#------------------------------------------------------------------------------ #$Date: 2025-02-09 19:01:10 +0100 (Sun, 09 Feb 2025) $ #$Revision: 297647 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/33/2023390.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023390 loop_ _publ_author_name 'Nuss, J\"urgen' 'M\"uhle, Claus' 'Hayama, Kyouhei' 'Abdolazimi, Vahideh' 'Takagi, Hidenori' _publ_section_title ; Tilting structures ininverseperovskites,M3TtO (M= Ca, Sr, Ba, Eu;Tt= Si, Ge, Sn, Pb) ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B Structural Science, Crystal Engineering and Materials' _journal_page_first 300 _journal_page_last 312 _journal_paper_doi 10.1107/S2052520615006150 _journal_volume 71 _journal_year 2015 _chemical_formula_moiety 'Ba3 Pb O' _chemical_formula_sum 'Ba3 O Pb' _chemical_formula_weight 635.21 _space_group_crystal_system cubic _space_group_IT_number 221 _space_group_name_Hall '-P 4 2 3' _space_group_name_H-M_alt 'P m -3 m' _symmetry_cell_setting cubic _symmetry_space_group_name_H-M 'P m -3 m' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2013 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 1 _cell_length_a 5.489(7) _cell_length_b 5.489(7) _cell_length_c 5.489(7) _cell_measurement_reflns_used 1270 _cell_measurement_temperature 295(2) _cell_measurement_theta_max 36.40 _cell_measurement_theta_min 3.71 _cell_volume 165.4(4) _computing_cell_refinement 'Bruker Suite (Bruker AXS, 2013)' _computing_data_collection 'Bruker Suite (Bruker AXS, 2013)' _computing_data_reduction 'Bruker Suite (Bruker AXS, 2013)' _computing_structure_refinement 'SHELXL (Sheldrick, 2008)' _computing_structure_solution 'SHELXL (Sheldrick, 2008)' _diffrn_ambient_temperature 295(2) _diffrn_measured_fraction_theta_full 0.980 _diffrn_measured_fraction_theta_max 1.00 _diffrn_measurement_device_type 'SMART APEX II, Bruker AXS' _diffrn_measurement_method \wscan _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0425 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_l_max 9 _diffrn_reflns_limit_l_min -9 _diffrn_reflns_number 3016 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 36.895 _diffrn_reflns_theta_min 3.712 _exptl_absorpt_coefficient_mu 42.854 _exptl_absorpt_correction_T_max 0.275 _exptl_absorpt_correction_T_min 0.134 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; Sheldrick, G. M. (2012) SADABS - Bruker AXS area detector scaling and absorption, version 2012/1, University of G\"ottingen. Germany. ; _exptl_crystal_colour 'dark grey metallic' _exptl_crystal_density_diffrn 6.377 _exptl_crystal_description block _exptl_crystal_F_000 258 _exptl_crystal_size_max 0.050 _exptl_crystal_size_mid 0.030 _exptl_crystal_size_min 0.020 _refine_diff_density_max 0.954 _refine_diff_density_min -0.735 _refine_ls_extinction_coef 0.102(4) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method SHELXL _refine_ls_goodness_of_fit_ref 1.224 _refine_ls_matrix_type full _refine_ls_number_parameters 6 _refine_ls_number_reflns 117 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.224 _refine_ls_R_factor_all 0.0137 _refine_ls_R_factor_gt 0.0124 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details ; w=1/[\s^2^(Fo^2^)+(0.0151P)^2^+0.0671P] where P=(Fo^2^+2Fc^2^)/3 ; _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0328 _refine_ls_wR_factor_ref 0.0332 _reflns_number_gt 116 _reflns_number_total 117 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file dk5032sup1.cif _cod_data_source_block Ba3PbO_295K _cod_original_cell_volume 165.4(7) _cod_database_code 2023390 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.223 _shelx_estimated_absorpt_t_max 0.481 _shelx_hkl_file ; -1 0 0 214.739 9.854 1 -1 0 0 237.798 11.079 2 0 -1 0 228.793 10.341 2 0 -1 0 230.685 12.898 3 0 0 -1 231.193 11.530 2 0 0 1 213.700 10.331 1 0 0 1 218.841 11.999 3 0 1 0 206.946 11.769 1 1 0 0 214.363 11.843 3 -1 -1 0 586.644 23.655 2 -1 -1 0 507.873 26.356 3 -1 0 -1 503.032 23.827 2 -1 0 1 499.983 23.181 1 -1 0 1 500.846 24.921 2 -1 0 1 505.736 24.989 3 -1 1 0 471.057 25.329 1 -1 1 0 530.647 23.617 2 0 -1 -1 522.076 24.837 2 0 -1 -1 520.626 25.299 3 0 -1 1 509.111 23.428 1 0 -1 1 486.923 28.359 3 0 1 -1 516.596 22.738 2 0 1 1 543.298 24.644 1 1 -1 0 485.953 26.507 3 1 0 1 527.952 22.457 1 1 0 1 508.166 26.352 3 1 1 0 546.803 23.694 1 -1 -1 -1 8315.69 359.00 2 -1 -1 -1 8784.28 403.73 3 -1 -1 1 9646.06 367.61 1 -1 -1 1 7715.07 358.76 2 -1 -1 1 8200.88 399.52 3 -1 1 -1 8331.46 362.70 1 -1 1 -1 8545.91 360.03 2 -1 1 1 9020.43 363.48 1 1 -1 -1 8303.23 360.51 2 1 -1 1 8751.29 400.64 3 1 1 1 8443.61 362.85 1 -2 0 0 9999.99 396.61 1 -2 0 0 8134.89 390.45 2 0 -2 0 9726.57 390.28 2 0 -2 0 9969.49 436.61 3 0 0 -2 8807.98 391.59 2 0 0 2 9567.70 399.35 1 0 0 2 8794.35 435.28 3 0 2 0 9047.06 397.52 1 2 0 0 9699.19 434.79 3 -2 0 -1 173.464 10.528 2 -2 0 1 162.526 9.030 1 -2 0 1 183.898 11.768 2 -1 -2 0 182.577 9.465 2 -1 -2 0 175.932 12.386 3 -1 2 0 165.346 12.548 1 -1 2 0 176.239 9.755 2 0 -1 -2 184.678 12.291 2 0 -1 2 163.161 9.343 1 0 -1 2 154.439 13.838 3 0 1 -2 173.957 10.043 2 0 1 2 162.963 10.018 1 1 -2 0 161.593 12.892 3 1 2 0 167.524 11.069 1 2 0 -1 169.857 10.369 3 2 0 1 168.539 11.693 3 -2 -1 0 182.350 10.699 2 -2 -1 0 201.305 12.117 3 -2 1 0 180.392 10.725 1 -2 1 0 170.081 10.417 2 -1 0 -2 169.862 10.892 2 -1 0 2 171.149 9.626 1 0 -2 -1 188.197 11.554 2 0 -2 -1 168.878 11.271 3 0 -2 1 162.564 14.321 3 0 2 -1 170.064 10.667 1 0 2 1 179.117 12.725 1 1 0 -2 202.544 12.610 2 1 0 2 169.853 8.842 1 1 0 2 161.477 11.670 3 2 -1 0 163.982 11.181 3 2 1 0 179.308 8.977 1 -2 -1 -1 441.043 23.407 2 -2 -1 1 449.572 21.641 1 -2 -1 1 472.314 24.055 2 -2 -1 1 474.122 25.115 3 -2 1 -1 471.715 23.497 1 -2 1 -1 472.336 22.691 2 -2 1 1 482.077 23.177 1 -2 1 1 494.788 24.980 2 -1 -2 -1 481.455 23.698 2 -1 -2 -1 482.231 25.544 3 -1 -2 1 500.029 22.095 2 -1 -2 1 467.924 26.760 3 -1 -1 -2 478.769 24.846 2 -1 -1 2 449.659 22.245 1 -1 -1 2 483.132 25.844 3 -1 1 -2 471.045 22.469 2 -1 1 2 457.372 23.128 1 -1 2 -1 455.231 24.154 1 -1 2 -1 481.821 21.138 2 -1 2 1 454.427 25.843 1 1 -2 -1 445.910 24.309 2 1 -2 -1 487.268 25.790 3 1 -2 1 450.386 28.176 3 1 -1 -2 482.367 25.734 2 1 -1 2 454.021 21.848 1 1 -1 2 449.659 27.410 3 1 1 -2 473.459 23.897 2 1 1 2 467.858 21.992 1 1 1 2 467.723 25.223 3 1 2 -1 461.572 23.154 1 1 2 1 419.757 24.803 1 2 -1 -1 461.996 23.997 3 2 -1 1 467.016 26.290 3 2 1 1 468.734 21.256 1 2 1 1 472.522 26.162 3 -2 -2 0 8631.96 359.33 2 -2 -2 0 8631.38 401.09 3 -2 0 -2 8101.04 360.02 2 -2 0 2 9101.33 363.02 1 -2 0 2 7575.58 362.30 2 -2 0 2 9183.86 398.49 3 -2 2 0 8220.77 366.82 1 -2 2 0 8441.15 359.28 2 0 -2 -2 8460.06 362.27 2 0 -2 -2 9373.40 399.19 3 0 -2 2 9392.32 363.37 1 0 -2 2 7749.56 404.60 3 0 2 -2 8499.69 357.38 2 0 2 2 8168.70 364.97 1 2 -2 0 8408.63 401.12 3 2 0 2 8459.16 363.00 1 2 0 2 8860.66 401.39 3 2 2 0 8262.96 363.69 1 -2 -2 -1 164.133 10.930 2 -2 -2 -1 166.162 12.285 3 -2 -2 1 144.823 9.187 1 -2 -2 1 178.520 10.989 2 -2 -2 1 154.180 12.314 3 -2 -1 -2 157.194 11.386 2 -2 -1 2 135.217 8.972 1 -2 -1 2 165.342 12.436 2 -2 -1 2 147.595 10.765 3 -2 1 -2 165.508 9.300 1 -2 1 -2 153.230 9.838 2 -2 1 2 134.254 9.726 1 -2 2 -1 165.157 12.060 1 -2 2 -1 159.341 9.416 2 -2 2 1 156.583 12.202 1 -2 2 1 166.433 11.483 2 -1 -2 -2 159.428 12.091 2 -1 -2 -2 136.977 11.019 3 -1 -2 2 142.610 9.350 1 -1 -2 2 154.851 13.210 3 -1 2 -2 145.627 10.048 1 -1 2 -2 155.327 8.561 2 -1 2 2 143.007 10.998 1 1 -2 -2 165.269 12.780 2 1 -2 2 166.226 15.341 3 1 2 -2 166.714 9.701 2 1 2 2 156.568 10.530 1 2 -2 -1 165.776 11.405 3 2 -2 1 155.745 13.235 3 2 -1 -2 148.778 12.936 2 2 -1 2 146.812 12.751 3 2 1 2 159.714 7.995 1 2 1 2 158.584 12.080 3 2 2 1 136.502 10.864 1 -2 -2 -2 7473.56 323.69 2 -2 -2 2 7896.11 324.09 1 -2 -2 2 6567.80 321.69 2 -2 -2 2 7503.98 358.67 3 -2 2 -2 7993.45 325.86 1 -2 2 -2 7778.52 319.84 2 -2 2 2 7956.88 327.27 1 2 -2 -2 7704.97 325.19 2 2 -2 2 7737.73 361.10 3 2 2 2 7191.43 323.73 1 2 2 2 7792.98 358.96 3 -3 0 0 281.042 13.347 1 -3 0 0 308.743 17.187 2 0 -3 0 301.574 14.832 2 0 -3 0 265.099 19.402 3 0 0 -3 282.991 17.438 2 0 0 3 301.916 15.296 1 0 0 3 277.360 19.098 3 0 3 0 284.159 19.054 1 3 0 0 282.021 17.573 3 -3 0 -1 298.404 16.832 2 -3 0 1 267.759 14.206 1 -3 0 1 314.531 18.068 2 -1 -3 0 292.269 14.716 2 -1 -3 0 283.441 19.521 3 -1 3 0 288.596 19.668 1 0 -1 -3 269.185 18.208 2 0 -1 3 279.447 15.190 1 0 -1 3 267.904 21.424 3 0 1 -3 316.226 16.954 2 0 1 3 275.907 15.640 1 1 -3 0 296.253 15.772 2 1 -3 0 312.277 20.875 3 1 3 0 284.109 18.319 1 3 0 -1 273.666 16.772 3 3 0 1 274.536 18.315 3 0 3 1 301.836 20.029 1 1 0 -3 294.218 18.793 2 1 0 3 284.160 14.674 1 3 -1 0 270.934 17.461 3 3 1 0 279.978 18.412 3 0 3 -1 298.037 17.944 1 -1 0 3 273.346 15.473 1 0 -3 -1 290.989 17.029 2 0 -3 -1 277.115 18.609 3 0 -3 1 265.819 21.111 3 -3 1 0 280.538 14.956 1 -3 1 0 290.551 16.927 2 -3 -1 0 303.743 13.806 1 -3 -1 0 284.877 17.009 2 -1 3 -1 7719.18 315.97 1 -1 3 -1 7409.07 306.15 2 1 -1 3 6817.33 346.88 3 1 1 -3 7375.88 310.56 2 1 -1 -3 7567.73 313.46 2 1 -1 3 7711.49 310.92 1 3 1 1 7637.98 345.11 3 1 -3 -1 7699.11 310.67 2 1 -3 -1 7471.17 344.64 3 1 -3 1 7451.04 348.55 3 3 -1 1 7629.17 344.72 3 1 1 3 7517.06 311.10 1 1 1 3 7035.02 343.42 3 1 3 -1 7341.91 313.67 1 1 3 1 7042.26 316.49 1 3 -1 -1 7675.84 342.50 3 -3 -1 -1 6783.45 309.58 2 -3 -1 1 7468.66 310.33 1 -3 -1 1 6402.36 310.07 2 -3 -1 1 7408.39 343.89 3 -3 1 -1 6886.49 311.55 1 -3 1 -1 7325.12 309.23 2 -3 1 1 7682.17 311.58 1 -3 1 1 6873.55 310.65 2 -1 -3 -1 7347.27 309.52 2 -1 -3 -1 7435.44 344.57 3 -1 -3 1 7609.82 306.73 2 -1 -3 1 7357.17 346.49 3 -1 -1 -3 6690.57 311.26 2 -1 -1 3 7918.95 311.91 1 -1 -1 3 6967.29 344.05 3 -1 1 -3 6665.17 308.17 2 -1 1 3 7338.51 312.46 1 -1 3 1 6944.23 317.17 1 3 0 2 239.931 17.292 3 3 0 -2 232.268 13.958 3 0 -2 -3 256.407 17.362 2 0 -2 3 223.318 13.406 1 0 -2 3 193.775 20.193 3 0 2 -3 229.773 13.078 2 0 2 3 223.154 14.760 1 2 -3 0 229.631 17.756 3 2 3 0 227.458 15.407 1 -3 0 -2 224.002 14.768 2 -3 0 2 220.343 12.981 1 -3 0 2 234.154 17.312 2 -2 -3 0 267.183 14.298 2 -2 -3 0 228.289 17.058 3 -2 3 0 235.257 17.662 1 -2 3 0 235.325 13.662 2 0 3 2 225.414 17.091 1 2 0 -3 211.152 16.959 2 2 0 3 241.946 12.059 1 2 0 3 259.596 17.705 3 3 -2 0 237.172 16.580 3 3 2 0 244.073 13.487 1 0 -3 -2 212.986 15.931 2 0 -3 -2 226.898 14.839 3 0 -3 2 205.978 20.048 3 0 3 -2 226.237 14.708 1 -3 2 0 221.803 15.910 1 -3 2 0 221.464 14.234 2 -2 0 -3 228.754 15.271 2 -2 0 3 221.392 13.580 1 -3 -2 0 237.714 15.140 2 -3 -2 0 256.913 17.345 3 1 3 2 270.499 18.798 1 2 -1 -3 265.484 20.004 2 -3 -2 1 296.271 18.209 2 -1 2 3 265.424 17.504 1 -2 -1 3 274.340 17.400 3 1 -2 3 269.678 15.443 1 1 -2 3 280.604 23.605 3 1 2 -3 291.890 16.537 2 -3 -1 -2 272.184 17.753 2 3 2 1 263.967 16.065 1 -3 1 2 317.303 20.330 2 -2 1 -3 283.405 16.619 2 2 -3 1 297.576 21.753 3 2 3 -1 280.821 17.011 1 -2 -1 3 268.491 15.659 1 3 -1 2 305.955 20.601 3 -1 3 -2 292.464 17.822 1 -2 3 1 264.444 20.082 1 -1 -2 -3 307.380 20.056 2 -3 2 -1 310.892 18.958 1 1 -3 -2 300.244 19.670 2 1 -3 -2 299.710 17.664 3 2 1 3 279.804 14.270 1 -3 1 2 283.903 16.139 1 -3 2 -1 281.766 16.359 2 -2 -3 -1 287.689 17.269 2 -2 -3 -1 277.366 19.430 3 2 1 3 280.790 19.427 3 -3 -2 1 268.440 18.982 3 -1 -3 2 271.300 21.421 3 -3 -2 1 277.950 15.112 1 -1 3 -2 303.426 13.545 2 3 -2 -1 289.175 18.043 3 1 2 3 267.272 16.319 1 -2 3 -1 276.578 14.943 2 -1 2 -3 281.757 15.141 2 2 3 1 300.678 19.600 1 -2 -3 1 285.490 16.100 2 2 -3 -1 277.846 17.855 2 -3 -2 -1 309.593 18.088 2 -3 2 1 284.916 18.108 2 -2 -1 -3 273.093 18.553 2 -3 -1 2 297.339 15.436 1 -3 -1 2 302.338 20.125 2 2 -3 -1 288.672 19.412 3 -2 1 3 283.197 16.703 1 -1 -3 -2 306.358 19.323 2 -1 -3 -2 279.359 18.348 3 1 -2 -3 305.825 20.628 2 3 1 2 291.028 19.931 3 -3 2 1 279.557 17.738 1 -1 3 2 266.014 19.593 1 -2 -3 1 268.986 20.291 3 -2 3 -1 270.554 19.192 1 1 -3 2 263.451 23.156 3 1 3 -2 260.418 16.796 1 1 3 -2 281.224 13.442 2 -1 -2 3 296.365 15.988 1 -1 -2 3 297.063 20.990 3 2 -1 3 285.161 14.882 1 2 -1 3 298.417 21.347 3 2 1 -3 305.812 19.418 2 -3 -1 2 288.646 17.556 3 -3 1 -2 272.141 15.927 1 -3 1 -2 262.075 16.409 2 3 -2 1 277.512 19.865 3 1 2 3 300.613 18.432 3 -3 -2 -2 196.722 14.830 2 -3 -2 2 191.312 11.841 1 -3 -2 2 197.624 15.462 2 -3 -2 2 197.225 15.009 3 -3 2 -2 211.492 14.545 1 -3 2 -2 197.903 12.537 2 -3 2 2 175.699 13.948 1 -3 2 2 206.542 15.589 2 -2 -3 -2 187.963 15.062 2 -2 -3 -2 184.523 15.364 3 -2 -3 2 212.654 12.611 2 -2 -3 2 198.621 17.088 3 -2 -2 -3 207.791 16.025 2 -2 -2 3 178.195 12.055 1 -2 -2 3 204.527 15.861 3 -2 2 -3 190.924 12.537 1 -2 2 -3 196.662 11.970 2 -2 2 3 187.357 13.782 1 -2 3 -2 215.335 15.083 1 -2 3 -2 201.430 11.139 2 -2 3 2 206.286 16.162 1 2 -3 -2 184.984 15.000 2 2 -3 -2 189.117 13.552 3 2 -3 2 193.880 18.701 3 2 -2 -3 168.270 15.505 2 2 -2 3 206.139 18.802 3 2 2 -3 189.355 13.978 2 2 2 3 199.483 11.655 1 2 2 3 201.247 15.529 3 2 3 -2 185.875 13.144 1 2 3 2 204.509 14.411 1 3 -2 2 194.322 17.156 3 3 2 2 185.386 10.431 1 3 2 2 193.800 16.397 3 -3 -3 0 200.088 13.566 2 -3 -3 0 179.929 15.774 3 -3 0 -3 178.825 13.600 2 -3 0 3 177.094 11.896 1 -3 3 0 189.314 15.865 1 -3 3 0 187.821 12.831 2 0 -3 -3 200.658 16.099 2 0 -3 -3 134.403 11.966 3 0 -3 3 142.126 19.780 3 0 3 -3 182.386 13.113 1 0 3 -3 189.050 9.555 2 0 3 3 169.102 13.779 1 3 -3 0 168.313 15.482 3 3 0 -3 187.711 17.252 2 3 0 3 196.680 9.761 1 3 0 3 173.042 15.979 3 3 3 0 216.296 13.871 1 -3 -3 -1 5427.47 235.69 2 -3 -3 -1 4822.51 262.36 3 -3 -3 1 5388.93 235.42 2 -3 -3 1 5527.03 262.49 3 -3 -1 -3 5375.84 237.18 2 -3 -1 3 5528.61 235.78 1 -3 -1 3 5490.41 258.45 3 -3 1 -3 5730.14 235.21 1 -3 1 -3 5423.42 234.32 2 -3 1 3 5759.90 237.14 1 -3 3 -1 5577.50 241.15 1 -3 3 -1 5726.43 233.42 2 -3 3 1 5178.39 241.04 1 -3 3 1 5649.55 235.88 2 -1 -3 3 5345.91 236.06 1 -1 -3 3 5545.32 265.52 3 -1 3 -3 5571.36 237.64 1 -1 3 -3 5856.35 230.79 2 -1 3 3 5599.76 240.44 1 1 -3 -3 5277.59 238.92 2 1 -3 3 5515.07 269.18 3 1 3 -3 5284.94 230.96 2 1 3 3 5583.27 238.11 1 3 -3 -1 5563.09 261.06 3 3 -3 1 5592.61 263.94 3 3 -1 -3 5429.72 241.03 2 3 -1 3 5622.01 263.95 3 3 1 -3 5171.49 240.15 2 3 1 3 5740.09 232.72 1 3 1 3 5613.81 262.82 3 3 3 -1 5430.28 236.68 1 3 3 1 4893.94 238.35 1 -3 -3 -2 159.055 14.507 2 -3 -3 2 188.001 14.433 2 -3 -3 2 184.438 16.658 3 -3 -2 -3 173.268 15.794 2 -3 -2 3 184.801 12.141 1 -3 -2 3 186.641 14.900 3 -3 2 -3 214.276 13.781 1 -3 2 -3 200.765 12.839 2 -3 2 3 166.807 13.590 1 -3 3 -2 182.144 15.277 1 -3 3 -2 169.939 11.713 2 -3 3 2 196.818 16.074 1 -2 -3 -3 188.466 16.453 2 -2 -3 3 151.841 11.871 1 -2 -3 3 181.857 17.465 3 -2 3 -3 168.887 13.466 1 -2 3 -3 194.453 11.101 2 -2 3 3 191.185 15.823 1 2 -3 -3 166.185 15.508 2 2 -3 3 196.223 20.783 3 2 3 -3 202.092 12.895 2 2 3 3 179.178 12.735 1 2 3 3 173.639 15.787 3 3 -3 -2 164.997 15.012 2 3 -3 2 199.040 18.537 3 3 -2 -3 212.514 17.724 2 3 -2 3 191.456 18.811 3 3 2 -3 204.195 16.879 2 3 2 3 186.795 10.305 1 3 2 3 173.206 16.377 3 3 3 -2 201.462 13.466 1 3 3 2 185.161 12.801 1 -3 -3 -3 3994.76 182.46 2 -3 -3 3 4093.73 178.21 1 -3 -3 3 3948.81 198.41 3 -3 3 -3 4415.08 181.88 1 -3 3 -3 4199.26 175.18 2 3 -3 -3 3818.05 181.38 2 3 -3 3 3981.46 202.69 3 3 3 -3 4203.12 179.11 2 3 3 3 4049.11 199.46 3 -4 0 0 6477.81 273.17 1 -4 0 0 6067.79 275.54 2 0 -4 0 6964.73 271.69 2 0 -4 0 6222.66 307.40 3 0 0 -4 5906.85 275.97 2 0 0 4 6756.93 276.18 1 0 4 0 6311.14 282.30 1 4 0 0 6751.65 304.89 3 -4 0 -1 109.336 10.204 2 -4 0 1 109.466 7.224 1 -4 0 1 99.7289 10.7543 2 -1 -4 0 123.126 7.970 2 -1 -4 0 121.832 14.099 3 -1 4 0 130.824 14.222 1 0 -1 -4 103.594 11.511 2 0 -1 4 106.353 8.365 1 0 -1 4 103.450 15.831 3 0 1 -4 101.740 9.954 2 0 1 4 96.0626 8.4243 1 1 -4 0 115.093 9.005 2 1 -4 0 124.185 14.427 3 1 4 0 112.690 12.767 1 4 0 -1 105.531 9.943 3 4 0 1 104.720 11.296 3 1 0 4 115.785 8.157 1 1 0 4 148.281 15.159 3 4 -1 0 105.890 10.501 3 4 1 0 102.993 11.570 3 0 -4 -1 117.534 10.314 2 0 -4 -1 119.699 12.668 3 0 -4 1 131.541 15.592 3 0 4 -1 113.971 12.197 1 0 4 1 109.867 13.328 1 1 0 -4 127.924 11.942 2 -1 0 -4 129.397 11.332 2 -1 0 4 121.475 9.117 1 -4 1 0 111.500 10.236 2 -4 -1 0 107.191 10.282 2 -4 1 0 116.500 7.349 1 1 1 -4 413.842 24.232 2 1 4 1 395.888 26.482 1 4 -1 -1 409.432 23.657 3 -4 1 1 398.300 20.623 1 -4 1 1 396.173 24.368 2 -1 -4 -1 406.062 22.877 2 -1 -4 -1 407.784 26.397 3 -1 -4 1 371.548 27.821 3 -1 -1 -4 395.064 25.286 2 -1 -1 4 376.685 21.452 1 -1 -1 4 440.273 25.959 3 -1 1 -4 406.039 22.802 2 -1 1 4 384.350 22.115 1 -4 -1 -1 403.960 23.927 2 -4 -1 1 391.034 19.636 1 -4 -1 1 419.401 25.051 2 -4 1 -1 412.640 23.354 2 1 1 4 416.187 21.164 1 1 1 4 419.384 26.037 3 1 4 -1 417.701 24.823 1 1 -1 4 427.454 21.138 1 1 -1 4 372.444 29.470 3 -1 4 -1 361.859 25.451 1 -1 4 1 408.412 27.048 1 1 -4 -1 441.558 23.918 2 1 -4 -1 393.485 25.840 3 1 -4 1 398.083 28.938 3 1 -1 -4 393.676 25.962 2 4 -1 1 374.926 25.230 3 4 1 -1 410.150 24.858 3 4 1 1 377.718 25.544 3 4 2 0 5745.01 246.36 1 4 0 -2 5866.48 271.15 3 4 0 2 6033.06 275.62 3 -4 2 0 5412.04 246.22 2 -2 0 -4 5779.33 247.94 2 -2 0 4 5850.51 248.10 1 0 -4 -2 5983.43 249.49 2 0 -4 -2 5879.30 273.54 3 0 -4 2 5691.07 279.43 3 0 4 -2 5713.39 250.64 1 0 4 2 5883.01 254.54 1 2 0 -4 5578.46 250.43 2 2 0 4 5867.44 245.75 1 4 -2 0 5941.71 273.83 3 -2 -4 0 5762.79 244.28 2 -2 -4 0 5733.31 275.81 3 -2 4 0 5789.84 254.05 1 0 -2 -4 5805.36 250.85 2 0 -2 4 5742.67 247.38 1 0 -2 4 4975.22 279.68 3 0 2 -4 5664.79 244.70 2 0 2 4 5672.66 248.71 1 2 -4 0 6019.01 245.09 2 2 -4 0 6026.00 276.47 3 2 4 0 5949.74 252.38 1 -4 -2 0 5498.50 247.62 2 -4 2 0 5922.78 248.86 1 -4 0 2 5326.09 249.93 2 -4 0 2 5800.79 246.36 1 -4 0 -2 5394.27 246.50 2 -4 2 -1 61.6320 8.5082 1 -4 -2 1 78.8895 10.9738 3 -4 -1 -2 89.8606 10.3647 2 1 4 2 94.5201 12.4234 1 2 -1 -4 87.6730 12.4490 2 -1 2 4 75.0363 9.0952 1 -4 1 2 91.3337 7.9658 1 -4 1 2 93.4596 11.6539 2 -2 -4 -1 95.0808 9.7509 2 -2 -4 -1 108.504 12.561 3 -4 -2 1 111.375 11.632 2 2 1 4 108.512 12.725 3 4 -2 -1 102.089 10.857 3 -2 -1 4 87.9142 8.0699 1 -2 4 1 99.3636 13.3216 1 -1 -2 -4 122.753 13.376 2 1 -4 -2 117.153 11.463 3 2 1 4 93.5406 7.0521 1 -1 -4 2 77.7038 13.6746 3 -2 1 -4 101.816 9.414 2 -1 4 -2 103.314 11.294 1 1 -2 4 89.7691 7.9019 1 1 -2 4 96.8157 17.5534 3 1 2 -4 97.1059 9.4488 2 4 2 1 105.106 13.237 3 2 4 -1 113.576 10.512 1 1 -4 -2 109.034 11.575 2 -4 2 -1 103.972 9.373 2 2 -4 1 104.215 14.976 3 4 -1 2 125.643 13.792 3 -2 -1 4 89.8594 9.2647 3 2 4 1 86.8316 12.1729 1 1 2 4 117.888 11.843 3 -4 1 -2 89.1939 9.4129 2 -2 1 4 75.5083 8.6143 1 -1 -2 4 119.098 14.617 3 -1 -4 -2 86.4332 10.8566 3 -1 2 -4 89.6479 7.9274 2 1 2 4 99.9425 8.5290 1 -1 4 2 78.2146 12.2644 1 2 -4 -1 100.045 9.518 2 -1 -2 4 84.3399 7.8434 1 1 -4 2 101.503 15.757 3 1 4 -2 106.362 9.990 1 -4 -1 2 92.6388 7.3147 1 -4 -1 2 95.8318 12.3457 2 -1 -4 -2 109.930 11.680 2 2 -1 4 128.332 15.913 3 2 1 -4 99.2263 11.3477 2 4 -1 -2 95.2205 8.5334 3 -2 4 -1 100.677 13.222 1 2 -4 -1 122.160 12.976 3 -4 2 1 61.1121 8.2829 1 -4 2 1 93.4020 10.5305 2 -2 -1 -4 101.534 11.730 2 -2 4 -1 89.9700 7.0885 2 2 -1 4 85.2808 7.1557 1 4 1 2 114.168 13.160 3 -4 -2 -1 108.723 10.831 2 4 -2 1 98.4206 12.5237 3 1 -2 -4 92.7170 12.4509 2 -2 -4 1 98.0913 7.4090 2 -2 -4 1 112.773 14.310 3 -2 -2 4 4874.02 234.42 3 2 4 -2 4774.71 213.44 1 2 4 2 4584.06 215.77 1 4 2 2 4954.45 236.41 3 2 2 -4 5032.23 212.09 2 -2 -2 4 4808.88 211.24 1 -2 2 -4 4851.06 211.52 1 2 -2 -4 4520.33 215.91 2 2 -2 4 4755.58 240.31 3 -4 -2 -2 4407.60 212.01 2 -4 -2 2 4954.63 210.45 1 -4 -2 2 4379.11 213.91 2 -4 -2 2 5028.24 234.24 3 -4 2 -2 4778.94 213.06 1 -4 2 -2 5048.79 210.11 2 -4 2 2 5067.25 213.30 1 -4 2 2 4819.93 214.07 2 -2 -4 -2 4857.32 213.42 2 -2 -4 -2 4716.48 235.26 3 -2 -4 2 4962.85 238.22 3 -2 -2 -4 4715.92 214.56 2 -2 2 -4 4990.90 208.76 2 -2 2 4 4870.88 213.85 1 -2 4 -2 5175.05 217.14 1 -2 4 2 4879.41 218.54 1 2 -4 -2 5019.88 212.82 2 2 -4 -2 5357.53 233.15 3 4 -2 2 4956.60 236.62 3 2 -4 2 4875.21 239.93 3 2 2 4 5064.98 235.00 3 4 -2 -2 5089.56 231.40 3 2 2 4 4800.02 210.17 1 0 3 4 169.898 13.201 1 4 -3 0 143.403 14.384 3 4 0 -3 140.716 10.416 3 4 0 3 150.366 15.769 3 4 3 0 152.991 11.842 1 3 0 4 131.943 8.532 1 3 0 4 181.440 18.598 3 -4 -3 0 131.486 12.763 2 -4 -3 0 101.847 14.628 3 -4 3 0 142.164 13.782 1 3 -4 0 160.566 17.389 3 3 4 0 153.170 13.721 1 -4 0 -3 125.807 12.609 2 -4 0 3 137.946 10.414 1 -4 0 3 189.168 18.319 2 -3 -4 0 131.617 11.678 2 -3 -4 0 154.812 16.516 3 -3 4 0 124.463 14.811 1 -3 4 0 138.587 10.934 2 0 -3 -4 139.908 15.368 2 0 -3 4 108.446 9.931 1 0 -3 4 99.5991 19.2720 3 0 3 -4 147.689 9.126 2 0 4 -3 139.557 12.305 1 0 4 3 118.084 14.020 1 3 0 -4 121.679 15.448 2 0 -4 -3 114.166 11.226 3 0 -4 3 153.884 20.907 3 -4 3 0 164.452 12.698 2 -3 0 -4 161.936 13.711 2 -3 0 4 136.962 10.945 1 0 -4 -3 136.494 14.821 2 4 -1 3 291.484 23.099 3 -4 3 -1 299.268 17.751 2 3 -4 1 312.140 24.069 3 3 4 -1 269.181 18.449 1 -4 -3 1 275.967 21.638 3 -4 -1 -3 267.645 19.490 2 -4 -3 1 326.085 20.836 2 -1 3 4 297.653 19.912 1 -1 -4 3 277.096 25.187 3 -1 4 -3 250.886 18.406 1 -4 1 3 272.907 17.172 1 -4 1 3 305.876 22.934 2 -3 -4 -1 265.530 18.638 2 -3 -4 -1 231.262 20.747 3 1 4 3 278.788 20.049 1 3 -1 -4 295.688 23.147 2 -3 1 -4 257.613 17.558 2 4 -3 -1 267.590 19.982 3 -3 1 -4 270.046 15.653 1 3 1 4 269.707 22.050 3 -3 -1 4 274.029 16.746 3 -3 -1 4 254.253 16.517 1 -4 3 -1 275.252 20.204 1 1 -4 -3 275.174 21.178 2 1 3 -4 274.240 15.618 2 -1 -3 -4 302.514 22.615 2 1 -3 4 269.212 28.014 3 -3 4 1 244.638 21.020 1 -4 -1 3 281.516 22.841 2 1 4 -3 272.141 18.526 1 -1 -4 -3 237.516 19.117 3 -3 1 4 259.038 17.493 1 4 -3 1 280.163 22.286 3 4 3 -1 254.677 16.545 1 -4 -1 3 224.573 17.208 3 -1 -4 -3 257.770 20.978 2 -3 -1 -4 270.561 20.172 2 -3 -4 1 245.092 17.201 2 3 -1 4 249.849 22.747 3 3 1 -4 301.586 22.268 2 -1 4 3 240.411 20.128 1 4 1 3 295.634 22.485 3 3 -4 -1 286.608 21.284 3 -4 -3 -1 264.339 18.882 2 -4 -1 3 257.068 16.038 1 3 4 1 261.924 20.275 1 -3 4 -1 281.854 21.465 1 -3 4 -1 302.156 16.709 2 -4 3 1 271.463 20.055 1 -4 3 1 262.804 18.642 2 -1 -3 4 268.236 16.958 1 -1 -3 4 293.965 24.891 3 -1 3 -4 256.539 17.818 1 -1 3 -4 255.868 14.803 2 -4 1 -3 283.939 18.212 2 1 -3 -4 268.389 21.941 2 -3 -4 1 270.432 22.100 3 1 -4 3 265.147 26.449 3 1 3 4 247.224 17.299 1 1 3 4 284.574 19.732 3 3 -4 -1 253.046 18.291 2 -2 -3 -4 116.259 14.763 2 4 -3 -2 115.173 14.153 2 4 -2 3 116.264 16.320 3 4 3 2 114.357 15.534 3 3 -4 2 132.948 18.027 3 3 4 -2 112.383 10.867 1 2 -4 -3 97.0427 12.6127 2 2 -3 4 118.106 19.676 3 2 3 -4 123.760 10.563 2 2 4 3 113.058 11.896 1 3 -2 -4 123.358 15.269 2 -3 -2 4 113.125 11.901 3 -4 -2 -3 108.778 13.432 2 -4 -3 2 121.045 13.573 2 3 2 4 126.724 15.761 3 -2 3 4 122.928 12.979 1 -4 3 -2 123.901 10.140 2 -4 2 3 122.220 11.928 1 -3 -4 -2 124.942 13.521 2 -3 -4 -2 91.4009 13.4158 3 -3 -2 4 100.333 9.411 1 -4 -3 2 110.027 14.046 3 -3 2 -4 114.001 10.085 1 -3 4 2 136.202 15.635 1 -3 2 -4 93.6107 9.2547 2 -4 3 -2 130.632 13.555 1 -2 4 -3 107.306 12.157 1 -2 -4 3 93.4074 15.9778 3 -2 -3 4 112.097 15.675 3 4 -2 -3 110.553 15.023 2 3 4 2 106.278 12.158 1 -4 -2 3 116.636 9.540 1 3 -4 -2 128.165 12.897 2 -2 -3 4 112.645 9.997 1 -4 2 -3 111.381 10.145 2 -4 3 2 86.6596 12.0903 1 -4 3 2 102.875 11.986 2 -3 -2 -4 123.638 14.283 2 -3 -4 2 101.374 14.716 3 -3 4 -2 113.195 14.159 1 -3 4 -2 117.876 8.851 2 -4 -3 -2 95.1549 12.0071 2 -3 2 4 109.949 11.734 1 -2 -4 -3 127.341 14.693 2 -2 3 -4 99.9705 10.6050 1 -2 3 -4 116.297 8.813 2 -2 4 3 92.6472 13.5070 1 2 -3 -4 99.8981 13.9742 2 2 -4 3 113.034 19.115 3 2 4 -3 110.288 11.745 1 2 3 4 117.050 9.781 1 2 3 4 125.563 14.433 3 3 -2 4 133.430 18.141 3 3 2 -4 131.207 13.753 2 -4 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2 0 -4 4 3573.79 186.39 3 0 4 -4 3603.40 162.38 1 0 4 4 3651.53 164.38 1 4 -4 0 3685.43 179.18 3 4 0 -4 3478.61 167.70 2 4 0 4 3597.37 180.73 3 4 4 0 3552.47 162.48 1 -4 -4 -1 72.1603 10.4206 2 -4 -4 -1 34.4419 10.3958 3 -4 -4 1 55.8601 9.5350 2 -4 -4 1 63.7795 12.6418 3 -4 -1 -4 45.7408 9.4866 2 -4 -1 4 56.2579 7.5346 1 -4 1 -4 64.8011 8.9386 2 -4 1 4 55.2888 8.2909 1 -4 4 -1 66.5117 11.3360 1 -4 4 -1 72.6067 8.5452 2 -4 4 1 74.6427 12.4580 1 -4 4 1 56.2991 8.5911 2 -1 -4 4 81.1490 16.8758 3 -1 4 -4 55.6261 9.4197 1 1 -4 -4 55.1256 11.0649 2 1 -4 4 75.2557 18.1038 3 1 4 -4 58.7200 9.5368 1 1 4 4 48.9899 8.9691 1 1 4 4 72.6667 11.5121 3 4 -4 -1 72.2212 12.4912 3 4 -4 1 85.6892 14.6360 3 4 -1 -4 72.6433 14.0389 2 4 -1 4 70.0300 14.1796 3 4 1 -4 68.5059 13.5928 2 4 1 4 73.1229 13.7305 3 4 4 -1 64.5282 9.1433 1 -4 -4 -2 2856.56 139.08 2 -4 -4 2 2966.96 153.59 3 -4 -2 -4 3071.24 141.45 2 -4 -2 4 3015.87 135.38 1 -4 -2 4 3123.72 148.70 3 -4 2 -4 3067.53 134.87 2 -4 2 4 2856.40 137.91 1 -4 4 -2 3178.35 141.82 1 -4 4 -2 3253.26 134.05 2 -4 4 2 3008.06 142.45 1 -2 -4 -4 2958.90 142.29 2 -2 -4 4 3089.14 156.68 3 -2 4 -4 2991.60 138.46 1 2 -4 -4 3051.04 140.79 2 2 -4 4 3153.12 161.43 3 2 4 -4 3151.66 139.38 1 2 4 4 2992.01 151.88 3 4 -4 -2 3032.74 139.05 2 4 -4 2 3050.16 155.99 3 4 -2 -4 2962.03 143.07 2 4 -2 4 3144.88 156.87 3 4 2 -4 3133.24 142.23 2 4 2 4 2988.75 153.83 3 4 4 -2 3084.46 137.32 1 4 4 2 3017.28 154.83 3 -4 -4 -3 73.5651 13.1033 2 -4 -4 3 84.7536 14.3636 3 -4 -3 -4 58.4533 12.5692 2 -4 -3 4 90.5110 9.7840 1 -4 -3 4 74.6314 12.2090 3 -4 3 -4 63.8649 8.3351 2 -4 3 4 77.0692 12.0815 1 -4 4 -3 93.4797 13.4547 1 -4 4 3 55.1726 11.6096 1 -3 -4 -4 61.4553 12.9080 2 -3 -4 4 67.3045 14.4528 3 -3 4 -4 81.4469 11.6940 1 -3 4 4 76.7312 12.8781 1 3 -4 -4 66.6224 11.9993 2 3 -4 4 54.9717 16.2105 3 3 4 -4 85.0566 11.1881 1 3 4 4 71.1050 13.8810 3 4 -4 -3 55.7248 10.9368 2 4 -4 3 96.5056 17.9686 3 4 -3 -4 59.7545 12.2023 2 4 -3 4 81.2927 16.8867 3 4 3 -4 72.9593 11.7237 2 4 3 4 80.2825 14.4549 3 4 4 -3 80.7798 10.6677 1 4 4 3 86.5195 15.4446 3 -4 -4 -4 1867.74 96.29 2 -4 -4 4 1886.74 100.30 3 -4 4 4 1814.81 94.40 1 4 -4 -4 1887.51 93.54 2 4 -4 4 1949.37 106.75 3 4 4 -4 1911.44 90.95 1 4 4 4 1858.54 101.71 3 -5 0 0 304.653 20.773 2 0 -5 0 290.528 23.344 3 0 0 -5 272.215 20.603 2 0 0 5 290.708 17.586 1 0 0 5 295.833 24.589 3 0 5 0 292.902 22.987 1 5 0 0 279.067 20.465 3 -5 0 -1 92.5712 11.2865 2 -5 0 1 112.142 7.655 1 -5 0 1 114.873 12.781 2 -1 -5 0 96.5768 14.9394 3 -1 5 0 116.363 15.424 1 0 -1 -5 99.3906 12.9873 2 0 -1 5 101.386 9.148 1 0 -1 5 145.831 19.971 3 0 1 -5 128.045 12.066 2 0 1 5 123.905 10.378 1 1 -5 0 141.414 15.994 3 1 5 0 117.026 14.961 1 5 0 -1 118.072 11.815 3 5 0 1 130.329 13.664 3 0 -5 -1 118.150 11.285 2 0 -5 -1 115.241 15.030 3 0 -5 1 129.408 17.120 3 0 5 -1 112.874 14.204 1 0 5 1 109.817 14.968 1 1 0 -5 93.3506 12.3909 2 1 0 5 102.154 8.782 1 1 0 5 108.343 17.068 3 5 -1 0 122.499 13.070 3 5 1 0 129.574 13.950 3 -1 0 -5 105.868 12.281 2 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1 -5 0 -2 231.217 17.841 2 -5 0 2 226.736 14.381 1 -5 0 2 265.339 21.130 2 0 -2 -5 237.087 20.482 2 0 -2 5 249.119 16.003 1 0 -2 5 257.268 27.051 3 0 2 -5 240.499 16.718 2 5 0 2 226.594 20.439 3 -2 0 5 253.871 16.857 1 0 -5 -2 311.189 21.154 2 0 -5 -2 253.147 20.071 3 0 -5 2 256.667 24.080 3 0 5 -2 212.312 18.313 1 0 5 2 256.467 21.315 1 2 0 -5 250.700 20.544 2 2 5 0 275.824 21.315 1 5 0 -2 224.531 17.013 3 5 -2 0 268.360 20.104 3 5 2 0 252.174 21.102 3 2 0 5 262.676 15.027 1 2 0 5 260.050 24.012 3 -1 2 5 102.054 11.313 1 2 1 5 134.000 17.259 3 1 5 2 114.964 15.078 1 2 -1 -5 136.495 16.400 2 1 2 -5 118.061 11.475 2 5 1 -2 117.058 12.250 3 -1 -2 -5 127.783 15.287 2 -1 -5 2 140.504 19.345 3 -1 5 -2 126.579 14.773 1 1 -2 5 136.428 10.739 1 -5 -1 -2 125.231 13.218 2 -5 -2 1 136.923 14.712 2 5 -1 2 135.703 16.441 3 1 -2 5 156.925 23.857 3 -5 1 2 112.428 9.662 1 -5 1 2 131.510 14.796 2 -2 -5 -1 123.383 11.721 2 5 2 1 132.747 16.309 3 1 -5 -2 151.568 13.903 2 2 1 5 127.374 9.594 1 1 -5 -2 150.182 15.006 3 -5 2 -1 121.007 11.750 2 -2 -5 -1 117.129 15.156 3 -2 -1 5 126.920 10.826 1 -2 5 1 149.417 17.031 1 2 5 -1 134.008 14.365 1 5 -2 -1 126.897 13.162 3 2 -5 1 121.394 17.430 3 -2 1 -5 120.729 12.075 2 1 -5 2 137.643 18.863 3 1 5 -2 125.059 13.676 1 2 -5 -1 123.262 11.498 2 2 -5 -1 132.316 14.119 3 2 1 -5 126.144 14.011 2 -2 -1 -5 143.377 15.108 2 2 5 1 142.972 16.129 1 5 -1 -2 129.174 11.544 3 -5 -1 2 134.217 15.668 2 -5 -1 2 109.983 8.888 1 -1 -5 -2 111.017 13.855 3 -1 -2 5 120.777 10.580 1 -1 -2 5 107.971 16.356 3 -1 2 -5 111.087 10.287 2 -5 2 1 136.665 14.120 2 1 -2 -5 129.965 15.814 2 -1 5 2 119.373 15.521 1 -5 1 -2 134.406 12.382 2 -2 1 5 136.056 11.800 1 1 2 5 122.157 10.543 1 -5 -2 -1 145.800 13.683 2 -2 -5 1 151.541 18.795 3 -2 5 -1 132.411 16.195 1 -1 -5 -2 142.991 14.592 2 5 1 2 131.683 15.867 3 2 -1 5 126.798 19.066 3 2 -1 5 130.117 9.758 1 -5 2 1 121.584 10.586 1 5 -2 1 121.574 14.984 3 5 2 -1 120.677 9.277 1 5 2 -1 149.891 16.166 3 2 -5 -2 190.619 15.989 2 -5 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1 3138.99 150.43 3 -1 -3 5 2891.95 152.65 3 -1 3 -5 3092.78 135.16 1 -1 -5 -3 3045.33 138.09 2 1 -3 -5 2800.56 138.65 2 -1 5 3 2884.85 139.74 1 1 3 5 3002.80 133.91 1 3 -5 -1 2889.81 132.44 2 3 -5 -1 3098.48 147.97 3 1 -5 3 3082.15 155.86 3 -3 1 5 2956.96 134.89 1 -5 -3 -1 2817.68 135.79 2 -1 -5 -3 2881.59 148.53 3 3 -1 5 3042.96 153.86 3 3 1 -5 2952.37 138.36 2 -1 -3 5 3081.05 133.86 1 -5 -1 3 3032.95 141.10 2 3 5 1 3156.41 139.63 1 1 5 -3 2959.22 136.55 1 -5 3 1 2955.90 135.18 2 -3 5 -1 3001.03 139.82 1 5 1 3 2953.79 150.77 3 5 3 2 96.7920 15.9433 3 -3 -5 -2 97.3024 13.1497 2 -5 -2 -3 92.6115 13.1915 2 3 5 -2 89.8538 11.8660 1 -2 -5 3 67.4598 16.1295 3 -2 5 -3 96.8412 13.5997 1 -2 -3 -5 93.6959 14.5219 2 2 -5 -3 99.9306 12.6246 2 -5 -3 2 101.491 14.520 2 -5 -3 2 84.2496 13.5948 3 -3 -5 -2 55.3075 12.2963 3 3 -2 -5 86.4288 15.3050 2 -3 2 -5 97.1249 9.9904 2 -5 2 3 97.7270 11.2500 1 3 2 5 116.341 16.478 3 -2 3 5 114.497 13.247 1 2 5 3 118.775 14.187 1 2 -3 5 111.482 21.581 3 -3 2 -5 95.0904 9.7842 1 -3 5 2 95.7589 14.6764 1 -5 3 -2 108.468 10.784 2 3 -5 2 69.9366 16.0329 3 -3 -2 5 87.3004 9.7666 1 5 -2 3 115.704 17.317 3 2 -3 -5 80.6128 13.9689 2 3 -2 5 94.6007 18.1919 3 5 2 3 86.4518 15.0694 3 -3 -5 2 90.4547 16.0401 3 -2 -5 -3 61.0124 11.7981 3 2 3 5 95.1204 9.5475 1 -2 5 3 90.7923 14.3529 1 -2 -3 5 92.1441 10.2426 1 3 2 -5 91.4720 12.6489 2 -2 3 -5 84.1574 10.2327 1 5 -2 -3 110.134 16.371 2 2 3 5 129.668 16.280 3 -5 3 2 79.8998 11.6665 1 -5 3 2 117.339 13.748 2 5 -3 2 94.4133 16.1293 3 -3 5 -2 102.028 15.061 1 -5 -3 -2 79.0502 11.9774 2 3 5 2 92.6307 13.2877 1 -3 2 5 76.3100 10.9293 1 -3 -2 -5 103.217 14.633 2 5 3 -2 82.4366 9.2033 1 -5 -2 3 107.319 15.568 2 -2 -3 5 71.6596 14.1030 3 -5 -2 3 94.3766 8.9556 1 -2 -5 -3 89.1728 14.0207 2 -5 -2 3 59.5358 10.0023 3 -5 2 -3 116.800 11.371 2 2 -5 3 82.7164 17.7357 3 2 5 -3 98.4016 12.2396 1 3 -5 -2 85.7447 11.0234 2 3 -5 -3 2036.97 100.11 2 -5 -3 3 2136.28 110.17 3 3 -5 3 2070.28 115.80 3 5 -3 3 2230.60 114.81 3 5 3 3 2072.37 112.56 3 -3 5 3 2113.05 104.99 1 -3 -3 -5 2113.93 104.98 2 -3 -3 5 2127.72 98.38 1 -5 -3 3 2004.27 103.12 2 -3 -5 3 2024.62 113.40 3 5 -3 -3 2162.05 104.75 2 -3 3 5 2154.20 102.58 1 -3 5 -3 2186.85 104.14 1 3 5 -3 2072.03 100.49 1 3 5 3 2188.50 100.46 1 -5 3 -3 2166.22 97.20 2 -5 3 3 2170.51 102.31 1 -3 3 -5 2172.47 99.01 1 -3 3 -5 2295.70 95.97 2 -5 -3 -3 1942.81 102.45 2 -5 -3 3 2043.56 96.50 1 -3 -5 -3 2047.82 103.85 2 -3 -3 5 2104.60 109.04 3 3 3 5 2212.82 112.03 3 3 -3 5 2128.78 118.38 3 3 -3 -5 2123.44 105.29 2 4 -5 0 131.091 13.730 2 4 5 0 186.605 18.020 1 5 0 -4 126.907 19.322 2 5 0 4 161.786 20.644 3 0 4 5 148.607 15.284 1 0 4 -5 127.001 14.622 1 0 5 4 143.078 16.712 1 4 0 -5 145.867 19.545 2 0 -5 -4 140.665 17.283 2 0 -5 4 217.098 27.276 3 0 5 -4 142.780 15.618 1 -5 4 0 136.392 16.204 1 -5 4 0 131.227 13.515 2 4 0 5 146.747 21.127 3 4 -5 0 151.088 19.437 3 0 -4 5 166.265 26.724 3 -5 0 -4 142.813 15.236 2 -5 0 4 151.765 12.543 1 -4 -5 0 123.210 18.525 3 -4 5 0 131.260 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1481.08 89.55 3 -5 -5 -2 51.0315 12.0797 2 -5 -5 2 72.4638 17.2449 3 -5 -2 -5 55.3743 12.6751 2 -5 -2 5 58.6159 9.2306 1 -5 2 -5 55.9422 9.4617 2 -5 2 5 57.5047 11.0670 1 -5 5 2 47.4305 11.9287 1 -2 -5 -5 68.9404 14.8954 2 -2 -5 5 27.3020 15.1543 3 -2 5 -5 49.7095 10.8588 1 -2 5 5 38.7943 10.8441 1 2 -5 -5 79.0528 13.2437 2 2 -5 5 43.1582 18.0164 3 2 5 -5 57.2494 11.6539 1 2 5 5 50.7727 9.5113 1 5 -5 -2 60.5222 11.6752 2 5 -5 2 48.6130 15.7365 3 5 -2 -5 42.6706 12.3166 2 5 -2 5 57.3607 17.0698 3 5 2 -5 59.2850 14.4307 2 5 2 5 70.2278 16.8131 3 5 5 -2 60.0040 10.9718 1 5 5 2 55.4083 15.7486 3 -5 -5 -3 1110.54 65.83 2 -5 -5 3 1151.24 70.32 3 -5 -3 -5 1117.98 66.07 2 -5 -3 5 1132.49 58.50 1 -5 3 5 1144.41 63.50 1 -5 5 3 1214.49 66.11 1 -3 -5 -5 1239.99 69.09 2 -3 5 -5 1116.81 62.19 1 -3 5 5 1173.99 65.90 1 3 -5 -5 1121.27 63.04 2 3 -5 5 1217.24 77.05 3 3 5 -5 1233.99 63.38 1 5 -5 -3 1149.66 62.38 2 5 -5 3 1123.20 71.96 3 5 -3 -5 1112.86 65.92 2 5 -3 5 1153.98 74.62 3 5 3 5 1111.56 70.07 3 5 5 -3 1141.91 60.48 1 5 5 3 1159.11 71.26 3 -5 -5 -4 90.1243 17.5404 2 -5 -5 4 79.3515 18.1950 3 -5 -4 -5 62.8693 15.0649 2 -5 4 5 69.7267 14.7595 1 -5 5 4 31.7457 11.1533 1 -4 -5 -5 72.7051 16.3262 2 -4 -5 5 46.3842 15.7802 3 -4 5 5 68.1565 15.0328 1 4 -5 -5 47.3790 11.8269 2 4 -5 5 45.6302 18.9576 3 4 5 -5 52.8272 12.0773 1 5 -5 -4 40.6641 11.2858 2 5 -5 4 57.7097 18.5421 3 5 -4 -5 57.1868 13.6346 2 5 -4 5 68.0901 20.0929 3 5 4 -5 66.5410 12.1463 1 5 4 5 63.5972 17.8467 3 5 5 -4 68.9589 12.4237 1 5 5 4 72.4347 18.0494 3 -5 -5 -5 598.782 46.160 2 -5 5 5 635.605 44.079 1 5 -5 -5 625.278 42.527 2 5 -5 5 537.652 49.495 3 5 5 -5 638.757 40.722 1 5 5 5 715.733 51.043 3 -6 0 0 2865.47 142.36 2 0 -6 0 3219.94 159.17 3 0 0 -6 3072.44 143.20 2 0 0 6 3169.73 139.73 1 0 6 0 3241.12 148.40 1 6 0 0 3219.96 155.18 3 -6 0 -1 60.4298 10.5041 2 -6 0 1 44.3515 10.0794 2 -1 -6 0 64.9941 14.8784 3 -1 6 0 62.1610 12.9761 1 0 -1 -6 58.3460 11.3281 2 0 -1 6 48.7463 7.4927 1 0 1 -6 67.4706 10.7136 2 0 1 6 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0 7 5 13.7292 8.7855 1 5 0 -7 25.2925 13.5220 2 5 0 7 28.8952 19.6504 3 7 5 0 13.5600 13.1295 3 7 0 -5 27.2347 13.0306 2 -7 0 -5 23.3229 9.5699 2 -5 -7 0 25.5832 17.3874 3 7 0 5 18.7255 15.8788 3 0 -5 -7 51.3091 13.5524 2 0 5 7 8.03837 7.35746 1 -1 7 -5 647.069 45.103 1 7 -5 -1 681.517 43.311 2 5 -7 1 591.327 45.926 3 7 5 1 699.600 50.797 3 7 -1 5 665.458 52.244 3 7 1 -5 651.484 49.543 2 -5 7 1 710.386 43.693 1 1 5 -7 682.616 43.331 1 -5 1 -7 722.185 41.768 2 -1 5 7 750.733 44.968 1 -7 -1 -5 633.529 44.054 2 -5 -1 7 657.748 40.281 1 5 1 7 643.843 53.738 3 1 -5 7 605.659 57.075 3 -1 -5 -7 580.681 44.955 2 5 -1 -7 670.284 49.982 2 5 -1 7 612.893 53.698 3 1 -7 5 664.042 52.951 3 7 -1 -5 700.546 50.165 2 7 5 -1 552.196 46.835 3 -7 1 -5 702.623 41.964 2 -5 1 7 595.145 40.756 1 5 1 -7 701.330 48.217 2 -5 -7 1 735.712 54.596 3 1 7 -5 682.831 45.394 1 7 1 5 653.521 51.304 3 -1 5 -7 654.204 42.056 1 -5 -1 -7 665.231 44.472 2 2 5 -7 23.7265 9.9030 1 5 -2 -7 15.3092 11.2693 2 -2 -7 5 8.8640 18.7691 3 7 -2 5 17.5233 16.8927 3 7 2 -5 20.9645 11.8598 2 -5 -2 7 29.4268 9.1260 1 2 -5 7 40.8237 21.6134 3 -5 7 2 27.8848 10.1169 1 5 -7 2 26.2169 15.8481 3 7 5 2 21.1583 15.2164 3 -2 5 7 25.4254 10.5256 1 -7 -2 -5 25.4939 10.9062 2 -2 7 -5 25.3518 11.4835 1 -2 -5 -7 27.4808 12.1768 2 7 -5 -2 10.2055 8.1080 2 2 -5 -7 20.4783 10.0341 2 2 -7 5 29.4072 17.8935 3 -7 2 -5 34.6644 9.9105 2 -5 -2 -7 32.6957 11.6534 2 7 2 5 14.9771 15.5659 3 -5 -7 2 15.7910 17.2618 3 7 -2 -5 23.8586 11.3869 2 -5 2 7 19.3131 9.3850 1 -2 7 5 11.6595 8.7048 1 7 5 -2 26.6987 14.8168 3 2 7 -5 32.8335 11.7759 1 5 7 2 29.2258 17.9692 3 5 -2 7 29.3174 20.4249 3 -2 5 -7 21.7416 9.1932 1 7 -5 2 35.8393 16.1826 3 -3 7 -5 470.278 37.805 1 -3 -5 -7 530.030 42.479 2 7 -5 -3 565.395 39.153 2 -5 -3 7 504.566 34.145 1 7 5 -3 520.447 41.837 3 -7 -5 -3 567.179 43.887 2 0 6 7 61.1155 14.1430 1 0 7 6 56.3884 14.4315 1 -8 0 0 1022.27 62.20 2 0 -8 0 1081.15 66.45 3 0 0 -8 1067.76 61.68 2 0 0 8 1185.79 58.54 1 0 8 0 1080.67 63.64 1 8 0 0 1137.00 65.11 3 -8 0 -1 11.9495 7.7215 2 -8 0 1 20.8290 9.5983 2 -1 -8 0 13.2026 12.0421 3 -1 8 0 29.7428 11.1314 1 0 -1 -8 16.0092 9.0452 2 0 -1 8 19.9013 7.0369 1 0 1 -8 8.40778 6.65440 2 0 1 8 8.73473 6.50413 1 1 -8 0 21.6603 11.5216 3 1 8 0 18.6011 10.1584 1 8 0 1 16.9526 11.6139 3 1 0 8 16.7095 6.1636 1 8 -1 0 17.3542 11.5804 3 8 1 0 32.2750 12.6703 3 0 -8 -1 21.0762 11.8814 3 0 -8 1 15.9983 11.4869 3 0 8 -1 15.5945 9.1434 1 0 8 1 3.39242 8.21696 1 1 0 -8 6.32671 7.35990 2 -1 0 8 9.66228 6.80214 1 -1 0 -8 8.96119 8.00811 2 -8 -1 0 11.1336 7.6283 2 -8 1 0 11.5490 7.4810 2 1 8 -1 190.281 23.236 1 8 1 1 199.685 24.882 3 -8 1 1 218.420 23.758 2 -1 -8 1 164.922 24.599 3 -1 -1 -8 162.871 20.706 2 -8 -1 1 195.523 23.460 2 -8 1 -1 206.650 21.401 2 -1 1 -8 244.677 21.256 2 -1 1 8 223.383 19.288 1 -8 -1 -1 226.581 23.712 2 1 -1 8 217.257 17.700 1 1 8 1 181.397 21.816 1 8 -1 1 211.116 25.059 3 8 1 -1 177.929 21.988 3 1 1 8 223.537 18.043 1 -1 8 -1 124.800 19.692 1 -1 8 1 150.432 20.445 1 1 -1 -8 208.022 23.586 2 -1 -1 8 193.475 17.722 1 1 1 -8 222.951 22.171 2 0 8 -2 909.171 57.891 1 -8 2 0 1024.79 57.86 2 -2 0 -8 987.776 56.939 2 -2 0 8 968.267 53.905 1 8 0 2 953.777 61.700 3 -8 -2 0 974.016 58.746 2 2 0 -8 1031.78 58.75 2 8 2 0 884.080 59.519 3 2 -8 0 1013.13 59.54 3 2 8 0 898.214 56.713 1 -8 0 -2 984.169 57.023 2 -8 0 2 813.300 57.578 2 -2 -8 0 1010.83 62.90 3 -2 8 0 963.359 58.361 1 0 -2 8 1009.77 52.73 1 0 2 8 1011.15 53.68 1 8 -1 2 8.0736 11.9806 3 -8 -2 1 6.14604 7.79795 2 -8 2 -1 17.4322 8.1159 2 2 -1 -8 17.3907 9.6415 2 2 8 -1 21.1663 10.3142 1 -2 -1 8 17.2477 7.1212 1 -2 1 -8 20.7867 8.6889 2 -1 8 -2 12.0446 8.9641 1 -8 -1 -2 19.3209 9.1523 2 1 -2 8 13.4688 6.3985 1 1 8 2 -4.5960 6.7117 1 -8 1 2 14.6150 9.1240 2 -2 -8 -1 7.1402 10.1990 3 -1 -8 2 -3.7284 11.7650 3 2 -8 1 16.4202 11.2593 3 -2 8 1 6.59898 7.70702 1 -1 -2 -8 17.6284 10.0192 2 8 2 1 9.7716 11.4455 3 -1 2 8 -0.0247 5.2431 1 -2 -8 1 19.1353 14.0389 3 -2 1 8 16.9634 7.7992 1 -8 1 -2 11.6231 7.9179 2 -2 8 -1 24.0941 10.6638 1 -2 -1 -8 24.3469 10.2249 2 2 8 1 12.1709 9.1790 1 -8 -2 -1 15.7525 9.2178 2 -8 -1 2 25.3362 10.9418 2 8 -2 1 18.2149 12.6668 3 8 2 -1 4.3262 10.0267 3 8 1 2 13.7610 12.3460 3 1 -2 -8 12.0514 9.3371 2 -1 -2 8 18.0376 7.3043 1 -1 8 2 18.6243 9.4150 1 1 -8 2 24.4775 12.8119 3 1 8 -2 17.7821 10.0008 1 1 2 8 14.0217 6.8480 1 -8 2 1 20.5949 10.0067 2 2 1 -8 16.2210 8.8435 2 -8 -2 -2 910.448 54.982 2 -8 -2 2 895.640 57.565 2 -8 2 -2 838.298 49.826 2 2 -2 -8 863.696 56.179 2 2 8 -2 793.234 52.992 1 8 -2 2 819.796 56.680 3 8 2 2 846.899 58.152 3 -2 8 2 827.663 52.550 1 2 -8 2 829.435 55.175 3 -2 -2 8 825.999 48.106 1 -8 2 2 972.693 56.370 2 -2 8 -2 860.838 53.821 1 -2 -8 -2 923.702 58.467 3 -2 2 8 850.025 50.489 1 -2 -2 -8 801.164 53.405 2 -2 -8 2 834.670 59.946 3 0 -3 8 17.3554 6.8801 1 0 3 8 26.5562 8.9277 1 3 8 0 11.6744 10.1770 1 8 0 3 44.1699 16.0720 3 -8 0 3 -0.2152 7.8235 2 0 -3 -8 24.7281 11.5525 2 -3 8 0 26.0220 10.8434 1 -3 0 -8 22.0385 10.1759 2 -3 -8 0 20.1974 14.4550 3 0 -8 3 10.5631 13.6945 3 -8 -3 0 20.0670 10.1815 2 -8 3 0 22.0949 9.1031 2 0 8 -3 12.9837 10.2477 1 0 8 3 18.3887 9.1594 1 3 0 -8 14.0953 9.7316 2 8 3 0 26.2534 13.9037 3 -8 0 -3 9.04788 7.84352 2 -3 0 8 17.3039 7.5865 1 -3 8 1 104.655 17.278 1 -1 8 -3 114.406 19.099 1 3 8 -1 150.989 20.811 1 -8 -1 -3 172.685 21.328 2 -3 1 -8 158.477 18.146 2 -1 3 8 152.990 18.085 1 -8 1 3 152.490 21.778 2 1 8 3 169.430 20.349 1 -1 -8 3 58.5939 19.5569 3 -8 -3 1 173.807 23.810 2 -8 3 -1 156.791 18.418 2 3 -8 1 132.228 20.749 3 -1 -3 -8 167.072 22.411 2 8 3 1 138.833 23.486 3 8 -1 3 130.476 22.980 3 3 -1 -8 132.389 21.106 2 -3 -8 -1 109.545 21.505 3 -3 -1 8 158.290 17.715 1 -8 3 1 189.985 20.792 2 1 8 -3 103.416 18.675 1 -1 8 3 186.038 21.467 1 -3 8 -1 113.910 18.408 1 -8 -1 3 168.924 23.877 2 -8 1 -3 161.002 18.655 2 1 -3 -8 136.083 21.428 2 -3 1 8 146.433 17.633 1 -3 -8 1 127.156 24.931 3 1 -8 3 130.814 22.487 3 -3 -1 -8 130.903 19.358 2 -1 -3 8 141.222 16.108 1 -1 3 -8 116.705 15.362 1 8 -3 1 165.636 23.910 3 8 3 -1 172.709 23.590 3 3 8 1 152.292 19.825 1 -8 -3 -1 147.100 21.274 2 3 1 -8 136.398 18.845 2 8 1 3 166.107 25.450 3 -8 -2 -3 9.95127 9.12515 2 -3 -2 8 25.3256 8.7436 1 3 -8 2 8.7572 12.3542 3 3 8 -2 18.1478 9.7656 1 -2 8 -3 15.8921 10.0369 1 8 -2 3 2.8368 13.3741 3 -8 -3 2 12.9588 11.2459 2 -8 3 -2 14.5047 7.8662 2 2 8 3 18.5750 10.1888 1 -2 -8 3 20.6573 17.4762 3 8 3 2 -9.0058 11.5529 3 -3 8 2 20.2037 9.8688 1 -2 -3 -8 11.4358 8.8928 2 -3 -8 -2 24.8363 13.2318 3 3 -2 -8 21.5252 11.5405 2 -2 3 8 8.11241 7.51651 1 -8 -3 -2 -2.0941 7.6232 2 8 2 3 13.3965 13.9160 3 2 8 -3 0.92305 8.68799 1 2 -3 -8 12.6379 10.1538 2 -3 -2 -8 16.0182 9.5291 2 -3 8 -2 6.95852 9.66604 1 -3 2 8 19.6675 8.6984 1 -3 -8 2 0.6476 15.6121 3 -2 -3 8 11.2405 6.9917 1 -8 -2 3 18.9226 11.5757 2 -8 2 -3 16.5261 7.9302 2 -8 3 2 3.69907 7.26243 2 8 -2 -3 25.5734 13.0134 2 8 -3 2 4.8252 13.6602 3 2 -8 3 20.6050 13.4071 3 -2 8 3 11.7700 8.7937 1 -3 -3 -8 77.2934 17.5006 2 -3 8 -3 85.5348 16.6410 1 -8 3 -3 118.832 15.567 2 8 -3 -3 77.6808 18.1810 2 8 -3 3 101.529 22.437 3 3 8 -3 104.351 18.305 1 3 -3 -8 111.336 20.534 2 -3 -3 8 111.965 15.343 1 -3 3 8 94.2181 16.6988 1 -8 -3 -3 93.1786 18.8137 2 -3 8 3 106.131 17.525 1 3 -8 3 117.208 20.905 3 0 8 -4 572.255 44.361 1 8 4 0 610.817 48.161 3 -8 0 -4 646.967 43.052 2 4 0 -8 632.692 46.972 2 -8 -4 0 651.277 47.386 2 -8 4 0 684.763 42.315 2 -4 -8 0 685.188 52.364 3 0 4 -8 579.098 39.997 1 0 4 8 723.581 42.206 1 -4 0 8 595.890 40.546 1 0 8 4 651.698 43.610 1 0 -8 4 680.176 52.416 3 8 0 -4 655.887 50.226 2 8 0 4 528.845 47.936 3 -4 0 -8 692.756 43.717 2 4 -1 -8 3.22968 9.81151 2 8 1 -4 15.9258 12.7226 2 -8 -1 -4 8.55368 8.66760 2 -1 -8 4 5.1664 17.1094 3 -1 8 -4 9.72786 9.88196 1 -4 8 1 10.1110 8.8556 1 1 4 -8 1.27368 6.87856 1 -4 -8 -1 20.5393 15.9258 3 -4 1 -8 18.3283 8.9971 2 -4 -1 8 16.7461 7.8822 1 -1 -4 -8 7.20431 9.71652 2 4 -8 1 1.7667 11.2717 3 -1 4 8 13.4922 8.7702 1 -8 4 -1 18.3314 8.5196 2 1 8 4 16.4013 9.9793 1 -1 8 4 6.78724 9.64097 1 8 -1 -4 0.45360 8.66250 2 -1 4 -8 11.7047 7.5658 1 -8 1 -4 13.4275 7.7259 2 -8 4 1 1.83386 7.03636 2 -4 -1 -8 15.8134 9.6230 2 -8 -4 -1 10.7829 10.9886 2 -4 8 -1 6.68693 9.00284 1 4 1 -8 5.42091 8.96920 2 8 4 -1 -9.4224 11.3792 3 1 -4 -8 -1.3509 7.6101 2 -4 1 8 8.53964 7.48866 1 1 -8 4 9.8874 15.1053 3 1 8 -4 0.82362 8.13575 1 4 8 -2 486.198 38.124 1 8 2 -4 499.944 43.393 2 8 -4 -2 568.054 41.215 2 4 -8 2 557.619 41.765 3 -8 -4 -2 558.563 43.232 2 -8 2 -4 516.736 35.658 2 8 4 -2 517.606 41.786 3 -9 0 0 207.529 24.282 2 0 -9 0 46.9420 15.6005 3 0 0 -9 122.913 18.271 2 0 0 9 162.352 17.043 1 0 9 0 98.5376 17.2863 1 -9 0 -1 5.32696 8.75014 2 -9 0 1 7.52750 9.73335 2 -1 -9 0 4.5347 10.9949 3 -1 9 0 12.9039 9.2141 1 0 -1 -9 23.2681 10.8270 2 0 -1 9 18.0274 8.2445 1 0 1 9 9.21283 7.69215 1 1 -9 0 10.5519 11.7835 3 1 9 0 10.7097 9.1333 1 9 0 1 15.7356 14.0010 3 0 9 1 7.57880 8.68967 1 1 0 -9 10.4878 9.0011 2 -9 -1 0 10.9308 9.2171 2 -9 1 0 30.9966 11.1720 2 -1 0 -9 11.5833 9.6020 2 -1 0 9 5.03260 7.06809 1 0 -9 1 10.0598 12.3645 3 0 9 -1 -2.2287 8.2677 1 9 1 0 10.6577 13.1536 3 9 -1 1 501.779 40.988 3 -1 1 9 549.050 36.322 1 -1 -9 -1 500.508 39.562 3 -1 -1 -9 558.048 40.006 2 -1 -1 9 519.162 34.985 1 0 -2 9 114.656 15.161 1 0 2 9 103.361 15.360 1 2 0 -9 126.934 19.785 2 -2 0 -9 81.8445 16.1726 2 2 -9 1 -5.0036 10.9309 3 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 16790 _shelx_res_file ; TITL tak10_0m in Pm-3m Ba3PbO 295K CELL 0.71073 5.4893 5.4893 5.4893 90.000 90.000 90.000 ZERR 1.00 0.0073 0.0073 0.0073 0.000 0.000 0.000 LATT 1 SYMM -X, -Y, Z SYMM -X, Y, -Z SYMM X, -Y, -Z SYMM Z, X, Y SYMM Z, -X, -Y SYMM -Z, -X, Y SYMM -Z, X, -Y SYMM Y, Z, X SYMM -Y, Z, -X SYMM Y, -Z, -X SYMM -Y, -Z, X SYMM Y, X, -Z SYMM -Y, -X, -Z SYMM Y, -X, Z SYMM -Y, X, Z SYMM X, Z, -Y SYMM -X, Z, Y SYMM -X, -Z, -Y SYMM X, -Z, Y SYMM Z, Y, -X SYMM Z, -Y, X SYMM -Z, Y, X SYMM -Z, -Y, -X SFAC O BA PB UNIT 1 3 1 TEMP 24.840 SIZE 0.02 0.03 0.05 ACTA L.S. 4 BOND FMAP 2 PLAN 20 WGHT 0.015100 0.067100 EXTI 0.101546 FVAR 0.76523 PB 3 0.500000 0.500000 0.500000 10.02083 0.01680 0.01680 = 0.01680 0.00000 0.00000 0.00000 BA 2 0.500000 0.000000 0.000000 10.06250 0.01372 0.03063 = 0.03063 0.00000 0.00000 0.00000 O 1 0.000000 0.000000 0.000000 10.02083 0.01538 0.01538 = 0.01538 0.00000 0.00000 0.00000 HKLF 4 REM tak10_0m in Pm-3m Ba3PbO 295K REM R1 = 0.0124 for 116 Fo > 4sig(Fo) and 0.0137 for all 117 data REM 6 parameters refined using 0 restraints END WGHT 0.0150 0.0664 REM Highest difference peak 0.954, deepest hole -0.735, 1-sigma level 0.156 Q1 1 0.5000 0.0000 0.1238 10.25000 0.05 0.95 Q2 1 0.3779 0.0000 0.0000 10.12500 0.05 0.90 Q3 1 0.3965 0.0000 0.0561 10.50000 0.05 0.76 Q4 1 0.4322 0.4322 0.4322 10.16667 0.05 0.71 Q5 1 0.5000 0.5000 0.3498 10.12500 0.05 0.61 Q6 1 0.5000 0.0000 0.5000 10.06250 0.05 0.51 Q7 1 0.0000 0.1005 0.1005 10.25000 0.05 0.29 Q8 1 0.0942 0.0942 0.0942 10.16667 0.05 0.28 Q9 1 0.3654 0.3013 0.1783 11.00000 0.05 0.22 Q10 1 0.1878 0.4244 0.4244 10.50000 0.05 0.21 Q11 1 0.5000 0.5000 0.2031 10.12500 0.05 0.20 Q12 1 0.4079 0.2476 0.4079 10.50000 0.05 0.19 Q13 1 0.1943 0.0000 0.0000 10.12500 0.05 0.19 Q14 1 0.2684 0.0000 0.1012 10.50000 0.05 0.19 Q15 1 0.4319 0.0000 0.2727 10.50000 0.05 0.17 Q16 1 0.5000 0.3094 0.1869 10.50000 0.05 0.17 Q17 1 0.3264 0.3264 0.4200 10.50000 0.05 0.16 Q18 1 0.3755 0.3755 0.0780 10.50000 0.05 0.15 Q19 1 0.1318 0.1318 0.1844 10.50000 0.05 0.13 Q20 1 0.5000 0.1697 0.1697 10.25000 0.05 0.13 ; _shelx_res_checksum 98835 _shelxl_version_number 20.13 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' '-x, y, -z' 'x, -y, -z' 'z, x, y' 'z, -x, -y' '-z, -x, y' '-z, x, -y' 'y, z, x' '-y, z, -x' 'y, -z, -x' '-y, -z, x' 'y, x, -z' '-y, -x, -z' 'y, -x, z' '-y, x, z' 'x, z, -y' '-x, z, y' '-x, -z, -y' 'x, -z, y' 'z, y, -x' 'z, -y, x' '-z, y, x' '-z, -y, -x' '-x, -y, -z' 'x, y, -z' 'x, -y, z' '-x, y, z' '-z, -x, -y' '-z, x, y' 'z, x, -y' 'z, -x, y' '-y, -z, -x' 'y, -z, x' '-y, z, x' 'y, z, -x' '-y, -x, z' 'y, x, z' '-y, x, -z' 'y, -x, -z' '-x, -z, y' 'x, -z, -y' 'x, z, y' '-x, z, -y' '-z, -y, x' '-z, y, -x' 'z, -y, -x' 'z, y, x' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pb Pb 0.5000 0.5000 0.5000 0.01680(15) Uani d 1 . . Ba Ba 0.5000 0.0000 0.0000 0.02499(13) Uani d 1 . . O O 0.0000 0.0000 0.0000 0.0154(11) Uani d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Pb 0.01680(15) 0.01680(15) 0.01680(15) 0.000 0.000 0.000 Ba 0.01372(16) 0.03063(15) 0.03063(15) 0.000 0.000 0.000 O 0.0154(11) 0.0154(11) 0.0154(11) 0.000 0.000 0.000 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ba Ba -0.3244 2.2819 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Pb Pb -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle Ba Pb Ba 9_665 . 120.0 Ba Pb Ba 9_665 9 180.0 Ba Pb Ba . 9 60.0 Ba Pb Ba 9_665 5_656 60.0 Ba Pb Ba . 5_656 120.0 Ba Pb Ba 9 5_656 120.0 Ba Pb Ba 9_665 1_566 60.0 Ba Pb Ba . 1_566 180.0 Ba Pb Ba 9 1_566 120.0 Ba Pb Ba 5_656 1_566 60.0 Ba Pb Ba 9_665 5 120.0 Ba Pb Ba . 5 60.0 Ba Pb Ba 9 5 60.0 Ba Pb Ba 5_656 5 180.0 Ba Pb Ba 1_566 5 120.0 Ba Pb Ba 9_665 1_565 60.0 Ba Pb Ba . 1_565 90.0 Ba Pb Ba 9 1_565 120.0 Ba Pb Ba 5_656 1_565 120.0 Ba Pb Ba 1_566 1_565 90.0 Ba Pb Ba 5 1_565 60.0 Ba Pb Ba 9_665 5_556 120.0 Ba Pb Ba . 5_556 120.0 Ba Pb Ba 9 5_556 60.0 Ba Pb Ba 5_656 5_556 90.0 Ba Pb Ba 1_566 5_556 60.0 Ba Pb Ba 5 5_556 90.0 Ba Pb Ba 1_565 5_556 120.0 Ba Pb Ba 9_665 5_655 60.0 Ba Pb Ba . 5_655 60.0 Ba Pb Ba 9 5_655 120.0 Ba Pb Ba 5_656 5_655 90.0 Ba Pb Ba 1_566 5_655 120.0 Ba Pb Ba 5 5_655 90.0 Ba Pb Ba 1_565 5_655 60.0 Ba Pb Ba 5_556 5_655 180.0 Ba Pb Ba 9_665 1_556 120.0 Ba Pb Ba . 1_556 90.0 Ba Pb Ba 9 1_556 60.0 Ba Pb Ba 5_656 1_556 60.0 Ba Pb Ba 1_566 1_556 90.0 Ba Pb Ba 5 1_556 120.0 Ba Pb Ba 1_565 1_556 180.0 Ba Pb Ba 5_556 1_556 60.0 Ba Pb Ba 5_655 1_556 120.0 Ba Pb Ba 9_665 9_655 90.0 Ba Pb Ba . 9_655 60.0 Ba Pb Ba 9 9_655 90.0 Ba Pb Ba 5_656 9_655 60.0 Ba Pb Ba 1_566 9_655 120.0 Ba Pb Ba 5 9_655 120.0 Ba Pb Ba 1_565 9_655 120.0 Ba Pb Ba 5_556 9_655 120.0 Ba Pb Ba 5_655 9_655 60.0 Ba Pb Ba 1_556 9_655 60.0 Ba Pb Ba 9_665 9_565 90.0 Ba Pb Ba . 9_565 120.0 Ba Pb Ba 9 9_565 90.0 Ba Pb Ba 5_656 9_565 120.0 Ba Pb Ba 1_566 9_565 60.0 Ba Pb Ba 5 9_565 60.0 Ba Pb Ba 1_565 9_565 60.0 Ba Pb Ba 5_556 9_565 60.0 Ba Pb Ba 5_655 9_565 120.0 Ba Pb Ba 1_556 9_565 120.0 Ba Pb Ba 9_655 9_565 180.0 O Ba O 1_655 . 180.0 O Ba Pb 1_655 . 90.0 O Ba Pb . . 90.0 O Ba Pb 1_655 1_544 90.0 O Ba Pb . 1_544 90.0 Pb Ba Pb . 1_544 180.0 O Ba Ba 1_655 9_655 45.0 O Ba Ba . 9_655 135.0 Pb Ba Ba . 9_655 60.0 Pb Ba Ba 1_544 9_655 120.0 O Ba Ba 1_655 9_554 135.0 O Ba Ba . 9_554 45.0 Pb Ba Ba . 9_554 120.0 Pb Ba Ba 1_544 9_554 60.0 Ba Ba Ba 9_655 9_554 180.0 O Ba Ba 1_655 5_545 135.0 O Ba Ba . 5_545 45.0 Pb Ba Ba . 5_545 120.0 Pb Ba Ba 1_544 5_545 60.0 Ba Ba Ba 9_655 5_545 120.0 Ba Ba Ba 9_554 5_545 60.0 O Ba Ba 1_655 5_655 45.0 O Ba Ba . 5_655 135.0 Pb Ba Ba . 5_655 60.0 Pb Ba Ba 1_544 5_655 120.0 Ba Ba Ba 9_655 5_655 60.0 Ba Ba Ba 9_554 5_655 120.0 Ba Ba Ba 5_545 5_655 180.0 O Ba Pb 1_655 1_554 90.0 O Ba Pb . 1_554 90.0 Pb Ba Pb . 1_554 90.0 Pb Ba Pb 1_544 1_554 90.0 Ba Ba Pb 9_655 1_554 120.0 Ba Ba Pb 9_554 1_554 60.0 Ba Ba Pb 5_545 1_554 120.0 Ba Ba Pb 5_655 1_554 60.0 O Ba Ba 1_655 5 135.0 O Ba Ba . 5 45.0 Pb Ba Ba . 5 60.0 Pb Ba Ba 1_544 5 120.0 Ba Ba Ba 9_655 5 120.0 Ba Ba Ba 9_554 5 60.0 Ba Ba Ba 5_545 5 90.0 Ba Ba Ba 5_655 5 90.0 Pb Ba Ba 1_554 5 60.0 O Ba Ba 1_655 5_645 45.0 O Ba Ba . 5_645 135.0 Pb Ba Ba . 5_645 120.0 Pb Ba Ba 1_544 5_645 60.0 Ba Ba Ba 9_655 5_645 60.0 Ba Ba Ba 9_554 5_645 120.0 Ba Ba Ba 5_545 5_645 90.0 Ba Ba Ba 5_655 5_645 90.0 Pb Ba Ba 1_554 5_645 120.0 Ba Ba Ba 5 5_645 180.0 O Ba Ba 1_655 9_654 45.0 O Ba Ba . 9_654 135.0 Pb Ba Ba . 9_654 120.0 Pb Ba Ba 1_544 9_654 60.0 Ba Ba Ba 9_655 9_654 90.0 Ba Ba Ba 9_554 9_654 90.0 Ba Ba Ba 5_545 9_654 120.0 Ba Ba Ba 5_655 9_654 60.0 Pb Ba Ba 1_554 9_654 60.0 Ba Ba Ba 5 9_654 120.0 Ba Ba Ba 5_645 9_654 60.0 Ba O Ba 9 . 90.0 Ba O Ba 9 1_455 90.0 Ba O Ba . 1_455 180.0 Ba O Ba 9 5_545 90.0 Ba O Ba . 5_545 90.0 Ba O Ba 1_455 5_545 90.0 Ba O Ba 9 5 90.0 Ba O Ba . 5 90.0 Ba O Ba 1_455 5 90.0 Ba O Ba 5_545 5 180.0 Ba O Ba 9 9_554 180.0 Ba O Ba . 9_554 90.0 Ba O Ba 1_455 9_554 90.0 Ba O Ba 5_545 9_554 90.0 Ba O Ba 5 9_554 90.0 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance Pb Ba 9_665 3.882(5) Pb Ba . 3.882(5) Pb Ba 9 3.882(5) Pb Ba 5_656 3.882(5) Pb Ba 1_566 3.882(5) Pb Ba 5 3.882(5) Pb Ba 1_565 3.882(5) Pb Ba 5_556 3.882(5) Pb Ba 5_655 3.882(5) Pb Ba 1_556 3.882(5) Pb Ba 9_655 3.882(5) Pb Ba 9_565 3.882(5) Ba O 1_655 2.745(4) Ba O . 2.745(4) Ba Pb 1_544 3.882(5) Ba Ba 9_655 3.882(5) Ba Ba 9_554 3.882(5) Ba Ba 5_545 3.882(5) Ba Ba 5_655 3.882(5) Ba Pb 1_554 3.882(5) Ba Ba 5 3.882(5) Ba Ba 5_645 3.882(5) Ba Ba 9_654 3.882(5) O Ba 9 2.745(4) O Ba 1_455 2.745(4) O Ba 5_545 2.745(4) O Ba 5 2.745(4) O Ba 9_554 2.745(4)