#------------------------------------------------------------------------------ #$Date: 2025-05-03 21:20:12 +0200 (Sat, 03 May 2025) $ #$Revision: 299520 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/34/2023423.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023423 loop_ _publ_author_name 'Naghiyev, Farid N.' 'Hökelek, Tuncer' 'Khrustalev, Victor N.' 'Mamedov, Huseyn M.' 'Belay, Alebel N.' 'Ashurov, Jamshid' 'Mamedov, Ibrahim G.' _publ_section_title ; Crystal structure and Hirshfeld surface analyses, inter-molecular inter-action energies and energy frameworks of methyl 6-amino-5-cyano-2-(2-meth-oxy-2-oxoeth-yl)-4-(4-nitro-phen-yl)-4H-pyran-3-carboxyl-ate. ; _journal_coeditor_code DX2064 _journal_issue 'Pt 4' _journal_name_full 'Acta crystallographica. Section E, Crystallographic communications' _journal_page_first 296 _journal_page_last 302 _journal_paper_doi 10.1107/S2056989025001276 _journal_volume 81 _journal_year 2025 _chemical_formula_iupac 'C17 H15 N3 O7' _chemical_formula_moiety 'C17 H15 N3 O7' _chemical_formula_sum 'C17 H15 N3 O7' _chemical_formula_weight 373.32 _chemical_name_systematic 'Methyl 6-amino-5-cyano-2-(2-methoxy-2-oxoethyl)-4-(4-nitrophenyl)-4H-pyran-3-carboxylate' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary difmap _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2013 _cell_angle_alpha 90 _cell_angle_beta 105.6759(5) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 10.27958(5) _cell_length_b 11.18770(6) _cell_length_c 15.09983(8) _cell_measurement_reflns_used 36303 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 77.653 _cell_measurement_theta_min 3.959 _cell_volume 1671.964(16) _computing_cell_refinement ; CrysAlisPro 1.171.42.72a (Rigaku OD, 2022) ; _computing_data_collection ; CrysAlisPro 1.171.42.72a (Rigaku OD, 2022) ; _computing_data_reduction ; CrysAlisPro 1.171.42.72a (Rigaku OD, 2022) ; _computing_molecular_graphics ; SHELXTL (Sheldrick, 2008) ; _computing_publication_material ; SHELXTL (Sheldrick, 2008) ; _computing_structure_refinement ; SHELXL2018/3 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2014/5 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'XtaLAB Synergy-i CCD diffractometer' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0244 _diffrn_reflns_av_unetI/netI 0.0100 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 43458 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 77.800 _diffrn_reflns_theta_min 4.467 _diffrn_source 'micro-focus sealed X-ray tube' _exptl_absorpt_coefficient_mu 1.001 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.399 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; (CrysAlisPro; Rigaku OD, 2022) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.483 _exptl_crystal_description prism _exptl_crystal_F_000 776 _exptl_crystal_size_max 0.21 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.13 _refine_diff_density_max 0.252 _refine_diff_density_min -0.263 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.051 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 254 _refine_ls_number_reflns 3550 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.051 _refine_ls_R_factor_all 0.0316 _refine_ls_R_factor_gt 0.0314 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0426P)^2^+0.66P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0818 _refine_ls_wR_factor_ref 0.0821 _reflns_number_gt 3505 _reflns_number_total 3550 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file dx2064.cif _cod_data_source_block I _cod_depositor_comments 'Adding full bibliography for 2023423.cif.' _cod_original_cell_volume 1671.964(15) _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 2023423 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.817 _shelx_estimated_absorpt_t_max 0.881 _shelx_hkl_file ; 0 0 -1 0.30 0.10 0 0 -1 0.22 0.09 0 0 -2 1488.40 26.77 0 0 -2 1491.10 26.79 0 0 -3 0.20 0.25 0 0 -3 0.10 0.23 0 0 -3 0.39 0.24 0 0 -4 0.97 0.40 0 0 -4 0.47 0.32 0 0 -4 0.47 0.29 0 0 -5 0.54 0.40 0 0 5 0.43 0.17 0 0 5 0.24 0.15 0 0 -5 0.26 0.31 0 0 -6 251.34 7.26 0 0 6 237.30 5.18 0 0 6 237.76 5.07 0 0 -6 254.81 7.32 0 0 -6 243.95 7.06 0 0 -7 0.41 0.23 0 0 -7 0.56 0.49 0 0 -7 0.38 0.44 0 0 -7 0.55 0.45 0 0 -7 0.17 0.21 0 0 -8 1104.06 20.12 0 0 -8 1109.56 24.16 0 0 -8 1110.71 24.11 0 0 -8 1054.22 20.03 0 0 -8 1069.38 23.68 0 0 -9 -0.20 0.49 0 0 -9 0.25 0.29 0 0 -9 0.05 0.27 0 0 -9 -0.40 0.57 0 0 -9 -0.18 0.45 0 0 -10 612.32 16.55 0 0 -10 595.04 11.94 0 0 -10 586.82 11.70 0 0 -10 581.75 11.62 0 0 -10 609.80 11.84 0 0 -10 579.38 11.88 0 0 -10 618.85 12.23 0 0 -10 602.36 12.06 0 0 -10 597.71 11.88 0 0 -10 593.32 12.04 0 0 -10 582.18 11.82 0 0 -10 584.77 11.79 0 0 -10 608.45 16.86 0 0 -10 597.18 11.80 0 0 -10 595.63 12.13 0 0 -10 611.61 16.89 0 0 -11 0.30 0.28 0 0 -11 -0.27 0.66 0 0 -11 -0.12 0.31 0 0 -11 0.36 0.29 0 0 -11 -0.07 0.36 0 0 -11 0.06 0.34 0 0 -11 1.12 0.39 0 0 -11 0.73 0.76 0 0 -11 0.14 0.27 0 0 -11 1.56 0.39 0 0 -11 0.26 0.32 0 0 -11 0.12 0.32 0 0 -11 0.27 0.26 0 0 -11 0.05 0.26 0 0 -11 0.45 0.36 0 0 -11 -0.26 0.65 0 0 -12 270.28 6.35 0 0 -12 272.70 6.70 0 0 -12 275.64 6.85 0 0 -12 252.93 10.43 0 0 -12 272.83 6.65 0 0 -12 283.40 6.61 0 0 -12 273.75 6.25 0 0 -12 274.43 6.37 0 0 -12 268.78 6.80 0 0 -12 268.65 6.67 0 0 -12 277.56 6.51 0 0 -12 272.72 6.50 0 0 -12 265.55 6.77 0 0 -12 254.40 10.83 0 0 -13 0.06 0.31 0 0 -13 -0.07 0.36 0 0 -13 -0.28 0.69 0 0 -13 0.37 0.34 0 0 -13 0.26 0.32 0 0 -13 -0.07 0.40 0 0 -13 0.16 0.30 0 0 -13 0.37 0.35 0 0 -13 0.19 0.36 0 0 -13 2.26 0.59 0 0 -13 0.31 0.76 0 0 -13 -0.15 0.39 0 0 -13 0.37 0.50 0 0 -14 133.55 3.91 0 0 -14 117.36 6.82 0 0 -14 123.72 3.85 0 0 -14 123.65 3.75 0 0 -14 124.23 3.50 0 0 -14 127.28 4.02 0 0 -14 133.71 3.83 0 0 -14 127.23 3.96 0 0 -14 125.65 3.81 0 0 -14 132.14 3.94 0 0 -14 122.46 4.03 0 0 -14 126.51 4.05 0 0 -15 0.16 0.32 0 0 -15 0.11 0.34 0 0 -15 0.26 0.32 0 0 -15 1.38 0.36 0 0 -15 -0.06 0.37 0 0 -15 0.35 0.34 0 0 -15 0.24 0.39 0 0 -15 0.16 0.34 0 0 -15 0.51 0.37 0 0 -15 -0.07 0.38 0 0 -15 0.26 0.37 0 0 -16 1.36 0.42 0 0 -16 0.82 0.37 0 0 -16 1.89 0.43 0 0 -16 1.40 0.44 0 0 -16 1.97 0.47 0 0 -16 2.06 0.44 0 0 -16 1.42 0.44 0 0 -16 1.38 0.38 0 0 -16 1.64 0.37 0 0 -17 0.04 0.25 0 0 -17 0.04 0.29 0 0 -17 0.03 0.22 0 0 -17 0.10 0.22 0 0 -17 0.04 0.25 0 0 -17 0.19 0.23 0 0 -17 -0.04 0.26 0 0 -18 289.67 5.77 0 0 -18 298.96 5.82 0 1 0 1.15 0.20 0 -1 0 -0.02 0.08 0 -1 -1 166.27 3.41 0 1 -1 166.59 3.42 0 -1 -1 165.82 3.71 0 1 1 173.40 3.60 0 1 -1 178.59 3.39 0 -1 -1 173.44 3.37 0 -1 -1 157.52 3.40 0 1 -1 172.72 3.69 0 1 -1 161.48 3.41 0 1 -2 0.16 0.16 0 1 -2 0.76 0.22 0 -1 -2 0.23 0.17 0 1 2 0.30 0.14 0 1 -2 0.49 0.19 0 -1 -2 0.16 0.16 0 1 -3 1353.76 24.32 0 -1 -3 1311.64 24.25 0 1 -3 1367.72 24.29 0 -1 -3 1338.12 24.25 0 1 -4 9812.06 169.07 0 1 -4 9999.00 169.14 0 -1 -4 9224.87 168.99 0 -1 -4 9555.51 168.94 0 -1 -4 9700.68 169.02 0 1 -4 9820.02 169.08 0 -1 -5 159.00 5.05 0 1 -5 168.18 5.14 0 1 -5 148.99 4.80 0 -1 -5 154.00 4.86 0 -1 -5 153.30 4.87 0 1 -5 151.19 4.93 0 -1 -5 160.63 5.02 0 1 -6 1645.36 31.62 0 -1 -6 1585.85 31.51 0 1 -6 1702.35 31.68 0 -1 -6 1628.24 31.52 0 1 -6 1641.09 28.66 0 -1 -6 1621.19 31.33 0 -1 -6 1593.18 31.16 0 -1 -7 1019.06 21.50 0 -1 7 967.97 18.92 0 1 -7 1024.67 22.00 0 1 -7 1010.74 18.66 0 -1 -7 1030.42 18.68 0 -1 -7 1033.19 21.97 0 1 -7 1049.94 18.73 0 -1 -7 1011.65 18.70 0 -1 -7 1025.84 21.83 0 1 -7 1033.53 22.10 0 -1 -7 964.80 21.85 0 1 -8 59.86 2.04 0 -1 -8 60.69 2.06 0 -1 -8 58.23 3.68 0 1 -8 58.50 3.65 0 1 -8 59.36 2.06 0 -1 -8 60.84 2.08 0 -1 -8 61.85 3.66 0 1 -8 60.57 3.80 0 -1 -8 63.51 3.87 0 1 -9 31.18 2.92 0 -1 -9 34.64 1.59 0 1 -9 35.70 1.60 0 -1 -9 34.11 3.00 0 -1 -9 39.24 3.27 0 1 -9 37.39 3.19 0 -1 -9 36.06 3.00 0 1 -9 34.94 1.61 0 -1 -9 36.56 1.64 0 1 -10 195.57 4.94 0 -1 -10 218.49 8.53 0 1 -10 189.79 8.04 0 -1 -10 215.76 5.13 0 1 -10 211.47 5.23 0 1 -10 210.23 5.17 0 1 -10 209.83 4.92 0 1 -10 198.07 4.87 0 -1 -10 209.71 4.98 0 1 -10 202.06 5.02 0 -1 -10 214.31 5.26 0 -1 -10 214.50 5.33 0 -1 -10 218.90 8.77 0 1 -10 206.46 8.63 0 1 -10 214.48 5.33 0 -1 -10 205.21 5.22 0 1 -10 208.34 5.00 0 -1 -10 213.83 5.23 0 1 -10 214.73 5.26 0 -1 -10 209.79 4.98 0 1 -10 224.04 5.24 0 1 -10 215.17 5.32 0 1 -10 220.48 5.24 0 1 -10 223.60 8.93 0 -1 -10 207.60 4.91 0 1 -10 220.86 5.21 0 -1 -10 215.25 8.88 0 -1 -10 216.13 5.39 0 1 -10 219.36 5.39 0 1 -11 59.22 4.43 0 -1 -11 55.53 2.32 0 -1 -11 54.64 4.22 0 1 -11 61.00 2.33 0 1 -11 58.49 2.33 0 -1 -11 56.29 2.19 0 1 -11 58.54 2.04 0 -1 -11 59.37 2.23 0 1 -11 57.81 2.26 0 -1 -11 57.06 2.10 0 1 -11 54.30 2.03 0 1 -11 53.73 2.13 0 -1 -11 60.58 2.35 0 1 -11 60.19 2.42 0 -1 -11 59.52 2.42 0 1 -11 63.77 4.74 0 -1 -11 62.61 4.69 0 -1 -11 59.12 2.36 0 1 -11 58.36 2.36 0 1 -11 56.61 2.14 0 -1 -11 60.38 2.33 0 1 -11 54.06 2.20 0 -1 -11 59.68 2.27 0 1 -11 57.26 2.35 0 1 -11 55.39 2.24 0 1 -11 60.43 4.71 0 -1 -11 55.37 4.56 0 -1 -11 57.79 2.10 0 1 -11 55.39 2.22 0 -1 -11 56.73 2.39 0 1 -11 58.63 2.43 0 1 -12 603.69 12.05 0 -1 -12 565.46 11.74 0 1 -12 598.84 12.14 0 -1 -12 607.21 12.14 0 1 -12 574.84 12.12 0 1 -12 600.33 12.40 0 1 -12 583.37 12.12 0 -1 -12 528.68 12.09 0 1 -12 600.04 12.50 0 1 -12 578.40 17.89 0 -1 -12 596.01 17.95 0 -1 -12 596.56 12.48 0 -1 -12 596.45 12.36 0 -1 -12 596.11 12.23 0 1 -12 591.31 17.47 0 -1 -12 604.23 17.58 0 -1 -12 593.59 12.37 0 1 -12 596.86 12.22 0 -1 -12 606.26 12.05 0 1 -12 581.93 11.63 0 1 -12 593.23 12.29 0 -1 -12 599.17 12.08 0 1 -12 588.41 12.10 0 -1 -12 583.02 11.77 0 -1 -12 596.41 12.25 0 1 -12 589.83 11.98 0 1 -12 605.81 12.49 0 1 -12 606.66 12.54 0 -1 -12 566.81 12.43 0 1 -13 38.17 1.77 0 1 -13 37.90 1.83 0 -1 -13 37.54 1.93 0 -1 -13 36.85 1.86 0 -1 -13 39.69 1.94 0 -1 -13 39.67 4.00 0 -1 -13 35.56 1.94 0 1 -13 34.63 1.94 0 1 -13 36.70 3.90 0 1 -13 36.27 3.68 0 1 -13 36.38 1.85 0 -1 -13 42.73 3.95 0 -1 -13 37.13 1.83 0 -1 -13 37.97 1.96 0 -1 -13 37.85 1.80 0 -1 -13 41.99 1.83 0 1 -13 35.53 1.54 0 1 -13 36.01 1.87 0 1 -13 38.10 1.80 0 -1 -13 35.54 1.62 0 1 -13 36.25 1.73 0 1 -13 38.29 2.00 0 -1 -13 37.94 1.84 0 -1 -13 34.91 1.88 0 1 -13 38.65 1.99 0 1 -13 40.03 2.07 0 -1 -13 37.50 2.01 0 -1 -14 352.68 7.71 0 -1 -14 342.78 7.96 0 -1 -14 305.84 11.93 0 1 -14 349.33 7.81 0 1 -14 306.67 11.93 0 1 -14 345.67 7.86 0 -1 -14 337.30 7.45 0 -1 -14 338.22 7.56 0 -1 -14 325.20 7.19 0 1 -14 346.47 7.58 0 1 -14 354.17 8.09 0 1 -14 342.38 7.99 0 -1 -14 340.94 7.69 0 -1 -14 306.93 7.76 0 1 -14 362.68 7.97 0 -1 -14 343.22 7.81 0 -1 -14 345.83 12.83 0 1 -14 350.11 8.14 0 -1 -14 351.65 8.12 0 1 -14 324.25 12.57 0 -1 -14 342.00 8.11 0 1 -14 348.14 8.13 0 -1 -14 350.44 7.92 0 1 -14 345.19 7.55 0 1 -14 342.11 7.67 0 -1 -15 15.40 1.02 0 -1 -15 15.99 1.17 0 1 -15 18.94 1.24 0 1 -15 15.21 1.07 0 1 -15 16.83 1.16 0 1 -15 14.84 0.96 0 1 -15 16.06 1.19 0 -1 -15 15.80 1.07 0 1 -15 16.11 1.16 0 1 -15 14.57 1.16 0 -1 -15 13.58 1.10 0 1 -15 16.10 1.17 0 -1 -15 16.98 1.15 0 1 -15 16.25 1.22 0 -1 -15 13.98 1.14 0 -1 -15 17.21 1.26 0 1 -15 15.10 1.20 0 -1 -15 15.96 1.14 0 1 -16 1.55 0.38 0 -1 -16 1.20 0.40 0 -1 -16 1.30 0.32 0 1 -16 1.29 0.38 0 1 -16 1.04 0.35 0 -1 -16 1.38 0.42 0 1 -16 1.13 0.28 0 1 -16 1.13 0.40 0 -1 -16 1.23 0.45 0 1 -16 1.92 0.44 0 -1 -16 0.99 0.33 0 -1 -16 0.68 0.36 0 1 -16 0.85 0.37 0 1 -16 1.61 0.40 0 -1 -16 0.98 0.35 0 1 -16 1.15 0.39 0 1 -16 1.55 0.43 0 -1 -16 1.58 0.38 0 1 -17 34.05 1.42 0 -1 -17 31.38 1.37 0 1 -17 30.17 1.29 0 1 -17 31.57 1.37 0 -1 -17 32.25 1.37 0 1 -17 32.91 1.23 0 1 -17 30.82 1.25 0 -1 -17 26.98 0.98 0 1 -17 31.94 1.29 0 1 -17 31.86 1.35 0 -1 -17 31.54 1.30 0 -1 -17 31.89 1.33 0 1 -17 27.98 1.26 0 -1 -18 4.35 0.35 0 -1 -18 5.02 0.41 0 1 -18 4.61 0.38 0 -1 -18 4.96 0.40 0 2 0 0.72 0.28 0 2 0 0.77 0.28 0 -2 0 0.97 0.27 0 -2 -1 1322.63 23.83 0 2 -1 1335.81 23.67 0 -2 -1 1357.62 23.63 0 2 -1 1379.46 23.67 0 2 -1 1348.13 23.62 0 -2 -1 1394.71 23.62 0 2 1 1393.61 24.70 0 2 1 1435.52 24.67 0 -2 -1 1390.16 24.85 0 -2 1 1371.95 24.49 0 2 -2 69.91 2.36 0 2 -2 70.65 2.44 0 2 -2 70.13 2.10 0 -2 -2 64.34 2.04 0 -2 -2 67.18 2.05 0 2 -2 66.20 2.05 0 -2 -2 71.93 2.05 0 2 -2 74.40 2.08 0 -2 2 70.33 2.21 0 2 2 69.84 2.30 0 2 -3 1043.90 19.54 0 2 -3 1080.94 19.38 0 -2 -3 1023.01 19.31 0 -2 -3 1031.66 19.28 0 2 -3 995.76 19.21 0 2 -3 970.05 19.11 0 -2 -3 1009.99 19.17 0 2 3 997.31 19.03 0 2 -4 908.43 17.47 0 -2 -4 891.10 17.41 0 2 -4 917.43 17.49 0 -2 -4 885.56 17.29 0 2 -4 862.19 17.26 0 -2 -4 795.32 17.48 0 -2 -4 879.08 17.47 0 2 -4 836.63 17.33 0 -2 -5 1928.98 36.10 0 2 -5 1955.44 36.12 0 2 -5 1936.66 35.91 0 -2 -5 1890.57 35.84 0 -2 -5 1917.67 36.28 0 2 -5 1862.66 36.29 0 -2 -5 1893.84 36.11 0 2 -5 1896.42 36.10 0 2 -6 886.54 18.52 0 2 -6 903.05 18.45 0 -2 -6 855.45 18.28 0 2 -6 886.96 18.36 0 -2 -6 852.87 18.20 0 2 -6 837.92 15.41 0 -2 -6 811.59 15.40 0 -2 -6 819.17 15.43 0 2 -6 832.54 15.45 0 -2 -6 851.90 18.23 0 2 -6 863.02 18.02 0 -2 -6 842.42 17.93 0 2 -7 1162.85 24.40 0 -2 -7 1149.19 24.36 0 -2 -7 1154.67 24.26 0 2 -7 1131.58 20.84 0 2 -7 1169.29 24.32 0 -2 -7 1147.66 20.85 0 2 -7 1125.95 20.88 0 -2 -7 1131.59 20.87 0 -2 -7 1170.61 24.22 0 -2 -7 1139.08 24.02 0 2 -7 1153.82 24.06 0 2 -8 16.17 1.95 0 -2 -8 20.31 2.16 0 -2 -8 18.51 1.07 0 2 -8 18.57 1.06 0 2 -8 21.50 2.18 0 2 -8 19.17 1.06 0 -2 -8 19.05 2.09 0 -2 -8 18.47 1.04 0 2 -8 17.84 1.96 0 -2 -8 22.39 2.18 0 -2 -8 17.95 2.00 0 2 -9 253.66 5.84 0 2 -9 283.00 6.17 0 2 -9 270.86 6.19 0 -2 -9 267.87 9.43 0 2 -9 261.58 9.42 0 -2 -9 267.01 6.10 0 2 -9 256.01 6.06 0 2 -9 275.02 9.26 0 -2 -9 279.16 9.33 0 2 -9 268.64 6.11 0 2 -9 262.37 9.36 0 -2 -9 258.63 9.42 0 -2 -9 260.79 6.11 0 -2 -9 268.50 6.21 0 -2 -9 265.71 6.14 0 2 -9 264.04 6.15 0 2 -10 14.15 2.14 0 -2 -10 15.57 2.24 0 -2 -10 13.44 1.04 0 2 -10 13.72 1.02 0 -2 -10 16.43 1.13 0 2 -10 16.79 1.14 0 -2 -10 15.60 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158.31 6.35 0 -7 -1 148.44 6.47 0 7 -1 163.36 7.12 0 7 -1 161.36 7.07 0 7 1 154.26 6.83 0 7 -2 35.63 3.23 0 7 2 32.26 2.89 0 -7 2 33.15 2.88 0 -7 -2 31.53 2.90 0 7 -2 30.96 2.74 0 7 -2 33.77 1.60 0 7 -2 33.82 2.85 0 -7 -2 32.33 1.53 0 -7 -2 30.81 1.45 0 7 3 186.88 4.78 0 7 3 196.13 7.75 0 -7 -3 191.98 7.81 0 -7 3 192.83 7.35 0 7 -3 192.95 8.04 0 7 -3 194.33 7.55 0 -7 -3 186.60 4.73 0 7 -3 198.00 4.96 0 -7 -3 188.43 4.75 0 7 3 191.30 4.74 0 7 -3 194.38 4.68 0 7 -3 201.97 7.81 0 -7 -3 199.30 4.85 0 -7 3 193.34 4.71 0 -7 -3 192.93 4.75 0 7 -4 90.43 2.93 0 7 4 86.80 2.80 0 -7 -4 91.53 5.32 0 7 -4 90.91 5.43 0 7 -4 85.92 5.16 0 7 4 91.58 5.00 0 -7 4 86.20 4.58 0 7 -4 82.97 4.83 0 -7 -4 87.65 2.86 0 7 -4 89.36 2.98 0 -7 -4 89.82 2.88 0 -7 -4 90.27 2.91 0 7 -4 86.90 2.74 0 7 -4 91.56 2.81 0 7 -4 82.99 5.03 0 -7 4 83.95 2.70 0 -7 4 88.35 2.74 0 -7 -4 86.77 2.76 0 -7 -4 91.67 2.88 0 -7 -5 215.52 5.26 0 -7 5 210.24 5.07 0 -7 -5 214.76 5.18 0 7 -5 210.70 5.11 0 -7 -5 214.34 5.39 0 7 -5 219.09 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281.52 10.31 0 7 -8 282.60 6.49 0 -7 -8 291.51 6.74 0 -7 -9 28.34 1.54 0 7 -9 23.87 2.81 0 -7 -9 23.41 3.02 0 7 -9 28.92 1.63 0 7 -9 27.16 1.59 0 -7 -9 27.02 1.46 0 7 -9 27.00 1.66 0 7 -9 28.18 1.70 0 7 -9 27.29 1.53 0 7 -9 25.88 1.52 0 -7 -9 27.12 1.64 0 7 -9 25.71 1.51 0 -7 -9 28.47 1.55 0 -7 -9 26.14 1.62 0 7 -9 24.31 1.33 0 7 -10 110.63 3.45 0 -7 -10 105.76 3.39 0 -7 -10 106.54 6.60 0 7 -10 100.04 3.40 0 7 -10 106.43 3.43 0 -7 -10 105.48 3.25 0 -7 -10 102.90 3.11 0 7 -10 105.85 3.38 0 -7 -10 105.78 3.28 0 7 -10 102.57 3.31 0 -7 -10 104.14 3.53 0 -7 -10 103.09 3.18 0 -7 -10 106.81 3.59 0 -7 -10 106.22 3.48 0 7 -10 105.39 3.59 0 7 -10 106.03 3.60 0 7 -11 514.70 10.78 0 -7 -11 530.55 10.84 0 -7 -11 508.82 10.48 0 7 -11 515.97 10.74 0 7 -11 504.18 10.56 0 -7 -11 501.52 10.91 0 -7 -11 507.77 10.55 0 7 -11 522.20 10.90 0 7 -11 511.82 10.78 0 7 -11 525.72 11.18 0 -7 -11 496.32 10.88 0 -7 -11 500.05 10.37 0 -7 -11 518.44 10.92 0 7 -11 506.60 11.01 0 7 -11 510.04 11.05 0 -7 -12 30.05 1.63 0 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5.12 0 8 -4 187.41 8.23 0 8 -4 194.43 8.53 0 8 -4 179.72 8.65 0 -8 -4 194.11 8.64 0 8 -4 192.73 8.79 0 8 4 188.30 8.16 0 8 -4 197.24 5.21 0 8 4 192.02 5.03 0 -8 -4 184.19 5.01 0 -8 4 199.09 5.00 0 -8 -4 194.33 5.02 0 -8 -4 191.30 5.07 0 8 4 192.26 5.01 0 8 -5 0.33 0.32 0 8 -5 0.83 0.35 0 -8 -5 0.19 0.34 0 8 -5 1.08 0.89 0 8 -5 0.80 1.01 0 -8 -5 0.55 0.60 0 8 -5 0.85 0.76 0 -8 5 0.48 0.30 0 -8 -5 0.83 0.41 0 8 5 0.35 0.32 0 -8 -5 1.68 0.44 0 -8 -5 0.12 0.29 0 8 -5 0.99 0.81 0 8 5 0.18 0.30 0 -8 -5 0.27 0.32 0 8 -5 0.32 0.31 0 8 -6 31.33 3.49 0 -8 -6 32.83 3.54 0 8 -6 28.21 3.31 0 8 -6 27.23 3.12 0 8 -6 27.72 1.66 0 8 -6 29.75 1.48 0 8 -6 31.78 1.63 0 8 6 32.89 1.66 0 -8 -6 30.26 1.72 0 -8 -6 29.56 1.59 0 -8 -6 29.50 1.54 0 -8 6 29.21 1.47 0 8 6 28.20 1.57 0 8 -6 29.60 1.51 0 -8 -6 29.44 1.73 0 8 -6 32.42 1.72 0 8 -6 31.50 3.23 0 -8 -7 188.63 4.92 0 -8 -7 186.83 4.76 0 8 -7 199.18 4.80 0 8 -7 193.49 5.14 0 8 -7 193.80 5.06 0 8 -7 185.59 5.22 0 8 -7 194.65 5.32 0 -8 -7 193.07 5.31 0 8 -7 191.45 4.78 0 8 -7 181.95 8.85 0 8 -7 191.24 8.58 0 8 7 196.94 5.02 0 -8 -7 189.95 5.23 0 8 -7 189.50 4.81 0 8 -7 190.99 5.10 0 8 -7 189.35 4.79 0 8 -7 181.78 8.99 0 -8 8 290.31 6.81 0 8 -8 302.87 6.72 0 8 -8 302.25 7.04 0 8 -8 290.87 6.72 0 8 -8 274.26 10.57 0 8 -8 300.27 6.92 0 8 -8 285.32 6.56 0 -8 -8 284.49 7.20 0 8 -8 279.29 6.53 0 -8 -8 303.61 7.13 0 8 8 296.68 6.79 0 8 -8 304.61 7.28 0 8 -8 306.07 7.26 0 8 -8 288.33 6.88 0 8 -9 670.07 13.13 0 8 -9 667.87 13.38 0 8 -9 652.47 13.14 0 -8 -9 647.16 13.02 0 -8 -9 672.99 19.72 0 -8 -9 646.54 13.33 0 8 -9 673.88 13.32 0 8 -9 653.44 13.32 0 -8 -9 650.42 13.30 0 8 -9 655.60 13.67 0 8 -9 655.44 13.64 0 8 -10 45.21 1.97 0 -8 -10 48.09 2.18 0 -8 -10 47.12 2.20 0 8 10 48.14 1.92 0 8 -10 44.53 2.15 0 -8 -10 46.96 2.06 0 8 -10 46.92 2.18 0 8 -10 46.23 2.04 0 8 -10 45.16 1.98 0 -8 -10 48.80 2.01 0 8 -10 47.77 1.96 0 -8 -10 42.31 1.85 0 8 -10 46.91 1.97 0 8 -11 5.35 0.63 0 -8 -11 6.53 0.78 0 8 11 6.31 0.62 0 -8 -11 5.61 0.74 0 8 -11 5.17 0.64 0 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38.96 1.80 0 -9 -4 38.82 1.92 0 9 4 37.14 1.90 0 9 -4 40.97 2.05 0 9 -4 42.01 3.85 0 9 -5 1003.06 19.27 0 9 -5 999.80 19.09 0 9 -5 1026.12 19.76 0 9 5 994.27 19.47 0 -9 -5 1009.42 19.68 0 9 -5 1000.20 25.27 0 9 -5 1010.09 19.74 0 -9 -5 1003.38 19.89 0 9 5 1020.73 19.56 0 9 -5 1028.12 26.10 0 -9 -5 985.21 25.89 0 9 -5 1004.58 25.98 0 -9 -5 964.84 19.50 0 -9 5 1015.36 19.34 0 -9 5 1028.17 19.37 0 -9 -5 1010.80 19.46 0 9 -6 26.88 1.66 0 9 -6 28.40 1.54 0 9 -6 29.55 1.67 0 9 -6 27.11 1.46 0 9 6 26.96 1.55 0 -9 -6 27.05 1.70 0 -9 -6 27.22 3.31 0 9 -6 25.35 3.15 0 9 -6 26.21 3.11 0 9 -6 27.56 1.42 0 -9 -6 29.63 1.74 0 9 6 27.99 1.58 0 -9 -6 28.88 1.56 0 -9 6 28.63 1.49 0 9 -6 29.56 3.46 0 -9 -7 272.92 6.36 0 9 -7 296.21 7.04 0 9 -7 267.36 6.48 0 9 -7 280.49 6.90 0 9 -7 264.62 10.74 0 -9 -7 277.23 11.40 0 9 -7 281.28 6.75 0 9 7 277.51 6.60 0 -9 -7 286.27 6.99 0 9 7 277.98 6.58 0 9 -7 273.46 6.33 0 -9 -7 272.95 6.89 0 9 -7 287.33 6.47 0 9 -7 285.62 6.46 0 -9 -7 268.33 6.36 0 9 -7 276.67 11.49 0 9 -8 174.49 4.95 0 9 -8 180.71 5.00 0 -9 -8 173.02 4.55 0 9 -8 180.66 4.58 0 9 -8 176.29 4.58 0 9 -8 180.21 4.83 0 -9 -8 173.64 4.93 0 9 8 174.34 4.57 0 -9 -8 174.79 4.90 0 9 8 173.71 4.63 0 -9 -8 185.52 5.09 0 -9 8 177.16 4.67 0 9 -9 64.56 2.44 0 9 -9 66.04 2.35 0 9 -9 68.95 2.37 0 9 -9 64.10 2.59 0 9 -9 68.54 2.66 0 -9 -9 65.33 2.34 0 -9 -9 67.95 2.70 0 9 9 68.56 2.38 0 9 -9 63.54 2.19 0 -9 -9 66.07 2.44 0 -9 -9 70.01 2.56 0 9 -10 23.21 1.23 0 9 -10 25.43 1.31 0 9 -10 23.86 1.20 0 -9 -10 23.49 1.28 0 9 -10 25.48 1.48 0 -9 -10 23.77 1.28 0 9 -10 26.91 1.51 0 9 -10 26.59 1.36 0 9 10 22.21 1.17 0 -9 -11 4.06 0.62 0 9 -11 3.60 0.48 0 -9 -11 4.26 0.61 0 9 -11 4.17 0.49 0 9 -11 4.61 0.54 0 9 -11 3.99 0.49 0 9 -11 3.69 0.62 0 -9 -11 4.11 0.60 0 9 -11 3.75 0.57 0 -9 -11 4.10 0.52 0 -9 -12 2.21 0.42 0 -9 -12 1.89 0.42 0 9 -12 2.32 0.45 0 9 -12 2.19 0.44 0 -9 -12 2.00 0.35 0 -9 -12 2.21 0.31 0 -9 -13 158.00 3.39 0 9 -13 161.07 3.54 0 9 -13 158.49 3.51 0 -9 -13 153.35 3.47 0 -9 -13 155.88 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293.43 7.00 0 10 -7 285.74 6.89 0 10 -7 276.26 6.37 0 -10 -7 288.19 6.95 0 10 7 283.49 6.62 0 10 -7 294.31 6.81 0 -10 7 293.08 6.77 0 -10 -8 8.52 0.89 0 -10 -8 7.66 0.84 0 10 -8 7.60 0.86 0 10 -8 7.65 0.86 0 10 8 9.79 0.82 0 -10 -8 8.26 0.88 0 -10 8 8.40 0.78 0 10 -8 8.84 0.84 0 10 -9 122.96 3.37 0 -10 -9 116.63 3.54 0 -10 -9 121.39 3.44 0 10 -9 124.14 3.61 0 10 -9 119.38 3.53 0 -10 -9 122.54 3.61 0 10 9 113.94 3.13 0 -10 -9 118.37 3.34 0 10 -9 118.21 3.03 0 -10 -10 68.32 2.35 0 10 -10 67.30 2.36 0 10 -10 59.14 1.82 0 10 -10 63.16 2.23 0 10 -10 63.35 2.24 0 10 -10 64.95 2.04 0 -10 -11 71.44 2.26 0 10 -11 74.37 2.29 0 -10 -11 71.12 2.22 0 10 -11 67.53 2.14 0 -10 -12 108.58 2.77 0 -10 -12 107.04 2.71 0 -10 -12 107.94 2.70 0 10 -12 112.25 2.77 0 10 -13 0.20 0.14 0 -10 -13 0.59 0.17 0 10 -13 0.21 0.14 0 11 0 0.06 0.34 0 11 0 0.21 0.38 0 -11 0 -0.14 0.38 0 -11 0 0.27 0.42 0 11 -1 105.90 3.31 0 11 1 103.87 3.25 0 11 -1 101.81 3.51 0 11 1 98.96 3.42 0 -11 1 104.91 3.49 0 11 -1 93.82 3.46 0 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5.93 0.63 0 11 -7 6.06 0.73 0 -11 -7 5.31 0.64 0 -11 -7 6.23 0.75 0 -11 7 6.19 0.68 0 -11 -8 73.10 2.37 0 11 -8 80.02 2.41 0 -11 -8 79.23 2.55 0 11 8 69.55 2.15 0 -11 -8 78.26 2.53 0 11 8 74.01 2.29 0 11 -8 81.45 2.53 0 11 -8 76.10 2.52 0 -11 -8 78.11 2.45 0 -11 8 73.26 2.23 0 -11 -8 78.15 2.55 0 -11 -9 0.25 0.31 0 11 -9 0.20 0.25 0 11 -9 0.57 0.28 0 11 9 0.12 0.22 0 -11 -9 0.04 0.25 0 -11 -9 0.29 0.30 0 11 -9 -0.09 0.21 0 -11 -9 0.08 0.29 0 -11 -10 32.50 1.24 0 11 -10 33.27 1.30 0 -11 -10 33.35 1.29 0 11 -11 66.97 1.81 0 -11 -11 64.83 1.77 0 -11 -11 63.30 1.71 0 11 -11 68.96 1.82 0 12 0 49.53 1.96 0 -12 0 48.36 2.04 0 -12 0 49.02 2.12 0 -12 0 51.04 2.18 0 12 1 36.65 1.64 0 -12 1 38.65 1.83 0 -12 1 37.03 1.80 0 -12 -1 37.57 1.85 0 12 1 40.94 1.95 0 12 -1 36.39 1.85 0 -12 1 38.79 1.71 0 -12 -1 38.89 1.84 0 12 2 24.92 1.31 0 12 -2 23.35 1.38 0 12 2 24.09 1.37 0 -12 2 25.16 1.42 0 -12 2 25.79 1.43 0 -12 -2 24.51 1.42 0 12 -2 24.16 1.45 0 -12 -2 23.20 1.41 0 12 2 21.25 1.41 0 12 3 271.70 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3.69 2 -9 -4 110.60 3.52 2 -9 -4 111.95 3.62 -2 -9 4 111.32 3.61 -2 -9 4 111.99 3.59 2 -9 -4 111.72 3.67 -2 9 4 110.64 3.71 2 9 -3 2.67 1.10 2 9 -3 2.34 0.54 -2 9 3 2.40 0.46 2 9 -3 1.90 0.90 -2 9 3 1.76 0.92 2 9 -3 1.19 0.98 2 -9 -3 1.75 0.87 2 9 -3 1.53 0.95 -2 -9 3 1.99 0.94 -2 9 3 2.37 0.56 2 -9 -3 1.93 0.46 2 -9 -3 1.91 0.50 -2 -9 3 2.03 0.52 -2 -9 3 1.78 0.50 -2 -9 3 1.72 0.45 2 9 -3 1.85 0.52 -2 9 3 2.41 0.56 2 9 -2 538.12 16.17 2 9 -2 520.90 11.20 -2 9 2 545.25 10.87 2 9 -2 524.02 15.56 -2 9 2 508.04 15.85 -2 9 2 558.69 17.09 2 -9 -2 541.18 15.74 2 9 -2 577.02 17.34 2 9 -2 540.69 16.93 2 -9 -2 523.61 10.96 -2 9 2 552.63 11.62 2 -9 -2 537.78 11.50 -2 -9 2 530.86 11.44 -2 -9 2 548.24 11.58 -2 -9 2 533.67 11.43 -2 9 2 542.99 11.60 2 9 -2 548.62 11.71 2 9 -1 0.74 0.60 -2 9 1 2.39 0.46 2 9 -1 1.99 0.49 2 9 -1 1.71 0.99 -2 9 1 2.07 1.12 2 -9 -1 1.81 0.86 -2 -9 1 2.76 1.17 -2 9 1 1.26 0.44 2 9 -1 3.17 0.60 2 -9 -1 1.65 0.49 2 9 -1 3.08 1.10 -2 9 1 2.63 1.15 -2 -9 1 2.27 0.53 2 -9 -1 2.71 0.58 -2 -9 1 1.54 0.52 -2 -9 1 2.09 0.54 -2 -9 0 72.54 2.81 2 9 0 65.63 2.51 -2 9 0 67.15 2.61 -2 9 0 69.21 2.39 2 -9 0 63.93 4.30 2 9 0 67.34 5.02 -2 -9 0 63.95 4.94 -2 -9 0 68.59 2.64 2 -9 0 68.36 2.67 2 -9 0 67.89 2.69 -2 9 0 68.41 2.47 2 9 0 68.10 2.59 -2 9 0 73.76 5.17 -2 9 0 64.13 2.36 2 9 0 69.31 4.72 2 -9 1 30.75 1.62 -2 -9 -1 33.13 1.84 2 9 1 29.95 1.58 -2 9 -1 32.41 1.72 -2 9 -1 29.06 1.48 -2 9 -1 31.18 3.49 -2 -9 -1 30.56 3.42 2 9 1 29.22 3.26 -2 -9 -1 29.71 1.68 -2 -9 -1 29.15 1.69 2 -9 1 30.30 1.69 2 -9 1 29.54 1.68 -2 9 -1 29.88 1.56 2 9 1 29.08 1.57 -2 -9 -1 28.02 1.52 -2 9 -1 27.66 3.18 -2 9 -1 28.52 1.52 -2 9 -1 28.32 2.92 2 -9 2 12.61 0.98 -2 -9 -2 12.62 1.16 -2 9 -2 12.48 1.08 2 9 2 13.66 1.08 -2 -9 -2 12.52 2.22 2 9 2 9.23 1.79 -2 9 -2 9.76 2.04 -2 -9 -2 13.81 1.17 -2 9 -2 12.91 1.04 2 9 2 11.19 0.95 -2 -9 -2 11.77 1.00 -2 9 -2 14.94 1.25 -2 9 -2 11.09 2.06 2 -9 2 11.11 1.02 -2 -9 -2 14.99 1.19 2 -9 2 14.37 1.15 -2 9 -2 12.50 2.01 -2 9 -2 13.67 1.07 -2 -9 -2 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4 2 441.98 9.28 -7 -4 2 438.33 9.29 -7 -4 2 433.99 9.47 -7 4 2 444.24 9.55 -7 4 2 444.20 9.31 -7 -4 2 445.19 9.36 -7 4 1 396.32 12.64 -7 -4 1 386.88 12.59 -7 4 1 393.18 8.66 -7 -4 1 399.02 8.72 -7 -4 1 423.79 14.11 -7 -4 1 408.23 8.71 -7 4 1 423.63 8.78 -7 -4 1 408.40 8.48 -7 4 1 403.95 8.60 -7 -4 1 390.77 8.45 -7 4 1 388.79 8.74 -7 4 1 405.69 8.69 -7 -4 1 406.00 8.70 -7 4 1 405.51 8.64 -7 -4 1 409.19 8.66 -7 -4 1 399.55 8.83 -7 -4 1 393.73 8.63 -7 4 1 379.59 8.55 -7 4 1 399.41 8.89 -7 -4 1 403.75 8.81 -7 -4 1 417.64 12.60 -7 4 1 399.77 12.39 -7 4 1 404.97 12.10 -7 -4 1 394.93 12.75 -7 -4 0 10.81 2.11 -7 -4 0 8.90 0.86 -7 4 0 9.52 0.89 -7 4 0 9.53 0.89 -7 -4 0 9.15 0.90 -7 4 0 9.77 0.87 -7 -4 0 9.81 0.84 -7 -4 0 9.21 1.59 -7 4 0 8.92 0.92 -7 -4 0 12.53 1.94 -7 4 0 8.68 1.41 -7 4 0 9.13 0.91 -7 4 0 8.06 0.80 -7 -4 0 9.51 0.88 -7 -4 0 9.64 0.93 -7 4 0 9.19 0.80 -7 4 0 9.79 0.95 -7 4 0 9.07 0.85 -7 -4 0 8.85 0.85 -7 -4 0 9.67 0.92 -7 4 0 5.63 1.31 -7 -4 0 7.67 1.57 -7 -4 0 9.85 1.75 -7 4 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288.56 6.43 -7 -4 -9 300.12 6.40 -7 4 -9 296.71 6.54 -7 -4 -9 295.35 6.43 -7 -4 -10 32.93 1.34 -7 4 -10 31.86 1.35 -7 -4 -10 34.01 1.33 -7 4 -10 33.87 1.38 -7 -4 -10 31.87 1.30 -7 -4 -11 87.39 2.19 -7 4 -11 89.77 2.26 7 5 -16 59.72 1.69 -7 5 16 61.25 1.77 -7 5 16 63.53 1.83 -7 -5 16 62.32 1.71 -7 -5 16 58.60 1.69 7 -5 -15 4.01 0.45 -7 5 15 4.27 0.52 -7 -5 15 3.35 0.38 -7 5 15 3.80 0.51 7 5 -15 3.70 0.46 7 5 -15 4.02 0.49 -7 -5 15 4.10 0.50 -7 -5 15 4.11 0.50 -7 5 14 143.70 3.77 -7 5 14 142.59 3.86 -7 -5 14 137.31 3.64 7 -5 -14 129.97 3.31 7 -5 -14 142.07 3.68 7 5 -14 145.07 3.80 7 5 -14 146.02 3.81 -7 -5 14 142.26 3.75 -7 -5 14 145.53 3.86 7 -5 -13 20.68 1.10 -7 -5 13 22.74 1.35 7 -5 -13 22.17 1.26 7 -5 -13 21.49 1.30 7 5 -13 23.36 1.37 -7 -5 13 23.51 1.34 -7 -5 13 23.27 1.40 -7 5 13 21.38 1.23 -7 5 13 22.51 1.33 7 5 -12 26.91 1.56 7 -5 -12 26.39 1.33 7 -5 -12 30.92 1.58 -7 5 12 26.62 1.51 -7 -5 12 27.70 1.61 7 5 -12 26.43 1.35 7 -5 -12 25.99 1.45 -7 -5 12 25.21 1.53 -7 -5 12 24.58 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398.99 8.70 -7 -5 5 405.82 8.74 -7 -5 5 395.99 8.46 -7 5 5 409.53 9.03 -7 5 5 400.15 8.49 -7 -5 5 402.67 8.51 7 5 -5 405.04 8.71 -7 5 5 394.17 12.15 -7 -5 5 399.29 12.24 -7 5 5 445.85 13.99 -7 -5 5 415.36 14.18 -7 5 4 30.49 2.88 -7 -5 4 30.25 2.86 -7 -5 4 34.41 1.54 7 5 -4 32.64 1.60 -7 -5 4 28.50 2.84 -7 5 4 34.23 3.09 -7 -5 4 39.72 3.85 -7 -5 4 31.89 1.53 -7 5 4 33.15 1.55 -7 -5 4 30.83 1.44 -7 -5 4 33.25 1.75 7 5 -4 30.96 1.58 -7 5 4 31.84 1.56 -7 -5 4 32.18 1.43 -7 5 4 28.92 1.73 -7 -5 4 30.34 1.52 -7 -5 4 30.45 1.55 -7 5 4 33.74 3.35 -7 -5 4 31.90 3.47 -7 -5 4 29.47 1.48 -7 -5 4 31.43 2.88 -7 5 4 36.65 3.03 -7 -5 4 34.04 1.61 -7 -5 4 31.51 1.50 -7 -5 4 30.27 1.65 -7 5 4 33.47 1.78 -7 5 4 33.14 1.55 -7 -5 4 33.23 1.54 -7 5 3 22.11 2.45 -7 -5 3 24.32 2.57 -7 -5 3 25.28 1.39 7 5 -3 26.30 1.37 -7 -5 3 30.89 2.93 -7 5 3 20.81 2.45 -7 -5 3 26.96 3.27 -7 -5 3 24.44 1.33 -7 5 3 26.44 1.37 -7 -5 3 25.89 1.31 -7 -5 3 23.05 1.41 7 5 -3 24.16 1.33 -7 5 3 23.19 1.28 -7 -5 3 25.84 1.29 -7 -5 3 25.51 1.36 -7 5 3 24.94 1.57 -7 5 3 25.47 2.86 -7 -5 3 25.91 3.14 -7 -5 3 25.53 1.35 -7 -5 3 24.11 1.40 -7 -5 3 25.04 2.55 -7 5 3 24.09 2.48 -7 -5 3 25.65 1.34 -7 -5 3 23.19 1.43 -7 5 3 26.92 1.59 -7 5 3 26.39 1.37 -7 -5 3 23.37 1.30 -7 5 2 275.03 9.73 -7 -5 2 267.39 9.64 -7 -5 2 282.93 6.53 -7 -5 2 261.22 10.99 -7 -5 2 279.45 6.35 -7 5 2 274.97 6.33 -7 -5 2 290.07 6.27 -7 5 2 278.96 6.56 -7 -5 2 262.05 6.42 -7 -5 2 268.48 6.21 -7 5 2 275.98 6.79 -7 5 2 280.65 6.35 -7 -5 2 276.22 6.34 -7 -5 2 272.23 6.30 -7 -5 2 274.62 6.60 -7 5 2 296.28 6.92 -7 -5 2 278.01 6.32 -7 -5 2 282.21 6.61 -7 5 2 277.23 9.46 -7 -5 2 279.77 9.60 -7 5 2 265.22 9.83 -7 -5 2 281.77 10.86 -7 -5 1 4.46 0.59 -7 -5 1 5.85 0.67 -7 5 1 5.50 0.74 -7 5 1 5.46 0.71 -7 -5 1 5.42 1.45 -7 5 1 7.46 1.40 -7 5 1 4.71 0.75 -7 -5 1 2.08 1.04 -7 -5 1 5.24 0.63 -7 5 1 5.35 0.65 -7 -5 1 5.00 0.67 -7 -5 1 4.15 0.57 -7 -5 1 5.06 0.69 -7 -5 1 3.83 0.57 -7 -5 1 4.92 0.71 -7 5 1 4.91 1.16 -7 -5 1 4.19 1.12 -7 5 1 2.33 0.90 -7 -5 1 4.05 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82.97 1.97 -7 6 16 81.87 1.93 -7 -6 16 81.52 1.91 7 6 -16 81.34 1.91 -7 6 15 62.92 1.93 -7 6 15 59.87 1.85 -7 -6 15 61.81 1.87 -7 -6 15 62.30 1.86 7 6 -15 60.49 1.86 -7 6 14 77.86 2.39 7 6 -14 80.42 2.43 -7 -6 14 78.62 2.28 -7 6 14 81.04 2.49 7 -6 -14 71.38 2.00 -7 -6 14 76.95 2.38 -7 -6 14 79.79 2.46 7 -6 -14 77.52 2.34 7 -6 -13 65.26 2.25 7 -6 -13 65.99 2.32 7 6 -13 63.67 2.23 -7 -6 13 65.56 2.29 -7 -6 13 65.65 2.35 -7 -6 13 67.44 2.32 -7 6 13 66.60 2.31 7 6 -12 11.03 0.94 7 -6 -12 10.35 0.90 7 -6 -12 10.79 0.95 -7 -6 12 11.26 0.98 -7 6 12 8.97 0.83 7 -6 -12 10.31 0.87 -7 -6 12 10.74 0.96 -7 6 12 11.76 0.97 7 -6 -11 83.44 2.91 7 6 -11 89.80 3.00 7 6 -11 86.29 3.01 -7 6 11 86.16 2.97 -7 6 11 83.89 3.00 -7 -6 11 85.51 3.05 7 -6 -11 82.66 2.89 -7 6 11 87.43 2.97 7 6 -10 11.45 1.06 -7 -6 10 10.68 1.01 -7 6 10 10.84 1.04 -7 6 10 12.56 1.07 -7 6 10 11.75 1.07 -7 -6 10 11.50 1.08 7 -6 -10 11.66 1.03 -7 6 9 62.77 2.54 -7 -6 9 57.84 2.54 7 -6 -9 54.02 2.42 -7 -6 9 58.44 2.46 -7 6 9 58.56 2.55 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2.75 -7 6 4 84.30 3.20 -7 -6 4 84.03 2.77 -7 -6 4 87.22 2.81 -7 -6 4 90.84 3.01 -7 -6 4 85.37 2.73 7 6 -4 82.67 2.88 -7 -6 4 90.42 6.08 7 -6 -4 95.17 3.05 -7 6 4 87.43 2.83 -7 -6 3 32.52 1.44 7 6 -3 31.20 1.59 -7 -6 3 30.98 1.67 -7 6 3 33.08 1.60 -7 -6 3 34.18 3.69 -7 6 3 32.65 3.25 -7 -6 3 31.69 1.41 -7 -6 3 30.81 1.49 -7 -6 3 33.92 1.63 7 6 -3 31.20 1.60 -7 -6 3 34.11 1.67 -7 -6 3 37.34 3.81 -7 -6 3 34.67 1.72 7 -6 -3 34.12 1.68 -7 6 3 31.71 1.52 -7 6 2 667.63 13.30 -7 -6 2 639.65 12.74 -7 -6 2 641.76 13.20 7 6 -2 654.04 13.00 -7 -6 2 632.76 18.99 -7 6 2 632.98 17.56 -7 -6 2 658.82 13.25 -7 6 2 647.89 13.65 -7 -6 2 669.66 13.27 -7 6 2 667.69 13.42 -7 -6 2 657.21 13.29 -7 -6 2 681.08 19.68 -7 -6 2 655.74 12.78 7 -6 -2 665.90 13.08 -7 6 1 631.84 13.24 -7 -6 1 618.42 12.96 7 -6 -1 658.13 13.12 -7 6 1 679.33 13.79 -7 -6 1 670.20 13.25 -7 -6 1 624.53 19.28 -7 -6 1 647.95 13.30 -7 -6 1 660.85 19.01 -7 -6 1 636.98 17.14 7 -6 -1 653.08 12.91 -7 6 1 664.81 13.54 -7 -6 1 677.40 12.86 -7 6 1 662.33 13.45 -7 -6 1 667.25 13.41 -7 6 1 649.88 13.47 -7 -6 0 20.42 1.37 -7 -6 0 14.79 2.33 -7 6 0 16.14 1.29 -7 6 0 16.76 1.09 -7 6 0 17.29 1.39 -7 -6 0 20.06 1.28 -7 -6 0 18.27 1.13 -7 6 0 19.15 1.38 -7 -6 0 16.60 1.28 -7 6 0 19.50 1.40 -7 6 0 18.14 1.32 -7 6 0 16.77 1.26 -7 -6 -1 54.43 2.39 -7 -6 -1 52.31 4.26 -7 6 -1 63.59 2.29 -7 6 -1 60.22 2.62 -7 -6 -1 59.26 2.28 -7 -6 -1 57.70 2.15 -7 6 -1 62.10 2.55 -7 -6 -1 59.21 2.48 -7 6 -1 58.12 2.50 -7 6 -1 59.37 2.41 -7 6 -1 58.30 2.44 -7 6 -1 58.55 2.54 -7 -6 -1 58.46 2.22 -7 6 -2 656.72 13.49 -7 -6 -2 638.11 12.78 -7 6 -2 654.77 13.66 -7 -6 -2 657.59 13.13 -7 6 -2 630.58 13.09 -7 -6 -2 661.82 13.55 -7 6 -2 654.30 13.65 -7 6 -2 683.86 13.64 -7 -6 -2 662.61 12.99 -7 6 -2 662.03 13.61 -7 -6 -2 649.48 13.40 -7 6 -2 667.63 13.41 -7 6 -2 641.24 13.22 -7 6 -2 650.84 13.73 -7 -6 -2 640.07 13.02 -7 -6 -2 686.71 13.59 -7 6 -3 259.49 6.41 -7 6 -3 258.29 5.91 -7 -6 -3 250.01 5.91 -7 -6 -3 249.66 6.13 -7 6 -3 256.23 6.14 -7 6 -3 261.02 6.55 -7 6 -3 250.08 6.43 -7 6 -3 267.29 6.54 -7 -6 -3 255.84 6.02 -7 -6 -3 260.01 6.30 -7 6 -3 258.88 6.31 -7 6 -3 263.20 6.26 -7 -6 -3 263.53 5.94 -7 6 -3 259.82 6.61 -7 -6 -3 245.27 5.91 -7 -6 -3 260.19 6.44 -7 6 -4 43.96 2.04 -7 -6 -4 43.60 1.87 -7 6 -4 42.10 1.94 -7 -6 -4 46.02 1.84 -7 -6 -4 41.51 1.90 -7 6 -4 43.99 1.78 -7 -6 -4 44.56 1.86 -7 -6 -4 46.52 2.00 -7 6 -4 40.62 1.88 -7 6 -4 44.00 2.15 -7 6 -4 44.64 2.11 -7 6 -4 43.45 2.07 -7 6 -4 43.63 2.01 -7 6 -4 38.55 1.99 -7 -6 -4 45.88 1.89 -7 6 -5 0.61 0.38 -7 6 -5 0.80 0.41 -7 -6 -5 0.97 0.36 -7 -6 -5 0.48 0.38 -7 6 -5 1.06 0.45 -7 6 -5 1.00 0.48 -7 -6 -5 0.75 0.35 -7 6 -5 0.69 0.32 -7 6 -5 0.72 0.38 -7 -6 -5 0.78 0.38 -7 6 -5 0.73 0.39 -7 -6 -5 1.81 0.44 -7 -6 -5 1.40 0.47 -7 6 -5 0.53 0.40 -7 -6 -5 1.20 0.41 -7 6 -5 0.88 0.42 -7 6 -6 128.43 3.39 -7 -6 -6 135.86 3.68 -7 6 -6 134.11 3.74 -7 -6 -6 131.42 3.78 -7 6 -6 132.99 3.77 -7 -6 -6 130.86 3.79 -7 -6 -6 137.62 3.81 -7 6 -6 127.98 3.73 -7 6 -6 132.61 3.73 -7 -6 -6 137.16 3.58 -7 6 -6 136.43 3.80 -7 6 -6 134.65 3.89 -7 -6 -6 130.73 3.62 -7 6 -7 59.64 1.93 -7 -6 -7 64.31 2.19 -7 -6 -7 62.97 2.22 -7 6 -7 65.10 2.38 -7 6 -7 67.26 2.27 -7 -6 -7 63.27 2.15 -7 6 -7 63.93 2.27 -7 -6 -7 65.56 2.26 -7 6 -7 62.99 2.21 -7 6 -7 66.67 2.28 -7 -6 -7 68.72 2.17 -7 -6 -7 65.48 2.28 -7 -6 -7 64.11 2.29 -7 -6 -8 74.32 2.31 -7 -6 -8 72.94 2.32 -7 6 -8 74.58 2.41 -7 -6 -8 76.68 2.26 -7 6 -8 73.51 2.29 -7 6 -8 78.17 2.38 -7 -6 -8 72.60 2.21 -7 6 -8 72.79 2.27 -7 -6 -8 73.57 2.19 -7 -6 -8 70.93 2.23 -7 -6 -9 20.80 0.97 -7 6 -9 21.71 0.98 -7 -6 -9 21.29 0.96 -7 6 -9 20.31 1.02 -7 -6 -9 19.70 0.94 -7 -6 -10 2.00 0.28 -7 6 -10 1.99 0.32 -7 -6 -10 2.19 0.28 -7 -6 -10 1.99 0.28 -7 6 -10 2.05 0.29 -7 7 15 42.54 1.32 7 7 -15 45.96 1.35 -7 7 15 47.51 1.38 7 -7 -15 42.99 1.27 -7 7 15 44.34 1.30 -7 -7 15 45.27 1.34 -7 -7 15 45.81 1.35 -7 -7 14 128.78 3.17 -7 7 14 135.44 3.23 7 -7 -14 128.50 3.10 7 7 -14 129.96 3.16 -7 7 14 126.70 3.10 -7 -7 13 6.66 0.66 -7 7 13 7.14 0.66 -7 -7 13 7.16 0.65 -7 7 13 6.27 0.64 7 -7 -13 7.38 0.67 7 -7 -13 7.41 0.66 -7 -7 12 137.69 3.69 -7 7 12 144.01 3.78 7 -7 -12 134.08 3.63 -7 -7 12 145.93 3.86 7 -7 -12 137.61 3.73 7 7 -12 136.12 3.61 -7 -7 11 39.74 1.75 -7 7 11 44.48 1.90 -7 -7 11 42.03 1.90 7 -7 -11 42.36 1.84 -7 7 11 39.93 1.86 7 7 -11 42.18 1.79 7 -7 -11 36.96 1.80 7 7 -11 41.01 1.87 -7 -7 10 8.54 0.86 -7 7 10 7.73 0.83 -7 -7 10 8.69 0.90 7 -7 -10 8.02 0.84 -7 7 10 8.16 0.87 7 7 -10 8.76 0.89 7 -7 -10 7.89 0.85 -7 -7 9 119.95 3.68 -7 7 9 120.92 3.74 -7 -7 9 119.90 3.80 -7 7 9 117.84 3.70 7 -7 -9 117.00 3.64 7 -7 -9 117.14 3.69 7 7 -9 115.22 3.66 -7 -7 8 240.64 5.88 -7 -7 8 239.57 6.03 -7 7 8 245.87 6.18 7 7 -8 249.18 6.15 7 -7 -8 249.30 6.11 7 -7 -8 230.79 6.09 -7 7 8 250.65 6.18 7 -7 -7 18.15 1.29 7 7 -7 18.66 1.31 -7 7 7 19.68 1.30 -7 -7 7 17.81 2.76 -7 7 7 21.61 2.86 -7 -7 7 18.99 1.39 7 7 -7 19.29 1.36 7 -7 -7 21.61 1.47 -7 7 7 19.13 1.34 -7 -7 7 21.57 1.30 -7 -7 7 19.89 1.30 -7 -7 7 16.32 2.52 -7 7 7 21.82 1.45 7 -7 -6 67.67 2.58 7 7 -6 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181.49 4.73 -8 5 9 200.28 4.84 -8 -5 9 188.65 4.79 8 5 -9 192.67 4.81 -8 5 9 210.27 5.24 -8 -5 9 185.51 4.76 -8 -5 9 193.01 5.16 -8 5 9 193.69 5.37 -8 -5 9 211.95 5.33 -8 5 9 198.68 5.25 8 5 -9 199.22 5.12 -8 5 8 7.93 0.78 -8 -5 8 8.80 0.82 -8 5 8 8.89 0.95 -8 5 8 8.51 0.80 -8 -5 8 8.64 0.80 8 5 -8 8.33 0.77 8 -5 -8 8.90 0.82 -8 5 8 9.57 0.92 -8 -5 8 8.07 1.82 -8 -5 8 8.38 0.79 -8 5 8 9.40 0.84 -8 5 8 8.33 0.94 -8 -5 8 9.01 0.92 -8 -5 8 9.51 0.94 -8 5 8 8.28 1.81 8 -5 -8 8.61 0.92 8 5 -8 8.90 0.87 -8 -5 7 4.69 0.63 -8 5 7 4.38 0.59 -8 5 7 4.86 0.62 -8 -5 7 4.82 0.63 8 -5 -7 4.80 0.69 8 5 -7 5.00 0.68 -8 -5 7 5.70 0.67 -8 5 7 5.62 0.66 -8 -5 7 5.16 0.70 -8 -5 7 5.49 0.70 -8 -5 7 5.16 0.79 -8 5 7 3.67 0.59 -8 -5 7 5.45 1.61 8 5 -7 5.69 0.66 8 -5 -7 4.88 0.64 -8 -5 7 3.45 1.33 -8 5 7 4.09 1.36 -8 5 7 5.48 0.75 -8 -5 6 120.87 3.88 -8 -5 6 118.64 7.22 -8 5 6 118.82 3.54 -8 5 6 123.83 4.01 -8 -5 6 120.07 3.62 -8 -5 6 122.51 3.70 -8 5 6 117.78 3.44 -8 -5 6 120.16 3.49 -8 -5 6 120.23 3.78 -8 5 6 124.35 3.86 -8 5 6 110.24 3.38 -8 -5 6 114.82 3.47 8 5 -6 121.57 3.58 8 -5 -6 125.76 3.75 -8 -5 6 122.39 3.55 -8 5 6 115.54 3.48 -8 5 6 121.86 3.51 -8 -5 6 119.24 3.51 -8 5 6 124.05 7.02 -8 -5 6 113.83 7.03 -8 5 5 111.76 3.36 -8 -5 5 112.54 3.37 -8 5 5 105.80 5.79 -8 5 5 106.97 5.94 -8 -5 5 108.30 3.33 -8 5 5 108.70 3.35 -8 -5 5 114.79 3.68 -8 5 5 112.55 3.30 -8 -5 5 111.61 3.16 -8 -5 5 110.25 3.34 -8 -5 5 115.85 3.51 -8 5 5 115.35 3.82 -8 5 5 109.80 3.29 -8 -5 5 110.15 3.32 -8 5 5 112.43 3.68 -8 -5 5 115.88 3.65 -8 5 5 109.39 3.29 -8 -5 5 111.12 3.36 8 5 -5 109.77 3.30 -8 -5 5 98.60 5.52 -8 5 5 111.20 6.52 -8 -5 5 113.36 6.91 -8 5 4 235.18 9.24 -8 -5 4 260.31 5.87 -8 5 4 253.17 5.99 -8 -5 4 260.93 11.02 -8 -5 4 248.87 5.99 -8 5 4 231.60 5.91 -8 -5 4 257.99 5.85 -8 -5 4 252.24 6.24 -8 -5 4 242.73 10.45 -8 -5 4 257.05 5.80 -8 -5 4 238.07 5.76 -8 -5 4 253.43 6.05 -8 5 4 252.12 6.46 -8 5 4 260.41 10.24 -8 -5 4 269.12 10.89 -8 5 4 252.71 5.93 -8 -5 4 249.36 5.96 -8 -5 4 236.67 9.12 -8 5 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5 2 0.67 0.60 -8 -5 1 125.98 3.56 -8 5 1 129.47 3.73 -8 -5 1 119.89 6.13 -8 -5 1 124.18 3.84 -8 5 1 122.55 3.89 -8 -5 1 126.31 6.74 -8 5 1 134.18 3.96 -8 5 1 129.28 3.64 -8 -5 1 124.68 3.63 -8 -5 1 125.95 3.69 -8 5 1 128.01 3.70 -8 -5 1 127.48 3.84 -8 5 1 125.03 3.99 -8 5 1 124.06 3.60 -8 -5 1 120.78 3.59 -8 -5 1 126.22 3.88 -8 5 1 124.42 6.39 -8 -5 1 122.40 3.64 -8 5 1 125.52 3.65 -8 5 0 950.78 18.14 -8 5 0 906.85 17.68 -8 5 0 919.46 18.17 -8 -5 0 939.45 18.04 -8 -5 0 896.56 17.63 -8 5 0 908.72 17.63 -8 -5 0 925.97 17.97 -8 5 0 916.06 18.03 -8 5 0 900.08 17.52 -8 -5 0 887.35 17.52 -8 -5 0 911.84 17.65 -8 5 0 934.68 17.69 -8 5 0 928.25 18.21 -8 -5 0 943.27 17.57 -8 5 0 901.71 18.15 -8 5 0 896.60 17.54 -8 -5 0 926.68 17.62 -8 -5 0 916.43 17.94 -8 -5 -1 1.20 0.41 -8 5 -1 1.25 0.40 -8 -5 -1 1.09 0.49 -8 -5 -1 1.95 0.46 -8 5 -1 1.27 0.55 -8 -5 -1 1.19 0.40 -8 5 -1 1.75 0.54 -8 5 -1 0.67 0.36 -8 5 -1 1.80 0.53 -8 5 -1 1.14 0.49 -8 5 -1 1.27 0.39 -8 -5 -1 2.37 0.47 -8 5 -1 1.19 0.40 -8 -5 -1 2.04 0.47 -8 -5 -1 1.93 0.54 -8 -5 -1 1.31 0.48 -8 5 -1 1.47 0.54 -8 -5 -1 1.43 0.43 -8 5 -1 1.35 0.43 -8 -5 -2 90.01 2.93 -8 5 -2 92.99 2.96 -8 -5 -2 103.26 3.34 -8 5 -2 94.46 3.02 -8 -5 -2 93.22 2.98 -8 5 -2 96.66 3.36 -8 -5 -2 91.30 2.95 -8 -5 -2 90.47 2.74 -8 5 -2 93.14 3.27 -8 -5 -2 96.33 2.89 -8 5 -2 92.98 2.90 -8 -5 -2 95.93 2.95 -8 5 -2 93.73 3.27 -8 5 -2 95.41 2.82 -8 -5 -2 96.52 3.15 -8 5 -2 92.25 2.92 -8 -5 -2 96.42 2.97 -8 -5 -2 93.58 2.99 -8 5 -2 88.84 2.92 -8 5 -2 97.67 3.29 -8 5 -2 95.94 3.30 -8 5 -2 88.90 3.24 -8 -5 -2 94.23 3.23 -8 -5 -3 554.02 11.19 -8 5 -3 556.00 11.87 -8 -5 -3 557.08 11.33 -8 5 -3 570.99 11.29 -8 -5 -3 563.95 11.56 -8 5 -3 543.69 11.26 -8 5 -3 561.25 11.84 -8 -5 -3 571.71 11.81 -8 5 -3 573.58 11.83 -8 -5 -3 575.34 11.47 -8 5 -3 587.62 12.02 -8 -5 -3 545.59 11.34 -8 5 -3 558.44 11.82 -8 -5 -3 579.67 11.73 -8 5 -3 569.54 11.75 -8 -5 -3 574.73 11.86 -8 -5 -4 3.19 0.51 -8 5 -4 3.60 0.56 -8 -5 -4 2.73 0.48 -8 5 -4 2.99 0.61 -8 5 -4 2.46 0.45 -8 5 -4 2.92 0.47 -8 -5 -4 2.57 0.51 -8 -5 -4 2.95 0.54 -8 5 -4 2.96 0.57 -8 5 -4 3.03 0.61 -8 5 -4 2.96 0.57 -8 -5 -4 2.83 0.55 -8 5 -4 3.03 0.58 -8 -5 -4 3.40 0.58 -8 5 -4 2.72 0.60 -8 -5 -4 2.84 0.53 -8 5 -5 40.60 1.89 -8 5 -5 36.45 1.50 -8 5 -5 40.22 1.74 -8 -5 -5 40.49 1.81 -8 -5 -5 37.39 1.68 -8 -5 -5 42.36 1.68 -8 5 -5 39.76 1.68 -8 -5 -5 38.70 1.67 -8 -5 -5 39.90 1.86 -8 -5 -5 40.25 1.71 -8 5 -5 42.06 1.84 -8 -5 -5 39.16 1.80 -8 5 -6 170.12 4.32 -8 -5 -6 169.23 4.31 -8 -5 -6 166.25 4.10 -8 5 -6 173.85 4.12 -8 -5 -6 168.83 4.17 -8 -5 -6 163.21 4.14 -8 5 -6 168.55 4.39 -8 5 -6 161.35 3.81 -8 5 -6 168.86 4.30 -8 5 -6 169.58 4.35 -8 5 -7 14.62 0.94 -8 -5 -7 15.61 0.93 -8 -5 -7 15.22 0.89 -8 5 -7 17.09 0.91 -8 -5 -7 16.12 0.94 -8 5 -7 15.56 1.00 -8 5 -7 16.18 0.98 -8 5 -7 16.33 1.00 -8 -5 -8 0.59 0.26 -8 5 -8 0.67 0.26 -8 5 -8 1.07 0.34 -8 -5 -8 0.55 0.27 -8 -5 -8 0.74 0.25 -8 5 -9 0.18 0.18 -8 -5 -9 0.04 0.15 -8 -5 -9 0.40 0.20 -8 -6 15 20.61 0.85 -8 -6 15 19.38 0.83 -8 6 15 20.73 0.85 8 6 -15 19.99 0.79 8 6 -14 0.18 0.22 -8 -6 14 0.29 0.24 -8 -6 14 0.26 0.20 -8 -6 14 0.50 0.25 -8 6 14 0.41 0.26 8 6 -14 0.43 0.22 8 -6 -14 0.18 0.23 -8 6 14 0.20 0.24 8 -6 -13 37.50 1.47 8 -6 -13 36.60 1.52 8 6 -13 37.93 1.51 -8 -6 13 36.01 1.52 -8 6 13 36.39 1.53 -8 6 13 32.89 1.46 8 -6 -12 24.93 1.28 -8 -6 12 27.86 1.45 -8 6 12 24.63 1.33 8 -6 -12 25.74 1.32 8 6 -12 27.05 1.37 8 -6 -11 32.19 1.59 -8 -6 11 30.75 1.64 -8 6 11 31.26 1.59 -8 -6 11 32.21 1.59 -8 -6 11 31.84 1.60 -8 6 11 33.99 1.67 8 -6 -11 31.87 1.57 8 6 -11 33.06 1.62 -8 -6 10 126.97 3.86 8 -6 -10 121.92 3.70 -8 6 10 125.65 3.70 -8 -6 10 120.11 3.62 -8 -6 10 126.82 3.73 -8 6 10 126.59 3.82 8 6 -10 122.58 3.64 -8 6 9 47.17 2.07 -8 -6 9 49.89 2.09 -8 -6 9 50.59 2.13 -8 6 9 43.58 2.13 8 -6 -9 48.48 2.10 8 6 -9 45.69 2.02 -8 -6 8 24.57 1.56 -8 6 8 24.06 1.44 8 -6 -8 25.22 1.49 8 6 -8 24.55 1.43 -8 -6 8 25.97 1.48 -8 6 8 24.14 1.56 -8 -6 8 24.63 1.44 -8 -6 7 53.08 2.23 -8 6 7 50.61 2.29 -8 -6 7 49.78 2.31 -8 6 7 53.13 2.17 -8 -6 7 50.55 2.13 -8 -6 7 52.22 2.15 -8 6 7 49.11 2.35 8 -6 -7 50.19 2.18 8 6 -7 48.63 2.08 -8 -6 6 11.38 0.95 -8 -6 6 11.99 0.99 8 6 -6 13.40 1.04 8 -6 -6 12.83 1.06 -8 -6 6 12.07 1.05 -8 6 6 14.98 1.22 -8 -6 6 13.61 2.33 -8 -6 6 11.46 2.24 -8 6 6 13.90 2.29 -8 -6 6 13.83 1.16 -8 6 6 12.71 1.00 -8 -6 5 642.38 13.09 -8 -6 5 665.97 13.24 -8 -6 5 670.74 13.51 -8 6 5 688.27 13.84 8 -6 -5 667.30 13.42 8 6 -5 660.34 13.24 -8 -6 5 705.41 20.13 -8 6 5 680.79 18.98 8 6 -5 639.94 13.20 -8 -6 5 677.61 13.66 -8 6 5 669.44 13.20 -8 -6 5 646.84 19.59 -8 -6 4 148.12 3.74 -8 6 4 148.27 4.17 8 6 -4 143.97 3.96 -8 -6 4 144.22 4.23 -8 -6 4 142.93 3.94 -8 -6 4 155.85 4.30 -8 6 4 150.85 4.48 8 -6 -4 148.55 4.14 8 6 -4 145.88 3.98 -8 -6 4 148.04 3.89 -8 6 4 142.93 4.13 -8 -6 4 150.35 8.02 -8 6 4 151.84 7.47 -8 -6 4 143.95 3.76 -8 -6 4 150.47 8.09 -8 -6 3 1.10 0.35 -8 -6 3 0.29 0.64 -8 6 3 0.28 0.45 -8 6 3 0.71 0.64 -8 -6 3 0.51 0.32 -8 6 3 0.60 0.37 -8 -6 3 0.93 0.38 -8 -6 3 1.20 0.38 -8 6 3 0.59 0.39 8 6 -3 1.01 0.35 8 -6 -3 1.09 0.39 -8 -6 3 1.01 0.37 -8 -6 3 0.63 0.78 -8 -6 3 0.31 0.36 -8 6 2 613.16 12.53 -8 -6 2 599.18 11.77 -8 -6 2 571.62 11.93 -8 -6 2 538.80 16.59 -8 -6 2 559.99 17.39 -8 6 2 609.26 12.33 -8 -6 2 596.36 11.76 -8 6 2 604.67 12.63 -8 -6 2 604.08 12.27 -8 6 2 606.18 12.41 8 -6 -2 599.05 11.96 -8 6 2 574.72 12.38 -8 -6 2 598.50 12.23 -8 6 2 589.33 12.20 -8 -6 2 620.22 18.77 -8 -6 2 596.12 12.11 -8 6 1 37.41 1.85 -8 -6 1 37.32 1.64 8 -6 -1 38.91 1.70 -8 6 1 35.74 1.95 -8 -6 1 39.12 1.85 -8 6 1 34.49 1.84 8 -6 -1 36.52 1.62 -8 6 1 37.16 1.92 -8 -6 1 36.85 1.60 -8 -6 1 37.60 1.83 -8 -6 1 34.82 3.47 -8 6 1 38.85 1.96 -8 -6 1 35.81 1.82 -8 6 1 36.31 1.80 -8 6 0 331.65 8.01 -8 -6 0 342.44 7.65 -8 6 0 346.32 7.97 -8 -6 0 340.79 7.35 -8 6 0 328.77 7.90 -8 -6 0 338.22 7.82 -8 -6 0 348.87 7.83 -8 6 0 344.94 7.94 -8 6 0 341.72 7.79 -8 6 0 331.39 7.67 -8 6 -1 81.15 2.83 -8 6 -1 83.44 3.09 -8 -6 -1 80.03 2.74 -8 -6 -1 87.48 3.02 -8 6 -1 85.47 3.10 -8 6 -1 80.86 3.01 -8 -6 -1 83.20 2.93 -8 6 -1 75.41 2.90 -8 -6 -1 82.88 2.87 -8 6 -1 80.64 2.89 -8 6 -1 87.16 2.85 -8 6 -1 84.33 3.03 -8 -6 -1 81.83 2.63 -8 6 -2 9.13 0.87 -8 6 -2 9.62 0.98 -8 -6 -2 8.96 0.76 -8 6 -2 9.93 1.01 -8 -6 -2 8.02 0.87 -8 6 -2 9.20 0.95 -8 6 -2 10.42 0.99 -8 -6 -2 8.63 0.89 -8 -6 -2 9.03 0.85 -8 6 -2 9.48 0.98 -8 -6 -2 10.40 0.86 -8 6 -2 9.39 0.92 -8 -6 -2 8.48 0.87 -8 6 -2 8.76 0.86 -8 -6 -3 3.59 0.52 -8 6 -3 3.05 0.62 -8 -6 -3 2.65 0.56 -8 6 -3 3.67 0.61 -8 6 -3 3.98 0.66 -8 6 -3 3.85 0.57 -8 -6 -3 3.71 0.58 -8 6 -3 3.91 0.60 -8 6 -3 3.59 0.61 -8 6 -3 3.58 0.62 -8 -6 -3 3.48 0.60 -8 6 -3 3.48 0.60 -8 -6 -3 3.78 0.49 -8 6 -3 3.23 0.47 -8 6 -3 3.09 0.60 -8 -6 -3 3.14 0.50 -8 -6 -4 6.10 0.64 -8 6 -4 4.46 0.66 -8 6 -4 4.92 0.67 -8 -6 -4 7.87 0.76 -8 6 -4 4.95 0.67 -8 -6 -4 5.61 0.71 -8 6 -4 4.09 0.63 -8 6 -4 5.38 0.57 -8 -6 -4 4.61 0.52 -8 6 -4 5.67 0.73 -8 -6 -4 4.84 0.58 -8 6 -4 5.69 0.67 -8 6 -5 29.69 1.47 -8 -6 -5 31.27 1.51 -8 6 -5 30.97 1.47 -8 -6 -5 30.37 1.49 -8 -6 -5 33.82 1.43 -8 6 -5 31.77 1.56 -8 6 -5 32.02 1.47 -8 6 -5 33.32 1.53 -8 6 -5 29.80 1.24 -8 -6 -5 30.26 1.30 -8 -6 -5 29.97 1.36 -8 -6 -6 24.96 1.16 -8 -6 -6 24.26 1.13 -8 -6 -6 24.04 1.21 -8 6 -6 24.17 1.19 -8 6 -6 21.76 1.15 -8 6 -6 22.46 0.97 -8 -6 -6 23.13 1.07 -8 -6 -7 8.43 0.67 -8 -6 -7 8.19 0.60 -8 6 -7 6.75 0.60 -8 -6 -7 8.33 0.62 -8 -6 -7 8.14 0.57 -8 6 -7 7.96 0.62 -8 -6 -8 5.64 0.46 -8 6 -8 4.55 0.42 -8 -6 -8 4.36 0.41 -8 -6 -8 5.25 0.43 -8 -6 -8 5.40 0.40 -8 -6 -9 9.23 0.45 -8 6 -9 10.47 0.50 -8 6 -9 10.68 0.52 -8 -6 -9 9.78 0.45 8 7 -14 51.02 1.43 -8 -7 14 49.80 1.45 -8 7 14 50.71 1.44 -8 7 13 43.54 1.53 -8 -7 13 39.68 1.39 8 7 -13 43.09 1.51 -8 -7 13 46.64 1.53 -8 -7 13 41.86 1.49 -8 7 13 43.81 1.54 8 -7 -13 41.54 1.50 8 -7 -13 43.10 1.48 8 -7 -12 45.95 1.66 -8 -7 12 45.24 1.74 -8 7 12 47.65 1.74 -8 -7 12 47.07 1.74 -8 -7 12 43.34 1.64 -8 -7 12 42.32 1.58 -8 7 12 46.66 1.74 8 -7 -12 44.68 1.68 8 7 -12 46.12 1.65 8 -7 -11 9.01 0.78 -8 -7 11 8.30 0.80 -8 7 11 8.66 0.77 -8 -7 11 9.44 0.80 -8 -7 11 9.72 0.80 -8 -7 11 9.70 0.78 -8 7 11 10.54 0.85 8 7 -11 9.28 0.78 8 -7 -11 8.63 0.78 -8 -7 10 57.72 2.25 8 -7 -10 53.21 2.13 -8 7 10 56.12 2.13 -8 -7 10 55.74 2.12 -8 -7 10 61.66 2.15 -8 -7 10 54.00 2.03 -8 7 10 58.31 2.22 8 -7 -10 56.66 2.15 8 -7 -10 58.11 2.21 8 7 -10 57.00 2.14 -8 7 9 16.79 1.14 -8 -7 9 17.72 1.14 -8 -7 9 17.13 1.11 -8 -7 9 17.56 1.12 -8 7 9 16.67 1.18 8 -7 -9 17.02 1.15 8 7 -9 17.05 1.15 8 -7 -9 20.47 1.26 -8 -7 8 115.54 3.57 8 -7 -8 108.08 3.43 -8 7 8 107.49 3.29 -8 -7 8 107.11 3.23 -8 -7 8 106.25 3.18 -8 -7 8 107.15 3.23 -8 7 8 96.62 3.31 8 -7 -8 109.88 3.35 8 7 -8 106.11 3.27 -8 -7 7 125.47 3.83 8 -7 -7 123.77 3.78 -8 7 7 122.25 3.57 8 -7 -7 119.42 3.60 8 7 -7 121.31 3.57 -8 -7 7 118.86 3.47 -8 -7 7 119.22 3.43 -8 -7 7 120.63 3.54 8 -7 -6 526.34 10.93 8 7 -6 535.02 10.85 -8 -7 6 537.60 11.18 8 -7 -6 538.67 11.16 -8 7 6 532.78 10.82 -8 -7 6 523.61 10.86 -8 7 6 504.12 10.55 -8 7 6 516.72 10.49 -8 7 5 12.06 1.01 8 7 -5 13.00 1.00 8 -7 -5 13.19 1.03 -8 -7 5 10.98 0.95 8 7 -5 12.17 0.97 -8 -7 5 11.20 1.01 8 -7 -5 12.32 1.06 -8 7 5 11.51 0.94 -8 7 5 12.72 0.93 -8 -7 4 2.94 0.55 -8 -7 4 2.40 0.44 -8 7 4 2.64 0.50 8 -7 -4 2.68 0.52 -8 7 4 2.81 0.55 8 7 -4 3.24 0.54 -8 7 4 2.30 0.46 8 7 -4 3.07 0.52 8 -7 -4 4.04 0.63 -8 7 4 2.68 0.53 -8 -7 4 2.28 0.51 -8 7 3 20.60 1.12 -8 -7 3 22.35 1.24 -8 7 3 18.98 1.26 -8 -7 3 22.60 1.28 8 -7 -3 20.09 1.20 8 7 -3 20.55 1.20 -8 7 3 20.50 1.32 -8 7 3 19.40 1.20 8 7 -3 19.10 1.14 -8 -7 3 19.18 1.23 8 -7 -3 21.56 1.32 -8 7 3 20.47 1.32 -8 -7 3 19.66 1.23 -8 7 2 23.43 1.54 -8 -7 2 22.13 1.29 -8 7 2 24.73 1.51 8 -7 -2 27.10 1.32 -8 7 2 23.23 1.27 -8 -7 2 23.78 1.34 -8 7 2 23.21 1.41 -8 -7 2 24.77 1.39 -8 7 2 22.35 1.40 8 7 -2 22.78 1.23 8 -7 -2 22.38 1.29 -8 7 2 22.84 1.31 -8 -7 2 22.30 1.11 -8 7 2 25.26 1.47 -8 -7 2 24.49 1.16 -8 7 1 58.97 2.51 -8 7 1 58.33 2.16 -8 -7 1 59.47 2.26 -8 7 1 58.21 2.34 -8 -7 1 54.47 1.90 -8 7 1 54.25 2.29 -8 -7 1 59.10 2.29 -8 7 1 57.04 2.37 -8 7 1 56.76 2.16 -8 7 1 52.18 1.93 -8 -7 1 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121.78 3.16 -10 2 13 116.39 3.12 -10 -2 13 118.60 3.14 -10 2 13 121.88 3.28 10 2 -13 122.39 3.22 10 -2 -13 118.41 3.18 -10 2 13 123.93 3.13 -10 -2 13 124.01 3.14 -10 -2 13 119.73 3.06 10 2 -13 123.08 3.20 -10 -2 12 186.28 4.68 -10 2 12 190.92 4.71 10 2 -12 196.03 4.74 10 2 -12 192.90 4.71 10 -2 -12 193.64 4.70 -10 2 12 197.48 4.74 -10 -2 12 190.00 4.72 -10 2 12 203.79 4.93 -10 -2 12 202.73 4.88 10 2 -12 192.45 4.75 10 -2 -12 197.15 4.76 -10 2 12 205.66 4.74 -10 -2 12 199.79 4.73 -10 -2 12 201.48 4.68 -10 -2 11 37.28 1.69 -10 2 11 36.80 1.68 10 -2 -11 34.90 1.52 10 2 -11 37.32 1.68 10 2 -11 38.28 1.69 10 -2 -11 37.74 1.67 -10 2 11 36.42 1.68 -10 -2 11 37.04 1.68 -10 -2 11 34.51 1.75 -10 -2 11 38.65 1.77 10 2 -11 38.98 1.73 10 -2 -11 39.03 1.72 -10 2 11 40.79 1.71 -10 -2 11 43.34 1.76 -10 -2 11 34.98 1.63 -10 2 10 1.79 0.47 -10 -2 10 0.90 0.39 -10 -2 10 0.48 0.37 10 -2 -10 1.14 0.38 10 2 -10 1.09 0.40 -10 2 10 1.32 0.46 -10 -2 10 1.07 0.42 10 2 -10 1.82 0.48 10 -2 -10 1.55 0.44 -10 2 10 1.76 0.47 -10 -2 10 0.72 0.34 -10 -2 10 1.50 0.44 -10 2 10 1.49 0.44 -10 -2 9 265.90 6.44 -10 2 9 264.78 6.41 10 2 -9 271.65 6.30 10 -2 -9 268.15 6.27 -10 2 9 270.52 6.56 -10 -2 9 257.77 6.34 10 2 -9 267.24 6.34 10 -2 -9 268.20 6.34 -10 2 9 273.07 6.47 -10 -2 9 266.55 6.44 -10 2 9 277.82 6.40 -10 -2 9 275.03 6.40 -10 -2 9 272.96 6.43 -10 -2 9 261.48 6.59 -10 2 8 15.18 1.19 -10 -2 8 15.95 1.21 -10 2 8 14.35 1.12 -10 -2 8 16.31 1.20 -10 -2 8 16.86 1.23 -10 2 8 16.77 1.02 -10 2 8 15.34 1.20 -10 -2 8 15.12 1.12 -10 2 8 15.18 1.18 -10 -2 8 15.44 1.18 10 -2 -8 16.56 1.16 10 2 -8 15.51 1.12 -10 -2 8 15.30 1.17 -10 2 8 14.96 1.16 -10 -2 8 15.94 1.23 -10 2 7 53.45 2.25 -10 -2 7 52.31 2.25 -10 -2 7 52.55 2.27 -10 2 7 53.63 2.03 -10 2 7 51.92 2.28 -10 -2 7 53.56 2.31 -10 2 7 53.21 2.27 -10 -2 7 52.86 2.14 -10 2 7 52.77 2.26 -10 -2 7 52.43 2.27 -10 -2 7 50.89 2.26 -10 2 7 56.51 2.36 -10 -2 7 55.41 2.35 -10 -2 6 63.10 2.52 -10 -2 6 64.67 2.30 -10 2 6 65.10 2.60 -10 -2 6 64.48 2.60 -10 2 6 63.81 2.51 -10 -2 6 62.59 2.58 -10 2 6 63.99 2.60 -10 2 6 64.79 2.55 -10 -2 6 66.11 2.58 -10 -2 6 65.46 2.59 -10 2 6 60.10 2.47 -10 -2 6 68.33 2.60 -10 2 6 62.26 2.30 -10 -2 5 12.49 1.03 -10 2 5 14.21 1.15 -10 -2 5 13.73 1.14 -10 -2 5 14.05 1.04 -10 -2 5 13.47 1.16 -10 2 5 14.49 1.19 -10 2 5 13.30 1.05 -10 2 5 12.32 1.10 -10 -2 5 12.67 1.12 -10 -2 5 11.94 1.09 -10 2 5 11.66 1.05 -10 -2 5 12.98 1.10 -10 2 5 13.25 1.00 -10 2 4 29.80 1.43 -10 -2 4 30.70 1.57 -10 -2 4 31.60 1.77 -10 2 4 30.06 1.73 -10 2 4 29.73 1.49 -10 -2 4 30.42 1.45 -10 2 4 31.81 1.74 -10 -2 4 28.66 1.67 -10 -2 4 32.22 1.66 -10 2 4 30.74 1.56 -10 2 4 32.29 1.78 -10 -2 4 33.53 1.82 -10 2 4 31.50 1.60 -10 -2 4 31.59 1.77 -10 2 4 33.26 1.78 -10 -2 4 32.45 1.76 -10 -2 3 60.63 2.57 -10 2 3 63.61 2.62 -10 2 3 63.54 2.34 -10 -2 3 63.63 2.29 -10 -2 3 60.74 2.35 -10 -2 3 65.12 2.63 -10 2 3 63.85 2.60 -10 2 3 63.82 2.55 -10 -2 3 64.71 2.59 -10 2 3 61.40 2.38 -10 -2 3 65.48 2.63 -10 2 3 59.47 2.50 -10 -2 3 63.71 2.57 -10 -2 3 62.70 2.47 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104.11 2.96 -10 2 0 106.22 3.40 -10 -2 0 105.49 3.41 -10 2 0 102.53 3.24 -10 2 0 107.60 3.43 -10 -2 0 100.19 3.36 -10 2 0 98.76 3.29 -10 -2 0 105.41 3.38 -10 -2 0 106.20 3.43 -10 2 0 102.43 3.40 -10 -2 0 92.19 3.04 -10 -2 0 99.94 2.91 -10 2 -1 4.64 0.66 -10 -2 -1 4.85 0.72 -10 2 -1 4.18 0.67 -10 2 -1 5.03 0.68 -10 -2 -1 5.46 0.69 -10 -2 -1 4.83 0.72 -10 2 -1 5.17 0.72 -10 -2 -1 5.34 0.60 -10 2 -1 4.87 0.70 -10 -2 -1 4.07 0.68 -10 2 -1 3.87 0.66 -10 2 -1 5.79 0.71 -10 -2 -1 4.91 0.73 -10 -2 -1 4.64 0.69 -10 2 -1 4.19 0.63 -10 -2 -1 4.05 0.64 -10 2 -1 4.64 0.56 -10 2 -1 4.60 0.69 -10 -2 -1 5.64 0.61 -10 2 -2 152.09 4.13 -10 -2 -2 155.99 4.33 -10 2 -2 149.73 4.25 -10 2 -2 150.08 4.12 -10 -2 -2 161.73 4.22 -10 -2 -2 156.20 4.31 -10 2 -2 156.16 4.32 -10 -2 -2 152.00 3.90 -10 2 -2 159.68 4.27 -10 -2 -2 157.07 4.26 -10 2 -2 155.06 4.15 -10 2 -2 155.05 4.25 -10 -2 -2 153.56 4.26 -10 2 -2 156.03 4.13 -10 2 -2 150.39 4.24 -10 -2 -2 158.84 3.97 -10 -2 -3 5.81 0.60 -10 2 -3 4.74 0.63 -10 -2 -3 6.60 0.71 -10 2 -3 5.30 0.64 -10 -2 -3 5.50 0.68 -10 2 -3 5.14 0.66 -10 -2 -3 5.57 0.68 -10 -2 -3 6.25 0.71 -10 2 -3 5.76 0.68 -10 2 -3 6.14 0.66 -10 -2 -3 5.89 0.63 -10 -2 -3 6.43 0.70 -10 -2 -3 4.80 0.63 -10 -2 -3 5.46 0.68 -10 2 -3 5.45 0.65 -10 -2 -3 5.98 0.64 -10 -2 -3 6.24 0.63 -10 -2 -4 18.44 1.02 -10 2 -4 18.04 1.09 -10 -2 -4 18.36 1.00 -10 2 -4 19.83 1.10 -10 -2 -4 18.47 1.08 -10 2 -4 18.02 1.06 -10 -2 -4 17.08 1.07 -10 2 -4 18.85 1.10 -10 -2 -4 18.58 1.09 -10 -2 -4 18.36 1.11 -10 2 -4 17.90 1.09 -10 -2 -4 20.04 1.04 -10 2 -4 18.18 1.08 -10 -2 -4 18.53 1.00 -10 -2 -4 18.43 1.02 -10 2 -4 18.90 1.07 -10 -2 -4 18.58 1.07 -10 2 -5 10.74 0.75 -10 -2 -5 11.55 0.77 -10 -2 -5 9.97 0.75 -10 2 -5 10.86 0.75 -10 -2 -5 10.75 0.76 -10 -2 -5 10.38 0.73 -10 2 -5 9.97 0.75 -10 -2 -5 10.63 0.70 -10 2 -5 11.91 0.79 -10 -2 -5 9.81 0.67 -10 2 -5 11.67 0.78 -10 -2 -5 11.69 0.75 -10 2 -5 10.98 0.74 -10 -2 -6 47.20 1.48 -10 2 -6 46.96 1.53 -10 2 -6 44.61 1.46 -10 2 -6 46.38 1.49 -10 -2 -6 44.23 1.37 -10 -2 -6 45.93 1.48 -10 -2 -6 43.57 1.39 -10 2 -6 47.08 1.48 -10 -2 -6 45.23 1.48 -10 2 -7 3.17 0.30 -10 -2 -7 2.59 0.28 -10 2 -7 3.26 0.33 -10 -3 15 107.75 2.44 10 3 -15 107.00 2.42 -10 3 14 4.43 0.38 -10 3 14 5.92 0.50 10 3 -14 5.98 0.51 -10 3 14 4.81 0.40 -10 -3 14 5.56 0.46 10 -3 -14 5.44 0.42 -10 3 13 101.85 2.85 10 3 -13 104.19 2.83 -10 3 13 106.96 2.67 -10 -3 13 103.06 2.75 -10 -3 12 275.83 6.16 -10 3 12 275.91 6.15 10 -3 -12 282.81 6.05 10 3 -12 296.45 6.35 10 3 -12 283.01 6.17 10 -3 -12 278.01 6.13 -10 3 12 283.90 6.18 -10 -3 12 285.98 6.19 -10 -3 12 301.73 6.52 -10 3 12 289.86 6.43 -10 -3 12 292.65 6.37 10 3 -12 282.11 6.20 10 -3 -12 284.37 6.20 -10 3 12 304.67 6.19 -10 -3 12 291.70 6.16 -10 -3 12 297.00 6.29 -10 -3 11 0.86 0.33 -10 3 11 0.85 0.34 10 3 -11 0.82 0.32 10 -3 -11 0.26 0.27 -10 3 11 1.63 0.47 -10 -3 11 1.12 0.40 10 3 -11 1.07 0.35 10 -3 -11 0.62 0.32 -10 3 11 0.62 0.33 -10 -3 11 0.49 0.30 -10 3 11 0.68 0.33 -10 -3 11 0.77 0.36 -10 -3 11 0.74 0.36 10 -3 -11 0.16 0.28 10 3 -11 0.90 0.36 -10 -3 10 56.71 2.18 -10 3 10 58.58 2.20 10 3 -10 60.30 2.26 10 -3 -10 60.07 2.18 -10 3 10 61.80 2.24 -10 -3 10 60.45 2.23 -10 -3 10 61.44 2.28 10 3 -10 60.32 2.21 10 -3 -10 58.95 2.18 -10 3 10 64.92 2.25 -10 -3 10 65.48 2.26 -10 -3 10 61.95 2.29 -10 3 9 56.32 2.13 -10 -3 9 51.81 2.06 -10 -3 9 51.88 2.16 -10 3 9 50.41 2.06 -10 -3 9 51.40 2.09 10 -3 -9 56.60 2.14 -10 3 9 52.68 2.24 -10 -3 9 51.30 2.08 -10 3 9 54.29 2.14 -10 -3 9 51.95 2.11 10 3 -9 53.67 2.09 10 -3 -9 52.02 2.06 -10 -3 9 52.56 2.12 -10 3 9 51.54 2.09 -10 -3 9 54.44 2.28 -10 3 8 6.19 0.74 -10 -3 8 7.90 0.82 -10 3 8 6.46 0.73 -10 -3 8 5.95 0.72 -10 -3 8 7.30 0.82 -10 -3 8 5.65 0.68 -10 3 8 5.19 0.73 -10 3 8 6.16 0.74 -10 -3 8 5.68 0.71 10 -3 -8 6.06 0.71 10 3 -8 6.49 0.72 -10 -3 8 5.78 0.71 -10 3 8 6.60 0.76 -10 -3 8 6.04 0.79 -10 -3 7 25.56 1.52 -10 -3 7 25.31 1.26 -10 3 7 25.84 1.49 -10 -3 7 23.98 1.45 -10 3 7 25.46 1.52 -10 -3 7 26.49 1.52 -10 3 7 25.69 1.49 -10 3 7 27.22 1.50 -10 -3 7 26.32 1.49 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32.93 1.29 -11 -4 2 30.61 1.35 -11 4 2 34.70 1.37 11 -4 -2 33.46 1.32 -11 -4 2 35.41 1.53 -11 -4 2 35.76 1.57 -11 4 2 34.47 1.38 -11 -4 2 32.43 1.50 -11 4 2 34.51 1.56 -11 -4 2 34.75 1.40 -11 -4 1 379.51 7.83 -11 -4 1 382.72 7.83 -11 -4 1 358.10 7.77 -11 4 1 381.27 7.74 11 -4 -1 382.77 7.58 -11 -4 1 400.77 7.82 -11 -4 1 403.00 8.11 -11 -4 1 403.51 8.13 -11 4 1 386.46 7.77 -11 -4 1 400.02 8.13 -11 4 1 407.11 8.18 -11 -4 1 399.25 7.85 -11 4 0 38.70 1.36 -11 -4 0 42.43 1.60 -11 4 0 40.46 1.39 -11 -4 0 38.93 1.44 -11 4 0 42.80 1.61 -11 -4 0 41.02 1.59 -11 4 0 39.66 1.58 -11 -4 0 38.77 1.44 -11 4 0 42.68 1.63 -11 -4 0 41.75 1.48 -11 4 0 41.03 1.55 -11 -4 -1 0.23 0.18 -11 4 -1 0.25 0.20 -11 4 -1 0.02 0.17 -11 -4 -1 0.19 0.22 -11 -4 -1 0.48 0.23 -11 4 -1 0.10 0.22 -11 -4 -1 0.20 0.23 -11 4 -1 0.17 0.26 -11 -4 -1 0.14 0.25 -11 -4 -1 0.26 0.23 -11 4 -1 -0.03 0.23 -11 4 -1 0.03 0.25 -11 4 -1 0.06 0.21 -11 4 -2 61.57 1.68 -11 4 -2 64.17 1.85 -11 -4 -2 64.55 1.80 -11 -4 -2 60.24 1.81 -11 4 -2 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65.19 1.83 -11 5 -1 65.61 1.76 -11 -5 -1 64.44 1.73 -11 5 -1 63.81 1.81 -11 -5 -1 68.48 1.79 -11 5 -2 8.17 0.53 -11 5 -2 9.60 0.55 -11 -5 -2 10.30 0.56 -11 5 -2 8.62 0.50 -11 -5 -2 8.70 0.49 -11 5 -2 9.20 0.55 -11 -5 -2 8.70 0.54 -11 5 -3 0.88 0.17 -11 -5 -3 0.52 0.15 -11 -6 10 12.98 0.60 11 -6 -10 14.50 0.65 11 -6 -10 13.73 0.63 11 -6 -10 13.24 0.59 11 6 -10 15.08 0.65 -11 -6 9 43.57 1.35 11 6 -9 45.79 1.39 11 -6 -9 46.14 1.38 11 -6 -9 43.00 1.28 -11 -6 8 7.82 0.51 11 -6 -8 9.41 0.60 -11 -6 8 8.15 0.56 11 -6 -8 9.60 0.60 11 6 -8 9.45 0.60 11 -6 -8 7.58 0.50 -11 6 8 7.11 0.50 11 -6 -7 111.66 2.65 11 -6 -7 99.84 2.40 -11 -6 7 103.31 2.61 -11 6 7 97.91 2.41 11 -6 -7 108.90 2.64 -11 -6 7 110.64 2.69 -11 6 7 98.73 2.45 -11 6 7 114.62 2.65 11 -6 -6 146.76 3.21 -11 -6 6 142.57 3.33 -11 6 6 139.88 3.12 11 -6 -6 146.24 3.20 -11 -6 6 143.15 3.29 -11 6 6 144.47 3.29 -11 6 6 143.38 3.20 -11 -6 6 132.42 2.99 -11 6 5 38.12 1.34 -11 -6 5 41.26 1.49 11 -6 -5 39.40 1.28 -11 6 5 43.71 1.50 11 -6 -5 40.39 1.34 -11 6 5 41.52 1.43 -11 -6 5 40.94 1.35 11 -6 -4 41.52 1.33 -11 6 4 45.62 1.54 -11 -6 4 45.57 1.51 -11 6 4 45.69 1.47 -11 -6 4 46.16 1.60 -11 6 4 46.04 1.58 -11 6 3 4.86 0.50 -11 6 3 4.54 0.48 -11 -6 3 4.90 0.50 -11 6 3 3.86 0.45 -11 6 3 3.65 0.41 -11 -6 3 3.92 0.47 -11 6 2 216.75 4.60 -11 6 2 214.30 4.57 -11 -6 2 220.06 4.58 -11 6 2 214.56 4.60 -11 6 2 204.50 4.41 -11 6 1 23.86 0.99 -11 6 1 24.91 1.03 -11 -6 1 24.55 1.03 -11 6 1 23.65 1.02 -11 6 1 23.08 0.86 -11 -6 1 24.12 1.01 -11 6 0 17.77 0.82 -11 6 0 16.78 0.70 -11 -6 0 17.46 0.69 -11 -6 0 19.58 0.82 -11 6 0 17.65 0.74 -11 -6 -1 0.13 0.14 -11 6 -1 0.38 0.17 -11 6 -1 0.36 0.14 -11 -6 -1 0.37 0.13 11 7 -8 4.24 0.33 11 -7 -8 4.58 0.35 -11 -7 7 51.35 1.44 -11 7 7 49.46 1.44 -11 -7 6 5.22 0.42 -11 7 6 5.17 0.42 -11 7 5 71.67 1.81 -11 7 5 86.38 2.10 -11 -7 5 71.87 1.80 -11 -7 5 82.62 2.06 11 -7 -5 82.39 1.96 -11 7 4 276.30 5.22 -11 -7 4 264.24 5.02 -11 7 3 30.15 1.03 -11 -7 3 35.14 1.12 -11 -7 2 4.37 0.37 -11 7 2 4.38 0.38 -11 -7 2 4.63 0.37 -11 7 2 4.09 0.34 -11 7 1 41.49 1.20 -11 -7 1 45.53 1.26 -12 0 11 0.35 0.19 -12 0 11 0.16 0.19 -12 0 10 30.19 1.18 -12 0 10 30.59 1.18 -12 0 9 0.46 0.25 -12 0 9 -0.02 0.16 -12 0 9 0.23 0.24 -12 0 8 13.83 0.85 -12 0 8 12.37 0.83 -12 0 8 13.48 0.81 -12 0 8 13.62 0.72 -12 0 8 13.05 0.83 12 0 -8 13.18 0.81 -12 0 8 13.70 0.87 -12 0 7 0.08 0.22 -12 0 7 0.03 0.23 -12 0 7 0.31 0.29 -12 0 7 0.09 0.21 -12 0 7 -0.04 0.27 12 0 -7 -0.14 0.25 -12 0 7 0.04 0.24 -12 0 6 139.76 3.67 -12 0 6 143.61 3.52 -12 0 6 145.06 3.45 -12 0 6 143.93 3.65 -12 0 6 146.55 3.65 -12 0 6 140.99 3.68 12 0 -6 132.03 3.47 -12 0 5 -0.04 0.26 -12 0 5 0.04 0.25 -12 0 5 -0.04 0.30 -12 0 5 0.24 0.26 -12 0 5 -0.04 0.28 -12 0 5 0.22 0.27 -12 0 4 22.65 1.20 -12 0 4 23.32 1.11 -12 0 4 24.56 1.22 -12 0 4 22.33 1.20 -12 0 4 22.46 1.09 -12 0 4 24.05 1.20 -12 0 3 0.33 0.27 -12 0 3 0.23 0.26 -12 0 3 0.29 0.25 -12 0 3 -0.08 0.27 -12 0 3 0.21 0.25 -12 0 2 7.31 0.65 -12 0 2 8.32 0.64 -12 0 2 8.35 0.68 -12 0 2 7.92 0.67 -12 0 2 7.97 0.67 -12 0 1 0.22 0.24 -12 0 1 0.07 0.23 -12 0 1 0.34 0.24 -12 0 1 0.05 0.19 -12 0 1 0.04 0.19 -12 0 1 0.03 0.24 -12 0 0 85.39 2.17 -12 0 0 82.16 2.23 -12 0 0 85.38 2.32 -12 0 0 85.91 2.31 -12 0 -1 0.17 0.19 -12 0 -1 0.16 0.18 -12 0 -1 0.29 0.21 -12 0 -1 0.19 0.18 -12 0 -1 -0.10 0.15 -12 0 -2 13.93 0.63 -12 0 -2 14.76 0.64 -12 0 -2 14.99 0.63 -12 1 11 3.11 0.33 -12 -1 11 3.29 0.35 -12 1 11 3.14 0.33 -12 -1 11 3.21 0.34 -12 -1 10 3.92 0.34 -12 1 10 4.12 0.43 -12 -1 10 5.05 0.46 -12 1 10 4.24 0.43 -12 -1 10 4.91 0.45 -12 1 9 5.45 0.51 -12 -1 9 4.33 0.47 12 -1 -9 4.47 0.42 -12 -1 9 4.29 0.41 -12 1 9 4.94 0.49 -12 -1 9 4.18 0.47 -12 1 9 4.66 0.48 12 -1 -8 -0.03 0.21 -12 1 8 0.31 0.23 -12 -1 8 0.35 0.27 -12 -1 8 0.33 0.24 -12 1 8 -0.11 0.24 -12 1 8 -0.03 0.24 -12 1 8 0.42 0.27 -12 -1 8 0.31 0.25 -12 -1 8 0.12 0.21 12 -1 -8 0.20 0.21 12 1 -8 0.07 0.20 -12 1 8 0.29 0.21 -12 -1 8 -0.04 0.21 -12 1 7 46.38 1.68 -12 -1 7 46.68 1.69 -12 -1 7 47.84 1.75 -12 1 7 46.35 1.73 -12 1 7 47.72 1.70 -12 1 7 42.24 1.36 -12 -1 7 48.06 1.64 -12 1 7 50.63 1.75 -12 -1 7 42.31 1.63 -12 1 7 46.63 1.72 -12 -1 7 48.30 1.75 12 -1 -7 45.06 1.63 12 1 -7 46.05 1.64 -12 1 6 11.50 0.80 -12 -1 6 10.83 0.78 -12 -1 6 11.18 0.81 -12 1 6 11.14 0.81 12 -1 -6 9.68 0.72 12 1 -6 9.64 0.72 -12 -1 6 10.25 0.78 -12 1 6 10.45 0.80 -12 1 6 10.35 0.63 -12 -1 6 9.61 0.72 -12 1 6 10.31 0.77 -12 -1 6 9.35 0.74 -12 1 6 10.26 0.75 -12 1 5 0.35 0.30 -12 -1 5 0.78 0.33 -12 -1 5 0.67 0.29 -12 1 5 0.50 0.27 -12 1 5 0.45 0.27 -12 -1 5 0.56 0.20 -12 1 5 0.72 0.30 -12 1 5 0.79 0.34 -12 -1 5 0.52 0.30 -12 1 5 0.74 0.27 -12 -1 5 1.07 0.34 -12 -1 5 0.76 0.30 -12 1 5 0.67 0.28 -12 -1 4 0.04 0.25 -12 1 4 0.29 0.25 -12 1 4 0.78 0.32 -12 -1 4 0.28 0.31 -12 1 4 0.27 0.23 -12 -1 4 0.37 0.27 -12 -1 4 0.23 0.20 -12 1 4 0.26 0.24 -12 -1 4 0.17 0.23 -12 1 4 0.12 0.23 -12 1 4 0.35 0.30 -12 -1 4 0.35 0.31 -12 1 3 30.89 1.33 -12 -1 3 28.10 1.29 -12 1 3 28.57 1.17 -12 -1 3 30.55 1.31 -12 1 3 30.37 1.33 -12 -1 3 28.98 1.31 -12 -1 3 27.99 1.03 -12 1 3 28.95 1.23 -12 -1 3 29.52 1.34 -12 1 3 28.93 1.33 -12 -1 3 29.64 1.19 -12 1 3 29.93 1.29 -12 -1 3 30.17 1.36 -12 1 3 30.54 1.36 -12 -1 2 44.29 1.69 -12 1 2 45.54 1.70 -12 -1 2 47.31 1.72 -12 1 2 47.14 1.71 -12 1 2 49.29 1.71 -12 -1 2 46.48 1.66 -12 -1 2 45.30 1.43 -12 1 2 46.57 1.62 -12 1 2 47.39 1.56 -12 -1 2 50.44 1.71 -12 1 2 48.37 1.71 -12 -1 2 48.01 1.70 -12 1 1 34.98 1.35 -12 -1 1 33.09 1.32 -12 -1 1 33.12 1.17 -12 1 1 34.14 1.28 -12 1 1 33.13 1.22 -12 -1 1 35.27 1.35 -12 1 1 35.14 1.35 -12 -1 1 33.45 1.33 -12 1 0 0.64 0.24 -12 -1 0 0.48 0.23 -12 1 0 0.96 0.27 -12 1 0 1.00 0.28 -12 -1 0 0.34 0.23 -12 1 0 1.03 0.24 -12 -1 0 1.08 0.27 -12 -1 0 0.53 0.20 -12 -1 -1 14.72 0.69 -12 1 -1 16.05 0.74 -12 -1 -1 15.94 0.75 -12 -1 -1 15.95 0.76 -12 1 -1 15.69 0.74 -12 -1 -1 15.85 0.75 -12 1 -1 16.50 0.74 -12 -1 -1 14.48 0.68 -12 1 -1 14.99 0.73 -12 1 -2 5.13 0.36 -12 -1 -2 3.85 0.32 -12 1 -2 4.36 0.32 -12 -1 -2 5.52 0.36 -12 1 -2 4.89 0.35 -12 -1 -2 5.11 0.36 -12 2 11 39.95 1.22 12 -2 -11 42.42 1.21 -12 2 10 9.12 0.59 -12 -2 10 9.46 0.55 -12 2 10 7.68 0.52 -12 -2 10 8.63 0.55 -12 2 10 9.95 0.57 -12 -2 10 8.87 0.55 12 -2 -10 8.82 0.52 -12 2 9 9.70 0.66 12 -2 -9 8.93 0.58 -12 -2 9 9.74 0.62 -12 2 9 10.17 0.64 -12 -2 9 9.51 0.63 -12 2 9 10.83 0.65 -12 -2 9 9.92 0.64 -12 -2 8 63.02 1.91 -12 2 8 62.97 1.89 -12 -2 8 62.40 1.90 -12 2 8 63.52 1.91 -12 -2 8 61.82 1.89 -12 -2 7 60.83 1.93 -12 2 7 59.43 1.90 -12 -2 7 57.95 1.88 -12 2 7 62.09 1.92 -12 -2 7 63.40 1.94 -12 2 6 -0.17 0.28 -12 -2 6 0.10 0.25 -12 2 6 0.14 0.23 -12 -2 6 0.04 0.24 -12 -2 6 0.04 0.25 -12 -2 6 0.07 0.18 -12 2 6 0.14 0.25 12 -2 -6 0.70 0.27 -12 -2 6 -0.11 0.23 -12 2 6 0.15 0.23 12 -2 -6 0.03 0.22 12 2 -6 -0.03 0.20 -12 -2 6 0.26 0.22 -12 2 6 0.07 0.21 -12 -2 5 30.93 1.09 -12 -2 5 32.04 1.37 -12 2 5 34.60 1.41 -12 -2 5 33.60 1.40 -12 2 5 33.08 1.38 -12 2 5 34.38 1.38 -12 2 5 31.93 1.34 -12 -2 5 34.36 1.38 -12 -2 5 30.89 1.19 -12 -2 5 33.59 1.39 -12 2 5 33.27 1.35 -12 -2 5 36.25 1.41 -12 -2 4 41.54 1.41 -12 2 4 44.82 1.62 -12 2 4 45.60 1.62 -12 -2 4 44.97 1.61 -12 -2 4 42.30 1.61 -12 2 4 43.49 1.62 -12 -2 4 41.51 1.60 -12 2 4 43.33 1.62 -12 2 4 44.34 1.59 -12 -2 4 44.77 1.51 -12 2 4 45.50 1.65 -12 -2 4 43.91 1.64 -12 2 4 44.35 1.60 -12 -2 4 44.72 1.61 -12 -2 3 3.05 0.39 -12 2 3 4.01 0.46 -12 2 3 4.15 0.47 -12 -2 3 4.12 0.48 -12 -2 3 4.20 0.49 -12 2 3 3.64 0.45 -12 2 3 3.66 0.45 -12 2 3 3.55 0.46 -12 -2 3 3.04 0.43 -12 -2 3 3.11 0.31 -12 2 3 3.70 0.35 -12 -2 3 3.87 0.49 -12 2 3 3.58 0.46 -12 -2 3 3.58 0.46 -12 -2 3 3.78 0.43 -12 2 3 4.01 0.48 -12 -2 2 36.33 1.32 -12 2 2 35.05 1.35 -12 -2 2 35.20 1.28 -12 2 2 35.10 1.30 -12 -2 2 32.29 1.10 -12 2 2 33.79 1.30 -12 -2 2 34.70 1.32 -12 -2 2 35.90 1.39 -12 2 2 34.84 1.33 -12 -2 2 35.67 1.34 -12 2 1 95.61 2.46 -12 -2 1 95.20 2.41 -12 -2 1 93.39 2.23 -12 -2 1 93.65 2.48 -12 2 1 93.51 2.41 -12 -2 1 95.74 2.43 -12 2 1 93.27 2.41 -12 -2 1 91.32 2.40 -12 -2 0 42.34 1.28 -12 -2 0 43.45 1.43 -12 2 0 41.41 1.34 -12 -2 0 42.17 1.36 -12 2 0 44.88 1.42 -12 2 0 41.00 1.33 -12 -2 0 43.03 1.36 -12 2 -1 -0.06 0.15 -12 2 -1 0.18 0.14 -12 -2 -1 0.24 0.16 -12 2 -1 0.16 0.17 -12 -2 -1 0.39 0.16 -12 2 -1 0.02 0.14 -12 -2 -1 0.31 0.15 12 -3 -10 5.01 0.40 12 -3 -10 4.60 0.35 -12 -3 10 5.20 0.39 -12 3 10 4.46 0.38 -12 -3 9 13.16 0.70 12 -3 -9 12.86 0.67 -12 3 9 12.57 0.59 -12 3 9 13.38 0.71 -12 -3 8 70.80 1.97 -12 3 8 64.63 1.75 -12 3 8 68.37 1.95 -12 3 7 0.03 0.19 -12 -3 7 0.19 0.22 12 -3 -7 0.19 0.22 -12 3 7 0.28 0.22 -12 -3 7 0.28 0.15 -12 3 7 0.22 0.24 -12 3 6 4.99 0.45 -12 -3 6 4.71 0.41 -12 3 6 4.80 0.51 12 -3 -6 4.56 0.46 -12 3 6 4.68 0.50 -12 -3 6 5.32 0.54 -12 3 6 5.22 0.47 -12 3 5 20.35 0.92 12 -3 -5 19.70 0.93 -12 -3 5 19.03 0.88 -12 3 5 19.69 1.00 -12 3 5 19.29 0.98 -12 -3 5 18.05 0.77 -12 -3 5 21.10 1.04 -12 3 5 19.29 0.91 -12 3 4 19.33 0.88 12 -3 -4 18.07 0.85 -12 -3 4 18.24 0.89 -12 3 4 17.09 0.93 -12 3 4 19.20 0.96 -12 -3 4 17.72 0.80 -12 -3 4 17.39 0.93 -12 3 4 16.76 0.84 12 -3 -3 15.37 0.74 -12 -3 3 16.46 0.84 -12 -3 3 14.39 0.76 -12 3 3 15.22 0.85 -12 3 3 16.00 0.85 -12 3 3 13.68 0.74 -12 3 3 14.91 0.76 -12 3 2 0.46 0.21 12 -3 -2 0.35 0.18 -12 -3 2 0.48 0.23 -12 3 2 0.28 0.20 -12 -3 2 0.16 0.13 -12 -3 2 0.60 0.22 -12 3 2 0.56 0.23 -12 3 2 0.43 0.20 -12 3 1 46.79 1.42 -12 -3 1 55.03 1.63 -12 3 1 59.30 1.64 -12 3 1 50.63 1.44 -12 -3 1 49.69 1.38 -12 3 1 57.05 1.60 -12 -3 1 55.49 1.61 -12 3 1 54.57 1.58 -12 3 0 165.63 3.45 -12 -3 0 161.07 3.47 -12 -3 0 145.81 3.24 -12 3 0 152.25 3.34 -12 3 -1 0.68 0.17 -12 -3 -1 0.31 0.14 -12 3 -1 0.35 0.15 -12 3 -1 0.65 0.16 -12 4 9 76.84 1.95 12 -4 -9 80.14 1.96 -12 4 9 79.98 1.92 12 -4 -8 70.28 1.81 -12 4 8 69.13 1.85 12 -4 -8 65.06 1.76 -12 4 8 61.03 1.72 -12 -4 8 73.44 1.89 -12 4 8 68.35 1.80 -12 4 7 -0.03 0.19 -12 4 7 -0.02 0.17 -12 4 7 -0.07 0.22 12 -4 -7 -0.14 0.19 -12 4 6 5.45 0.48 12 -4 -6 4.50 0.38 -12 -4 6 5.55 0.41 -12 4 6 6.00 0.50 12 -4 -6 5.14 0.43 -12 4 6 6.07 0.50 -12 4 5 25.52 1.07 12 -4 -5 27.91 1.00 -12 -4 5 27.85 1.02 -12 4 5 27.95 1.10 -12 -4 5 21.97 0.79 -12 4 5 28.62 1.10 -12 -4 4 1.31 0.24 -12 4 4 2.04 0.32 -12 -4 4 2.01 0.30 -12 4 4 1.43 0.23 -12 4 4 1.68 0.31 12 -4 -4 1.96 0.27 -12 -4 4 2.43 0.35 -12 -4 3 6.64 0.46 -12 -4 3 6.22 0.51 -12 -4 3 6.48 0.50 -12 4 3 7.74 0.55 -12 4 3 6.70 0.44 12 -4 -3 5.28 0.37 -12 4 2 75.01 2.00 -12 -4 2 77.80 2.01 -12 -4 2 81.19 1.98 -12 -4 2 79.57 2.03 -12 4 2 74.52 2.02 -12 4 2 71.40 1.85 -12 -4 1 17.61 0.73 -12 4 1 17.32 0.73 -12 4 1 15.71 0.67 -12 -4 1 17.27 0.75 -12 4 1 15.43 0.65 -12 4 1 16.86 0.73 -12 -4 1 14.72 0.68 -12 -4 0 7.07 0.41 -12 4 0 6.90 0.42 12 -5 -7 23.05 0.80 -12 5 7 24.99 0.85 -12 -5 7 25.08 0.87 -12 -5 6 53.06 1.43 -12 5 6 46.28 1.40 -12 5 6 51.92 1.38 12 -5 -6 47.03 1.29 -12 5 6 48.41 1.32 -12 5 6 54.25 1.45 -12 5 5 0.67 0.19 -12 5 5 0.71 0.19 -12 -5 5 0.65 0.19 -12 -5 5 0.49 0.16 -12 5 5 0.34 0.15 -12 5 5 0.71 0.20 -12 5 4 12.34 0.60 -12 5 4 15.03 0.67 -12 -5 4 14.03 0.63 -12 5 4 13.67 0.66 -12 5 4 13.48 0.61 -12 -5 4 13.30 0.63 -12 5 3 92.94 2.15 -12 5 3 87.74 2.13 -12 5 3 87.85 2.06 -12 -5 3 89.87 2.13 -12 -5 2 14.29 0.62 -12 5 2 15.06 0.63 -13 0 6 17.73 0.72 -13 0 6 21.96 0.77 -13 0 5 0.04 0.12 13 0 -5 0.11 0.11 -13 0 5 0.24 0.14 -13 0 4 0.15 0.14 -13 0 4 0.23 0.13 0 0 0 0.00 0.00 TITL 22ERO_r2_g in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 1.54184 10.279581 11.186971 15.099831 90.0000 105.6759 90.0000 ZERR 7.00 0.000052 0.000058 0.000080 0.0000 0.0005 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O UNIT 77.00 70.00 7.00 7.00 REM CrysAlisPro recorded range (K): Min=100.0; max=100.0; aver:100.0 TEMP -173 SIZE 0.13 0.15 0.21 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 72027 _shelx_res_file ; TITL T480 in P2(1)/c CELL 1.54184 10.27958 11.18770 15.09983 90.0000 105.6759 90.0000 ZERR 4.00 0.00005 0.00006 0.00008 0.0000 0.0005 0.0000 LATT 1 SYMM -X, 0.5+Y, 0.5-Z SFAC C H N O UNIT 68 60 12 28 TEMP -173.0 SIZE 0.13 0.15 0.21 L.S. 12 BOND $H ACTA CONF EQIV $1 +X,0.5-Y,0.5+Z EQIV $2 2-X,1-Y,2-Z HTAB N1 O4_$1 HTAB N1 N2_$2 WGHT 0.042600 0.660000 FVAR 0.61387 O1 4 0.772510 0.283107 0.737827 11.00000 0.02275 0.01681 = 0.01932 0.00036 0.00775 -0.00203 O2 4 0.602221 1.023723 0.726264 11.00000 0.02982 0.01532 = 0.02751 -0.00201 0.00824 0.00101 O3 4 0.419121 0.922309 0.667874 11.00000 0.01805 0.02326 = 0.03729 0.00583 0.00922 0.00470 O4 4 0.725603 0.393165 0.458604 11.00000 0.02952 0.02123 = 0.01805 -0.00424 0.00253 0.00005 O5 4 0.852818 0.551168 0.518614 11.00000 0.01969 0.02246 = 0.01473 0.00168 0.00529 -0.00200 O6 4 0.477076 0.314753 0.614568 11.00000 0.02146 0.02212 = 0.03144 -0.00626 0.00702 0.00100 O7 4 0.457679 0.137992 0.540796 11.00000 0.02178 0.01994 = 0.02203 -0.00348 0.00324 -0.00328 N1 3 0.866407 0.298136 0.888565 11.00000 0.02279 0.02132 = 0.02014 0.00540 0.00616 -0.00016 H1A 2 0.815107 0.235042 0.890768 11.00000 0.02790 H1B 2 0.900889 0.340121 0.939759 11.00000 0.03348 N2 3 1.035455 0.589759 0.922549 11.00000 0.02917 0.03173 = 0.01888 0.00288 0.00158 -0.00871 N3 3 0.542513 0.930947 0.695450 11.00000 0.02135 0.01674 = 0.01879 0.00330 0.00742 0.00236 C2 1 0.847140 0.353250 0.807154 11.00000 0.01413 0.01913 = 0.01847 0.00120 0.00562 0.00364 C3 1 0.897692 0.460043 0.789662 11.00000 0.01409 0.01759 = 0.01595 0.00138 0.00361 0.00253 C4 1 0.866935 0.513444 0.693947 11.00000 0.01362 0.01544 = 0.01513 0.00015 0.00456 -0.00010 AFIX 13 H4 2 0.954015 0.538498 0.681974 11.00000 -1.20000 AFIX 0 C5 1 0.801380 0.420056 0.623450 11.00000 0.01454 0.01581 = 0.01699 -0.00159 0.00522 0.00230 C6 1 0.754926 0.316210 0.647263 11.00000 0.01667 0.01715 = 0.01849 -0.00092 0.00719 0.00258 C7 1 0.973479 0.529937 0.863934 11.00000 0.01727 0.02251 = 0.01694 0.00555 0.00444 0.00051 C8 1 0.777986 0.623765 0.688532 11.00000 0.01549 0.01565 = 0.01053 0.00078 0.00362 0.00019 C9 1 0.638197 0.613741 0.672952 11.00000 0.01608 0.01545 = 0.01887 0.00018 0.00408 -0.00204 AFIX 43 H9 2 0.596322 0.537530 0.661186 11.00000 -1.20000 AFIX 0 C10 1 0.560151 0.714435 0.674560 11.00000 0.01412 0.01892 = 0.01910 0.00174 0.00374 -0.00041 AFIX 43 H10 2 0.465027 0.708156 0.664074 11.00000 -1.20000 AFIX 0 C11 1 0.623972 0.824279 0.691787 11.00000 0.01832 0.01509 = 0.01331 0.00163 0.00473 0.00262 C12 1 0.762250 0.837568 0.706646 11.00000 0.01936 0.01509 = 0.01712 -0.00118 0.00467 -0.00344 AFIX 43 H12 2 0.803531 0.914070 0.717891 11.00000 -1.20000 AFIX 0 C13 1 0.838523 0.736008 0.704621 11.00000 0.01415 0.01884 = 0.01751 -0.00055 0.00408 -0.00217 AFIX 43 H13 2 0.933452 0.742999 0.714340 11.00000 -1.20000 AFIX 0 C14 1 0.786350 0.450243 0.525356 11.00000 0.01544 0.01628 = 0.01794 -0.00095 0.00550 0.00398 C15 1 0.845116 0.589141 0.425516 11.00000 0.02156 0.02943 = 0.01585 0.00579 0.00684 0.00370 AFIX 137 H15A 2 0.877775 0.524782 0.393051 11.00000 -1.50000 H15B 2 0.901224 0.660403 0.427354 11.00000 -1.50000 H15C 2 0.751143 0.607901 0.393227 11.00000 -1.50000 AFIX 0 C16 1 0.674546 0.220331 0.587680 11.00000 0.02177 0.01587 = 0.02398 -0.00377 0.00982 -0.00212 AFIX 23 H16A 2 0.708050 0.140908 0.612645 11.00000 -1.20000 H16B 2 0.685888 0.226744 0.524799 11.00000 -1.20000 AFIX 0 C17 1 0.526260 0.232165 0.583915 11.00000 0.02180 0.01662 = 0.01561 0.00074 0.00420 -0.00104 C18 1 0.314743 0.137715 0.535170 11.00000 0.01974 0.02608 = 0.02738 -0.00015 -0.00059 -0.00270 AFIX 137 H18A 2 0.270847 0.205387 0.497592 11.00000 -1.50000 H18B 2 0.302531 0.144707 0.597121 11.00000 -1.50000 H18C 2 0.274158 0.062866 0.506992 11.00000 -1.50000 AFIX 0 HKLF 4 REM T480 in P2(1)/c REM R1 = 0.0314 for 3505 Fo > 4sig(Fo) and 0.0316 for all 3550 data REM 254 parameters refined using 0 restraints END WGHT 0.0426 0.6599 REM Highest difference peak 0.252, deepest hole -0.263, 1-sigma level 0.048 Q1 1 0.8194 0.5669 0.6939 11.00000 0.05 0.25 Q2 1 0.7190 0.2686 0.6133 11.00000 0.05 0.21 Q3 1 0.8370 0.4628 0.6606 11.00000 0.05 0.21 Q4 1 0.6045 0.2220 0.5875 11.00000 0.05 0.21 Q5 1 0.7834 0.4358 0.5762 11.00000 0.05 0.20 Q6 1 0.7460 0.3795 0.6322 11.00000 0.05 0.20 Q7 1 0.8038 0.6782 0.6909 11.00000 0.05 0.19 Q8 1 0.8967 0.3947 0.7957 11.00000 0.05 0.19 Q9 1 0.7149 0.6157 0.6895 11.00000 0.05 0.19 Q10 1 0.8825 0.4812 0.7452 11.00000 0.05 0.18 Q11 1 0.6912 0.8268 0.7107 11.00000 0.05 0.18 Q12 1 0.7933 0.7812 0.7183 11.00000 0.05 0.17 Q13 1 0.5958 0.7666 0.6908 11.00000 0.05 0.17 Q14 1 0.6034 0.6645 0.6755 11.00000 0.05 0.17 Q15 1 0.8094 0.3575 0.6336 11.00000 0.05 0.16 Q16 1 0.8464 0.4252 0.8030 11.00000 0.05 0.16 Q17 1 0.5861 0.8711 0.6904 11.00000 0.05 0.15 Q18 1 0.3515 0.1804 0.6194 11.00000 0.05 0.13 Q19 1 0.3725 1.0051 0.7021 11.00000 0.05 0.13 Q20 1 0.9450 0.4843 0.8210 11.00000 0.05 0.12 ; _shelx_res_checksum 18570 _shelxl_version_number .2013 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O O1 0.77251(7) 0.28311(6) 0.73783(5) 0.01923(16) Uani d 1 . . O O2 0.60222(8) 1.02372(7) 0.72626(6) 0.02412(17) Uani d 1 . . O O3 0.41912(8) 0.92231(7) 0.66787(6) 0.02586(18) Uani d 1 . . O O4 0.72560(8) 0.39316(7) 0.45860(5) 0.02369(17) Uani d 1 . . O O5 0.85282(7) 0.55117(7) 0.51861(5) 0.01883(16) Uani d 1 . . O O6 0.47708(8) 0.31475(7) 0.61457(6) 0.02503(18) Uani d 1 . . O O7 0.45768(8) 0.13799(7) 0.54080(5) 0.02177(17) Uani d 1 . . N N1 0.86641(9) 0.29814(9) 0.88857(7) 0.02135(19) Uani d 1 . . H H1A 0.8151(15) 0.2350(14) 0.8908(10) 0.028(4) Uiso d 1 . . H H1B 0.9009(16) 0.3401(14) 0.9398(11) 0.033(4) Uiso d 1 . . N N2 1.03545(10) 0.58976(9) 0.92255(7) 0.0275(2) Uani d 1 . . N N3 0.54251(9) 0.93095(8) 0.69545(6) 0.01857(18) Uani d 1 . . C C2 0.84714(10) 0.35325(9) 0.80715(7) 0.0170(2) Uani d 1 . . C C3 0.89769(10) 0.46004(9) 0.78966(7) 0.0160(2) Uani d 1 . . C C4 0.86693(9) 0.51344(9) 0.69395(6) 0.01460(19) Uani d 1 . . H H4 0.9540 0.5385 0.6820 0.018 Uiso calc 1 . . C C5 0.80138(9) 0.42006(9) 0.62345(7) 0.0156(2) Uani d 1 . . C C6 0.75493(10) 0.31621(9) 0.64726(7) 0.0170(2) Uani d 1 . . C C7 0.97348(10) 0.52994(10) 0.86393(7) 0.0189(2) Uani d 1 . . C C8 0.77799(9) 0.62376(9) 0.68853(6) 0.01387(19) Uani d 1 . . C C9 0.63820(10) 0.61374(9) 0.67295(7) 0.0169(2) Uani d 1 . . H H9 0.5963 0.5375 0.6612 0.020 Uiso calc 1 . . C C10 0.56015(10) 0.71444(9) 0.67456(7) 0.0175(2) Uani d 1 . . H H10 0.4650 0.7082 0.6641 0.021 Uiso calc 1 . . C C11 0.62397(10) 0.82428(9) 0.69179(6) 0.01549(19) Uani d 1 . . C C12 0.76225(10) 0.83757(9) 0.70665(7) 0.0172(2) Uani d 1 . . H H12 0.8035 0.9141 0.7179 0.021 Uiso calc 1 . . C C13 0.83852(10) 0.73601(9) 0.70462(7) 0.0169(2) Uani d 1 . . H H13 0.9335 0.7430 0.7143 0.020 Uiso calc 1 . . C C14 0.78635(10) 0.45024(9) 0.52536(7) 0.0164(2) Uani d 1 . . C C15 0.84512(11) 0.58914(11) 0.42552(7) 0.0219(2) Uani d 1 . . H H15A 0.8778 0.5248 0.3931 0.033 Uiso calc 1 . . H H15B 0.9012 0.6604 0.4274 0.033 Uiso calc 1 . . H H15C 0.7511 0.6079 0.3932 0.033 Uiso calc 1 . . C C16 0.67455(11) 0.22033(9) 0.58768(7) 0.0198(2) Uani d 1 . . H H16A 0.7080 0.1409 0.6126 0.024 Uiso calc 1 . . H H16B 0.6859 0.2267 0.5248 0.024 Uiso calc 1 . . C C17 0.52626(10) 0.23216(9) 0.58392(7) 0.0182(2) Uani d 1 . . C C18 0.31474(11) 0.13772(11) 0.53517(8) 0.0258(2) Uani d 1 . . H H18A 0.2708 0.2054 0.4976 0.039 Uiso calc 1 . . H H18B 0.3025 0.1447 0.5971 0.039 Uiso calc 1 . . H H18C 0.2742 0.0629 0.5070 0.039 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.0228(4) 0.0168(3) 0.0193(4) -0.0020(3) 0.0077(3) 0.0004(3) O2 0.0298(4) 0.0153(4) 0.0275(4) 0.0010(3) 0.0082(3) -0.0020(3) O3 0.0180(4) 0.0233(4) 0.0373(5) 0.0047(3) 0.0092(3) 0.0058(3) O4 0.0295(4) 0.0212(4) 0.0180(4) 0.0001(3) 0.0025(3) -0.0042(3) O5 0.0197(4) 0.0225(4) 0.0147(3) -0.0020(3) 0.0053(3) 0.0017(3) O6 0.0215(4) 0.0221(4) 0.0314(4) 0.0010(3) 0.0070(3) -0.0063(3) O7 0.0218(4) 0.0199(4) 0.0220(4) -0.0033(3) 0.0032(3) -0.0035(3) N1 0.0228(4) 0.0213(5) 0.0201(5) -0.0002(4) 0.0062(4) 0.0054(4) N2 0.0292(5) 0.0317(5) 0.0189(4) -0.0087(4) 0.0016(4) 0.0029(4) N3 0.0213(4) 0.0167(4) 0.0188(4) 0.0024(3) 0.0074(3) 0.0033(3) C2 0.0141(4) 0.0191(5) 0.0185(5) 0.0036(4) 0.0056(4) 0.0012(4) C3 0.0141(4) 0.0176(5) 0.0160(5) 0.0025(4) 0.0036(4) 0.0014(4) C4 0.0136(4) 0.0154(5) 0.0151(4) -0.0001(3) 0.0046(3) 0.0002(3) C5 0.0145(4) 0.0158(5) 0.0170(5) 0.0023(3) 0.0052(4) -0.0016(4) C6 0.0167(4) 0.0172(5) 0.0185(5) 0.0026(4) 0.0072(4) -0.0009(4) C7 0.0173(5) 0.0225(5) 0.0169(5) 0.0005(4) 0.0044(4) 0.0056(4) C8 0.0155(4) 0.0157(5) 0.0105(4) 0.0002(3) 0.0036(3) 0.0008(3) C9 0.0161(5) 0.0155(5) 0.0189(5) -0.0020(4) 0.0041(4) 0.0002(4) C10 0.0141(4) 0.0189(5) 0.0191(5) -0.0004(4) 0.0037(4) 0.0017(4) C11 0.0183(5) 0.0151(5) 0.0133(4) 0.0026(4) 0.0047(3) 0.0016(3) C12 0.0194(5) 0.0151(5) 0.0171(5) -0.0034(4) 0.0047(4) -0.0012(4) C13 0.0141(4) 0.0188(5) 0.0175(5) -0.0022(4) 0.0041(4) -0.0006(4) C14 0.0154(4) 0.0163(5) 0.0179(5) 0.0040(4) 0.0055(4) -0.0009(4) C15 0.0216(5) 0.0294(6) 0.0159(5) 0.0037(4) 0.0068(4) 0.0058(4) C16 0.0218(5) 0.0159(5) 0.0240(5) -0.0021(4) 0.0098(4) -0.0038(4) C17 0.0218(5) 0.0166(5) 0.0156(5) -0.0010(4) 0.0042(4) 0.0007(4) C18 0.0197(5) 0.0261(6) 0.0274(6) -0.0027(4) -0.0006(4) -0.0002(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 2 2 -1 0.0805 -2 -2 1 0.0505 2 -2 -1 0.0978 -2 2 1 0.0477 0 0 -1 0.0590 1 0 2 0.1294 -3 2 9 0.1131 3 6 -6 0.0779 5 -4 -6 0.0722 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C2 O1 C6 . . 120.07(8) ? C14 O5 C15 . . 115.20(8) ? C17 O7 C18 . . 115.07(8) ? C2 N1 H1A . . 117.3(10) ? C2 N1 H1B . . 118.5(10) ? H1A N1 H1B . . 119.2(14) ? O3 N3 O2 . . 123.95(9) ? O3 N3 C11 . . 118.11(9) ? O2 N3 C11 . . 117.94(8) ? N1 C2 C3 . . 127.86(10) ? N1 C2 O1 . . 110.58(9) ? C3 C2 O1 . . 121.46(9) ? C2 C3 C7 . . 119.33(9) ? C2 C3 C4 . . 122.70(9) ? C7 C3 C4 . . 117.77(9) ? C5 C4 C3 . . 109.69(8) ? C5 C4 C8 . . 111.99(8) ? C3 C4 C8 . . 109.73(8) ? C5 C4 H4 . . 108.5 ? C3 C4 H4 . . 108.5 ? C8 C4 H4 . . 108.5 ? C6 C5 C14 . . 121.02(9) ? C6 C5 C4 . . 122.16(9) ? C14 C5 C4 . . 116.79(9) ? C5 C6 O1 . . 122.47(9) ? C5 C6 C16 . . 129.65(9) ? O1 C6 C16 . . 107.84(8) ? N2 C7 C3 . . 177.84(11) ? C13 C8 C9 . . 119.51(9) ? C13 C8 C4 . . 119.14(8) ? C9 C8 C4 . . 121.25(9) ? C10 C9 C8 . . 120.37(9) ? C10 C9 H9 . . 119.8 ? C8 C9 H9 . . 119.8 ? C11 C10 C9 . . 118.51(9) ? C11 C10 H10 . . 120.7 ? C9 C10 H10 . . 120.7 ? C10 C11 C12 . . 122.61(9) ? C10 C11 N3 . . 118.87(9) ? C12 C11 N3 . . 118.52(9) ? C13 C12 C11 . . 118.05(9) ? C13 C12 H12 . . 121.0 ? C11 C12 H12 . . 121.0 ? C12 C13 C8 . . 120.94(9) ? C12 C13 H13 . . 119.5 ? C8 C13 H13 . . 119.5 ? O4 C14 O5 . . 122.65(9) ? O4 C14 C5 . . 126.85(10) ? O5 C14 C5 . . 110.49(8) ? O5 C15 H15A . . 109.5 ? O5 C15 H15B . . 109.5 ? H15A C15 H15B . . 109.5 ? O5 C15 H15C . . 109.5 ? H15A C15 H15C . . 109.5 ? H15B C15 H15C . . 109.5 ? C6 C16 C17 . . 110.25(8) ? C6 C16 H16A . . 109.6 ? C17 C16 H16A . . 109.6 ? C6 C16 H16B . . 109.6 ? C17 C16 H16B . . 109.6 ? H16A C16 H16B . . 108.1 ? O6 C17 O7 . . 124.87(10) ? O6 C17 C16 . . 125.10(9) ? O7 C17 C16 . . 110.03(8) ? O7 C18 H18A . . 109.5 ? O7 C18 H18B . . 109.5 ? H18A C18 H18B . . 109.5 ? O7 C18 H18C . . 109.5 ? H18A C18 H18C . . 109.5 ? H18B C18 H18C . . 109.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag O1 C2 . 1.3661(13) ? O1 C6 . 1.3807(12) ? O2 N3 . 1.2313(12) ? O3 N3 . 1.2273(12) ? O4 C14 . 1.2139(13) ? O5 C14 . 1.3378(13) ? O5 C15 . 1.4501(12) ? O6 C17 . 1.2042(13) ? O7 C17 . 1.3353(12) ? O7 C18 . 1.4487(13) ? N1 C2 . 1.3413(14) ? N1 H1A . 0.887(16) ? N1 H1B . 0.892(17) ? N2 C7 . 1.1543(15) ? N3 C11 . 1.4674(13) ? C2 C3 . 1.3570(14) ? C3 C7 . 1.4156(14) ? C3 C4 . 1.5162(13) ? C4 C5 . 1.5137(13) ? C4 C8 . 1.5250(13) ? C4 H4 . 1.0000 ? C5 C6 . 1.3416(14) ? C5 C14 . 1.4860(14) ? C6 C16 . 1.4970(14) ? C8 C13 . 1.3934(14) ? C8 C9 . 1.3965(13) ? C9 C10 . 1.3870(14) ? C9 H9 . 0.9500 ? C10 C11 . 1.3842(14) ? C10 H10 . 0.9500 ? C11 C12 . 1.3858(14) ? C12 C13 . 1.3855(14) ? C12 H12 . 0.9500 ? C13 H13 . 0.9500 ? C15 H15A . 0.9800 ? C15 H15B . 0.9800 ? C15 H15C . 0.9800 ? C16 C17 . 1.5157(14) ? C16 H16A . 0.9900 ? C16 H16B . 0.9900 ? C18 H18A . 0.9800 ? C18 H18B . 0.9800 ? C18 H18C . 0.9800 ? loop_ _geom_contact_atom_site_label_1 _geom_contact_atom_site_label_2 _geom_contact_distance _geom_contact_site_symmetry_1 _geom_contact_site_symmetry_2 _geom_contact_publ_flag C17 O2 3.1242(13) . 1_545 yes C18 O3 3.1325(15) . 1_545 yes O4 C16 2.8924(13) . . yes N1 O4 2.9361(13) . 4_566 yes O5 C8 2.9834(12) . . yes O2 H12 2.44 . . yes H16A O2 2.62 . 1_545 yes O3 H10 2.4456 . . yes H10 O4 2.57 . 3_666 yes O4 H16B 2.20 . . yes H1A O4 2.112(16) . 4_566 yes O4 H15A 2.54 . . yes O4 H15C 2.64 . . yes O5 H4 2.41 . . yes H15C O6 2.47 . 3_666 yes O6 H18A 2.66 . . yes O6 H18B 2.58 . . yes N2 N1 3.0282(14) . 3_767 yes H1B N2 2.152(16) . 3_767 yes C7 C13 3.3501(15) . . yes C5 H9 2.67 . . yes C7 H1B 2.616(16) . . yes C14 H16B 2.70 . . yes H4 H13 2.36 . . yes loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA N1 H1A O4 4_566 0.887(16) 2.112(16) 2.9362(12) 154.1(13) N1 H1B N2 3_767 0.892(17) 2.152(17) 3.0283(14) 167.2(14) loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C6 O1 C2 N1 . . . . -172.01(8) ? C6 O1 C2 C3 . . . . 4.55(14) ? N1 C2 C3 C7 . . . . -4.60(16) ? O1 C2 C3 C7 . . . . 179.47(9) ? N1 C2 C3 C4 . . . . -179.38(9) ? O1 C2 C3 C4 . . . . 4.70(14) ? C2 C3 C4 C5 . . . . -12.33(13) ? C7 C3 C4 C5 . . . . 172.82(8) ? C2 C3 C4 C8 . . . . 111.09(10) ? C7 C3 C4 C8 . . . . -63.76(11) ? C3 C4 C5 C6 . . . . 12.41(13) ? C8 C4 C5 C6 . . . . -109.67(10) ? C3 C4 C5 C14 . . . . -169.57(8) ? C8 C4 C5 C14 . . . . 68.34(10) ? C14 C5 C6 O1 . . . . 177.07(8) ? C4 C5 C6 O1 . . . . -5.00(15) ? C14 C5 C6 C16 . . . . -5.52(16) ? C4 C5 C6 C16 . . . . 172.42(9) ? C2 O1 C6 C5 . . . . -4.43(14) ? C2 O1 C6 C16 . . . . 177.66(8) ? C5 C4 C8 C13 . . . . -144.02(9) ? C3 C4 C8 C13 . . . . 93.92(10) ? C5 C4 C8 C9 . . . . 39.64(12) ? C3 C4 C8 C9 . . . . -82.42(11) ? C13 C8 C9 C10 . . . . -0.79(15) ? C4 C8 C9 C10 . . . . 175.54(9) ? C8 C9 C10 C11 . . . . 0.07(15) ? C9 C10 C11 C12 . . . . 0.57(15) ? C9 C10 C11 N3 . . . . -178.79(9) ? O3 N3 C11 C10 . . . . -12.19(14) ? O2 N3 C11 C10 . . . . 167.63(9) ? O3 N3 C11 C12 . . . . 168.42(9) ? O2 N3 C11 C12 . . . . -11.75(13) ? C10 C11 C12 C13 . . . . -0.46(15) ? N3 C11 C12 C13 . . . . 178.90(9) ? C11 C12 C13 C8 . . . . -0.29(15) ? C9 C8 C13 C12 . . . . 0.91(15) ? C4 C8 C13 C12 . . . . -175.50(9) ? C15 O5 C14 O4 . . . . 1.14(13) ? C15 O5 C14 C5 . . . . 179.93(8) ? C6 C5 C14 O4 . . . . 5.60(16) ? C4 C5 C14 O4 . . . . -172.44(9) ? C6 C5 C14 O5 . . . . -173.13(9) ? C4 C5 C14 O5 . . . . 8.83(12) ? C5 C6 C16 C17 . . . . -99.61(12) ? O1 C6 C16 C17 . . . . 78.09(10) ? C18 O7 C17 O6 . . . . -2.19(15) ? C18 O7 C17 C16 . . . . 178.38(8) ? C6 C16 C17 O6 . . . . 8.59(15) ? C6 C16 C17 O7 . . . . -171.99(8) ?