 4.20
-31 1 -2 2.00 3.40
31 1 2 5.40 3.30
-31 1 -2 3.30 3.50
-31 -1 -2 0.10 3.90
31 -1 2 1.30 3.30
31 -1 2 3.90 4.50
-31 -1 -2 5.50 3.50
31 -1 2 2.50 3.50
29 1 4 5.90 3.30
-29 1 -4 7.20 3.50
-29 1 -4 1.80 2.80
29 -1 4 6.90 4.10
-29 -1 -4 3.40 4.10
-29 -1 -4 3.40 4.20
29 -1 4 2.90 3.60
-27 1 -6 20.60 4.30
27 1 6 15.50 4.10
27 -1 6 29.40 5.40
27 -1 6 40.90 7.30
-27 -1 -6 22.70 5.70
-25 1 -8 3.20 3.60
-25 1 -8 11.10 3.40
25 1 8 7.70 3.40
-25 -1 -8 8.80 4.80
25 -1 8 6.00 3.70
25 -1 8 2.70 4.20
-23 1 -10 6.20 3.10
-23 1 -10 2.60 3.40
23 1 10 5.00 3.30
23 1 10 -0.30 2.10
23 -1 10 4.20 3.70
-23 -1 -10 4.10 4.10
21 1 12 4.80 3.20
-21 1 -12 9.90 3.90
-21 1 -12 8.80 3.20
21 1 12 2.00 2.20
21 -1 12 -0.50 3.70
-21 -1 -12 6.50 4.60
-21 -1 -12 4.30 4.50
-19 1 -14 35.90 5.80
19 1 14 33.00 4.30
-19 1 -14 39.20 5.50
19 1 14 30.50 5.20
19 -1 14 27.40 5.40
-19 -1 -14 30.20 5.60
19 -1 14 32.10 5.80
-19 -1 -14 39.10 6.80
17 1 16 19.70 3.70
17 1 16 23.60 4.70
-17 1 -16 14.50 4.40
-17 1 -16 12.30 4.30
-17 -1 -16 15.30 4.30
17 -1 16 15.90 4.90
-17 -1 -16 22.30 6.50
17 -1 16 20.20 4.90
-15 1 -18 -5.40 3.20
15 1 18 0.20 2.70
-15 1 -18 4.60 3.70
15 1 18 2.90 3.40
-15 -1 -18 -1.30 4.50
-15 -1 -18 3.00 3.70
15 -1 18 -2.80 2.90
15 -1 18 3.10 3.90
-28 2 -5 5.60 3.20
-28 2 -5 7.70 3.40
28 2 5 5.10 3.00
28 -2 5 7.10 5.00
28 -2 5 12.20 4.60
-28 -2 -5 11.80 4.10
-28 -2 -5 2.70 5.00
28 -2 5 6.30 4.20
26 2 7 3.80 2.90
-26 2 -7 0.20 3.10
-26 2 -7 3.90 3.00
26 -2 7 1.80 4.20
26 -2 7 5.30 3.80
-26 -2 -7 -0.90 4.40
-26 -2 -7 5.60 3.70
-24 2 -9 29.90 4.90
24 2 9 42.90 5.50
-24 2 -9 26.70 4.90
24 -2 9 33.60 5.50
-24 -2 -9 38.70 7.40
-24 -2 -9 35.80 5.90
24 -2 9 45.60 7.30
22 2 11 24.20 4.10
-22 2 -11 19.40 4.20
-22 2 -11 28.40 4.80
-22 -2 -11 23.70 6.40
22 -2 11 28.20 6.10
-22 -2 -11 27.20 5.40
22 -2 11 27.30 6.10
22 -2 11 30.20 5.20
-20 -2 -13 35.50 7.60
34 0 0 26.30 4.90
34 0 0 30.80 4.90
-34 0 0 22.80 5.40
-34 0 0 19.20 4.70
-32 0 -2 29.20 5.90
32 0 2 36.90 5.10
32 0 2 32.70 5.60
32 0 2 29.80 6.40
-32 0 -2 33.40 5.70
-30 0 -4 -1.40 3.00
30 0 4 1.60 3.00
-30 0 -4 -0.70 3.60
30 0 4 4.10 3.90
28 0 6 1.20 3.10
-28 0 -6 3.00 3.90
-28 0 -6 4.20 3.80
-26 0 -8 0.60 3.80
26 0 8 -3.60 3.80
-26 0 -8 -0.70 3.40
26 0 8 4.30 3.10
24 0 10 7.60 3.30
-24 0 -10 3.10 3.90
-24 0 -10 8.80 3.90
24 0 10 2.40 4.80
22 0 12 20.90 4.00
-22 0 -12 15.10 4.50
-22 0 -12 27.10 5.30
-20 0 -14 38.20 6.70
-20 0 -14 36.30 6.00
-18 0 -16 111.49 11.20
-18 0 -16 115.69 10.80
18 0 16 109.89 9.80
18 0 16 125.09 10.90
31 1 3 4.50 3.40
-31 1 -3 5.70 3.20
-31 1 -3 9.20 3.90
31 -1 3 5.80 4.00
-31 -1 -3 13.00 4.10
-31 -1 -3 3.70 4.50
31 -1 3 9.90 4.90
31 -1 3 12.10 4.00
29 1 5 46.40 6.00
-29 1 -5 40.80 6.10
-29 1 -5 42.90 6.90
-29 -1 -5 41.20 7.40
29 -1 5 58.79 8.40
29 -1 5 47.30 6.80
-29 -1 -5 43.00 6.10
29 -1 5 54.39 6.90
-27 1 -7 12.70 3.70
27 1 7 6.00 3.40
-27 -1 -7 8.30 3.30
27 -1 7 15.50 5.30
-27 -1 -7 5.50 4.70
27 -1 7 11.80 4.30
27 -1 7 9.60 4.30
25 1 9 2.20 3.10
-25 1 -9 5.00 3.70
25 1 9 4.10 3.00
-25 -1 -9 0.50 4.10
25 -1 9 15.90 8.00
25 -1 9 7.50 4.00
25 -1 9 13.30 4.20
-25 -1 -9 0.80 3.10
23 1 11 3.80 3.10
-23 1 -11 2.90 3.50
23 1 11 2.80 2.30
-23 -1 -11 9.50 3.90
23 -1 11 6.00 3.80
-23 -1 -11 7.90 4.60
23 -1 11 1.60 3.70
-21 1 -13 4.70 5.20
-21 1 -13 6.80 3.80
21 1 13 12.00 4.00
21 1 13 9.10 2.60
-21 -1 -13 8.30 3.90
21 -1 13 6.50 4.10
-21 -1 -13 4.30 5.30
21 -1 13 7.30 4.00
19 1 15 0.40 2.70
-19 1 -15 2.10 3.40
-19 1 -15 5.80 3.60
19 1 15 4.20 3.20
19 -1 15 -0.60 3.50
-19 -1 -15 -0.30 3.20
19 -1 15 2.90 3.60
-28 0 -7 5.10 3.80
-28 0 -7 1.70 3.30
28 0 7 0.00 3.30
28 0 7 -1.10 3.00
-26 0 -9 1.80 3.60
-26 0 -9 0.80 3.20
26 0 9 -5.60 3.10
26 0 9 -0.30 2.90
-24 0 -11 -3.40 3.30
24 0 11 7.30 3.20
-24 0 -11 -4.80 3.10
24 0 11 -0.70 3.30
0 0 0 0.00 0.00
_computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)'
;
_shelx_hkl_checksum 98637
_shelx_res_file
;
TITL SYPD_a.res in C2/c
shelx.res
created by SHELXL-2019/3 at 11:23:50 on 09-Mar-2025
CELL 0.71073 32.1977 4.6431 26.4005 90.000 127.495 90.000
ZERR 8.00 0.0019 0.0003 0.0024 0.000 0.002 0.000
LATT 7
SYMM - X, Y, 1/2 - Z
SFAC C H N O CL
UNIT 104 120 32 32 8
MERG 2
EQIV $1 -x+1/2, -y+1/2, -z+1
HTAB C5 N1_$1
EQIV $2 -x+1/2, y+1/2, -z+3/2
HTAB C12 N4_$2
HTAB O2 O4
HTAB N3 N2_$1
EQIV $3 -x+1, -y+1, -z+2
HTAB O4 O1_$3
HTAB O4 O2_$3
EQIV $4 x, y+1, z
HTAB O4 O2_$4
FMAP 2
PLAN 20
SIZE 0.103 0.254 0.445
ACTA
BOND $H
CONF
L.S. 4
TEMP 25.00
WGHT 0.056400 2.070100
FVAR 0.54853
C1 1 0.129781 0.845606 0.419791 11.00000 0.04651 0.06095 =
0.05451 0.00890 0.03005 -0.00767
C2 1 0.144223 0.925624 0.479555 11.00000 0.06558 0.05747 =
0.07208 0.00189 0.04780 -0.00189
AFIX 43
H2 2 0.125598 1.064179 0.483681 11.00000 -1.20000
AFIX 0
C3 1 0.186870 0.791698 0.531686 11.00000 0.06974 0.05785 =
0.05317 -0.00577 0.04252 -0.01068
AFIX 43
H3 2 0.198656 0.837253 0.572787 11.00000 -1.20000
AFIX 0
C4 1 0.212232 0.583098 0.520994 11.00000 0.04777 0.05232 =
0.03861 -0.00298 0.02786 -0.01269
C5 1 0.317926 0.320411 0.668962 11.00000 0.04853 0.06098 =
0.03612 -0.00875 0.02768 -0.01065
AFIX 43
H5 2 0.328952 0.194971 0.651841 11.00000 -1.20000
AFIX 0
C6 1 0.347380 0.330535 0.738330 11.00000 0.04091 0.05148 =
0.03470 -0.00676 0.02303 -0.01045
C7 1 0.390762 0.149767 0.775206 11.00000 0.04435 0.05450 =
0.04362 -0.01331 0.02775 -0.00557
AFIX 43
H7 2 0.400366 0.030334 0.755628 11.00000 -1.20000
AFIX 0
C8 1 0.419508 0.148624 0.841090 11.00000 0.03599 0.04627 =
0.04313 -0.00601 0.01940 0.00067
C9 1 0.405162 0.325207 0.870544 11.00000 0.03714 0.04546 =
0.03112 -0.00400 0.01577 -0.00068
C10 1 0.361269 0.503281 0.833307 11.00000 0.03559 0.04610 =
0.03306 -0.00537 0.01870 -0.00104
C11 1 0.332697 0.508530 0.767414 11.00000 0.03501 0.04919 =
0.03199 -0.00078 0.01677 -0.00061
AFIX 43
H11 2 0.303949 0.630052 0.742856 11.00000 -1.20000
AFIX 0
C12 1 0.304070 0.828147 0.833034 11.00000 0.04672 0.07362 =
0.05806 -0.00809 0.02881 0.01315
AFIX 33
H12A 2 0.301109 0.929493 0.862401 11.00000 -1.50000
H12B 2 0.305110 0.964118 0.806431 11.00000 -1.50000
H12C 2 0.274442 0.703171 0.806886 11.00000 -1.50000
AFIX 0
C13 1 0.484344 -0.177219 0.857382 11.00000 0.06180 0.06815 =
0.08763 -0.01021 0.04442 0.01533
AFIX 33
H13A 2 0.514242 -0.283563 0.891218 11.00000 -1.50000
H13B 2 0.458548 -0.308440 0.825325 11.00000 -1.50000
H13C 2 0.494847 -0.047217 0.838793 11.00000 -1.50000
AFIX 0
N1 3 0.153690 0.650259 0.410764 11.00000 0.04754 0.06871 =
0.04040 0.00363 0.02370 -0.00698
N2 3 0.195376 0.513444 0.461883 11.00000 0.05038 0.06451 =
0.03572 -0.00075 0.02510 -0.00448
N3 3 0.254583 0.430416 0.567432 11.00000 0.05358 0.06676 =
0.03298 -0.00521 0.02569 -0.00295
N4 3 0.277668 0.477021 0.630978 11.00000 0.04993 0.06027 =
0.03228 -0.00629 0.02581 -0.01278
O1 4 0.462767 -0.018298 0.882220 11.00000 0.04986 0.06847 =
0.05181 -0.00891 0.01930 0.01911
O2 4 0.434090 0.312908 0.935499 11.00000 0.05401 0.05693 =
0.03171 -0.00269 0.01481 0.01281
O3 4 0.350561 0.662597 0.867493 11.00000 0.04729 0.07307 =
0.03446 -0.00528 0.01967 0.01692
O4 4 0.443341 0.781072 1.000287 11.00000 0.05816 0.06416 =
0.03789 -0.00418 0.01612 -0.00479
CL1 5 0.077355 1.014266 0.351244 11.00000 0.05718 0.09521 =
0.07704 0.03003 0.03369 0.00742
H2O 2 0.431228 0.471660 0.949513 11.00000 0.07209
H3N 2 0.268922 0.303605 0.558204 11.00000 0.05380
H4W 2 0.473780 0.790948 1.028331 11.00000 0.09998
H5W 2 0.436212 0.936577 0.979648 11.00000 0.08379
HKLF 4 1.0 1.00 0.00 0.00 0.00 1.00 0.00 0.00 0.00 1.00
REM SYPD_a.res in C2/c
REM wR2 = 0.1324, GooF = S = 1.068, Restrained GooF = 1.068 for all data
REM R1 = 0.0492 for 3259 Fo > 4sig(Fo) and 0.0581 for all 3867 data
REM 215 parameters refined using 0 restraints
END
WGHT 0.0566 2.0697
REM Highest difference peak 0.320, deepest hole -0.270, 1-sigma level 0.041
Q1 1 0.0705 0.8293 0.3413 11.00000 0.05 0.32
Q2 1 0.4724 0.1243 0.8715 11.00000 0.05 0.24
Q3 1 0.0860 1.0772 0.3892 11.00000 0.05 0.24
Q4 1 0.2694 0.6207 0.6410 11.00000 0.05 0.23
Q5 1 0.4177 0.2956 0.8507 11.00000 0.05 0.23
Q6 1 0.3747 0.3464 0.8503 11.00000 0.05 0.22
Q7 1 0.1882 0.6344 0.5235 11.00000 0.05 0.21
Q8 1 0.3502 0.5271 0.8009 11.00000 0.05 0.21
Q9 1 0.3289 0.3167 0.7022 11.00000 0.05 0.21
Q10 1 0.2030 0.5658 0.4917 11.00000 0.05 0.21
Q11 1 0.3888 0.4633 0.8513 11.00000 0.05 0.20
Q12 1 0.3555 0.1730 0.7530 11.00000 0.05 0.20
Q13 1 0.4128 0.2151 0.8098 11.00000 0.05 0.19
Q14 1 0.3377 0.3976 0.7512 11.00000 0.05 0.19
Q15 1 0.1406 0.8777 0.4484 11.00000 0.05 0.19
Q16 1 0.3786 0.3201 0.7580 11.00000 0.05 0.17
Q17 1 0.2104 0.7416 0.5296 11.00000 0.05 0.16
Q18 1 0.1329 0.6925 0.4198 11.00000 0.05 0.16
Q19 1 0.4460 0.0960 0.8568 11.00000 0.05 0.15
Q20 1 0.2860 0.3170 0.6508 11.00000 0.05 0.14
;
_shelx_res_checksum 26671
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C C1 0.12978(7) 0.8456(4) 0.41979(9) 0.0544(4) Uani d 1 . .
C C2 0.14422(8) 0.9256(4) 0.47956(10) 0.0612(5) Uani d 1 . .
H H2 0.125598 1.064179 0.483681 0.073 Uiso calc 1 . .
C C3 0.18687(8) 0.7917(4) 0.53169(9) 0.0570(4) Uani d 1 . .
H H3 0.198656 0.837253 0.572787 0.068 Uiso calc 1 . .
C C4 0.21223(6) 0.5831(4) 0.52099(7) 0.0452(4) Uani d 1 . .
C C5 0.31793(6) 0.3204(4) 0.66896(7) 0.0473(4) Uani d 1 . .
H H5 0.328952 0.194971 0.651841 0.057 Uiso calc 1 . .
C C6 0.34738(6) 0.3305(4) 0.73833(7) 0.0424(3) Uani d 1 . .
C C7 0.39076(6) 0.1498(4) 0.77521(7) 0.0469(4) Uani d 1 . .
H H7 0.400366 0.030334 0.755628 0.056 Uiso calc 1 . .
C C8 0.41951(6) 0.1486(4) 0.84109(7) 0.0448(3) Uani d 1 . .
C C9 0.40516(5) 0.3252(3) 0.87054(6) 0.0411(3) Uani d 1 . .
C C10 0.36127(6) 0.5033(3) 0.83331(7) 0.0397(3) Uani d 1 . .
C C11 0.33270(6) 0.5085(3) 0.76741(7) 0.0411(3) Uani d 1 . .
H H11 0.303949 0.630052 0.742856 0.049 Uiso calc 1 . .
C C12 0.30407(7) 0.8281(5) 0.83303(9) 0.0615(5) Uani d 1 . .
H H12A 0.301109 0.929493 0.862401 0.092 Uiso calc 1 . .
H H12B 0.305110 0.964118 0.806431 0.092 Uiso calc 1 . .
H H12C 0.274442 0.703171 0.806886 0.092 Uiso calc 1 . .
C C13 0.48434(8) -0.1772(5) 0.85738(12) 0.0732(6) Uani d 1 . .
H H13A 0.514242 -0.283563 0.891218 0.110 Uiso calc 1 . .
H H13B 0.458548 -0.308440 0.825325 0.110 Uiso calc 1 . .
H H13C 0.494847 -0.047217 0.838793 0.110 Uiso calc 1 . .
N N1 0.15369(6) 0.6503(4) 0.41076(7) 0.0542(4) Uani d 1 . .
N N2 0.19538(6) 0.5134(3) 0.46188(6) 0.0509(3) Uani d 1 . .
N N3 0.25458(6) 0.4304(4) 0.56743(6) 0.0515(4) Uani d 1 . .
N N4 0.27767(5) 0.4770(3) 0.63098(6) 0.0470(3) Uani d 1 . .
O O1 0.46277(5) -0.0183(3) 0.88222(6) 0.0642(4) Uani d 1 . .
O O2 0.43409(5) 0.3129(3) 0.93550(5) 0.0548(3) Uani d 1 . .
O O3 0.35056(4) 0.6626(3) 0.86749(5) 0.0550(3) Uani d 1 . .
O O4 0.44334(6) 0.7811(3) 1.00029(6) 0.0619(4) Uani d 1 . .
Cl Cl1 0.07736(2) 1.01427(14) 0.35124(3) 0.0811(2) Uani d 1 . .
H H2O 0.4312(9) 0.472(5) 0.9495(11) 0.072(7) Uiso d 1 . .
H H3N 0.2689(8) 0.304(4) 0.5582(9) 0.054(5) Uiso d 1 . .
H H4W 0.4738(12) 0.791(6) 1.0283(15) 0.100(10) Uiso d 1 . .
H H5W 0.4362(10) 0.937(6) 0.9796(13) 0.084(8) Uiso d 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
C1 0.0465(8) 0.0610(10) 0.0545(9) -0.0077(8) 0.0300(8) 0.0089(8)
C2 0.0656(11) 0.0575(10) 0.0721(12) -0.0019(9) 0.0478(10) 0.0019(9)
C3 0.0697(11) 0.0578(10) 0.0532(9) -0.0107(9) 0.0425(9) -0.0058(8)
C4 0.0478(8) 0.0523(9) 0.0386(7) -0.0127(7) 0.0279(7) -0.0030(6)
C5 0.0485(8) 0.0610(10) 0.0361(7) -0.0106(7) 0.0277(7) -0.0088(7)
C6 0.0409(7) 0.0515(9) 0.0347(7) -0.0104(6) 0.0230(6) -0.0068(6)
C7 0.0444(8) 0.0545(9) 0.0436(8) -0.0056(7) 0.0278(7) -0.0133(7)
C8 0.0360(7) 0.0463(8) 0.0431(8) 0.0007(6) 0.0194(6) -0.0060(6)
C9 0.0371(7) 0.0455(8) 0.0311(7) -0.0007(6) 0.0158(6) -0.0040(6)
C10 0.0356(7) 0.0461(8) 0.0331(7) -0.0010(6) 0.0187(6) -0.0054(6)
C11 0.0350(7) 0.0492(8) 0.0320(7) -0.0006(6) 0.0168(6) -0.0008(6)
C12 0.0467(9) 0.0736(13) 0.0581(10) 0.0132(9) 0.0288(8) -0.0081(9)
C13 0.0618(11) 0.0681(13) 0.0876(15) 0.0153(10) 0.0444(11) -0.0102(11)
N1 0.0475(7) 0.0687(10) 0.0404(7) -0.0070(7) 0.0237(6) 0.0036(7)
N2 0.0504(7) 0.0645(9) 0.0357(6) -0.0045(6) 0.0251(6) -0.0007(6)
N3 0.0536(8) 0.0668(9) 0.0330(6) -0.0029(7) 0.0257(6) -0.0052(6)
N4 0.0499(7) 0.0603(8) 0.0323(6) -0.0128(6) 0.0258(6) -0.0063(6)
O1 0.0499(7) 0.0685(8) 0.0518(7) 0.0191(6) 0.0193(6) -0.0089(6)
O2 0.0540(7) 0.0569(7) 0.0317(5) 0.0128(6) 0.0148(5) -0.0027(5)
O3 0.0473(6) 0.0731(8) 0.0345(5) 0.0169(6) 0.0197(5) -0.0053(5)
O4 0.0582(8) 0.0642(9) 0.0379(6) -0.0048(7) 0.0161(6) -0.0042(6)
Cl1 0.0572(3) 0.0952(4) 0.0770(4) 0.0074(3) 0.0337(3) 0.0300(3)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
N1 C1 C2 . . 124.38(17) ?
N1 C1 Cl1 . . 115.54(14) ?
C2 C1 Cl1 . . 120.07(16) ?
C3 C2 C1 . . 117.16(18) ?
C3 C2 H2 . . 121.4 ?
C1 C2 H2 . . 121.4 ?
C2 C3 C4 . . 117.59(17) ?
C2 C3 H3 . . 121.2 ?
C4 C3 H3 . . 121.2 ?
N2 C4 N3 . . 113.48(16) ?
N2 C4 C3 . . 121.83(16) ?
N3 C4 C3 . . 124.68(15) ?
N4 C5 C6 . . 122.62(15) ?
N4 C5 H5 . . 118.7 ?
C6 C5 H5 . . 118.7 ?
C11 C6 C7 . . 120.26(13) ?
C11 C6 C5 . . 122.03(15) ?
C7 C6 C5 . . 117.69(14) ?
C8 C7 C6 . . 119.86(14) ?
C8 C7 H7 . . 120.1 ?
C6 C7 H7 . . 120.1 ?
O1 C8 C7 . . 125.21(14) ?
O1 C8 C9 . . 114.48(13) ?
C7 C8 C9 . . 120.32(14) ?
O2 C9 C8 . . 118.24(13) ?
O2 C9 C10 . . 122.15(13) ?
C8 C9 C10 . . 119.59(13) ?
O3 C10 C11 . . 125.35(13) ?
O3 C10 C9 . . 114.20(12) ?
C11 C10 C9 . . 120.45(13) ?
C10 C11 C6 . . 119.51(14) ?
C10 C11 H11 . . 120.2 ?
C6 C11 H11 . . 120.2 ?
O3 C12 H12A . . 109.5 ?
O3 C12 H12B . . 109.5 ?
H12A C12 H12B . . 109.5 ?
O3 C12 H12C . . 109.5 ?
H12A C12 H12C . . 109.5 ?
H12B C12 H12C . . 109.5 ?
O1 C13 H13A . . 109.5 ?
O1 C13 H13B . . 109.5 ?
H13A C13 H13B . . 109.5 ?
O1 C13 H13C . . 109.5 ?
H13A C13 H13C . . 109.5 ?
H13B C13 H13C . . 109.5 ?
C1 N1 N2 . . 118.93(15) ?
C4 N2 N1 . . 120.08(15) ?
C4 N3 N4 . . 121.38(15) y
C4 N3 H3N . . 121.0(13) ?
N4 N3 H3N . . 117.6(13) ?
C5 N4 N3 . . 113.84(14) y
C8 O1 C13 . . 118.39(15) ?
C9 O2 H2O . . 109.7(16) ?
C10 O3 C12 . . 117.64(12) ?
H4W O4 H5W . . 104(3) ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
C1 N1 . 1.302(2) ?
C1 C2 . 1.397(3) ?
C1 Cl1 . 1.7374(19) ?
C2 C3 . 1.366(3) ?
C2 H2 . 0.9300 ?
C3 C4 . 1.402(3) ?
C3 H3 . 0.9300 ?
C4 N2 . 1.343(2) ?
C4 N3 . 1.353(2) y
C5 N4 . 1.278(2) y
C5 C6 . 1.463(2) ?
C5 H5 . 0.9300 ?
C6 C11 . 1.392(2) ?
C6 C7 . 1.396(2) ?
C7 C8 . 1.386(2) ?
C7 H7 . 0.9300 ?
C8 O1 . 1.3706(19) ?
C8 C9 . 1.388(2) ?
C9 O2 . 1.3664(17) ?
C9 C10 . 1.399(2) ?
C10 O3 . 1.3636(18) ?
C10 C11 . 1.3874(19) ?
C11 H11 . 0.9300 ?
C12 O3 . 1.415(2) ?
C12 H12A . 0.9600 ?
C12 H12B . 0.9600 ?
C12 H12C . 0.9600 ?
C13 O1 . 1.418(2) ?
C13 H13A . 0.9600 ?
C13 H13B . 0.9600 ?
C13 H13C . 0.9600 ?
N1 N2 . 1.350(2) y
N3 N4 . 1.3769(17) y
N3 H3N . 0.87(2) ?
O2 H2O . 0.85(2) ?
O4 H4W . 0.79(3) ?
O4 H5W . 0.85(3) ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
C5 H5 N1 7_556 0.93 2.60 3.519(2) 171.9 yes
C12 H12A N4 4_556 0.96 2.66 3.369(2) 131.5 yes
O2 H2O O4 . 0.85(2) 1.84(2) 2.668(2) 164(2) yes
N3 H3N N2 7_556 0.87(2) 2.12(2) 2.993(2) 178.3(18) yes
O4 H4W O1 5_667 0.79(3) 2.23(3) 2.9254(19) 146(3) yes
O4 H4W O2 5_667 0.79(3) 2.55(3) 3.239(2) 147(3) yes
O4 H5W O2 1_565 0.85(3) 2.08(3) 2.914(2) 169(3) yes
C12 H12B Cg(C6--C11) 1_545 0.96 2.87 3.6710(10) 142 yes
C13 H13B Cg(C6--C11) 1_565 0.96 2.90 3.6660(10) 138 yes
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
N1 C1 C2 C3 . . . . 1.1(3) ?
Cl1 C1 C2 C3 . . . . -177.81(14) ?
C1 C2 C3 C4 . . . . -0.7(3) ?
C2 C3 C4 N2 . . . . -0.6(3) ?
C2 C3 C4 N3 . . . . -179.46(17) ?
N4 C5 C6 C11 . . . . 1.3(2) y
N4 C5 C6 C7 . . . . -179.98(15) ?
C11 C6 C7 C8 . . . . -0.3(2) ?
C5 C6 C7 C8 . . . . -179.12(15) ?
C6 C7 C8 O1 . . . . -179.85(15) ?
C6 C7 C8 C9 . . . . 0.4(2) ?
O1 C8 C9 O2 . . . . -1.0(2) ?
C7 C8 C9 O2 . . . . 178.82(15) ?
O1 C8 C9 C10 . . . . -179.37(15) ?
C7 C8 C9 C10 . . . . 0.4(2) ?
O2 C9 C10 O3 . . . . 0.5(2) ?
C8 C9 C10 O3 . . . . 178.88(15) ?
O2 C9 C10 C11 . . . . -179.61(14) ?
C8 C9 C10 C11 . . . . -1.3(2) ?
O3 C10 C11 C6 . . . . -178.86(15) ?
C9 C10 C11 C6 . . . . 1.3(2) ?
C7 C6 C11 C10 . . . . -0.5(2) ?
C5 C6 C11 C10 . . . . 178.22(14) ?
C2 C1 N1 N2 . . . . -0.1(3) ?
Cl1 C1 N1 N2 . . . . 178.86(12) ?
N3 C4 N2 N1 . . . . -179.38(14) ?
C3 C4 N2 N1 . . . . 1.6(2) ?
C1 N1 N2 C4 . . . . -1.3(2) ?
N2 C4 N3 N4 . . . . 178.88(14) ?
C3 C4 N3 N4 . . . . -2.2(3) y
C6 C5 N4 N3 . . . . -178.31(14) y
C4 N3 N4 C5 . . . . -178.52(15) y
C7 C8 O1 C13 . . . . 8.3(3) y
C9 C8 O1 C13 . . . . -171.94(17) ?
C11 C10 O3 C12 . . . . 5.9(3) y
C9 C10 O3 C12 . . . . -174.30(16) ?