#------------------------------------------------------------------------------ #$Date: 2025-02-09 19:06:48 +0100 (Sun, 09 Feb 2025) $ #$Revision: 297649 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/33/2023385.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023385 loop_ _publ_author_name 'Nuss, J\"urgen' 'M\"uhle, Claus' 'Hayama, Kyouhei' 'Abdolazimi, Vahideh' 'Takagi, Hidenori' _publ_section_title ; Tilting structures ininverseperovskites,M3TtO (M= Ca, Sr, Ba, Eu;Tt= Si, Ge, Sn, Pb) ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B Structural Science, Crystal Engineering and Materials' _journal_page_first 300 _journal_page_last 312 _journal_paper_doi 10.1107/S2052520615006150 _journal_volume 71 _journal_year 2015 _chemical_formula_moiety 'Eu3 Sn O' _chemical_formula_sum 'Eu3 O Sn' _chemical_formula_weight 590.57 _space_group_crystal_system cubic _space_group_IT_number 221 _space_group_name_Hall '-P 4 2 3' _space_group_name_H-M_alt 'P m -3 m' _symmetry_cell_setting cubic _symmetry_space_group_name_H-M 'P m -3 m' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2013 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 1 _cell_length_a 5.077(3) _cell_length_b 5.077(3) _cell_length_c 5.077(3) _cell_measurement_reflns_used 704 _cell_measurement_temperature 295(2) _cell_measurement_theta_max 36.44 _cell_measurement_theta_min 4.01 _cell_volume 130.86(13) _computing_cell_refinement 'Bruker Suite (Bruker AXS, 2013)' _computing_data_collection 'Bruker Suite (Bruker AXS, 2013)' _computing_data_reduction 'Bruker Suite (Bruker AXS, 2013)' _computing_structure_refinement 'SHELXL (Sheldrick, 2008)' _computing_structure_solution 'SHELXL (Sheldrick, 2008)' _diffrn_ambient_temperature 295(2) _diffrn_measured_fraction_theta_full 0.976 _diffrn_measured_fraction_theta_max 1.00 _diffrn_measurement_device_type 'SMART APEX II, Bruker AXS' _diffrn_measurement_method \wscan _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0237 _diffrn_reflns_limit_h_max 8 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_k_max 8 _diffrn_reflns_limit_k_min -8 _diffrn_reflns_limit_l_max 8 _diffrn_reflns_limit_l_min -8 _diffrn_reflns_number 2477 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 36.436 _diffrn_reflns_theta_min 4.014 _exptl_absorpt_coefficient_mu 39.998 _exptl_absorpt_correction_T_max 0.166 _exptl_absorpt_correction_T_min 0.084 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; Sheldrick, G. M. (2012) SADABS - Bruker AXS area detector scaling and absorption, version 2012/1, University of G\"ottingen. Germany. ; _exptl_crystal_colour 'dark grey metallic' _exptl_crystal_density_diffrn 7.494 _exptl_crystal_description block _exptl_crystal_F_000 247 _exptl_crystal_size_max 0.060 _exptl_crystal_size_mid 0.040 _exptl_crystal_size_min 0.020 _refine_diff_density_max 1.097 _refine_diff_density_min -0.602 _refine_ls_extinction_coef 0.096(4) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method SHELXL _refine_ls_goodness_of_fit_ref 1.123 _refine_ls_matrix_type full _refine_ls_number_parameters 6 _refine_ls_number_reflns 93 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.123 _refine_ls_R_factor_all 0.0123 _refine_ls_R_factor_gt 0.0117 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details ; w=1/[\s^2^(Fo^2^)+(0.0171P)^2^+0.0340P] where P=(Fo^2^+2Fc^2^)/3 ; _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0320 _refine_ls_wR_factor_ref 0.0327 _reflns_number_gt 89 _reflns_number_total 93 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file dk5032sup1.cif _cod_data_source_block Eu3SnO_295K _cod_depositor_comments 'Adding Fobs data.' _cod_original_cell_volume 130.9(2) _cod_database_code 2023385 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.198 _shelx_estimated_absorpt_t_max 0.502 _shelx_hkl_file ; -1 0 0 213.512 7.887 1 -1 0 0 227.760 8.256 2 0 -1 0 218.775 8.148 2 0 0 -1 214.639 7.668 1 0 0 1 235.079 7.931 2 0 0 1 210.448 7.711 3 0 1 0 216.951 7.316 1 0 1 0 230.055 7.617 3 1 0 0 215.182 7.477 3 -1 -1 0 26.2126 1.8777 1 -1 -1 0 25.2755 1.9553 2 -1 0 -1 19.9286 2.7165 1 -1 0 1 22.8507 1.2930 1 -1 0 1 22.2175 2.0022 2 -1 0 1 26.5809 1.7791 3 -1 1 0 25.9537 1.8767 1 0 -1 -1 27.4611 1.7810 2 0 -1 1 23.7786 2.1648 2 0 1 -1 28.0858 1.6988 1 0 1 -1 28.7108 1.9468 3 0 1 1 23.2350 1.6985 1 0 1 1 24.4970 1.9617 3 1 -1 0 20.5990 2.3165 2 1 0 1 25.0069 1.8946 2 1 1 0 24.8837 2.0209 3 -1 -1 -1 8652.99 270.49 1 -1 -1 1 9233.98 287.29 2 -1 1 -1 8663.13 270.78 1 -1 1 1 9319.40 272.31 1 -1 1 1 9451.29 284.94 2 -1 1 1 8881.09 273.19 3 1 -1 1 8668.49 285.05 2 1 -1 1 8533.71 272.25 3 1 1 -1 9050.26 272.33 3 1 1 1 8331.95 272.66 3 -2 0 0 9362.18 289.08 1 -2 0 0 8889.45 304.18 2 0 -2 0 9755.65 304.15 2 0 0 -2 9466.44 288.78 1 0 0 2 9999.99 303.80 2 0 0 2 9518.93 290.83 3 0 2 0 9478.76 289.03 1 0 2 0 9430.41 292.62 3 2 0 0 9405.73 292.13 3 -2 0 -1 156.327 8.351 1 -2 0 1 176.742 6.164 1 -2 0 1 156.087 7.545 2 -1 -2 0 164.448 7.125 2 -1 2 0 157.680 6.612 1 -1 2 0 175.789 6.025 3 0 -1 -2 171.932 6.995 1 0 -1 2 145.180 7.364 2 0 -1 2 165.706 6.877 3 0 1 -2 144.270 7.081 1 0 1 2 167.707 6.426 2 0 1 2 169.966 7.285 3 1 -2 0 159.161 7.902 2 1 2 0 157.911 6.180 1 1 2 0 162.625 7.177 3 2 0 -1 154.694 6.574 3 2 0 1 161.745 7.338 2 2 0 1 158.382 6.954 3 -2 -1 0 167.888 7.608 1 -2 -1 0 162.987 7.121 2 -2 1 0 164.054 7.045 1 -1 0 -2 165.445 8.122 1 -1 0 2 160.978 6.048 1 -1 0 2 163.116 7.324 2 -1 0 2 161.684 6.840 3 0 -2 -1 164.454 6.882 2 0 -2 1 160.507 7.753 2 0 2 -1 169.732 6.174 1 0 2 -1 165.701 6.762 3 0 2 1 157.767 6.491 1 0 2 1 180.289 7.362 3 1 0 2 166.768 6.711 2 1 0 2 150.253 6.988 3 2 -1 0 158.924 8.070 2 2 -1 0 165.928 5.702 3 2 1 0 156.768 7.058 3 -2 -1 -1 15.5880 2.7220 1 -2 -1 -1 18.4665 1.7144 2 -2 -1 1 17.5848 1.2637 1 -2 -1 1 13.4839 2.1215 2 -2 1 -1 14.4161 2.6031 1 -2 1 1 15.1817 1.6337 1 -2 1 1 16.4215 2.4642 2 -1 -2 -1 14.1252 1.8802 1 -1 -2 -1 17.3355 1.5195 2 -1 -2 1 16.1895 2.2774 2 -1 -1 -2 15.1262 2.3277 1 -1 -1 2 14.2566 2.1903 2 -1 1 -2 14.8797 2.7920 1 -1 1 2 13.5710 1.4952 1 -1 1 2 16.0603 2.0610 2 -1 1 2 15.4185 1.8018 3 -1 2 -1 14.6983 1.8807 1 -1 2 -1 14.1496 1.4075 3 -1 2 1 13.1270 1.6614 1 -1 2 1 17.7248 1.6180 3 1 -2 -1 17.8812 2.4502 2 1 -2 1 15.3540 2.5561 2 1 -1 2 14.9865 2.1347 2 1 -1 2 16.6324 1.8569 3 1 1 -2 17.1334 1.4722 1 1 1 -2 12.5988 1.9311 3 1 1 2 12.7964 2.1657 3 1 2 -1 13.9125 1.0627 1 1 2 -1 16.4688 2.0765 3 1 2 1 18.6889 2.4588 3 2 -1 -1 15.1762 1.4106 3 2 -1 1 10.2504 2.2079 2 2 -1 1 13.9661 1.3157 3 2 1 -1 16.7307 2.0330 3 2 1 1 18.6009 2.3676 3 -2 -2 0 8405.84 259.30 1 -2 -2 0 8271.98 273.00 2 -2 0 -2 8067.87 261.97 1 -2 0 2 8295.36 258.92 1 -2 0 2 8720.41 274.06 2 -2 2 0 8885.43 259.62 1 0 -2 -2 9181.12 272.44 2 0 -2 2 8577.91 274.21 2 0 2 -2 8771.09 258.69 1 0 2 -2 8376.27 261.44 3 0 2 2 9143.57 259.23 1 0 2 2 8804.50 262.12 3 2 -2 0 8395.28 274.72 2 2 0 -2 8578.89 261.32 3 2 0 2 8024.20 272.81 2 2 0 2 7319.37 261.35 3 2 2 0 8576.92 262.04 3 -2 -2 -1 112.101 6.241 1 -2 -2 -1 124.203 5.276 2 -2 -2 1 124.321 5.062 1 -2 -2 1 104.262 6.261 2 -2 -1 -2 119.348 7.149 1 -2 -1 2 112.428 6.614 2 -2 1 -2 109.302 7.391 1 -2 1 2 117.928 5.157 1 -2 1 2 110.491 6.611 2 -2 1 2 118.879 5.407 3 -2 2 -1 123.183 6.475 1 -2 2 1 113.654 5.611 1 -2 2 1 120.443 4.603 3 -1 -2 -2 122.068 6.252 1 -1 -2 2 117.414 6.817 2 -1 2 -2 118.392 6.214 1 -1 2 2 108.398 5.436 1 -1 2 2 117.522 5.734 3 1 -2 -2 128.582 6.600 2 1 -2 2 113.095 6.813 2 1 -2 2 121.998 5.441 3 1 2 -2 110.309 4.022 1 1 2 -2 115.268 6.197 3 1 2 2 113.921 6.576 3 2 -2 -1 125.493 7.317 2 2 -2 1 122.326 7.351 2 2 -1 2 118.471 6.612 2 2 1 -2 107.548 5.967 3 2 1 2 113.817 4.811 2 2 1 2 126.521 6.711 3 2 2 -1 118.103 6.212 3 2 2 1 121.763 6.687 3 -2 -2 -2 7500.31 232.68 1 -2 -2 2 7747.20 244.87 2 -2 2 -2 7568.27 233.06 1 -2 2 2 7697.67 230.85 1 -2 2 2 7436.91 244.52 2 -2 2 2 7721.19 232.10 3 2 -2 2 7384.59 245.19 2 2 -2 2 7365.03 231.84 3 2 2 -2 7721.99 233.83 3 2 2 2 7368.44 234.32 3 -3 0 0 63.9164 4.3469 1 -3 0 0 61.0795 4.3794 2 0 -3 0 51.1791 4.0814 2 0 0 -3 59.9031 4.2700 1 0 0 3 56.0162 3.7992 2 0 0 3 52.0002 3.8390 3 0 3 0 56.8546 3.2703 1 0 3 0 59.1400 3.8807 3 3 0 0 52.0468 3.4208 3 -3 0 -1 31.2317 4.0891 1 -3 0 -1 29.3479 2.9588 2 -3 0 1 28.7157 2.4122 1 -3 0 1 28.8793 3.4393 2 -1 -3 0 29.9955 2.9939 2 -1 3 0 32.0738 2.7428 1 -1 3 0 31.0747 2.3846 3 0 -1 -3 35.4639 3.2917 1 0 -1 3 28.7636 3.2202 2 0 -1 3 29.1253 2.9385 3 0 1 -3 28.0732 3.4564 1 0 1 3 30.3349 2.4296 2 0 1 3 26.6545 3.0953 3 1 -3 0 33.1557 3.7836 2 1 3 0 31.1903 2.3077 1 1 3 0 30.7454 3.2764 3 3 0 -1 29.4791 2.5606 3 3 0 1 32.5902 2.9204 3 0 3 -1 25.4739 2.1647 1 0 3 -1 36.9951 3.0931 3 0 3 1 31.0270 2.6375 1 0 3 1 32.4968 3.1991 3 1 0 -3 32.4690 2.6997 1 1 0 3 30.0725 2.5791 2 1 0 3 24.5866 2.9602 3 3 -1 0 32.5062 2.1339 3 3 1 0 35.7311 3.1842 3 0 -3 -1 36.4814 3.0559 2 0 -3 1 32.6844 3.6443 2 -1 0 3 22.3156 2.7889 2 -1 0 3 29.9672 2.9697 3 -1 0 -3 28.4519 3.7944 1 -3 1 0 35.6223 3.7189 2 -3 1 0 29.2012 3.0999 1 -3 -1 0 22.7412 2.7694 2 -3 -1 0 30.9934 3.4151 1 -1 3 -1 7283.21 223.42 1 -1 1 3 7539.25 225.73 3 1 1 3 7358.67 226.51 3 1 1 -3 7454.73 223.45 1 1 -1 3 7187.59 236.09 2 1 -1 3 7164.62 225.60 3 1 -3 -1 7566.38 236.62 2 1 -3 1 7268.87 237.15 2 1 3 -1 7404.21 222.30 1 1 3 -1 7403.11 225.97 3 1 3 1 7449.46 223.32 1 1 3 1 7352.74 226.52 3 3 -1 -1 7415.17 224.25 3 3 -1 1 6880.84 236.93 2 3 -1 1 7032.67 224.34 3 3 1 -1 7344.86 225.60 3 3 1 1 7193.87 226.05 3 -3 -1 -1 7033.20 226.04 1 -3 -1 -1 6901.97 235.10 2 -3 -1 1 7248.43 222.69 1 -3 -1 1 7044.70 236.33 2 -3 1 -1 7310.23 225.82 1 -3 1 1 7330.99 223.41 1 -3 1 1 6925.57 236.77 2 -1 -3 -1 7502.30 234.89 2 -1 -3 1 7267.91 236.42 2 -1 -1 -3 7451.65 225.16 1 -1 -1 3 7331.38 236.63 2 -1 -1 3 7432.28 225.78 3 -1 1 -3 7088.32 225.76 1 -1 1 3 7634.50 223.17 1 -1 1 3 7424.83 235.83 2 -1 3 1 7470.35 224.86 3 -1 3 1 7267.26 223.43 1 -1 3 -1 7647.11 224.63 3 3 0 2 55.8644 4.0914 3 3 0 2 43.5582 3.8052 2 0 2 -3 47.0131 3.5666 1 0 2 -3 44.6093 3.9853 3 0 2 3 44.3799 4.1636 3 2 -3 0 59.2361 5.4687 2 2 3 0 42.0117 4.2999 3 3 0 -2 48.1814 3.7261 3 -3 0 -2 43.3621 5.4371 1 -3 0 2 44.6128 2.7235 1 -3 0 2 42.0603 4.4200 2 -2 -3 0 41.3151 3.3118 1 -2 -3 0 48.7273 3.8140 2 -2 3 0 47.6449 3.7670 1 0 -2 -3 51.3905 4.1135 1 0 -2 -3 49.7442 3.2267 2 0 -2 3 44.3220 4.4849 2 2 0 3 46.8045 3.4540 2 2 0 3 41.7232 3.9513 3 3 -2 0 58.8093 5.6548 2 3 2 0 56.3609 4.5885 3 -2 0 3 52.4114 3.8385 3 0 -3 -2 52.9237 3.5035 2 0 -3 2 52.6248 4.9657 2 0 3 -2 51.6585 3.0467 1 0 3 -2 54.4574 4.1012 3 0 3 2 44.6225 3.4054 1 0 3 2 60.4538 4.4670 3 -2 0 -3 38.3810 5.1130 1 -2 0 3 45.4671 2.7958 1 -3 2 0 49.2512 4.1469 1 -3 -2 0 48.8515 4.4220 1 -3 -2 0 48.3531 3.8366 2 -1 -2 -3 15.4149 2.8891 1 -1 2 3 25.3542 2.7808 2 -1 2 3 16.7263 2.6086 3 1 -2 3 16.7233 3.1767 2 1 -2 3 16.8609 2.3488 3 1 2 -3 16.8891 1.3710 1 1 2 -3 15.2298 2.8099 3 -2 1 -3 9.57585 3.10969 1 -3 1 2 16.1086 1.9351 1 2 -3 1 19.5008 3.6179 2 2 3 -1 20.7530 3.0715 3 1 3 2 16.2197 2.9393 3 -3 2 -1 17.7312 3.1611 1 3 -1 2 18.9886 3.2123 2 3 -1 2 21.2054 2.3504 3 3 1 -2 18.2055 2.7570 3 3 -2 -1 10.1526 3.0248 2 3 -2 -1 17.8179 1.4441 3 -1 -3 2 18.7780 3.3365 2 -2 -3 -1 19.0339 2.6780 1 -1 2 3 16.3673 2.2440 1 -2 3 1 15.7397 2.3509 1 -2 3 1 15.6691 1.3807 3 -1 3 -2 17.0346 2.4179 1 -3 1 2 13.2729 2.8948 2 -3 -2 1 18.7665 1.9487 1 -2 -3 -1 16.0820 2.0285 2 1 -3 -2 20.9151 2.8844 2 3 2 1 21.1078 3.2644 3 2 1 3 10.3002 2.6684 3 -3 -1 -2 12.9753 3.4467 1 -1 3 -2 16.1975 2.2811 3 -3 -2 1 14.1714 2.7180 2 -2 -1 3 15.8290 3.0459 2 -2 -3 1 14.8516 2.6958 2 2 -3 -1 15.5160 3.1922 2 -1 2 -3 18.9502 3.2225 1 -3 -2 -1 18.6538 3.4539 1 3 -1 -2 15.9325 2.0865 3 -3 -1 2 19.7457 1.2700 1 -2 -1 -3 21.8315 3.9059 1 -1 -2 3 16.8124 3.1560 2 1 2 3 14.3125 2.9438 3 -2 1 3 15.3592 1.8734 1 -2 1 3 16.7938 2.8918 2 -2 1 3 19.1102 2.4650 3 -1 -3 -2 17.0890 2.7045 1 -1 -3 -2 15.6618 1.5812 2 -3 1 -2 24.5781 4.4811 1 -2 3 -1 22.5655 2.9326 1 -3 2 1 19.9502 2.5072 1 -1 3 2 15.9741 2.2700 1 -1 3 2 17.0557 2.3567 3 -2 -3 1 16.9219 1.8465 1 1 -3 2 16.3954 3.3027 2 1 3 -2 17.0736 1.3307 1 1 3 -2 19.0761 2.9141 3 2 3 1 15.0672 3.0465 3 2 -1 3 17.7086 2.7494 2 2 -1 3 17.7815 2.5079 3 2 1 -3 14.2482 2.6528 3 -3 -2 -1 16.1972 2.1076 2 3 1 2 14.1473 2.0267 2 3 1 2 15.7699 2.8705 3 3 -2 1 15.1701 3.3213 2 3 2 -1 11.6165 2.4153 3 -3 -1 2 20.1718 3.2277 2 -3 -2 -2 36.4118 4.9316 1 -3 -2 -2 45.0816 2.8260 2 -3 -2 2 45.4855 4.7973 2 -3 2 -2 39.2576 5.1146 1 -3 2 2 39.7743 3.3444 1 -3 2 2 33.5548 4.3561 2 -2 -3 -2 46.5274 4.4618 1 -2 -3 2 42.6511 4.5929 2 -2 -2 -3 33.2672 4.4493 1 -2 -2 3 37.1736 4.5507 2 -2 2 -3 38.6417 4.9926 1 -2 2 3 38.1879 3.2578 1 -2 2 3 35.2339 4.0889 2 -2 2 3 39.1792 3.3611 3 -2 3 -2 46.3028 4.4169 1 -2 3 -2 48.5058 3.2280 3 -2 3 2 36.1167 3.4218 1 -2 3 2 39.3424 2.8408 3 2 -3 -2 47.4716 5.0454 2 2 -3 2 50.9227 5.4254 2 2 -2 3 45.3594 4.6905 2 2 -2 3 44.9168 3.5535 3 2 2 -3 36.2294 4.1388 3 2 2 3 41.3299 4.6651 3 2 3 -2 45.2385 4.4440 3 2 3 2 43.8708 4.7388 3 3 -2 -2 45.4118 3.0370 3 3 -2 2 39.8766 4.8060 2 3 -2 2 38.2388 2.7184 3 3 2 -2 40.2212 4.0910 3 3 2 2 43.2659 4.6626 3 -3 -3 0 17.7627 3.0396 1 -3 -3 0 29.7999 3.3939 2 -3 0 -3 28.8276 5.1930 1 -3 0 3 33.7643 2.3042 1 -3 0 3 29.3120 4.1628 2 -3 3 0 25.2448 3.3833 1 0 -3 -3 29.1146 2.4940 2 0 -3 3 40.3393 4.8429 2 0 3 -3 29.7867 2.6179 1 0 3 -3 31.2509 3.7535 3 0 3 3 25.0368 2.9729 1 0 3 3 32.9667 3.9928 3 3 -3 0 24.1774 4.4108 2 3 0 -3 30.9555 3.4551 3 3 0 3 36.5076 3.2864 2 3 0 3 31.0875 3.6730 3 3 3 0 32.1491 4.1561 3 -3 -3 -1 5432.33 175.17 1 -3 -3 1 5958.12 173.34 1 -3 -3 1 5495.15 183.82 2 -3 -1 -3 5292.19 177.41 1 -3 -1 3 5637.60 185.08 2 -3 1 -3 5790.41 177.84 1 -3 1 3 5557.44 172.80 1 -3 1 3 5754.73 185.19 2 -3 3 -1 5627.74 175.46 1 -3 3 1 5566.82 174.20 1 -1 -3 -3 5567.69 174.95 1 -1 -3 3 5661.04 185.36 2 -1 3 -3 5655.65 174.21 1 -1 3 -3 5375.73 175.45 3 -1 3 3 5637.25 173.90 1 -1 3 3 5655.82 175.63 3 1 -3 -3 6129.09 183.52 2 1 -3 3 5535.49 185.46 2 1 3 -3 5523.01 176.34 3 1 3 3 5747.41 177.20 3 3 -3 -1 5663.52 186.12 2 3 -3 1 5727.12 186.31 2 3 -1 -3 5667.04 175.10 3 3 -1 3 5550.09 183.92 2 3 1 -3 5707.26 176.12 3 3 1 3 5563.98 176.51 3 3 3 -1 5664.06 176.68 3 3 3 1 5605.56 177.15 3 -3 -3 -2 16.8181 3.7224 1 -3 -3 2 16.6184 3.5572 2 -3 -2 -3 17.8669 4.3002 1 -3 -2 3 24.3778 4.1656 2 -3 2 -3 16.5512 4.1798 1 -3 2 3 21.3575 2.7189 1 -3 2 3 13.8435 3.3298 2 -3 2 3 18.7682 2.4387 3 -3 3 -2 12.2168 3.3660 1 -3 3 2 25.7216 3.1444 1 -2 -3 -3 11.8985 3.1373 1 -2 -3 3 15.7844 3.4784 2 -2 3 -3 6.02142 2.51062 1 -2 3 -3 18.7131 2.7018 3 -2 3 3 15.0751 2.6757 1 -2 3 3 16.9167 2.4705 3 2 -3 -3 18.9392 3.7999 2 2 -3 3 15.2109 3.7042 2 2 3 -3 20.4542 3.7038 3 2 3 3 20.8495 3.8259 3 3 -3 -2 19.4711 4.4519 2 3 -3 2 15.0826 3.8678 2 3 -2 3 23.9621 3.9680 2 3 -2 3 17.6820 2.4875 3 3 2 -3 18.4784 3.4065 3 3 2 3 16.3679 3.5399 3 3 3 -2 16.6297 3.4224 3 3 3 2 20.6442 3.9042 3 -3 -3 -3 4155.82 131.65 1 -3 -3 3 4159.02 137.65 2 -3 3 -3 4035.22 131.64 1 -3 3 3 4088.78 128.61 1 -3 3 3 4233.89 128.37 3 3 -3 -3 4218.85 138.64 2 3 -3 3 4073.67 138.11 2 3 3 -3 3998.58 131.15 3 3 3 3 4076.54 131.77 3 -4 0 0 6741.74 210.25 1 -4 0 0 6663.44 221.32 2 0 -4 0 6679.47 221.07 2 0 0 -4 6994.59 210.45 1 0 0 4 6970.40 211.87 3 0 4 0 6938.12 208.62 1 0 4 0 6726.48 211.20 3 4 0 0 6742.22 210.39 3 -4 0 -1 69.8137 6.4999 1 -4 0 -1 85.7317 5.7060 2 -4 0 1 79.8180 4.7584 1 -4 0 1 84.5308 6.3604 2 -1 -4 0 86.5522 5.6836 2 -1 4 0 89.8500 5.1100 1 -1 4 0 77.1799 4.7218 3 0 -1 -4 75.5487 5.5860 1 0 -1 4 78.3997 5.9134 2 0 -1 4 67.6739 5.1676 3 0 1 -4 91.7251 6.3476 1 0 1 4 68.1563 4.6075 2 0 1 4 80.9583 5.8086 3 1 -4 0 76.6458 6.2465 2 1 4 0 82.7828 4.5393 1 1 4 0 79.3945 5.8373 3 4 0 -1 87.3340 5.0135 3 4 0 1 83.9280 5.1910 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2.09053 1.97235 3 -4 3 1 0.10514 1.46167 1 -4 -3 -1 1.20867 2.74757 1 4 3 -1 3.38112 2.08947 3 1 3 4 4.62385 2.39764 3 3 1 -4 4.46608 2.01607 3 -3 1 4 4.35776 2.48729 2 -3 1 4 0.66629 1.52505 3 -4 -1 3 1.89194 2.12480 2 -4 1 -3 0.17708 2.70988 1 1 4 -3 1.68959 1.98300 3 3 -4 -1 1.91503 2.33304 2 -1 4 3 1.55127 1.52724 1 -1 4 3 3.36944 1.87686 3 -3 -4 1 -1.0305 1.5643 2 -3 4 -1 0.10090 1.66488 1 -1 -3 4 8.31167 3.04238 2 -1 3 -4 1.05538 2.08985 1 -4 -3 -1 3.22317 1.72812 2 -4 -2 -3 21.1552 5.2973 1 4 -2 3 30.9513 4.8242 2 4 2 -3 35.5343 4.5892 3 3 -4 2 27.9114 5.3502 2 3 4 -2 30.3380 4.5803 3 -4 3 -2 26.5203 4.9943 1 -3 4 2 25.5340 3.6066 1 -3 2 -4 34.5244 5.7272 1 2 -3 4 27.8428 4.9548 2 2 3 -4 35.0321 4.8073 3 -4 2 3 31.5092 3.4134 1 -4 2 3 29.2583 4.8821 2 -2 -3 -4 20.2045 4.3808 1 -4 -3 2 22.3401 4.2252 2 2 4 3 26.6253 4.4738 3 3 2 4 37.1027 4.9294 3 -2 3 4 26.5133 3.4628 1 -2 3 4 29.7628 3.6639 3 4 3 2 31.6287 4.8811 3 -2 -4 3 37.1896 5.1588 2 -2 4 -3 33.0482 4.4131 1 -3 -2 4 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2.99419 2 -3 3 -4 1.53298 2.64819 1 -3 3 4 1.56492 1.69574 1 -3 3 4 2.68735 1.83764 3 -3 4 -3 2.59713 2.42829 1 -3 4 3 4.69790 2.18372 1 3 -4 -3 2.45292 2.69801 2 3 -4 3 3.52349 2.80776 2 3 -3 -4 -0.1762 2.5182 2 3 -3 4 1.64144 2.53375 2 3 3 -4 0.74704 2.28447 3 3 3 4 7.45113 2.92696 3 3 4 -3 5.63388 2.89888 3 3 4 3 0.46862 1.96089 3 4 -3 -3 6.50844 3.39904 2 4 -3 3 3.42034 2.82966 2 4 3 -3 2.09861 2.25997 3 4 3 3 0.30602 1.92241 3 -4 -4 0 3830.63 124.15 2 -4 0 -4 3736.37 122.41 1 -4 0 4 3710.30 127.20 2 -4 4 0 3738.68 119.37 1 0 -4 -4 3725.80 119.23 1 0 -4 4 3719.56 127.40 2 0 4 -4 3752.39 120.52 3 0 4 4 3606.67 120.37 3 4 -4 0 3688.04 128.13 2 4 0 -4 3817.20 119.54 3 4 0 4 3872.66 119.90 3 4 4 0 3784.53 121.29 3 -4 -4 -1 49.9161 5.7458 1 -4 -4 1 49.9224 5.3210 2 -4 -1 -4 44.1917 7.1096 1 -4 -1 4 38.8588 5.9355 2 -4 1 -4 46.9424 6.6105 1 -4 1 4 51.2585 6.2784 2 -4 4 -1 38.9979 5.3272 1 -4 4 1 46.7791 5.1133 1 -1 -4 -4 45.2196 5.5354 1 -1 -4 4 59.4135 6.7129 2 -1 4 -4 58.4893 4.9139 1 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-4 3 15.6973 4.1559 2 -4 -3 -4 16.1220 5.1503 1 -4 -3 4 17.6349 4.5043 2 -4 3 -4 29.3993 5.9340 1 -4 3 4 19.0525 3.4950 1 -4 4 -3 25.8427 5.2502 1 -4 4 3 21.6166 3.8054 1 -3 -4 -4 18.3023 4.9236 1 -3 -4 4 16.8048 4.5270 2 -3 4 -4 23.8224 4.7936 1 -3 4 4 19.5216 3.7413 1 3 -4 -4 26.6126 5.1993 2 3 -4 4 19.8815 4.9563 2 3 4 -4 24.3148 4.8346 3 3 4 4 21.9236 4.6553 3 4 -4 -3 18.1537 5.2120 2 4 -4 3 30.6675 5.9076 2 4 -3 -4 21.3240 5.4306 2 4 -3 4 25.2032 5.0567 2 4 3 -4 26.3244 4.8554 3 4 3 4 24.4762 4.7650 3 4 4 -3 26.9684 4.8613 3 4 4 3 27.4765 4.9642 3 -4 -4 -4 2040.23 71.72 1 -4 -4 4 2097.63 74.05 2 -4 4 -4 2003.47 70.87 1 -4 4 4 2048.93 67.76 1 4 -4 -4 2005.58 74.76 2 4 -4 4 2165.18 74.92 2 4 4 -4 1971.42 70.33 3 4 4 4 2045.58 70.40 3 -5 0 0 4.33596 2.19898 1 -5 0 0 1.19229 1.95591 2 0 -5 0 -0.0485 1.7812 2 0 0 -5 3.85003 2.80304 1 0 0 5 3.76810 2.18732 2 0 0 5 4.57765 2.15537 3 0 5 0 1.77479 1.46025 1 0 5 0 9.55047 2.67534 3 5 0 0 4.24016 1.92068 3 -5 0 -1 22.2618 4.4845 1 -5 0 1 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1 5 3.83381 3.81403 2 -6 5 -1 4.93234 3.37955 1 5 6 -1 0.08465 3.00958 3 1 -6 -5 0.99816 3.10567 1 6 1 -5 -0.6292 3.0341 3 6 -5 -1 4.13882 4.16087 2 -1 5 6 0.59044 3.04724 3 -6 -1 -5 0.05506 3.75688 1 1 5 -6 2.35523 3.69406 3 6 5 -1 2.57141 3.68086 3 5 -6 -1 -1.8797 3.3516 2 -5 1 6 11.0085 4.9537 2 -1 -6 -5 -1.1071 2.8105 1 -5 6 -1 0.54618 3.37440 1 5 6 1 4.33256 3.37226 3 5 1 -6 -0.4467 2.7011 3 -1 -5 6 0.23467 3.38232 2 6 -5 1 -0.0469 3.4004 2 1 5 6 4.74571 3.53836 3 1 -6 5 -1.1182 3.2296 2 -6 1 -5 -0.8254 3.0154 1 1 6 -5 1.51412 4.32635 3 -6 5 1 0.60936 3.00701 1 -5 -1 -6 1.71122 4.21122 1 -6 -1 5 -3.6438 2.9820 2 1 -5 -6 1.95134 3.14706 1 -6 -2 -5 7.08062 5.03823 1 -6 2 5 3.64871 3.99689 2 5 6 -2 -0.5329 3.3509 3 -2 -5 -6 -0.6299 3.5128 1 -6 -5 2 -0.4285 2.9081 2 6 2 -5 0.48611 2.98990 3 2 -5 6 1.27213 3.34216 2 -2 -6 5 -0.9919 3.0557 2 6 5 2 1.61317 3.19995 3 5 2 6 1.79939 3.02139 3 -5 -2 6 2.94240 4.03875 2 -5 2 -6 5.66576 3.95711 1 2 6 5 3.59429 3.36485 3 -6 5 -2 5.93611 4.33755 1 2 5 -6 0.59676 3.74845 3 2 -6 -5 3.36084 3.15811 1 5 -6 2 -1.0896 3.1532 2 -5 6 2 -0.4607 2.8108 1 6 -5 -2 9.04323 5.10513 2 5 2 -6 2.95614 3.45919 3 -5 -2 -6 1.55474 4.15714 1 -5 2 6 5.17819 4.90522 2 6 5 -2 6.44104 4.04415 3 -6 -2 5 3.47402 4.00066 2 -6 2 -5 2.11386 3.73777 1 -6 5 2 -1.7733 2.5379 1 -5 -6 2 -0.7823 2.9511 2 5 6 2 3.55722 3.52059 3 2 6 -5 2.77902 4.14782 3 -5 6 -2 5.45828 3.99309 1 -2 -5 6 -1.5319 3.3683 2 2 -5 -6 2.11688 3.43923 1 6 2 5 2.09788 2.98940 3 6 -5 2 11.4428 5.1211 2 2 5 6 5.54431 3.36352 3 5 -6 -2 2.92459 3.80884 2 2 -6 5 -3.2914 3.6423 2 -2 -6 -5 5.29955 4.25903 1 -5 3 -6 -1.3178 3.5170 1 6 3 -5 7.37756 4.08678 3 -6 -5 3 -1.4237 3.1059 2 -6 -3 -5 0.45489 4.59022 1 3 6 5 -2.7679 2.9636 3 -6 5 -3 -1.0669 3.5639 1 5 3 6 3.71716 3.28418 3 6 -5 -3 5.07137 4.69742 2 -5 6 3 0.70304 2.98099 1 -3 -5 -6 0.58884 4.41958 1 6 5 3 0.38250 3.20221 3 -3 -6 5 4.18588 3.90768 2 3 -5 6 3.92993 4.35921 2 3 5 -6 -0.7623 3.6509 3 5 6 -3 3.20809 3.95188 3 -5 -3 6 -1.9767 3.7657 2 5 -6 3 5.21305 4.14354 2 3 5 6 -2.8947 2.6488 3 5 6 3 -2.6201 2.7869 3 6 -3 -5 0.24837 4.11249 2 -6 3 -5 -2.7600 3.6212 1 -6 5 3 4.32257 3.25784 1 -5 -3 -6 0.90701 4.59154 1 5 -6 -3 2.39768 4.84165 2 6 3 5 -2.8546 2.8056 3 -3 -6 -5 4.94808 4.85271 1 3 -5 -6 0.41892 3.32065 1 -3 6 5 3.04322 2.75734 1 3 -6 5 0.62157 3.78852 2 3 6 -5 2.02190 3.89822 3 -6 -3 5 -3.6813 3.0374 2 5 3 -6 3.93267 3.58857 3 -5 -6 3 -3.7831 2.8684 2 -5 6 -3 0.50571 3.94066 1 6 -5 3 -2.5172 3.3682 2 6 5 -3 1.96474 3.97101 3 -3 -5 6 -2.1882 3.4943 2 -6 0 6 1070.93 45.53 2 -7 0 0 4.89313 3.11466 1 0 -7 0 0.35710 2.79998 2 0 0 7 4.77738 3.39472 3 0 7 0 2.48034 2.52870 1 7 0 0 6.96793 3.66062 2 -7 0 -1 13.2783 4.3155 1 -7 0 1 21.2582 4.9251 2 -1 -7 0 11.1578 3.8190 2 -1 7 0 16.0142 3.6456 1 0 -1 -7 11.8655 5.0801 1 0 -1 7 22.2098 4.7137 3 0 1 7 27.6352 5.2869 3 1 -7 0 10.4904 4.1839 2 7 0 1 17.5053 4.7928 2 -7 -1 0 26.1779 4.8379 2 -7 1 0 22.8541 4.6748 1 -1 0 -7 15.5616 5.2272 1 -1 0 7 17.2881 4.3592 3 0 -7 1 19.2395 4.7636 2 0 7 1 20.8388 3.8441 1 1 0 7 19.4630 4.6744 3 7 -1 0 19.5289 5.2014 2 -1 7 1 1923.39 63.46 1 1 -7 -1 1913.51 68.02 2 1 -7 1 1827.19 69.30 2 -1 -7 -1 1868.97 63.68 1 -1 -7 1 1875.79 68.18 2 -1 -1 -7 1982.34 67.49 1 -1 -1 7 1871.74 65.90 3 -7 -1 1 1920.48 68.38 2 -7 1 -1 1851.88 65.64 1 -1 1 7 1901.70 66.03 3 -1 7 -1 1962.81 63.04 1 -7 -1 -1 1882.00 64.93 1 7 1 1 1854.44 67.43 2 7 -1 -1 1851.49 70.55 2 7 -1 1 1927.45 69.07 2 1 1 7 1900.41 66.28 3 1 7 1 1882.13 65.93 3 1 -1 7 1851.49 65.55 3 -7 -2 0 1.24615 2.74104 2 -7 0 2 2.27336 3.00464 2 -2 7 0 1.22394 2.50512 1 2 -7 0 -0.5690 3.1538 2 2 7 0 6.89799 4.00465 3 0 -2 -7 6.13271 4.21087 1 2 0 7 1.96520 2.92806 3 7 -2 0 9.09628 4.15814 2 7 2 0 1.29756 3.08372 3 0 2 -7 2.59327 3.29554 3 0 2 7 6.89164 3.56481 3 -7 0 -2 3.64482 3.49464 1 0 -7 2 2.12152 3.04302 2 0 7 2 2.41330 2.53110 1 -2 0 7 1.26442 2.64009 3 -7 2 0 2.31639 2.98932 1 -2 0 -7 1.89808 3.98089 1 -7 1 2 7.93223 3.98169 2 -2 7 1 11.9876 3.5054 1 2 1 7 18.3291 4.8548 3 -7 -2 1 5.14788 3.04320 2 -7 2 -1 8.66160 4.00092 1 -1 -2 -7 11.9130 4.2945 1 1 2 -7 6.13490 4.03712 3 -2 1 -7 9.40832 4.41435 1 2 7 -1 12.2997 4.8851 3 -7 -1 -2 4.57031 3.55346 1 -1 -7 2 5.21711 3.26888 2 7 2 1 15.4299 4.2608 3 7 -1 2 12.9863 4.1582 2 2 -7 1 10.2024 4.2922 2 -1 2 7 7.00285 3.39029 3 1 7 2 12.5299 4.3431 3 1 -2 7 12.7809 3.9126 3 7 -2 -1 7.07501 4.05954 2 2 1 -7 18.7112 4.9100 3 -2 1 7 3.29094 3.14672 3 -7 2 1 12.1431 3.8106 1 -7 -1 2 17.5558 4.9206 2 -7 1 -2 8.81650 4.03794 1 2 -7 -1 10.2492 4.1176 2 -2 -7 1 9.37735 3.79065 2 2 -1 7 8.85060 3.64936 3 2 7 1 6.07972 4.22073 3 1 -7 2 9.87065 4.36417 2 -1 7 2 11.6129 3.4287 1 -2 7 -1 8.34994 3.18420 1 1 -2 -7 10.7781 4.5271 1 -1 -7 -2 14.8337 4.1435 1 -2 -1 -7 11.7466 5.5668 1 1 2 7 10.6479 4.1387 3 7 2 -1 10.6905 3.9253 3 7 -2 1 8.33513 3.84221 2 -1 -2 7 11.1931 4.5823 2 -2 2 7 3.04280 3.07845 3 -2 7 2 -0.1747 2.0727 1 2 -7 2 12.7968 4.5455 2 7 -2 2 1.18358 3.14686 2 -2 -2 7 1.22324 3.53845 2 -2 -2 -7 1.60051 4.19474 1 2 -2 7 6.46577 3.54915 3 2 2 -7 4.19044 3.42470 3 2 2 7 -2.0508 2.6278 3 2 7 -2 -1.5198 3.7848 3 2 7 2 0.41160 3.28162 3 7 -2 -2 1.54364 3.44503 2 -7 -2 -2 0.63383 3.79270 1 7 2 -2 1.82883 3.09792 3 7 2 2 3.45529 3.05054 3 -2 -7 -2 3.21191 3.22244 1 -2 -7 2 -0.3647 2.9049 2 -7 -2 2 1.37675 2.99809 2 -7 2 -2 5.26564 4.03991 1 -2 7 -2 4.11290 2.89923 1 0 -7 3 7.00741 3.88447 2 0 -3 -7 21.2647 5.2511 1 0 -3 7 16.0135 5.2955 2 0 3 -7 14.4428 4.8807 3 0 3 7 11.1715 4.3011 3 3 0 7 17.6930 4.7571 3 -3 7 0 9.66822 3.67062 1 -7 0 -3 18.1591 5.1002 1 3 -7 0 10.5631 4.4733 2 3 7 0 17.8867 5.5050 3 -7 0 3 15.8490 5.1590 2 -7 3 0 19.6148 5.0952 1 -3 0 -7 10.7925 5.1933 1 0 -7 -3 16.0065 4.5744 1 7 3 0 8.85371 4.08364 3 3 0 -7 15.1217 4.5820 3 7 -3 0 13.6541 4.7924 2 -7 -1 -3 1338.97 51.85 1 -3 7 1 1367.46 49.96 1 -3 -1 7 1435.74 55.55 2 7 3 1 1443.82 51.24 3 3 -1 -7 1387.86 51.27 3 -1 -3 -7 1399.23 52.25 1 -7 -3 1 1448.26 52.89 2 -7 3 -1 1370.15 52.19 1 3 7 -1 1407.31 53.34 3 -1 -7 3 1354.41 54.32 2 -7 1 3 1473.72 55.27 2 -3 1 -7 1399.72 51.82 1 3 -7 1 1316.60 55.02 2 3 1 7 1499.02 51.90 3 -1 3 7 1448.43 51.77 3 1 7 3 1414.79 51.35 3 1 3 -7 1376.13 52.49 3 7 -3 -1 1403.44 56.43 2 1 -3 -7 1460.28 51.17 1 -1 3 -7 1379.18 51.55 3 1 3 7 1438.89 52.13 3 3 1 -7 1460.18 52.55 3 -3 -7 1 1454.15 52.50 2 -3 7 -1 1421.24 50.03 1 7 -3 1 1365.78 54.91 2 3 7 1 1403.50 53.27 3 3 -7 -1 1364.91 54.26 2 -1 -7 -3 1431.80 51.07 1 -7 3 1 1421.29 50.38 1 -3 -1 -7 1356.21 53.19 1 -1 7 3 1440.24 49.77 1 1 -7 3 1421.27 55.76 2 -7 1 -3 1359.14 52.48 1 -7 -1 3 1445.50 54.69 2 3 -1 7 1484.01 51.07 3 -1 -3 7 1442.55 54.73 2 7 3 -1 1381.25 50.92 3 7 -3 -2 6.67678 4.59748 2 -7 -3 2 12.0610 4.4028 2 -7 3 -2 5.49231 4.35788 1 -7 -2 -3 3.41347 3.88120 1 7 2 -3 6.27426 3.55203 3 -2 -3 -7 8.98806 5.18139 1 -3 2 -7 4.58496 3.93732 1 -2 3 7 3.70217 3.15741 3 2 3 -7 5.67562 4.45332 3 -2 -7 3 3.72712 3.40127 2 2 7 3 13.2820 4.7528 3 -3 -2 7 2.36484 3.99587 2 3 2 7 7.63974 3.87697 3 7 3 2 4.03388 3.56262 3 3 -7 2 4.41981 3.96820 2 3 7 -2 9.57320 4.92722 3 -3 7 2 8.94527 3.47073 1 3 7 2 4.77790 3.98275 3 -7 3 2 10.7459 3.9539 1 -3 -2 -7 3.11697 4.73329 1 -3 -7 2 7.34237 3.87125 2 3 -7 -2 10.1689 4.5852 2 7 -3 2 6.17283 4.16720 2 7 3 -2 8.94532 4.09628 3 2 3 7 11.8129 4.0621 3 7 -2 -3 9.52995 4.72679 2 -7 -2 3 3.95154 3.94079 2 -7 2 -3 11.7315 4.7090 1 -2 7 3 4.96231 2.93046 1 2 -7 3 10.0587 4.7921 2 -3 7 -2 17.9923 4.6064 1 -3 2 7 7.88580 3.68180 3 -2 -7 -3 1.11352 3.22616 1 2 7 -3 7.15927 4.84288 3 -2 -3 7 3.57854 3.98943 2 3 2 -7 11.4671 4.6659 3 7 2 3 8.05773 3.66434 3 -3 3 7 1152.91 40.84 3 3 3 7 1089.14 42.23 3 3 -7 3 1067.18 46.10 2 3 3 -7 1052.76 42.89 3 7 -3 3 1035.58 43.29 2 7 3 -3 1093.92 41.37 3 7 3 3 1102.76 40.87 3 7 -3 -3 1092.41 46.75 2 -7 -3 -3 1124.43 42.44 1 3 7 -3 1071.06 43.73 3 -3 7 3 1105.33 40.60 1 -3 -7 3 1070.11 43.66 2 -3 7 -3 1093.14 40.27 1 -7 -3 3 1072.50 43.97 2 -3 -7 -3 1125.10 42.08 1 3 7 3 1071.68 42.41 3 -3 -3 -7 1022.66 43.50 1 4 -7 0 0.97661 3.39394 2 4 7 0 0.20318 3.38664 3 0 -4 7 2.45403 3.94372 2 0 4 -7 8.22605 4.72401 3 -7 0 -4 1.04523 3.70494 1 0 -4 -7 -0.8480 3.4633 1 7 -4 0 -1.2417 3.3210 2 7 4 0 1.79953 3.32249 3 0 4 7 2.35676 3.54314 3 -4 7 0 -1.4267 2.5332 1 -7 4 0 -0.1735 3.1058 1 -4 0 -7 -1.4838 3.9067 1 -4 0 7 -2.5169 4.4382 2 0 -7 -4 2.51177 3.48151 1 0 -7 4 2.89154 3.52362 2 4 0 -7 -0.4792 3.1553 3 4 0 7 -1.6081 3.3247 3 -7 0 4 6.18555 3.91304 2 -7 -1 -4 0.85299 4.05167 1 4 1 7 1.95832 3.22287 3 -7 1 4 -0.0475 3.2711 2 4 -1 -7 -0.0884 3.2355 3 1 -7 -4 5.74100 3.75723 1 -1 -4 -7 1.54834 3.85051 1 7 -4 -1 1.89422 3.91373 2 -1 4 7 5.63113 3.56797 3 -4 -1 7 1.35973 4.08380 2 1 -4 7 3.68671 3.85134 2 1 4 -7 2.98861 3.82974 3 -1 -7 4 2.64195 3.42641 2 7 4 1 2.10057 3.52088 3 4 -7 1 0.53744 3.51916 2 4 7 -1 8.95076 4.78555 3 1 7 4 -1.8588 3.4398 3 -7 4 -1 2.25987 3.97022 1 -4 1 -7 0.74245 4.02950 1 -4 7 1 4.14871 3.15134 1 4 7 1 0.05221 3.76444 3 -7 4 1 0.69862 3.40689 1 1 -4 -7 2.67340 3.57391 1 1 4 7 2.40971 3.30207 3 -7 -1 4 1.41859 3.67907 2 -1 -7 -4 2.97538 3.89980 1 7 -4 1 3.21350 4.22236 2 7 4 -1 0.37336 3.60493 3 4 -7 -1 3.13369 3.96381 2 -1 -4 7 5.70193 4.32238 2 -4 -1 -7 2.21075 4.65265 1 -4 7 -1 0.65161 3.32725 1 4 1 -7 0.81484 3.69347 3 -7 1 -4 4.65500 4.15281 1 1 -7 4 7.63567 4.85172 2 -7 -2 -4 4.28193 4.48669 1 -2 4 7 0.94268 3.30630 3 -4 -2 7 5.17616 4.09457 2 2 7 4 0.12416 3.40049 3 4 -7 2 1.98561 4.10251 2 4 7 -2 2.95700 4.10301 3 4 -2 -7 5.90502 4.10970 3 7 -4 -2 -0.7777 3.6169 2 7 2 -4 1.34931 3.18828 3 2 4 -7 -2.0456 3.7044 3 -7 4 -2 3.35030 3.68328 1 -4 7 2 1.26956 3.01942 1 -2 -4 -7 -3.9217 3.6978 1 4 2 7 1.24997 3.19995 3 -7 -4 2 -3.4089 2.6695 2 -4 2 -7 -0.8843 3.2980 1 7 4 2 -1.1391 3.0035 3 -2 -7 4 2.68923 3.71093 2 -4 -7 2 -0.5463 2.9821 2 2 4 7 2.12766 3.29657 3 -7 4 2 2.00846 3.44993 1 -4 -2 -7 -3.5625 3.9266 1 -2 -4 7 2.33803 4.03152 2 2 -4 -7 4.72390 3.84151 1 -2 -7 -4 -1.2397 3.8376 1 -4 7 -2 8.93121 4.36354 1 -2 7 4 -2.4434 2.2752 1 2 -7 4 4.24553 4.39848 2 2 7 -4 -2.2043 4.0586 3 4 -7 -2 6.98852 4.62893 2 4 7 2 -3.4300 3.0720 3 4 2 -7 4.29886 3.79001 3 -7 2 -4 4.81153 3.86904 1 7 -2 -4 -1.7427 3.4292 2 7 -4 2 -3.7299 3.3115 2 7 4 -2 4.95644 4.01332 3 -7 -2 4 -2.1338 3.2038 2 0 0 8 1316.51 49.29 3 8 0 0 1321.16 51.57 2 -1 8 0 25.0907 4.7581 1 0 -1 8 8.43475 4.06348 3 0 1 8 19.2828 5.4487 3 1 -8 0 26.1638 5.8371 2 8 0 -1 17.9571 5.7742 2 8 1 0 27.1431 5.9787 2 1 0 8 21.7867 5.2877 3 8 -1 0 27.0622 6.4423 2 0 -8 1 15.1411 4.9831 2 0 8 1 19.9838 4.4166 1 -1 0 8 18.4997 5.0564 3 -1 8 1 12.7606 4.0720 1 1 -1 8 10.4126 4.3364 3 1 1 -8 17.9759 5.0519 3 8 -1 -1 25.0008 6.7291 2 8 -1 1 22.3316 5.5699 2 1 1 8 18.0197 4.9861 3 -8 -1 1 25.5771 5.5448 2 -8 1 -1 22.8939 5.8067 1 -1 -8 1 13.3145 4.5784 2 -1 1 8 21.1730 5.2255 3 1 -8 1 15.8885 5.0953 2 2 -8 0 1196.84 47.82 2 0 2 -8 1153.98 45.49 3 0 2 8 1223.55 45.80 3 -8 0 -2 1168.27 44.58 1 -8 0 2 1246.94 47.72 2 -2 8 0 1230.53 43.40 1 2 0 8 1227.58 45.41 3 8 -2 0 1118.88 47.89 2 0 -8 2 1146.24 47.50 2 2 0 -8 1139.55 45.16 3 0 -8 -2 1177.30 44.07 1 -8 2 0 1151.12 43.75 1 -1 2 8 19.3971 5.4049 3 1 2 -8 16.7016 5.2112 3 -2 8 1 23.3162 4.8928 1 2 -8 1 18.2899 5.7670 2 -8 2 -1 19.4990 5.4545 1 2 1 8 19.6754 5.3574 3 -1 -2 -8 22.6567 6.9543 1 8 -2 -1 19.6988 6.1149 2 -8 -2 1 18.5452 5.1167 2 -1 -8 2 21.7915 5.6644 2 -8 -1 2 17.2821 5.4134 2 1 2 8 20.3548 5.4376 3 8 -1 -2 17.9888 6.1835 2 -2 -1 -8 23.8726 6.8065 1 -2 1 8 15.9714 4.8942 3 -1 -8 -2 26.7817 5.7002 1 -1 2 -8 22.0476 5.6951 3 -1 8 2 21.1424 4.6410 1 1 -8 2 17.1103 5.6227 2 2 -1 8 15.9449 4.6438 3 2 1 -8 10.0538 4.3525 3 -8 1 -2 19.7496 5.5347 1 -2 8 -1 11.3442 4.2065 1 8 -2 1 18.5673 5.3558 2 -8 -2 2 1075.54 42.27 2 -2 -8 2 988.195 41.431 2 8 -2 2 1026.51 41.77 2 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 98166 _shelx_res_file ; TITL abd1_0m in Pm-3m Eu3SnO at 295K CELL 0.71073 5.0770 5.0770 5.0770 90.000 90.000 90.000 ZERR 1.00 0.0029 0.0029 0.0029 0.000 0.000 0.000 LATT 1 SYMM -X, -Y, Z SYMM -X, Y, -Z SYMM X, -Y, -Z SYMM Z, X, Y SYMM Z, -X, -Y SYMM -Z, -X, Y SYMM -Z, X, -Y SYMM Y, Z, X SYMM -Y, Z, -X SYMM Y, -Z, -X SYMM -Y, -Z, X SYMM Y, X, -Z SYMM -Y, -X, -Z SYMM Y, -X, Z SYMM -Y, X, Z SYMM X, Z, -Y SYMM -X, Z, Y SYMM -X, -Z, -Y SYMM X, -Z, Y SYMM Z, Y, -X SYMM Z, -Y, X SYMM -Z, Y, X SYMM -Z, -Y, -X SFAC O SN EU UNIT 1 1 3 TEMP 25 SIZE 0.02 0.04 0.06 ACTA L.S. 4 BOND FMAP 2 PLAN 20 WGHT 0.017100 0.034000 EXTI 0.095513 FVAR 0.76800 EU1 3 0.500000 0.000000 0.000000 10.06250 0.00971 0.01801 = 0.01801 0.00000 0.00000 0.00000 SN1 2 0.500000 0.500000 0.500000 10.02083 0.01222 0.01222 = 0.01222 0.00000 0.00000 0.00000 O1 1 0.000000 0.000000 0.000000 10.02083 0.01126 0.01126 = 0.01126 0.00000 0.00000 0.00000 HKLF 4 REM abd1_0m in Pm-3m Eu3SnO at 295K REM R1 = 0.0117 for 89 Fo > 4sig(Fo) and 0.0123 for all 93 data REM 6 parameters refined using 0 restraints END WGHT 0.0171 0.0348 REM Highest difference peak 1.097, deepest hole -0.602, 1-sigma level 0.166 Q1 1 0.5000 0.1372 0.0000 10.25000 0.05 1.10 Q2 1 0.3548 0.0000 0.0000 10.12500 0.05 0.91 Q3 1 0.3514 0.5000 0.5000 10.12500 0.05 0.74 Q4 1 0.5000 0.3336 0.0000 10.25000 0.05 0.46 Q5 1 0.5000 0.5000 0.2494 10.12500 0.05 0.31 Q6 1 0.1148 0.5000 0.5000 10.12500 0.05 0.31 Q7 1 0.1254 0.0000 0.0000 10.12500 0.05 0.30 Q8 1 0.3722 0.1413 0.1413 10.50000 0.05 0.28 Q9 1 0.4212 0.2505 0.0000 10.50000 0.05 0.23 Q10 1 0.2721 0.3162 0.5000 10.50000 0.05 0.23 Q11 1 0.2316 0.1608 0.0000 10.50000 0.05 0.22 Q12 1 0.5000 0.0770 0.2532 10.50000 0.05 0.21 Q13 1 0.3412 0.0000 0.2286 10.50000 0.05 0.21 Q14 1 0.2697 0.4311 0.4311 10.50000 0.05 0.20 Q15 1 0.5000 0.1680 0.1680 10.25000 0.05 0.19 Q16 1 0.3564 0.3564 0.3564 10.16667 0.05 0.18 Q17 1 0.5000 0.1521 0.2834 10.50000 0.05 0.18 Q18 1 0.2529 0.0000 0.0475 10.50000 0.05 0.14 Q19 1 0.3217 0.0000 0.1694 10.50000 0.05 0.13 Q20 1 0.4152 0.0000 0.4152 10.25000 0.05 0.07 ; _shelx_res_checksum 1722 _shelxl_version_number 20.13 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' '-x, y, -z' 'x, -y, -z' 'z, x, y' 'z, -x, -y' '-z, -x, y' '-z, x, -y' 'y, z, x' '-y, z, -x' 'y, -z, -x' '-y, -z, x' 'y, x, -z' '-y, -x, -z' 'y, -x, z' '-y, x, z' 'x, z, -y' '-x, z, y' '-x, -z, -y' 'x, -z, y' 'z, y, -x' 'z, -y, x' '-z, y, x' '-z, -y, -x' '-x, -y, -z' 'x, y, -z' 'x, -y, z' '-x, y, z' '-z, -x, -y' '-z, x, y' 'z, x, -y' 'z, -x, y' '-y, -z, -x' 'y, -z, x' '-y, z, x' 'y, z, -x' '-y, -x, z' 'y, x, z' '-y, x, -z' 'y, -x, -z' '-x, -z, y' 'x, -z, -y' 'x, z, y' '-x, z, -y' '-z, -y, x' '-z, y, -x' 'z, -y, -x' 'z, y, x' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Eu Eu1 0.5000 0.0000 0.0000 0.01524(15) Uani d 1 . . Sn Sn1 0.5000 0.5000 0.5000 0.01222(14) Uani d 1 . . O O1 0.0000 0.0000 0.0000 0.0113(7) Uani d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Eu1 0.00971(15) 0.01801(15) 0.01801(15) 0.000 0.000 0.000 Sn1 0.01222(14) 0.01222(14) 0.01222(14) 0.000 0.000 0.000 O1 0.0113(7) 0.0113(7) 0.0113(7) 0.000 0.000 0.000 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Eu Eu -0.1578 3.6682 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle O1 Eu1 O1 1_655 . 180.0 O1 Eu1 Sn1 1_655 . 90.0 O1 Eu1 Sn1 . . 90.0 O1 Eu1 Eu1 1_655 5_545 135.0 O1 Eu1 Eu1 . 5_545 45.0 Sn1 Eu1 Eu1 . 5_545 120.0 O1 Eu1 Sn1 1_655 1_544 90.0 O1 Eu1 Sn1 . 1_544 90.0 Sn1 Eu1 Sn1 . 1_544 180.0 Eu1 Eu1 Sn1 5_545 1_544 60.0 O1 Eu1 Eu1 1_655 9_655 45.0 O1 Eu1 Eu1 . 9_655 135.0 Sn1 Eu1 Eu1 . 9_655 60.0 Eu1 Eu1 Eu1 5_545 9_655 120.0 Sn1 Eu1 Eu1 1_544 9_655 120.0 O1 Eu1 Eu1 1_655 5_655 45.0 O1 Eu1 Eu1 . 5_655 135.0 Sn1 Eu1 Eu1 . 5_655 60.0 Eu1 Eu1 Eu1 5_545 5_655 180.0 Sn1 Eu1 Eu1 1_544 5_655 120.0 Eu1 Eu1 Eu1 9_655 5_655 60.0 O1 Eu1 Eu1 1_655 9_554 135.0 O1 Eu1 Eu1 . 9_554 45.0 Sn1 Eu1 Eu1 . 9_554 120.0 Eu1 Eu1 Eu1 5_545 9_554 60.0 Sn1 Eu1 Eu1 1_544 9_554 60.0 Eu1 Eu1 Eu1 9_655 9_554 180.0 Eu1 Eu1 Eu1 5_655 9_554 120.0 O1 Eu1 Eu1 1_655 5_645 45.0 O1 Eu1 Eu1 . 5_645 135.0 Sn1 Eu1 Eu1 . 5_645 120.0 Eu1 Eu1 Eu1 5_545 5_645 90.0 Sn1 Eu1 Eu1 1_544 5_645 60.0 Eu1 Eu1 Eu1 9_655 5_645 60.0 Eu1 Eu1 Eu1 5_655 5_645 90.0 Eu1 Eu1 Eu1 9_554 5_645 120.0 O1 Eu1 Eu1 1_655 9 135.0 O1 Eu1 Eu1 . 9 45.0 Sn1 Eu1 Eu1 . 9 60.0 Eu1 Eu1 Eu1 5_545 9 60.0 Sn1 Eu1 Eu1 1_544 9 120.0 Eu1 Eu1 Eu1 9_655 9 90.0 Eu1 Eu1 Eu1 5_655 9 120.0 Eu1 Eu1 Eu1 9_554 9 90.0 Eu1 Eu1 Eu1 5_645 9 120.0 O1 Eu1 Eu1 1_655 9_654 45.0 O1 Eu1 Eu1 . 9_654 135.0 Sn1 Eu1 Eu1 . 9_654 120.0 Eu1 Eu1 Eu1 5_545 9_654 120.0 Sn1 Eu1 Eu1 1_544 9_654 60.0 Eu1 Eu1 Eu1 9_655 9_654 90.0 Eu1 Eu1 Eu1 5_655 9_654 60.0 Eu1 Eu1 Eu1 9_554 9_654 90.0 Eu1 Eu1 Eu1 5_645 9_654 60.0 Eu1 Eu1 Eu1 9 9_654 180.0 O1 Eu1 Eu1 1_655 5 135.0 O1 Eu1 Eu1 . 5 45.0 Sn1 Eu1 Eu1 . 5 60.0 Eu1 Eu1 Eu1 5_545 5 90.0 Sn1 Eu1 Eu1 1_544 5 120.0 Eu1 Eu1 Eu1 9_655 5 120.0 Eu1 Eu1 Eu1 5_655 5 90.0 Eu1 Eu1 Eu1 9_554 5 60.0 Eu1 Eu1 Eu1 5_645 5 180.0 Eu1 Eu1 Eu1 9 5 60.0 Eu1 Eu1 Eu1 9_654 5 120.0 Eu1 Sn1 Eu1 9_665 . 120.0 Eu1 Sn1 Eu1 9_665 9 180.0 Eu1 Sn1 Eu1 . 9 60.0 Eu1 Sn1 Eu1 9_665 5_656 60.0 Eu1 Sn1 Eu1 . 5_656 120.0 Eu1 Sn1 Eu1 9 5_656 120.0 Eu1 Sn1 Eu1 9_665 1_566 60.0 Eu1 Sn1 Eu1 . 1_566 180.0 Eu1 Sn1 Eu1 9 1_566 120.0 Eu1 Sn1 Eu1 5_656 1_566 60.0 Eu1 Sn1 Eu1 9_665 5 120.0 Eu1 Sn1 Eu1 . 5 60.0 Eu1 Sn1 Eu1 9 5 60.0 Eu1 Sn1 Eu1 5_656 5 180.0 Eu1 Sn1 Eu1 1_566 5 120.0 Eu1 Sn1 Eu1 9_665 1_565 60.0 Eu1 Sn1 Eu1 . 1_565 90.0 Eu1 Sn1 Eu1 9 1_565 120.0 Eu1 Sn1 Eu1 5_656 1_565 120.0 Eu1 Sn1 Eu1 1_566 1_565 90.0 Eu1 Sn1 Eu1 5 1_565 60.0 Eu1 Sn1 Eu1 9_665 5_556 120.0 Eu1 Sn1 Eu1 . 5_556 120.0 Eu1 Sn1 Eu1 9 5_556 60.0 Eu1 Sn1 Eu1 5_656 5_556 90.0 Eu1 Sn1 Eu1 1_566 5_556 60.0 Eu1 Sn1 Eu1 5 5_556 90.0 Eu1 Sn1 Eu1 1_565 5_556 120.0 Eu1 Sn1 Eu1 9_665 5_655 60.0 Eu1 Sn1 Eu1 . 5_655 60.0 Eu1 Sn1 Eu1 9 5_655 120.0 Eu1 Sn1 Eu1 5_656 5_655 90.0 Eu1 Sn1 Eu1 1_566 5_655 120.0 Eu1 Sn1 Eu1 5 5_655 90.0 Eu1 Sn1 Eu1 1_565 5_655 60.0 Eu1 Sn1 Eu1 5_556 5_655 180.0 Eu1 Sn1 Eu1 9_665 1_556 120.0 Eu1 Sn1 Eu1 . 1_556 90.0 Eu1 Sn1 Eu1 9 1_556 60.0 Eu1 Sn1 Eu1 5_656 1_556 60.0 Eu1 Sn1 Eu1 1_566 1_556 90.0 Eu1 Sn1 Eu1 5 1_556 120.0 Eu1 Sn1 Eu1 1_565 1_556 180.0 Eu1 Sn1 Eu1 5_556 1_556 60.0 Eu1 Sn1 Eu1 5_655 1_556 120.0 Eu1 Sn1 Eu1 9_665 9_655 90.0 Eu1 Sn1 Eu1 . 9_655 60.0 Eu1 Sn1 Eu1 9 9_655 90.0 Eu1 Sn1 Eu1 5_656 9_655 60.0 Eu1 Sn1 Eu1 1_566 9_655 120.0 Eu1 Sn1 Eu1 5 9_655 120.0 Eu1 Sn1 Eu1 1_565 9_655 120.0 Eu1 Sn1 Eu1 5_556 9_655 120.0 Eu1 Sn1 Eu1 5_655 9_655 60.0 Eu1 Sn1 Eu1 1_556 9_655 60.0 Eu1 Sn1 Eu1 9_665 9_565 90.0 Eu1 Sn1 Eu1 . 9_565 120.0 Eu1 Sn1 Eu1 9 9_565 90.0 Eu1 Sn1 Eu1 5_656 9_565 120.0 Eu1 Sn1 Eu1 1_566 9_565 60.0 Eu1 Sn1 Eu1 5 9_565 60.0 Eu1 Sn1 Eu1 1_565 9_565 60.0 Eu1 Sn1 Eu1 5_556 9_565 60.0 Eu1 Sn1 Eu1 5_655 9_565 120.0 Eu1 Sn1 Eu1 1_556 9_565 120.0 Eu1 Sn1 Eu1 9_655 9_565 180.0 Eu1 O1 Eu1 9 . 90.0 Eu1 O1 Eu1 9 1_455 90.0 Eu1 O1 Eu1 . 1_455 180.0 Eu1 O1 Eu1 9 5_545 90.0 Eu1 O1 Eu1 . 5_545 90.0 Eu1 O1 Eu1 1_455 5_545 90.0 Eu1 O1 Eu1 9 5 90.0 Eu1 O1 Eu1 . 5 90.0 Eu1 O1 Eu1 1_455 5 90.0 Eu1 O1 Eu1 5_545 5 180.0 Eu1 O1 Eu1 9 9_554 180.0 Eu1 O1 Eu1 . 9_554 90.0 Eu1 O1 Eu1 1_455 9_554 90.0 Eu1 O1 Eu1 5_545 9_554 90.0 Eu1 O1 Eu1 5 9_554 90.0 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance Eu1 O1 1_655 2.5385(14) Eu1 O1 . 2.5385(14) Eu1 Sn1 . 3.590(2) Eu1 Eu1 5_545 3.590(2) Eu1 Sn1 1_544 3.590(2) Eu1 Eu1 9_655 3.590(2) Eu1 Eu1 5_655 3.590(2) Eu1 Eu1 9_554 3.590(2) Eu1 Eu1 5_645 3.590(2) Eu1 Eu1 9 3.590(2) Eu1 Eu1 9_654 3.590(2) Eu1 Eu1 5 3.590(2) Sn1 Eu1 9_665 3.590(2) Sn1 Eu1 9 3.590(2) Sn1 Eu1 5_656 3.590(2) Sn1 Eu1 1_566 3.590(2) Sn1 Eu1 5 3.590(2) Sn1 Eu1 1_565 3.590(2) Sn1 Eu1 5_556 3.590(2) Sn1 Eu1 5_655 3.590(2) Sn1 Eu1 1_556 3.590(2) Sn1 Eu1 9_655 3.590(2) Sn1 Eu1 9_565 3.590(2) O1 Eu1 9 2.5385(14) O1 Eu1 1_455 2.5385(14) O1 Eu1 5_545 2.5385(14) O1 Eu1 5 2.5385(14) O1 Eu1 9_554 2.5385(14) _cod_database_fobs_code 2023385