#------------------------------------------------------------------------------
#$Date: 2025-03-20 04:19:43 +0100 (Thu, 20 Mar 2025) $
#$Revision: 298538 $
#$URL: svn://www.crystallography.net/cod/cif/2/02/34/2023449.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2023449
loop_
_publ_author_name
'Thiam, El Waleda Moustapha'
'Ba, Kalidou Mamadou'
'Kane, Aichata Yaya'
'Thiam, Ibrahima Elhadji'
'Claiser, Nicolas'
'Souhassou, Mohamed'
'Barry, Aliou Hamady'
'Gaye, Mohamed'
_publ_section_title
;
 Synthesis and crystal structure of dipotassium nickel polyphosphate
;
_journal_coeditor_code           EV2014
_journal_issue                   4
_journal_name_full
'Acta Crystallographica Section E Crystallographic Communications'
_journal_paper_doi               10.1107/S2056989025002221
_journal_volume                  81
_journal_year                    2025
_chemical_formula_iupac          'K2 Ni (P O3)4'
_chemical_formula_moiety         'K2 Ni O12 P4'
_chemical_formula_sum            'K2 Ni O12 P4'
_chemical_formula_weight         452.79
_chemical_name_systematic
;
Dipotassium nickel polyphosphate
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           9
_space_group_name_Hall           'C -2yc'
_space_group_name_H-M_alt        'C 1 c 1'
_audit_creation_method
;
Olex2 1.5
(compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928)
;
_cell_angle_alpha                90
_cell_angle_beta                 103.2349(14)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   11.07179(16)
_cell_length_b                   12.50386(16)
_cell_length_c                   7.53969(11)
_cell_measurement_reflns_used    5641
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      45.229
_cell_measurement_theta_min      2.495
_cell_volume                     1016.07(3)
_computing_cell_refinement
;
CrysAlisPro (Rigaku OD, 2022)
;
_computing_data_collection
;
CrysAlisPro (Rigaku OD, 2022)
;
_computing_data_reduction
;
CrysAlisPro (Rigaku OD, 2022)
;
_computing_molecular_graphics
;
<i>ORTEP-3 for Windows</i> (Farrugia, 2012), <i>DIAMOND</i>
(Brandenburg,
2006)
;
_computing_publication_material
;
publCIF (Westrip, 2010)
;
_computing_structure_refinement
;
SHELXL  (Sheldrick, 2015b)
;
_computing_structure_solution
;
<i>SHELXT</i>  (Sheldrick, 2015a)
;
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  SuperNova
_diffrn_measurement_method       \q/2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0345
_diffrn_reflns_av_unetI/netI     0.0276
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_k_max       24
_diffrn_reflns_limit_k_min       -24
_diffrn_reflns_limit_l_max       14
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            33158
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         45.229
_diffrn_reflns_theta_min         2.495
_diffrn_standards_decay_%        0
_diffrn_standards_interval_time  120
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    3.425
_exptl_absorpt_correction_T_max  0.710
_exptl_absorpt_correction_T_min  0.509
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
(CrysAlisPro; Rigaku OD, 2022)
;
_exptl_crystal_colour            'metallic reddish red'
_exptl_crystal_density_diffrn    2.960
_exptl_crystal_description       block
_exptl_crystal_F_000             888
_exptl_crystal_size_max          0.12
_exptl_crystal_size_mid          0.08
_exptl_crystal_size_min          0.07
_refine_diff_density_max         0.825
_refine_diff_density_min         -2.854
_refine_ls_abs_structure_details
;
 Refined as an inversion twin
;
_refine_ls_abs_structure_Flack   0.539(9)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.066
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     173
_refine_ls_number_reflns         8076
_refine_ls_number_restraints     2
_refine_ls_restrained_S_all      1.066
_refine_ls_R_factor_all          0.0318
_refine_ls_R_factor_gt           0.0306
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0564P)^2^+1.2215P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0870
_refine_ls_wR_factor_ref         0.0884
_reflns_number_gt                7869
_reflns_number_total             8076
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            ev2014.cif
_cod_data_source_block           I
_cod_database_code               2023449
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_hkl_file
;
 -22   0   3-196.699 140.601  12
 -22   0   4 895.885 245.183  12
 -22  -2   3 4792.15 484.313   8
 -22   2   3 5486.93 562.781  12
 -21  -1  -1 6286.19 552.958   2
 -21   1  -1 5609.69 498.935   2
 -21  -1  -1 5570.17 571.461  12
 -21   1   0 4881.40 473.836   2
 -21  -1   0 5230.67 508.579   2
 -21   1   0 3557.11 449.931  12
 -21  -1   0 4932.88 540.143  12
 -21  -1   1 3143.38 443.848  12
 -21  -1   1 3825.33 431.076   2
 -21   1   1 3545.57 458.853  12
 -21  -1   2 2555.07 342.263   8
 -21   1   2 2486.62 386.019  12
 -21  -1   2 3089.31 415.147  12
 -21  -1   2 2755.47 362.069   2
 -21  -1   3 2802.12 369.981   8
 -21   1   3 2708.10 399.691  12
 -21  -1   3 3001.77 430.488  12
 -21  -1   4 470.946 175.507   8
 -21   1   4 343.717 147.654   8
 -21   1   4 320.702 156.094  12
 -21  -1   4 604.195 212.841  12
 -21  -1   5 6602.41 595.924   8
 -21   1   5 6983.59 594.295   8
 -21   1   5 7170.30 665.667  12
 -21  -1   5 7160.70 665.886  12
 -21  -1   6 4476.34 495.030   8
 -21   1   6 3173.91 424.315   8
 -21   1   6 4151.30 502.266  12
 -21  -1   6 4133.72 506.538  12
 -21   1   7 1679.47 316.237   8
 -21  -1   7 1303.98 285.315   8
 -21   1   7 1650.34 325.046  12
 -21  -1   7 1394.12 309.207  12
 -21  -3   0 4841.61 473.296   8
 -21  -3   0 6192.51 568.846   2
 -21  -3   0 5484.31 596.539  12
 -21  -3   1 688.271 191.788   8
 -21   3   1 695.238 202.602  12
 -21  -3   1 933.561 255.311  12
 -21  -3   1 872.920 242.681   2
 -21  -3   2 481.186 172.551   8
 -21   3   2 534.015 196.085  12
 -21  -3   2 463.178 195.765  12
 -21  -3   3 2540.26 358.361   8
 -21  -3   3 2660.52 404.109  12
 -21   3   3 2612.49 391.594  12
 -21  -3   4 3945.90 458.722   8
 -21   3   4 3821.49 480.284  12
 -21  -3   4 3749.07 487.517  12
 -21  -3   5 1911.76 334.943   8
 -21   3   5 2270.12 376.466  12
 -21  -3   5 2603.70 416.920  12
 -21  -3   6 12705.0 858.336   8
 -21   3   6 13512.2 910.123  12
 -21  -3   6 15011.3 978.073  12
 -21   3   7 2231.00 339.283   8
 -21  -3   7 2435.12 378.482   8
 -21  -3   7 2439.04 397.596  12
 -21   3   7 2162.25 373.636  12
 -21  -5   0 694.681 203.788   8
 -21  -5   0 764.488 241.341  12
 -21  -5   0 894.126 235.602   2
 -21  -5   1-71.0723 103.365   8
 -21  -5   1 314.483 189.053  12
 -21  -5   2 6106.63 562.964   8
 -21  -5   2 6193.38 629.855  12
 -21  -5   3 1093.76 268.162   8
 -21  -5   3 1721.08 347.708  12
 -21  -5   4 555.803 191.227   8
 -21  -5   4 1164.78 299.468  12
 -21   5   4 567.560 191.662  12
 -21  -5   5 5532.78 558.409   8
 -21   5   5 4516.43 504.622  12
 -21  -5   6 419.210 173.866   8
 -21   5   6 844.246 230.022  12
 -21  -5   6 836.893 252.685  12
 -21  -7   2 6846.76 614.057   8
 -21  -7   2 8726.03 748.143  12
 -21  -7   3 368.532 139.980   8
 -21  -7   3 470.681 189.786  12
 -21  -7   4 2829.41 401.813   8
 -21  -7   4 3211.28 456.932  12
 -21  -7   5 1173.93 260.797   8
 -20   0  -3 23.3261 75.0910   2
 -20   0  -2 22838.4 1089.06   2
 -20   0  -2 21728.3 1119.82  12
 -20   0  -1 86.8201 125.648  12
 -20   0  -1 76.7002 83.4253   2
 -20   0   0 97.7930 115.303  12
 -20   0   0-13.9160 51.7421   2
 -20   0   1 72.4652 169.615  12
 -20   0   1-101.828 91.9351   2
 -20   0   2 6229.55 531.322   8
 -20   0   2 6667.14 613.400  12
 -20   0   3 29.7908 64.6385   8
 -20   0   3 23.6359 144.756  12
 -20   0   4 358.361 145.218   8
 -20   0   4 193.377 144.134  12
 -20   0   5-0.54234 150.731   8
 -20   0   5-63.8407 163.485  12
 -20   0   6 706.834 225.732   8
 -20   0   6 699.366 218.577  12
 -20   0   7 107.130 116.035   8
 -20   0   7 85.7525 175.435  12
 -20   0   8 12933.7 893.664   8
 -20   0   8 13803.1 925.381  12
 -20   0   9 384.326 189.134   8
 -20   0   9-3.22012 135.627  12
 -20  -2  -2 1324.07 297.123  12
 -20  -2  -2 1138.33 246.750   2
 -20   2  -2 1444.28 257.968   2
 -20  -2  -1 1077.13 267.440  12
 -20   2  -1 1040.22 232.316  12
 -20  -2  -1 1012.23 246.979   2
 -20   2  -1 1049.12 216.738   2
 -20  -2   0 517.135 154.889   8
 -20  -2   0 592.425 214.262  12
 -20   2   0 745.893 215.540  12
 -20  -2   0 438.373 167.712   2
 -20   2   0 931.875 203.063   2
 -20  -2   1 6604.62 558.725   8
 -20  -2   1 6884.78 632.811  12
 -20   2   1 6419.13 587.031  12
 -20  -2   2 2340.06 334.145   8
 -20  -2   2 2379.81 379.036  12
 -20   2   2 2763.15 397.518  12
 -20  -2   3 17131.2 948.453   8
 -20  -2   3 18318.5 1055.27  12
 -20   2   3 18174.3 1026.81  12
 -20   2   4 4838.47 476.738   8
 -20  -2   4 4458.32 478.614   8
 -20   2   4 5366.44 552.813  12
 -20  -2   4 5807.42 592.125  12
 -20  -2   5 5632.90 548.085   8
 -20   2   5 4530.79 473.450   8
 -20   2   5 4944.15 534.939  12
 -20  -2   5 5997.57 597.741  12
 -20   2   6 324.801 147.865   8
 -20  -2   6 607.433 201.299   8
 -20  -2   6 132.145 147.266  12
 -20   2   6 366.446 182.170  12
 -20   2   7 1270.95 280.643   8
 -20  -2   7 1833.34 331.903   8
 -20   2   7 1321.55 300.134  12
 -20  -2   7 1885.30 342.552  12
 -20  -2   8 548.586 222.676   8
 -20   2   8 798.294 233.881   8
 -20   2   8 313.130 176.190  12
 -20  -2   8 417.165 195.416  12
 -20   2   9 5608.47 591.832   8
 -20  -2   9 6510.67 631.356   8
 -20   2   9 6063.90 602.784  12
 -20  -2   9 6517.91 630.498  12
 -20  -4  -2 11667.7 726.774   8
 -20  -4  -2 13252.6 844.831   2
 -20  -4  -2 13044.5 890.060  12
 -20  -4  -1 2551.13 353.577   8
 -20  -4  -1 3353.09 429.966   2
 -20  -4  -1 3280.15 455.240  12
 -20  -4   0 563.433 162.104   8
 -20  -4   0 581.838 227.135  12
 -20  -4   0 518.983 189.644   2
 -20  -4   1 2547.99 359.263   8
 -20   4   1 2209.21 325.442  12
 -20  -4   1 3055.75 438.413  12
 -20  -4   2 1959.45 308.324   8
 -20  -4   2 2148.00 378.672  12
 -20   4   2 2533.37 365.569  12
 -20  -4   3 4114.93 459.040   8
 -20  -4   3 4096.20 499.841  12
 -20   4   3 3638.90 441.088  12
 -20  -4   4 7273.78 620.581   8
 -20  -4   4 8022.15 695.053  12
 -20   4   4 7444.13 642.408  12
 -20  -4   5 725.710 221.770   8
 -20  -4   5 668.411 216.715  12
 -20   4   5 435.799 189.929  12
 -20  -4   6 762.240 221.924   8
 -20   4   6 1111.59 245.178   8
 -20  -4   6 767.664 248.567  12
 -20   4   6 1253.21 285.529  12
 -20   4   7 1453.80 297.374   8
 -20  -4   7 1950.92 335.707   8
 -20   4   7 1633.45 331.581  12
 -20  -4   7 1986.03 365.321  12
 -20  -4   8 2572.34 377.966   8
 -20   4   8 2424.09 383.086   8
 -20   4   8 2976.51 430.210  12
 -20  -4   8 2938.26 411.097  12
 -20  -6  -1 907.794 222.108   8
 -20  -6  -1 866.620 247.711  12
 -20  -6  -1 743.266 212.579   2
 -20  -6   0 1212.36 253.751   8
 -20  -6   0 1534.42 314.168  12
 -20  -6   1 850.973 210.836   8
 -20  -6   1 1036.73 283.713  12
 -20  -6   2 6573.59 582.307   8
 -20  -6   2 6485.75 632.137  12
 -20  -6   3 3105.13 410.470   8
 -20  -6   3 2931.46 434.481  12
 -20  -6   4 16453.2 959.617   8
 -20   6   4 14869.1 894.630  12
 -20  -6   4 17386.7 1043.68  12
 -20  -6   5 3108.34 416.905   8
 -20   6   5 2658.42 384.522  12
 -20  -6   5 3192.99 445.033  12
 -20  -6   6 1164.31 280.702   8
 -20   6   6 459.898 174.629  12
 -20  -6   6 1085.20 272.682  12
 -20  -6   7-70.5579 117.629   8
 -20  -6   7 159.968 115.702  12
 -20   6   7 234.660 151.627  12
 -20  -6   8 300.058 163.114   8
 -20  -6   8 278.644 154.858  12
 -20   6   8 349.994 179.406  12
 -20  -8   0 3999.25 456.399   8
 -20  -8   0 4512.24 546.872  12
 -20  -8   1 5337.58 539.131   8
 -20  -8   1 6190.68 619.412  12
 -20  -8   2 894.458 244.358   8
 -20  -8   2 1414.26 311.890  12
 -20  -8   3 1878.50 327.830   8
 -20  -8   3 2697.86 399.696  12
 -20  -8   4 9248.60 716.608   8
 -20  -8   4 9388.04 756.665  12
 -20  -8   5 1969.87 339.305   8
 -20  -8   5 1614.71 330.407  12
 -20  -8   6 7566.67 651.533   8
 -20  -8   6 7942.59 691.141  12
 -20  -8   7 1797.25 337.760   8
 -20  -8   7 1190.06 253.935  12
 -20 -10   2 755.729 226.149   8
 -20 -10   2 1021.72 275.355  12
 -20  10   2 1132.30 244.047  13
 -20 -10   3 851.936 228.656   8
 -20 -10   3 1122.06 264.728  12
 -20 -10   4 5054.00 521.972   8
 -20 -10   4 5616.48 585.390  12
 -19  -1  -4 470.811 182.632  12
 -19   1  -4 575.803 163.869   2
 -19  -1  -4 945.970 222.487   2
 -19  -1  -3 1543.30 303.420  12
 -19   1  -3 1990.12 318.773  12
 -19  -1  -3 1805.07 294.077   2
 -19   1  -3 1941.76 308.824   2
 -19  -1  -2 1686.19 316.478  12
 -19   1  -2 1318.49 272.547  12
 -19   1  -2 1225.51 239.323   2
 -19  -1  -2 1183.85 254.658   2
 -19  -1  -1 2753.74 327.438   8
 -19  -1  -1 2376.13 375.249  12
 -19   1  -1 2867.29 390.199  12
 -19   1  -1 2815.73 359.008   2
 -19  -1  -1 3570.90 413.462   2
 -19  -1   0 8266.03 586.444   8
 -19  -1   0 8132.11 620.622   2
 -19   1   0 9442.13 653.149   2
 -19   1   0 9120.63 687.966  12
 -19  -1   0 8803.68 695.013  12
 -19  -1   1 5333.60 482.519   8
 -19   1   1 5375.47 457.980   8
 -19   1   1 5716.04 496.160   2
 -19  -1   1 5667.09 556.046  12
 -19   1   1 5246.88 521.584  12
 -19   1   2 7345.06 547.585   8
 -19  -1   2 7301.10 570.451   8
 -19  -1   2 6969.44 622.212  12
 -19   1   2 7394.02 624.436  12
 -19   1   3 4076.19 425.225   8
 -19  -1   3 3735.41 421.279   8
 -19   1   3 4370.07 489.754  12
 -19  -1   3 4427.35 503.930  12
 -19  -1   4 317.468 164.687   8
 -19   1   4 482.002 177.231   8
 -19  -1   4 187.180 160.180  12
 -19   1   4 447.356 200.413  12
 -19   1   5 10908.8 746.731   8
 -19  -1   5 11935.8 790.740   8
 -19   1   5 12357.3 834.023  12
 -19  -1   5 13291.4 868.718  12
 -19   1   6 1554.22 310.416   8
 -19  -1   6 1557.41 293.923   8
 -19   1   6 1634.82 326.464  12
 -19  -1   6 2210.69 375.608  12
 -19   1   7 7329.14 654.574   8
 -19  -1   7 7838.05 679.157   8
 -19   1   7 8097.12 696.786  12
 -19  -1   7 8502.21 708.885  12
 -19   1   8 1521.78 319.560   8
 -19  -1   8 1591.50 342.412   8
 -19  -1   8 1365.59 306.464  12
 -19   1   8 1789.67 337.671  12
 -19   1   9 7290.70 700.161   8
 -19  -1   9 7436.23 695.003   8
 -19  -1   9 7917.95 694.367  12
 -19   1   9 7502.52 679.239  12
 -19   1  10 3116.80 469.593   8
 -19  -1  10 2897.50 441.831   8
 -19  -1  10 3293.26 444.781  12
 -19   1  10 3072.57 438.986  12
 -19  -3  -4 7100.17 592.775   2
 -19   3  -4 5863.91 494.219   2
 -19   3  -4 6636.67 583.450  13
 -19  -3  -4 6215.42 588.911  12
 -19  -3  -3 3333.28 435.290  12
 -19   3  -3 2818.97 344.964   2
 -19  -3  -3 3215.68 407.811   2
 -19  -3  -2 854.922 211.961   8
 -19  -3  -2 967.676 253.578  12
 -19   3  -2 887.994 195.418   2
 -19  -3  -2 1053.61 249.848   2
 -19  -3  -1 1012.25 222.968   8
 -19   3  -1 1404.30 264.650  12
 -19  -3  -1 1317.46 293.769  12
 -19  -3  -1 1315.00 259.840   2
 -19   3  -1 1445.43 240.203   2
 -19  -3   0 2188.81 319.523   8
 -19   3   0 2050.78 320.111  12
 -19  -3   0 2291.31 365.326  12
 -19   3   0 1978.55 277.214   2
 -19  -3   1 967.490 220.498   8
 -19   3   1 1013.46 228.428  12
 -19  -3   1 1127.38 290.894  12
 -19  -3   2 7439.63 591.890   8
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   1  -1   7 32894.0 1285.13   1
   1   1   7 33941.3 1324.49   1
   1   1   7 31675.0 809.558   6
   1  -1   7 32990.1 794.901   6
   1  -1   8 1241.63 226.714   7
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   1   5   7 564.624 114.571   7
   1  -5   7 549.581 90.2881   4
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   1   5   9 4806.83 384.435   7
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   1   5  11 8980.87 469.701   6
   1  -5  11 8545.60 615.905   9
   1   5  11 8891.13 669.105   7
   1   5  12 771.792 143.340   6
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   1   5  12 569.630 200.434   7
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   1  -5  13 719.935 341.896   7
   1   5  13 1237.60 333.199   7
   1  -5  14 1092.35 437.088   7
   1   7 -14 3187.43 299.934   2
   1   7 -13 695.585 142.827   2
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   1   7 -12 173.438 92.9280   2
   1   7 -11 19483.8 653.950  13
   1   7 -11 18291.7 718.994   2
   1   7 -10 7598.19 372.415  13
   1   7 -10 7327.53 409.823   2
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   1   7  -9 2446.42 197.636  13
   1   7  -9 2693.34 236.300   2
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   1  -7  -8 39356.7 1146.23  10
   1   7  -8 41689.4 1010.07  13
   1  -7  -8 37495.6 1210.11   5
   1   7  -8 41147.5 1069.11   2
   1  -7  -8 38927.7 915.073   2
   1  -7  -7 3299.63 269.394  10
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   1   7  -4 42971.1 965.889   2
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   1   7  -4 43777.2 954.490  13
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   1  -7  -3 1393.71 69.1330   2
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   1  -7  -3 1518.77 130.327   3
   1   7  -2 74763.8 1524.88   2
   1  -7  -2 81266.9 1707.86   5
   1   7  -2 79311.3 1534.74  13
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   1  -7  -2 77668.4 1648.28  10
   1  -7  -2 78244.2 1576.64   9
   1  -7  -2 81900.2 1554.74   8
   1  -7  -2 81582.0 1579.91   3
   1   7  -1 2017.84 111.116   2
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   1  -7  -1 1910.00 114.404  12
   1  -7  -1 1836.67 156.567   5
   1  -7  -1 1921.98 137.104   9
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   1  -7  -1 2012.56 110.670   8
   1  -7  -1 1861.06 129.323   3
   1   7   0 1331.38 80.9161  13
   1  -7   0 1265.84 73.2526  12
   1  -7   0 1217.58 81.4476  11
   1  -7   0 1080.58 116.082   4
   1  -7   0 1234.84 122.511   5
   1  -7   0 1184.80 114.694  10
   1  -7   0 1159.16 113.454   9
   1  -7   0 1223.75 72.7914   8
   1  -7   0 1172.04 101.928   3
   1  -7   1 133559. 2435.01   6
   1  -7   1 131706. 2404.52  11
   1  -7   1 141230. 2552.93   5
   1  -7   1 124574. 2548.13   4
   1  -7   1 135829. 2554.34  10
   1  -7   1 128131. 2591.72   9
   1  -7   1 134423. 2344.81   8
   1  -7   1 142393. 2554.46   3
   1  -7   2 5418.93 200.458   6
   1  -7   2 5382.77 185.643  11
   1  -7   2 5322.29 248.759   4
   1  -7   2 5873.46 241.944   5
   1  -7   2 5670.69 256.808  10
   1  -7   2 5574.48 296.672   9
   1  -7   2 5599.93 279.278   3
   1   7   3 5075.01 241.957   7
   1  -7   3 5007.73 195.791   6
   1  -7   3 5208.63 191.728  11
   1  -7   3 5496.64 215.518   5
   1  -7   3 5202.88 249.083  10
   1  -7   3 4962.26 302.532   9
   1  -7   3 5002.81 150.723   8
   1  -7   3 3827.04 415.519   7
   1  -7   3 5132.68 295.852   3
   1  -7   3 5214.81 244.263   4
   1  -7   4 135022. 2652.60   4
   1  -7   4 141841. 2566.70  11
   1   7   4 136664. 2831.22  14
   1  -7   4 143411. 2508.90   5
   1   7   4 137330. 2689.89   7
   1  -7   4 140383. 2570.23   6
   1  -7   5 5041.34 252.485   4
   1  -7   5 5084.25 221.619  11
   1   7   5 5201.71 340.409  14
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   2   4  10 6078.51 500.073   7
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   2  -6   7 34496.7 1567.44   7
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   2   6   9 1439.30 219.945   7
   2  -6  10 9474.00 640.857   9
   2   6  10 9084.10 596.826   7
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   2   6  13 4573.26 615.627   7
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   2   8 -14 729.816 143.369   2
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   2  -8   0 6522.48 267.150   3
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   2   8   2 349.452 70.9030   7
   2  -8   2 369.483 45.3498  11
   2  -8   2 411.168 72.9754   5
   2  -8   2 295.627 67.1028  10
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   2  -8   2 327.154 73.6654   4
   2   8   3 96061.9 1976.35   7
   2  -8   3 96426.9 1823.39   6
   2  -8   3 97032.0 1792.56  11
   2  -8   3 99055.6 1900.22   5
   2  -8   3 95944.3 2120.47   9
   2  -8   3 100826. 1973.79  10
   2  -8   3 93372.5 1965.97   4
   2  -8   3 98991.5 2068.76   3
   2  -8   4 13142.5 469.689   4
   2  -8   4 12931.9 546.064   3
   2   8   4 13183.7 561.562  14
   2  -8   4 13125.8 365.221  11
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   2  -8   4 13849.0 469.788  10
   2  -8   4 10760.2 779.376   7
   2   8   4 13016.1 482.351   7
   2  -8   4 13090.4 377.126   6
   2  -8   5 39853.0 1006.17   4
   2   8   5 40526.1 1182.05  14
   2  -8   5 40079.7 882.050  11
   2   8   5 40463.1 1925.45   1
   2  -8   5 41052.2 997.802  10
   2  -8   5 40728.5 1215.74   9
   2  -8   5 35698.6 1577.21   7
   2  -8   5 40431.4 889.976   6
   2   8   5 41561.9 1080.37   7
   2  -8   6 10581.2 437.935   4
   2   8   6 10838.9 572.140  14
   2  -8   6 11219.5 372.270  11
   2   8   6 10523.5 964.249   1
   2  -8   6 11416.6 431.009  10
   2  -8   6 10523.7 582.841   9
   2  -8   6 9429.13 827.134   7
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   2 -18   4 3417.25 341.269   3
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   2 -22  -4 219.192 164.630  10
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   2 -22   2 1051.45 230.395   9
   2 -22   2 961.744 256.694  10
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   2 -22   3 6194.66 481.242   3
   2 -22   3 5715.81 555.069   9
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   2  22   4 2183.89 359.969  14
   2 -22   4 2024.19 344.871   9
   2 -22   4 2786.38 324.721   3
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   2 -22   5 9054.08 690.574  10
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   2  22   6 4642.30 540.128  14
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   2 -24  -3 3221.05 418.707   3
   2 -24  -3 2864.71 423.222  10
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   2 -24  -2 6422.08 531.477   3
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   2 -24  -2 4892.34 558.646   5
   2 -24  -1 13197.7 740.101   3
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   2 -24   0 3226.21 350.909   3
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   2 -24   1 591.081 157.889   3
   2 -24   1 543.971 196.000  10
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   2 -24   2 881.937 235.989  10
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   2 -24   3 817.194 177.731   3
   2 -24   3 846.512 207.673  10
   3   1 -14 5599.08 366.466   2
   3   1 -13 17475.2 681.468   2
   3  -1 -13 18344.6 681.310   2
   3   1 -12 7435.06 404.754   2
   3  -1 -12 7648.63 398.497   2
   3   1 -11 865.524 135.109   2
   3  -1 -11 851.962 128.961   2
   3   1 -10 3752.39 258.484   2
   3  -1 -10 3695.18 244.359   2
   3   1  -9 251.296 75.1477   2
   3  -1  -9 163.971 60.0999   2
   3  -1  -9 197.659 62.1755   5
   3   1  -8 23025.3 663.289   2
   3  -1  -8 23206.2 644.254   2
   3   1  -8 21380.0 695.272   5
   3  -1  -8 22167.3 746.505   5
   3   1  -7 5196.63 208.212  13
   3   1  -7 4847.95 241.744   2
   3  -1  -7 4946.51 231.882   2
   3   1  -7 4067.17 256.538   5
   3  -1  -7 4526.36 287.219   5
   3   1  -6 138378. 2392.04  13
   3   1  -6 129939. 2453.14   2
   3  -1  -6 130399. 2425.91   2
   3   1  -6 119622. 2536.44   5
   3  -1  -6 121506. 2586.61   5
   3   1  -5 3398.83 147.622  13
   3   1  -5 3235.31 206.701   5
   3  -1  -5 3245.84 221.052   5
   3   1  -5 3214.28 166.749   2
   3   1  -4 22321.7 625.383   5
   3  -1  -4 22486.3 649.356   5
   3  -1  -4 22380.4 655.144  10
   3   1  -4 23106.9 541.642   2
   3  -1  -4 23498.4 519.413   2
   3   1  -3 1224.74 114.704   5
   3  -1  -3 1284.66 126.393   5
   3  -1  -3 1462.49 129.116  10
   3   1  -3 1313.85 84.0546   2
   3  -1  -3 1425.94 76.8759   2
   3   1  -2 118790. 2263.60   5
   3  -1  -2 115476. 2269.40   5
   3  -1  -2 123987. 2146.69   4
   3  -1  -2 117749. 2094.24   2
   3   1  -2 118768. 2127.50   2
   3   1  -2 112448. 2279.83   1
   3  -1  -2 117440. 2259.15  10
   3  -1  -1 104812. 1936.88  10
   3  -1  -1 104967. 1925.81   9
   3   1  -1 98619.0 1897.55   4
   3  -1  -1 105016. 1870.33   4
   3  -1  -1 96178.8 2103.54   1
   3   1  -1 92994.9 2116.86   1
   3  -1  -1 104753. 1960.22   5
   3  -1   0 72607.2 1372.58   5
   3  -1   0 68721.8 1267.61   7
   3  -1   0 64247.5 1628.35   1
   3   1   0 63198.4 1645.63   1
   3  -1   0 69992.5 1359.01   4
   3  -1   0 71607.7 1332.68  10
   3  -1   0 68718.8 1339.20   9
   3   1   0 70079.8 1318.94   9
   3  -1   1 2111.76 123.318   7
   3   1   1 1366.39 94.4604   7
   3   1   1 1228.50 187.495   1
   3  -1   1 1535.03 202.306   1
   3  -1   1 1723.87 140.309   4
   3  -1   1 1554.44 101.948   9
   3   1   1 1749.14 89.3464   9
   3   1   2 90171.6 1701.91   7
   3  -1   2 97286.3 1725.44   7
   3   1   2 88049.7 1612.53   9
   3  -1   2 84682.4 1678.87   9
   3   1   2 84386.7 2211.25   1
   3  -1   2 81726.1 2158.63   1
   3  -1   2 76704.9 1841.10   4
   3  -1   3 5663.62 164.867   6
   3  -1   3 6404.50 271.198   7
   3  -1   3 5745.03 244.588   9
   3   1   3 5722.92 205.636   9
   3  -1   3 4682.90 332.624   4
   3  -1   3 5148.89 441.213   1
   3   1   3 6038.24 487.478   1
   3  -1   4 55589.5 1801.31   1
   3   1   4 54616.0 1824.94   1
   3  -1   4 58078.9 1106.45   6
   3   1   4 62690.6 1329.05   7
   3  -1   4 59451.1 1260.12   9
   3   1   4 58711.0 1181.51   9
   3  -1   4 60279.9 1308.01   7
   3  -1   5 5230.80 503.509   1
   3   1   5 5300.00 519.977   1
   3  -1   5 5773.36 210.493   6
   3   1   5 5772.40 311.121   7
   3   1   5 5837.98 256.638   9
   3  -1   5 5811.57 290.746   9
   3  -1   5 5830.25 320.442   7
   3  -1   5 4354.10 372.610   4
   3  -1   6 87866.9 1696.18   6
   3   1   6 91929.8 1814.30   9
   3  -1   6 92747.2 1905.15   9
   3   1   6 89327.4 1947.77   7
   3  -1   6 86610.5 1979.79   7
   3  -1   6 83863.1 2568.69   1
   3   1   6 83529.6 2608.10   1
   3   1   7 6562.03 283.335   6
   3  -1   7 6794.66 271.199   6
   3  -1   7 6291.24 468.849   4
   3   1   7 7061.76 334.984   9
   3  -1   7 7417.06 386.942   9
   3   1   7 6690.03 402.759   7
   3  -1   7 6613.06 434.068   7
   3  -1   7 6315.11 614.345   1
   3   1   7 6241.98 620.845   1
   3  -1   8 16417.6 1058.58   1
   3   1   8 16713.2 1089.31   1
   3  -1   8 20166.0 558.404   6
   3  -1   8 20072.4 725.969   9
   3   1   8 19689.2 581.059   6
   3   1   8 20636.2 820.099   7
   3  -1   8 18226.0 834.411   7
   3  -1   8 17198.3 817.383   4
   3  -1   9 20357.9 594.747   6
   3  -1   9 20436.1 773.180   9
   3  -1   9 19296.6 967.467   7
   3   1   9 19957.7 905.335   7
   3  -1   9 17875.3 825.421   4
   3   1   9 19244.1 609.527   6
   3  -1  10 2197.34 276.466   4
   3   1  10 1376.73 266.352   4
   3  -1  10 1576.30 327.326   7
   3   1  10 1998.89 333.325   7
   3   1  11 8070.57 713.229   7
   3  -1  11 8259.54 786.615   7
   3  -1  12 1588.22 419.440   7
   3   1  12 1884.58 400.688   7
   3  -1  12 2401.32 247.495  11
   3  -1  13 2229.86 507.512   7
   3   1  13 2204.00 496.412   7
   3   1  13 2669.86 275.020  11
   3  -1  14 1860.88 517.814   7
   3   1  14 1776.46 502.456   7
   3   3 -14 719.670 142.437   2
   3   3 -13 5038.93 350.475   2
   3   3 -12 35682.3 1056.08   2
   3  -3 -12 35976.7 994.496   2
   3   3 -11 848.876 140.953   2
   3  -3 -11 737.624 114.817   2
   3  -3 -10 963.676 121.257   2
   3   3 -10 702.046 123.147   2
   3  -3  -9 26982.6 923.032   5
   3   3  -9 30253.9 748.594  13
   3   3  -9 28462.2 820.043   2
   3  -3  -9 28849.8 762.287   2
   3  -3  -8 2681.40 252.158   5
   3   3  -8 3102.97 214.195   2
   3  -3  -8 2911.49 181.736   2
   3   3  -8 3246.97 186.020  13
   3  -3  -7 708.121 126.015   5
   3  -3  -7 771.578 136.088  10
   3   3  -7 831.619 107.489   2
   3  -3  -7 777.439 87.1670   2
   3   3  -7 861.823 91.0191  13
   3  -3  -6 143414. 3029.99  10
   3   3  -6 159915. 2998.35   1
   3   3  -6 155101. 2877.39   2
   3  -3  -6 152576. 2793.00   2
   3   3  -6 157298. 2817.11  13
   3  -3  -6 140990. 3035.15   5
   3  -3  -5 27539.3 813.063  10
   3   3  -5 29664.8 710.223   2
   3  -3  -5 29212.0 637.716   2
   3   3  -5 30559.9 842.396   1
   3   3  -5 30297.9 671.849  13
   3  -3  -5 27661.5 825.783   5
   3  -3  -4 3502.97 225.537  10
   3   3  -4 3756.98 177.862   2
   3  -3  -4 4149.06 145.699   2
   3   3  -4 3972.53 165.535  13
   3  -3  -4 3555.14 234.242   5
   3  -3  -3 42745.1 1028.17  10
   3   3  -3 44020.1 915.564   2
   3  -3  -3 44408.9 829.590   2
   3  -3  -3 42481.1 1045.30   5
   3  -3  -2 33230.5 810.629  10
   3  -3  -2 34660.8 788.652   9
   3   3  -2 31787.8 699.450   2
   3  -3  -2 35637.4 765.697   4
   3  -3  -2 33646.3 833.394   5
   3  -3  -2 34616.4 727.442   3
   3  -3  -1 124218. 2329.10   5
   3  -3  -1 119631. 2255.47   4
   3  -3  -1 122690. 2146.84   3
   3  -3  -1 120712. 2294.10  10
   3  -3  -1 119016. 2277.63   9
   3  -3   0 402911. 7021.77   5
   3  -3   0 411426. 6983.91  10
   3  -3   0 390804. 7003.11   9
   3  -3   0 411348. 6919.99   7
   3  -3   0 397724. 6990.13   4
   3  -3   0 416998. 6893.57   3
   3  -3   1 27751.1 662.495   4
   3   3   1 27461.3 632.208  14
   3  -3   1 28490.4 629.675   5
   3  -3   1 25228.9 976.710   1
   3  -3   1 25325.6 658.042   9
   3  -3   1 26805.9 598.864  10
   3  -3   1 28896.9 634.075   7
   3   3   1 25171.5 625.599   7
   3  -3   2 4489.87 228.029   4
   3   3   2 4785.31 226.216  14
   3  -3   2 5091.13 171.592   5
   3  -3   2 4597.69 166.040  10
   3  -3   2 4609.98 225.650   9
   3   3   2 4387.89 205.766   7
   3  -3   2 4336.49 115.488   6
   3  -3   2 4833.03 226.206   7
   3   3   2 4490.15 422.093   1
   3  -3   2 4530.48 395.369   1
   3  -3   3 73584.6 1569.86   4
   3  -3   3 72960.2 2086.22   1
   3   3   3 73377.2 2187.39   1
   3   3   3 73937.4 1564.23  14
   3  -3   3 76926.2 1586.81   7
   3  -3   3 74245.5 1361.54  10
   3  -3   3 74007.4 1553.54   9
   3   3   3 72301.8 1511.91   7
   3  -3   3 72080.7 1322.20   6
   3   3   4 1149.71 241.278   1
   3  -3   4 1050.50 217.223   1
   3  -3   4 1263.80 70.8970  10
   3  -3   4 1095.01 130.143   9
   3   3   4 1299.95 71.7082   9
   3  -3   4 1243.04 73.9814   6
   3   3   4 1469.22 152.265   7
   3  -3   4 1293.95 152.187   7
   3  -3   4 1371.01 150.518   4
   3   3   5 23884.1 1224.88   1
   3  -3   5 25864.0 1199.40   1
   3  -3   5 25771.2 782.366   9
   3   3   5 25324.3 577.067   9
   3  -3   5 25824.4 575.820   6
   3  -3   5 26158.8 847.039   7
   3  -3   5 25178.1 801.527   4
   3  -3   6 107307. 3056.91   1
   3   3   6 106515. 3161.56   1
   3  -3   6 112338. 2393.10   9
   3  -3   6 109428. 2529.34   7
   3  -3   6 104564. 2392.06   4
   3  -3   6 112910. 2084.04   6
   3   3   6 116771. 2383.91   7
   3   3   7 410.708 173.738   1
   3  -3   7 496.526 172.651   1
   3  -3   7 675.197 171.526   7
   3  -3   7 575.793 74.3711   6
   3   3   7 505.931 117.451   7
   3  -3   7 359.934 106.713   9
   3  -3   7 579.510 122.695   4
   3  -3   8 8051.57 308.274   6
   3  -3   8 7946.95 472.916   9
   3  -3   8 8811.09 645.469   7
   3   3   8 7764.98 469.528   7
   3  -3   8 7179.77 433.090   4
   3   3   9 1813.39 175.357   6
   3  -3   9 1852.90 240.427   9
   3  -3   9 1405.11 317.686   7
   3   3   9 1541.68 239.892   7
   3  -3   9 1700.22 215.712   4
   3  -3  10 6913.34 373.466  11
   3   3  10 6676.26 358.689   6
   3  -3  10 7218.95 495.996   9
   3   3  10 6956.06 543.618   7
   3  -3  10 5374.07 638.651   7
   3   3  11 11272.4 807.084   7
   3  -3  11 9835.80 940.452   7
   3   3  11 9664.13 780.988   4
   3  -3  11 11058.8 510.126  11
   3   3  12 8617.17 778.122   7
   3  -3  12 8019.97 920.030   7
   3  -3  13 1192.38 425.088   7
   3   3  13 1078.36 327.050   7
   3   5 -14 2430.58 250.287   2
   3   5 -13 5893.62 389.064   2
   3   5 -12 27.2527 72.9487   2
   3   5 -11 3644.79 284.955   2
   3   5 -10 2349.23 219.569   2
   3  -5 -10 2444.56 184.008   2
   3   5 -10 2594.43 193.696  13
   3  -5 -10 2358.39 265.535   5
   3   5  -9 16815.8 602.846   2
   3  -5  -9 17323.7 520.355   2
   3   5  -9 17894.2 550.937  13
   3  -5  -9 15646.5 710.101   5
   3  -5  -8 13977.8 617.982  10
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   3   5  -7 22738.9 877.789   1
   3  -5  -7 18912.8 749.258   5
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   3   5  -6 565.810 126.887   1
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   3  -5   3 33269.8 1015.42   7
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   3  -5   5 17446.9 789.409   7
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   3   5   7 17618.9 682.176   7
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   3  -5   7 14873.5 881.628   7
   3  -5   7 15704.9 599.291   4
   3  -5   8 1832.73 354.127   7
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   3   5   8 2830.76 278.469   7
   3  -5   8 2386.21 225.725   4
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   3  -5   9 934.429 123.523  11
   3  -5   9 993.175 203.775   9
   3  -5   9 522.058 272.244   7
   3   5   9 918.612 185.860   7
   3  -5  10 192.302 234.799   7
   3   5  10 983.972 219.707   7
   3  -5  10 891.444 130.620  11
   3   5  10 953.814 141.673   6
   3  -5  10 1014.38 211.778   9
   3   5  10-86.4265 146.615   4
   3  -5  11 3132.60 590.889   7
   3   5  11 3707.29 435.091   7
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   3  -5  12 2004.45 548.641   7
   3   5  12 3630.90 484.670   7
   3  -5  13 1461.97 510.218   7
   3   5  13 1620.95 370.145   7
   3   7 -14 3056.75 289.759   2
   3   7 -13 353.515 114.682   2
   3   7 -12 17290.9 704.443   2
   3   7 -11 3482.79 287.458   2
   3   7 -10 314.437 101.094   2
   3   7 -10 208.193 72.0766  13
   3  -7 -10 228.143 105.354   5
   3  -7  -9 35845.4 1153.23  10
   3   7  -9 36352.2 1012.14   2
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   3  -7  -9 33429.1 1184.89   5
   3  -7  -8 17543.2 740.178  10
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   3   7  -8 20192.9 660.427   2
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   3  -7  -7 5190.01 360.523  10
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   3   7  -7 5199.69 294.736   2
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   3  -7  -6 26720.1 904.700  10
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   3   7  -6 33398.6 1302.07   1
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   3  -7  -5 581.420 120.283  10
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   3   7  -5 695.879 96.9938   2
   3  -7  -5 858.952 52.8579   2
   3   7  -5 940.540 101.809  13
   3   7  -4 20351.4 529.717  13
   3  -7  -4 18330.3 653.030  10
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   3  -7  -3 34702.9 783.184   3
   3   7  -3 30175.2 747.724   2
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   3  -7  -3 30044.2 872.442  10
   3  -7  -2 78978.6 1656.71   9
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   3  -7   0 114091. 2326.36   9
   3  -7   0 117066. 2305.36  10
   3  -7   0 110910. 2304.22   4
   3  -7   0 119160. 2345.27   5
   3  -7   0 121756. 2213.45   3
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   3  -7   2 5331.45 271.196   3
   3  -7   3 144505. 2870.19   3
   3  -7   3 141000. 2812.64   4
   3   7   3 150749. 2923.99  14
   3  -7   3 140831. 2576.88  11
   3  -7   3 151789. 2688.10   5
   3  -7   3 150656. 2763.02  10
   3  -7   3 148086. 2951.52   9
   3   7   3 146722. 2823.69   7
   3  -7   3 143286. 2607.99   6
   3  -7   4 6955.23 336.711   4
   3   7   4 7002.72 393.020  14
   3  -7   4 7469.17 234.841  11
   3   7   4 8184.90 776.432   1
   3  -7   4 7981.72 315.125  10
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   3  -7   4 6871.58 542.263   7
   3   7   4 7637.26 358.993   7
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   3  -7   5 5038.38 291.082   4
   3   7   5 5308.88 362.213  14
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   3   7   5 4668.89 624.433   1
   3  -7   5 5953.98 398.251   9
   3  -7   5 5655.71 264.008  10
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   3   7   5 5378.43 326.322   7
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   3  -7   6 21734.3 708.863   4
   3   7   6 20099.0 1356.85   1
   3   7   6 22219.5 855.064  14
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   3  -7   6 20445.8 1106.69   7
   3  -7   6 22577.2 567.703   6
   3   7   7 362.653 181.346   1
   3   7   7 111.002 89.2795   7
   3  -7   7 160.791 50.3231  11
   3  -7   7 216.682 53.1362   6
   3  -7   7 122.873 111.430   9
   3  -7   7 151.166 66.8533   4
   3  -7   8 4346.69 241.377  11
   3   7   8 4914.36 372.100   7
   3  -7   8 3473.24 532.012   7
   3  -7   8 3779.85 277.220   4
   3  -7   8 4321.56 401.401   9
   3   7   9 8335.10 521.650   7
   3  -7   9 7068.17 808.078   7
   3  -7   9 7338.37 553.224   9
   3   7  10 39395.6 1355.97   7
   3  -7  10 38445.2 1428.52   9
   3   7  11 7149.05 586.697   7
   3  -7  11 6809.69 579.867   9
   3   7  12 7824.93 692.004   7
   3  -7  12 5983.66 894.836   7
   3  -7  13 861.156 385.548   7
   3   7  13 1208.00 297.946   7
   3   9 -13 1373.74 200.517   2
   3   9 -12 1587.70 211.078   2
   3   9 -11 8507.46 471.218   2
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   3   9 -10 7307.09 420.197   2
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   3  -9  -8 2037.10 254.260  10
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   3  -9  -7 41593.6 1301.84  10
   3   9  -7 46741.4 1102.29  13
   3   9  -7 47626.4 1162.19   2
   3  -9  -7 41589.3 1358.15   5
   3  -9  -6 6709.31 427.376  10
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   3  -9  -3 131599. 2759.52   5
   3   9  -3 138322. 2472.34  13
   3  -9  -3 128760. 2686.99  10
   3  -9  -3 127432. 2583.49   9
   3  -9  -3 131805. 2511.92   3
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   3   9   3 19204.9 630.580   7
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   3  -9   3 18306.7 441.416  11
   3  -9   3 19559.7 573.300   5
   3  -9   3 20370.2 622.226  10
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   3  -9   3 19157.1 652.740   3
   3  -9   3 17995.5 613.773   4
   3  -9   4 6370.30 338.563   4
   3  -9   4 6278.94 376.075   3
   3   9   4 7096.84 419.019  14
   3  -9   4 6618.66 226.880  11
   3  -9   4 6774.53 430.672   9
   3  -9   4 7163.95 340.029  10
   3  -9   4 5612.70 588.085   7
   3   9   4 6850.70 361.043   7
   3  -9   4 6350.52 245.596   6
   3  -9   5 59220.6 1435.90   4
   3  -9   5 58692.4 1569.66   3
   3   9   5 64298.2 1654.97  14
   3  -9   5 60989.1 1231.29  11
   3   9   5 59293.6 2592.31   1
   3  -9   5 61416.5 1671.91   9
   3  -9   5 64518.4 1417.98  10
   3   9   5 62469.1 1508.87   7
   3  -9   5 62416.8 1261.31   6
   3  -9   6 9645.34 443.119   4
   3  -9   6 9287.89 533.299   3
   3  -9   6 9991.49 334.310  11
   3  -9   6 9947.80 588.744   9
   3  -9   6 9960.81 417.294  10
   3   9   6 9994.88 577.947  14
   3  -9   6 8649.11 813.700   7
   3  -9   6 10197.3 346.922   6
   3  -9   7 11099.5 490.080   4
   3  -9   7 11086.5 662.770   9
   3   9   7 11951.6 667.760  14
   3  -9   7 9868.55 936.917   7
   3  -9   8 3627.42 396.742   9
   3  -9   8 2752.13 542.992   7
   3   9   8 4009.79 344.695   7
   3  -9   9 10813.6 715.579   9
   3   9   9 10688.9 604.629   7
   3  -9  10 1735.12 311.011   9
   3  -9  10 822.668 344.032   7
   3   9  10 1572.22 255.159   7
   3   9  11 11435.5 744.997   7
   3  -9  11 10413.9 754.645   9
   3  -9  11 9938.91 713.355   3
   3  -9  12 566.671 384.903   7
   3   9  12 1754.32 326.035   7
   3  -9  12 1265.90 273.589   9
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   3   9  12 145.962 186.797   4
   3  -9  13 2157.07 603.693   7
   3  -9  13 2727.29 391.846   3
   3  11 -13 12030.5 608.991   2
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   3  11 -11 931.488 164.731   2
   3 -11 -11 808.127 202.669   5
   3  11 -10 2388.36 249.525   2
   3 -11 -10 1776.38 297.330   5
   3 -11  -9 4102.06 389.055  10
   3 -11  -9 4214.26 431.850   5
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   3 -11  -8 60.4867 97.8930  10
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   3  11  -8 193.695 92.4394   2
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   3 -11  -7 3502.84 344.335  10
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   3  11  -7 3861.92 274.987   2
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   3 -11  -6 15775.0 742.243  10
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   3 -11  -5 12876.1 623.468  10
   3 -11  -5 12968.1 667.122   5
   3  11  -5 12969.4 488.799   2
   3 -11  -5 11032.1 614.934   3
   3  11  -4 1664.96 148.889  13
   3 -11  -4 1721.26 176.250   9
   3 -11  -4 1471.77 202.538  10
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   3  11  -4 1846.46 164.628   2
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   3 -11  -3 71573.3 1829.66   5
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   3 -11  -3 72504.0 1583.64   3
   3 -11  -3 68551.4 1745.63  10
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   3 -11  -2 34737.5 1047.66  10
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   3 -11  -2 36168.2 1108.49   5
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   3 -11  -1 21758.0 750.512  10
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   3 -11  -1 21480.2 778.665   5
   3 -11   0 24894.1 818.523   9
   3 -11   0 26610.0 832.920  10
   3 -11   0 24005.5 816.449   4
   3 -11   0 25762.7 849.855   5
   3 -11   0 26376.4 730.566   3
   3 -11   1 32620.3 946.838  10
   3 -11   1 31524.2 978.960   9
   3 -11   1 30448.1 925.713   4
   3 -11   1 30302.5 701.665  11
   3 -11   1 33183.8 871.960   3
   3 -11   2 639.718 112.675   3
   3  11   2 572.553 112.234   7
   3 -11   2 535.350 61.7274  11
   3 -11   2 437.899 95.7039   5
   3 -11   2 614.739 119.722  10
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   4   0  -2 224930. 4260.95   1
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   4   0  -1 29.3564 24.1349   4
   4   0  -1 32.0025 41.2374   1
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   4   0   0 244348. 4149.44   9
   4   0   0 214160. 4582.84   1
   4   0   0 233038. 4244.70   4
   4   0   0 226193. 4072.69   7
   4   0   1 56.1818 57.3047   1
   4   0   1 79.7748 31.0850   7
   4   0   1 247.065 44.3831   9
   4   0   1 132.882 67.0217   4
   4   0   2 67072.9 1266.41   9
   4   0   2 63848.2 1873.19   1
   4   0   3 16.1657 31.0578   1
   4   0   3 32.4633 28.8735   9
   4   0   3 95.6529 92.8046   4
   4   0   4 272489. 4418.81   9
   4   0   4 264520. 5465.83   1
   4   0   5 235.073 117.369   1
   4   0   5 28.4803 20.5753   6
   4   0   5 13.8841 56.8217   7
   4   0   5 55.7067 37.8024   9
   4   0   5 48.1293 110.309   4
   4   0   6 15143.9 419.105   6
   4   0   6 15805.3 532.493   9
   4   0   6 14946.2 597.645   7
   4   0   6 13688.9 946.176   1
   4   0   7 15.9891 60.6396   1
   4   0   7 116.223 40.3028   6
   4   0   7 26.2473 89.7609   7
   4   0   7-9.30986 37.9748   9
   4   0   7-58.2515 127.942   4
   4   0   8 5014.28 407.463   7
   4   0   8 4374.82 227.462   6
   4   0   8 3830.88 423.528   4
   4   0   9-32.6845 75.1627   4
   4   0   9 12.2149 127.519   7
   4   0  10 25348.3 1213.65   7
   4   0  10 24711.4 1080.95   4
   4   0  11-13.0877 128.631   7
   4   0  12 1239.79 332.914   7
   4   0  13 360.019 239.537   7
   4   2 -14 3060.62 271.620   2
   4   2 -13 4843.52 335.557   2
   4   2 -12 7333.79 403.689   2
   4  -2 -12 7360.61 377.585   2
   4   2 -11 1756.45 187.796   2
   4  -2 -11 1663.55 166.104   2
   4   2 -10-4.19301 56.8399   2
   4  -2 -10 55.7750 44.1196   2
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   4   2  -9 9671.50 408.453   2
   4  -2  -9 9970.86 384.217   2
   4  -2  -8 626.406 130.710   5
   4   2  -8 766.528 106.920   2
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   4   2  -7 5910.28 272.897   2
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   4  -2  -6 4493.30 298.170   5
   4  -2  -6 4607.51 306.260  10
   4   2  -6 5264.85 239.784   2
   4  -2  -6 4828.98 205.490   2
   4  -2  -5 31995.5 928.702   5
   4  -2  -5 33190.1 939.138  10
   4   2  -5 35176.5 791.315   2
   4  -2  -5 35472.3 741.843   2
   4  -2  -4 1498.48 155.714   5
   4  -2  -4 1479.37 151.371  10
   4   2  -4 1606.36 109.800   2
   4  -2  -4 1717.17 92.5482   2
   4   2  -4 1517.74 111.070   1
   4  -2  -3 105541. 2196.57   5
   4   2  -3 106313. 2013.68   2
   4   2  -3 106145. 2220.79   1
   4  -2  -3 105832. 2176.57  10
   4  -2  -2 61711.4 1310.98   9
   4  -2  -2 62497.3 1335.73  10
   4  -2  -2 65323.6 1244.60   4
   4   2  -2 61687.3 1179.75   4
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   4  -2  -2 60663.4 1357.84   5
   4  -2  -1 31845.3 693.625   9
   4  -2  -1 33845.8 706.355  10
   4  -2  -1 34604.6 658.343   4
   4  -2  -1 32617.6 961.050   1
   4   2  -1 31348.0 978.649   1
   4  -2  -1 33287.3 735.749   5
   4  -2   0 5557.35 248.747   5
   4  -2   0 6892.35 207.027   7
   4  -2   0 5301.70 236.342   9
   4  -2   0 5405.00 224.884  10
   4  -2   0 5064.75 378.080   1
   4   2   0 5091.66 402.685   1
   4  -2   0 5622.22 237.941   4
   4  -2   0 5375.76 153.820   3
   4  -2   1 6186.98 246.393   5
   4  -2   1 5458.68 240.671   9
   4   2   1 6145.55 204.859   9
   4  -2   1 5812.13 213.810  10
   4   2   1 5548.19 227.433   7
   4  -2   1 6364.94 227.449   7
   4  -2   1 5425.76 431.044   1
   4   2   1 5505.44 454.916   1
   4  -2   1 5380.03 258.042   4
   4  -2   2 6787.54 282.453   9
   4   2   2 7387.39 223.897   9
   4  -2   2 7304.22 219.130  10
   4   2   2 7076.73 280.103   7
   4  -2   2 7555.27 285.408   7
   4  -2   2 7037.90 526.696   1
   4   2   2 6238.68 518.499   1
   4  -2   2 6713.49 327.388   4
   4  -2   3 38822.6 946.548   9
   4  -2   3 38774.3 732.150   6
   4  -2   3 40374.9 960.902   7
   4   2   3 41618.1 973.183   7
   4  -2   3 40324.2 1081.21   4
   4   2   3 39795.0 1525.87   1
   4  -2   3 41023.2 1486.03   1
   4  -2   4 5589.21 533.031   1
   4   2   4 5847.83 569.569   1
   4  -2   4 5905.61 175.810   6
   4   2   4 6445.47 227.424   9
   4  -2   4 5944.46 298.720   9
   4  -2   4 6763.54 327.710   7
   4  -2   4 6057.46 375.496   4
   4   2   5 55.3476 56.6254   1
   4  -2   5 32.6440 47.5911   1
   4  -2   5 200.342 33.4108   6
   4  -2   5 25.4933 58.4938   7
   4   2   5 117.434 71.3105   7
   4  -2   5 82.0756 55.1382   9
   4   2   5 85.4419 34.8320   9
   4  -2   5 161.853 97.7747   4
   4   2   6 973.781 250.331   1
   4  -2   6 1136.15 262.763   1
   4   2   6 1373.93 122.088   9
   4  -2   6 1207.65 155.036   9
   4  -2   6 1401.47 97.6328   6
   4   2   6 1372.57 177.436   7
   4  -2   6 1344.37 190.365   7
   4  -2   6 1308.05 199.304   4
   4   2   7 1738.37 358.591   1
   4  -2   7 1468.01 314.125   1
   4  -2   7 1880.08 124.405   6
   4  -2   7 1641.50 245.414   7
   4  -2   7 2058.55 213.198   9
   4   2   7 1577.41 208.204   7
   4  -2   7 1983.10 247.277   4
   4   2   8 642.466 93.7070   6
   4  -2   8 766.321 193.282   7
   4   2   8 871.343 175.225   7
   4  -2   8 643.665 133.318   9
   4  -2   8 627.127 154.561   4
   4   2   8 215.801 183.630   4
   4   2   9 10805.3 641.617   7
   4  -2   9 10559.7 741.862   7
   4  -2   9 10957.8 566.375   9
   4  -2   9 10517.5 590.665   4
   4   2  10 13455.4 891.899   4
   4  -2  10 15369.6 728.471   4
   4  -2  10 12546.7 904.771   7
   4   2  10 13921.9 822.921   7
   4  -2  11 2958.89 501.915   7
   4   2  11 4061.76 474.868   4
   4   2  11 3703.37 471.706   7
   4  -2  12 827.467 341.007   7
   4   2  12 1212.68 307.642   7
   4  -2  13 4049.77 700.606   7
   4   2  13 3736.64 582.264   7
   4   4 -14 5363.45 370.844   2
   4   4 -13 2321.43 236.470   2
   4   4 -12 82.2410 82.9634   2
   4   4 -11 8519.53 436.333   2
   4  -4 -11 9047.62 386.590   2
   4   4 -10 1937.76 195.552   2
   4  -4 -10 2081.81 167.435   2
   4  -4 -10 2056.62 251.047   5
   4   4  -9 23036.0 708.567   2
   4  -4  -9 22413.6 621.069   2
   4  -4  -9 20941.9 830.321   5
   4   4  -8 50040.3 1179.48   2
   4  -4  -8 49705.8 1074.33   2
   4  -4  -7 1577.04 192.850  10
   4   4  -7 1902.45 161.625   2
   4  -4  -7 1997.25 128.433   2
   4   4  -7 2016.79 144.097  13
   4  -4  -7 1547.89 197.112   5
   4  -4  -6 998.225 150.781  10
   4   4  -6 530.713 100.206   1
   4   4  -6 713.611 96.1740   2
   4  -4  -6 1074.59 83.4888   2
   4   4  -6 772.230 87.2427  13
   4  -4  -6 769.586 141.552   5
   4  -4  -5 39277.2 1120.01   5
   4   4  -5 47219.2 1205.24   1
   4   4  -5 44321.9 971.071   2
   4  -4  -5 43014.3 859.226   2
   4  -4  -5 39709.3 1101.81  10
   4  -4  -4 3802.94 266.843   5
   4  -4  -4 4080.38 134.935   2
   4   4  -4 4028.42 194.103   2
   4  -4  -4 3771.55 253.230  10
   4  -4  -3 6150.40 272.860   4
   4  -4  -3 6034.44 319.961   5
   4   4  -3 5556.79 223.058   2
   4  -4  -3 6129.71 287.610   9
   4  -4  -3 5671.23 298.024  10
   4  -4  -2 368207. 6641.54  10
   4  -4  -2 371322. 6599.21   9
   4  -4  -2 372062. 6561.89   4
   4  -4  -2 364540. 6676.77   5
   4  -4  -2 387073. 6434.72   3
   4  -4  -1 2821.95 184.697  10
   4  -4  -1 2714.34 176.868   9
   4  -4  -1 2788.29 196.961   5
   4  -4  -1 2570.25 106.704   3
   4  -4  -1 2772.94 168.615   4
   4   4   0 18230.1 458.626  14
   4  -4   0 17985.7 537.240   5
   4  -4   0 16888.1 515.952   9
   4  -4   0 17889.9 505.282  10
   4  -4   0 18180.1 475.798   7
   4  -4   0 19012.1 522.914   4
   4  -4   0 17433.7 413.777   3
   4  -4   1 87497.7 1692.38   3
   4  -4   1 85414.8 1766.67   4
   4   4   1 89828.7 1736.28  14
   4  -4   1 89380.1 1752.85   5
   4   4   1 86621.4 2464.49   1
   4  -4   1 86199.0 2359.16   1
   4  -4   1 86033.6 1789.31   9
   4  -4   1 88566.4 1716.76  10
   4  -4   1 93793.3 1760.66   7
   4   4   1 84745.6 1741.12   7
   4  -4   2 77260.7 1597.72   4
   4  -4   2 78696.8 2228.63   1
   4   4   2 79741.9 2356.24   1
   4   4   2 78144.5 1589.07  14
   4  -4   2 81336.1 1495.90   5
   4  -4   2 76423.1 1611.14   9
   4  -4   2 78243.7 1484.61  10
   4  -4   2 83428.6 1621.68   7
   4  -4   2 71213.8 1332.26   6
   4   4   2 76734.9 1557.69   7
   4  -4   3 9601.25 400.748   4
   4   4   3 10306.4 412.459  14
   4  -4   3 9970.66 247.960  11
   4  -4   3 9939.85 414.429   9
   4  -4   3 10170.2 302.786  10
   4   4   3 9475.61 377.516   7
   4  -4   3 9375.49 221.784   6
   4  -4   3 10583.9 434.051   7
   4  -4   3 10032.4 709.040   1
   4   4   3 9886.42 754.914   1
   4  -4   4 85699.4 2568.25   1
   4   4   4 83667.6 2684.35   1
   4  -4   4 87305.0 1611.16  10
   4  -4   4 88329.3 1887.98   9
   4   4   4 92670.5 1870.69   7
   4  -4   4 83001.7 1551.25   6
   4  -4   4 91165.4 1965.13   7
   4  -4   4 84715.0 1868.27   4
   4  -4   5 17737.6 1049.02   1
   4   4   5 16825.7 1100.38   1
   4  -4   5 16960.6 638.353   9
   4  -4   5 16802.8 401.806   6
   4  -4   5 17081.2 700.073   7
   4  -4   5 15949.9 616.287   4
   4   4   6 3390.41 501.985   1
   4  -4   6 3529.20 476.921   1
   4  -4   6 3928.46 163.135   6
   4   4   6 4373.19 316.220   7
   4  -4   6 3768.21 299.898   9
   4  -4   6 3932.06 355.554   7
   4  -4   6 3635.96 283.594   4
   4   4   7 24783.4 1475.43   1
   4   4   7 26277.1 898.831   7
   4  -4   7 25730.7 689.400  11
   4  -4   7 25579.2 1078.96   7
   4  -4   7 25711.7 873.611   4
   4  -4   7 27398.7 936.591   9
   4  -4   8 3372.11 218.945  11
   4  -4   8 3800.29 339.586   9
   4  -4   8 3961.53 468.741   7
   4   4   8 3597.96 322.713   7
   4  -4   8 3267.38 289.269   4
   4  -4   9 1518.29 327.807   7
   4   4   9 1148.32 211.761   7
   4  -4   9 1195.67 139.358  11
   4  -4   9 1311.03 189.776   4
   4  -4   9 1195.84 203.272   9
   4   4   9 1109.18 137.765   6
   4   4  10 12487.5 736.702   7
   4  -4  10 10800.4 904.105   7
   4  -4  10 12115.5 675.663   9
   4  -4  11 1019.25 364.843   7
   4   4  11 1027.12 253.201   7
   4   4  11 797.811 272.525   4
   4  -4  12 1971.95 530.051   7
   4   4  12 2555.39 436.686   7
   4  -4  13 2487.15 577.923   7
   4   4  13 2486.36 484.491   7
   4   6 -14 10920.4 557.618   2
   4   6 -13 6402.26 410.599   2
   4   6 -12 5685.28 377.497   2
   4   6 -11 8278.48 440.922   2
   4   6 -10 2987.43 250.194   2
   4  -6 -10 2692.02 298.642   5
   4   6  -9 24266.8 750.800   2
   4  -6  -9 23073.8 890.676  10
   4  -6  -8 6736.73 439.967  10
   4   6  -8 7772.93 370.738   2
   4   6  -8 7603.45 326.959  13
   4  -6  -8 6125.40 438.224   5
   4  -6  -7 10108.0 525.240  10
   4   6  -7 11845.8 407.747  13
   4   6  -7 11605.2 443.715   2
   4  -6  -7 11475.8 329.161   2
   4  -6  -7 10264.3 549.801   5
   4  -6  -6 2723.13 250.755  10
   4   6  -6 3110.81 185.747  13
   4   6  -6 3378.05 333.979   1
   4   6  -6 3130.03 206.638   2
   4  -6  -6 3072.37 131.854   2
   4  -6  -6 2744.21 263.000   5
   4  -6  -5 28517.1 921.548  10
   4   6  -5 34317.8 775.229  13
   4  -6  -5 32639.9 632.894   2
   4   6  -5 31950.9 799.719   2
   4  -6  -5 29610.1 962.168   5
   4  -6  -4 6959.97 363.747  10
   4  -6  -4 7173.60 386.813   5
   4   6  -4 7382.58 281.054   2
   4  -6  -3 38328.2 1042.45  10
   4  -6  -3 40992.4 1001.41   9
   4  -6  -3 38177.9 1075.14   5
   4  -6  -3 42589.7 1024.27   4
   4  -6  -3 43550.2 928.982   3
   4   6  -3 38765.4 895.498   2
   4  -6  -2 265519. 4959.74   4
   4  -6  -2 266589. 5060.25   5
   4  -6  -2 276714. 4789.52   3
   4  -6  -2 275711. 5010.85  10
   4  -6  -2 265564. 4962.49   9
   4  -6  -1 9791.93 379.440   4
   4  -6  -1 10110.7 418.428   5
   4  -6  -1 9582.65 286.847   3
   4  -6  -1 9761.06 387.688  10
   4  -6  -1 9325.61 379.459   9
   4  -6   0 12442.1 451.024   5
   4  -6   0 11887.7 341.341   3
   4  -6   0 11896.6 425.772   4
   4  -6   0 12319.4 421.917  10
   4  -6   0 11070.5 426.870   9
   4  -6   1 67101.0 1418.62   5
   4  -6   1 65158.2 1388.66  10
   4  -6   1 63520.0 1452.38   9
   4  -6   1 64645.6 1423.23   4
   4  -6   1 68928.4 1354.44   3
   4  -6   2 15624.6 516.744   4
   4  -6   2 15279.9 489.302   3
   4   6   2 15921.3 525.696  14
   4  -6   2 14238.5 293.696  11
   4  -6   2 14944.7 459.527   5
   4  -6   2 16122.8 468.659  10
   4  -6   2 15362.4 549.588   9
   4  -6   2 14589.1 617.892   7
   4  -6   2 14468.7 339.799   6
   4   6   2 15389.8 504.679   7
   4  -6   3 40836.9 1030.51   4
   4   6   3 42966.4 1826.88   1
   4   6   3 42916.0 1086.03  14
   4  -6   3 40842.0 780.882  11
   4  -6   3 43372.8 874.708   5
   4  -6   3 43518.3 948.624  10
   4  -6   3 41760.8 1103.57   9
   4  -6   3 39590.2 1203.13   7
   4   6   3 42342.1 1030.94   7
   4  -6   3 39607.1 802.172   6
   4  -6   4 27503.9 807.886   4
   4   6   4 30437.4 903.402  14
   4  -6   4 28280.1 597.453  11
   4   6   4 29571.0 1526.13   1
   4  -6   4 29033.7 706.317  10
   4  -6   4 29040.5 897.529   9
   4  -6   4 27709.9 1018.33   7
   4   6   4 29299.2 830.467   7
   4  -6   4 27081.9 589.879   6
   4  -6   5 9955.43 443.907   4
   4   6   5 10315.7 511.582  14
   4  -6   5 10609.3 310.676  11
   4   6   5 11225.4 498.834   7
   4  -6   5 9821.21 282.745   6
   4  -6   5 10244.6 512.259   9
   4  -6   5 10074.0 341.663  10
   4  -6   5 9934.72 612.794   7
   4   6   5 9162.65 865.523   1
   4  -6   6 1870.37 127.801  11
   4  -6   6 1537.29 280.638   7
   4  -6   6 1757.23 225.716   9
   4   6   6 1393.11 350.549   1
   4  -6   6 1385.32 171.296   4
   4  -6   7 3411.28 331.427   9
   4  -6   7 3549.35 196.384  11
   4  -6   7 3318.03 267.388   4
   4  -6   7 2461.37 383.775   7
   4   6   7 3299.22 298.729   7
   4  -6   8 283.250 212.568   7
   4   6   8 120.867 94.4558   7
   4  -6   8 154.251 107.918   9
   4  -6   8 175.516 81.5112   4
   4   6   9 28523.4 1063.55   7
   4  -6   9 28205.8 1120.49   9
   4   6  10 28762.3 1103.84   7
   4  -6  10 27870.4 1110.14   9
   4  -6  11 971.820 363.386   7
   4   6  11 1068.60 243.362   7
   4   6  11 864.431 302.298   4
   4  -6  12 1699.34 505.354   7
   4   6  12 2288.80 396.025   7
   4   6  12 1623.21 373.850   4
   4  -6  13 1175.72 431.657   7
   4   6  13 837.488 283.340   7
   4   8 -14 3739.58 321.926   2
   4   8 -13 2967.90 285.808   2
   4   8 -12 1381.91 199.661   2
   4  -8 -11 6840.10 523.997   5
   4   8 -11 7860.13 442.860   2
   4  -8 -10 1274.85 220.117   5
   4  -8 -10 1934.90 267.115  10
   4   8 -10 1986.77 215.342   2
   4   8  -9 38398.3 1052.82   2
   4  -8  -9 37047.5 1228.14  10
   4  -8  -8 17.4605 74.0767  10
   4   8  -8 101.356 67.2633  13
   4   8  -8 129.094 85.1032   2
   4  -8  -8-29.9726 84.2005   5
   4  -8  -7 15975.4 713.741  10
   4   8  -7 17735.5 604.274   2
   4  -8  -7 16138.7 753.759   5
   4  -8  -6 14151.3 641.159  10
   4   8  -6 15606.3 495.498  13
   4   8  -6 17026.6 934.148   1
   4   8  -6 15181.2 524.453   2
   4  -8  -6 13584.0 660.406   5
   4   8  -5 19045.1 537.956  13
   4   8  -5 18069.3 559.649   2
   4  -8  -5 16924.1 715.213   5
   4  -8  -4 2526.19 206.423   9
   4  -8  -4 2033.44 215.038  10
   4  -8  -4 2624.37 263.609   5
   4  -8  -4 1910.86 191.214   3
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   5   1 -14 997.666 150.750   2
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   5  -3   2 271679. 4755.67   7
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   5  -3   4 24615.2 745.878   7
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   5   3   9 3239.55 351.568   7
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   5   3   9 1824.00 394.433   4
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   5  -3  10 7097.50 712.055   7
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   5   3  10 6725.14 687.951   4
   5   3  11 1025.21 265.055   4
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   5  -3  12 3257.15 616.959   7
   5   3  12 3476.21 503.702   7
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   5   3  13 4110.47 631.042   7
   5   5 -14 1061.41 168.753   2
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   5  -5  -9 1489.15 230.076   5
   5   5  -9 1721.14 179.569   2
   5  -5  -8 2121.27 252.821   5
   5  -5  -8 2150.19 253.895  10
   5   5  -8 2261.14 193.214   2
   5  -5  -8 2430.43 146.058   2
   5  -5  -7 12876.4 630.926   5
   5  -5  -7 13452.5 627.807  10
   5  -5  -7 16357.8 418.666   2
   5   5  -7 15559.0 521.524   2
   5  -5  -6 15318.6 668.703   5
   5  -5  -6 17697.7 423.522   2
   5   5  -6 19374.9 701.509   1
   5   5  -6 17459.7 540.594   2
   5  -5  -6 15662.9 653.501  10
   5  -5  -5 37073.9 1104.22   5
   5   5  -5 39908.3 916.889   2
   5  -5  -5 36564.2 1068.47  10
   5  -5  -4 5507.07 347.088   5
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   5  -5  -3 10266.8 411.376   9
   5  -5  -3 9604.05 426.795  10
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   6   2   4 1315.21 111.284   9
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   6  -2   4 1146.00 146.703   7
   6  -2   4 1119.56 181.771   4
   6  -2   5 32102.2 1581.74   1
   6   2   5 31452.9 1630.46   1
   6  -2   5 31871.0 896.916   9
   6   2   5 32426.2 744.722   9
   6  -2   5 31613.8 935.497   7
   6  -2   5 29584.0 1024.63   4
   6   2   5 35231.1 1002.93   7
   6   2   6 815.889 291.801   1
   6  -2   6 746.959 247.655   1
   6  -2   6 822.133 157.889   7
   6   2   6 901.993 163.000   7
   6  -2   6 806.572 134.010   9
   6  -2   6 956.000 187.738   4
   6   2   6 131.448 161.372   4
   6  -2   7 4781.05 334.663   9
   6   2   7 4563.44 364.020   7
   6  -2   7 3986.87 370.372   7
   6  -2   7 3715.83 362.337   4
   6   2   8 6954.72 486.972   7
   6  -2   8 6385.57 524.111   7
   6  -2   8 7047.57 430.109   9
   6  -2   8 6681.85 493.362   4
   6   2   9 2103.33 303.091   7
   6   2   9 1837.79 360.989   4
   6  -2   9 2191.01 287.304   4
   6  -2   9 2308.85 364.289   7
   6  -2  10 446.095 149.371   4
   6   2  10 319.745 151.061   4
   6  -2  10 237.745 196.062   7
   6   2  10 495.343 195.571   7
   6   2  11 4471.68 522.963   7
   6  -2  11 4486.57 619.920   7
   6   2  11 4192.64 469.721   4
   6  -2  12 2698.16 523.048   7
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   6  -2  13 4369.53 728.706   7
   6   2  13 5475.51 715.449   7
   6   4 -14 112.581 67.6712   2
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   6  -4  -3 102600. 2211.97   9
   6  -4  -3 104947. 2256.13  10
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   6  -4   0 78073.9 1652.51   4
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   6  -4   0 73771.8 2246.08   1
   6   4   0 75005.4 2351.39   1
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   6  -4   1 5346.68 282.423   5
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   6   4   2 6899.60 670.006   1
   6  -4   2 7315.51 360.731   9
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   6  -4   2 8197.23 342.424   7
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   6  -4   3 16027.7 1022.05   1
   6   4   3 17469.8 1134.34   1
   6   4   3 16286.3 574.017   7
   6  -4   3 16636.0 602.835   9
   6  -4   3 16708.6 462.496  10
   6  -4   3 17522.1 592.441   7
   6  -4   3 16554.2 620.576   4
   6  -4   4 14924.7 1018.80   1
   6   4   4 14249.7 1071.00   1
   6  -4   4 13399.6 335.054  11
   6  -4   4 13936.8 564.551   9
   6   4   4 15221.1 581.834   7
   6  -4   4 14681.0 587.003   7
   6  -4   4 13556.5 580.172   4
   6  -4   5 2984.02 478.905   1
   6   4   5 3246.68 530.082   1
   6  -4   5 2951.77 260.282   9
   6   4   5 4569.93 381.535   7
   6  -4   5 3427.29 300.890   7
   6  -4   5 3343.44 286.736   4
   6  -4   6 32275.3 1044.35   9
   6  -4   6 31929.8 1134.04   7
   6  -4   6 32951.1 1072.99   4
   6  -4   7 9471.60 522.980   9
   6   4   7 9435.35 531.053   7
   6  -4   7 8616.61 593.439   7
   6  -4   7 8076.05 491.396   4
   6  -4   8 15951.9 728.967   9
   6   4   8 15559.5 734.076   7
   6  -4   8 14500.0 868.486   7
   6  -4   8 14446.9 687.486   4
   6   4   9 42319.8 1397.69   7
   6  -4   9 42099.4 1333.56   9
   6  -4   9 39775.9 1283.24   4
   6   4  10 7183.95 577.274   7
   6  -4  10 5438.73 657.616   7
   6  -4  10 6832.49 474.756   4
   6   4  10 5058.90 633.741   4
   6   4  11 1408.52 308.871   4
   6  -4  11 1599.34 434.279   7
   6   4  11 1914.13 340.795   7
   6  -4  12 3831.64 673.383   7
   6   4  12 3989.80 526.555   7
   6   6 -14 125.264 67.0394   2
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   6   6 -12 22815.7 816.272   2
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   6  -6 -10 28500.0 1126.22   5
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   6  -6  -9 11455.2 653.543   5
   6   6  -9 12853.8 517.749   2
   6  -6  -9 11641.6 650.517  10
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   6  -6  -7 28554.3 1043.72   5
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   6  -6   2 72239.9 1720.37   7
   6   6   2 77779.5 2697.59   1
   6  -6   3 21944.8 734.681   4
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   6  -6   3 22776.6 823.934   7
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   6  -6   4 23064.3 894.133   7
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   6  -6   5 31596.9 1037.89   9
   6  -6   5 31095.3 1161.98   7
   6  -6   5 28600.3 948.593   4
   6  -6   6 11624.0 609.883   9
   6  -6   6 10099.4 523.990   4
   6  -6   6 10875.1 704.102   7
   6  -6   7 1313.60 294.468   7
   6   6   7 1617.65 242.487   7
   6  -6   7 1482.57 237.158   9
   6  -6   7 1149.23 180.909   4
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   6  -6   9 2088.30 294.212   9
   6  -6   9 1596.83 218.118   4
   6  -6   9 1394.74 365.057   7
   6   6   9 1540.07 257.081   7
   6   6  10 329.961 216.829   4
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   6  -6  11 7029.66 884.560   7
   6   6  11 8570.35 684.609   7
   6   6  11 6302.34 741.866   4
   6   6  12 8974.50 767.952   7
   6   6  12 7984.27 756.511   4
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   6  -8  -8 10694.4 645.177   5
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   6  -8  -7 15536.9 769.445   5
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   6  -8  -6 168.730 128.211   5
   6   8  -6 390.150 98.1998   2
   6  -8  -6 142.582 96.8813  10
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   6  -8  -5 62509.5 1695.73   5
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   6  -8  -2 7346.21 429.916   5
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   6  -8   0 24481.4 797.384   9
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   6  -8   0 24090.9 759.038   4
   6   8   1 9415.13 412.067  14
   6  -8   1 10138.5 454.979   5
   6  -8   1 9377.17 469.545   9
   6  -8   1 9721.47 432.881  10
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   6  -8   2 4177.66 244.793   3
   6  -8   2 3754.62 276.554   4
   6   8   2 4063.48 280.709  14
   6  -8   2 4250.23 266.650   5
   6  -8   2 4329.49 272.443  10
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   6   8   2 4278.22 291.587   7
   6  -8   2 3463.28 359.054   7
   6   8   2 3543.96 558.961   1
   6  -8   3 2710.41 240.128   4
   6  -8   3 2645.04 217.109   3
   6   8   3 2718.36 501.822   1
   6  -8   3 2939.20 218.606  10
   6  -8   3 2612.83 267.480   9
   6   8   3 3218.11 270.215  14
   6  -8   3 2489.73 321.610   7
   6   8   3 2714.79 242.668   7
   6  -8   4 17368.2 671.491   4
   6  -8   4 17413.0 661.093   3
   6  -8   4 18807.6 601.636  10
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   6  -8   4 15824.5 881.049   7
   6   8   4 17582.5 683.736   7
   6  -8   5 8703.15 532.672   9
   6   8   5 9150.04 497.341   7
   6  -8   5 7593.83 644.404   7
   6  -8   5 8551.97 459.862   4
   6  -8   5 7882.64 455.323   3
   6  -8   6 3167.94 345.480   9
   6  -8   6 2588.24 416.341   7
   6  -8   6 2944.77 276.835   4
   6  -8   7 27647.0 1105.49   9
   6  -8   7 26190.8 928.534   4
   6  -8   8 7824.90 579.036   9
   6   8   8 8499.16 561.950   7
   6  -8   8 6308.66 737.707   7
   6  -8   8 7472.77 464.573   4
   6  -8   9 17049.7 904.987   9
   6   8   9 16989.8 848.984   7
   6  -8  10 600.592 187.245   9
   6  -8  10 477.541 263.616   7
   6   8  10 589.252 196.394   7
   6   8  11 853.801 335.620   4
   6  -8  11 708.865 323.103   7
   6   8  11 1120.94 263.645   7
   6   8  12 495.206 173.438   7
   6   8  12 737.745 297.361   4
   6  -8  12 328.047 139.187   3
   6 -10 -12 7183.93 590.322   5
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   6 -10 -11 4450.15 460.095   5
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   6 -10 -10 5851.39 522.746   5
   6 -10 -10 6274.72 513.408  10
   6  10 -10 6421.37 401.876   2
   6 -10  -9 39521.5 1472.29   5
   6 -10  -9 40558.3 1429.48  10
   6 -10  -8 1481.99 277.767   5
   6  10  -8 1902.68 211.345   2
   6 -10  -8 1797.47 275.902  10
   6 -10  -7 4504.57 401.721  10
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   6 -10  -4 9852.53 554.092  10
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   6 -10  -4 10924.5 466.784   3
   6 -10  -4 10434.7 591.907   5
   6 -10  -3 8778.38 502.504  10
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   6 -10  -3 9283.93 355.771   3
   6 -10  -3 9313.44 539.517   5
   6 -10  -3 9684.15 490.115   4
   6 -10  -2 11016.8 523.193   9
   6 -10  -2 10897.3 546.184  10
   6 -10  -2 11315.3 388.714   3
   6 -10  -2 11645.8 535.326   4
   6 -10  -2 11178.3 578.417   5
   6 -10  -1 10493.2 515.583  10
   6 -10  -1 9362.23 485.959   9
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   6 -10  -1 9966.62 527.186   5
   6 -10  -1 10488.1 501.952   4
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   6 -10   0 20257.4 766.767   9
   6 -10   0 21034.3 596.716   3
   6 -10   0 20403.2 739.722   4
   6 -10   0 21746.9 797.604   5
   6 -10   1 22535.6 776.937   4
   6 -10   1 24255.6 806.757   5
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   6 -10   1 22443.0 827.167   9
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   6 -10   2 5329.40 294.461   3
   6 -10   2 5651.79 360.596   4
   6 -10   2 5546.06 336.700   5
   6 -10   2 5215.07 387.449   9
   6 -10   2 5232.01 337.144  10
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   6 -10   2 4248.84 467.459   7
   6  10   2 5235.79 350.660   7
   6 -10   3 68333.9 1697.10   4
   6 -10   3 69877.4 1623.29   3
   6 -10   3 72616.2 1679.13  10
   6 -10   3 71455.9 1851.03   9
   6  10   3 71425.4 1768.94  14
   6  10   3 70283.3 1723.25   7
   6 -10   4 17853.9 686.982   3
   6 -10   4 17049.2 693.443   4
   6 -10   4 19030.6 671.613  10
   6 -10   4 18343.0 817.791   9
   6  10   4 18505.1 780.154  14
   6  10   4 18810.0 737.793   7
   6 -10   5 23378.9 867.221   3
   6 -10   5 23205.9 846.829   4
   6 -10   5 24181.5 998.773   9
   6  10   5 25590.4 980.581  14
   6 -10   5 21366.5 1293.38   7
   6  10   5 25350.2 916.817   7
   6 -10   6 4906.81 449.568   9
   6  10   6 5725.95 445.936   7
   6 -10   6 3931.49 579.429   7
   6 -10   6 4633.57 352.080   4
   6 -10   6 4500.70 373.704   3
   6 -10   7 3223.15 380.137   9
   6 -10   7 2945.28 327.051   3
   6 -10   7 2866.87 281.083   4
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   6  24  -1 120.767 109.173   7
   7   1 -13 61.2626 59.1614   2
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   7   1 -12 523.615 109.813   2
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   7  -1 -10 4827.54 272.793   2
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   7  -1  -9 23413.8 660.704   2
   7   1  -9 23227.2 683.551   2
   7  -1  -8 6669.89 291.654   2
   7   1  -8 6406.37 304.302   2
   7  -1  -8 5329.78 390.881   5
   7  -1  -7 869.153 97.7244   2
   7   1  -7 1002.99 116.663   2
   7   1  -7 810.465 159.082   5
   7  -1  -7 1084.50 174.818   5
   7   1  -6 1038.95 167.774   5
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   7  -1  -5 14323.9 609.124   5
   7   1  -4 56895.4 1445.42   1
   7  -1  -4 59542.7 1203.16   4
   7   1  -4 59116.5 1132.85   4
   7  -1  -3 46151.1 1199.01  10
   7  -1  -3 42296.9 1194.74   5
   7  -1  -3 45257.9 1363.24   1
   7   1  -3 44359.1 1369.97   1
   7   1  -3 47815.4 975.881   4
   7  -1  -3 47230.5 1016.17   4
   7  -1  -2 127071. 2389.55   7
   7  -1  -2 135128. 2667.21  10
   7  -1  -2 124303. 2693.00   5
   7  -1  -2 130291. 2625.03   9
   7  -1  -2 124096. 3028.30   1
   7   1  -2 118605. 3022.28   1
   7   1  -2 139824. 2505.79   4
   7  -1  -2 138110. 2512.42   4
   7  -1  -1 1458.12 102.617   7
   7   1  -1 1525.43 119.963   7
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   7  -1  -1 1578.01 157.780   9
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   7   1   0 2724.27 169.725   7
   7  -1   0 2830.55 362.907   1
   7   1   0 2681.67 362.087   1
   7   1   0 2632.05 234.859   4
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   7   1   1 55943.7 1217.99   9
   7  -1   1 53815.3 1247.36   9
   7   1   1 50669.3 1189.39   7
   7  -1   1 55892.2 1938.89   1
   7   1   1 51898.2 1905.69   1
   7  -1   1 53110.3 1344.16   4
   7   1   1 50037.4 1466.56   4
   7   1   2 16140.2 508.049   9
   7  -1   2 15292.3 532.284   9
   7   1   2 17134.5 552.587   7
   7  -1   2 16461.4 1018.97   1
   7   1   2 15270.8 1002.92   1
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   7  -1   3 9877.95 410.471   9
   7   1   3 13123.5 536.802   7
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   7   1   3 9014.76 792.494   1
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   7   1   4 22330.9 643.733   9
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   7   1   4 26449.1 827.474   7
   7  -1   4 22932.8 744.384   7
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   7   1   4 21266.8 1320.81   1
   7  -1   4 20133.3 855.655   4
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   7   1   5 4232.34 243.982   9
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   7   1   7 5828.05 427.000   7
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   7   1   8 16382.8 796.655   7
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   7   1   8 13677.0 881.994   4
   7  -1   9 620.286 167.581   4
   7   1   9 684.204 185.502   4
   7  -1   9 764.857 221.835   7
   7   1   9 636.956 189.315   7
   7  -1  10 6571.24 646.038   7
   7   1  10 6792.37 620.965   7
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   7   1  10 5992.02 554.013   4
   7  -1  11 171.002 97.0922   4
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   7  -1  11 77.4289 160.738   7
   7   1  11 417.143 215.970   7
   7  -1  12 1548.28 403.686   7
   7   1  12 1766.46 397.622   7
   7   3 -14 11707.3 550.275   2
   7   3 -13 3204.69 270.717   2
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   7  -3  -9 23777.4 637.383   2
   7   3  -9 22653.6 703.458   2
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   7   3  -8 87101.5 1822.13   2
   7   3  -7 72.2574 50.7471   2
   7  -3  -7 91.7611 98.0088   5
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   7  -3  -2 101613. 2732.99   1
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   7  -3  -2 108549. 2209.51   4
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   7   3   0 8735.28 696.342   1
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   7  -3   0 8446.55 211.485   3
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   7   3   1 5819.10 597.071   1
   7  -3   1 6355.89 595.157   1
   7  -3   1 6197.09 336.149   4
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   7  -3   2 9750.52 383.105   7
   7   3   2 9168.76 397.013   7
   7  -3   2 9332.20 446.797   4
   7   3   2 8984.64 790.321   1
   7  -3   2 8821.60 744.356   1
   7  -3   3 35201.3 1624.04   1
   7   3   3 33492.9 1668.22   1
   7   3   3 35760.8 807.183   9
   7  -3   3 33639.9 959.976   9
   7   3   3 35585.4 966.543   7
   7  -3   3 34454.2 934.207   7
   7  -3   3 33571.9 1033.69   4
   7  -3   4 125291. 3459.67   1
   7   3   4 117568. 3516.31   1
   7  -3   4 118584. 2251.64   9
   7  -3   4 122891. 2274.25   7
   7  -3   4 116113. 2388.03   4
   7  -3   5 15135.8 604.746   9
   7  -3   5 15382.1 640.328   7
   7  -3   5 14323.4 668.149   4
   7  -3   6 8732.02 468.537   9
   7   3   6 9386.34 520.518   7
   7  -3   6 7419.55 492.661   4
   7  -3   6 8261.82 505.393   7
   7  -3   7 1019.00 214.003   7
   7   3   7 1089.19 199.894   7
   7  -3   7 1178.06 185.098   9
   7  -3   7 1242.56 220.527   4
   7   3   7 576.821 224.832   4
   7  -3   8 3488.02 416.107   7
   7   3   8 3799.46 370.872   7
   7  -3   8 3247.27 307.717   9
   7  -3   8 3488.59 355.356   4
   7   3   8 2771.54 444.434   4
   7  -3   9 7715.95 677.362   7
   7   3   9 8382.59 595.613   7
   7  -3   9 7334.05 525.162   4
   7   3   9 7042.51 714.606   4
   7   3  10 10914.1 752.298   7
   7  -3  10 10601.1 883.322   7
   7   3  10 10018.8 805.412   4
   7  -3  10 10787.5 652.451   4
   7   3  11 391.184 152.990   4
   7  -3  11 350.401 227.550   7
   7   3  11 330.886 189.122   7
   7  -3  12 4275.43 699.573   7
   7   3  12 5501.65 644.652   7
   7   5 -13 1120.95 168.565   2
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   7   5 -11 3876.67 292.900   2
   7  -5 -10 71.6096 101.664   5
   7   5 -10 9.63107 62.4010   2
   7  -5  -9 7455.87 518.616   5
   7   5  -9 9083.41 419.195   2
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   7  -5  -8 1845.13 249.183   5
   7   5  -8 2080.33 188.836   2
   7  -5  -7 2738.95 296.963   5
   7   5  -7 3291.69 225.367   2
   7  -5  -7 2831.01 293.191  10
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   7  -5  -5 3366.74 307.265   5
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   7  -5  -4 46367.2 1323.68   5
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   7  -5  -4 44911.8 1275.34  10
   7  -5  -3 83763.5 1897.63   9
   7  -5  -3 85800.4 1946.12  10
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   7   5  -3 84829.4 1737.54   4
   7  -5  -3 83521.5 1990.56   5
   7  -5  -2 146.218 79.4345   5
   7   5  -2 98.8198 71.9459   1
   7  -5  -2 69.6593 69.7486   9
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   7  -5  -2 71.1016 22.2383   3
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   7   5  -2-34.4001 73.0461   4
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   7  -5  -1 7965.43 416.377   5
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   7   5   1 16639.4 1097.69   1
   7  -5   1 16127.9 1010.49   1
   7  -5   1 15547.3 565.743   5
   7  -5   1 16546.3 599.174   9
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   7  -5   1 16885.5 520.906   7
   7  -5   1 15423.0 567.028   4
   7  -5   1 14608.7 421.753   3
   7  -5   2 432.350 75.0980   3
   7  -5   2 782.043 223.614   1
   7   5   2 455.083 187.075   1
   7  -5   2 717.718 103.024  10
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   7  -5   2 566.957 101.886   7
   7  -5   2 654.879 125.558   9
   7  -5   2 558.754 117.431   4
   7  -5   3 11712.6 927.584   1
   7   5   3 11803.5 1001.97   1
   7  -5   3 11416.0 521.805   9
   7  -5   3 11777.3 407.007  10
   7   5   3 11461.5 495.952   7
   7  -5   3 11971.2 515.474   7
   7  -5   3 11620.0 522.817   4
   7  -5   4 5656.01 667.877   1
   7   5   4 5678.99 722.314   1
   7  -5   4 6318.83 390.474   9
   7   5   4 6211.73 379.643   7
   7  -5   4 6209.32 393.890   7
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   7  -5   6 4652.12 421.897   7
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   7  -5   7 7939.23 506.522   9
   7   5   7 8985.18 542.056   7
   7  -5   7 7604.57 604.392   7
   7  -5   7 7801.56 492.977   4
   7  -5   8 4909.29 413.888   9
   7   5   8 5018.71 425.369   7
   7  -5   8 4269.84 503.347   7
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   7   5   9 9506.65 630.256   7
   7  -5   9 9189.43 821.581   7
   7  -5   9 9430.17 599.822   9
   7  -5   9 9819.44 578.023   4
   7   5  10 1013.69 306.763   4
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   7   5  10 1324.59 267.197   7
   7  -5  11 12204.2 1151.40   7
   7   5  11 13458.8 1009.91   4
   7  -5  12 290.194 246.004   7
   7   5  12 577.877 212.642   7
   7   5  12 644.664 226.552   4
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   7  -7  -8 61231.2 1806.49   5
   7  -7  -8 59343.9 1749.25  10
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   7   7  -1 203.388 51.5191  14
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   7   7   1 21378.2 656.717  14
   7  -7   1 21219.6 710.249   5
   7   7   1 21267.9 1349.08   1
   7  -7   1 20596.1 687.534  10
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   7  -7   1 18693.3 725.238   7
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   7  -7   2 53426.3 1369.12   4
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   7   7   2 55034.4 1345.95  14
   7  -7   2 54994.2 1309.62   5
   7  -7   2 55345.9 1322.39  10
   7  -7   2 54832.6 1433.25   9
   7   7   2 52891.8 1354.36   7
   7  -7   2 52866.2 1465.50   7
   7  -7   3 13623.4 517.763   3
   7  -7   3 13568.5 580.745   4
   7   7   3 15556.3 1230.00   1
   7  -7   3 14264.5 519.929  10
   7  -7   3 13694.5 620.008   9
   7   7   3 13998.1 586.884  14
   7  -7   3 14779.3 692.851   7
   7   7   3 14279.2 586.106   7
   7   7   4 64309.5 1622.97   7
   7  -7   4 66845.2 1858.69   7
   7  -7   4 62350.5 1599.38   4
   7  -7   4 63539.9 1548.94   3
   7  -7   4 65995.5 1704.52   9
   7   7   5 6528.56 437.304   7
   7  -7   5 5159.44 481.997   7
   7  -7   5 4973.46 359.853   4
   7  -7   5 6022.59 433.304   9
   7  -7   6 2325.87 354.024   7
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   7  -7   6 2431.22 291.013   9
   7  -7   7 22194.0 1234.28   7
   7  -7   7 24394.2 923.757   4
   7  -7   7 25711.4 1048.50   9
   7  -7   8 2130.38 412.304   7
   7   7   8 2905.27 334.365   7
   7  -7   8 2831.92 293.212   4
   7  -7   8 2676.56 332.400   9
   7   7   9 5230.07 465.488   7
   7  -7   9 4813.18 658.202   7
   7  -7   9 5107.06 402.118   4
   7  -7   9 5422.53 488.573   9
   7   7  10 2138.17 490.262   4
   7  -7  10 1335.99 402.911   7
   7   7  10 1861.53 306.635   7
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   7  -7  11 161.398 140.497   7
   7   7  11 442.273 175.383   7
   7   7  12 712.820 236.663   4
   7  -7  12 1226.61 409.082   7
   7   7  12 1415.70 309.303   7
   7  -9 -12 3282.60 399.400   5
   7  -9 -11 6193.83 541.935   5
   7  -9 -10 99.6199 102.621   5
   7  -9 -10 587.099 201.528  10
   7  -9  -9 1530.26 266.101   5
   7  -9  -9 1517.43 259.708  10
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   7  -9  -6 5916.30 442.664  10
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   7  -9  -5 14194.5 688.704  10
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   7  -9  -4 8079.24 446.509   9
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   7  -9  -4 8589.69 531.332   5
   7  -9  -3 113998. 2594.48  10
   7  -9  -3 111339. 2505.72   9
   7  -9  -3 119135. 2518.24   4
   7  -9  -3 114400. 2650.09   5
   7  -9  -3 116493. 2247.34   3
   7  -9  -2 61534.6 1602.76  10
   7  -9  -2 60192.7 1557.87   9
   7  -9  -2 61677.9 1654.32   5
   7  -9  -2 65714.2 1560.52   4
   7  -9  -2 61588.0 1279.40   3
   7  -9  -1 19798.0 746.918  10
   7  -9  -1 18968.8 731.818   9
   7  -9  -1 20597.5 789.290   5
   7  -9  -1 19769.7 712.375   4
   7  -9  -1 19739.7 530.543   3
   7   9   0 12013.6 461.103  14
   7  -9   0 10741.9 500.988   4
   7  -9   0 11226.3 541.323   5
   7  -9   0 10672.0 512.485  10
   7  -9   0 10177.3 520.844   9
   7  -9   0 10865.4 366.480   3
   7  -9   1 6613.34 288.724   3
   7  -9   1 5923.13 372.290   4
   7   9   1 7062.34 369.571  14
   7  -9   1 6968.40 399.297   5
   7   9   1 6604.31 800.240   1
   7  -9   1 6759.59 390.114  10
   7  -9   1 6359.67 415.468   9
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   7 -21   1 11376.3 600.778   3
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   7 -21   2 1975.46 340.468  10
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   8   2   7 30019.5 1081.77   7
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   8  -2   7 30681.4 1146.16   7
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   8   4   1 23717.8 1345.46   1
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   8  -6   6 15238.4 850.771   7
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   8   6   7 14294.5 732.777   7
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   8  -8  -5 7705.27 523.092   5
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   8  -8  -2 33960.4 1067.21   9
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   8  -8  -1 81050.4 1836.70   4
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   8  -8  -1 77356.6 1879.87  10
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   8   8   0 10115.9 406.686  14
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   8   8   0 8797.18 891.320   1
   8  -8   0 9593.08 482.729  10
   8  -8   0 8540.07 481.440   9
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   8  -8   0 9117.41 307.357   3
   8  -8   0 9379.98 465.361   4
   8  -8   1 18209.3 516.795   3
   8  -8   1 18107.1 694.581   4
   8   8   1 19243.3 642.821  14
   8  -8   1 18435.7 698.830   5
   8   8   1 18448.7 1350.69   1
   8  -8   1 18712.3 691.608  10
   8  -8   1 17903.5 733.515   9
   8  -8   1 17196.8 774.435   7
   8   8   1 18789.3 699.600   7
   8  -8   2 699.778 147.530   4
   8  -8   2 721.453 99.9543   3
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   8  18   7 2412.40 368.949   7
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   9   7   4 42631.0 1279.51   7
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   9  -7   7 85.5836 123.234   7
   9   7   7-90.5266 121.013   7
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   9   7   8 7663.32 577.403   7
   9  -7   9 4822.17 425.136   4
   9   7   9 3873.27 619.473   4
   9  -7   9 4281.78 626.015   7
   9  -7  10 1747.72 295.015   3
   9   7  10 2450.95 468.312   4
   9  -7  10 1999.69 463.583   7
   9   7  10 2582.09 371.061   7
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   9  -9 -11 12608.1 808.395   5
   9  -9 -10 7286.68 606.469   5
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   9  -9  -9 7742.03 613.556   5
   9  -9  -8 3651.99 398.902  10
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   9  -9  -7 11260.4 673.975  10
   9  -9  -7 10017.9 664.595   5
   9  -9  -6 3424.49 365.530  10
   9  -9  -6 4142.62 419.797   5
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  10   0   0 75744.1 1808.39   4
  10   0   1 49.6429 66.1589   9
  10   0   1-78.0203 54.8240   7
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  13 -13   4 8130.39 604.372   4
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  13 -13   5 634.768 162.257   4
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  13 -13   5 496.892 199.747   9
  13 -13   6 3464.26 389.510   4
  13 -13   6 3643.57 473.022   9
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  13 -15  -9 550.813 199.646  10
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  13 -15   1 2395.02 326.356   4
  13 -15   1 1938.24 343.959   9
  13 -15   2 9925.46 675.716   4
  13  15   2 10087.9 706.141   7
  13 -15   2 8929.84 721.838   9
  13  15   3 512.975 181.493   7
  13 -15   3 702.098 196.343   4
  13 -15   3 562.835 206.290   9
  13  15   4 69.2810 94.3339   7
  13 -15   4 376.478 140.470   4
  13 -15   4 305.499 176.053   9
  13 -15   5 3823.80 423.195   4
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  13 -17  -8 2729.60 404.825  10
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  14   2   8 686.318 216.307   4
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  14  -6   5 369.841 138.627   7
  14   6   5 534.136 171.295   7
  14  -6   5 311.900 154.503   4
  14   6   5 580.243 212.155   4
  14  -6   5 870.592 197.439   9
  14  -6   6 23.6868 65.9719   4
  14   6   6 60.1975 138.451   4
  14  -6   6 144.817 95.5096   7
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  14   8   7 506.171 189.694   7
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  14 -10  -1 13059.7 772.880   9
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  14 -10   6 3293.40 385.432   4
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  14 -12   5 782.712 233.442   9
  14 -12   5 819.336 201.611   4
  14  12   5 705.429 285.675   4
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  14 -12   6 9224.66 736.904   9
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  14 -14  -9 4225.20 519.769   5
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  14 -14  -6 7468.04 681.606   5
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  14 -14   1 5976.19 582.345   9
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  14 -14   2 283.575 141.458   4
  14  14   2 308.549 201.375   4
  14 -14   2 373.425 196.192   9
  14 -14   3 6963.28 560.624   4
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  14 -14   3 6162.88 608.669   9
  14  14   4 121.733 114.856   7
  14 -14   4 185.814 122.534   4
  14  14   4 187.243 152.748   4
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  14 -16  -8 4314.32 528.294   5
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  15  -1  -4 26856.7 859.274   4
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  15  -1   4 658.374 205.241   4
  15   1   4 616.674 203.183   4
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  15   1   6 8742.91 701.934   4
  15  -1   6 9218.07 667.258   7
  15   1   6 9497.44 664.143   7
  15  -1   7 610.419 204.588   4
  15   1   7 523.258 189.945   4
  15  -1   7 412.101 176.762   7
  15   1   7 651.047 207.231   7
  15  -1   8 7762.60 703.776   7
  15   1   8 8139.45 691.428   7
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  18  12  -3 1626.70 269.967   7
  18  12  -2 8100.58 610.146   7
  18 -12  -2 8284.44 615.229   4
  18 -12  -1 1238.11 275.266   9
  18  12  -1 1114.38 237.413   7
  18 -12  -1 1261.71 245.460   4
  18  12   0 5602.62 518.672   7
  18 -12   0 5493.58 565.173   9
  18 -12   0 5368.29 497.254   4
  18 -12   1 1302.43 289.259   9
  18  12   1 1994.44 313.566   7
  18 -12   1 1695.66 272.912   4
  18  14  -4 343.890 146.508   7
  18  14  -3 2441.20 349.489   7
  18 -14  -3 3004.95 363.540   4
  18 -14  -2 2239.05 320.404   4
  18  14  -2 2339.60 321.226   7
  19   1  -2 7323.36 486.837   4
  19  -1  -2 7452.71 504.367   4
  19  -1  -1 5393.22 444.628   4
  19   1  -1 5373.50 438.372   4
  19  -1   0 7309.04 539.348   4
  19   1   0 8266.18 564.166   4
  19  -1   1 2658.58 338.771   4
  19   1   1 2573.17 328.324   4
  19  -1   2 1187.35 233.527   4
  19   1   2 1106.63 231.074   4
  19  -1   3 2160.85 327.820   4
  19   1   3 1533.24 273.939   4
  19  -1   4 1001.30 224.795   4
  19   1   4 651.067 192.190   4
  19  -3  -3 301.421 116.536   4
  19  -3  -2 8121.63 539.866   4
  19  -3  -1 801.719 180.334   4
  19   3  -1 1191.00 206.043   4
  19  -3   0 2193.28 297.121   4
  19   3   0 1625.33 253.205   4
  19  -3   1 995.773 212.418   4
  19   3   1 1147.18 226.730   4
  19  -3   2 1173.57 235.829   4
  19   3   2 829.427 197.871   4
  19  -3   3 2666.57 360.333   4
  19   3   3 2526.33 357.072   4
  19   3   3 2917.74 348.236   7
  19  -3   4 5601.21 523.067   4
  19   3   4 6022.08 557.967   4
  19   3   4 5904.36 512.260   7
  19  -5  -3 1549.40 230.053   4
  19  -5  -2 2745.59 316.847   4
  19  -5  -1 12428.2 710.744   4
  19  -5   0 917.684 200.836   4
  19   5   0 1113.66 209.291   4
  19   5   1 4099.46 419.594   4
  19  -5   1 4417.57 445.482   4
  19  -5   2 1562.88 267.238   4
  19   5   2 1105.79 239.727   4
  19   5   2 1667.50 270.759   7
  19  -5   3 5288.95 503.377   4
  19   5   3 5384.86 517.555   4
  19   5   3 5686.66 509.337   7
  19  -7  -4 5582.01 443.574   4
  19  -7  -3 4439.58 404.926   4
  19  -7  -2 7827.92 558.383   4
  19   7  -2 8905.40 581.217   7
  19  -7  -1 897.693 195.250   4
  19   7  -1 961.840 198.193   7
  19  -7   0 1366.08 247.851   4
  19   7   0 1511.25 260.743   7
  19   7   1 2755.74 346.167   4
  19  -7   1 2878.31 359.808   4
  19   7   1 3931.52 495.928   7
  19  -7   2 836.199 206.731   4
  19   7   2 567.034 177.818   4
  19   7   2 1173.11 262.287   7
  19  -7   3 616.779 186.043   4
  19   7   3 549.765 183.593   4
  19   7   3 741.117 205.400   7
  19  -9  -4 952.199 190.166   4
  19  -9  -3 2898.31 337.107   4
  19   9  -3 2981.54 342.148   7
  19  -9  -2 6277.93 507.990   4
  19   9  -2 6410.70 517.213   7
  19  -9  -1 15016.9 835.343   4
  19   9  -1 16384.0 868.422   7
  19  -9   0 1387.81 247.855   4
  19   9   0 1122.96 228.897   7
  19  -9   1 653.509 175.867   4
  19   9   1 1071.62 228.551   7
  19   9   2 6398.41 553.182   4
  19  -9   2 7342.58 586.538   4
  19 -11  -4 3234.06 365.645   4
  19  11  -4 3563.30 380.897   7
  19 -11  -3 1244.15 233.621   4
  19  11  -3 1311.69 239.160   7
  19 -11  -2 5219.09 480.344   4
  19  11  -2 5415.70 489.432   7
  19 -11  -1 333.975 119.816   4
  19  11  -1 132.542 107.616   7
  19 -11   0 503.403 138.900   4
  19  11   0 739.892 201.157   7
  20   0  -1 51.6255 78.5510   4
  20   0   0 43.2096 68.4109   4
  20   0   1 71.6703 85.0056   4
  20   0   2 20493.4 1002.03   4
  20  -2  -2 2030.33 260.909   4
  20   2  -1 5485.29 442.351   4
  20  -2  -1 6065.66 478.616   4
  20  -2   0 825.102 196.296   4
  20   2   0 872.017 178.885   4
  20  -2   1 896.568 211.603   4
  20   2   1 676.418 183.495   4
  20  -2   2 1287.21 248.422   4
  20   2   2 1161.48 237.138   4
  20  -4  -3 4650.53 395.565   4
  20  -4  -2 1659.91 254.107   4
  20  -4  -1 2390.72 310.990   4
  20  -4   0 487.095 157.360   4
  20   4   0 624.240 160.711   4
  20   4   1 2518.31 324.181   4
  20  -4   1 2783.84 348.563   4
  20   4   2 10125.1 689.478   4
  20  -4   2 11698.0 744.241   4
  20  -6  -3 2803.85 315.835   4
  20  -6  -2 5896.22 476.292   4
  20  -6  -1 1122.48 220.164   4
  20  -6   0 1557.78 262.189   4
  20  -6   1 1076.67 218.067   4
  20   6   1 709.540 177.419   4
  20  -8  -3 1682.80 256.179   4
  20  -8  -2 903.633 195.130   4
  20  -8  -1 5391.82 475.594   4
  20  -8   0 4231.22 431.623   4
  20   8   0 4826.17 504.870   7
  20 -10  -3 652.667 172.874   4
  20 -10  -2 811.018 195.160   4
  21  -1  -1 3813.06 375.626   4
  21   1   0 4427.60 413.661   4
  21  -1   0 3871.24 396.346   4
  21  -1   1 5103.02 466.781   4
  21   1   1 4948.28 455.682   4
  21  -3  -2 563.420 146.145   4
  21  -3  -1 754.726 163.952   4
  21  -3   0 5133.78 461.613   4
  21  -5  -2 5691.15 459.368   4
  21  -5  -1 212.494 113.784   4
  21  -7  -2 6621.52 509.413   4
   0   0   0    0.00    0.00   0
TITL S3-Barry-1_auto in Cc
REM Cc (#9 in standard setting)
CELL 0.71073  11.071786  12.503859   7.539687  90.0000 103.2349  90.0000
ZERR    4.00   0.000156   0.000157   0.000112   0.0000   0.0014   0.0000
LATT -7
SYMM  x,-y, z+1/2
SFAC C H N O
UNIT 44.00 40.00 4.00 4.00
REM  CrysAlisPro recorded range (K): Min=100.0; max=100.0; aver:100.0
TEMP -173
TREF
HKLF 4
END
;
_shelx_hkl_checksum              2163
_shelx_res_file
;
TITL S3-Barry-1_auto in Cc
    article2.res
    created by SHELXL-2019/1 at 17:02:18 on 19-Feb-2025
REM OMIT 4.00 180.00
REM CONF
CELL 0.71073 11.07179 12.50386 7.53969 90 103.2349 90
ZERR 4 0.00016 0.00016 0.00011 0 0.0014 0
LATT -7
SYMM +X,-Y,0.5+Z
SFAC O P K Ni
UNIT 48 16 8 4
L.S. 20
PLAN  5
CONF
MORE -1
fmap 2
acta
TWIN -1 0 0 0 -1 0 0 0 -1 2
REM <olex2.extras>
REM <HklSrc "%.\\Article%202.hkl">
REM </olex2.extras>
WGHT    0.056400    1.221500
BASF   0.53897
FVAR       2.33173
NI1   4    0.946421    0.346691    0.793868    11.00000    0.00581    0.00526 =
         0.00660    0.00007    0.00160    0.00012
K1    3    0.613585    0.633406    0.125304    11.00000    0.00615    0.00922 =
         0.00764   -0.00036    0.00283   -0.00002
K2    3    1.316000    0.373927    0.968915    11.00000    0.00994    0.00745 =
         0.01295   -0.00230    0.00245   -0.00041
P1    2    1.054698    0.575114    0.707584    11.00000    0.00303    0.00325 =
         0.00364   -0.00030    0.00081   -0.00080
P2    2    0.835902    0.576882    0.865780    11.00000    0.00332    0.00287 =
         0.00425   -0.00014    0.00139    0.00051
P3    2    0.628066    0.689630    0.623806    11.00000    0.00380    0.00497 =
         0.00343    0.00020    0.00079    0.00063
P4    2    1.284542    0.660687    0.973446    11.00000    0.00303    0.00393 =
         0.00437   -0.00040    0.00048   -0.00011
O1    1    0.940414    0.624290    0.774947    11.00000    0.00585    0.00510 =
         0.01011    0.00007    0.00516    0.00005
O2    1    0.847659    0.459260    0.890167    11.00000    0.00589    0.00300 =
         0.00755    0.00048    0.00200    0.00091
O3    1    0.711769    0.589657    0.709544    11.00000    0.00503    0.00509 =
         0.00845    0.00031   -0.00078    0.00070
O4    1    1.166502    0.593142    0.876936    11.00000    0.00735    0.01098 =
         0.00635    0.00034   -0.00230   -0.00484
O5    1    1.045082    0.457039    0.687905    11.00000    0.00650    0.00367 =
         0.00759   -0.00069    0.00256   -0.00063
O6    1    0.828061    0.647833    1.021982    11.00000    0.00686    0.00529 =
         0.00575   -0.00143    0.00195    0.00087
O7    1    1.072177    0.642674    0.552545    11.00000    0.00649    0.00670 =
         0.00479    0.00081    0.00167   -0.00148
O8    1    1.316742    0.737232    0.840747    11.00000    0.00725    0.00747 =
         0.00821    0.00134    0.00351   -0.00108
O9    1    1.233259    0.721978    1.127812    11.00000    0.00873    0.00645 =
         0.00637   -0.00111    0.00286    0.00200
O10   1    1.376791    0.582796    1.070075    11.00000    0.00603    0.00684 =
         0.01125    0.00161   -0.00069    0.00233
O11   1    0.555853    0.723015    0.758582    11.00000    0.00849    0.00777 =
         0.00778    0.00046    0.00434    0.00227
O12   1    0.560998    0.660487    0.438652    11.00000    0.00736    0.01285 =
         0.00445   -0.00080   -0.00041   -0.00059
HKLF 4
REM  S3-Barry-1_auto in Cc
REM wR2 = 0.0884, GooF = S = 1.066, Restrained GooF = 1.066 for all data
REM R1 = 0.0306 for 7869 Fo > 4sig(Fo) and 0.0318 for all 8076 data
REM 173 parameters refined using 2 restraints
END
WGHT      0.0565      1.1991
REM Highest difference peak  0.825,  deepest hole -2.854,  1-sigma level  0.169
Q1    1   1.3125  0.7100  0.9232  11.00000  0.05    0.82
Q2    1   1.0688  0.5058  0.7151  11.00000  0.05    0.69
Q3    1   0.8522  0.5081  0.8727  11.00000  0.05    0.66
Q4    1   0.9554  0.3481  0.7047  11.00000  0.05    0.63
Q5    1   1.3344  0.6235  1.0284  11.00000  0.05    0.62
;
_shelx_res_checksum              79115
loop_
_space_group_symop_operation_xyz
'x, y, z'
'x, -y, z+1/2'
'x+1/2, y+1/2, z'
'x+1/2, -y+1/2, z+1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ni Ni1 0.94642(3) 0.34669(2) 0.79387(4) 0.00586(5) Uani d 1 . .
K K1 0.61359(4) 0.63341(3) 0.12530(6) 0.00747(6) Uani d 1 . .
K K2 1.31600(5) 0.37393(4) 0.96892(7) 0.01014(7) Uani d 1 . .
P P1 1.05470(5) 0.57511(4) 0.70758(7) 0.00330(7) Uani d 1 . .
P P2 0.83590(5) 0.57688(4) 0.86578(7) 0.00340(7) Uani d 1 . .
P P3 0.62807(5) 0.68963(4) 0.62381(7) 0.00407(7) Uani d 1 . .
P P4 1.28454(5) 0.66069(4) 0.97345(7) 0.00384(7) Uani d 1 . .
O O1 0.94041(16) 0.62429(12) 0.7749(2) 0.0065(2) Uani d 1 . .
O O2 0.84766(14) 0.45926(12) 0.8902(2) 0.00540(19) Uani d 1 . .
O O3 0.71177(15) 0.58966(12) 0.7095(2) 0.0066(2) Uani d 1 . .
O O4 1.16650(16) 0.59314(15) 0.8769(2) 0.0088(2) Uani d 1 . .
O O5 1.04508(15) 0.45704(12) 0.6879(2) 0.0058(2) Uani d 1 . .
O O6 0.82806(16) 0.64783(12) 1.0220(2) 0.0059(2) Uani d 1 . .
O O7 1.07218(15) 0.64267(13) 0.5525(2) 0.0059(2) Uani d 1 . .
O O8 1.31674(15) 0.73723(13) 0.8407(2) 0.0074(2) Uani d 1 . .
O O9 1.23326(16) 0.72198(13) 1.1278(2) 0.0070(2) Uani d 1 . .
O O10 1.37679(15) 0.58280(13) 1.0701(2) 0.0085(2) Uani d 1 . .
O O11 0.55585(16) 0.72302(13) 0.7586(2) 0.0076(2) Uani d 1 . .
O O12 0.56100(16) 0.66049(14) 0.4387(2) 0.0085(2) Uani d 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Ni1 0.00581(9) 0.00526(8) 0.00660(8) 0.00012(7) 0.00160(7) 0.00007(7)
K1 0.00615(13) 0.00922(13) 0.00764(13) -0.00002(12) 0.00283(10) -0.00036(12)
K2 0.00994(16) 0.00745(14) 0.01295(17) -0.00041(12) 0.00245(13) -0.00230(12)
P1 0.00303(16) 0.00325(16) 0.00364(15) -0.00080(12) 0.00081(12) -0.00030(12)
P2 0.00332(16) 0.00287(15) 0.00425(15) 0.00051(12) 0.00139(12) -0.00014(12)
P3 0.00380(16) 0.00497(16) 0.00343(15) 0.00063(12) 0.00079(12) 0.00020(13)
P4 0.00303(16) 0.00393(17) 0.00437(16) -0.00011(12) 0.00048(13) -0.00040(12)
O1 0.0059(5) 0.0051(4) 0.0101(6) 0.0000(4) 0.0052(4) 0.0001(4)
O2 0.0059(5) 0.0030(4) 0.0075(5) 0.0009(3) 0.0020(4) 0.0005(3)
O3 0.0050(5) 0.0051(4) 0.0085(5) 0.0007(4) -0.0008(4) 0.0003(4)
O4 0.0073(5) 0.0110(6) 0.0063(5) -0.0048(4) -0.0023(4) 0.0003(4)
O5 0.0065(5) 0.0037(4) 0.0076(5) -0.0006(4) 0.0026(4) -0.0007(4)
O6 0.0069(5) 0.0053(5) 0.0057(5) 0.0009(4) 0.0019(4) -0.0014(4)
O7 0.0065(5) 0.0067(5) 0.0048(5) -0.0015(4) 0.0017(4) 0.0008(4)
O8 0.0073(5) 0.0075(5) 0.0082(5) -0.0011(4) 0.0035(4) 0.0013(4)
O9 0.0087(5) 0.0064(5) 0.0064(5) 0.0020(4) 0.0029(4) -0.0011(4)
O10 0.0060(5) 0.0068(5) 0.0112(6) 0.0023(4) -0.0007(4) 0.0016(4)
O11 0.0085(5) 0.0078(5) 0.0078(5) 0.0023(4) 0.0043(4) 0.0005(4)
O12 0.0074(5) 0.0129(6) 0.0044(5) -0.0006(4) -0.0004(4) -0.0008(4)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
K1 Ni1 K1 2_565 3_546 125.300(12) ?
K1 Ni1 K2 2_565 4_454 67.218(12) ?
K1 Ni1 K2 3_546 . 62.662(11) ?
K1 Ni1 K2 2_565 . 171.099(12) ?
K2 Ni1 K1 4_454 3_546 88.300(11) ?
K2 Ni1 K2 4_454 . 119.195(13) ?
O2 Ni1 K1 . 3_546 118.16(5) ?
O2 Ni1 K1 . 2_565 59.09(5) ?
O2 Ni1 K2 . 4_454 126.08(5) ?
O2 Ni1 K2 . . 114.71(5) ?
O2 Ni1 O5 . . 92.99(6) ?
O2 Ni1 O6 . 2_564 93.34(6) ?
O2 Ni1 O7 . 2_565 85.48(6) ?
O2 Ni1 O8 . 3_445 86.88(7) ?
O2 Ni1 O11 . 3_545 166.65(7) ?
O5 Ni1 K1 . 3_546 120.40(5) ?
O5 Ni1 K1 . 2_565 114.24(5) ?
O5 Ni1 K2 . . 58.20(5) ?
O5 Ni1 K2 . 4_454 113.79(5) ?
O5 Ni1 O6 . 2_564 82.52(6) ?
O5 Ni1 O7 . 2_565 91.15(6) ?
O5 Ni1 O8 . 3_445 166.15(7) ?
O6 Ni1 K1 2_564 2_565 47.10(5) ?
O6 Ni1 K1 2_564 3_546 137.45(4) ?
O6 Ni1 K2 2_564 . 131.17(5) ?
O6 Ni1 K2 2_564 4_454 49.19(4) ?
O7 Ni1 K1 2_565 3_546 47.74(4) ?
O7 Ni1 K1 2_565 2_565 135.89(5) ?
O7 Ni1 K2 2_565 4_454 135.94(4) ?
O7 Ni1 K2 2_565 . 44.68(5) ?
O7 Ni1 O6 2_565 2_564 173.50(6) ?
O8 Ni1 K1 3_445 2_565 54.26(5) ?
O8 Ni1 K1 3_445 3_546 71.27(5) ?
O8 Ni1 K2 3_445 4_454 56.46(5) ?
O8 Ni1 K2 3_445 . 133.93(5) ?
O8 Ni1 O6 3_445 2_564 83.66(6) ?
O8 Ni1 O7 3_445 2_565 102.64(7) ?
O11 Ni1 K1 3_545 3_546 48.53(5) ?
O11 Ni1 K1 3_545 2_565 126.83(5) ?
O11 Ni1 K2 3_545 4_454 60.25(5) ?
O11 Ni1 K2 3_545 . 60.75(5) ?
O11 Ni1 O5 3_545 . 94.32(7) ?
O11 Ni1 O6 3_545 2_564 98.67(7) ?
O11 Ni1 O7 3_545 2_565 83.22(7) ?
O11 Ni1 O8 3_545 3_445 88.67(7) ?
Ni1 K1 P2 2_564 2_564 51.633(11) ?
P2 K1 Ni1 1_554 2_564 55.151(12) ?
P2 K1 P2 1_554 2_564 70.573(13) ?
P2 K1 P4 1_554 1_454 128.817(18) ?
P4 K1 Ni1 1_454 2_564 170.418(17) ?
P4 K1 P2 1_454 2_564 136.511(17) ?
O2 K1 Ni1 2_564 2_564 33.80(3) ?
O2 K1 P2 2_564 2_564 22.39(3) ?
O2 K1 P2 2_564 1_554 72.46(3) ?
O2 K1 P4 2_564 1_454 151.52(3) ?
O3 K1 Ni1 2_564 2_564 72.55(3) ?
O3 K1 P2 2_564 1_554 70.67(4) ?
O3 K1 P2 2_564 2_564 24.11(3) ?
O3 K1 P4 2_564 1_454 116.65(3) ?
O3 K1 O2 2_564 2_564 46.48(4) ?
O6 K1 Ni1 1_554 2_564 36.48(4) ?
O6 K1 P2 1_554 2_564 70.19(4) ?
O6 K1 P2 1_554 1_554 22.61(3) ?
O6 K1 P4 1_554 1_454 144.02(4) ?
O6 K1 O2 1_554 2_564 63.03(5) ?
O6 K1 O3 1_554 2_564 79.73(5) ?
O6 K1 O7 1_554 4_464 89.55(5) ?
O6 K1 O8 1_554 4_464 60.32(5) ?
O6 K1 O11 1_554 1_554 73.37(5) ?
O7 K1 Ni1 4_464 2_564 96.04(4) ?
O7 K1 P2 4_464 2_564 146.15(4) ?
O7 K1 P2 4_464 1_554 100.93(4) ?
O7 K1 P4 4_464 1_454 74.89(4) ?
O7 K1 O2 4_464 2_564 124.00(4) ?
O7 K1 O3 4_464 2_564 168.30(5) ?
O7 K1 O8 4_464 4_464 68.73(5) ?
O7 K1 O11 4_464 1_554 56.84(5) ?
O8 K1 Ni1 4_464 2_564 34.89(3) ?
O8 K1 P2 4_464 2_564 77.60(3) ?
O8 K1 P2 4_464 1_554 82.80(3) ?
O8 K1 P4 4_464 1_454 135.97(4) ?
O8 K1 O2 4_464 2_564 55.29(4) ?
O8 K1 O3 4_464 2_564 101.52(5) ?
O10 K1 Ni1 1_454 2_564 165.34(4) ?
O10 K1 P2 1_454 2_564 115.13(4) ?
O10 K1 P2 1_454 1_554 130.96(4) ?
O10 K1 P4 1_454 1_454 21.38(4) ?
O10 K1 O2 1_454 2_564 131.63(5) ?
O10 K1 O3 1_454 2_564 96.26(5) ?
O10 K1 O6 1_454 1_554 152.78(6) ?
O10 K1 O7 1_454 4_464 95.42(5) ?
O10 K1 O8 1_454 4_464 145.79(5) ?
O10 K1 O11 1_454 1_554 87.03(5) ?
O11 K1 Ni1 1_554 2_564 106.92(4) ?
O11 K1 P2 1_554 2_564 134.53(4) ?
O11 K1 P2 1_554 1_554 65.34(3) ?
O11 K1 P4 1_554 1_454 70.95(4) ?
O11 K1 O2 1_554 2_564 136.18(5) ?
O11 K1 O3 1_554 2_564 123.15(5) ?
O11 K1 O8 1_554 4_464 106.65(5) ?
O12 K1 Ni1 . 2_564 95.42(4) ?
O12 K1 P2 . 1_554 149.42(4) ?
O12 K1 P2 . 2_564 84.87(4) ?
O12 K1 P4 . 1_454 81.60(4) ?
O12 K1 O2 . 2_564 77.92(5) ?
O12 K1 O3 . 2_564 94.28(5) ?
O12 K1 O6 . 1_554 131.32(5) ?
O12 K1 O7 . 4_464 89.27(5) ?
O12 K1 O8 . 4_464 74.13(5) ?
O12 K1 O10 . 1_454 75.61(6) ?
O12 K1 O11 . 1_554 140.45(5) ?
P3 K2 P4 2_665 . 108.365(18) ?
O4 K2 P3 . 2_665 134.00(3) ?
O4 K2 P4 . . 26.10(3) ?
O4 K2 O5 . . 42.80(4) ?
O4 K2 O10 . 2_564 82.19(5) ?
O4 K2 O11 . 2_665 140.01(4) ?
O5 K2 P3 . 2_665 160.47(3) ?
O5 K2 P4 . . 68.28(3) ?
O6 K2 P3 3_545 2_665 73.47(4) ?
O6 K2 P4 3_545 . 170.35(4) ?
O6 K2 O4 3_545 . 152.31(5) ?
O6 K2 O5 3_545 . 113.25(4) ?
O6 K2 O7 3_545 2_565 85.13(5) ?
O6 K2 O8 3_545 2_565 56.20(5) ?
O6 K2 O10 3_545 2_564 106.24(5) ?
O6 K2 O11 3_545 2_665 62.17(5) ?
O7 K2 P3 2_565 2_665 143.99(4) ?
O7 K2 P4 2_565 . 88.43(3) ?
O7 K2 O4 2_565 . 69.44(5) ?
O7 K2 O5 2_565 . 55.30(4) ?
O7 K2 O8 2_565 2_565 65.62(5) ?
O7 K2 O10 2_565 2_564 127.26(5) ?
O7 K2 O11 2_565 2_665 118.74(5) ?
O8 K2 P3 2_565 2_665 78.40(3) ?
O8 K2 P4 2_565 . 114.47(3) ?
O8 K2 O4 2_565 . 118.08(5) ?
O8 K2 O5 2_565 . 120.88(4) ?
O8 K2 O10 2_565 2_564 159.73(5) ?
O8 K2 O11 2_565 2_665 53.12(4) ?
O9 K2 P3 2_564 2_665 107.59(4) ?
O9 K2 P4 2_564 . 115.06(4) ?
O9 K2 O4 2_564 . 97.12(5) ?
O9 K2 O5 2_564 . 60.22(4) ?
O9 K2 O6 2_564 3_545 72.48(5) ?
O9 K2 O7 2_564 2_565 92.51(5) ?
O9 K2 O8 2_564 2_565 124.55(5) ?
O9 K2 O10 2_564 2_564 47.05(4) ?
O9 K2 O11 2_564 2_665 120.12(5) ?
O9 K2 O12 2_564 2_665 88.78(5) ?
O10 K2 P3 2_564 2_665 87.07(3) ?
O10 K2 P3 . 2_665 87.87(4) ?
O10 K2 P4 2_564 . 83.39(3) ?
O10 K2 P4 . . 22.17(3) ?
O10 K2 O4 . . 47.91(4) ?
O10 K2 O5 2_564 . 73.49(4) ?
O10 K2 O5 . . 90.43(4) ?
O10 K2 O6 . 3_545 153.87(5) ?
O10 K2 O7 . 2_565 100.77(5) ?
O10 K2 O8 . 2_565 102.85(5) ?
O10 K2 O9 . 2_564 131.91(5) ?
O10 K2 O10 . 2_564 90.52(4) ?
O10 K2 O11 . 2_665 93.26(5) ?
O10 K2 O12 . 2_665 89.34(5) ?
O11 K2 P3 2_665 2_665 25.28(3) ?
O11 K2 P4 2_665 . 115.41(3) ?
O11 K2 O5 2_665 . 173.59(4) ?
O11 K2 O10 2_665 2_564 111.68(4) ?
O12 K2 P3 2_665 2_665 24.16(3) ?
O12 K2 P4 2_665 . 104.51(4) ?
O12 K2 O4 2_665 . 125.18(5) ?
O12 K2 O5 2_665 . 136.41(5) ?
O12 K2 O6 2_665 3_545 81.05(5) ?
O12 K2 O7 2_665 2_565 165.05(5) ?
O12 K2 O8 2_665 2_565 101.57(5) ?
O12 K2 O10 2_665 2_564 62.93(5) ?
O12 K2 O11 2_665 2_665 48.97(4) ?
K1 P1 K2 4_565 2_564 65.244(13) ?
O1 P1 K1 . 4_565 81.92(6) ?
O1 P1 K2 . 2_564 146.61(6) ?
O4 P1 K1 . 4_565 82.08(7) ?
O4 P1 K2 . 2_564 79.50(7) ?
O4 P1 O1 . . 102.73(10) ?
O5 P1 K1 . 4_565 162.46(7) ?
O5 P1 K2 . 2_564 99.47(7) ?
O5 P1 O1 . . 111.84(9) ?
O5 P1 O4 . . 104.35(10) ?
O5 P1 O7 . . 120.29(9) ?
O7 P1 K1 . 4_565 42.80(6) ?
O7 P1 K2 . 2_564 44.18(7) ?
O7 P1 O1 . . 106.67(9) ?
O7 P1 O4 . . 109.57(10) ?
K1 P2 K1 1_556 2_565 86.856(17) ?
K1 P2 K2 1_556 3_455 67.271(14) ?
K1 P2 K2 2_565 3_455 135.710(18) ?
O1 P2 K1 . 1_556 146.03(6) ?
O1 P2 K1 . 2_565 120.85(7) ?
O1 P2 K2 . 3_455 78.82(6) ?
O1 P2 O3 . . 103.48(9) ?
O2 P2 K1 . 1_556 100.44(7) ?
O2 P2 K1 . 2_565 52.96(6) ?
O2 P2 K2 . 3_455 161.42(7) ?
O2 P2 O1 . . 111.80(9) ?
O2 P2 O3 . . 103.08(9) ?
O2 P2 O6 . . 120.69(9) ?
O3 P2 K1 . 2_565 50.17(6) ?
O3 P2 K1 . 1_556 78.39(7) ?
O3 P2 K2 . 3_455 88.45(6) ?
O6 P2 K1 . 2_565 130.12(7) ?
O6 P2 K1 . 1_556 43.42(7) ?
O6 P2 K2 . 3_455 40.83(6) ?
O6 P2 O1 . . 107.34(9) ?
O6 P2 O3 . . 109.04(9) ?
K2 P3 K1 3_455 . 134.104(18) ?
K2 P3 K1 2_464 . 79.126(15) ?
K2 P3 K2 2_464 3_455 136.71(2) ?
O3 P3 K1 . . 98.32(7) ?
O3 P3 K2 . 2_464 113.32(6) ?
O3 P3 K2 . 3_455 91.25(6) ?
O9 P3 K1 4_464 . 90.70(6) ?
O9 P3 K2 4_464 3_455 43.41(6) ?
O9 P3 K2 4_464 2_464 145.79(6) ?
O9 P3 O3 4_464 . 100.37(9) ?
O11 P3 K1 . . 145.19(7) ?
O11 P3 K2 . 3_455 69.63(7) ?
O11 P3 K2 . 2_464 69.25(7) ?
O11 P3 O3 . . 107.15(10) ?
O11 P3 O9 . 4_464 107.19(10) ?
O12 P3 K1 . . 27.68(7) ?
O12 P3 K2 . 2_464 51.45(8) ?
O12 P3 K2 . 3_455 153.56(7) ?
O12 P3 O3 . . 108.05(9) ?
O12 P3 O9 . 4_464 113.35(10) ?
O12 P3 O11 . . 118.97(11) ?
K1 P4 K1 1_656 4_565 126.000(18) ?
K1 P4 K2 1_656 2_565 79.159(15) ?
K1 P4 K2 1_656 . 79.311(16) ?
K2 P4 K1 . 4_565 133.819(19) ?
K2 P4 K1 2_565 4_565 133.235(18) ?
K2 P4 K2 . 2_565 84.614(14) ?
O4 P4 K1 . 4_565 79.54(7) ?
O4 P4 K1 . 1_656 140.19(8) ?
O4 P4 K2 . . 62.42(7) ?
O4 P4 K2 . 2_565 106.16(7) ?
O4 P4 O9 . . 101.31(10) ?
O8 P4 K1 . 4_565 42.82(7) ?
O8 P4 K1 . 1_656 83.87(7) ?
O8 P4 K2 . . 126.58(7) ?
O8 P4 K2 . 2_565 140.74(7) ?
O8 P4 O4 . . 109.49(10) ?
O8 P4 O9 . . 111.14(9) ?
O9 P4 K1 . 4_565 88.55(6) ?
O9 P4 K1 . 1_656 108.51(6) ?
O9 P4 K2 . 2_565 44.69(6) ?
O9 P4 K2 . . 122.27(6) ?
O10 P4 K1 . 1_656 40.58(7) ?
O10 P4 K1 . 4_565 162.48(8) ?
O10 P4 K2 . 2_565 61.96(8) ?
O10 P4 K2 . . 44.86(7) ?
O10 P4 O4 . . 106.22(10) ?
O10 P4 O8 . . 120.76(10) ?
O10 P4 O9 . . 106.09(10) ?
P2 O1 P1 . . 134.80(10) ?
Ni1 O2 K1 . 2_565 87.11(5) ?
P2 O2 Ni1 . . 133.34(10) ?
P2 O2 K1 . 2_565 104.66(7) ?
P2 O3 K1 . 2_565 105.71(7) ?
P2 O3 P3 . . 134.04(11) ?
P3 O3 K1 . 2_565 119.39(8) ?
P1 O4 K2 . . 108.94(9) ?
P1 O4 P4 . . 149.18(13) ?
P4 O4 K2 . . 91.47(8) ?
Ni1 O5 K2 . . 91.39(5) ?
P1 O5 Ni1 . . 131.91(10) ?
P1 O5 K2 . . 102.00(7) ?
Ni1 O6 K1 2_565 1_556 96.42(6) ?
Ni1 O6 K2 2_565 3_455 95.74(5) ?
K1 O6 K2 1_556 3_455 95.26(5) ?
P2 O6 Ni1 . 2_565 129.30(10) ?
P2 O6 K1 . 1_556 113.98(9) ?
P2 O6 K2 . 3_455 119.17(9) ?
Ni1 O7 K1 2_564 4_565 99.02(6) ?
Ni1 O7 K2 2_564 2_564 104.50(6) ?
K1 O7 K2 4_565 2_564 89.74(5) ?
P1 O7 Ni1 . 2_564 125.44(10) ?
P1 O7 K1 . 4_565 116.54(8) ?
P1 O7 K2 . 2_564 114.96(9) ?
Ni1 O8 K1 3 4_565 90.84(6) ?
Ni1 O8 K2 3 2_564 90.02(6) ?
K1 O8 K2 4_565 2_564 84.52(4) ?
P4 O8 Ni1 . 3 145.38(11) ?
P4 O8 K1 . 4_565 117.09(9) ?
P4 O8 K2 . 2_564 111.44(8) ?
P3 O9 K2 4_565 2_565 113.41(8) ?
P3 O9 P4 4_565 . 133.93(11) ?
P4 O9 K2 . 2_565 111.54(8) ?
K1 O10 K2 1_656 . 116.20(6) ?
K1 O10 K2 1_656 2_565 102.79(5) ?
K2 O10 K2 . 2_565 108.77(6) ?
P4 O10 K1 . 1_656 118.04(9) ?
P4 O10 K2 . 2_565 94.57(8) ?
P4 O10 K2 . . 112.97(9) ?
Ni1 O11 K1 3_455 1_556 100.21(6) ?
Ni1 O11 K2 3_455 2_464 87.23(6) ?
K1 O11 K2 1_556 2_464 117.41(6) ?
P3 O11 Ni1 . 3_455 137.44(11) ?
P3 O11 K1 . 1_556 120.26(9) ?
P3 O11 K2 . 2_464 85.46(7) ?
K1 O12 K2 . 2_464 118.61(6) ?
P3 O12 K1 . . 136.99(11) ?
P3 O12 K2 . 2_464 104.38(9) ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Ni1 K1 2_565 3.6212(6) ?
Ni1 K1 3_546 3.8294(5) ?
Ni1 K2 4_454 3.7520(6) ?
Ni1 K2 . 4.0161(6) ?
Ni1 O2 . 2.0168(15) ?
Ni1 O5 . 2.0335(16) ?
Ni1 O6 2_564 2.1666(16) ?
Ni1 O7 2_565 2.1253(16) ?
Ni1 O8 3_445 2.0717(16) ?
Ni1 O11 3_545 2.0194(16) ?
K1 P2 1_554 3.5486(7) ?
K1 P2 2_564 3.7705(7) ?
K1 P4 1_454 3.5763(7) ?
K1 O2 2_564 3.1108(16) ?
K1 O3 2_564 3.0080(16) ?
K1 O6 1_554 2.6693(18) ?
K1 O7 4_464 2.8697(16) ?
K1 O8 4_464 2.9396(17) ?
K1 O10 1_454 2.6358(18) ?
K1 O11 1_554 2.9154(17) ?
K1 O12 . 2.5817(18) ?
K2 P3 2_665 3.4765(7) ?
K2 P4 . 3.6034(7) ?
K2 O4 . 3.195(2) ?
K2 O5 . 3.4141(17) ?
K2 O6 3_545 2.8540(16) ?
K2 O7 2_565 2.9168(18) ?
K2 O8 2_565 3.1274(18) ?
K2 O9 2_564 2.7951(17) ?
K2 O10 2_564 3.273(2) ?
K2 O10 . 2.7605(18) ?
K2 O11 2_665 3.2612(18) ?
K2 O12 2_665 2.8069(19) ?
P1 O1 . 1.5910(17) ?
P1 O4 . 1.5779(16) ?
P1 O5 . 1.4852(16) ?
P1 O7 . 1.4903(16) ?
P2 O1 . 1.5882(17) ?
P2 O2 . 1.4842(16) ?
P2 O3 . 1.6002(16) ?
P2 O6 . 1.4928(16) ?
P3 O3 . 1.6016(16) ?
P3 O9 4_464 1.6009(17) ?
P3 O11 . 1.4893(17) ?
P3 O12 . 1.4691(17) ?
P4 O4 . 1.5860(17) ?
P4 O8 . 1.4858(17) ?
P4 O9 . 1.6022(17) ?
P4 O10 . 1.4771(16) ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
K1 P1 O1 P2 4_565 . . . -175.17(16) ?
K1 P1 O4 K2 4_565 . . . -149.54(7) ?
K1 P1 O4 P4 4_565 . . . -20.6(3) ?
K1 P1 O5 Ni1 4_565 . . . -159.81(12) ?
K1 P1 O5 K2 4_565 . . . 97.2(2) ?
K1 P1 O7 Ni1 4_565 . . 2_564 -124.79(16) ?
K1 P1 O7 K2 4_565 . . 2_564 103.12(10) ?
K1 P2 O1 P1 2_565 . . . -59.95(18) ?
K1 P2 O1 P1 1_556 . . . 159.50(8) ?
K1 P2 O2 Ni1 1_556 . . . 178.03(11) ?
K1 P2 O2 Ni1 2_565 . . . 100.09(14) ?
K1 P2 O2 K1 1_556 . . 2_565 77.94(5) ?
K1 P2 O3 K1 1_556 . . 2_565 -95.65(6) ?
K1 P2 O3 P3 2_565 . . . 168.9(2) ?
K1 P2 O3 P3 1_556 . . . 73.22(15) ?
K1 P2 O6 Ni1 1_556 . . 2_565 121.48(15) ?
K1 P2 O6 Ni1 2_565 . . 2_565 115.61(10) ?
K1 P2 O6 K1 2_565 . . 1_556 -5.87(12) ?
K1 P2 O6 K2 1_556 . . 3_455 -111.29(12) ?
K1 P2 O6 K2 2_565 . . 3_455 -117.17(7) ?
K1 P3 O3 K1 . . . 2_565 -63.59(8) ?
K1 P3 O3 P2 . . . . 128.73(15) ?
K1 P3 O11 Ni1 . . . 3_455 -54.8(2) ?
K1 P3 O11 K1 . . . 1_556 145.33(7) ?
K1 P3 O11 K2 . . . 2_464 26.10(12) ?
K1 P3 O12 K2 . . . 2_464 178.75(19) ?
K1 P4 O4 K2 4_565 . . . 152.97(5) ?
K1 P4 O4 K2 1_656 . . . 17.57(12) ?
K1 P4 O4 P1 1_656 . . . -115.0(2) ?
K1 P4 O4 P1 4_565 . . . 20.4(3) ?
K1 P4 O8 Ni1 4_565 . . 3 140.4(2) ?
K1 P4 O8 Ni1 1_656 . . 3 -29.95(18) ?
K1 P4 O8 K1 1_656 . . 4_565 -170.31(8) ?
K1 P4 O8 K2 4_565 . . 2_564 -94.92(10) ?
K1 P4 O8 K2 1_656 . . 2_564 94.78(6) ?
K1 P4 O9 K2 4_565 . . 2_565 -179.35(6) ?
K1 P4 O9 K2 1_656 . . 2_565 -51.64(8) ?
K1 P4 O9 P3 1_656 . . 4_565 141.58(13) ?
K1 P4 O9 P3 4_565 . . 4_565 13.87(15) ?
K1 P4 O10 K1 4_565 . . 1_656 45.8(3) ?
K1 P4 O10 K2 4_565 . . 2_565 153.0(2) ?
K1 P4 O10 K2 1_656 . . . -140.27(15) ?
K1 P4 O10 K2 4_565 . . . -94.4(2) ?
K1 P4 O10 K2 1_656 . . 2_565 107.12(10) ?
K2 P1 O1 P2 2_564 . . . 174.58(7) ?
K2 P1 O4 K2 2_564 . . . -83.38(6) ?
K2 P1 O4 P4 2_564 . . . 45.5(3) ?
K2 P1 O5 Ni1 2_564 . . . 171.95(10) ?
K2 P1 O5 K2 2_564 . . . 69.00(5) ?
K2 P1 O7 Ni1 2_564 . . 2_564 132.09(15) ?
K2 P1 O7 K1 2_564 . . 4_565 -103.12(10) ?
K2 P2 O1 P1 3_455 . . . 163.00(16) ?
K2 P2 O2 Ni1 3_455 . . . -135.19(15) ?
K2 P2 O2 K1 3_455 . . 2_565 124.72(18) ?
K2 P2 O3 K1 3_455 . . 2_565 -162.76(6) ?
K2 P2 O3 P3 3_455 . . . 6.11(15) ?
K2 P2 O6 Ni1 3_455 . . 2_565 -127.23(17) ?
K2 P2 O6 K1 3_455 . . 1_556 111.29(12) ?
K2 P3 O3 K1 3_455 . . 2_565 161.44(8) ?
K2 P3 O3 K1 2_464 . . 2_565 18.10(11) ?
K2 P3 O3 P2 3_455 . . . -6.24(16) ?
K2 P3 O3 P2 2_464 . . . -149.58(13) ?
K2 P3 O11 Ni1 3_455 . . 3_455 85.23(15) ?
K2 P3 O11 Ni1 2_464 . . 3_455 -80.91(15) ?
K2 P3 O11 K1 3_455 . . 1_556 -74.63(8) ?
K2 P3 O11 K1 2_464 . . 1_556 119.23(10) ?
K2 P3 O11 K2 3_455 . . 2_464 166.14(5) ?
K2 P3 O12 K1 3_455 . . . 62.0(2) ?
K2 P3 O12 K1 2_464 . . . -178.75(19) ?
K2 P3 O12 K2 3_455 . . 2_464 -119.20(14) ?
K2 P4 O4 K2 2_565 . . . -74.83(5) ?
K2 P4 O4 P1 . . . . -132.6(3) ?
K2 P4 O4 P1 2_565 . . . 152.6(3) ?
K2 P4 O8 Ni1 2_565 . . 3 34.6(3) ?
K2 P4 O8 Ni1 . . . 3 -101.76(18) ?
K2 P4 O8 K1 . . . 4_565 117.88(7) ?
K2 P4 O8 K1 2_565 . . 4_565 -105.80(10) ?
K2 P4 O8 K2 . . . 2_564 22.96(11) ?
K2 P4 O8 K2 2_565 . . 2_564 159.29(5) ?
K2 P4 O9 K2 . . . 2_565 37.22(10) ?
K2 P4 O9 P3 . . . 4_565 -129.56(12) ?
K2 P4 O9 P3 2_565 . . 4_565 -166.8(2) ?
K2 P4 O10 K1 2_565 . . 1_656 -107.12(10) ?
K2 P4 O10 K1 . . . 1_656 140.27(15) ?
K2 P4 O10 K2 . . . 2_565 -112.61(10) ?
K2 P4 O10 K2 2_565 . . . 112.61(10) ?
O1 P1 O4 K2 . . . . 130.66(8) ?
O1 P1 O4 P4 . . . . -100.4(3) ?
O1 P1 O5 Ni1 . . . . -19.87(16) ?
O1 P1 O5 K2 . . . . -122.82(8) ?
O1 P1 O7 Ni1 . . . 2_564 -67.44(13) ?
O1 P1 O7 K1 . . . 4_565 57.35(10) ?
O1 P1 O7 K2 . . . 2_564 160.47(8) ?
O1 P2 O2 Ni1 . . . . -12.87(16) ?
O1 P2 O2 K1 . . . 2_565 -112.96(8) ?
O1 P2 O3 K1 . . . 2_565 119.13(8) ?
O1 P2 O3 P3 . . . . -72.00(17) ?
O1 P2 O6 Ni1 . . . 2_565 -79.45(13) ?
O1 P2 O6 K1 . . . 1_556 159.07(8) ?
O1 P2 O6 K2 . . . 3_455 47.77(11) ?
O2 P2 O1 P1 . . . . -1.07(19) ?
O2 P2 O3 K1 . . . 2_565 2.53(10) ?
O2 P2 O3 P3 . . . . 171.40(15) ?
O2 P2 O6 Ni1 . . . 2_565 50.18(16) ?
O2 P2 O6 K1 . . . 1_556 -71.30(12) ?
O2 P2 O6 K2 . . . 3_455 177.41(8) ?
O3 P2 O1 P1 . . . . -111.34(16) ?
O3 P2 O2 Ni1 . . . . 97.66(13) ?
O3 P2 O2 K1 . . . 2_565 -2.43(10) ?
O3 P2 O6 Ni1 . . . 2_565 169.07(11) ?
O3 P2 O6 K1 . . . 1_556 47.60(11) ?
O3 P2 O6 K2 . . . 3_455 -63.70(11) ?
O3 P3 O11 Ni1 . . . 3_455 170.05(14) ?
O3 P3 O11 K1 . . . 1_556 10.20(12) ?
O3 P3 O11 K2 . . . 2_464 -109.04(7) ?
O3 P3 O12 K1 . . . . -72.92(16) ?
O3 P3 O12 K2 . . . 2_464 105.83(9) ?
O4 P1 O1 P2 . . . . -95.24(17) ?
O4 P1 O5 Ni1 . . . . 90.47(14) ?
O4 P1 O5 K2 . . . . -12.48(10) ?
O4 P1 O7 Ni1 . . . 2_564 -177.97(11) ?
O4 P1 O7 K1 . . . 4_565 -53.18(12) ?
O4 P1 O7 K2 . . . 2_564 49.94(12) ?
O4 P4 O8 Ni1 . . . 3 -171.34(17) ?
O4 P4 O8 K1 . . . 4_565 48.30(12) ?
O4 P4 O8 K2 . . . 2_564 -46.62(12) ?
O4 P4 O9 K2 . . . 2_565 101.62(9) ?
O4 P4 O9 P3 . . . 4_565 -65.16(17) ?
O4 P4 O10 K1 . . . 1_656 152.89(10) ?
O4 P4 O10 K2 . . . . 12.62(13) ?
O4 P4 O10 K2 . . . 2_565 -99.99(9) ?
O5 P1 O1 P2 . . . . 16.13(19) ?
O5 P1 O4 K2 . . . . 13.82(11) ?
O5 P1 O4 P4 . . . . 142.7(3) ?
O5 P1 O7 Ni1 . . . 2_564 61.21(15) ?
O5 P1 O7 K1 . . . 4_565 -174.00(8) ?
O5 P1 O7 K2 . . . 2_564 -70.88(11) ?
O6 P2 O1 P1 . . . . 133.43(16) ?
O6 P2 O2 Ni1 . . . . -140.52(12) ?
O6 P2 O2 K1 . . . 2_565 119.39(9) ?
O6 P2 O3 K1 . . . 2_565 -126.86(8) ?
O6 P2 O3 P3 . . . . 42.01(19) ?
O7 P1 O1 P2 . . . . 149.54(15) ?
O7 P1 O4 K2 . . . . -116.23(9) ?
O7 P1 O4 P4 . . . . 12.7(3) ?
O7 P1 O5 Ni1 . . . . -146.17(12) ?
O7 P1 O5 K2 . . . . 110.88(9) ?
O8 P4 O4 K2 . . . . 121.90(8) ?
O8 P4 O4 P1 . . . . -10.7(3) ?
O8 P4 O9 K2 . . . 2_565 -142.14(9) ?
O8 P4 O9 P3 . . . 4_565 51.08(18) ?
O8 P4 O10 K1 . . . 1_656 27.62(15) ?
O8 P4 O10 K2 . . . . -112.65(11) ?
O8 P4 O10 K2 . . . 2_565 134.73(9) ?
O9 P3 O3 K1 4_464 . . 2_565 -155.84(9) ?
O9 P3 O3 P2 4_464 . . . 36.48(18) ?
O9 P3 O11 Ni1 4_464 . . 3_455 63.04(18) ?
O9 P3 O11 K1 4_464 . . 1_556 -96.82(10) ?
O9 P3 O11 K2 4_464 . . 2_464 143.95(7) ?
O9 P3 O12 K1 4_464 . . . 37.38(18) ?
O9 P3 O12 K2 4_464 . . 2_464 -143.87(8) ?
O9 P4 O4 K2 . . . . -120.65(7) ?
O9 P4 O4 P1 . . . . 106.8(3) ?
O9 P4 O8 Ni1 . . . 3 77.6(2) ?
O9 P4 O8 K1 . . . 4_565 -62.80(11) ?
O9 P4 O8 K2 . . . 2_564 -157.72(8) ?
O9 P4 O10 K1 . . . 1_656 -99.86(11) ?
O9 P4 O10 K2 . . . . 119.87(9) ?
O9 P4 O10 K2 . . . 2_565 7.26(9) ?
O10 P4 O4 K2 . . . . -10.01(10) ?
O10 P4 O4 P1 . . . . -142.6(3) ?
O10 P4 O8 Ni1 . . . 3 -47.6(2) ?
O10 P4 O8 K1 . . . 4_565 172.04(9) ?
O10 P4 O8 K2 . . . 2_564 77.12(12) ?
O10 P4 O9 K2 . . . 2_565 -9.12(11) ?
O10 P4 O9 P3 . . . 4_565 -175.90(14) ?
O11 P3 O3 K1 . . . 2_565 92.39(11) ?
O11 P3 O3 P2 . . . . -75.29(18) ?
O11 P3 O12 K1 . . . . 164.75(12) ?
O11 P3 O12 K2 . . . 2_464 -16.50(12) ?
O12 P3 O3 K1 . . . 2_565 -36.92(13) ?
O12 P3 O3 P2 . . . . 155.39(15) ?
O12 P3 O11 Ni1 . . . 3_455 -67.17(19) ?
O12 P3 O11 K1 . . . 1_556 132.98(10) ?
O12 P3 O11 K2 . . . 2_464 13.74(10) ?
loop_
_twin_individual_id
_twin_individual_mass_fraction_refined
1 0.461(9)
2 0.539(9)