#------------------------------------------------------------------------------ #$Date: 2025-02-09 19:01:10 +0100 (Sun, 09 Feb 2025) $ #$Revision: 297647 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/33/2023388.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023388 loop_ _publ_author_name 'Nuss, J\"urgen' 'M\"uhle, Claus' 'Hayama, Kyouhei' 'Abdolazimi, Vahideh' 'Takagi, Hidenori' _publ_section_title ; Tilting structures ininverseperovskites,M3TtO (M= Ca, Sr, Ba, Eu;Tt= Si, Ge, Sn, Pb) ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B Structural Science, Crystal Engineering and Materials' _journal_page_first 300 _journal_page_last 312 _journal_paper_doi 10.1107/S2052520615006150 _journal_volume 71 _journal_year 2015 _chemical_formula_moiety 'Sr3 Pb O' _chemical_formula_sum 'O Pb Sr3' _chemical_formula_weight 486.05 _space_group_crystal_system cubic _space_group_IT_number 221 _space_group_name_Hall '-P 4 2 3' _space_group_name_H-M_alt 'P m -3 m' _symmetry_cell_setting cubic _symmetry_space_group_name_H-M 'P m -3 m' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2013 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 1 _cell_length_a 5.151(3) _cell_length_b 5.151(3) _cell_length_c 5.151(3) _cell_measurement_reflns_used 1032 _cell_measurement_temperature 295(2) _cell_measurement_theta_max 36.87 _cell_measurement_theta_min 3.95 _cell_volume 136.67(14) _computing_cell_refinement 'Bruker Suite (Bruker AXS, 2013)' _computing_data_collection 'Bruker Suite (Bruker AXS, 2013)' _computing_data_reduction 'Bruker Suite (Bruker AXS, 2013)' _computing_structure_refinement 'SHELXL (Sheldrick, 2008)' _computing_structure_solution 'SHELXL (Sheldrick, 2008)' _diffrn_ambient_temperature 295(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'SMART APEX II, Bruker AXS' _diffrn_measurement_method \wscan _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0592 _diffrn_reflns_limit_h_max 8 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_k_max 6 _diffrn_reflns_limit_k_min -8 _diffrn_reflns_limit_l_max 8 _diffrn_reflns_limit_l_min -8 _diffrn_reflns_number 1691 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 36.977 _diffrn_reflns_theta_min 3.956 _exptl_absorpt_coefficient_mu 59.674 _exptl_absorpt_correction_T_max 0.111 _exptl_absorpt_correction_T_min 0.025 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; Sheldrick, G. M. (2012) SADABS - Bruker AXS area detector scaling and absorption, version 2012/1, University of G\"ottingen. Germany. ; _exptl_crystal_colour 'dark grey metallic' _exptl_crystal_density_diffrn 5.907 _exptl_crystal_description block _exptl_crystal_F_000 204 _exptl_crystal_size_max 0.120 _exptl_crystal_size_mid 0.120 _exptl_crystal_size_min 0.040 _refine_diff_density_max 1.743 _refine_diff_density_min -1.718 _refine_ls_extinction_coef 0.159(9) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method SHELXL _refine_ls_goodness_of_fit_ref 1.240 _refine_ls_matrix_type full _refine_ls_number_parameters 6 _refine_ls_number_reflns 101 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.240 _refine_ls_R_factor_all 0.0181 _refine_ls_R_factor_gt 0.0181 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0167P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0365 _refine_ls_wR_factor_ref 0.0365 _reflns_number_gt 101 _reflns_number_total 101 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file dk5032sup1.cif _cod_data_source_block Sr3PbO_295K _cod_original_cell_volume 136.6(2) _cod_database_code 2023388 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.053 _shelx_estimated_absorpt_t_max 0.199 _shelx_hkl_file ; 0 -1 0 954.184 66.852 1 0 -1 0 871.649 63.400 2 0 0 -1 928.931 61.667 2 0 0 1 953.027 65.888 1 1 0 0 1000.15 67.70 1 1 0 0 928.313 61.566 2 -1 -1 0 1971.09 115.40 2 -1 0 -1 1619.70 115.66 2 -1 0 1 1962.63 125.35 1 0 -1 -1 1754.88 117.33 2 0 -1 1 1655.39 124.61 1 0 -1 1 1830.22 115.36 2 0 1 1 1850.70 122.57 1 1 -1 0 2018.13 122.65 1 1 -1 0 1805.42 117.79 2 1 0 -1 1483.41 117.86 2 1 0 1 1603.52 123.34 1 1 1 0 1740.82 127.23 1 -1 -1 -1 9412.71 568.66 2 -1 -1 1 8837.02 607.99 1 1 -1 -1 8403.82 572.98 2 1 -1 1 8244.29 603.52 1 1 -1 1 9262.68 568.99 2 1 1 1 8769.84 604.26 1 0 -2 0 9568.00 545.47 2 0 0 -2 7263.26 542.09 2 0 0 2 7724.15 575.74 1 2 0 0 9180.18 580.55 1 -2 0 1 805.696 67.866 1 -1 -2 0 798.714 58.227 2 0 -1 -2 855.152 59.941 2 0 -1 2 932.914 64.812 1 0 1 -2 954.270 57.660 2 0 1 2 911.983 61.281 1 1 -2 0 862.816 62.643 2 1 2 0 827.007 66.372 1 2 0 -1 819.919 58.136 2 2 0 1 864.607 63.625 1 2 0 1 831.622 57.921 2 -2 -1 0 903.739 56.751 2 -1 0 -2 873.790 58.252 2 -1 0 2 876.297 62.984 1 0 -2 -1 777.342 60.490 2 0 -2 1 899.162 65.430 1 0 -2 1 908.190 58.836 2 0 2 1 882.948 62.125 1 1 0 -2 862.505 60.570 2 1 0 2 809.893 62.307 1 2 -1 0 830.307 63.249 1 2 -1 0 861.495 59.623 2 2 1 0 820.676 67.936 1 -2 -1 -1 1513.19 99.39 2 -2 1 1 1583.02 107.41 1 -1 -2 -1 1560.76 101.05 2 -1 -2 1 1281.26 110.03 1 -1 -1 -2 1524.13 100.69 2 -1 -1 2 1560.11 110.38 1 -1 1 -2 1654.99 100.41 2 -1 1 2 1511.71 105.44 1 1 -2 -1 1338.07 104.09 2 1 -2 1 1547.46 101.88 2 1 -1 -2 1227.00 103.33 2 1 -1 2 1448.52 107.61 1 1 1 -2 1596.92 100.10 2 1 1 2 1445.25 106.44 1 1 2 1 1576.81 108.90 1 2 -1 -1 1546.59 104.24 2 2 -1 1 1593.19 107.36 1 2 -1 1 1468.06 100.77 2 2 1 -1 1663.77 98.07 2 2 1 1 1489.21 109.33 1 -2 -2 0 9999.99 581.67 2 -2 0 -2 7586.75 582.12 2 -2 0 2 9341.79 620.91 1 0 -2 -2 9082.40 585.98 2 0 -2 2 9334.95 581.82 2 0 2 2 9200.26 617.30 1 2 -2 0 9348.88 617.80 1 2 -2 0 9272.47 587.16 2 2 0 -2 9772.43 586.95 2 2 0 2 7931.77 619.22 1 2 2 0 8430.23 625.46 1 -2 -2 -1 741.056 50.666 2 -2 -2 1 689.565 60.485 1 -2 -1 -2 752.437 51.245 2 -2 -1 2 782.928 61.506 1 -2 1 2 793.669 53.961 1 -1 -2 -2 749.671 52.628 2 -1 -2 2 762.491 60.961 1 -1 2 2 747.675 51.990 1 1 -2 -2 603.258 55.251 2 1 -2 2 706.635 51.234 2 1 2 -2 810.567 48.968 2 1 2 2 757.583 55.091 1 2 -2 -1 637.521 56.504 2 2 -2 1 726.895 54.570 1 2 -2 1 725.948 53.347 2 2 -1 -2 576.582 55.762 2 2 -1 2 780.457 56.328 1 2 -1 2 757.492 51.619 2 2 1 -2 778.148 49.425 2 2 1 2 782.168 56.521 1 2 2 1 750.019 58.754 1 -2 -2 -2 8086.97 516.94 2 -2 -2 2 6924.80 555.10 1 -2 2 2 8393.05 545.57 1 2 -2 -2 8034.04 524.06 2 2 -2 2 7773.52 550.39 1 2 -2 2 8463.33 518.37 2 2 2 2 8182.96 551.15 1 0 -3 0 828.153 63.007 1 0 -3 0 927.095 61.214 2 0 0 -3 828.807 59.317 2 0 0 3 865.600 63.168 1 3 0 0 818.425 68.800 1 3 0 0 843.110 58.133 2 -1 -3 0 952.726 76.724 1 -1 -3 0 900.560 70.655 2 0 -1 -3 1081.40 72.97 2 0 -1 3 1127.59 78.16 1 0 1 -3 1018.89 69.95 2 0 1 3 1059.32 74.26 1 1 -3 0 943.389 74.170 2 3 0 -1 1021.13 69.75 2 3 0 1 938.384 77.870 1 3 0 1 1083.31 70.20 2 0 3 1 995.660 75.288 1 1 0 -3 1044.95 73.79 2 1 0 3 1074.32 76.02 1 3 -1 0 1062.30 79.58 1 3 -1 0 1035.13 71.41 2 3 1 0 961.545 82.664 1 0 -3 1 1138.76 73.87 2 0 -3 -1 855.892 72.395 2 0 -3 1 1022.80 77.92 1 -1 0 -3 1023.09 70.70 2 -1 0 3 1163.84 76.68 1 -3 -1 0 1158.95 68.57 2 -1 -1 -3 7235.94 477.15 2 3 -1 1 7333.14 507.95 1 1 3 1 7484.92 508.56 1 3 -1 -1 6909.16 478.05 2 1 1 3 7450.88 505.75 1 3 -1 1 7316.56 477.01 2 3 1 -1 7435.69 473.81 2 3 1 1 6615.83 509.76 1 1 -1 -3 6918.71 481.17 2 1 -1 3 6934.63 507.31 1 1 1 -3 7480.95 477.46 2 -3 -1 -1 7331.06 474.90 2 -1 -3 -1 7592.42 478.38 2 -1 -3 1 8231.69 509.99 1 -1 -3 1 7266.11 476.93 2 1 -3 -1 8158.15 481.06 2 -1 -1 3 7732.16 509.55 1 -1 1 -3 7007.32 475.96 2 -1 1 3 7417.37 504.56 1 3 0 2 702.546 56.022 1 3 0 -2 735.909 49.973 2 0 -2 -3 709.034 53.671 2 0 -2 3 585.670 56.521 1 0 2 -3 732.394 48.757 2 0 2 3 692.360 51.310 1 2 -3 0 715.713 49.872 1 2 -3 0 676.942 55.413 2 2 3 0 665.296 59.304 1 -3 0 -2 796.874 50.269 2 -3 0 2 732.609 58.154 1 -2 -3 0 708.323 49.270 2 3 -2 0 723.561 55.262 1 3 -2 0 738.802 53.685 2 3 2 0 693.764 62.274 1 0 -3 2 605.658 56.918 1 0 -3 2 660.533 48.929 2 0 3 2 731.808 52.526 1 2 0 -3 537.216 54.891 2 2 0 3 738.753 55.061 1 0 -3 -2 622.845 53.086 2 -2 0 3 751.175 54.778 1 -3 -2 0 735.896 47.361 2 -2 0 -3 728.195 50.190 2 -1 2 3 921.326 65.237 1 3 -2 -1 911.506 69.706 2 -3 -1 -2 939.069 63.196 2 2 -3 1 869.271 67.299 1 2 -3 1 988.964 69.207 2 -2 1 -3 1016.28 64.89 2 1 -3 -2 788.719 67.729 2 3 -1 2 969.148 70.810 1 3 -1 2 912.599 64.362 2 3 1 -2 1002.85 60.87 2 2 1 3 929.958 69.169 1 -3 1 2 928.945 67.902 1 1 -2 3 958.813 71.851 1 1 2 -3 949.266 62.496 2 1 3 2 958.394 69.269 1 -2 -3 -1 945.551 63.965 2 -3 -2 1 825.833 75.851 1 -2 -1 3 1007.40 73.39 1 -1 -2 -3 930.214 65.654 2 -1 -3 2 794.857 72.284 1 -1 -3 2 876.343 60.740 2 2 -1 -3 721.062 69.887 2 3 2 1 901.036 73.514 1 -3 -2 1 969.448 60.198 2 -2 -3 1 844.566 71.434 1 -3 -2 -1 941.031 62.291 2 -3 2 1 915.429 65.818 1 -2 -1 -3 957.789 64.336 2 3 -1 -2 947.650 68.672 2 2 3 1 907.788 72.594 1 -2 1 3 884.726 66.889 1 -1 -3 -2 888.709 65.936 2 -1 -2 3 984.242 75.031 1 2 -3 -1 832.303 68.650 2 -1 3 2 953.246 65.123 1 -2 -3 1 885.035 61.600 2 1 -3 2 888.972 64.981 2 -1 2 -3 981.262 63.932 2 -3 -1 2 807.446 75.799 1 2 -1 3 946.229 70.279 1 2 1 -3 879.315 66.488 2 3 1 2 951.609 71.622 1 1 2 3 902.918 67.405 1 3 -2 1 946.187 69.149 1 3 -2 1 899.011 65.804 2 1 -2 -3 925.933 70.329 2 -3 -2 -2 616.159 43.176 2 -3 -2 2 585.741 56.295 1 -3 2 2 622.478 43.209 1 -3 2 2 623.391 43.210 1 -2 -3 -2 583.742 44.279 2 -2 -3 2 607.817 53.044 1 -2 -2 -3 625.476 44.855 2 -2 -2 3 544.300 53.578 1 -2 2 3 653.299 43.637 1 2 -3 -2 656.835 50.250 2 2 -3 2 610.931 49.640 1 2 -3 2 569.894 46.219 2 2 -2 -3 556.477 51.628 2 2 -2 3 588.089 50.044 1 2 -2 3 560.175 43.896 2 2 2 3 604.570 47.740 1 2 3 2 565.529 48.955 1 3 -2 -2 575.512 51.341 2 3 -2 2 611.010 49.090 1 3 -2 2 588.620 45.256 2 3 2 2 573.170 50.471 1 -3 -3 0 797.323 50.246 2 -3 0 -3 739.529 52.314 2 -3 0 3 676.662 56.943 1 0 -3 -3 674.516 56.562 2 0 3 -3 731.504 50.634 2 0 3 3 714.914 53.510 1 3 -3 0 734.378 59.013 2 3 0 -3 678.111 53.766 2 3 0 3 731.805 58.396 1 3 3 0 709.728 64.368 1 -3 -3 -1 5878.74 368.62 2 -3 -3 1 5609.76 399.63 1 -3 -1 -3 5589.28 369.66 2 -3 -1 3 5831.29 399.57 1 -3 1 -3 5678.64 370.61 2 -3 1 3 5970.25 391.89 1 -1 -3 -3 5940.13 373.01 2 -1 -3 3 5408.66 400.37 1 -1 3 3 6096.48 389.64 1 1 -3 -3 4855.94 375.21 2 1 -3 3 5987.30 399.55 1 1 -3 3 5861.35 370.12 2 1 3 3 5799.31 392.60 1 3 -3 -1 4942.59 376.32 2 3 -3 1 5699.75 392.56 1 3 -3 1 6014.78 375.52 2 3 -1 -3 5323.46 376.84 2 3 -1 3 5780.53 396.22 1 3 1 -3 5320.57 367.14 2 3 1 3 5533.71 395.49 1 3 3 1 6055.63 400.49 1 -3 -3 -2 583.588 43.112 2 -3 -3 2 594.069 53.512 1 -3 -2 -3 641.098 44.194 2 -3 -2 3 605.061 56.978 1 -3 2 3 486.682 42.580 1 -2 -3 -3 595.737 44.873 2 -2 -3 3 484.670 52.143 1 2 -3 -3 656.044 52.216 2 2 -3 3 634.105 52.355 1 2 -3 3 601.068 45.287 2 2 3 3 623.621 48.539 1 3 -3 -2 583.337 51.001 2 3 -3 2 572.232 48.571 1 3 -3 2 639.460 48.083 2 3 -2 -3 511.859 50.742 2 3 -2 3 628.948 51.322 1 3 -2 3 547.799 44.355 2 3 2 3 691.110 50.894 1 3 3 2 610.607 51.198 1 -3 -3 -3 4215.59 279.94 2 -3 -3 3 3928.32 305.82 1 3 -3 -3 4737.04 289.92 2 3 -3 3 4285.91 302.38 1 3 -3 3 4330.86 282.70 2 3 3 3 4122.23 300.51 1 0 0 -4 5595.55 367.62 2 0 0 4 5541.22 389.31 1 4 0 0 6419.01 400.71 1 4 0 0 5102.44 364.71 2 -1 -4 0 522.953 42.922 1 -1 -4 0 519.129 39.658 2 0 -1 -4 503.923 42.303 2 0 -1 4 539.261 44.958 1 0 1 -4 536.710 40.039 2 0 1 4 554.801 41.923 1 1 -4 0 553.587 42.866 1 1 -4 0 510.087 42.649 2 4 0 -1 526.880 38.495 2 4 0 1 496.168 47.401 1 4 0 1 560.583 39.466 2 4 1 0 473.669 51.168 1 0 -4 -1 511.268 41.759 2 0 -4 1 584.273 44.703 1 0 -4 1 535.440 43.114 2 1 0 -4 534.400 44.196 2 1 0 4 553.422 43.620 1 4 -1 0 454.771 47.785 1 4 -1 0 519.951 40.043 2 -4 -1 0 531.522 37.078 2 -1 0 -4 552.175 40.711 2 -1 0 4 546.816 43.539 1 0 -4 -1 550.647 41.157 1 4 1 -1 904.090 59.421 2 -1 -4 1 910.056 68.605 1 -1 -4 1 927.748 63.970 2 -1 -1 -4 911.129 64.343 2 -1 -1 4 914.766 70.083 1 -1 1 -4 894.336 62.979 2 -1 1 4 970.312 65.879 1 4 1 1 887.718 73.656 1 -4 -1 -1 909.672 60.745 2 1 4 1 888.718 69.486 1 4 -1 -1 814.899 62.977 2 4 -1 1 917.725 71.945 1 4 -1 1 906.703 63.332 2 1 -4 -1 878.973 65.169 2 1 -4 1 715.409 66.149 2 1 -1 -4 858.032 68.796 2 1 -1 4 897.540 69.274 1 1 1 -4 933.941 65.423 2 1 1 4 869.034 66.626 1 -1 -4 -1 811.177 64.275 2 -4 1 1 860.822 74.627 1 4 0 2 5418.42 396.83 1 4 0 -2 4869.06 367.12 2 4 -2 0 5522.55 371.61 2 4 2 0 5631.33 404.04 1 0 -2 4 5850.14 397.59 1 0 2 -4 5478.43 368.02 2 0 2 4 5773.67 390.01 1 2 -4 0 5739.40 374.52 2 -4 0 2 5655.30 399.74 1 -2 -4 0 5833.75 395.28 1 -2 -4 0 5453.53 367.93 2 0 -2 -4 6180.43 374.45 2 -4 -2 0 6094.28 365.92 2 0 4 2 6250.18 391.96 1 0 -4 -2 5126.40 372.25 2 0 -4 2 6473.30 397.70 1 0 -4 2 6571.55 371.02 2 2 0 4 4940.37 392.75 1 -4 0 -2 5446.26 368.19 2 -2 0 -4 5174.79 369.06 2 -2 0 4 5493.90 392.67 1 4 -1 2 495.976 42.505 1 -2 -1 4 481.376 41.498 1 -2 1 -4 465.885 35.604 2 -4 -2 1 363.077 45.133 1 -2 -4 -1 421.330 35.633 2 1 -4 -2 442.619 38.497 2 -1 2 4 425.337 34.234 1 2 -4 1 388.044 35.847 1 1 -2 4 437.804 40.910 1 1 2 -4 473.918 35.561 2 -4 1 2 407.623 37.811 1 2 -1 -4 328.135 42.530 2 2 1 4 455.558 38.498 1 2 -4 1 493.140 41.932 2 -1 -4 2 466.310 40.795 1 4 -2 -1 463.308 39.217 2 -4 -1 -2 443.531 33.534 2 4 -1 2 475.523 35.889 2 4 1 -2 455.361 30.772 2 -1 -2 -4 443.887 36.957 2 4 2 1 447.675 44.235 1 1 4 2 440.652 38.284 1 2 -4 -1 464.363 38.855 2 1 -4 2 474.611 39.432 2 2 1 -4 452.821 42.450 2 -4 -2 -1 442.853 32.581 2 4 -1 -2 452.985 36.771 2 4 1 2 465.159 43.028 1 4 -2 1 436.187 36.498 2 -4 -1 2 341.296 48.217 1 -4 2 1 471.493 37.587 1 -2 -4 1 483.459 39.879 1 4 -2 1 420.381 39.979 1 -2 1 4 490.254 36.378 1 -1 -4 -2 400.894 37.159 2 -1 -2 4 483.816 44.384 1 -1 2 -4 470.037 35.015 2 2 4 1 372.840 40.333 1 1 -2 -4 431.759 41.818 2 -2 -1 -4 472.777 36.319 2 2 -1 4 447.144 39.765 1 1 2 4 424.277 36.013 1 -4 -2 -2 5027.08 335.69 2 2 4 2 4991.81 361.25 1 4 -2 -2 5292.55 344.71 2 -2 -4 2 5557.42 362.96 1 -2 -2 -4 5172.71 338.70 2 -2 -2 4 5483.65 367.02 1 -2 2 -4 5279.07 338.35 2 -2 2 4 5356.13 354.96 1 2 -4 -2 5482.60 342.32 2 2 -4 2 4533.02 361.11 1 2 -4 2 5855.37 344.94 2 2 -2 -4 4364.49 346.50 2 2 -2 4 4965.32 362.55 1 2 2 4 5225.76 359.12 1 4 -2 2 5180.03 362.49 1 4 -2 2 5177.08 339.04 2 4 2 2 4956.18 364.30 1 -4 -2 2 4655.58 369.88 1 -2 -4 -2 5459.54 339.46 2 -3 0 4 397.712 37.205 1 3 0 -4 411.757 38.967 2 3 0 4 434.668 39.516 1 4 -3 0 448.438 41.270 2 4 3 0 397.601 45.930 1 0 -3 4 388.451 42.973 1 0 3 -4 426.796 32.760 2 0 3 4 427.225 33.858 1 3 -4 0 361.657 39.078 2 4 0 -3 412.702 32.682 2 4 0 3 501.473 42.894 1 -3 -4 0 418.159 41.247 1 -3 0 -4 429.102 34.824 2 0 4 3 435.510 34.910 1 -4 0 -3 451.548 34.635 2 -4 0 3 397.144 38.809 1 0 -4 3 413.098 32.646 2 0 -3 -4 409.910 39.063 2 0 -4 -3 425.230 39.781 2 -4 -1 -3 579.678 45.067 2 1 4 3 590.841 48.752 1 -1 3 4 617.047 45.432 1 -4 1 3 622.165 48.188 1 1 -3 4 672.916 56.470 1 -3 -1 4 602.916 53.390 1 1 -4 -3 522.784 50.796 2 3 -4 1 575.848 53.169 2 4 -1 3 675.824 55.066 1 3 1 4 672.920 52.569 1 4 -3 -1 528.871 52.730 2 -1 -4 3 606.923 54.854 1 4 3 1 616.074 56.951 1 -1 -3 -4 629.410 49.382 2 -4 -3 1 614.923 57.595 1 -3 1 -4 651.324 47.436 2 -3 -4 -1 635.248 45.904 2 3 -1 -4 465.640 52.816 2 3 4 1 587.046 54.924 1 -1 -4 -3 552.789 48.656 2 1 3 4 573.180 47.582 1 -3 -1 -4 648.453 46.849 2 -1 3 -4 618.069 46.003 2 1 -4 3 608.724 47.082 2 -3 1 4 630.310 48.173 1 -4 -3 -1 653.284 43.951 2 4 -1 -3 577.313 49.019 2 4 1 3 596.283 53.931 1 4 -3 1 561.263 49.924 2 -3 -4 1 599.547 52.386 1 3 -4 -1 606.491 51.899 2 -1 -3 4 579.947 57.372 1 -4 -1 3 654.895 58.346 1 -4 1 -3 631.002 46.949 2 1 -3 -4 634.512 54.869 2 3 -1 4 599.097 53.260 1 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2532.05 180.74 1 5 -3 3 2592.17 170.59 2 3 -5 3 2562.09 175.85 2 5 -3 3 2280.45 182.84 1 -3 -3 -5 2548.39 168.71 2 -5 0 -4 309.213 28.593 2 -4 0 5 310.114 31.220 1 0 -5 -4 246.412 33.684 2 -4 -5 0 312.437 34.816 1 -5 0 4 308.759 31.521 1 0 -4 5 207.226 35.989 1 4 -5 0 304.715 36.244 2 5 0 4 300.406 36.564 1 0 -5 4 181.575 31.769 1 4 0 5 298.348 34.481 1 5 -4 0 330.857 36.971 2 -5 -4 0 248.978 35.978 1 0 -4 -5 298.002 36.805 2 -4 0 -5 299.824 29.380 2 -4 1 -5 318.406 31.718 2 1 -4 5 264.588 39.538 1 -1 -4 -5 307.028 34.378 2 -5 -1 -4 335.628 30.279 2 -4 -5 -1 335.415 37.403 1 5 -1 4 363.392 41.607 1 -4 -1 5 344.888 37.205 1 4 -5 1 267.655 37.623 2 5 4 1 367.152 42.150 1 -5 -4 1 286.428 36.762 1 4 1 5 345.914 36.967 1 5 -4 -1 371.049 43.045 2 1 -5 -4 319.594 36.859 2 -1 -5 4 302.917 36.744 1 -1 -5 -4 296.100 33.639 2 -5 1 -4 370.098 32.344 2 1 -5 4 374.959 39.304 1 4 -1 5 334.724 39.104 1 -4 -1 -5 370.842 32.216 2 5 1 4 343.317 39.671 1 5 -4 1 321.114 38.573 2 -5 -1 4 336.192 39.021 1 4 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1 5 -4 -3 239.536 35.800 2 -5 -3 -4 240.896 25.549 2 -4 -3 5 234.504 40.562 1 -4 3 -5 234.311 28.178 2 -4 -5 -3 246.390 27.083 2 -5 -4 3 177.462 33.465 1 -3 -4 -5 209.978 27.927 2 4 3 5 241.103 31.003 1 3 5 4 256.525 30.170 1 4 -3 -5 323.948 43.349 2 3 -5 -4 295.592 33.673 2 -3 -4 5 217.043 37.217 1 -5 -4 -3 257.879 25.620 2 5 3 4 264.060 35.405 1 -4 -3 -5 260.410 27.348 2 -5 -3 4 257.683 43.829 1 -5 3 -4 236.679 29.551 2 -3 -5 -4 230.377 27.791 2 -4 -5 3 266.182 32.201 1 5 -3 -4 170.071 34.317 2 3 -5 4 226.122 34.515 2 -3 4 -5 251.278 30.117 2 3 -4 -5 282.467 37.298 2 4 -3 5 271.984 40.848 1 3 4 5 240.357 29.590 1 4 -5 -3 270.483 33.600 2 5 -4 3 291.908 35.497 2 4 5 3 264.623 33.719 1 -5 -4 -4 207.525 25.025 2 -5 -4 4 192.509 35.973 1 -5 4 -4 186.969 27.707 2 -4 -5 -4 200.287 25.526 2 -4 -5 4 190.335 29.654 1 -4 -4 -5 158.308 23.874 2 -4 -4 5 192.099 36.769 1 -4 4 -5 176.434 28.875 2 4 -5 -4 176.592 30.251 2 4 -5 4 113.123 31.473 2 4 -4 -5 183.076 32.682 2 4 -4 5 166.849 36.517 1 4 4 5 214.893 29.638 1 4 5 4 181.269 27.937 1 5 -4 -4 171.937 32.820 2 5 4 4 163.179 29.209 1 -5 -5 0 215.311 32.307 1 -5 0 -5 230.138 27.596 2 -5 0 5 209.803 26.739 1 0 -5 -5 171.035 30.192 2 0 -5 5 175.000 31.010 1 5 -5 0 192.396 31.266 2 5 0 5 260.507 36.934 1 -5 -5 -1 1933.39 142.62 1 -5 -5 1 1967.89 140.34 1 -5 -1 -5 1936.56 128.51 2 -5 -1 5 1739.36 138.58 1 -5 1 -5 1788.87 128.50 2 -1 -5 -5 1653.55 131.26 2 1 -5 -5 1856.52 135.05 2 5 -5 -1 1739.99 133.80 2 5 -5 1 1594.66 133.62 2 5 -1 5 1896.15 145.74 1 5 1 5 1953.73 144.33 1 -5 -5 2 169.424 27.450 1 -5 -2 -5 164.726 23.517 2 -5 -2 5 201.137 37.239 1 -5 2 -5 200.144 26.586 2 -2 -5 -5 154.592 26.237 2 -2 -5 5 104.630 27.108 1 2 -5 -5 241.294 32.327 2 2 -5 5 204.987 33.418 1 5 -5 -2 201.188 30.929 2 5 -5 2 223.109 34.250 2 5 -2 5 224.195 37.697 1 5 2 5 241.707 34.989 1 5 5 2 236.861 34.553 1 -5 -5 3 1409.75 112.76 1 -5 -3 -5 1361.41 101.11 2 -5 -3 5 1256.23 121.15 1 -5 3 -5 1344.58 104.12 2 -3 -5 -5 1387.39 103.95 2 -3 -5 5 1597.19 116.55 1 -3 5 -5 1211.21 105.09 2 3 5 5 1500.61 110.84 1 5 -5 -3 1632.00 110.46 2 5 -5 3 1454.03 111.16 2 5 -3 5 1380.29 121.61 1 5 3 5 1517.52 115.36 1 5 5 3 1397.72 113.56 1 -5 -5 4 202.413 32.124 1 -5 -4 -5 155.305 23.593 2 -5 -4 5 171.299 38.169 1 -5 4 -5 169.492 29.417 2 -5 5 -4 159.499 30.008 2 -4 -5 -5 139.533 24.281 2 -4 -5 5 176.502 30.719 1 -4 5 -5 141.482 29.692 2 4 -5 -5 118.818 29.672 2 4 5 5 136.969 26.402 1 5 -5 -4 180.069 31.401 2 5 -4 -5 152.656 34.689 2 5 4 5 166.320 29.689 1 5 5 4 145.724 28.147 1 -5 -5 -5 791.951 64.629 2 -5 5 -5 785.130 72.522 2 5 5 5 813.568 72.358 1 0 -6 0 3759.14 217.99 2 0 0 -6 3231.47 221.70 2 0 0 6 3061.35 231.65 1 6 0 0 2937.13 244.36 1 -6 0 -1 236.734 22.439 2 -6 0 1 207.802 37.490 1 -1 -6 0 232.609 23.285 1 0 -1 -6 296.252 30.274 2 0 -1 6 255.421 28.731 1 0 1 -6 225.480 26.742 2 0 1 6 238.157 25.097 1 1 -6 0 255.013 24.652 2 6 0 -1 235.843 21.273 2 6 0 1 236.311 37.043 1 0 -6 1 260.470 24.692 2 1 0 -6 263.274 33.400 2 1 0 6 230.121 27.311 1 6 -1 0 282.025 39.972 1 6 -1 0 210.185 23.058 2 6 1 0 193.883 37.356 1 -1 0 6 272.685 26.819 1 0 -6 -1 205.494 23.314 2 -1 0 -6 248.654 26.639 2 -6 -1 0 238.221 20.902 2 1 1 6 485.864 42.868 1 1 -1 6 478.108 45.150 1 6 -1 1 469.472 38.983 2 1 -6 -1 461.787 40.007 2 -6 -1 -1 468.995 36.668 2 -6 -1 1 455.802 54.826 1 -6 1 1 541.557 52.070 1 -1 -6 -1 511.962 39.536 2 -1 -6 1 568.835 42.198 1 6 1 1 432.338 51.929 1 -1 -1 -6 505.965 44.014 2 -1 -1 6 497.375 44.957 1 -1 1 -6 508.415 42.718 2 -1 1 6 477.095 41.107 1 1 -6 1 525.537 42.074 2 1 -1 -6 462.681 48.292 2 6 -1 1 403.583 49.876 1 6 -1 -1 479.051 39.112 2 0 -2 -6 3052.38 206.08 2 6 2 0 3191.60 229.05 1 2 0 6 2927.59 214.04 1 6 -2 0 2967.13 199.95 2 -2 0 -6 2764.89 200.43 2 -2 0 6 2783.53 210.82 1 0 -6 -2 3166.70 200.61 2 2 0 -6 2579.30 211.22 2 -6 0 -2 2926.74 197.27 2 0 -2 6 2853.49 216.03 1 0 2 6 2982.96 209.44 1 2 -6 0 3212.53 200.53 2 6 0 2 2821.13 222.04 1 -2 -6 0 3311.89 211.70 1 -6 0 2 2888.15 220.13 1 1 -6 -2 226.133 24.409 2 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2746.91 181.68 2 2 -2 -6 2347.84 191.10 2 -2 2 -6 2546.47 180.05 2 2 -6 2 2985.63 184.54 2 6 -2 2 2475.82 178.25 2 2 -6 -2 2793.55 179.78 2 2 -2 6 2853.59 196.47 1 -3 0 6 274.044 27.098 1 3 0 6 189.483 28.256 1 0 -6 -3 205.567 26.628 2 -3 -6 0 216.467 25.425 1 -6 0 -3 179.598 22.065 2 0 -3 6 202.173 32.959 1 6 0 3 179.002 34.913 1 -6 -3 0 188.849 31.980 1 -3 0 -6 234.242 27.002 2 0 3 6 184.614 21.474 1 0 -3 -6 227.252 32.456 2 -6 0 3 109.735 24.868 1 6 -3 0 185.573 28.149 2 3 -6 0 213.923 26.315 2 -6 -3 1 415.290 45.687 1 6 -3 -1 375.874 40.452 2 -1 -3 -6 344.727 39.410 2 -3 1 -6 361.094 36.538 2 1 -6 -3 356.017 36.434 2 -3 -1 6 339.973 38.055 1 -3 -6 -1 363.781 37.823 1 6 3 1 356.571 48.694 1 -6 -1 -3 397.028 32.745 2 3 1 6 371.550 38.716 1 -1 -6 3 375.728 36.938 1 1 -3 6 385.489 45.483 1 6 -1 3 364.793 45.932 1 3 -6 1 357.659 37.195 2 -6 -1 3 254.771 44.042 1 1 -3 -6 329.335 44.829 2 6 -3 1 370.634 37.715 2 -3 -6 1 357.429 35.827 1 -1 -6 -3 379.665 37.302 2 -6 1 -3 409.879 34.874 2 1 3 6 340.003 34.158 1 -1 -3 6 376.857 45.302 1 -3 1 6 426.173 34.768 1 3 -1 6 403.294 42.989 1 6 1 3 450.475 49.523 1 -3 -1 -6 393.014 37.185 2 3 -6 -1 419.116 36.576 2 3 -2 -6 227.739 39.442 2 -6 -3 2 251.611 36.627 1 -3 2 -6 200.918 26.534 2 2 -3 6 232.418 35.411 1 -3 -2 6 139.018 28.914 1 3 2 6 177.153 25.520 1 2 -6 -3 202.764 25.480 2 6 -3 -2 185.004 30.097 2 6 -2 3 141.180 31.088 1 6 3 2 181.256 33.381 1 -2 -3 -6 211.734 28.314 2 -2 -6 3 121.466 21.019 1 3 -6 2 155.615 27.120 2 -6 -2 -3 180.783 19.885 2 -3 -6 -2 198.912 27.293 1 -2 -6 -3 154.166 24.699 2 -2 -3 6 100.393 29.893 1 6 -3 2 200.066 26.512 2 -3 -2 -6 143.796 23.650 2 2 -6 3 171.410 27.455 2 6 2 3 178.129 33.290 1 2 -3 -6 180.005 34.134 2 -3 -6 2 185.045 24.250 1 2 3 6 190.708 23.639 1 -6 2 -3 186.985 22.886 2 -2 3 -6 166.442 24.995 2 3 -6 -2 211.566 25.377 2 3 -2 6 169.416 31.586 1 6 -2 -3 168.024 25.190 2 -6 -2 3 152.792 35.550 1 3 -6 -3 297.501 32.065 2 -3 3 -6 306.278 32.886 2 -6 -3 3 234.292 41.778 1 -3 -6 -3 216.575 30.674 2 3 6 3 274.247 32.880 1 6 -3 -3 341.778 39.407 2 3 -3 -6 329.262 44.341 2 3 -6 3 246.128 35.773 2 -6 -3 -3 299.877 26.899 2 3 3 6 263.996 30.833 1 6 3 3 283.490 40.763 1 -3 -6 3 264.664 30.198 1 -3 -3 -6 270.885 31.152 2 -3 -3 6 220.116 40.507 1 6 -3 3 189.811 29.602 2 3 -3 6 298.135 43.053 1 0 -6 -4 2053.30 145.20 2 6 0 4 1993.08 162.47 1 -4 0 6 2033.16 150.34 1 -6 0 -4 2023.94 141.04 2 -4 0 -6 1964.56 143.20 2 -4 -6 0 2240.29 153.35 1 0 -4 -6 1939.30 149.04 2 0 -4 6 1999.75 160.29 1 6 -4 0 2098.77 150.34 2 4 0 6 1926.05 155.75 1 4 -6 0 2107.62 145.09 2 -6 -4 0 2126.19 159.17 1 4 1 6 165.376 28.276 1 4 -6 1 145.678 25.392 2 -1 -6 4 114.330 22.694 1 -6 -1 -4 170.293 21.762 2 6 -1 4 161.685 33.622 1 6 4 1 162.262 33.495 1 -4 -1 6 97.5623 23.0781 1 -4 1 -6 174.531 25.698 2 1 -6 -4 151.290 24.903 2 -4 -6 -1 164.690 27.185 1 6 -4 -1 104.737 28.490 2 1 -4 6 130.274 29.761 1 -1 -4 -6 176.180 28.904 2 -6 -4 1 147.597 28.082 1 -1 -6 -4 133.789 24.340 2 -4 -6 1 115.663 22.409 1 4 -6 -1 170.042 24.261 2 4 -1 6 161.913 30.669 1 -6 -1 4 155.668 28.411 1 -6 1 -4 166.920 22.072 2 1 -6 4 83.2673 21.0326 1 -4 -1 -6 184.303 25.706 2 1 -4 -6 130.002 29.148 2 6 -4 1 169.531 29.399 2 -1 -4 6 110.813 29.104 1 6 1 4 200.705 35.886 1 -4 -6 -2 1821.93 134.59 1 2 -4 6 1770.40 139.99 1 6 -2 4 1627.18 140.77 1 -4 -2 6 1546.86 136.25 1 2 -6 -4 2011.51 127.09 2 6 -4 -2 1688.99 131.68 2 -6 -4 2 1860.59 138.09 1 -2 -4 -6 1889.58 127.51 2 -2 -6 4 1533.72 129.39 1 -4 2 -6 1584.00 123.79 2 4 -6 2 1790.61 128.21 2 6 4 2 1783.50 140.02 1 -6 -2 -4 1668.40 119.63 2 4 2 6 1787.23 134.40 1 6 -4 2 1849.90 128.64 2 2 4 6 1779.92 130.21 1 -2 -6 -4 1479.96 122.90 2 6 2 4 1771.03 140.28 1 4 -2 6 1745.64 140.15 1 -6 2 -4 1665.52 121.91 2 -4 -2 -6 1737.48 123.73 2 2 -4 -6 2166.61 137.10 2 -6 -2 4 1412.94 139.39 1 -4 -6 2 1734.10 130.58 1 4 -6 -2 1807.36 124.74 2 -6 -3 -4 124.795 19.376 2 -4 3 -6 125.001 24.874 2 -6 -4 3 94.0394 26.5868 1 4 -6 3 105.071 27.153 2 4 -3 -6 172.647 36.633 2 3 -6 -4 135.742 24.105 2 4 3 6 143.636 26.334 1 6 -4 -3 98.2820 27.9982 2 -4 -3 6 88.8388 31.6571 1 6 4 3 122.576 28.130 1 3 -4 6 145.149 33.352 1 -3 -6 4 107.981 21.842 1 -3 -4 -6 135.517 24.320 2 6 -3 -4 109.132 27.210 2 3 4 6 117.365 22.751 1 -6 3 -4 97.8161 21.2482 2 -3 4 -6 92.8401 23.5407 2 3 -4 -6 184.719 33.480 2 4 -6 -3 121.222 23.781 2 6 -4 3 101.393 24.019 2 4 6 3 135.411 25.837 1 -4 -6 3 145.234 22.872 1 6 3 4 139.675 29.459 1 -3 -4 6 49.0370 25.9757 1 3 -6 4 30.5919 23.8877 2 4 -3 6 165.929 35.503 1 -3 -6 -4 107.103 21.514 2 -6 -3 4 102.041 32.177 1 -4 -3 -6 154.468 24.012 2 4 -4 6 1243.68 108.05 1 -4 -6 4 1138.31 92.12 1 -4 4 -6 1102.93 90.94 2 6 4 4 1173.34 98.19 1 -4 -4 -6 1123.68 86.83 2 6 -4 -4 1029.19 95.12 2 4 4 6 1127.07 93.57 1 4 6 4 1191.37 95.05 1 -6 -4 4 1195.04 102.02 1 -6 4 -4 1156.30 89.12 2 5 0 6 157.792 33.247 1 -6 0 -5 174.786 25.304 2 -6 -5 0 207.998 31.176 1 -5 0 -6 167.537 26.723 2 0 -6 -5 171.295 27.953 2 -5 -6 0 195.563 28.775 1 0 -5 -6 170.518 31.184 2 0 -5 6 141.000 28.748 1 5 -6 0 163.119 27.473 2 0 -6 5 101.355 24.245 1 6 0 5 192.593 36.774 1 6 -5 0 148.804 31.513 2 1 -5 6 196.016 33.347 1 -5 -1 6 117.085 27.480 1 -5 1 -6 262.877 31.774 2 -6 -1 -5 235.750 27.628 2 6 -5 -1 242.168 36.401 2 5 -6 1 258.590 33.570 2 -6 -5 1 263.182 35.217 1 6 -1 5 233.450 42.195 1 -1 -5 -6 170.209 29.855 2 5 1 6 222.011 35.632 1 -5 -6 -1 204.013 32.749 1 1 -6 -5 259.523 33.301 2 -6 -5 -1 242.340 37.158 1 -5 -6 1 146.708 28.090 1 -6 1 -5 228.172 27.000 2 -1 -5 6 166.194 31.841 1 -6 -1 5 235.901 32.952 1 1 -6 5 265.372 31.642 1 6 1 5 303.393 43.110 1 5 -1 6 200.421 37.931 1 6 -5 1 244.807 36.710 2 1 -5 -6 202.902 33.680 2 -5 -1 -6 255.835 31.291 2 5 -6 -1 261.586 32.353 2 -1 -6 -5 159.145 27.695 2 5 2 6 179.745 32.505 1 5 -6 2 169.098 29.236 2 6 -2 5 133.588 35.188 1 -2 -6 5 80.3634 21.7309 1 -6 -2 -5 129.221 21.642 2 -6 -5 2 115.759 25.524 1 -2 -5 -6 117.949 25.418 2 -5 -2 6 93.4267 28.7294 1 -5 2 -6 164.284 25.154 2 2 -5 6 166.349 31.160 1 6 5 2 146.252 29.963 1 -5 -6 -2 123.884 27.869 1 6 -5 -2 128.681 29.276 2 2 -6 -5 113.763 25.083 2 5 -2 6 146.823 34.806 1 2 -5 -6 138.405 29.527 2 -2 -6 -5 96.7650 22.9165 2 5 -6 -2 144.933 25.710 2 6 -5 2 136.368 30.547 2 -2 -5 6 67.8644 23.2300 1 -5 -2 -6 110.622 23.086 2 -5 -6 2 124.828 23.322 1 -6 -2 5 147.091 33.275 1 -6 2 -5 182.667 25.453 2 6 2 5 141.178 32.702 1 3 -6 -5 149.005 28.546 2 -3 -6 5 124.911 24.868 1 5 -6 3 101.527 28.392 2 -6 -5 3 177.986 30.548 1 6 5 3 170.814 32.041 1 3 -5 6 256.448 39.653 1 -5 3 -6 172.059 28.858 2 -6 -3 -5 137.744 22.057 2 6 -5 -3 197.133 33.767 2 5 3 6 147.039 30.903 1 -5 -3 6 181.168 40.263 1 -3 -5 -6 190.278 28.131 2 -3 -5 6 92.5447 27.1305 1 -5 -3 -6 128.187 23.584 2 -5 -6 3 204.274 28.728 1 5 -6 -3 155.810 26.473 2 -3 -6 -5 103.167 24.502 2 5 6 3 200.526 30.890 1 6 3 5 185.609 34.121 1 5 -3 6 172.169 41.202 1 -6 3 -5 165.038 27.241 2 -6 -3 5 157.423 38.809 1 6 -5 3 149.466 32.998 2 3 -5 -6 145.784 31.408 2 -6 -6 0 1185.86 89.18 1 -6 0 -6 1023.37 81.92 2 0 -6 -6 1012.99 84.90 2 6 -6 0 950.803 83.896 2 6 0 6 1086.42 99.41 1 -6 -6 -1 110.016 26.364 1 -6 -6 1 52.9258 19.0730 1 -6 -1 -6 93.0179 23.0699 2 -6 1 -6 69.4344 21.2247 2 -1 -6 -6 59.4040 21.2070 2 -1 -6 6 74.1074 20.7754 1 1 -6 6 91.2027 23.4128 1 6 -6 1 91.4511 24.9360 2 6 -1 6 106.644 34.697 1 6 1 6 129.525 33.092 1 6 -2 6 936.239 95.180 1 -7 0 0 347.708 28.436 2 0 0 -7 298.546 35.579 2 0 0 7 291.188 32.611 1 7 0 0 269.802 46.930 1 -7 0 -1 202.438 22.032 2 -7 0 1 236.626 39.189 1 0 -1 -7 183.189 30.865 2 0 -1 7 210.497 28.742 1 0 1 7 190.361 24.491 1 1 -7 0 214.777 22.900 2 7 0 1 234.893 40.865 1 1 0 -7 185.922 33.064 2 1 0 7 229.177 27.871 1 7 -1 0 206.241 23.087 2 7 1 0 167.508 38.979 1 -1 0 7 219.758 26.528 1 0 -7 -1 230.848 23.802 2 -1 0 -7 175.327 27.889 2 7 1 1 1962.42 157.75 1 7 -1 -1 1873.66 130.24 2 1 -1 -7 1798.48 142.09 2 -7 -1 1 1822.59 153.52 1 -7 1 -1 1921.18 130.80 2 -1 -1 -7 1947.08 137.93 2 -1 -1 7 1916.02 143.29 1 -1 1 7 1884.14 139.16 1 1 1 7 2017.15 141.91 1 -1 1 -7 1821.40 135.88 2 1 -7 -1 2021.12 131.81 2 1 -1 7 1903.58 144.06 1 -7 0 -2 302.504 26.868 2 0 -2 -7 282.959 37.814 2 0 2 7 247.638 27.330 1 7 0 2 285.300 44.230 1 -2 0 -7 283.928 32.434 2 0 -2 7 283.558 36.409 1 -7 -2 0 223.277 39.277 1 -2 0 7 266.548 30.210 1 0 -7 -2 261.175 28.009 2 2 0 7 257.450 31.791 1 7 -2 0 268.844 28.820 2 2 -7 0 227.855 26.621 2 1 -7 -2 213.606 24.670 2 7 -2 -1 211.297 25.627 2 2 1 7 210.947 27.668 1 -7 -1 -2 199.153 21.218 2 2 -7 1 167.663 23.946 2 -7 -2 1 223.459 38.265 1 7 -1 2 211.954 38.338 1 -2 -1 7 236.015 29.407 1 -2 1 -7 195.873 28.512 2 7 2 1 229.631 41.232 1 -1 -2 -7 186.698 29.540 2 1 -2 7 202.254 31.268 1 -7 -1 2 169.846 36.411 1 -1 -2 7 187.099 30.144 1 1 -2 -7 176.527 33.855 2 -7 1 -2 218.337 23.629 2 1 2 7 177.984 24.369 1 2 -7 -1 210.725 23.994 2 -1 -7 -2 156.485 22.999 2 -2 -1 -7 152.392 26.910 2 2 -1 7 228.176 32.126 1 7 -2 1 172.223 24.212 2 -2 1 7 214.909 24.161 1 7 1 2 192.906 38.249 1 -7 -2 2 233.224 39.937 1 -2 -7 2 190.901 24.591 1 -2 -2 -7 257.564 32.412 2 2 -2 7 261.698 36.718 1 2 2 7 220.983 28.179 1 7 -2 -2 226.430 28.193 2 -7 2 -2 215.270 25.673 2 2 -7 -2 253.620 26.512 2 2 -2 -7 252.036 41.313 2 7 2 2 270.144 43.575 1 -2 -2 7 205.849 33.290 1 -2 2 -7 254.269 32.095 2 3 0 7 164.618 28.938 1 7 0 3 218.595 40.480 1 -3 -7 0 128.646 22.150 1 0 -3 -7 168.977 31.935 2 0 -3 7 186.528 34.442 1 3 -7 0 165.856 22.665 2 -3 0 -7 183.313 28.039 2 -7 0 -3 189.946 22.853 2 -3 0 7 184.111 24.846 1 7 -3 0 159.157 25.869 2 0 -7 -3 166.149 24.136 2 -7 -3 0 169.040 34.109 1 3 1 7 1515.96 116.70 1 7 -1 3 1438.65 126.84 1 1 -3 7 1609.21 123.69 1 7 -3 -1 1549.33 110.98 2 -7 -1 -3 1429.93 103.76 2 -1 -3 -7 1446.92 113.41 2 -7 -3 1 1593.34 122.81 1 7 3 1 1515.80 128.88 1 -3 -1 7 1402.93 114.68 1 -3 1 -7 1472.38 109.97 2 1 -7 -3 1535.91 107.34 2 1 -3 -7 1397.07 116.76 2 -3 -1 -7 1393.68 109.41 2 7 -3 1 1514.05 109.31 2 -3 -7 1 1536.26 112.16 1 -7 1 -3 1566.97 105.92 2 -1 -7 -3 1464.10 106.56 2 -1 -3 7 1573.61 123.52 1 3 -1 7 1596.83 120.77 1 1 3 7 1396.45 111.22 1 7 1 3 1412.36 127.04 1 3 -7 -1 1416.42 105.36 2 -7 -3 2 141.791 31.855 1 -2 -3 -7 183.322 29.489 2 -7 -2 -3 141.358 19.564 2 7 -3 -2 191.066 29.095 2 3 2 7 188.777 27.135 1 7 3 2 153.850 35.493 1 2 -7 -3 153.260 24.111 2 -3 -2 7 109.530 27.808 1 -3 2 -7 126.927 26.183 2 -2 -7 3 129.111 21.513 1 2 -3 7 192.357 34.682 1 3 -7 2 176.223 25.325 2 3 -2 7 211.563 35.256 1 -3 -2 -7 190.028 27.660 2 -2 -3 7 130.036 31.942 1 3 -7 -2 151.280 23.524 2 7 -3 2 123.627 22.941 2 7 2 3 143.638 35.088 1 -3 -7 2 168.197 22.821 1 2 3 7 157.080 23.917 1 -7 2 -3 149.370 22.575 2 -7 -2 3 91.9272 30.0467 1 2 -3 -7 182.400 35.404 2 -3 -3 -7 1125.59 90.00 2 3 -7 -3 1255.16 88.26 2 -3 -7 3 1158.32 90.71 1 7 -3 -3 1129.27 91.65 2 7 3 3 1191.32 104.98 1 3 -3 7 1294.12 105.94 1 3 -3 -7 1538.02 104.93 2 -7 3 -3 1046.20 86.25 2 3 3 7 1134.66 93.55 1 -3 3 -7 996.445 89.381 2 -7 0 -4 217.588 25.035 2 -4 0 -7 182.025 29.370 2 0 -4 7 166.394 34.837 1 -4 -7 0 158.078 25.068 1 4 -7 0 173.977 25.595 2 7 0 4 243.129 44.179 1 4 0 7 211.699 34.337 1 7 -4 0 238.848 34.082 2 -7 -4 0 196.526 33.921 1 0 -7 -4 134.807 24.671 2 0 -4 -7 160.984 32.877 2 7 -1 4 155.532 37.657 1 -1 -4 -7 141.247 28.997 2 4 1 7 172.901 30.668 1 7 -4 -1 138.294 31.374 2 -7 -4 1 176.266 30.223 1 4 -7 1 153.209 24.059 2 -4 -1 7 130.371 25.683 1 -4 1 -7 208.582 29.620 2 -7 -1 -4 134.627 21.327 2 -4 -7 -1 149.294 25.002 1 1 -7 -4 112.917 22.144 2 1 -4 7 171.818 35.576 1 -1 -4 7 111.215 31.280 1 -4 -7 1 121.198 21.930 1 -7 -4 -1 152.951 31.368 1 -4 -1 -7 134.176 25.986 2 1 -4 -7 129.642 31.224 2 7 1 4 166.763 37.329 1 4 -7 -1 177.846 24.696 2 7 -4 1 184.368 30.627 2 4 -1 7 212.330 34.859 1 -1 -7 -4 132.552 23.745 2 -7 1 -4 186.806 23.821 2 -2 -4 -7 157.317 27.665 2 7 4 2 230.729 39.661 1 -4 2 -7 159.053 28.259 2 -7 -2 -4 149.563 21.449 2 2 -7 -4 148.925 25.242 2 -7 -4 2 130.117 28.946 1 4 2 7 151.604 28.641 1 -4 -2 7 82.4363 26.4918 1 2 -4 7 189.304 36.479 1 4 -7 2 200.747 27.066 2 7 -4 -2 137.232 31.136 2 -7 -2 4 192.384 36.593 1 4 -7 -2 145.036 23.715 2 -2 -4 7 137.313 33.489 1 -4 -2 -7 85.6308 23.5591 2 -2 -7 -4 104.989 22.356 2 2 -4 -7 145.806 32.011 2 7 2 4 249.847 41.291 1 7 -4 2 175.465 30.915 2 -7 2 -4 185.754 25.375 2 -4 -7 2 138.189 22.307 1 4 -2 7 174.648 36.293 1 3 -4 7 181.964 38.128 1 -4 -3 7 47.6135 27.5427 1 4 -7 3 113.904 25.064 2 -4 3 -7 103.523 26.131 2 7 -4 -3 129.163 30.467 2 4 3 7 138.797 27.201 1 -3 -7 4 80.8887 18.7932 1 4 -3 7 158.584 38.540 1 3 -4 -7 85.8837 29.5466 2 -7 -3 4 126.589 33.738 1 -4 -7 3 122.173 21.342 1 3 4 7 103.430 23.288 1 7 0 5 90.0219 34.1869 1 0 -5 7 105.752 28.163 1 -5 -7 0 119.688 23.109 1 0 -7 -5 75.5383 20.0596 2 7 -1 5 873.434 94.518 1 -5 -7 -1 985.325 79.934 1 -5 -7 1 954.315 78.367 1 0 0 8 1363.77 105.68 1 0 -1 -8 70.5134 25.8766 2 0 -1 8 95.3131 22.7744 1 0 1 8 105.550 20.280 1 8 0 1 64.9347 31.1238 1 1 0 8 115.186 23.130 1 -1 0 8 99.2815 20.7549 1 -8 -1 0 151.437 34.562 1 -1 0 -8 116.857 28.250 2 8 1 1 252.575 48.187 1 -1 -1 -8 233.941 36.900 2 -1 -1 8 272.507 34.707 1 -8 1 -1 279.084 28.220 2 -8 -1 1 234.748 41.887 1 -1 1 8 291.322 30.548 1 1 -1 8 251.784 34.996 1 1 1 8 260.910 31.573 1 1 -8 -1 276.384 28.552 2 8 0 2 1072.89 111.65 1 2 -8 0 1262.77 89.31 2 2 0 8 1263.06 100.96 1 -2 0 -8 1204.59 97.37 2 -2 0 8 1344.49 97.93 1 -8 0 -2 1233.56 89.21 2 0 -2 -8 1193.15 100.82 2 0 -2 8 1306.45 103.91 1 -8 -2 0 1235.42 109.31 1 -8 2 -1 94.0373 18.7591 2 -8 -2 1 94.7350 28.9818 1 -1 -2 -8 107.135 26.516 2 -2 -1 8 108.778 23.877 1 -2 1 -8 92.9516 25.4467 2 1 -2 8 111.356 27.346 1 1 -8 -2 94.8971 18.8289 2 2 1 8 103.094 23.007 1 8 2 1 115.752 36.189 1 1 -2 -8 79.0510 27.9365 2 1 2 8 108.445 20.464 1 2 -1 8 128.465 26.597 1 -2 -1 -8 108.738 27.095 2 -1 -2 8 111.729 25.552 1 -8 1 -2 113.901 19.544 2 2 -8 -1 97.0455 19.0578 2 8 1 2 151.613 39.632 1 -8 -2 2 849.760 94.214 1 -8 2 -2 1045.92 81.91 2 -2 -2 -8 1161.46 91.20 2 -2 -2 8 1079.61 93.28 1 2 -8 -2 1221.68 83.04 2 2 2 8 1144.32 90.14 1 8 2 2 1264.68 110.43 1 2 -2 8 1214.69 98.53 1 -8 0 -3 104.348 19.471 2 0 -3 -8 57.5837 25.6179 2 0 -3 8 63.7661 26.1831 1 3 -8 0 92.9765 18.9348 2 8 0 3 71.2438 32.8970 1 -3 0 -8 86.6393 24.5989 2 0 -8 -3 117.412 20.041 2 -8 -3 0 98.6867 29.8185 1 8 -3 0 71.5928 20.7078 2 3 0 8 74.7585 24.2490 1 -3 1 -8 181.028 31.805 2 3 -8 1 149.469 22.869 2 8 -3 -1 223.389 30.768 2 -3 -1 8 189.191 28.684 1 -8 -3 1 231.622 36.771 1 1 -8 -3 167.290 24.897 2 -8 1 -3 199.081 25.253 2 1 -3 -8 164.670 35.103 2 3 -8 -1 160.194 23.300 2 -8 -3 -1 204.368 37.629 1 8 1 3 231.308 46.410 1 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 92385 _shelx_res_file ; TITL tak11_0m in Pm-3m Sr3PbO at 295K CELL 0.71073 5.1505 5.1505 5.1505 90.000 90.000 90.000 ZERR 1.00 0.0031 0.0031 0.0031 0.000 0.000 0.000 LATT 1 SYMM -X, -Y, Z SYMM -X, Y, -Z SYMM X, -Y, -Z SYMM Z, X, Y SYMM Z, -X, -Y SYMM -Z, -X, Y SYMM -Z, X, -Y SYMM Y, Z, X SYMM -Y, Z, -X SYMM Y, -Z, -X SYMM -Y, -Z, X SYMM Y, X, -Z SYMM -Y, -X, -Z SYMM Y, -X, Z SYMM -Y, X, Z SYMM X, Z, -Y SYMM -X, Z, Y SYMM -X, -Z, -Y SYMM X, -Z, Y SYMM Z, Y, -X SYMM Z, -Y, X SYMM -Z, Y, X SYMM -Z, -Y, -X SFAC O SR PB UNIT 1 3 1 TEMP 24.860 SIZE 0.04 0.12 0.12 ACTA L.S. 4 BOND FMAP 2 PLAN 20 WGHT 0.016700 EXTI 0.158842 FVAR 0.98042 PB 3 0.500000 0.500000 0.500000 10.02083 0.01312 0.01312 = 0.01312 0.00000 0.00000 0.00000 SR 2 0.500000 0.000000 0.000000 10.06250 0.01089 0.01875 = 0.01875 0.00000 0.00000 0.00000 O 1 0.000000 0.000000 0.000000 10.02083 0.01349 0.01349 = 0.01349 0.00000 0.00000 0.00000 HKLF 4 REM tak11_0m in Pm-3m Sr3PbO at 295K REM R1 = 0.0181 for 101 Fo > 4sig(Fo) and 0.0181 for all 101 data REM 6 parameters refined using 0 restraints END WGHT 0.0163 0.0000 REM Highest difference peak 1.743, deepest hole -1.718, 1-sigma level 0.373 Q1 1 0.5000 0.5000 0.3714 10.12500 0.05 1.74 Q2 1 0.1085 0.1085 0.1085 10.16667 0.05 0.77 Q3 1 0.5000 0.1288 0.0000 10.25000 0.05 0.65 Q4 1 0.3605 0.2724 0.3605 10.50000 0.05 0.58 Q5 1 0.3793 0.0825 0.3793 10.50000 0.05 0.55 Q6 1 0.1960 0.1960 0.1960 10.16667 0.05 0.55 Q7 1 0.3655 0.1846 0.1846 10.50000 0.05 0.52 Q8 1 0.4178 0.0988 0.0988 10.50000 0.05 0.51 Q9 1 0.2780 0.1534 0.1534 10.50000 0.05 0.49 Q10 1 0.2969 0.1835 0.2969 10.50000 0.05 0.42 Q11 1 0.3700 0.0000 0.0000 10.12500 0.05 0.31 Q12 1 0.3113 0.0000 0.3113 10.25000 0.05 0.22 Q13 1 0.5000 0.1639 0.3299 10.50000 0.05 0.18 ; _shelx_res_checksum 22076 _shelxl_version_number .2013 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' '-x, y, -z' 'x, -y, -z' 'z, x, y' 'z, -x, -y' '-z, -x, y' '-z, x, -y' 'y, z, x' '-y, z, -x' 'y, -z, -x' '-y, -z, x' 'y, x, -z' '-y, -x, -z' 'y, -x, z' '-y, x, z' 'x, z, -y' '-x, z, y' '-x, -z, -y' 'x, -z, y' 'z, y, -x' 'z, -y, x' '-z, y, x' '-z, -y, -x' '-x, -y, -z' 'x, y, -z' 'x, -y, z' '-x, y, z' '-z, -x, -y' '-z, x, y' 'z, x, -y' 'z, -x, y' '-y, -z, -x' 'y, -z, x' '-y, z, x' 'y, z, -x' '-y, -x, z' 'y, x, z' '-y, x, -z' 'y, -x, -z' '-x, -z, y' 'x, -z, -y' 'x, z, y' '-x, z, -y' '-z, -y, x' '-z, y, -x' 'z, -y, -x' 'z, y, x' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pb Pb 0.5000 0.5000 0.5000 0.01312(16) Uani d 1 . . Sr Sr 0.5000 0.0000 0.0000 0.01613(19) Uani d 1 . . O O 0.0000 0.0000 0.0000 0.0135(12) Uani d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Pb 0.01312(16) 0.01312(16) 0.01312(16) 0.000 0.000 0.000 Sr 0.0109(2) 0.0187(2) 0.0187(2) 0.000 0.000 0.000 O 0.0135(12) 0.0135(12) 0.0135(12) 0.000 0.000 0.000 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sr Sr -1.5307 3.2498 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Pb Pb -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle Sr Pb Sr 9_665 . 120.0 Sr Pb Sr 9_665 9 180.0 Sr Pb Sr . 9 60.0 Sr Pb Sr 9_665 5_656 60.0 Sr Pb Sr . 5_656 120.0 Sr Pb Sr 9 5_656 120.0 Sr Pb Sr 9_665 1_566 60.0 Sr Pb Sr . 1_566 180.0 Sr Pb Sr 9 1_566 120.0 Sr Pb Sr 5_656 1_566 60.0 Sr Pb Sr 9_665 5 120.0 Sr Pb Sr . 5 60.0 Sr Pb Sr 9 5 60.0 Sr Pb Sr 5_656 5 180.0 Sr Pb Sr 1_566 5 120.0 Sr Pb Sr 9_665 1_565 60.0 Sr Pb Sr . 1_565 90.0 Sr Pb Sr 9 1_565 120.0 Sr Pb Sr 5_656 1_565 120.0 Sr Pb Sr 1_566 1_565 90.0 Sr Pb Sr 5 1_565 60.0 Sr Pb Sr 9_665 5_556 120.0 Sr Pb Sr . 5_556 120.0 Sr Pb Sr 9 5_556 60.0 Sr Pb Sr 5_656 5_556 90.0 Sr Pb Sr 1_566 5_556 60.0 Sr Pb Sr 5 5_556 90.0 Sr Pb Sr 1_565 5_556 120.0 Sr Pb Sr 9_665 5_655 60.0 Sr Pb Sr . 5_655 60.0 Sr Pb Sr 9 5_655 120.0 Sr Pb Sr 5_656 5_655 90.0 Sr Pb Sr 1_566 5_655 120.0 Sr Pb Sr 5 5_655 90.0 Sr Pb Sr 1_565 5_655 60.0 Sr Pb Sr 5_556 5_655 180.0 Sr Pb Sr 9_665 1_556 120.0 Sr Pb Sr . 1_556 90.0 Sr Pb Sr 9 1_556 60.0 Sr Pb Sr 5_656 1_556 60.0 Sr Pb Sr 1_566 1_556 90.0 Sr Pb Sr 5 1_556 120.0 Sr Pb Sr 1_565 1_556 180.0 Sr Pb Sr 5_556 1_556 60.0 Sr Pb Sr 5_655 1_556 120.0 Sr Pb Sr 9_665 9_655 90.0 Sr Pb Sr . 9_655 60.0 Sr Pb Sr 9 9_655 90.0 Sr Pb Sr 5_656 9_655 60.0 Sr Pb Sr 1_566 9_655 120.0 Sr Pb Sr 5 9_655 120.0 Sr Pb Sr 1_565 9_655 120.0 Sr Pb Sr 5_556 9_655 120.0 Sr Pb Sr 5_655 9_655 60.0 Sr Pb Sr 1_556 9_655 60.0 Sr Pb Sr 9_665 9_565 90.0 Sr Pb Sr . 9_565 120.0 Sr Pb Sr 9 9_565 90.0 Sr Pb Sr 5_656 9_565 120.0 Sr Pb Sr 1_566 9_565 60.0 Sr Pb Sr 5 9_565 60.0 Sr Pb Sr 1_565 9_565 60.0 Sr Pb Sr 5_556 9_565 60.0 Sr Pb Sr 5_655 9_565 120.0 Sr Pb Sr 1_556 9_565 120.0 Sr Pb Sr 9_655 9_565 180.0 O Sr O 1_655 . 180.0 O Sr Pb 1_655 . 90.0 O Sr Pb . . 90.0 O Sr Pb 1_655 1_544 90.0 O Sr Pb . 1_544 90.0 Pb Sr Pb . 1_544 180.0 O Sr Sr 1_655 9_655 45.0 O Sr Sr . 9_655 135.0 Pb Sr Sr . 9_655 60.0 Pb Sr Sr 1_544 9_655 120.0 O Sr Sr 1_655 9_554 135.0 O Sr Sr . 9_554 45.0 Pb Sr Sr . 9_554 120.0 Pb Sr Sr 1_544 9_554 60.0 Sr Sr Sr 9_655 9_554 180.0 O Sr Sr 1_655 5_545 135.0 O Sr Sr . 5_545 45.0 Pb Sr Sr . 5_545 120.0 Pb Sr Sr 1_544 5_545 60.0 Sr Sr Sr 9_655 5_545 120.0 Sr Sr Sr 9_554 5_545 60.0 O Sr Sr 1_655 5_655 45.0 O Sr Sr . 5_655 135.0 Pb Sr Sr . 5_655 60.0 Pb Sr Sr 1_544 5_655 120.0 Sr Sr Sr 9_655 5_655 60.0 Sr Sr Sr 9_554 5_655 120.0 Sr Sr Sr 5_545 5_655 180.0 O Sr Pb 1_655 1_554 90.0 O Sr Pb . 1_554 90.0 Pb Sr Pb . 1_554 90.0 Pb Sr Pb 1_544 1_554 90.0 Sr Sr Pb 9_655 1_554 120.0 Sr Sr Pb 9_554 1_554 60.0 Sr Sr Pb 5_545 1_554 120.0 Sr Sr Pb 5_655 1_554 60.0 O Sr Sr 1_655 5 135.0 O Sr Sr . 5 45.0 Pb Sr Sr . 5 60.0 Pb Sr Sr 1_544 5 120.0 Sr Sr Sr 9_655 5 120.0 Sr Sr Sr 9_554 5 60.0 Sr Sr Sr 5_545 5 90.0 Sr Sr Sr 5_655 5 90.0 Pb Sr Sr 1_554 5 60.0 O Sr Sr 1_655 5_645 45.0 O Sr Sr . 5_645 135.0 Pb Sr Sr . 5_645 120.0 Pb Sr Sr 1_544 5_645 60.0 Sr Sr Sr 9_655 5_645 60.0 Sr Sr Sr 9_554 5_645 120.0 Sr Sr Sr 5_545 5_645 90.0 Sr Sr Sr 5_655 5_645 90.0 Pb Sr Sr 1_554 5_645 120.0 Sr Sr Sr 5 5_645 180.0 O Sr Sr 1_655 9_654 45.0 O Sr Sr . 9_654 135.0 Pb Sr Sr . 9_654 120.0 Pb Sr Sr 1_544 9_654 60.0 Sr Sr Sr 9_655 9_654 90.0 Sr Sr Sr 9_554 9_654 90.0 Sr Sr Sr 5_545 9_654 120.0 Sr Sr Sr 5_655 9_654 60.0 Pb Sr Sr 1_554 9_654 60.0 Sr Sr Sr 5 9_654 120.0 Sr Sr Sr 5_645 9_654 60.0 Sr O Sr 9 . 90.0 Sr O Sr 9 1_455 90.0 Sr O Sr . 1_455 180.0 Sr O Sr 9 5_545 90.0 Sr O Sr . 5_545 90.0 Sr O Sr 1_455 5_545 90.0 Sr O Sr 9 5 90.0 Sr O Sr . 5 90.0 Sr O Sr 1_455 5 90.0 Sr O Sr 5_545 5 180.0 Sr O Sr 9 9_554 180.0 Sr O Sr . 9_554 90.0 Sr O Sr 1_455 9_554 90.0 Sr O Sr 5_545 9_554 90.0 Sr O Sr 5 9_554 90.0 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance Pb Sr 9_665 3.642(2) Pb Sr . 3.642(2) Pb Sr 9 3.642(2) Pb Sr 5_656 3.642(2) Pb Sr 1_566 3.642(2) Pb Sr 5 3.642(2) Pb Sr 1_565 3.642(2) Pb Sr 5_556 3.642(2) Pb Sr 5_655 3.642(2) Pb Sr 1_556 3.642(2) Pb Sr 9_655 3.642(2) Pb Sr 9_565 3.642(2) Sr O 1_655 2.5753(15) Sr O . 2.5753(15) Sr Pb 1_544 3.642(2) Sr Sr 9_655 3.642(2) Sr Sr 9_554 3.642(2) Sr Sr 5_545 3.642(2) Sr Sr 5_655 3.642(2) Sr Pb 1_554 3.642(2) Sr Sr 5 3.642(2) Sr Sr 5_645 3.642(2) Sr Sr 9_654 3.642(2) O Sr 9 2.5753(15) O Sr 1_455 2.5753(15) O Sr 5_545 2.5753(15) O Sr 5 2.5753(15) O Sr 9_554 2.5753(15)