#------------------------------------------------------------------------------ #$Date: 2024-11-09 03:47:43 +0100 (Sat, 09 Nov 2024) $ #$Revision: 295856 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/33/2023316.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023316 loop_ _publ_author_name 'Matsuda, Yuki' 'Nakamura, Ryota' 'Ozawa, Yoshiki' 'Abe, Masaaki' _publ_section_title ; Crystal structures of two polymorphs for fac-bromidotricarbonyl[4-(4-methoxyphenyl)-2-(pyridin-2-yl)thiazole-\k2 N,N′]rhenium(I) ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E Crystallographic Communications' _journal_paper_doi 10.1107/S2056989024010727 _journal_volume 80 _journal_year 2024 _chemical_compound_source 'synthesis as described' _chemical_formula_iupac '[Re Br (C15 H12 N2 O1 S) (C O)3]' _chemical_formula_moiety 'C18 H12 Br N2 O4 Re S' _chemical_formula_sum 'C18 H12 Br N2 O4 Re S' _chemical_formula_weight 618.47 _chemical_name_systematic fac-Bromidotricarbonyl[4-(4-methoxyphenyl)-2-(pyridin-2-yl)thiazole-\k^2^N,N']rhenium(I) _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary dual _audit_conform_dict_name cif_core.dic _audit_conform_dict_version 2.4.5 _audit_creation_method 'WinGX routine CIF_UPDATE' _cell_angle_alpha 90 _cell_angle_beta 96.645(7) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 12.7442(6) _cell_length_b 10.6851(6) _cell_length_c 14.4027(6) _cell_measurement_reflns_used 18153 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 29.96 _cell_measurement_theta_min 2.27 _cell_volume 1948.08(17) _computing_cell_refinement ; Rapid-Auto (Rigaku, 2006) ; _computing_data_collection ; Rapid-Auto (Rigaku, 2006) ; _computing_data_reduction ; Rapid-Auto (Rigaku, 2006), SORTAV (Blessing, 1995) ; _computing_molecular_graphics ; PLATON (Spek, 2020) ; _computing_publication_material ; WinGX publication routines (Farrugia, 2012) ; _computing_structure_refinement ; SHELXL2018/3 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2018/2 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 296(2) _diffrn_detector 'curved image-plate' _diffrn_detector_area_resol_mean 10 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device 'fixed-\C diffractometer' _diffrn_measurement_device_type 'Rigaku R-Axis Rapid' _diffrn_measurement_method '\w oscillation scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0353 _diffrn_reflns_av_unetI/netI 0.0319 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_number 22185 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 29.995 _diffrn_reflns_theta_min 2.379 _diffrn_source 'sealed x-ray tube' _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 8.422 _exptl_absorpt_correction_T_max 1 _exptl_absorpt_correction_T_min 0.3732 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (ABSCOR; Higashi, 1995) ; _exptl_crystal_colour 'bright yellowish orange' _exptl_crystal_density_diffrn 2.109 _exptl_crystal_density_method 'not measured' _exptl_crystal_description rhomboid _exptl_crystal_F_000 1168 _exptl_crystal_size_max 0.48 _exptl_crystal_size_mid 0.38 _exptl_crystal_size_min 0.26 _refine_diff_density_max 2.318 _refine_diff_density_min -0.597 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.132 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_constraints 0 _refine_ls_number_parameters 244 _refine_ls_number_reflns 5657 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.132 _refine_ls_R_factor_all 0.0455 _refine_ls_R_factor_gt 0.0341 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0414P)^2^+0.8663P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0747 _refine_ls_wR_factor_ref 0.0786 _reflns_number_gt 4722 _reflns_number_total 5657 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file jp2014.cif _cod_data_source_block polymorph-_a _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 2023316 _shelx_estimated_absorpt_t_min 0.107 _shelx_estimated_absorpt_t_max 0.218 _shelx_hkl_file ; 0 0 2 365.98 4.38 0 0 -2 368.22 4.46 0 0 3 11.59 1.18 0 0 -3 12.85 0.72 0 0 -3 12.53 0.45 0 0 4 9999.00 1189.70 0 0 4 9113.50 1038.94 0 0 -4 9648.32 1161.53 0 0 -4 9784.20 1120.55 0 0 5 2.74 0.98 0 0 -5 6.01 0.97 0 0 -5 4.54 0.36 0 0 6 5168.60 381.37 0 0 6 4769.77 317.26 0 0 -6 4753.55 342.16 0 0 -6 5159.55 347.65 0 0 7 1.18 1.39 0 0 7 1.70 0.60 0 0 -7 1.52 2.22 0 0 -7 2.19 0.77 0 0 8 424.87 8.89 0 0 8 408.38 5.33 0 0 -8 433.00 9.14 0 0 9 -0.92 1.79 0 0 -9 0.60 1.87 0 0 -9 2.00 0.56 0 0 10 1669.44 71.96 0 0 10 1700.20 48.93 0 0 -10 1568.35 60.03 0 0 -10 1559.96 47.18 0 0 11 1.18 2.28 0 0 -11 -1.52 2.35 0 0 12 293.71 8.66 0 0 12 293.32 3.74 0 0 -12 281.82 8.77 0 0 13 8.71 5.10 0 0 13 2.76 0.89 0 0 -13 2.38 3.09 0 0 14 437.29 14.58 0 0 14 439.81 7.05 0 0 -14 433.24 15.39 0 0 15 0.56 3.39 0 0 15 -0.09 0.52 0 0 15 -0.05 0.53 0 0 -15 3.11 3.74 0 0 16 252.47 16.11 0 0 -16 244.06 11.36 0 0 17 -6.84 4.28 0 0 18 -1.21 4.52 0 0 19 -22.82 9.64 0 0 20 38.71 6.80 0 -1 0 -0.16 0.10 0 -1 1 996.00 18.48 0 -1 -1 1037.42 19.51 0 1 2 1654.42 46.05 0 -1 2 1720.83 45.53 0 -1 -2 1591.02 48.10 0 -1 -2 1635.67 44.73 0 1 -2 1708.33 45.92 0 1 3 4105.37 233.61 0 -1 3 3711.81 213.84 0 1 3 4062.53 221.15 0 -1 3 4019.38 215.14 0 -1 -3 4088.97 238.35 0 -1 -3 3936.54 215.12 0 1 4 549.73 10.66 0 -1 4 520.41 8.88 0 1 4 507.53 7.73 0 -1 4 537.05 6.85 0 -1 -4 527.92 8.94 0 -1 -4 514.46 7.89 0 1 5 113.91 2.14 0 -1 5 112.85 2.14 0 -1 5 118.82 1.42 0 1 5 118.15 1.70 0 -1 -5 117.76 2.19 0 1 -5 118.72 2.26 0 1 6 1086.42 28.03 0 -1 6 1090.74 28.36 0 1 6 1118.10 25.43 0 -1 -6 1077.77 28.21 0 1 -6 1077.01 28.40 0 -1 -6 1045.39 23.11 0 1 7 968.12 24.44 0 -1 7 941.62 27.68 0 -1 7 972.62 19.28 0 1 7 943.41 19.27 0 -1 -7 958.35 24.48 0 1 -7 942.56 24.42 0 -1 -7 916.69 20.63 0 1 8 1082.95 30.72 0 -1 8 1065.88 30.34 0 -1 8 1123.52 24.31 0 1 8 1028.73 24.77 0 -1 -8 1055.94 30.46 0 1 -8 1054.30 30.46 0 -1 -8 1118.86 27.79 0 1 9 998.62 27.75 0 -1 9 969.49 26.93 0 -1 9 917.93 17.82 0 1 9 924.15 19.53 0 -1 9 901.77 17.73 0 -1 -9 949.23 27.00 0 1 -9 957.31 27.14 0 -1 -9 974.72 23.24 0 1 10 77.46 3.28 0 -1 10 70.99 3.13 0 1 10 74.19 1.72 0 -1 10 72.34 1.22 0 -1 -10 71.00 3.25 0 1 -10 66.96 3.23 0 -1 -10 73.40 1.42 0 1 11 24.46 2.66 0 -1 11 27.78 4.32 0 -1 11 25.48 0.78 0 -1 -11 26.36 2.81 0 1 -11 25.92 2.76 0 -1 -11 26.34 1.05 0 1 12 166.84 8.63 0 -1 12 155.59 5.48 0 -1 -12 154.50 5.90 0 1 -12 150.49 5.65 0 1 13 738.06 23.83 0 -1 13 742.74 31.46 0 -1 13 734.65 13.01 0 1 13 723.10 15.80 0 -1 -13 750.40 25.33 0 -1 -13 664.43 16.51 0 1 14 14.22 3.59 0 -1 14 21.22 3.63 0 1 14 19.34 1.34 0 -1 -14 13.32 6.47 0 1 15 18.90 3.91 0 -1 15 18.25 4.00 0 1 15 21.04 0.82 0 -1 -15 25.41 4.19 0 1 16 -2.20 6.65 0 -1 16 0.96 6.49 0 -1 -16 5.10 4.09 0 1 17 65.01 6.06 0 -1 17 66.25 5.85 0 -1 -17 66.70 6.51 0 1 18 38.51 5.73 0 -1 18 36.53 9.27 0 -1 -18 33.55 6.36 0 1 19 67.11 6.89 0 -1 19 54.37 6.89 0 -1 20 0.06 5.31 0 -2 0 1280.91 30.25 0 2 0 1296.31 30.52 0 -2 1 756.34 12.59 0 -2 -1 714.36 12.24 0 2 -1 753.47 13.34 0 2 2 5.53 0.84 0 -2 2 3.03 0.39 0 -2 -2 2.42 0.82 0 2 -2 2.59 0.39 0 2 3 30.25 0.70 0 -2 3 30.29 0.50 0 -2 -3 28.56 0.68 0 2 -3 30.00 0.79 0 2 4 4.30 0.94 0 -2 -4 4.82 0.98 0 2 -4 3.51 0.37 0 -2 5 2195.53 103.37 0 2 5 2663.20 105.50 0 -2 5 2821.91 106.41 0 -2 -5 2272.72 105.51 0 -2 -5 2589.74 103.64 0 2 6 933.28 22.30 0 -2 6 866.65 21.46 0 -2 6 897.97 17.56 0 2 6 887.29 18.22 0 -2 -6 930.09 25.80 0 -2 -6 871.83 19.76 0 2 7 53.39 2.12 0 -2 7 56.39 3.30 0 2 7 53.75 1.66 0 -2 7 53.81 0.68 0 -2 -7 55.37 3.47 0 2 8 3.71 1.68 0 -2 8 2.19 2.78 0 -2 8 2.40 0.46 0 2 8 3.06 1.21 0 -2 8 1.47 0.60 0 -2 -8 3.37 1.73 0 -2 -8 0.87 0.74 0 2 9 748.54 18.79 0 -2 9 728.42 18.77 0 -2 9 682.45 12.39 0 2 9 696.31 13.51 0 -2 9 693.54 11.41 0 -2 -9 732.06 19.20 0 -2 -9 702.62 14.01 0 2 10 65.95 3.16 0 -2 10 66.83 3.07 0 2 10 61.04 2.05 0 -2 10 65.08 1.05 0 -2 -10 67.16 5.16 0 -2 -10 64.13 1.46 0 2 11 197.44 6.07 0 -2 11 184.50 5.81 0 -2 -11 191.15 6.09 0 -2 -11 190.69 3.30 0 2 12 184.17 6.40 0 -2 12 172.00 6.11 0 2 12 172.24 3.79 0 -2 12 177.80 1.93 0 -2 -12 183.65 9.80 0 -2 -12 177.53 3.18 0 2 13 3.90 3.07 0 -2 13 6.36 2.89 0 2 13 3.95 0.92 0 -2 -13 10.32 3.22 0 -2 -13 3.88 1.17 0 2 14 3.74 3.30 0 -2 14 5.07 3.26 0 2 14 4.68 0.95 0 -2 -14 3.76 5.93 0 -2 -14 3.86 1.98 0 2 15 175.19 7.82 0 -2 15 167.33 7.51 0 2 15 167.49 3.86 0 -2 -15 174.79 8.40 0 -2 -15 154.58 4.65 0 -2 16 73.84 5.83 0 -2 -16 84.50 10.09 0 -2 17 37.92 5.17 0 -2 -17 45.87 5.76 0 -2 18 49.45 9.94 0 -2 -18 48.79 6.61 0 -2 19 24.62 5.69 0 -2 -19 23.65 6.71 0 -3 0 9.92 0.66 0 3 0 7.93 0.64 0 -3 1 1.17 0.55 0 3 1 1.36 0.62 0 -3 -1 2.83 0.64 0 3 -1 1.34 0.56 0 3 2 93.56 1.99 0 -3 2 91.88 1.75 0 -3 -2 89.78 1.38 0 3 -2 93.16 1.23 0 -3 3 33.54 0.73 0 -3 -3 33.00 0.92 0 3 -3 36.27 1.16 0 3 4 193.84 2.68 0 -3 4 192.36 2.25 0 -3 -4 186.39 2.63 0 3 -4 187.73 2.81 0 3 5 146.58 2.98 0 -3 -5 141.16 2.94 0 -3 -5 139.93 2.12 0 3 -5 142.83 2.23 0 -3 6 5.47 1.53 0 3 6 5.03 1.41 0 -3 6 3.39 0.48 0 -3 -6 5.01 1.44 0 -3 -6 4.25 0.83 0 -3 7 169.28 4.02 0 3 7 171.14 3.71 0 -3 7 178.69 2.04 0 -3 -7 182.80 4.24 0 -3 -7 171.32 2.70 0 -3 8 443.90 10.41 0 -3 8 424.49 7.47 0 3 8 436.80 9.05 0 -3 8 436.87 5.99 0 -3 -8 446.32 10.14 0 -3 -8 414.36 7.27 0 -3 9 30.77 2.47 0 -3 9 31.87 1.28 0 3 9 34.93 1.24 0 -3 9 32.54 0.64 0 -3 -9 37.81 4.23 0 -3 -9 30.67 1.24 0 -3 10 182.49 8.12 0 -3 10 184.90 2.91 0 3 10 173.43 3.03 0 -3 -10 175.45 5.53 0 -3 -10 172.33 3.07 0 -3 11 5.20 2.41 0 -3 11 1.64 0.42 0 3 11 0.49 1.68 0 -3 11 0.16 0.62 0 -3 -11 -2.10 2.55 0 -3 -11 2.38 1.07 0 -3 12 48.85 3.58 0 3 12 48.65 1.51 0 -3 12 47.29 0.82 0 -3 -12 49.42 6.12 0 -3 -12 47.24 1.65 0 -3 13 2.56 3.01 0 3 13 4.34 1.82 0 -3 -13 2.26 3.33 0 -3 -13 2.62 1.32 0 -3 14 215.51 8.52 0 3 14 220.72 4.11 0 -3 -14 221.46 13.92 0 -3 -14 211.05 4.49 0 -3 15 -0.81 6.64 0 3 15 14.09 2.12 0 -3 -15 9.41 4.29 0 -3 -15 13.71 2.62 0 -3 16 -2.93 3.87 0 3 16 1.50 1.97 0 -3 -16 4.67 7.33 0 -3 -16 2.31 2.69 0 -3 17 3.46 4.23 0 -3 -17 4.48 4.83 0 -3 18 68.83 6.92 0 -3 -18 70.38 12.04 0 -3 19 10.65 5.29 0 -3 -19 6.72 5.94 0 -4 0 99.19 2.42 0 4 0 92.04 2.39 0 -4 1 919.85 20.07 0 4 1 941.62 20.73 0 -4 -1 924.94 20.41 0 4 -1 963.39 22.88 0 -4 2 72.61 1.32 0 4 2 72.81 1.49 0 -4 -2 74.17 1.50 0 4 -2 75.50 2.03 0 -4 3 149.58 2.13 0 4 3 152.63 2.51 0 -4 -3 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116.69 7.34 0 -5 -9 114.87 2.93 0 -5 10 1.80 2.76 0 5 10 2.35 2.50 0 -5 -10 1.60 2.78 0 -5 -10 2.63 1.49 0 -5 11 15.50 3.31 0 -5 11 12.95 1.16 0 5 11 16.71 2.81 0 -5 -11 16.66 3.34 0 -5 -11 14.92 1.72 0 -5 12 194.87 7.72 0 -5 12 198.59 2.72 0 5 12 199.58 4.49 0 -5 -12 186.97 7.89 0 -5 -12 189.68 6.68 0 -5 13 92.31 8.53 0 -5 13 78.99 1.35 0 -5 13 79.11 1.14 0 5 13 81.48 2.65 0 -5 -13 77.93 5.44 0 -5 -13 79.87 4.35 0 -5 14 90.05 5.82 0 5 14 86.89 2.87 0 -5 -14 83.08 6.14 0 -5 -14 77.87 4.33 0 -5 15 28.22 4.82 0 5 15 28.90 2.03 0 -5 -15 28.57 8.42 0 -5 -15 23.89 3.42 0 -5 16 15.84 8.15 0 5 16 21.01 2.02 0 -5 -16 25.34 5.36 0 -5 -16 18.46 3.84 0 -5 17 6.75 4.96 0 -5 -17 7.98 5.41 0 -5 -18 35.55 6.67 0 -6 0 2752.64 131.92 0 6 0 2777.59 141.92 0 -6 1 246.97 4.63 0 6 1 247.08 4.88 0 -6 -1 240.73 4.82 0 6 -1 247.78 4.69 0 -6 2 224.84 6.15 0 6 2 226.65 6.75 0 -6 -2 216.04 4.45 0 6 -2 213.98 4.23 0 -6 3 6.56 1.27 0 6 3 7.55 1.54 0 -6 -3 7.80 1.56 0 6 -3 9.87 2.15 0 -6 4 1192.32 34.40 0 6 4 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5 -7 -9 28.42 3.33 5 -7 -9 28.25 2.53 5 7 -9 33.75 1.51 -5 -7 9 30.62 2.19 -5 7 9 36.12 4.03 5 -7 -8 10.19 4.49 5 -7 -8 11.66 3.69 5 7 -8 13.57 2.17 -5 -7 8 12.84 2.12 -5 7 8 10.35 3.53 5 -7 -7 522.29 14.23 5 -7 -7 513.16 13.40 5 7 -7 520.51 13.72 -5 -7 7 507.57 10.71 -5 7 7 517.45 17.20 5 -7 -6 94.36 3.58 5 7 -6 88.40 3.75 5 -7 -6 93.02 3.42 -5 -7 6 94.88 2.50 -5 7 6 103.76 5.30 5 -7 -5 145.77 4.21 5 7 -5 131.49 4.87 5 -7 -5 133.39 6.65 -5 -7 5 139.56 4.87 -5 7 5 135.20 4.15 5 7 -4 1.03 1.52 5 -7 -4 4.64 2.04 -5 -7 4 -0.36 2.46 -5 7 4 0.22 1.89 5 7 -3 393.51 8.63 5 -7 -3 402.63 13.75 -5 -7 3 393.74 11.29 -5 7 3 388.67 9.43 5 7 -2 1.71 1.73 5 -7 -2 3.44 2.12 -5 -7 2 7.99 2.82 -5 7 2 -0.19 3.35 5 7 -1 624.58 15.69 5 -7 -1 650.27 21.89 -5 -7 1 617.29 19.81 -5 7 1 642.22 16.80 5 7 0 10.59 1.96 5 -7 0 7.14 2.20 -5 -7 0 7.58 3.32 -5 7 0 6.54 2.11 5 7 1 17.23 2.27 5 -7 1 15.11 2.37 -5 -7 -1 18.52 2.24 -5 7 -1 16.29 2.35 5 7 2 6.35 3.46 5 -7 2 2.74 3.54 -5 -7 -2 -1.42 2.06 -5 7 -2 3.59 2.06 5 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1.34 5.67 -5 -7 -14 6.63 3.20 5 -7 15 32.10 3.76 5 7 15 27.22 3.57 -5 -7 -15 29.39 7.43 -5 -7 -15 33.17 3.97 5 -7 16 -1.51 5.54 5 7 16 1.67 2.80 -5 -7 -16 -6.03 6.52 -5 -7 -16 0.22 3.35 5 -8 -16 63.33 12.45 5 -8 -16 83.63 6.84 -5 -8 16 64.50 9.57 -5 8 16 67.51 3.58 5 -8 -15 12.70 5.32 5 -8 -15 17.25 4.62 -5 8 15 15.10 4.11 5 -8 -14 35.94 8.85 5 -8 -14 31.12 4.82 -5 -8 14 27.44 7.28 -5 8 14 24.20 2.73 5 -8 -13 17.16 4.35 5 -8 -13 12.95 2.60 -5 -8 13 5.16 6.03 -5 8 13 12.54 2.51 5 -8 -12 14.75 6.90 5 -8 -12 18.01 2.73 -5 -8 12 31.79 9.42 -5 8 12 13.44 4.31 5 -8 -11 14.81 3.79 5 -8 -11 12.31 2.63 5 8 -11 16.11 2.50 -5 -8 11 20.71 5.55 -5 8 11 13.72 4.18 5 -8 -10 199.47 8.03 5 -8 -10 186.72 9.44 5 8 -10 201.62 4.18 -5 -8 10 198.03 5.42 -5 8 10 193.80 5.91 5 -8 -9 86.10 4.81 5 -8 -9 90.99 3.96 5 8 -9 96.23 2.64 -5 -8 9 88.97 3.80 -5 8 9 88.09 3.78 5 -8 -8 49.97 3.70 5 -8 -8 47.05 3.26 5 8 -8 52.20 2.07 -5 -8 8 49.52 2.00 -5 8 8 49.85 3.05 5 -8 -7 21.71 2.90 5 -8 -7 14.74 4.49 5 8 -7 19.73 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14 48.91 3.62 5 -9 -13 44.05 9.43 5 -9 -13 48.02 3.73 -5 -9 13 37.69 7.14 -5 9 13 49.24 3.48 5 -9 -12 119.83 7.29 5 -9 -12 113.05 5.19 -5 -9 12 100.62 9.18 -5 9 12 118.39 7.71 5 -9 -11 10.95 6.74 5 -9 -11 5.83 4.97 5 9 -11 10.92 3.04 -5 -9 11 7.74 2.23 -5 9 11 4.94 4.64 5 -9 -10 26.12 4.03 5 -9 -10 20.58 3.27 5 9 -10 23.02 1.96 -5 -9 10 23.44 1.81 -5 9 10 21.67 3.13 5 -9 -9 61.27 4.51 5 -9 -9 58.81 3.93 5 9 -9 59.92 2.56 -5 -9 9 62.89 2.41 -5 9 9 58.69 3.81 5 -9 -8 178.91 10.85 5 -9 -8 178.01 10.14 5 9 -8 191.62 6.88 -5 -9 8 190.59 4.72 -5 9 8 189.08 6.45 5 -9 -7 57.41 3.85 5 -9 -7 54.83 3.75 5 9 -7 55.38 2.63 -5 -9 7 56.50 3.98 -5 9 7 53.70 3.64 5 -9 -6 67.10 3.88 5 -9 -6 53.38 6.67 5 9 -6 65.08 2.88 -5 -9 6 64.56 2.72 -5 9 6 63.13 6.28 5 -9 -5 8.71 2.86 5 9 -5 6.58 2.00 -5 -9 5 6.43 1.97 -5 9 5 4.53 4.64 5 -9 -4 159.26 9.70 5 9 -4 178.39 7.77 -5 -9 4 170.57 4.85 -5 9 4 170.54 5.90 5 9 -3 69.63 3.27 5 -9 -3 79.58 4.08 -5 -9 3 75.24 3.22 -5 9 3 75.82 3.98 5 9 -2 204.09 5.99 5 -9 -2 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-8 -6 -14 29.38 4.70 8 -6 15 -0.95 4.08 8 -6 15 2.57 2.88 -8 -6 -15 1.58 8.25 -8 -6 -15 6.81 4.14 8 -7 -16 -1.37 4.71 -8 -7 16 1.45 6.79 8 -7 -15 73.14 6.84 8 -7 -15 98.01 7.61 -8 -7 15 90.19 9.85 8 -7 -14 15.71 4.55 8 -7 -14 16.22 4.81 8 -7 -13 165.31 7.99 8 -7 -13 158.48 8.73 -8 -7 13 187.19 12.03 8 -7 -12 -0.50 5.61 8 -7 -12 1.97 4.03 -8 -7 12 -10.48 5.23 -8 7 12 1.38 2.17 8 -7 -11 10.35 3.35 8 -7 -11 13.86 4.40 8 7 -11 10.17 1.36 -8 -7 11 8.60 5.03 -8 7 11 7.94 2.40 8 -7 -10 11.82 5.08 8 -7 -10 13.81 2.63 8 7 -10 8.02 2.40 -8 -7 10 11.94 4.91 -8 -7 10 10.83 2.34 -8 7 10 12.36 2.42 8 -7 -9 282.94 8.67 8 -7 -9 264.00 8.03 -8 -7 9 278.45 8.19 -8 7 9 279.11 7.93 8 -7 -8 8.10 4.24 8 7 -8 7.85 1.56 8 -7 -8 10.49 2.60 -8 -7 8 10.57 1.64 -8 7 8 11.07 2.47 8 -7 -7 120.28 4.31 8 7 -7 125.08 3.37 8 -7 -7 130.73 7.56 -8 -7 7 122.24 3.53 -8 7 7 128.70 4.67 8 -7 -6 21.80 3.84 8 7 -6 22.03 3.26 8 -7 -6 22.07 2.93 -8 -7 6 19.99 2.10 -8 7 6 21.45 2.78 8 -7 -5 278.02 6.79 8 7 -5 275.32 6.89 8 -7 -5 267.15 12.73 -8 -7 5 282.95 10.05 -8 7 5 272.02 8.22 8 -7 -4 57.90 2.42 8 7 -4 57.36 2.83 8 -7 -4 58.35 3.72 -8 -7 4 59.22 2.78 -8 7 4 51.66 3.58 8 -7 -3 482.84 13.72 8 7 -3 467.25 12.50 8 -7 -3 524.30 20.23 -8 -7 3 461.73 12.36 8 -7 -2 4.40 2.45 8 7 -2 10.61 3.86 8 -7 -2 8.20 2.89 -8 -7 2 7.64 2.27 8 -7 -1 2.90 1.34 8 7 -1 1.49 2.39 8 -7 -1 -7.35 4.81 -8 -7 1 2.38 2.34 8 7 0 86.91 3.95 8 -7 0 82.63 4.40 -8 -7 0 82.55 3.88 8 7 1 494.93 14.65 8 -7 1 493.74 15.28 -8 -7 -1 486.92 14.26 8 7 2 0.35 2.73 8 -7 2 4.53 2.80 -8 -7 -2 1.68 2.67 8 7 3 100.54 4.79 8 -7 3 103.68 7.49 -8 -7 -3 94.35 4.72 8 7 4 25.85 3.29 8 -7 4 15.62 3.21 -8 -7 -4 14.83 3.11 8 7 5 16.84 3.60 8 -7 5 24.07 3.33 -8 -7 -5 22.61 6.09 8 -7 6 4.67 2.25 8 7 6 5.93 3.28 8 -7 6 12.33 3.05 -8 -7 -6 8.46 3.36 8 -7 7 162.06 3.66 8 -7 7 168.62 6.65 8 7 7 173.38 7.32 8 -7 7 175.35 6.58 -8 -7 -7 178.35 7.41 8 -7 8 0.34 1.43 8 -7 8 0.06 3.16 8 7 8 5.41 3.38 8 -7 8 1.33 2.85 -8 -7 -8 -2.58 6.99 -8 -7 -8 2.20 3.34 8 -7 9 28.29 1.90 8 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8 -8 -9 -1.22 4.69 8 -8 -9 3.40 4.64 8 8 -9 1.09 1.56 -8 -8 9 1.43 1.63 -8 8 9 -1.98 4.32 8 -8 -8 2.10 2.58 8 8 -8 3.86 1.65 8 -8 -8 6.09 2.69 -8 -8 8 4.72 1.84 -8 8 8 1.01 4.45 8 -8 -7 143.55 4.98 8 8 -7 129.01 3.90 8 -8 -7 136.36 5.62 -8 -8 7 147.88 6.32 -8 8 7 135.87 8.37 8 -8 -6 211.81 6.09 8 8 -6 203.83 8.02 8 -8 -6 204.64 7.29 -8 -8 6 203.17 5.55 -8 8 6 208.67 10.57 8 -8 -5 19.14 2.30 8 8 -5 22.19 2.36 8 -8 -5 16.86 3.37 -8 -8 5 21.75 2.38 -8 8 5 24.92 3.16 8 -8 -4 145.60 6.23 8 8 -4 133.02 7.08 8 -8 -4 138.69 6.01 -8 -8 4 136.56 4.57 -8 8 4 144.04 5.66 8 -8 -3 117.83 3.39 8 8 -3 112.36 4.37 8 -8 -3 115.52 5.39 -8 -8 3 117.74 6.68 -8 8 3 113.11 5.05 8 8 -2 142.22 7.95 8 -8 -2 144.06 6.09 -8 -8 2 139.69 7.65 -8 8 2 139.67 5.70 8 8 -1 82.49 4.02 8 -8 -1 88.22 7.72 -8 -8 1 85.47 6.37 8 8 0 304.51 9.40 8 -8 0 301.78 10.27 -8 -8 0 299.91 13.36 8 8 1 2.63 2.86 8 -8 1 6.00 3.15 -8 -8 -1 1.64 4.83 8 8 2 11.56 3.14 8 -8 2 10.80 3.25 -8 -8 -2 2.47 5.26 8 8 3 102.81 5.09 8 -8 3 97.82 8.25 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25.29 3.38 8 -9 -12 31.14 7.55 8 -9 -12 33.14 3.88 -8 -9 12 27.47 12.23 -8 9 12 32.84 5.82 8 -9 -11 8.42 3.65 8 -9 -11 11.83 5.54 -8 -9 11 10.77 6.14 -8 9 11 7.05 4.99 8 -9 -10 24.06 6.34 8 -9 -10 26.04 3.72 8 9 -10 27.69 2.04 -8 -9 10 23.97 1.92 -8 9 10 24.41 3.37 8 -9 -9 7.08 3.18 8 -9 -9 6.64 3.28 8 9 -9 9.52 1.88 -8 -9 9 8.27 2.05 -8 9 9 3.76 3.03 8 -9 -8 159.62 9.45 8 -9 -8 154.80 10.34 -8 -9 8 154.26 6.81 -8 9 8 146.81 6.21 8 -9 -7 60.53 3.76 8 9 -7 55.33 2.88 8 -9 -7 57.98 4.29 -8 -9 7 58.13 3.01 -8 9 7 57.66 4.09 8 -9 -6 3.39 2.44 8 9 -6 5.10 3.64 8 -9 -6 0.29 5.44 -8 -9 6 4.12 2.22 -8 9 6 2.68 2.98 8 -9 -5 4.18 3.60 8 9 -5 0.03 2.28 8 -9 -5 -0.28 3.21 -8 -9 5 0.36 3.80 -8 9 5 0.23 4.96 8 -9 -4 85.65 3.51 8 9 -4 89.21 6.30 8 -9 -4 80.09 8.30 -8 -9 4 82.36 3.85 -8 9 4 84.90 4.89 8 -9 -3 74.44 3.14 8 9 -3 71.13 3.95 8 -9 -3 75.57 4.89 -8 -9 3 73.19 3.81 -8 9 3 70.87 4.65 8 9 -2 104.40 4.80 8 -9 -2 111.85 5.72 -8 -9 2 106.83 4.65 -8 9 2 111.15 5.44 8 9 -1 133.89 5.57 8 -9 -1 129.33 10.31 -8 -9 1 127.95 5.41 -8 9 1 135.04 6.03 8 9 0 15.62 3.11 8 -9 0 1.59 3.56 -8 -9 0 7.88 3.15 8 9 1 25.48 3.68 8 -9 1 25.24 4.03 -8 -9 -1 24.94 3.62 8 9 2 211.99 8.15 8 -9 2 199.68 8.29 -8 -9 -2 193.55 7.83 8 9 3 203.42 8.28 8 -9 3 193.23 12.76 -8 -9 -3 194.14 12.51 8 9 4 21.53 4.22 8 -9 4 32.81 6.56 -8 -9 -4 25.63 6.96 8 9 5 22.15 4.18 8 -9 5 24.74 6.52 -8 -9 -5 15.97 4.22 8 9 6 122.97 7.01 8 -9 6 117.34 6.11 -8 -9 -6 111.56 6.81 8 9 7 74.26 5.88 8 -9 7 71.38 4.94 -8 -9 -7 73.79 5.74 8 9 8 65.61 5.74 8 -9 8 54.40 7.80 -8 -9 -8 65.90 6.43 -8 -9 -8 62.33 9.94 8 -9 9 47.04 5.19 8 9 9 48.55 5.62 8 -9 9 49.65 7.29 -8 -9 -9 82.57 10.47 -8 -9 -9 53.40 5.74 8 -9 10 6.07 6.85 8 9 10 4.92 4.32 8 -9 10 -1.85 5.57 -8 -9 -10 -2.85 5.30 -8 -9 -10 4.80 4.49 8 -9 11 5.02 4.20 8 9 11 -2.44 7.31 8 -9 11 -0.48 3.22 -8 -9 -11 -4.90 5.71 8 -9 12 39.05 5.55 8 9 12 37.58 5.56 8 -9 12 34.63 4.02 -8 -9 -12 42.66 7.87 -8 -9 -12 31.92 5.60 8 -10 -13 5.00 7.30 8 -10 -13 5.10 3.72 -8 -10 13 -0.91 6.84 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9 -2.38 2.43 -8 11 9 -1.10 3.64 8 -11 -8 71.25 4.77 8 -11 -8 67.84 5.91 8 11 -8 58.35 5.79 -8 -11 8 68.42 3.87 -8 11 8 64.49 5.33 8 -11 -7 8.45 3.34 8 -11 -7 10.79 4.41 8 11 -7 14.24 2.82 -8 -11 7 19.12 4.73 -8 11 7 12.50 3.99 8 -11 -6 11.05 3.11 8 -11 -6 9.69 4.57 8 11 -6 16.37 2.99 -8 -11 6 13.51 3.05 -8 11 6 14.44 4.09 8 -11 -5 -1.65 2.76 8 -11 -5 1.17 6.98 8 11 -5 4.53 2.94 -8 -11 5 0.96 2.87 -8 11 5 -1.06 3.81 8 -11 -4 64.79 6.28 8 11 -4 69.15 4.52 8 -11 -4 73.43 6.00 -8 -11 4 72.66 4.54 -8 11 4 69.94 9.30 8 -11 -3 24.30 2.92 8 11 -3 17.07 3.62 8 -11 -3 23.66 4.59 -8 -11 3 22.76 3.59 -8 11 3 15.68 7.76 8 11 -2 73.21 8.17 8 -11 -2 86.11 9.91 -8 -11 2 67.22 4.90 -8 11 2 64.85 5.95 8 11 -1 6.26 3.64 8 -11 -1 4.39 4.36 -8 -11 1 0.47 3.53 -8 11 1 11.50 4.21 8 11 0 16.02 4.21 8 -11 0 16.68 4.76 -8 -11 0 16.24 4.07 -8 11 0 19.32 4.45 8 11 1 -2.43 3.92 8 -11 1 10.16 4.15 -8 -11 -1 -2.02 3.85 8 11 2 86.09 6.35 8 -11 2 78.48 10.44 -8 -11 -2 84.44 6.08 8 11 3 25.47 7.90 8 -11 3 17.20 7.72 -8 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6.71 9 -9 -12 24.05 4.33 9 -9 -12 17.02 6.52 -9 -9 12 34.41 6.89 9 -9 -11 21.92 6.85 9 -9 -11 31.95 4.08 -9 -9 11 33.69 6.96 -9 9 11 28.11 3.63 9 -9 -10 77.97 4.79 9 -9 -10 64.72 5.05 9 9 -10 72.78 3.10 -9 -9 10 71.23 2.82 -9 9 10 75.96 4.61 9 -9 -9 58.37 6.71 9 -9 -9 64.05 7.61 9 9 -9 55.55 2.82 -9 -9 9 60.00 3.02 -9 9 9 58.52 4.35 9 -9 -8 1.92 2.81 9 -9 -8 2.56 3.46 9 9 -8 6.34 2.07 -9 -9 8 10.47 3.70 -9 9 8 2.43 3.19 9 -9 -7 -1.97 4.33 9 9 -7 6.05 3.76 9 -9 -7 -0.13 5.72 -9 -9 7 4.51 2.37 -9 9 7 4.52 3.23 9 -9 -6 77.81 3.70 9 9 -6 71.71 3.62 9 -9 -6 65.47 5.20 -9 -9 6 69.15 3.76 -9 9 6 70.34 4.75 9 -9 -5 90.24 6.01 9 9 -5 94.77 4.34 9 -9 -5 87.38 9.34 -9 -9 5 91.38 6.56 9 -9 -4 148.15 4.61 9 9 -4 144.04 5.79 9 -9 -4 157.56 7.23 -9 -9 4 142.45 5.43 9 -9 -3 70.92 3.02 9 9 -3 72.61 6.83 9 -9 -3 66.04 5.34 -9 -9 3 63.19 4.05 9 -9 -2 4.21 3.09 9 9 -2 -0.44 3.04 9 -9 -2 -1.14 6.20 -9 -9 2 -0.11 2.92 9 -9 -1 63.92 2.62 9 9 -1 55.98 4.51 9 -9 -1 65.56 5.34 -9 -9 1 57.84 4.40 9 9 0 317.59 11.47 9 -9 0 311.68 12.87 -9 -9 0 315.25 11.40 9 9 1 190.00 12.75 9 -9 1 210.12 13.80 -9 -9 -1 177.09 7.83 9 9 2 10.37 6.63 9 -9 2 14.86 4.24 -9 -9 -2 15.67 3.74 9 9 3 -2.46 3.78 9 -9 3 2.47 3.82 -9 -9 -3 -0.29 3.61 9 9 4 98.41 6.46 9 -9 4 101.42 6.43 -9 -9 -4 89.46 10.14 9 9 5 101.62 6.98 9 -9 5 114.24 6.86 -9 -9 -5 119.63 12.11 9 9 6 55.98 9.63 9 -9 6 66.13 5.42 -9 -9 -6 66.19 6.06 9 9 7 29.50 8.64 9 -9 7 26.03 4.46 -9 -9 -7 31.04 5.26 9 -9 8 -2.47 4.12 9 9 8 -0.16 4.58 9 -9 8 -3.00 3.82 -9 -9 -8 11.23 4.70 -9 -9 -8 -4.97 4.44 9 -9 9 23.92 7.78 9 9 9 10.62 5.11 9 -9 9 9.21 4.11 -9 -9 -9 13.28 5.31 -9 -9 -9 41.90 8.61 9 -9 10 57.07 5.86 9 9 10 49.30 6.28 9 -9 10 45.64 4.99 -9 -9 -10 78.07 11.88 -9 -9 -10 49.89 6.21 9 -9 11 46.29 6.05 9 9 11 42.56 6.29 9 -9 11 51.03 8.02 -9 -9 -11 56.09 13.26 -9 -9 -11 45.60 6.12 9 -10 -12 3.61 4.06 9 -10 -12 8.72 3.96 -9 -10 12 12.82 11.46 -9 10 12 1.85 3.42 9 -10 -11 23.46 4.26 9 -10 -11 25.41 7.47 -9 -10 11 23.06 7.38 -9 10 11 28.28 3.95 9 -10 -10 1.69 3.42 9 -10 -10 -2.48 3.84 9 10 -10 3.90 2.42 -9 10 10 7.59 3.46 9 -10 -9 36.03 4.10 9 -10 -9 34.37 4.76 9 10 -9 36.67 2.85 -9 -10 9 44.88 4.86 -9 10 9 41.45 4.43 9 -10 -8 2.87 3.12 9 -10 -8 10.16 3.93 9 10 -8 4.54 2.42 -9 -10 8 5.14 2.58 -9 10 8 7.47 3.61 9 -10 -7 171.42 6.49 9 -10 -7 153.11 8.36 9 10 -7 152.25 8.55 -9 -10 7 172.35 6.16 -9 10 7 165.08 7.85 9 -10 -6 4.27 2.68 9 -10 -6 -3.43 3.89 9 10 -6 2.52 2.65 -9 -10 6 2.25 4.39 -9 10 6 3.03 3.59 9 -10 -5 7.09 2.54 9 10 -5 2.53 3.00 9 -10 -5 13.47 4.25 -9 -10 5 9.27 2.92 -9 10 5 8.33 3.84 9 -10 -4 0.71 3.94 9 10 -4 1.31 3.05 9 -10 -4 5.13 4.08 -9 -10 4 3.74 2.92 -9 10 4 7.35 3.75 9 -10 -3 179.09 5.55 9 10 -3 172.57 11.33 9 -10 -3 192.66 13.99 -9 -10 3 164.91 7.03 9 -10 -2 16.90 4.06 9 10 -2 21.84 3.76 9 -10 -2 19.66 4.72 -9 -10 2 19.09 3.63 9 -10 -1 132.75 4.28 9 10 -1 134.43 6.87 9 -10 -1 137.31 7.81 -9 -10 1 130.12 6.60 9 10 0 3.09 3.71 9 -10 0 -0.07 4.31 -9 -10 0 7.47 3.61 9 10 1 46.30 8.37 9 -10 1 52.18 9.04 -9 -10 -1 50.96 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39.94 5.53 9 11 -5 36.79 3.94 -9 -11 5 36.07 3.99 -9 11 5 36.97 5.09 9 -11 -4 65.92 6.12 9 -11 -4 63.50 6.17 9 11 -4 65.07 4.66 -9 -11 4 58.12 4.63 -9 11 4 62.97 5.72 9 -11 -3 2.54 2.40 9 11 -3 -2.43 3.42 9 -11 -3 2.49 4.41 -9 -11 3 -0.76 3.30 9 -11 -2 9.72 2.50 9 11 -2 13.50 3.80 9 -11 -2 8.05 4.68 -9 -11 2 8.61 6.25 9 11 -1 27.74 4.38 9 -11 -1 22.67 5.21 -9 -11 1 23.36 7.07 9 11 0 77.41 9.54 9 -11 0 63.83 10.68 -9 -11 0 67.42 9.14 9 11 1 38.45 8.39 9 -11 1 32.72 5.45 -9 -11 -1 28.20 8.11 9 11 2 22.62 4.85 9 -11 2 10.98 5.10 -9 -11 -2 25.44 4.72 9 11 3 1.25 4.53 9 -11 3 -2.42 4.59 -9 -11 -3 -7.93 4.41 9 11 4 15.05 5.17 9 -11 4 16.17 4.93 -9 -11 -4 19.02 4.84 9 11 5 48.14 6.38 9 -11 5 49.66 5.86 -9 -11 -5 53.19 6.07 9 11 6 68.47 7.39 9 -11 6 73.61 6.54 -9 -11 -6 73.60 7.19 9 11 7 -9.04 5.30 9 -11 7 0.04 4.47 -9 -11 -7 0.33 9.10 9 11 8 -0.07 5.37 9 -11 8 3.18 4.31 -9 -11 -8 0.15 6.92 -9 -11 -8 0.48 5.36 9 -12 -7 13.68 3.65 9 -12 -7 19.80 9.10 9 12 -7 13.58 3.40 -9 -12 7 17.71 3.42 -9 12 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2.07 1.24 -10 0 12 3.25 3.25 10 0 -11 2.58 1.38 -10 0 11 4.44 4.90 10 0 -10 565.16 15.36 10 0 -10 531.86 12.35 -10 0 10 553.03 16.37 10 0 -9 1.47 1.53 10 0 -9 1.00 1.53 -10 0 9 2.44 2.22 10 0 -8 71.37 2.54 -10 0 8 71.29 3.01 10 0 -7 1.14 1.66 10 0 -7 0.74 1.69 -10 0 7 1.94 2.86 10 0 -6 159.18 4.20 -10 0 6 157.18 5.28 10 0 -5 -1.21 3.07 -10 0 5 1.79 2.03 10 0 -4 505.40 16.42 -10 0 4 486.59 11.20 10 0 -3 -0.26 3.38 -10 0 3 0.04 1.38 10 0 -2 84.06 5.44 -10 0 2 73.82 1.88 10 0 -1 0.44 2.38 -10 0 1 0.79 0.75 10 0 0 142.22 5.13 10 0 1 1.89 2.47 10 0 2 628.39 18.83 10 0 3 4.12 3.01 10 0 4 51.59 4.07 10 0 5 2.16 3.27 10 0 6 283.23 9.76 10 0 7 -3.09 3.29 10 0 8 123.23 10.03 10 0 9 0.17 3.43 10 0 10 54.50 8.01 10 0 11 5.04 3.65 10 0 12 159.64 12.40 10 0 13 0.57 3.69 10 0 14 3.28 6.49 10 0 15 3.35 3.98 -10 1 17 84.70 8.28 -10 -1 17 85.92 8.83 -10 1 16 2.87 4.93 -10 -1 16 5.93 5.30 -10 1 15 4.69 7.30 -10 -1 15 1.30 8.02 -10 1 14 11.74 4.18 -10 -1 14 18.20 4.46 -10 1 13 180.95 7.81 -10 -1 13 178.40 8.29 10 -1 -12 6.17 2.27 10 1 -12 5.77 0.96 10 -1 -12 7.12 2.35 10 1 -12 6.52 1.13 -10 1 12 5.06 3.17 -10 -1 12 13.10 5.61 10 -1 -11 188.43 4.12 10 -1 -11 192.64 4.39 10 1 -11 201.68 5.56 -10 1 11 189.92 6.74 -10 -1 11 194.06 7.06 10 -1 -10 4.92 1.61 10 1 -10 4.79 2.11 10 -1 -10 7.02 2.72 10 1 -10 6.08 1.40 -10 1 10 -1.40 4.26 -10 -1 10 8.74 2.67 10 -1 -9 107.35 3.05 10 1 -9 96.58 2.62 10 -1 -9 100.75 3.05 10 1 -9 91.51 4.05 -10 1 9 100.91 6.05 -10 -1 9 108.37 6.38 10 -1 -8 -1.96 2.87 10 1 -8 -1.34 1.50 10 -1 -8 2.59 1.68 10 1 -8 -1.68 1.55 -10 1 8 4.03 3.21 -10 -1 8 2.97 2.05 10 -1 -7 533.27 12.82 10 1 -7 513.11 11.95 10 -1 -7 483.32 12.40 -10 1 7 521.53 15.68 -10 -1 7 527.14 12.83 10 -1 -6 85.44 3.10 10 1 -6 82.61 4.35 10 -1 -6 75.11 3.02 -10 1 6 77.66 3.81 -10 -1 6 83.07 4.20 10 -1 -5 25.97 2.32 10 1 -5 28.05 2.21 10 -1 -5 18.87 3.64 -10 1 5 22.80 1.51 -10 -1 5 23.83 1.66 10 -1 -4 5.08 2.11 10 1 -4 4.98 2.02 10 -1 -4 0.47 2.06 -10 1 4 1.02 1.03 -10 -1 4 2.01 2.03 10 -1 -3 375.85 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1 15 29.37 4.83 10 -1 15 32.29 4.49 -10 2 17 4.13 5.55 -10 -2 17 6.40 10.20 -10 2 16 56.01 6.66 -10 -2 16 60.29 7.32 -10 2 15 104.17 11.74 -10 -2 15 108.15 8.10 -10 2 14 119.25 6.91 -10 -2 14 120.47 7.67 10 -2 -13 12.31 1.57 10 -2 -13 12.58 1.70 -10 2 13 11.17 3.73 -10 -2 13 17.69 4.21 10 -2 -12 7.00 2.63 10 2 -12 4.20 1.32 10 -2 -12 0.96 2.71 10 2 -12 2.57 1.58 -10 2 12 4.32 3.17 -10 -2 12 -4.51 6.04 10 -2 -11 97.46 3.00 10 2 -11 98.48 2.18 10 -2 -11 105.44 3.16 10 2 -11 101.22 2.41 -10 2 11 104.04 4.77 -10 -2 11 96.41 5.31 10 -2 -10 321.92 7.40 10 2 -10 317.14 6.19 10 -2 -10 309.80 10.18 -10 2 10 326.18 9.55 -10 -2 10 322.93 10.13 10 -2 -9 195.06 4.97 10 2 -9 200.33 4.25 10 -2 -9 186.35 7.27 -10 2 9 211.97 5.99 -10 -2 9 210.23 6.53 10 -2 -8 124.09 3.76 10 2 -8 127.04 3.21 10 -2 -8 128.50 5.97 -10 2 8 136.71 4.12 -10 -2 8 136.16 4.57 10 -2 -7 33.49 3.82 10 2 -7 33.54 2.00 10 -2 -7 37.37 3.99 -10 2 7 38.95 2.22 -10 -2 7 37.85 2.50 10 -2 -6 190.67 7.80 10 2 -6 197.38 7.04 10 -2 -6 198.09 8.00 -10 2 6 219.82 6.64 -10 -2 6 208.46 5.03 10 -2 -5 465.04 16.02 10 2 -5 436.30 11.00 10 -2 -5 460.13 12.18 -10 -2 5 488.07 10.97 10 -2 -4 874.90 32.84 10 2 -4 845.92 24.91 10 -2 -4 850.84 26.03 -10 -2 4 928.60 28.17 10 -2 -3 106.55 4.05 10 2 -3 107.02 3.68 10 -2 -3 97.63 4.04 -10 -2 3 112.44 2.59 -10 -2 3 116.17 4.07 10 -2 -2 56.77 3.34 10 2 -2 55.15 3.04 10 -2 -2 48.41 3.25 -10 -2 2 55.47 1.69 -10 -2 2 57.78 3.19 10 -2 -1 163.70 5.50 10 2 -1 155.14 4.99 10 -2 -1 158.02 5.47 -10 -2 1 167.39 8.36 10 -2 0 596.36 17.43 10 2 0 566.81 16.25 -10 -2 0 591.22 17.14 10 -2 1 262.55 11.74 10 2 1 259.69 7.69 -10 -2 -1 257.71 8.00 10 -2 2 125.15 5.31 10 2 2 125.64 5.16 -10 -2 -2 120.74 5.12 10 -2 3 11.08 3.15 10 2 3 16.58 3.20 -10 -2 -3 12.26 0.95 -10 -2 -3 13.03 3.14 10 -2 4 163.16 10.70 10 2 4 171.01 10.81 -10 -2 -4 164.00 2.64 -10 -2 -4 168.77 6.54 10 -2 5 135.84 5.92 10 2 5 125.57 5.73 -10 -2 -5 120.73 2.17 -10 -2 -5 120.45 5.60 10 -2 6 166.85 10.88 10 2 6 140.40 6.30 -10 -2 -6 152.11 2.80 -10 -2 -6 157.55 6.53 10 -2 7 234.05 8.55 10 2 7 205.02 8.26 -10 -2 -7 208.03 3.99 -10 -2 -7 212.89 8.41 10 -2 8 7.16 6.36 10 2 8 11.81 6.01 -10 -2 -8 7.91 6.24 10 -2 9 4.02 3.83 10 2 9 2.05 3.59 -10 -2 -9 4.23 1.47 -10 -2 -9 1.03 3.71 10 -2 10 125.15 11.26 10 2 10 113.33 6.45 -10 -2 -10 110.34 4.87 -10 -2 -10 126.18 6.63 10 -2 11 142.46 7.36 10 2 11 124.46 7.14 -10 -2 -11 126.70 3.81 -10 -2 -11 131.90 7.09 10 -2 12 17.59 7.16 10 2 12 20.40 4.35 10 -2 12 16.89 3.83 -10 -2 -12 19.27 3.66 10 -2 13 7.78 4.04 10 2 13 9.02 4.09 10 -2 13 -0.28 3.65 -10 -2 -13 2.69 2.19 10 -2 14 7.74 4.13 10 2 14 14.50 4.22 10 -2 14 2.70 6.40 -10 -2 -14 9.97 2.55 10 -2 15 25.26 7.13 10 2 15 22.84 4.65 10 -2 15 16.27 4.01 -10 -3 17 23.09 6.99 -10 -3 16 85.02 13.83 10 -3 -15 0.95 4.07 -10 -3 15 5.37 5.05 10 -3 -14 56.75 5.05 -10 -3 14 76.61 10.44 10 -3 -13 16.06 3.61 10 -3 -13 19.19 1.96 10 -3 -13 21.61 3.34 -10 3 13 20.69 4.05 -10 -3 13 19.09 4.61 10 -3 -12 482.95 15.93 10 -3 -12 490.72 15.66 10 -3 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10 -3 -3 44.10 3.19 -10 -3 3 46.03 2.90 10 -3 -2 1246.92 44.40 10 3 -2 1177.82 41.50 10 -3 -2 1201.25 52.76 -10 -3 2 1259.71 52.67 10 -3 -1 37.04 3.20 10 3 -1 31.87 2.81 10 -3 -1 36.41 3.08 -10 -3 1 32.49 3.05 10 -3 0 133.49 5.15 10 3 0 126.52 4.72 10 -3 0 130.54 5.28 -10 -3 0 134.64 5.01 10 -3 1 7.13 4.90 10 3 1 4.53 2.60 10 -3 1 3.72 4.78 -10 -3 -1 4.92 2.74 10 -3 2 642.09 20.15 10 3 2 620.55 19.05 10 -3 2 607.41 19.44 -10 -3 -2 632.54 19.74 10 -3 3 13.71 3.36 10 3 3 8.45 5.29 10 -3 3 12.40 3.16 -10 -3 -3 14.83 3.19 10 -3 4 563.95 24.64 10 3 4 543.45 24.05 10 -3 4 521.79 17.14 -10 -3 -4 544.30 17.81 10 -3 5 49.72 4.34 10 3 5 48.78 4.24 10 -3 5 40.71 4.06 -10 -3 -5 55.25 3.11 -10 -3 -5 48.92 4.25 10 -3 6 26.59 6.88 10 3 6 32.11 4.00 10 -3 6 24.68 3.59 -10 -3 -6 30.69 1.75 -10 -3 -6 33.13 3.98 10 -3 7 3.37 3.48 10 3 7 1.82 3.41 10 -3 7 1.32 3.11 -10 -3 -7 0.65 1.46 -10 -3 -7 -1.46 5.77 10 -3 8 381.86 19.44 10 3 8 334.32 12.33 10 -3 8 318.19 11.45 -10 -3 -8 334.59 7.68 -10 -3 -8 328.53 18.70 10 -3 9 35.26 4.66 10 3 9 44.80 4.59 10 -3 9 39.59 4.03 -10 -3 -9 41.76 2.27 -10 -3 -9 37.61 4.60 10 -3 10 1.21 7.07 10 3 10 14.41 4.12 10 -3 10 15.24 5.93 -10 -3 -10 12.92 2.09 -10 -3 -10 14.75 4.07 10 -3 11 2.59 4.02 10 3 11 -5.18 3.88 10 -3 11 -2.93 5.56 -10 -3 -11 3.02 3.41 -10 -3 -11 0.08 6.61 10 -3 12 59.63 5.41 10 3 12 54.90 5.44 10 -3 12 51.90 4.56 -10 -3 -12 53.84 3.13 -10 -3 -12 60.10 5.47 10 -3 13 -3.60 6.76 10 3 13 0.03 6.92 10 -3 13 3.81 3.50 -10 -3 -13 5.39 2.51 -10 -3 -13 3.20 4.17 10 -3 14 75.18 5.95 10 3 14 70.62 6.06 10 -3 14 64.20 8.32 -10 -3 -14 60.82 6.11 10 -4 -17 9.90 5.12 -10 -4 17 4.09 6.63 10 -4 -16 17.91 4.94 -10 -4 16 14.20 6.42 10 -4 -15 153.67 13.22 -10 -4 15 162.69 10.89 10 -4 -14 25.52 6.71 -10 -4 14 20.62 5.58 10 -4 -13 69.52 4.80 10 -4 -13 65.33 4.48 10 -4 -13 80.59 3.38 -10 -4 13 84.32 6.60 10 -4 -12 -0.44 2.92 10 -4 -12 3.76 1.84 10 -4 -12 4.42 3.38 -10 -4 12 6.81 4.09 10 -4 -11 256.90 8.29 10 4 -11 269.57 6.34 10 -4 -11 282.89 10.51 -10 -4 11 295.53 11.02 10 -4 -10 61.35 5.61 10 4 -10 70.85 2.10 10 -4 -10 69.75 5.20 -10 -4 10 79.10 4.96 10 -4 -9 430.52 11.39 10 4 -9 464.42 10.12 10 -4 -9 432.57 16.19 -10 -4 9 495.25 15.72 10 -4 -8 9.10 1.84 10 4 -8 11.06 1.69 10 -4 -8 11.57 3.91 -10 -4 8 7.49 5.04 10 -4 -7 13.92 1.73 10 4 -7 13.23 3.04 10 -4 -7 13.10 2.49 -10 -4 7 16.87 2.72 -10 -4 7 13.56 3.36 10 -4 -6 102.86 2.69 10 4 -6 107.38 3.35 10 -4 -6 104.31 4.18 -10 -4 6 108.37 4.23 -10 -4 6 103.47 3.54 10 -4 -5 666.62 15.02 10 4 -5 694.13 23.31 10 -4 -5 696.71 26.83 -10 -4 5 649.97 23.41 10 -4 -4 114.79 2.22 10 4 -4 116.98 3.91 10 -4 -4 113.82 4.70 -10 -4 4 113.40 4.02 10 -4 -3 147.27 3.21 10 4 -3 148.56 4.69 10 -4 -3 158.36 5.37 -10 -4 3 151.99 4.76 10 -4 -2 -2.03 2.55 10 4 -2 -1.63 2.21 10 -4 -2 5.08 2.58 -10 -4 2 -4.99 3.76 10 -4 -1 132.37 5.12 10 4 -1 124.79 7.06 10 -4 -1 126.67 8.23 -10 -4 1 124.99 4.59 10 -4 0 223.02 7.26 10 4 0 214.17 9.98 10 -4 0 216.71 7.35 -10 -4 0 210.24 6.78 10 -4 1 666.16 28.08 10 4 1 611.46 25.30 10 -4 1 656.97 21.25 -10 -4 -1 617.23 19.13 10 -4 2 -0.29 3.13 10 4 2 3.37 4.65 10 -4 2 4.02 3.04 -10 -4 -2 6.38 2.81 10 -4 3 0.62 3.11 10 4 3 3.61 3.03 10 -4 3 4.45 5.18 -10 -4 -3 7.04 2.98 10 -4 4 95.71 5.41 10 4 4 100.85 5.11 10 -4 4 97.13 5.09 -10 -4 -4 90.34 5.06 10 -4 5 428.80 14.34 10 4 5 417.80 13.96 10 -4 5 377.49 12.75 -10 -4 -5 386.41 13.28 10 -4 6 87.26 8.77 10 4 6 101.70 5.51 10 -4 6 91.59 5.09 -10 -4 -6 100.30 3.45 -10 -4 -6 88.93 5.31 10 -4 7 162.84 7.43 10 4 7 153.84 11.98 -10 -4 -7 161.59 6.74 -10 -4 -7 153.67 11.77 10 -4 8 7.60 6.36 10 4 8 12.21 3.93 10 -4 8 12.32 3.42 -10 -4 -8 11.03 3.48 -10 -4 -8 11.86 3.96 10 -4 9 45.37 4.84 10 4 9 46.68 4.86 10 -4 9 38.07 6.84 -10 -4 -9 46.42 4.45 -10 -4 -9 39.82 4.82 10 -4 10 54.74 4.97 10 4 10 50.25 5.09 10 -4 10 45.08 7.00 -10 -4 -10 43.49 4.78 -10 -4 -10 41.46 5.00 10 -4 11 140.87 7.64 10 4 11 127.06 7.66 10 -4 11 121.15 6.29 -10 -4 -11 130.99 4.74 -10 -4 -11 123.67 11.96 10 -4 12 4.54 4.30 10 4 12 7.44 4.26 10 -4 12 1.73 3.42 -10 -4 -12 4.83 2.57 -10 -4 -12 4.18 4.14 10 -4 13 9.09 7.38 10 4 13 21.58 7.77 10 -4 13 12.06 3.76 -10 -4 -13 15.00 2.92 -10 -4 -13 6.08 4.61 10 -4 14 11.52 4.60 10 4 14 8.17 4.68 10 -4 14 10.65 6.12 -10 -4 -14 13.76 5.03 -10 -4 -14 11.30 4.72 10 -5 -16 17.07 4.68 -10 -5 16 -1.21 6.55 10 -5 -15 9.37 4.25 -10 -5 15 8.24 9.57 10 -5 -14 11.74 4.03 10 -5 -14 12.72 2.14 10 -5 -14 19.40 4.57 -10 -5 14 19.84 5.48 10 -5 -13 88.55 8.73 10 -5 -13 93.77 4.01 -10 -5 13 88.83 11.91 10 -5 -12 73.23 4.60 10 -5 -12 80.35 3.59 -10 -5 12 80.44 6.42 10 -5 -11 46.95 3.53 10 5 -11 43.61 2.65 10 -5 -11 47.25 3.09 -10 -5 11 48.23 8.39 10 -5 -10 1.44 4.01 10 5 -10 0.80 2.22 10 -5 -10 4.74 2.34 -10 -5 10 11.68 3.69 10 -5 -9 40.40 2.71 10 5 -9 47.08 3.14 10 -5 -9 39.60 3.06 -10 -5 9 46.56 4.15 -10 -5 9 46.78 2.38 10 5 -8 69.15 4.00 10 -5 -8 69.43 5.78 -10 -5 8 88.50 7.18 -10 -5 8 74.09 2.86 10 -5 -7 268.25 6.07 10 5 -7 297.75 6.93 10 -5 -7 271.45 8.27 -10 -5 7 292.56 9.12 -10 -5 7 273.03 9.68 10 -5 -6 128.47 4.58 10 5 -6 143.44 6.16 10 -5 -6 138.08 5.14 -10 -5 6 139.51 4.20 10 -5 -5 2.39 2.14 10 5 -5 5.97 2.03 10 -5 -5 0.28 4.47 -10 -5 5 4.24 2.05 10 -5 -4 6.98 1.12 10 5 -4 8.76 3.69 10 -5 -4 4.65 2.84 -10 -5 4 10.51 2.21 10 -5 -3 479.43 8.84 10 5 -3 503.81 13.49 10 -5 -3 511.39 20.89 -10 -5 3 480.31 13.09 10 -5 -2 117.10 1.83 10 5 -2 123.34 4.45 10 -5 -2 121.89 5.24 -10 -5 2 108.73 6.75 10 -5 -1 168.62 2.73 10 5 -1 180.68 5.72 10 -5 -1 181.48 6.50 -10 -5 1 169.94 5.58 10 5 0 89.44 4.13 10 -5 0 81.44 4.61 -10 -5 0 83.04 4.09 10 -5 1 139.05 5.70 10 5 1 133.45 5.27 10 -5 1 137.66 5.83 -10 -5 -1 129.58 5.31 10 -5 2 25.58 3.63 10 5 2 21.90 3.25 10 -5 2 26.82 3.71 -10 -5 -2 24.67 3.18 10 -5 3 236.44 12.74 10 5 3 223.90 8.11 10 -5 3 232.00 8.26 -10 -5 -3 218.14 8.01 10 -5 4 122.44 6.02 10 5 4 119.77 5.86 10 -5 4 128.02 9.07 -10 -5 -4 120.17 5.63 10 -5 5 15.84 3.74 10 5 5 22.63 3.64 10 -5 5 7.79 5.85 -10 -5 -5 10.18 5.94 10 -5 6 14.62 3.93 10 5 6 12.89 3.77 10 -5 6 6.33 5.96 -10 -5 -6 19.09 3.38 -10 -5 -6 13.91 6.23 10 -5 7 112.38 6.53 10 5 7 120.93 10.34 10 -5 7 108.81 9.37 -10 -5 -7 136.25 8.01 -10 -5 -7 104.75 6.31 10 -5 8 40.23 4.79 10 5 8 46.82 4.96 10 -5 8 45.76 7.13 -10 -5 -8 52.51 5.54 -10 -5 -8 41.31 4.71 10 -5 9 114.60 6.64 10 5 9 106.49 6.77 10 -5 9 97.10 9.03 -10 -5 -9 109.63 7.31 -10 -5 -9 99.10 6.44 10 -5 10 90.21 6.16 10 5 10 80.84 6.26 10 -5 10 72.25 5.17 -10 -5 -10 77.50 6.60 -10 -5 -10 75.07 10.35 10 -5 11 12.97 7.00 10 5 11 12.30 7.41 10 -5 11 5.63 3.51 -10 -5 -11 6.86 2.90 -10 -5 -11 10.81 4.39 10 -5 12 3.25 4.23 10 5 12 0.23 4.41 10 -5 12 3.25 3.44 -10 -5 -12 1.17 2.88 -10 -5 -12 6.40 4.28 10 -5 13 67.49 6.28 10 5 13 63.86 6.27 10 -5 13 52.75 7.98 -10 -5 -13 55.95 4.32 -10 -5 -13 58.91 10.16 10 -6 -15 11.75 4.38 -10 -6 15 -0.46 6.13 10 -6 -14 60.58 5.40 10 -6 -14 65.40 4.17 -10 -6 14 52.74 12.47 10 -6 -13 7.22 3.55 10 -6 -13 2.12 4.47 -10 -6 13 5.00 5.04 10 -6 -12 9.32 3.17 10 -6 -12 18.26 4.54 -10 -6 12 5.18 4.91 10 -6 -11 3.56 2.76 10 6 -11 4.53 2.31 10 -6 -11 0.25 2.52 -10 -6 11 -1.17 4.25 10 -6 -10 150.79 5.47 10 -6 -10 148.29 5.64 -10 -6 10 165.70 7.93 -10 -6 10 161.16 4.12 10 -6 -9 5.11 3.76 10 6 -9 4.14 1.58 10 -6 -9 3.32 2.66 -10 -6 9 3.77 5.95 -10 -6 9 4.22 1.77 10 -6 -8 47.46 2.71 10 6 -8 50.46 2.34 10 -6 -8 48.48 3.49 -10 -6 8 49.87 4.39 -10 -6 8 41.12 2.46 10 -6 -7 9.36 1.92 10 6 -7 14.92 3.31 10 -6 -7 9.23 2.83 -10 -6 7 9.37 3.31 10 -6 -6 140.67 5.32 10 6 -6 148.52 4.47 10 -6 -6 144.81 5.75 -10 -6 6 141.96 4.40 10 6 -5 34.68 2.65 10 -6 -5 35.85 5.77 -10 -6 5 28.45 4.18 10 -6 -4 211.00 5.70 10 6 -4 238.33 6.64 10 -6 -4 235.51 7.90 -10 -6 4 217.26 6.34 10 -6 -3 59.88 2.51 10 6 -3 59.41 5.44 10 -6 -3 58.18 6.75 -10 -6 3 53.32 3.21 10 -6 -2 4.04 0.94 10 6 -2 6.24 2.54 10 -6 -2 7.47 3.13 -10 -6 2 6.23 2.50 10 -6 -1 0.02 1.24 10 6 -1 2.95 2.53 10 -6 -1 0.05 3.08 -10 -6 1 9.15 4.26 10 -6 0 187.92 3.38 10 6 0 184.48 6.60 10 -6 0 204.76 11.42 -10 -6 0 188.98 9.73 10 -6 1 35.06 0.74 10 6 1 37.34 3.46 10 -6 1 41.69 3.97 -10 -6 -1 32.13 5.63 10 6 2 100.90 5.09 10 -6 2 106.44 5.90 -10 -6 -2 95.96 7.97 10 -6 3 35.24 4.07 10 6 3 39.20 3.93 10 -6 3 36.80 4.36 -10 -6 -3 38.23 6.35 10 -6 4 20.61 3.87 10 6 4 17.33 3.80 10 -6 4 21.11 3.87 -10 -6 -4 14.75 3.75 10 -6 5 8.43 6.13 10 6 5 4.34 3.61 10 -6 5 2.15 5.96 -10 -6 -5 3.36 3.45 10 -6 6 161.55 7.83 10 6 6 166.38 7.86 10 -6 6 171.41 11.62 -10 -6 -6 159.30 7.70 10 -6 7 60.37 8.74 10 6 7 71.88 8.94 10 -6 7 58.56 8.03 -10 -6 -7 65.51 5.28 10 -6 8 30.23 4.81 10 6 8 32.18 4.91 10 -6 8 33.27 7.06 -10 -6 -8 52.82 7.85 -10 -6 -8 30.38 7.74 10 -6 9 8.27 4.12 10 6 9 12.85 4.42 10 -6 9 3.56 3.73 -10 -6 -9 11.64 6.56 -10 -6 -9 9.62 4.29 10 -6 10 62.14 5.63 10 6 10 55.53 5.86 10 -6 10 46.26 4.87 -10 -6 -10 61.62 7.96 -10 -6 -10 49.95 5.60 10 -6 11 19.91 4.56 10 6 11 14.69 8.04 10 -6 11 13.02 3.85 -10 -6 -11 15.10 6.10 -10 -6 -11 11.25 4.64 10 -6 12 68.10 9.90 10 6 12 66.90 6.45 10 -6 12 55.27 5.13 -10 -6 -12 59.20 5.02 -10 -6 -12 74.17 10.69 10 -6 13 7.56 4.83 10 6 13 16.50 5.06 10 -6 13 5.86 6.59 -10 -6 -13 10.95 3.77 -10 -6 -13 7.21 5.10 10 -7 -15 2.14 4.39 10 -7 -14 0.42 6.66 10 -7 -14 2.90 3.22 -10 -7 14 6.05 5.91 10 -7 -13 53.70 4.88 10 -7 -13 56.32 4.18 -10 -7 13 61.44 7.41 10 -7 -12 -3.23 3.24 10 -7 -12 6.49 2.95 -10 -7 12 0.72 5.01 10 -7 -11 76.08 4.42 10 -7 -11 66.29 4.20 -10 -7 11 74.33 6.82 10 -7 -10 -0.20 2.68 10 7 -10 0.65 2.70 10 -7 -10 2.92 4.69 -10 -7 10 0.65 6.99 -10 -7 10 4.63 2.90 10 -7 -9 17.18 4.56 10 7 -9 16.71 1.97 10 -7 -9 18.83 3.25 -10 -7 9 23.25 4.47 -10 -7 9 17.79 2.06 10 -7 -8 5.27 2.19 10 7 -8 2.51 3.15 10 -7 -8 2.25 2.98 -10 -7 8 1.98 1.97 10 -7 -7 158.83 4.52 10 7 -7 152.26 6.97 10 -7 -7 142.98 9.83 -10 -7 7 149.87 6.86 10 -7 -6 5.95 3.06 10 7 -6 3.50 2.25 10 -7 -6 7.60 3.15 -10 -7 6 3.87 2.20 10 -7 -5 26.44 1.90 10 7 -5 21.17 4.53 10 -7 -5 26.94 6.16 -10 -7 5 24.89 4.45 10 7 -4 5.94 2.49 10 -7 -4 5.05 3.27 -10 -7 4 0.68 2.34 10 -7 -3 40.45 1.78 10 7 -3 40.64 3.33 10 -7 -3 47.20 6.79 -10 -7 3 37.41 3.14 10 -7 -2 -0.71 1.93 10 7 -2 -2.36 4.59 10 -7 -2 7.21 3.29 -10 -7 2 4.50 2.60 10 -7 -1 230.42 4.19 10 7 -1 233.64 7.81 10 -7 -1 226.59 8.98 -10 -7 1 230.66 7.68 10 -7 0 1.80 1.55 10 7 0 4.28 2.99 10 -7 0 -3.39 5.85 -10 -7 0 5.79 2.93 10 -7 1 2.31 1.38 10 7 1 0.86 3.12 10 -7 1 0.03 3.60 -10 -7 -1 3.74 3.11 10 -7 2 1.01 0.75 10 7 2 -0.30 3.28 10 -7 2 0.27 3.50 -10 -7 -2 -2.22 3.22 10 -7 3 222.47 3.41 10 7 3 227.67 8.99 10 -7 3 238.51 9.90 -10 -7 -3 220.52 8.73 10 7 4 -0.03 3.65 10 -7 4 0.48 3.84 -10 -7 -4 1.73 3.59 10 -7 5 98.68 6.45 10 7 5 105.30 6.53 10 -7 5 110.99 6.40 -10 -7 -5 97.90 6.28 10 -7 6 -2.45 6.42 10 7 6 2.97 3.94 10 -7 6 3.27 3.67 -10 -7 -6 1.55 3.82 10 -7 7 38.21 4.91 10 7 7 47.44 8.55 10 -7 7 37.43 4.59 -10 -7 -7 33.93 8.50 10 -7 8 7.79 6.86 10 7 8 11.89 7.34 10 -7 8 -0.24 3.76 -10 -7 -8 -6.12 5.21 -10 -7 -8 2.35 4.11 10 -7 9 105.19 7.12 10 7 9 107.34 7.53 10 -7 9 106.52 6.44 -10 -7 -9 98.16 7.15 10 -7 10 -3.54 7.12 10 7 10 2.27 4.62 10 -7 10 1.84 3.68 -10 -7 -10 -0.96 5.30 -10 -7 -10 19.25 7.46 10 -7 11 8.43 4.74 10 7 11 9.81 4.97 10 -7 11 10.43 3.90 -10 -7 -11 13.64 8.82 -10 -7 -11 9.94 4.87 10 -7 12 -1.07 4.62 10 -7 12 3.22 3.77 -10 -7 -12 -5.60 8.01 -10 -7 -12 4.35 4.67 10 -8 -14 63.07 5.82 10 -8 -14 59.04 7.27 10 -8 -13 -4.00 6.18 10 -8 -13 -2.53 5.71 -10 -8 13 8.90 5.98 10 -8 -12 -3.35 3.46 10 -8 -12 3.65 5.45 -10 -8 12 5.34 5.57 10 -8 -11 1.55 3.23 10 -8 -11 6.07 3.32 -10 -8 11 -1.06 5.01 10 -8 -10 160.67 6.23 10 8 -10 151.49 6.47 10 -8 -10 150.06 6.79 -10 -8 10 148.64 6.52 10 -8 -9 9.16 2.78 10 8 -9 9.40 3.38 10 -8 -9 5.83 5.52 -10 -8 9 9.85 1.96 10 -8 -8 51.85 5.49 10 8 -8 61.91 4.82 10 -8 -8 54.91 4.61 -10 -8 8 56.25 3.06 10 -8 -7 7.81 2.30 10 8 -7 6.69 2.34 10 -8 -7 1.64 3.50 -10 -8 7 8.89 2.34 10 -8 -6 69.41 4.84 10 8 -6 65.96 3.61 10 -8 -6 66.09 5.00 -10 -8 6 65.04 3.47 10 -8 -5 22.39 2.22 10 8 -5 24.79 2.93 10 -8 -5 21.92 4.04 -10 -8 5 18.48 2.77 10 -8 -4 183.21 6.77 10 8 -4 183.42 6.56 10 -8 -4 188.18 8.12 -10 -8 4 182.16 6.21 10 -8 -3 24.74 1.93 10 8 -3 25.25 3.36 10 -8 -3 25.24 6.95 -10 -8 3 34.24 5.38 10 -8 -2 4.66 2.50 10 8 -2 4.31 3.10 10 -8 -2 5.13 3.92 -10 -8 2 2.48 5.15 10 -8 -1 18.72 1.56 10 8 -1 24.44 6.00 10 -8 -1 18.66 4.31 -10 -8 1 15.54 3.55 10 -8 0 192.86 5.45 10 8 0 196.03 7.95 10 -8 0 197.02 14.02 -10 -8 0 190.93 8.06 10 -8 1 16.09 2.21 10 8 1 25.02 3.88 10 -8 1 12.47 4.21 -10 -8 -1 17.09 3.91 10 -8 2 152.37 3.03 10 8 2 154.62 7.44 10 -8 2 144.74 7.76 -10 -8 -2 143.54 7.38 10 8 3 2.09 3.84 10 -8 3 -2.04 4.09 -10 -8 -3 4.40 6.37 10 8 4 57.57 5.69 10 -8 4 60.25 5.73 -10 -8 -4 54.18 9.12 10 8 5 13.14 4.46 10 -8 5 6.44 4.29 -10 -8 -5 12.53 4.26 10 -8 6 96.20 6.71 10 8 6 93.81 7.07 10 -8 6 97.70 6.42 -10 -8 -6 92.12 6.78 10 -8 7 17.70 8.07 10 8 7 27.56 5.16 10 -8 7 23.78 4.61 -10 -8 -7 34.60 5.15 10 -8 8 6.35 4.47 10 -8 8 10.70 4.06 -10 -8 -8 11.08 8.22 -10 -8 -8 0.45 4.61 10 -8 9 2.24 7.33 10 8 9 -1.99 4.68 10 -8 9 0.94 3.90 -10 -8 -9 -0.02 9.67 -10 -8 -9 -0.56 4.59 10 -8 10 36.26 5.73 10 8 10 33.54 6.04 10 -8 10 29.55 4.81 -10 -8 -10 57.59 8.25 -10 -8 -10 35.33 5.87 10 -8 11 28.53 5.41 10 8 11 19.40 5.65 10 -8 11 24.05 4.44 -10 -8 -11 18.65 5.66 10 -9 -12 36.22 4.70 10 -9 -12 36.09 4.72 -10 -9 12 48.02 7.32 10 -9 -11 20.45 3.78 10 -9 -11 21.19 6.89 -10 -9 11 31.74 10.71 10 -9 -10 9.53 3.26 10 -9 -10 4.44 3.86 10 9 -10 9.92 3.94 -10 -9 10 4.03 5.49 10 -9 -9 17.87 5.13 10 9 -9 12.66 3.89 10 -9 -9 14.98 3.92 10 -9 -8 66.68 3.92 10 9 -8 58.10 5.42 10 -9 -8 69.67 8.50 -10 -9 8 65.98 5.77 10 -9 -7 86.41 6.64 10 9 -7 93.66 4.18 10 -9 -7 86.53 6.04 -10 -9 7 82.85 4.12 10 -9 -6 125.12 4.71 10 9 -6 127.34 5.35 10 -9 -6 130.53 11.54 -10 -9 6 132.75 5.18 10 -9 -5 25.40 4.13 10 9 -5 18.02 3.30 10 -9 -5 27.11 4.48 -10 -9 5 20.51 5.36 10 -9 -4 24.66 2.35 10 9 -4 21.58 3.50 10 -9 -4 27.05 4.68 -10 -9 4 27.43 3.44 10 -9 -3 61.14 4.42 10 9 -3 61.35 4.57 10 -9 -3 61.24 5.60 -10 -9 3 60.74 4.43 10 -9 -2 233.00 5.67 10 9 -2 237.98 9.08 10 -9 -2 229.84 10.73 -10 -9 2 226.37 9.08 10 -9 -1 81.23 4.38 10 9 -1 78.83 8.81 10 -9 -1 76.95 6.25 -10 -9 1 77.00 5.36 10 -9 0 6.02 2.72 10 9 0 6.69 3.82 10 -9 0 1.57 7.40 -10 -9 0 11.95 3.78 10 -9 1 8.36 1.58 10 9 1 6.02 3.85 10 -9 1 5.01 4.43 -10 -9 -1 6.90 3.99 10 9 2 74.44 5.86 10 -9 2 74.54 6.27 -10 -9 -2 75.13 5.90 10 9 3 69.50 5.97 10 -9 3 74.25 6.15 -10 -9 -3 67.92 5.99 10 9 4 89.91 6.55 10 -9 4 81.27 6.85 -10 -9 -4 81.13 6.65 10 9 5 9.23 4.86 10 -9 5 12.09 4.70 -10 -9 -5 15.11 4.75 10 9 6 -1.33 4.58 10 -9 6 1.57 4.29 -10 -9 -6 3.11 7.82 10 -9 7 11.04 4.71 10 9 7 12.34 5.00 10 -9 7 4.07 4.47 -10 -9 -7 12.06 4.91 10 -9 8 90.26 11.73 10 9 8 86.53 7.58 10 -9 8 87.21 6.64 -10 -9 -8 79.91 7.43 10 -9 9 34.31 5.61 10 -9 9 24.34 5.03 -10 -9 -9 29.55 6.08 -10 -9 -9 31.44 5.80 10 -9 10 11.01 5.41 10 9 10 24.59 5.89 10 -9 10 17.24 4.66 -10 -9 -10 23.34 6.35 10 -10 -11 44.79 4.67 10 -10 -11 40.05 5.36 -10 -10 11 49.07 7.94 10 -10 -10 3.59 5.77 10 -10 -10 7.70 6.97 10 -10 -9 115.90 5.89 10 -10 -9 121.24 7.39 10 10 -9 116.72 4.88 -10 -10 9 120.49 7.70 10 -10 -8 0.67 4.87 10 10 -8 -0.66 4.22 10 -10 -8 7.23 4.12 -10 -10 8 1.42 2.58 10 -10 -7 3.55 2.83 10 10 -7 6.50 2.74 10 -10 -7 3.77 4.30 -10 -10 7 3.03 2.79 10 -10 -6 1.64 4.46 10 10 -6 6.47 2.98 10 -10 -6 3.67 4.42 -10 -10 6 7.58 5.01 10 -10 -5 262.54 8.12 10 10 -5 253.19 9.63 10 -10 -5 261.96 12.42 -10 -10 5 265.12 9.65 10 -10 -4 1.96 4.02 10 10 -4 13.15 3.43 10 -10 -4 19.04 7.65 -10 -10 4 5.32 3.37 10 -10 -3 50.71 2.95 10 10 -3 57.30 4.70 10 -10 -3 54.09 5.93 -10 -10 3 51.99 4.57 10 -10 -2 -2.64 3.37 10 10 -2 -3.14 3.58 10 -10 -2 -4.07 4.50 -10 -10 2 4.00 3.53 10 -10 -1 96.90 3.53 10 10 -1 104.08 10.12 10 -10 -1 89.24 11.72 -10 -10 1 106.86 10.12 10 -10 0 1.13 3.11 10 10 0 1.36 3.88 10 -10 0 1.08 4.51 -10 -10 0 -3.17 6.55 10 10 1 150.78 8.19 10 -10 1 148.58 8.88 -10 -10 -1 141.40 8.13 10 10 2 6.94 4.37 10 -10 2 1.44 4.65 -10 -10 -2 9.63 4.34 10 10 3 0.60 4.42 10 -10 3 -2.84 4.56 -10 -10 -3 -3.28 4.42 10 10 4 12.25 4.84 10 -10 4 12.92 5.06 -10 -10 -4 8.94 4.86 10 10 5 111.35 8.29 10 -10 5 107.44 7.86 -10 -10 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11 -4 -2 81.35 4.48 -11 -4 2 84.24 4.17 11 -4 -1 515.95 16.30 11 4 -1 508.74 20.71 11 -4 -1 502.89 16.06 -11 -4 1 496.87 15.82 11 -4 0 3.66 3.17 11 4 0 1.45 4.85 11 -4 0 3.65 3.33 -11 -4 0 7.39 2.94 11 -4 1 -2.04 3.20 11 4 1 -1.02 4.93 11 -4 1 1.48 3.17 -11 -4 -1 3.59 2.95 11 -4 2 68.90 8.25 11 4 2 80.79 7.46 11 -4 2 74.57 7.95 -11 -4 -2 74.34 4.78 11 -4 3 325.64 11.72 11 4 3 306.12 16.36 11 -4 3 314.46 16.63 -11 -4 -3 316.04 11.21 11 -4 4 10.66 3.75 11 4 4 5.96 3.57 11 -4 4 9.99 3.48 -11 -4 -4 5.77 3.63 11 -4 5 63.61 5.13 11 4 5 68.50 5.14 11 -4 5 58.81 4.85 -11 -4 -5 74.70 4.17 -11 -4 -5 67.64 5.12 11 -4 6 36.86 4.56 11 4 6 32.13 4.78 11 -4 6 32.79 4.30 -11 -4 -6 35.69 2.09 -11 -4 -6 40.09 4.62 11 -4 7 5.90 6.68 11 4 7 1.53 4.09 11 -4 7 5.03 3.62 -11 -4 -7 8.60 1.76 -11 -4 -7 5.18 4.00 11 -4 8 15.11 4.23 11 4 8 15.92 7.32 11 -4 8 9.13 3.86 -11 -4 -8 13.69 1.89 -11 -4 -8 13.73 4.27 11 -4 9 121.73 11.09 11 4 9 115.49 6.99 11 -4 9 108.05 10.02 -11 -4 -9 100.87 3.58 -11 -4 -9 92.41 11.42 11 -4 10 5.04 4.20 11 4 10 1.08 4.28 11 -4 10 -0.65 6.10 -11 -4 -10 1.01 2.00 -11 -4 -10 0.21 4.34 11 -4 11 19.53 8.30 11 4 11 20.26 8.21 11 -4 11 15.38 4.07 -11 -4 -11 16.45 2.42 -11 -4 -11 18.38 4.90 11 -4 12 10.57 5.04 11 4 12 11.91 4.91 11 -4 12 9.03 4.01 -11 -4 -12 8.66 4.07 -11 -4 -12 3.71 8.19 11 -4 13 34.58 5.68 11 4 13 32.45 5.75 11 -4 13 32.00 4.79 -11 -4 -13 37.52 5.68 11 -5 -15 85.74 10.28 -11 -5 15 86.41 8.41 11 -5 -14 48.76 4.64 11 -5 -14 43.33 2.94 -11 -5 14 49.62 6.56 11 -5 -13 31.67 3.87 11 -5 -13 30.15 2.69 11 -5 -13 30.09 5.33 -11 -5 13 31.06 5.48 11 -5 -12 17.08 3.23 11 -5 -12 17.16 2.43 11 -5 -12 18.85 4.71 -11 -5 12 26.48 4.62 11 -5 -11 31.98 5.35 11 5 -11 33.93 1.93 11 -5 -11 31.35 5.23 -11 -5 11 39.30 4.73 11 -5 -10 40.21 4.85 11 5 -10 42.59 2.18 11 -5 -10 44.81 5.55 -11 -5 10 48.03 4.59 11 -5 -9 236.71 6.63 11 5 -9 252.78 6.10 11 -5 -9 227.81 7.84 -11 -5 9 257.61 13.96 11 -5 -8 93.17 3.31 11 5 -8 94.84 3.34 11 -5 -8 91.97 4.60 -11 -5 8 101.12 4.90 -11 -5 8 95.96 3.59 11 -5 -7 1.42 1.67 11 5 -7 1.91 3.41 11 -5 -7 3.62 4.68 -11 -5 7 7.07 4.68 -11 -5 7 4.59 2.15 11 -5 -6 0.87 1.44 11 5 -6 0.08 2.15 11 -5 -6 -0.29 2.88 -11 -5 6 5.19 2.50 -11 -5 6 2.32 3.76 11 -5 -5 282.76 5.56 11 5 -5 293.96 11.61 11 -5 -5 296.13 9.67 -11 -5 5 279.67 8.19 11 -5 -4 202.27 3.65 11 5 -4 209.12 6.34 11 -5 -4 206.05 7.69 -11 -5 4 199.80 6.52 11 -5 -3 51.25 1.97 11 5 -3 52.87 3.50 11 -5 -3 56.50 4.27 -11 -5 3 43.60 5.54 11 -5 -2 169.94 2.31 11 -5 -2 172.73 6.54 11 5 -2 170.77 6.07 11 -5 -2 176.75 7.03 -11 -5 2 167.00 5.98 11 -5 -1 51.00 4.17 11 5 -1 51.44 3.67 11 -5 -1 53.16 6.97 -11 -5 1 41.83 3.65 11 -5 0 77.55 4.87 11 5 0 77.99 4.29 11 -5 0 71.50 4.86 -11 -5 0 69.91 4.38 11 -5 1 128.40 9.81 11 5 1 118.07 8.74 11 -5 1 125.40 6.30 -11 -5 -1 116.52 5.53 11 -5 2 286.82 10.63 11 5 2 274.01 9.81 11 -5 2 273.18 10.60 -11 -5 -2 272.74 9.82 11 -5 3 13.21 3.98 11 5 3 14.88 3.66 11 -5 3 -0.20 6.23 -11 -5 -3 14.34 3.63 11 -5 4 30.94 7.55 11 5 4 33.09 4.32 11 -5 4 34.61 7.18 -11 -5 -4 30.30 4.35 11 -5 5 112.74 6.49 11 5 5 103.91 6.40 11 -5 5 105.79 9.95 -11 -5 -5 94.59 6.12 11 -5 6 158.99 8.25 11 5 6 159.49 7.95 11 -5 6 135.41 11.63 -11 -5 -6 149.13 7.64 11 -5 7 68.92 5.68 11 5 7 68.24 5.89 11 -5 7 52.22 8.60 -11 -5 -7 70.31 3.42 -11 -5 -7 57.16 9.24 11 -5 8 110.58 7.09 11 5 8 96.42 11.55 11 -5 8 97.78 10.05 -11 -5 -8 100.92 4.07 -11 -5 -8 96.41 6.86 11 -5 9 27.72 4.85 11 5 9 20.95 5.30 11 -5 9 16.25 7.07 -11 -5 -9 24.89 2.69 -11 -5 -9 18.73 5.08 11 -5 10 6.75 4.77 11 5 10 14.88 4.97 11 -5 10 16.14 4.04 -11 -5 -10 11.21 2.58 -11 -5 -10 10.77 4.75 11 -5 11 17.55 4.98 11 5 11 2.33 8.83 11 -5 11 18.80 4.17 -11 -5 -11 19.23 2.80 -11 -5 -11 14.47 8.64 11 -5 12 83.57 11.12 11 5 12 66.54 7.03 11 -5 12 53.77 5.52 -11 -5 -12 64.22 6.24 -11 -5 -12 66.74 6.85 11 -6 -15 1.19 4.05 -11 -6 15 4.67 5.83 11 -6 -14 12.13 6.23 11 -6 -14 1.86 2.31 11 -6 -14 -1.32 3.20 -11 -6 14 -0.73 5.29 11 -6 -13 6.14 3.50 11 -6 -13 4.12 3.05 -11 -6 13 6.85 4.86 11 -6 -12 100.50 5.27 11 -6 -12 103.63 4.98 -11 -6 12 105.19 7.39 11 -6 -11 27.13 3.22 11 -6 -11 28.88 3.48 -11 -6 11 31.76 4.89 11 -6 -10 65.02 5.77 11 6 -10 63.79 4.14 11 -6 -10 62.75 6.71 -11 -6 10 70.34 9.01 11 -6 -9 21.96 2.51 11 6 -9 25.73 3.56 11 -6 -9 22.53 5.45 -11 -6 9 26.85 4.00 -11 -6 9 24.19 3.79 11 -6 -8 54.24 2.65 11 6 -8 57.24 4.60 11 -6 -8 55.92 4.03 -11 -6 8 58.81 4.51 -11 -6 8 53.01 2.91 11 -6 -7 15.56 1.95 11 6 -7 20.29 2.39 11 -6 -7 16.90 3.32 -11 -6 7 17.18 3.36 -11 -6 7 14.81 2.52 11 -6 -6 193.92 6.44 11 6 -6 214.16 9.14 11 -6 -6 197.30 7.80 -11 -6 6 204.18 6.29 11 -6 -5 61.26 3.30 11 6 -5 70.58 3.58 11 -6 -5 65.94 4.65 -11 -6 5 66.33 3.53 11 -6 -4 8.34 1.97 11 6 -4 10.12 4.43 11 -6 -4 9.45 3.38 -11 -6 4 3.45 2.62 11 -6 -3 0.83 1.62 11 6 -3 1.61 2.66 11 -6 -3 6.60 3.33 -11 -6 3 0.33 2.63 11 -6 -2 159.61 3.37 11 6 -2 169.08 6.21 11 -6 -2 173.42 7.30 -11 -6 2 154.55 9.30 11 6 -1 45.18 3.93 11 -6 -1 62.57 7.62 -11 -6 1 47.39 3.80 11 6 0 197.49 7.66 11 -6 0 203.49 8.46 -11 -6 0 197.61 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15.98 5.69 11 -6 12 7.92 4.86 11 -6 12 10.45 4.18 -11 -6 -12 -4.07 5.22 -11 -6 -12 4.97 5.19 11 -7 -14 5.13 3.87 11 -7 -14 -7.96 4.56 -11 -7 14 -1.34 5.74 11 -7 -13 32.94 4.43 11 -7 -13 37.90 6.78 -11 -7 13 37.65 6.40 11 -7 -12 0.16 5.26 11 -7 -12 -1.12 5.36 -11 -7 12 -3.34 4.99 11 -7 -11 13.21 3.13 11 -7 -11 15.68 3.38 -11 -7 11 6.92 8.31 11 -7 -10 3.98 2.62 11 7 -10 -0.44 3.24 11 -7 -10 1.14 3.21 -11 -7 10 3.79 4.19 -11 -7 10 4.23 3.32 11 -7 -9 157.20 8.02 11 7 -9 161.28 7.22 11 -7 -9 157.42 10.76 -11 -7 9 162.97 8.35 -11 -7 9 150.31 7.13 11 -7 -8 2.18 2.10 11 7 -8 0.08 2.16 11 -7 -8 3.74 3.31 -11 -7 8 2.74 3.63 -11 -7 8 1.91 2.10 11 -7 -7 42.04 2.47 11 7 -7 41.78 3.03 11 -7 -7 42.49 4.27 -11 -7 7 40.55 4.82 11 -7 -6 4.84 2.93 11 7 -6 7.77 4.28 11 -7 -6 4.15 5.92 -11 -7 6 7.57 2.53 11 -7 -5 55.92 2.21 11 7 -5 62.00 3.73 11 -7 -5 58.00 4.92 -11 -7 5 52.38 5.89 11 -7 -4 6.13 1.40 11 7 -4 2.18 2.87 11 -7 -4 3.63 3.73 -11 -7 4 2.52 2.71 11 -7 -3 296.43 7.51 11 7 -3 311.73 14.75 11 -7 -3 307.13 11.75 -11 -7 3 305.29 9.81 11 -7 -2 4.14 1.78 11 7 -2 7.53 3.21 11 -7 -2 10.96 3.89 -11 -7 2 8.22 3.10 11 -7 -1 6.87 1.52 11 7 -1 13.92 3.35 11 -7 -1 5.96 6.79 -11 -7 1 11.50 3.33 11 7 0 4.79 3.53 11 -7 0 9.82 4.13 -11 -7 0 7.31 3.45 11 7 1 321.59 12.09 11 -7 1 317.06 13.29 -11 -7 -1 314.16 11.61 11 7 2 4.51 3.72 11 -7 2 2.54 4.27 -11 -7 -2 -1.19 3.74 11 -7 3 121.90 7.43 11 7 3 112.76 6.98 11 -7 3 121.22 7.48 -11 -7 -3 111.84 6.88 11 -7 4 4.17 4.39 11 7 4 3.89 4.20 11 -7 4 -1.46 7.29 -11 -7 -4 8.85 4.23 11 -7 5 66.18 6.00 11 7 5 61.20 5.97 11 -7 5 51.76 9.54 -11 -7 -5 52.30 5.86 11 -7 6 -0.95 4.32 11 7 6 9.85 4.54 11 -7 6 -9.13 7.14 -11 -7 -6 5.83 4.35 11 -7 7 129.78 13.36 11 7 7 137.12 8.64 11 -7 7 114.05 12.36 -11 -7 -7 129.43 8.23 11 -7 8 5.25 4.63 11 7 8 -2.14 8.35 11 -7 8 2.32 7.07 -11 -7 -8 4.14 9.05 -11 -7 -8 2.40 7.99 11 -7 9 20.85 8.22 11 7 9 15.48 9.04 11 -7 9 1.36 7.51 -11 -7 -9 11.25 8.37 -11 -7 -9 13.83 5.19 11 -7 10 2.47 4.76 11 7 10 -6.33 5.17 11 -7 10 3.72 4.16 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3.46 2.72 12 5 -8 0.94 2.15 12 -5 -8 -1.27 3.06 -12 -5 8 3.26 4.87 12 -5 -7 72.35 2.60 12 -5 -7 68.88 4.20 12 5 -7 76.43 3.58 12 -5 -7 68.06 4.64 -12 -5 7 64.53 4.03 -12 -5 7 75.04 3.63 12 -5 -6 268.71 7.60 12 -5 -6 274.86 9.48 12 5 -6 270.56 8.21 12 -5 -6 279.19 14.75 -12 -5 6 278.60 8.31 -12 -5 6 275.38 8.42 12 -5 -5 10.28 2.22 12 -5 -5 7.78 3.33 12 5 -5 16.21 4.63 12 -5 -5 10.53 3.57 -12 -5 5 13.09 2.53 -12 -5 5 18.35 2.87 12 -5 -4 108.34 2.14 12 -5 -4 114.80 5.60 12 5 -4 112.03 4.78 12 -5 -4 101.57 9.40 -12 -5 4 110.93 7.90 12 -5 -3 10.19 3.46 12 5 -3 6.87 2.94 12 -5 -3 8.53 3.60 -12 -5 3 3.16 3.09 12 -5 -2 133.69 10.29 12 5 -2 133.31 5.67 12 -5 -2 131.82 6.75 -12 -5 2 133.47 5.90 12 -5 -1 100.72 9.85 12 5 -1 105.04 8.30 12 -5 -1 103.25 9.83 -12 -5 1 106.66 5.50 12 -5 0 383.43 14.10 12 5 0 361.11 18.65 12 -5 0 386.14 14.84 -12 -5 0 365.16 13.22 12 -5 1 8.29 3.90 12 5 1 0.81 5.66 12 -5 1 -0.70 3.89 -12 -5 -1 -2.69 3.54 12 -5 2 1.78 4.06 12 5 2 -1.15 6.04 12 -5 2 -9.10 4.00 -12 -5 -2 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44.74 5.48 12 -6 -11 -3.09 4.43 12 -6 -11 -0.35 3.17 -12 -6 11 4.50 6.85 12 -6 -10 50.66 5.39 12 6 -10 52.35 2.92 12 -6 -10 53.29 4.39 -12 -6 10 51.22 5.12 12 -6 -9 51.96 3.05 12 6 -9 51.34 3.04 12 -6 -9 54.52 4.49 -12 -6 9 54.76 4.70 -12 -6 9 51.20 3.17 12 -6 -8 183.63 5.18 12 6 -8 192.38 5.98 12 -6 -8 178.61 11.91 -12 -6 8 180.84 7.35 -12 -6 8 175.59 8.49 12 -6 -7 55.18 2.57 12 6 -7 51.59 5.57 12 -6 -7 68.17 4.81 -12 -6 7 56.74 4.17 -12 -6 7 59.34 3.58 12 -6 -6 10.19 1.62 12 6 -6 15.14 2.77 12 -6 -6 11.00 6.13 -12 -6 6 8.39 4.77 12 -6 -5 3.40 1.29 12 6 -5 1.11 4.61 12 -6 -5 0.43 3.64 -12 -6 5 -0.57 2.80 12 -6 -4 188.35 3.61 12 6 -4 202.95 7.13 12 -6 -4 200.66 13.54 -12 -6 4 197.96 7.25 12 -6 -3 72.18 2.37 12 6 -3 65.55 4.56 12 -6 -3 78.80 5.62 -12 -6 3 71.92 7.20 12 -6 -2 234.90 9.84 12 6 -2 241.56 8.88 12 -6 -2 239.60 10.26 -12 -6 2 227.63 8.60 12 -6 -1 63.43 5.71 12 6 -1 70.29 4.85 12 -6 -1 74.18 9.62 -12 -6 1 65.05 4.93 12 -6 0 41.31 5.08 12 6 0 48.20 4.57 12 -6 0 46.14 5.22 -12 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12 -7 -11 107.46 5.04 12 -7 -11 119.66 9.84 -12 -7 11 112.19 7.67 12 -7 -10 2.78 2.58 12 7 -10 4.70 2.37 12 -7 -10 4.92 3.55 -12 -7 10 11.20 4.19 12 -7 -9 32.68 4.76 12 7 -9 41.74 3.07 12 -7 -9 34.72 4.60 -12 -7 9 40.51 4.65 -12 -7 9 38.83 4.77 12 -7 -8 1.45 2.07 12 7 -8 0.42 4.14 12 -7 -8 0.02 6.14 -12 -7 8 6.49 3.64 -12 -7 8 3.82 2.41 12 -7 -7 76.71 3.00 12 7 -7 82.31 4.14 12 -7 -7 79.49 5.62 -12 -7 7 70.83 4.20 12 -7 -6 16.82 1.88 12 7 -6 16.62 3.13 12 -7 -6 10.28 4.30 -12 -7 6 17.66 3.19 12 -7 -5 314.20 6.96 12 7 -5 347.92 11.42 12 -7 -5 328.54 13.59 -12 -7 5 323.78 10.79 12 -7 -4 2.54 2.10 12 7 -4 2.34 5.16 12 -7 -4 -14.19 6.59 -12 -7 4 1.66 2.98 12 7 -3 0.77 3.24 12 -7 -3 -0.51 4.10 -12 -7 3 4.48 3.14 12 7 -2 11.64 3.68 12 -7 -2 9.87 4.49 -12 -7 2 11.86 3.63 12 7 -1 349.26 13.28 12 -7 -1 353.20 23.06 -12 -7 1 345.39 19.66 12 7 0 6.98 3.76 12 -7 0 -0.38 4.43 -12 -7 0 -4.17 6.15 12 -7 1 75.44 6.46 12 7 1 75.05 5.78 12 -7 1 81.02 7.06 -12 -7 -1 64.24 9.42 12 -7 2 1.33 4.51 12 7 2 3.39 4.06 12 -7 2 1.84 4.64 -12 -7 -2 -3.85 6.67 12 -7 3 90.51 11.45 12 7 3 77.35 6.61 12 -7 3 82.50 11.19 -12 -7 -3 71.70 10.33 12 -7 4 4.82 4.84 12 7 4 5.87 4.77 12 -7 4 0.49 8.13 -12 -7 -4 22.10 8.02 12 -7 5 198.02 11.44 12 7 5 205.59 11.26 12 -7 5 203.64 16.85 -12 -7 -5 205.89 11.08 12 -7 6 4.37 5.03 12 7 6 9.05 5.15 12 -7 6 -0.72 8.01 -12 -7 -6 11.04 5.76 -12 -7 -6 5.28 5.08 12 -7 7 1.85 4.95 12 7 7 4.45 5.17 12 -7 7 -0.17 7.86 -12 -7 -7 3.09 4.85 -12 -7 -7 2.02 5.08 12 -7 8 20.83 8.96 12 7 8 13.46 5.72 12 -7 8 12.59 8.41 -12 -7 -8 11.97 4.06 -12 -7 -8 11.15 5.64 12 -7 9 110.52 9.10 12 7 9 150.96 16.42 12 -7 9 114.52 13.04 -12 -7 -9 121.49 6.18 -12 -7 -9 110.64 15.19 12 -7 10 -4.59 8.42 12 7 10 4.46 5.75 12 -7 10 -5.12 4.62 -12 -7 -10 2.80 3.01 -12 -7 -10 2.81 5.70 12 -8 -11 4.12 3.06 12 -8 -11 5.22 3.92 -12 -8 11 12.43 8.29 12 -8 -10 18.12 3.02 12 -8 -10 13.50 7.29 -12 -8 10 19.11 4.82 12 -8 -9 49.60 3.30 12 8 -9 52.09 3.47 12 -8 -9 48.48 5.23 -12 -8 9 48.48 5.69 -12 -8 9 36.77 5.27 12 -8 -8 70.98 5.60 12 8 -8 77.72 6.63 12 -8 -8 73.58 6.03 -12 -8 8 81.44 5.96 -12 -8 8 75.10 4.23 12 -8 -7 27.80 2.48 12 8 -7 29.80 3.45 12 -8 -7 24.02 8.20 -12 -8 7 39.16 5.45 12 -8 -6 0.58 1.85 12 8 -6 1.87 5.01 12 -8 -6 1.45 4.24 -12 -8 6 3.91 2.91 12 -8 -5 22.56 1.97 12 8 -5 24.82 3.62 12 -8 -5 14.63 4.94 -12 -8 5 21.56 3.53 12 8 -4 126.95 9.57 12 -8 -4 110.95 7.62 -12 -8 4 105.39 8.91 12 8 -3 85.07 5.54 12 -8 -3 94.71 6.92 -12 -8 3 83.28 5.19 12 8 -2 24.11 4.16 12 -8 -2 20.10 8.55 -12 -8 2 18.78 3.97 12 8 -1 3.12 3.85 12 -8 -1 1.47 4.60 -12 -8 1 6.32 3.73 12 8 0 19.51 4.36 12 -8 0 17.07 5.18 -12 -8 0 16.31 4.28 12 8 1 73.74 6.01 12 -8 1 63.46 6.55 -12 -8 -1 76.48 5.97 12 -8 2 54.59 6.20 12 8 2 56.77 5.88 12 -8 2 64.84 6.79 -12 -8 -2 49.75 5.76 12 -8 3 67.29 6.79 12 8 3 65.49 6.39 12 -8 3 61.36 11.42 -12 -8 -3 64.26 6.26 12 -8 4 13.14 8.73 12 8 4 8.86 5.05 12 -8 4 12.93 8.85 -12 -8 -4 8.30 4.90 12 -8 5 34.11 5.99 12 8 5 25.36 6.04 12 -8 5 36.60 9.80 -12 -8 -5 28.63 5.86 12 -8 6 19.31 5.56 12 8 6 12.14 5.74 12 -8 6 -7.80 9.01 -12 -8 -6 21.36 5.40 12 -8 7 61.87 7.61 12 8 7 69.94 7.84 12 -8 7 59.42 11.71 -12 -8 -7 85.91 12.89 12 -8 8 64.63 7.48 12 8 8 72.88 8.05 12 -8 8 59.43 11.48 -12 -8 -8 63.18 7.85 12 -9 -10 55.96 6.49 12 -9 -10 48.10 5.70 -12 -9 10 55.91 11.06 12 -9 -9 2.91 2.64 12 9 -9 -1.77 2.78 12 -9 -9 -4.00 7.24 -12 -9 9 -0.90 4.61 -12 -9 9 0.41 2.50 12 -9 -8 29.37 2.99 12 9 -8 29.76 5.75 12 -9 -8 36.74 5.33 -12 -9 8 24.84 5.51 12 -9 -7 18.18 4.17 12 9 -7 15.59 3.42 12 -9 -7 24.03 8.50 -12 -9 7 23.23 3.35 12 -9 -6 86.47 3.49 12 9 -6 96.24 8.36 12 -9 -6 89.26 7.16 -12 -9 6 86.08 8.20 12 9 -5 10.58 3.58 12 -9 -5 17.83 8.24 -12 -9 5 7.88 3.37 12 9 -4 7.06 6.05 12 -9 -4 9.95 4.73 -12 -9 4 0.75 3.41 12 9 -3 3.29 3.73 12 -9 -3 3.30 4.80 -12 -9 3 6.65 3.57 12 9 -2 39.26 4.86 12 -9 -2 49.80 10.24 -12 -9 2 40.52 4.72 12 9 -1 5.23 4.14 12 -9 -1 -1.39 5.03 -12 -9 1 18.18 6.89 12 9 0 91.16 6.53 12 -9 0 81.95 7.81 -12 -9 0 84.49 10.54 12 9 1 6.46 4.50 12 -9 1 5.80 5.17 -12 -9 -1 -0.87 7.49 12 9 2 18.76 7.95 12 -9 2 2.28 9.45 -12 -9 -2 -3.47 8.04 12 -9 3 8.14 5.08 12 9 3 23.29 8.45 12 -9 3 -3.81 9.25 -12 -9 -3 3.69 4.96 12 -9 4 78.31 7.63 12 -9 4 67.01 12.61 -12 -9 -4 74.50 7.27 12 -9 5 7.61 8.94 12 -9 5 1.48 5.36 -12 -9 -5 9.28 5.33 12 -9 6 13.51 5.64 12 9 6 -0.59 5.85 12 -9 6 8.08 5.34 -12 -9 -6 13.16 5.63 12 -9 7 -4.25 5.41 12 9 7 0.22 5.66 12 -9 7 6.07 5.12 -12 -9 -7 6.15 5.50 -12 -9 -7 3.65 5.50 12 -10 -8 3.36 4.49 12 -10 -8 2.71 7.98 12 10 -8 0.79 5.17 -12 -10 8 2.50 3.08 12 10 -7 11.96 3.65 12 -10 -7 18.47 5.40 -12 -10 7 19.69 5.93 12 10 -6 9.23 6.06 12 -10 -6 9.64 5.21 -12 -10 6 9.01 3.41 12 10 -5 28.49 4.39 12 -10 -5 26.97 5.92 -12 -10 5 28.68 4.13 12 10 -4 8.31 6.59 12 -10 -4 8.35 5.16 -12 -10 4 2.14 3.65 12 10 -3 67.88 5.76 12 -10 -3 71.89 11.99 -12 -10 3 63.39 8.63 12 10 -2 -0.77 4.13 12 -10 -2 4.09 5.29 -12 -10 2 1.91 3.93 12 10 -1 9.28 4.38 12 -10 -1 -3.90 5.32 -12 -10 1 -0.88 4.17 12 10 0 12.38 4.96 12 -10 0 15.11 5.84 -12 -10 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108.62 2.27 13 0 -3 2.88 3.25 -13 0 3 0.42 0.79 13 0 -2 139.28 6.65 13 0 -1 2.14 3.65 13 0 0 506.51 18.57 13 0 1 3.76 3.95 13 0 2 13.91 4.53 13 0 3 35.57 9.18 13 0 4 414.21 16.91 13 0 5 -1.72 4.36 13 0 6 265.89 12.79 13 0 7 -7.68 4.97 13 0 8 46.84 6.32 13 0 9 5.32 5.19 13 0 10 180.36 10.91 13 0 11 4.94 5.35 13 0 12 -3.26 9.07 -13 1 15 17.93 4.67 -13 -1 15 13.00 8.13 -13 1 14 44.09 4.92 -13 -1 14 41.77 5.16 -13 1 13 118.96 6.45 -13 -1 13 133.47 6.81 13 -1 -12 43.86 2.66 13 -1 -12 46.61 5.21 -13 1 12 34.56 3.89 -13 -1 12 38.23 6.97 13 -1 -11 29.36 2.79 13 1 -11 33.86 3.91 13 -1 -11 35.41 5.01 13 1 -11 29.83 4.34 -13 1 11 34.83 3.44 -13 -1 11 36.30 3.58 13 -1 -10 26.61 4.42 13 1 -10 24.52 2.36 13 -1 -10 18.89 4.68 13 1 -10 22.13 2.53 -13 1 10 20.03 2.87 -13 -1 10 25.49 3.00 13 -1 -9 175.22 5.50 13 1 -9 174.42 5.20 13 -1 -9 141.86 8.42 13 1 -9 154.96 5.30 -13 1 9 156.91 5.25 -13 -1 9 158.44 5.47 13 -1 -8 127.94 4.77 13 1 -8 129.37 4.51 13 -1 -8 109.25 7.34 13 1 -8 124.46 7.44 -13 1 8 112.12 3.93 -13 -1 8 120.09 4.17 13 -1 -7 200.24 6.52 13 1 -7 211.03 9.70 13 -1 -7 187.34 6.77 13 1 -7 201.33 6.70 -13 1 7 200.04 4.99 -13 -1 7 196.25 7.54 13 -1 -6 14.74 3.01 13 1 -6 21.30 2.96 13 -1 -6 13.89 3.32 -13 1 6 14.81 2.69 -13 -1 6 18.28 2.92 13 -1 -5 7.41 4.81 13 1 -5 7.64 2.83 13 -1 -5 2.10 3.06 -13 1 5 5.20 1.28 -13 -1 5 3.44 2.34 13 -1 -4 156.37 9.56 13 1 -4 162.93 6.13 13 -1 -4 153.60 6.70 -13 -1 4 145.56 4.28 13 -1 -3 372.29 17.61 13 1 -3 389.27 12.42 13 -1 -3 379.33 12.67 -13 -1 3 353.25 7.93 13 -1 -2 300.44 10.68 13 1 -2 318.28 10.99 13 -1 -1 78.65 5.14 13 1 -1 79.92 5.24 13 -1 0 32.09 4.39 13 1 0 37.35 4.50 13 -1 1 117.42 6.64 13 1 1 122.06 7.09 13 -1 2 246.82 10.33 13 1 2 238.76 10.35 13 -1 3 327.66 21.51 13 1 3 336.77 20.99 13 -1 4 6.89 4.56 13 1 4 0.54 4.25 13 -1 5 1.84 4.68 13 1 5 5.92 4.44 13 -1 6 76.25 11.52 13 1 6 60.37 6.59 13 -1 7 147.70 9.07 13 1 7 148.49 14.34 13 -1 8 48.29 6.21 13 1 8 47.95 6.21 13 -1 9 23.28 9.70 13 1 9 30.06 5.93 13 -1 10 4.06 5.26 13 1 10 2.87 8.84 13 -1 11 11.18 9.70 13 1 11 15.78 5.75 13 -1 12 42.68 6.58 13 1 12 30.67 11.05 -13 2 15 97.66 6.89 -13 -2 15 96.17 12.08 -13 2 14 9.67 3.96 -13 -2 14 10.06 4.27 -13 2 13 3.31 3.44 -13 -2 13 1.37 3.77 13 -2 -12 26.62 2.63 13 -2 -12 26.84 5.17 -13 2 12 33.53 3.71 -13 -2 12 31.53 6.67 13 -2 -11 192.11 8.47 13 2 -11 180.27 5.00 13 -2 -11 191.09 9.70 13 2 -11 165.49 7.75 -13 2 11 190.18 6.86 -13 -2 11 194.61 7.23 13 -2 -10 20.79 2.68 13 2 -10 12.74 3.69 13 -2 -10 20.62 4.87 13 2 -10 17.75 2.46 -13 2 10 18.34 2.77 -13 -2 10 19.88 3.05 13 -2 -9 54.97 3.39 13 2 -9 54.47 2.93 13 -2 -9 53.07 5.95 13 2 -9 51.25 3.28 -13 2 9 59.33 3.09 -13 -2 9 47.41 5.51 13 -2 -8 0.51 2.46 13 2 -8 1.58 2.26 13 -2 -8 0.59 2.70 -13 -2 8 0.79 2.17 13 -2 -7 87.60 6.72 13 2 -7 91.71 3.98 -13 -2 7 89.56 3.36 13 -2 -6 24.35 5.47 13 2 -6 32.18 4.97 13 -2 -6 23.22 3.58 -13 -2 6 29.99 2.13 13 -2 -5 378.51 17.60 13 2 -5 416.04 17.09 13 -2 -5 374.34 12.67 -13 -2 5 381.41 11.17 13 -2 -4 28.01 6.18 13 2 -4 26.94 3.44 13 -2 -4 32.83 3.86 -13 -2 4 26.87 1.66 13 -2 -3 11.32 5.67 13 2 -3 8.75 3.26 13 -2 -3 13.36 3.59 -13 -2 3 13.26 1.27 13 -2 -2 0.64 5.53 13 2 -2 -0.20 3.19 13 -2 -2 -5.76 5.84 -13 -2 2 1.61 1.64 13 -2 -1 322.01 11.84 13 2 -1 340.33 12.07 13 -2 -1 329.05 12.50 13 -2 0 49.66 4.83 13 2 0 57.91 4.96 13 -2 0 57.62 4.85 13 -2 1 193.80 8.64 13 2 1 204.38 9.01 13 -2 1 182.19 8.50 13 -2 2 10.19 4.19 13 2 2 13.85 4.54 13 -2 2 10.29 4.15 13 -2 3 43.26 5.44 13 2 3 53.05 9.51 13 -2 4 -4.48 4.21 13 2 4 -3.89 4.15 13 -2 5 231.05 11.20 13 2 5 230.77 11.24 13 -2 6 33.04 9.73 13 2 6 42.19 5.69 13 -2 7 14.70 5.21 13 2 7 12.18 8.80 13 -2 8 21.55 5.94 13 2 8 20.74 5.37 13 -2 9 66.38 7.01 13 2 9 58.27 7.07 13 -2 9 61.34 6.38 13 -2 10 30.70 6.17 13 2 10 30.27 10.26 13 -2 10 32.23 5.65 13 -2 11 63.72 7.34 13 2 11 58.66 7.34 13 -2 11 66.84 6.75 -13 -3 14 67.42 9.93 -13 -3 13 -1.80 3.86 13 -3 -12 74.86 3.69 13 -3 -12 82.15 4.41 -13 -3 12 77.86 8.61 13 -3 -11 2.46 4.02 13 3 -11 -0.03 1.92 13 -3 -11 2.58 2.83 13 3 -11 1.71 2.07 -13 -3 11 7.18 3.19 13 -3 -10 19.83 2.79 13 3 -10 19.94 2.31 13 -3 -10 16.07 3.19 13 3 -10 24.66 2.54 -13 -3 10 17.22 3.26 13 -3 -9 -1.24 2.50 13 3 -9 1.34 2.10 13 -3 -9 0.43 4.75 -13 -3 9 3.08 4.30 13 -3 -8 208.79 10.04 13 3 -8 208.52 6.13 13 -3 -8 204.74 7.63 -13 -3 8 220.08 6.65 13 -3 -7 0.96 4.33 13 3 -7 2.40 2.34 13 -3 -7 -1.49 2.97 -13 -3 7 1.70 3.53 13 -3 -6 4.57 5.11 13 3 -6 6.24 2.53 13 -3 -6 5.53 5.24 -13 -3 6 5.57 1.99 13 -3 -5 6.44 5.64 13 3 -5 13.98 2.78 13 -3 -5 8.01 3.36 -13 -3 5 13.44 1.92 13 -3 -4 153.92 10.24 13 -3 -4 144.46 10.43 -13 -3 4 141.61 3.69 13 -3 -3 4.56 5.56 13 3 -3 10.26 5.12 13 -3 -3 6.92 3.51 -13 -3 3 6.19 1.48 13 -3 -2 174.69 7.40 13 3 -2 178.94 7.00 13 -3 -2 178.34 11.95 -13 -3 2 168.17 3.61 13 -3 -1 10.13 3.82 13 3 -1 12.11 3.63 13 -3 -1 16.45 4.01 -13 -3 1 12.24 2.06 -13 -3 1 15.39 3.62 13 -3 0 4.16 3.63 13 3 0 -5.81 3.49 13 -3 0 0.24 3.73 -13 -3 0 2.11 1.07 -13 -3 0 2.10 3.49 13 -3 1 -2.47 3.86 13 3 1 6.91 3.81 13 -3 1 -1.42 3.89 -13 -3 -1 2.65 3.74 13 -3 2 163.14 13.08 13 3 2 166.28 12.65 13 -3 2 147.41 7.57 -13 -3 -2 147.93 7.62 13 -3 3 -0.12 4.15 13 3 3 -12.49 7.10 13 -3 3 -5.32 6.85 -13 -3 -3 -2.94 4.05 13 -3 4 155.86 8.70 13 3 4 169.02 8.93 13 -3 4 150.36 13.62 -13 -3 -4 144.72 8.58 13 -3 5 -5.70 7.81 13 3 5 8.14 4.78 13 -3 5 -4.99 7.43 -13 -3 -5 -2.80 4.32 13 -3 6 26.22 5.22 13 3 6 28.80 5.32 13 -3 6 31.01 8.60 -13 -3 -6 26.57 5.37 13 -3 7 -1.99 4.81 13 3 7 -8.70 4.96 13 -3 7 -7.85 7.76 -13 -3 -7 -6.74 4.83 13 -3 8 153.43 15.33 13 3 8 132.71 8.92 13 -3 8 148.19 13.92 -13 -3 -8 139.16 9.05 13 -3 9 16.34 5.61 13 3 9 16.34 5.54 13 -3 9 14.27 4.96 13 -3 10 0.07 9.31 13 3 10 6.22 5.40 13 -3 10 4.30 4.81 13 -3 11 7.98 5.29 13 3 11 5.13 9.09 13 -3 11 0.96 4.93 -13 -4 14 12.43 8.09 13 -4 -13 -0.79 2.43 13 -4 -13 2.66 3.01 -13 -4 13 -2.76 4.05 13 -4 -12 6.99 4.24 13 -4 -12 7.02 3.20 -13 -4 12 5.96 3.89 13 -4 -11 128.90 5.27 13 -4 -11 146.57 6.34 -13 -4 11 147.24 6.84 13 -4 -10 7.06 2.61 13 4 -10 1.64 3.49 13 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14 -2 2 17.89 4.85 14 -2 3 156.50 8.93 14 2 3 149.05 8.84 14 -2 3 144.90 8.77 14 -2 4 107.47 8.19 14 2 4 121.46 8.24 14 -2 4 105.69 7.99 14 -2 5 22.02 5.66 14 2 5 14.46 5.55 14 -2 5 23.49 5.14 14 -2 6 23.43 5.83 14 2 6 21.90 5.95 14 -2 6 20.07 5.38 14 -2 7 44.95 7.09 14 2 7 44.27 11.49 14 -2 7 48.79 6.38 14 -2 8 71.19 7.71 14 2 8 86.00 8.15 14 -2 8 74.83 7.44 14 -2 9 63.97 7.46 14 2 9 69.04 7.72 14 -2 9 53.10 7.21 14 -2 10 30.93 10.95 14 2 10 22.41 10.95 14 -2 10 18.88 6.11 -14 -3 13 11.04 6.82 14 -3 -12 4.33 4.45 14 -3 -12 11.95 3.30 -14 -3 12 2.28 3.55 14 -3 -11 1.38 2.65 14 -3 -11 3.32 3.15 -14 -3 11 3.88 3.13 14 -3 -10 184.35 6.61 14 3 -10 176.24 5.77 14 -3 -10 177.82 7.41 14 3 -10 195.92 6.33 -14 -3 10 183.03 10.55 14 -3 -9 11.91 5.07 14 3 -9 9.78 2.58 14 -3 -9 7.87 3.42 -14 -3 9 9.88 2.79 14 -3 -8 41.20 3.74 14 3 -8 45.69 3.31 14 -3 -8 44.29 6.90 -14 -3 8 46.88 3.11 14 -3 -7 16.14 3.28 14 3 -7 18.32 3.01 14 -3 -7 18.56 3.66 -14 -3 7 16.04 3.95 14 -3 -6 65.04 4.64 14 3 -6 67.36 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5.43 14 -3 9 -17.28 9.84 14 3 9 0.56 5.73 14 -3 9 8.05 5.21 14 -3 10 51.09 7.44 14 3 10 50.39 7.91 14 -3 10 51.91 7.07 -14 -4 13 112.74 11.29 14 -4 -12 2.08 2.78 14 -4 -12 6.02 5.65 -14 -4 12 -1.03 3.68 14 -4 -11 63.80 4.04 14 -4 -11 63.20 4.90 -14 -4 11 65.14 4.83 14 -4 -10 4.10 2.87 14 4 -10 1.58 2.43 14 -4 -10 2.76 3.46 -14 -4 10 4.04 5.27 14 -4 -9 44.15 6.45 14 4 -9 45.47 5.30 14 -4 -9 45.68 4.49 -14 -4 9 47.35 3.75 14 -4 -8 14.33 5.18 14 4 -8 0.41 2.63 14 -4 -8 2.18 5.97 -14 -4 8 5.21 4.39 14 -4 -7 195.77 8.00 14 4 -7 186.67 10.20 14 -4 -7 192.42 8.75 -14 -4 7 194.88 6.22 14 -4 -6 22.55 4.02 14 4 -6 21.09 3.40 14 -4 -6 29.46 4.29 -14 -4 6 23.80 2.53 14 -4 -5 21.78 4.10 14 4 -5 21.09 3.45 14 -4 -5 19.04 4.33 -14 -4 5 21.43 2.35 14 -4 -4 2.45 3.81 14 4 -4 6.70 3.15 14 -4 -4 -3.51 6.62 -14 -4 4 0.92 1.87 14 -4 -3 127.71 7.13 14 4 -3 120.73 9.70 14 -4 -3 119.66 7.07 -14 -4 3 117.90 3.60 14 -4 -2 26.99 7.97 14 4 -2 10.29 6.73 14 -4 -2 22.08 4.57 -14 -4 2 16.29 2.95 -14 -4 2 19.40 4.17 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112.91 12.52 14 -7 1 111.80 9.10 -14 -7 -1 104.57 8.05 14 -7 2 6.47 9.53 14 7 2 7.90 8.44 14 -7 2 6.09 5.49 -14 -7 -2 5.02 5.25 14 -7 3 3.20 5.70 14 7 3 -1.11 8.62 14 -7 3 -9.11 9.35 -14 -7 -3 12.46 5.30 14 -7 4 11.07 6.08 14 7 4 2.62 9.56 14 -7 4 9.17 9.89 -14 -7 -4 13.67 5.85 14 -7 5 90.11 14.98 14 7 5 82.06 8.62 14 -7 5 84.99 13.79 -14 -7 -5 85.33 8.76 14 -7 6 -0.20 5.80 14 7 6 -6.02 5.74 14 -7 6 1.01 5.42 -14 -7 -6 6.37 5.92 14 -8 -8 30.05 5.04 14 8 -8 28.96 3.93 14 -8 -8 34.88 5.70 -14 -8 8 34.06 4.35 -14 -8 8 24.50 5.74 14 -8 -7 19.98 4.90 14 8 -7 26.89 3.94 14 -8 -7 20.64 5.66 -14 -8 7 24.07 4.08 -14 -8 7 25.04 3.92 14 -8 -6 39.58 5.66 14 8 -6 42.79 4.46 14 -8 -6 43.79 6.31 -14 -8 6 29.79 7.48 14 -8 -5 11.58 4.90 14 8 -5 4.27 6.53 14 -8 -5 9.05 5.33 -14 -8 5 7.95 3.94 14 -8 -4 3.80 4.74 14 8 -4 -0.25 3.83 14 -8 -4 3.02 5.22 -14 -8 4 0.07 3.94 14 -8 -3 61.97 6.96 14 8 -3 65.60 5.81 14 -8 -3 63.49 7.44 -14 -8 3 63.33 5.86 14 -8 -2 86.13 7.85 14 8 -2 88.85 6.65 14 -8 -2 75.00 7.96 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3.86 -15 -1 8 35.92 2.60 15 -1 -7 195.57 7.68 15 1 -7 194.83 7.53 15 -1 -7 188.84 8.28 15 1 -7 190.80 7.90 -15 -1 7 182.93 4.98 15 -1 -6 5.83 3.37 15 1 -6 0.49 3.27 15 -1 -6 1.24 6.12 15 1 -6 1.20 3.37 -15 -1 6 2.04 1.55 15 -1 -5 43.84 7.38 15 1 -5 48.28 4.41 15 -1 -5 37.70 4.90 15 -1 -4 18.31 7.05 15 1 -4 23.99 6.87 15 -1 -4 20.83 4.38 15 -1 -3 97.93 10.04 15 1 -3 99.73 9.82 15 -1 -3 95.18 6.50 15 -1 -2 -3.21 6.90 15 1 -2 0.24 6.68 15 -1 -2 6.67 4.12 15 -1 -1 181.26 9.42 15 1 -1 194.78 14.75 15 -1 -1 192.71 9.32 15 -1 0 1.59 4.47 15 1 0 4.40 7.81 15 -1 1 0.77 4.62 15 1 1 0.40 4.52 15 -1 2 8.98 5.00 15 1 2 1.29 4.80 15 -1 3 153.94 9.88 15 1 3 135.81 9.33 15 -1 4 18.59 9.02 15 1 4 11.02 5.53 15 -1 5 63.01 7.31 15 1 5 77.72 12.85 15 -1 6 -1.72 5.70 15 1 6 -14.35 5.83 15 -1 7 18.02 10.48 15 1 7 14.53 6.33 15 -1 8 3.04 5.76 15 1 8 -0.01 5.90 15 -2 -12 12.24 2.91 15 -2 -12 2.72 2.89 -15 -2 12 12.27 5.83 15 -2 -11 40.31 3.53 15 -2 -11 34.40 4.15 -15 -2 11 35.10 3.76 15 -2 -10 48.72 6.20 15 2 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7.99 5.35 15 -2 5 54.95 7.23 15 2 5 49.88 7.22 15 -2 5 38.30 6.70 15 -2 6 132.18 10.28 15 -2 6 127.20 9.81 15 -2 7 40.33 6.95 15 2 7 47.93 7.30 15 -2 7 40.28 6.96 15 -2 8 14.58 6.59 15 2 8 25.80 6.84 15 -2 8 17.58 6.29 15 -3 -12 119.09 5.30 -15 -3 12 104.36 10.01 15 -3 -11 18.97 5.13 15 -3 -11 13.47 3.84 -15 -3 11 14.51 3.39 15 -3 -10 45.27 3.85 15 3 -10 39.65 3.35 15 -3 -10 39.21 4.38 15 3 -10 47.04 5.77 -15 -3 10 44.77 3.68 15 -3 -9 -1.50 3.07 15 3 -9 -0.06 2.76 15 -3 -9 0.51 3.51 15 3 -9 1.91 2.80 -15 -3 9 2.33 2.56 15 -3 -8 54.22 4.35 15 3 -8 54.00 3.93 15 -3 -8 57.56 8.04 -15 -3 8 50.13 5.33 15 -3 -7 5.14 3.42 15 3 -7 0.64 5.40 15 -3 -7 10.04 3.99 -15 -3 7 8.44 2.24 15 -3 -6 234.47 9.71 15 3 -6 254.31 9.29 15 -3 -6 234.46 16.18 -15 -3 6 236.53 6.27 15 -3 -5 1.35 3.87 15 3 -5 6.97 3.58 15 -3 -5 14.02 4.25 -15 -3 5 9.37 2.98 15 -3 -4 1.01 3.92 15 3 -4 2.84 3.51 15 -3 -4 2.93 7.14 -15 -3 4 4.44 2.56 15 -3 -3 6.13 4.19 15 3 -3 10.40 3.88 15 -3 -3 0.47 4.69 15 -3 -2 333.36 14.70 15 3 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-0.47 7.07 17 0 -5 -2.67 4.37 17 0 -4 63.32 6.11 17 0 -4 62.01 6.28 17 0 -3 1.00 4.43 17 0 -3 -4.64 4.58 17 0 -2 141.09 8.96 17 0 -2 138.96 9.17 17 0 -1 -6.12 5.31 17 0 0 -11.41 9.43 17 0 1 -16.71 10.09 17 0 2 167.27 11.56 17 0 3 -5.57 6.12 17 0 4 61.56 8.83 17 -1 -8 7.79 3.76 17 1 -8 9.37 3.68 17 -1 -8 11.17 4.27 17 1 -8 7.96 6.63 17 -1 -7 60.05 5.23 17 1 -7 65.31 5.22 17 -1 -7 62.00 9.99 17 1 -7 60.38 5.37 17 -1 -6 20.94 7.10 17 1 -6 18.92 7.30 17 -1 -6 15.22 4.89 17 1 -6 14.41 4.57 17 -1 -5 97.44 11.31 17 1 -5 96.27 6.80 17 -1 -5 95.94 11.96 17 1 -5 98.85 6.86 17 -1 -4 37.37 9.01 17 1 -4 31.87 5.32 17 -1 -4 33.45 5.61 17 -1 -3 5.00 8.21 17 1 -3 2.52 4.61 17 -1 -3 4.75 4.83 17 -1 -2 -5.33 8.93 17 1 -2 9.77 4.96 17 -1 -2 5.33 8.70 17 -1 -1 104.39 13.71 17 1 -1 109.26 8.58 17 -1 -1 107.68 8.95 17 -1 0 19.92 9.82 17 1 0 23.70 5.89 17 -1 0 18.41 6.08 17 -1 1 68.73 7.64 17 1 1 67.15 7.70 17 -1 1 51.28 7.71 17 -1 2 13.20 6.21 17 1 2 3.72 11.14 17 -1 2 17.63 6.13 17 -1 3 15.62 6.46 17 1 3 19.49 11.05 17 -1 3 16.09 6.32 17 -2 -7 62.27 5.69 17 2 -7 67.39 5.31 17 -2 -7 73.85 6.47 17 2 -7 66.95 5.48 17 -2 -6 -2.69 4.00 17 -2 -6 5.91 4.53 17 -2 -5 11.94 7.76 17 2 -5 19.53 4.56 17 -2 -5 -1.18 8.87 17 -2 -4 82.54 11.58 17 2 -4 85.66 6.89 17 -2 -4 87.23 7.78 17 -2 -3 88.07 12.02 17 2 -3 87.88 7.02 17 -2 -3 78.85 7.53 17 -2 -2 50.07 6.58 17 2 -2 48.80 6.31 17 -2 -2 42.65 11.38 17 -2 -1 6.80 5.67 17 2 -1 10.17 5.31 17 -2 -1 2.76 5.62 17 -2 0 25.61 6.56 17 2 0 39.35 6.42 17 -2 0 26.80 6.57 17 -2 1 41.93 7.34 17 2 1 46.28 7.37 17 -2 1 44.20 7.14 17 -2 2 60.27 7.74 17 2 2 44.12 7.63 17 -2 2 45.98 7.51 17 -2 3 40.58 7.61 17 2 3 34.41 12.41 17 -2 3 20.59 12.07 17 -3 -7 2.75 3.79 17 3 -7 -3.33 3.70 17 -3 -7 3.84 4.70 17 -3 -6 159.71 8.59 17 3 -6 179.31 13.35 17 -3 -6 187.46 16.56 17 -3 -5 11.20 4.74 17 3 -5 15.73 4.54 17 -3 -5 14.48 5.46 17 -3 -4 20.47 5.16 17 3 -4 18.62 4.95 17 -3 -4 25.21 5.72 17 -3 -3 0.30 4.84 17 3 -3 9.41 4.65 17 -3 -3 -4.33 8.86 17 -3 -2 67.12 7.18 17 3 -2 72.57 6.84 17 -3 -2 69.86 7.93 17 -3 -1 17.43 5.68 17 3 -1 15.43 5.43 17 -3 -1 12.19 6.08 17 -3 0 76.27 8.17 17 3 0 83.67 8.06 17 -3 0 82.64 8.49 17 -3 1 -0.53 5.69 17 3 1 2.08 5.63 17 -3 1 1.04 5.70 17 -3 2 -2.78 10.05 17 3 2 5.26 6.17 17 -3 2 -2.85 10.02 17 -4 -5 29.22 5.26 17 4 -5 22.43 4.91 17 -4 -5 15.02 6.18 17 -4 -4 23.11 5.42 17 4 -4 22.83 5.00 17 -4 -4 16.66 6.09 17 -4 -3 70.58 7.22 17 4 -3 66.39 6.74 17 -4 -3 78.14 8.09 17 -4 -2 14.13 5.55 17 4 -2 7.74 5.05 17 -4 -2 6.87 5.95 17 -4 -1 14.16 6.09 17 4 -1 21.00 5.65 17 -4 -1 18.82 6.35 17 -4 0 9.13 11.04 17 4 0 23.73 6.05 17 -4 0 17.07 11.17 17 -4 1 47.26 7.41 17 4 1 45.95 7.33 17 -4 1 51.15 13.17 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 26294 _shelx_res_file ; TITL shelxt_a.res in P2(1)/c shelxt_a.res created by SHELXL-2018/1 at 17:15:50 on 17-Oct-2024 CELL 0.71073 12.7442 10.6851 14.4027 90.000 96.645 90.000 ZERR 4.00 0.0006 0.0006 0.0006 0.000 0.007 0.000 LATT 1 SYMM - X, 1/2 + Y, 1/2 - Z SFAC C H BR N O RE S UNIT 72 48 4 8 16 4 4 MERG 2 OMIT -4.00 180.00 FMAP 2 PLAN 20 SIZE 0.260 0.380 0.480 ACTA BOND BOND $H CONF HTAB 2 LIST 4 L.S. 10 TEMP 23.00 WGHT 0.041400 0.866300 FVAR 0.20917 RE1 6 0.693317 0.573786 0.346237 11.00000 0.02619 0.04068 = 0.03484 0.00405 0.00720 0.00630 BR1 3 0.853817 0.727411 0.357715 11.00000 0.03962 0.05193 = 0.05098 0.00717 0.00401 -0.00480 C1 1 0.598073 0.703998 0.369997 11.00000 0.04116 0.06349 = 0.05306 0.00683 0.00993 0.01391 C2 1 0.660692 0.611433 0.215516 11.00000 0.03333 0.04165 = 0.04795 0.00718 0.00461 0.00566 C3 1 0.576594 0.455207 0.341942 11.00000 0.02928 0.05525 = 0.05918 -0.00986 -0.00495 0.01019 O4 5 0.729038 0.439809 -0.112473 11.00000 0.05982 0.10962 = 0.03714 0.00313 0.00112 -0.01918 O1 5 0.539507 0.780310 0.385571 11.00000 0.08193 0.09095 = 0.10544 0.01026 0.03149 0.05598 O2 5 0.639568 0.637444 0.138119 11.00000 0.06897 0.06563 = 0.04533 0.01147 -0.00081 0.01221 O3 5 0.510086 0.392593 0.336016 11.00000 0.05409 0.07665 = 0.10063 0.01357 0.01706 -0.00758 S1 7 0.970943 0.303770 0.421337 11.00000 0.03683 0.04932 = 0.04275 0.00154 0.00381 0.01404 N1 4 0.815675 0.429513 0.342512 11.00000 0.03305 0.03632 = 0.03234 0.00077 0.00789 0.00202 N2 4 0.747943 0.532772 0.493110 11.00000 0.03309 0.04362 = 0.03709 0.00281 0.01189 0.00564 C4 1 0.864316 0.397773 0.425623 11.00000 0.03214 0.03407 = 0.03856 0.00397 0.00755 0.00395 C5 1 0.864354 0.377518 0.270360 11.00000 0.03246 0.03899 = 0.03522 -0.00329 0.01055 0.00054 C6 1 0.949533 0.307962 0.301730 11.00000 0.03793 0.05465 = 0.03786 -0.00422 0.01039 0.01231 AFIX 43 H6 2 0.991785 0.266982 0.262858 11.00000 -1.20000 AFIX 0 C7 1 0.827608 0.448720 0.510081 11.00000 0.03092 0.03691 = 0.03467 0.00416 0.00873 0.00110 C8 1 0.870771 0.419233 0.599608 11.00000 0.04403 0.04967 = 0.04004 0.00666 0.00537 0.00314 AFIX 43 H8 2 0.925785 0.361826 0.609453 11.00000 -1.20000 AFIX 0 C9 1 0.831445 0.475841 0.674457 11.00000 0.05018 0.06876 = 0.03171 0.00367 0.00511 -0.00241 AFIX 43 H9 2 0.859435 0.456710 0.735313 11.00000 -1.20000 AFIX 0 C10 1 0.751214 0.560008 0.658226 11.00000 0.05752 0.05759 = 0.03629 -0.00507 0.01635 0.00085 AFIX 43 H10 2 0.723744 0.599092 0.707814 11.00000 -1.20000 AFIX 0 C11 1 0.710798 0.586814 0.566289 11.00000 0.04774 0.05567 = 0.04272 -0.00199 0.01369 0.01147 AFIX 43 H11 2 0.656012 0.644385 0.555517 11.00000 -1.20000 AFIX 0 C12 1 0.824458 0.396975 0.171528 11.00000 0.02885 0.04180 = 0.03709 -0.00452 0.00990 0.00299 C13 1 0.727552 0.351326 0.134002 11.00000 0.03706 0.05879 = 0.04146 0.00432 0.01025 -0.00775 AFIX 43 H13 2 0.684776 0.311444 0.172987 11.00000 -1.20000 AFIX 0 C14 1 0.692078 0.363297 0.039519 11.00000 0.03911 0.05663 = 0.04539 0.00042 0.00099 -0.01029 AFIX 43 H14 2 0.626769 0.330859 0.015642 11.00000 -1.20000 AFIX 0 C15 1 0.754708 0.423906 -0.018851 11.00000 0.04195 0.06127 = 0.03585 -0.00179 0.00446 -0.00119 C16 1 0.851130 0.471527 0.018147 11.00000 0.04546 0.08648 = 0.04229 0.00599 0.01089 -0.01817 AFIX 43 H16 2 0.892889 0.513764 -0.020479 11.00000 -1.20000 AFIX 0 C17 1 0.886120 0.457388 0.111017 11.00000 0.03674 0.06838 = 0.04271 0.00032 0.00845 -0.01170 AFIX 43 H17 2 0.952105 0.488540 0.134264 11.00000 -1.20000 AFIX 0 C18 1 0.625692 0.402647 -0.150756 11.00000 0.08296 0.10857 = 0.05272 0.01302 -0.02068 -0.02873 AFIX 33 H18A 2 0.616800 0.418214 -0.216846 11.00000 -1.50000 H18B 2 0.616401 0.315003 -0.139528 11.00000 -1.50000 H18C 2 0.574212 0.449674 -0.121700 11.00000 -1.50000 AFIX 0 HKLF 4 REM shelxt_a.res in P2(1)/c REM R1 = 0.0341 for 4722 Fo > 4sig(Fo) and 0.0455 for all 5657 data REM 244 parameters refined using 0 restraints END WGHT 0.0414 0.8664 REM Instructions for potential hydrogen bonds EQIV $1 -x+2, y-1/2, -z+1/2 HTAB C6 Br1_$1 EQIV $2 -x+2, -y+1, -z+1 HTAB C8 Br1_$2 EQIV $3 x, -y+3/2, z+1/2 HTAB C11 O2_$3 EQIV $4 x, -y+1/2, z-1/2 HTAB C18 O3_$4 REM Highest difference peak 2.318, deepest hole -0.597, 1-sigma level 0.226 Q1 1 0.6963 0.6460 0.3530 11.00000 0.05 2.32 Q2 1 0.7494 0.5839 0.3686 11.00000 0.05 2.22 Q3 1 0.6939 0.5018 0.3512 11.00000 0.05 1.90 Q4 1 0.6769 0.5778 0.3964 11.00000 0.05 1.84 Q5 1 0.7120 0.5738 0.2998 11.00000 0.05 1.81 Q6 1 0.6374 0.5813 0.3227 11.00000 0.05 1.66 Q7 1 0.5617 0.4209 0.3757 11.00000 0.05 1.35 Q8 1 0.6104 0.4890 0.3543 11.00000 0.05 1.04 Q9 1 0.7763 0.6860 0.3540 11.00000 0.05 1.04 Q10 1 0.8643 0.8062 0.3418 11.00000 0.05 1.01 Q11 1 0.6211 0.6459 0.3491 11.00000 0.05 0.97 Q12 1 0.8580 0.4326 0.3808 11.00000 0.05 0.82 Q13 1 0.5683 0.4479 0.3205 11.00000 0.05 0.78 Q14 1 0.9210 0.7398 0.3800 11.00000 0.05 0.76 Q15 1 0.6802 0.2763 -0.1527 11.00000 0.05 0.72 Q16 1 0.8444 0.4192 0.1436 11.00000 0.05 0.70 Q17 1 0.8173 0.7217 0.4016 11.00000 0.05 0.69 Q18 1 0.4843 0.4168 0.3289 11.00000 0.05 0.66 Q19 1 0.9027 0.5822 -0.0028 11.00000 0.05 0.65 Q20 1 0.8521 0.6410 0.3535 11.00000 0.05 0.64 ; _shelx_res_checksum 95567 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Re Re1 0.69332(2) 0.57379(2) 0.34624(2) 0.03362(6) Uani d 1 . . Br Br1 0.85382(3) 0.72741(4) 0.35771(3) 0.04761(11) Uani d 1 . . C C1 0.5981(4) 0.7040(5) 0.3700(3) 0.0522(11) Uani d 1 . . C C2 0.6607(3) 0.6114(4) 0.2155(3) 0.0410(9) Uani d 1 . . C C3 0.5766(4) 0.4552(5) 0.3419(3) 0.0487(10) Uani d 1 . . O O4 0.7290(3) 0.4398(4) -0.1125(2) 0.0692(11) Uani d 1 . . O O1 0.5395(4) 0.7803(4) 0.3856(3) 0.0912(14) Uani d 1 . . O O2 0.6396(3) 0.6374(3) 0.1381(2) 0.0606(9) Uani d 1 . . O O3 0.5101(3) 0.3926(4) 0.3360(3) 0.0765(11) Uani d 1 . . S S1 0.97094(8) 0.30377(10) 0.42134(7) 0.0430(2) Uani d 1 . . N N1 0.8157(3) 0.4295(3) 0.3425(2) 0.0336(6) Uani d 1 . . N N2 0.7479(3) 0.5328(3) 0.4931(2) 0.0373(7) Uani d 1 . . C C4 0.8643(3) 0.3978(3) 0.4256(3) 0.0347(8) Uani d 1 . . C C5 0.8644(3) 0.3775(4) 0.2704(3) 0.0350(7) Uani d 1 . . C C6 0.9495(3) 0.3080(4) 0.3017(3) 0.0430(9) Uani d 1 . . H H6 0.991785 0.266982 0.262858 0.052 Uiso calc 1 . . C C7 0.8276(3) 0.4487(3) 0.5101(3) 0.0338(8) Uani d 1 . . C C8 0.8708(4) 0.4192(4) 0.5996(3) 0.0445(9) Uani d 1 . . H H8 0.925785 0.361826 0.609453 0.053 Uiso calc 1 . . C C9 0.8314(4) 0.4758(5) 0.6745(3) 0.0502(10) Uani d 1 . . H H9 0.859435 0.456710 0.735313 0.060 Uiso calc 1 . . C C10 0.7512(4) 0.5600(4) 0.6582(3) 0.0496(11) Uani d 1 . . H H10 0.723744 0.599092 0.707814 0.060 Uiso calc 1 . . C C11 0.7108(4) 0.5868(4) 0.5663(3) 0.0480(10) Uani d 1 . . H H11 0.656012 0.644385 0.555517 0.058 Uiso calc 1 . . C C12 0.8245(3) 0.3970(4) 0.1715(3) 0.0354(8) Uani d 1 . . C C13 0.7276(3) 0.3513(4) 0.1340(3) 0.0453(10) Uani d 1 . . H H13 0.684776 0.311444 0.172987 0.054 Uiso calc 1 . . C C14 0.6921(3) 0.3633(4) 0.0395(3) 0.0473(10) Uani d 1 . . H H14 0.626769 0.330859 0.015642 0.057 Uiso calc 1 . . C C15 0.7547(4) 0.4239(4) -0.0189(3) 0.0464(10) Uani d 1 . . C C16 0.8511(4) 0.4715(6) 0.0181(3) 0.0576(12) Uani d 1 . . H H16 0.892889 0.513764 -0.020479 0.069 Uiso calc 1 . . C C17 0.8861(4) 0.4574(5) 0.1110(3) 0.0490(10) Uani d 1 . . H H17 0.952105 0.488540 0.134264 0.059 Uiso calc 1 . . C C18 0.6257(6) 0.4026(7) -0.1508(4) 0.084(2) Uani d 1 . . H H18A 0.616800 0.418214 -0.216846 0.125 Uiso calc 1 . . H H18B 0.616401 0.315003 -0.139528 0.125 Uiso calc 1 . . H H18C 0.574212 0.449674 -0.121700 0.125 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Re1 0.02619(8) 0.04068(9) 0.03484(9) 0.00630(6) 0.00720(6) 0.00405(6) Br1 0.0396(2) 0.0519(2) 0.0510(2) -0.00480(18) 0.00401(17) 0.00717(18) C1 0.041(2) 0.063(3) 0.053(3) 0.014(2) 0.0099(19) 0.007(2) C2 0.033(2) 0.042(2) 0.048(2) 0.0057(16) 0.0046(16) 0.0072(17) C3 0.029(2) 0.055(3) 0.059(3) 0.0102(19) -0.0049(18) -0.010(2) O4 0.060(2) 0.110(3) 0.0371(17) -0.019(2) 0.0011(16) 0.0031(17) O1 0.082(3) 0.091(3) 0.105(3) 0.056(3) 0.031(2) 0.010(2) O2 0.069(2) 0.066(2) 0.0453(18) 0.0122(18) -0.0008(15) 0.0115(15) O3 0.054(2) 0.077(3) 0.101(3) -0.008(2) 0.017(2) 0.014(2) S1 0.0368(5) 0.0493(6) 0.0428(5) 0.0140(4) 0.0038(4) 0.0015(4) N1 0.0330(17) 0.0363(16) 0.0323(16) 0.0020(12) 0.0079(12) 0.0008(11) N2 0.0331(17) 0.0436(17) 0.0371(16) 0.0056(14) 0.0119(13) 0.0028(13) C4 0.0321(19) 0.0341(18) 0.039(2) 0.0040(14) 0.0075(15) 0.0040(14) C5 0.0325(19) 0.0390(19) 0.0352(18) 0.0005(15) 0.0106(14) -0.0033(14) C6 0.038(2) 0.055(2) 0.038(2) 0.0123(18) 0.0104(16) -0.0042(17) C7 0.0309(18) 0.0369(19) 0.0347(18) 0.0011(14) 0.0087(14) 0.0042(13) C8 0.044(2) 0.050(2) 0.040(2) 0.0031(18) 0.0054(17) 0.0067(16) C9 0.050(3) 0.069(3) 0.032(2) -0.002(2) 0.0051(17) 0.0037(19) C10 0.058(3) 0.058(3) 0.036(2) 0.001(2) 0.0163(19) -0.0051(17) C11 0.048(3) 0.056(3) 0.043(2) 0.0115(19) 0.0137(19) -0.0020(18) C12 0.0289(18) 0.042(2) 0.0371(19) 0.0030(14) 0.0099(14) -0.0045(14) C13 0.037(2) 0.059(3) 0.041(2) -0.0078(19) 0.0103(17) 0.0043(18) C14 0.039(2) 0.057(3) 0.045(2) -0.0103(19) 0.0010(17) 0.0004(19) C15 0.042(2) 0.061(3) 0.036(2) -0.0012(19) 0.0045(17) -0.0018(17) C16 0.045(3) 0.086(4) 0.042(2) -0.018(2) 0.0109(19) 0.006(2) C17 0.037(2) 0.068(3) 0.043(2) -0.012(2) 0.0084(18) 0.0003(19) C18 0.083(5) 0.109(5) 0.053(3) -0.029(4) -0.021(3) 0.013(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.006 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Re Re -1.0185 7.231 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C1 Re1 C2 . . 87.31(18) ? C1 Re1 C3 . . 88.9(2) ? C2 Re1 C3 . . 91.56(19) ? C1 Re1 N2 . . 96.34(16) ? C2 Re1 N2 . . 174.02(14) ? C3 Re1 N2 . . 93.25(17) ? C1 Re1 N1 . . 170.47(17) ? C2 Re1 N1 . . 101.33(15) ? C3 Re1 N1 . . 94.84(16) ? N2 Re1 N1 . . 74.72(12) ? C1 Re1 Br1 . . 92.31(15) ? C2 Re1 Br1 . . 90.54(13) ? C3 Re1 Br1 . . 177.63(14) ? N2 Re1 Br1 . . 84.59(9) ? N1 Re1 Br1 . . 83.67(8) ? O1 C1 Re1 . . 178.3(5) ? O2 C2 Re1 . . 177.8(4) ? O3 C3 Re1 . . 176.7(5) ? C15 O4 C18 . . 117.0(4) ? C4 S1 C6 . . 89.20(19) ? C4 N1 C5 . . 111.8(3) ? C4 N1 Re1 . . 114.6(2) ? C5 N1 Re1 . . 132.8(3) ? C11 N2 C7 . . 118.1(3) ? C11 N2 Re1 . . 124.9(3) ? C7 N2 Re1 . . 117.0(2) ? N1 C4 C7 . . 119.7(3) ? N1 C4 S1 . . 114.3(3) ? C7 C4 S1 . . 125.9(3) ? C6 C5 N1 . . 112.5(3) ? C6 C5 C12 . . 125.2(3) ? N1 C5 C12 . . 122.3(3) ? C5 C6 S1 . . 112.3(3) ? C5 C6 H6 . . 123.9 ? S1 C6 H6 . . 123.9 ? N2 C7 C8 . . 122.0(4) ? N2 C7 C4 . . 113.7(3) ? C8 C7 C4 . . 124.3(4) ? C7 C8 C9 . . 119.3(4) ? C7 C8 H8 . . 120.4 ? C9 C8 H8 . . 120.4 ? C10 C9 C8 . . 119.3(4) ? C10 C9 H9 . . 120.4 ? C8 C9 H9 . . 120.4 ? C9 C10 C11 . . 119.1(4) ? C9 C10 H10 . . 120.4 ? C11 C10 H10 . . 120.4 ? N2 C11 C10 . . 122.3(4) ? N2 C11 H11 . . 118.8 ? C10 C11 H11 . . 118.8 ? C13 C12 C17 . . 117.5(4) ? C13 C12 C5 . . 121.6(3) ? C17 C12 C5 . . 120.9(4) ? C12 C13 C14 . . 121.8(4) ? C12 C13 H13 . . 119.1 ? C14 C13 H13 . . 119.1 ? C15 C14 C13 . . 119.5(4) ? C15 C14 H14 . . 120.2 ? C13 C14 H14 . . 120.2 ? O4 C15 C16 . . 116.0(4) ? O4 C15 C14 . . 124.8(4) ? C16 C15 C14 . . 119.2(4) ? C17 C16 C15 . . 120.8(4) ? C17 C16 H16 . . 119.6 ? C15 C16 H16 . . 119.6 ? C16 C17 C12 . . 121.2(4) ? C16 C17 H17 . . 119.4 ? C12 C17 H17 . . 119.4 ? O4 C18 H18A . . 109.5 ? O4 C18 H18B . . 109.5 ? H18A C18 H18B . . 109.5 ? O4 C18 H18C . . 109.5 ? H18A C18 H18C . . 109.5 ? H18B C18 H18C . . 109.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Re1 C1 . 1.903(5) yes Re1 C2 . 1.923(4) yes Re1 C3 . 1.950(5) yes Re1 N2 . 2.193(3) ? Re1 N1 . 2.198(3) ? Re1 Br1 . 2.6129(5) yes C1 O1 . 1.145(5) yes C2 O2 . 1.150(5) yes C3 O3 . 1.075(6) yes O4 C15 . 1.361(5) ? O4 C18 . 1.424(7) ? S1 C4 . 1.697(4) ? S1 C6 . 1.713(4) ? N1 C4 . 1.327(5) ? N1 C5 . 1.387(5) ? N2 C11 . 1.336(5) ? N2 C7 . 1.356(5) ? C4 C7 . 1.458(5) ? C5 C6 . 1.350(5) ? C5 C12 . 1.470(5) ? C6 H6 . 0.9300 ? C7 C8 . 1.379(5) ? C8 C9 . 1.380(6) ? C8 H8 . 0.9300 ? C9 C10 . 1.361(7) ? C9 H9 . 0.9300 ? C10 C11 . 1.394(6) ? C10 H10 . 0.9300 ? C11 H11 . 0.9300 ? C12 C13 . 1.379(5) ? C12 C17 . 1.397(5) ? C13 C14 . 1.389(6) ? C13 H13 . 0.9300 ? C14 C15 . 1.385(6) ? C14 H14 . 0.9300 ? C15 C16 . 1.379(6) ? C16 C17 . 1.368(6) ? C16 H16 . 0.9300 ? C17 H17 . 0.9300 ? C18 H18A . 0.9600 ? C18 H18B . 0.9600 ? C18 H18C . 0.9600 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C6 H6 Br1 2_745 0.93 2.80 3.691(4) 160.2 yes C8 H8 Br1 3_766 0.93 2.95 3.828(5) 157.5 yes C11 H11 O2 4_576 0.93 2.64 3.285(6) 127.4 yes C18 H18B O3 4_565 0.96 2.60 3.478(8) 151.8 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C5 N1 C4 C7 . . . . 176.9(3) ? Re1 N1 C4 C7 . . . . 6.1(4) ? C5 N1 C4 S1 . . . . 0.0(4) ? Re1 N1 C4 S1 . . . . -170.94(17) ? C6 S1 C4 N1 . . . . 0.3(3) ? C6 S1 C4 C7 . . . . -176.5(4) ? C4 N1 C5 C6 . . . . -0.4(5) ? Re1 N1 C5 C6 . . . . 168.3(3) ? C4 N1 C5 C12 . . . . 179.0(4) ? Re1 N1 C5 C12 . . . . -12.3(6) ? N1 C5 C6 S1 . . . . 0.6(5) ? C12 C5 C6 S1 . . . . -178.7(3) ? C4 S1 C6 C5 . . . . -0.5(3) ? C11 N2 C7 C8 . . . . -0.5(6) ? Re1 N2 C7 C8 . . . . 177.6(3) ? C11 N2 C7 C4 . . . . -178.4(4) ? Re1 N2 C7 C4 . . . . -0.3(4) ? N1 C4 C7 N2 . . . . -3.9(5) ? S1 C4 C7 N2 . . . . 172.7(3) ? N1 C4 C7 C8 . . . . 178.2(4) ? S1 C4 C7 C8 . . . . -5.1(6) ? N2 C7 C8 C9 . . . . 0.6(6) ? C4 C7 C8 C9 . . . . 178.2(4) ? C7 C8 C9 C10 . . . . -0.3(7) ? C8 C9 C10 C11 . . . . 0.0(7) ? C7 N2 C11 C10 . . . . 0.2(7) ? Re1 N2 C11 C10 . . . . -177.7(3) ? C9 C10 C11 N2 . . . . 0.0(7) ? C6 C5 C12 C13 . . . . 114.1(5) ? N1 C5 C12 C13 . . . . -65.2(5) ? C6 C5 C12 C17 . . . . -62.7(6) ? N1 C5 C12 C17 . . . . 118.0(4) yes C17 C12 C13 C14 . . . . 0.6(6) ? C5 C12 C13 C14 . . . . -176.3(4) ? C12 C13 C14 C15 . . . . -0.8(7) ? C18 O4 C15 C16 . . . . -173.9(5) ? C18 O4 C15 C14 . . . . 6.8(8) ? C13 C14 C15 O4 . . . . 179.1(4) ? C13 C14 C15 C16 . . . . -0.2(7) ? O4 C15 C16 C17 . . . . -178.0(5) ? C14 C15 C16 C17 . . . . 1.3(8) ? C15 C16 C17 C12 . . . . -1.5(8) ? C13 C12 C17 C16 . . . . 0.5(7) ? C5 C12 C17 C16 . . . . 177.4(5) ?