#------------------------------------------------------------------------------
#$Date: 2024-11-09 03:45:59 +0100 (Sat, 09 Nov 2024) $
#$Revision: 295851 $
#$URL: svn://www.crystallography.net/cod/cif/2/02/33/2023310.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2023310
loop_
_publ_author_name
'Le, Canh Dinh'
'Nguyen, Hoang Phuc'
'Pham, Chien Thang'
_publ_section_title
;
Crystal structure of a solvated dinuclear CuII complex derived from
3,3,3′,3′-tetraethyl-1,1′-(furan-2,5-dicarbonyl)bis(thiourea)
;
_journal_coeditor_code OO2007
_journal_issue 12
_journal_name_full
'Acta Crystallographica Section E Crystallographic Communications'
_journal_paper_doi 10.1107/S2056989024010703
_journal_volume 80
_journal_year 2024
_chemical_formula_iupac '[Cu2 (C16 H22 N4 O3 S2)2], 2C H2 Cl2'
_chemical_formula_moiety 'C32 H44 Cu2 N8 O6 S4, 2(C H2 Cl2)'
_chemical_formula_sum 'C34 H48 Cl4 Cu2 N8 O6 S4'
_chemical_formula_weight 1061.92
_chemical_name_systematic
'Bis[\m-3,3,3',3'-tetraethyl-1,1'-(furan-2,5-dicarbonyl)bis(thioureato)]dicopper(II) dichloromethane disolvate'
_space_group_crystal_system monoclinic
_space_group_IT_number 14
_space_group_name_Hall '-P 2yn'
_space_group_name_H-M_alt 'P 1 21/n 1'
_atom_sites_solution_hydrogens geom
_atom_sites_solution_primary dual
_audit_creation_method
;
Olex2 1.5
(compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928)
;
_cell_angle_alpha 90
_cell_angle_beta 98.377(3)
_cell_angle_gamma 90
_cell_formula_units_Z 2
_cell_length_a 10.2290(9)
_cell_length_b 13.0681(10)
_cell_length_c 16.9601(15)
_cell_measurement_reflns_used 8429
_cell_measurement_temperature 140(2)
_cell_measurement_theta_max 28.63
_cell_measurement_theta_min 2.89
_cell_volume 2242.9(3)
_computing_cell_refinement
;
APEX2 (Bruker, 2014)
;
_computing_data_collection
;
SAINT (Bruker, 2014)
;
_computing_data_reduction
;
SAINT (Bruker, 2014)
;
_computing_molecular_graphics
;
Olex2 1.5 (Dolomanov et al., 2009)
;
_computing_publication_material
;
Olex2 1.5 (Dolomanov et al., 2009)
;
_computing_structure_refinement
;
SHELXL2018/3 (Sheldrick, 2015b)
;
_computing_structure_solution
;
SHELXT2014/5 (Sheldrick, 2015a)
;
_diffrn_ambient_temperature 140(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type 'Bruker APEXII CCD'
_diffrn_measurement_method '\f and \w scans'
_diffrn_radiation_type MoK\a
_diffrn_radiation_wavelength 0.71073
_diffrn_reflns_av_R_equivalents 0.0619
_diffrn_reflns_av_unetI/netI 0.0554
_diffrn_reflns_limit_h_max 12
_diffrn_reflns_limit_h_min -13
_diffrn_reflns_limit_k_max 17
_diffrn_reflns_limit_k_min -16
_diffrn_reflns_limit_l_max 22
_diffrn_reflns_limit_l_min -22
_diffrn_reflns_number 29179
_diffrn_reflns_theta_full 25.242
_diffrn_reflns_theta_max 28.761
_diffrn_reflns_theta_min 2.885
_diffrn_source_current 30.0
_diffrn_source_power 1.5
_diffrn_source_voltage 50.0
_diffrn_standards_number 0
_exptl_absorpt_coefficient_mu 1.424
_exptl_absorpt_correction_T_max 0.7458
_exptl_absorpt_correction_T_min 0.6859
_exptl_absorpt_correction_type multi-scan
_exptl_absorpt_process_details
;
(SADABS; Krause et al., 2015)
;
_exptl_crystal_colour red
_exptl_crystal_density_diffrn 1.572
_exptl_crystal_description plate
_exptl_crystal_F_000 1092
_exptl_crystal_size_max 0.135
_exptl_crystal_size_mid 0.076
_exptl_crystal_size_min 0.054
_refine_diff_density_max 0.498
_refine_diff_density_min -0.445
_refine_ls_extinction_method none
_refine_ls_goodness_of_fit_ref 1.030
_refine_ls_hydrogen_treatment constr
_refine_ls_matrix_type full
_refine_ls_number_parameters 276
_refine_ls_number_reflns 5809
_refine_ls_number_restraints 0
_refine_ls_restrained_S_all 1.030
_refine_ls_R_factor_all 0.0713
_refine_ls_R_factor_gt 0.0376
_refine_ls_shift/su_max 0.001
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0292P)^2^+0.9669P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.0675
_refine_ls_wR_factor_ref 0.0760
_reflns_number_gt 4232
_reflns_number_total 5809
_reflns_threshold_expression 'I > 2\s(I)'
_cod_data_source_file oo2007.cif
_cod_data_source_block I
_cod_database_code 2023310
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min 0.831
_shelx_estimated_absorpt_t_max 0.927
_shelx_hkl_file
;
2 0 0 549.65 17.80
2 0 0 575.24 17.60
-2 0 0 551.64 18.00
-3 0 0 1.10 1.60
-3 0 0 -0.30 2.00
3 0 0 -1.60 1.70
3 0 0 -1.80 1.80
-4 0 0 31.80 4.20
-4 0 0 30.70 3.70
4 0 0 22.30 3.20
-5 0 0 0.10 2.40
5 0 0 -2.60 2.50
-5 0 0 -2.10 2.40
6 0 0 1375.86 45.10
-6 0 0 1372.36 45.10
-6 0 0 1371.36 44.00
-7 0 0 -1.20 4.20
-7 0 0 7.60 4.00
7 0 0 4.90 4.20
8 0 0 109.79 10.40
-8 0 0 98.39 9.80
-8 0 0 92.29 10.10
-9 0 0 -0.90 6.20
9 0 0 -5.90 6.80
-9 0 0 -0.60 5.00
10 0 0 345.17 21.00
-10 0 0 355.16 19.30
-10 0 0 332.37 21.30
-11 0 0 -5.80 7.60
-11 0 0 -1.00 10.50
-11 0 0 0.00 9.70
-12 0 0 186.88 19.90
-12 0 0 192.78 20.20
-13 0 0 -36.20 14.00
-13 0 0 19.20 13.40
-2 -1 0 42.50 3.40
2 -1 0 44.90 3.30
2 -1 0 45.20 3.10
-2 1 0 45.30 3.20
2 1 0 43.90 3.50
3 -1 0 20.60 2.80
-3 -1 0 23.80 3.20
3 -1 0 16.10 2.50
-3 -1 0 16.30 2.20
-3 1 0 20.70 2.80
-3 1 0 19.30 2.80
3 1 0 16.80 2.80
-4 -1 0 81.29 5.20
4 -1 0 86.19 5.80
-4 -1 0 83.29 6.00
4 -1 0 98.59 5.70
-4 1 0 75.99 5.70
4 1 0 95.09 6.10
-4 1 0 97.19 6.30
5 -1 0 156.98 8.50
-5 -1 0 148.19 8.80
5 -1 0 145.19 8.40
-5 -1 0 141.29 7.80
-5 1 0 149.88 8.50
5 1 0 153.68 8.70
-5 1 0 162.18 8.70
-6 -1 0 19.90 4.40
6 -1 0 24.00 5.00
-6 -1 0 24.60 4.30
-6 1 0 20.60 4.40
-6 1 0 26.70 4.60
-7 -1 0 339.27 16.70
-7 -1 0 346.57 15.10
7 -1 0 363.56 16.30
7 1 0 316.57 16.00
-7 1 0 349.37 16.30
-7 1 0 342.87 15.50
-8 -1 0 -0.30 4.20
-8 -1 0 -0.10 4.90
8 -1 0 2.00 5.40
8 1 0 3.20 4.90
-8 1 0 -2.50 4.90
-8 1 0 2.20 5.00
-9 -1 0 2.20 5.40
-9 -1 0 11.10 6.10
9 -1 0 1.80 7.10
-9 1 0 7.10 5.90
-9 1 0 10.30 6.40
9 1 0 14.10 7.10
10 -1 0 32.20 10.40
-10 -1 0 27.90 7.50
-10 -1 0 19.40 8.30
-10 -1 0 25.60 9.30
-10 1 0 23.40 8.40
-10 1 0 33.40 9.60
10 1 0 22.80 9.40
-11 -1 0 15.30 10.20
-11 -1 0 10.50 10.50
-11 1 0 19.70 9.30
-11 1 0 7.30 9.40
-12 -1 0 3.90 11.60
-12 -1 0 15.50 11.00
-12 1 0 -9.80 10.90
-12 1 0 8.00 11.10
-13 -1 0 24.40 16.20
-13 -1 0 63.09 14.40
-13 1 0 112.99 16.70
-13 1 0 44.50 16.10
0 -2 0 398.36 12.90
0 2 0 407.46 12.00
1 -2 0 138.79 5.60
1 -2 0 131.39 4.50
-1 -2 0 131.49 5.20
-1 -2 0 136.19 4.70
1 2 0 140.29 5.30
-1 2 0 138.59 4.50
1 2 0 132.29 4.70
2 -2 0 434.26 13.80
2 -2 0 438.76 14.70
-2 -2 0 433.56 13.60
-2 -2 0 425.36 14.60
-2 2 0 420.46 14.60
-2 2 0 435.56 13.90
2 2 0 427.66 14.60
2 2 0 427.26 13.60
-3 -2 0 84.59 5.70
3 -2 0 92.29 5.60
3 -2 0 83.79 4.80
-3 -2 0 84.69 4.50
3 2 0 76.99 5.30
-3 2 0 83.79 5.20
-3 2 0 88.99 5.10
4 -2 0 964.20 31.10
-4 -2 0 935.71 30.00
-4 -2 0 969.50 31.40
-4 -2 0 955.30 29.70
4 -2 0 958.10 30.60
-4 2 0 912.91 30.90
-4 2 0 941.71 30.60
4 2 0 972.90 31.40
-5 -2 0 32.40 3.90
-5 -2 0 44.80 5.00
5 -2 0 35.00 4.70
5 -2 0 31.90 4.40
-5 -2 0 38.00 5.20
5 2 0 40.60 6.30
-5 2 0 38.60 4.70
-5 2 0 36.50 5.10
6 -2 0 9.90 4.00
-6 -2 0 5.60 3.00
-6 -2 0 4.70 3.20
-6 -2 0 4.40 3.90
6 -2 0 6.90 3.80
-6 2 0 8.50 3.60
-6 2 0 9.10 3.40
6 2 0 3.50 3.80
-7 -2 0 5.90 3.40
-7 -2 0 3.40 4.20
-7 -2 0 7.80 4.00
7 -2 0 9.60 4.70
7 2 0 2.00 4.40
-7 2 0 9.90 4.70
-7 2 0 4.60 4.20
-8 -2 0 29.00 6.50
8 -2 0 41.50 7.20
-8 -2 0 15.90 6.00
-8 -2 0 29.60 5.50
-8 2 0 27.40 6.50
8 2 0 32.90 6.90
-8 2 0 41.20 7.00
-9 -2 0 -2.80 6.30
-9 -2 0 4.50 6.80
9 -2 0 0.50 6.70
-9 -2 0 1.60 5.30
-9 2 0 7.20 6.10
-9 2 0 -5.40 5.90
9 2 0 2.60 7.10
10 -2 0 251.97 19.10
-10 -2 0 191.08 17.60
-10 -2 0 244.58 17.90
-10 -2 0 217.98 14.90
10 2 0 202.18 16.90
-10 2 0 182.28 23.40
-11 -2 0 183.08 17.80
-11 -2 0 206.68 19.80
-11 -2 0 248.08 17.80
11 -2 0 252.47 27.10
-11 2 0 166.78 19.00
-11 2 0 182.38 18.30
-12 -2 0 62.29 13.80
-12 -2 0 86.99 12.90
-12 -2 0 94.19 15.80
-12 2 0 73.69 15.10
-12 2 0 66.59 14.40
-13 -2 0 11.90 13.30
-13 -2 0 -26.00 13.60
-13 2 0 -10.40 14.80
-13 2 0 26.80 14.30
0 -3 0 0.10 0.70
0 -3 0 -0.80 1.10
0 3 0 -0.10 0.60
0 3 0 -2.40 0.90
1 -3 0 1124.99 32.50
-1 -3 0 1078.49 31.40
-1 -3 0 962.20 32.40
-1 3 0 1074.49 32.50
1 3 0 1078.19 31.50
1 3 0 1042.00 31.80
-1 3 0 1078.29 30.60
2 -3 0 1582.94 45.50
-2 -3 0 1547.25 45.40
2 -3 0 1469.85 46.80
-2 -3 0 1555.14 46.70
-2 3 0 1640.04 45.50
-2 3 0 1517.25 46.90
2 3 0 1524.95 45.40
2 3 0 1556.04 46.70
-3 -3 0 727.23 24.00
3 -3 0 731.93 24.10
-3 -3 0 716.93 22.40
3 -3 0 702.23 22.70
-3 3 0 726.13 22.80
-3 3 0 711.43 24.00
3 3 0 712.73 23.90
-4 -3 0 556.84 20.00
4 -3 0 524.15 18.60
-4 -3 0 558.04 18.20
4 -3 0 521.35 19.50
-4 3 0 533.95 19.70
4 3 0 553.34 19.80
-4 3 0 539.15 18.70
5 -3 0 8.60 3.40
-5 -3 0 6.70 3.30
-5 -3 0 14.70 2.90
-5 -3 0 16.50 3.00
5 -3 0 13.10 3.40
5 3 0 8.40 3.20
-5 3 0 10.10 2.80
-5 3 0 10.90 3.60
-6 -3 0 9.80 3.40
6 -3 0 6.70 4.00
6 -3 0 3.90 3.30
-6 -3 0 8.00 3.10
-6 -3 0 4.90 3.90
-6 3 0 9.20 3.70
6 3 0 8.60 3.90
-6 3 0 6.60 3.60
7 -3 0 2.00 5.00
-7 -3 0 1.70 4.30
7 -3 0 9.60 4.60
-7 -3 0 3.10 3.30
-7 -3 0 2.00 6.90
-7 3 0 6.00 4.90
-7 3 0 3.00 4.10
7 3 0 0.90 4.70
8 -3 0 3.40 5.70
-8 -3 0 0.10 4.40
-8 -3 0 -0.10 5.20
-8 3 0 -7.70 4.70
-8 3 0 3.70 5.00
8 3 0 -4.30 5.80
-9 -3 0 350.06 16.90
9 -3 0 381.26 19.70
-9 -3 0 332.87 23.30
-9 -3 0 320.47 17.70
-9 3 0 344.07 18.70
-9 3 0 333.97 18.30
9 3 0 309.97 19.30
10 -3 0 195.58 17.00
-10 -3 0 187.18 14.50
-10 -3 0 190.38 16.10
-10 -3 0 223.68 16.80
10 3 0 233.68 18.00
-10 3 0 200.48 17.20
-10 3 0 220.18 17.90
11 -3 0 8.80 11.50
-11 -3 0 -2.70 9.90
-11 -3 0 12.40 8.40
-11 -3 0 -15.10 10.20
-11 3 0 -3.20 9.30
-11 3 0 -5.70 8.70
-12 -3 0 223.58 24.10
-12 -3 0 275.97 20.90
-12 -3 0 238.08 25.10
-12 3 0 258.17 23.00
-12 3 0 194.78 22.90
-13 -3 0 11.60 16.50
-13 -3 0 44.70 14.50
-13 3 0 68.29 17.70
-13 3 0 30.00 15.60
0 -4 0 894.41 26.70
0 -4 0 896.81 27.80
0 4 0 917.81 27.90
0 4 0 915.91 26.70
-1 -4 0 310.17 10.00
1 -4 0 292.87 10.90
-1 4 0 288.47 11.00
1 4 0 269.87 10.70
1 4 0 287.27 10.10
-2 -4 0 265.97 10.20
2 -4 0 255.87 8.50
2 -4 0 252.47 10.40
-2 -4 0 261.07 9.00
2 4 0 262.47 10.10
2 4 0 242.98 9.10
-2 4 0 258.37 8.50
-2 4 0 254.97 10.50
3 -4 0 4.00 1.60
-3 -4 0 2.50 1.50
3 -4 0 1.40 2.30
-3 -4 0 6.20 2.70
3 4 0 3.30 1.70
-3 4 0 2.40 1.60
-3 4 0 3.60 2.90
3 4 0 2.00 2.10
4 -4 0 44.70 5.40
-4 -4 0 47.90 6.00
-4 -4 0 48.50 4.20
4 -4 0 53.89 4.40
-4 4 0 56.79 4.60
-4 4 0 54.49 6.00
4 4 0 48.50 5.20
-5 -4 0 72.09 5.70
-5 -4 0 73.99 5.20
5 -4 0 80.49 6.20
5 -4 0 83.59 7.70
-5 -4 0 79.29 7.60
-5 4 0 88.49 7.50
-5 4 0 84.09 6.50
5 4 0 72.79 6.90
-6 -4 0 36.60 4.40
6 -4 0 40.00 6.40
-6 -4 0 32.80 4.60
6 -4 0 41.70 5.40
-6 -4 0 31.60 5.90
6 4 0 35.40 6.10
-6 4 0 45.00 6.30
-6 4 0 35.20 5.00
-7 -4 0 16.30 5.90
-7 -4 0 22.80 4.40
7 -4 0 24.80 6.20
-7 -4 0 23.60 4.70
-7 4 0 26.20 5.40
7 4 0 14.40 5.40
-7 4 0 25.60 5.40
8 -4 0 18.40 6.40
8 -4 0 13.40 6.60
-8 -4 0 9.70 6.00
-8 -4 0 10.20 4.30
-8 -4 0 10.90 5.30
8 4 0 6.70 6.10
-8 4 0 3.70 6.30
-8 4 0 14.30 5.50
-9 -4 0 39.90 9.60
-9 -4 0 24.50 6.20
-9 -4 0 4.60 6.40
9 -4 0 7.00 7.30
-9 4 0 23.10 7.30
9 4 0 8.40 8.40
-9 4 0 12.70 8.10
10 -4 0 -9.70 8.30
-10 -4 0 -7.00 7.80
-10 -4 0 -8.20 8.00
-10 -4 0 -4.00 6.00
-10 4 0 -6.80 7.70
-10 4 0 -12.30 7.40
-11 -4 0 241.08 20.90
-11 -4 0 293.57 21.50
11 -4 0 291.27 24.10
-11 -4 0 322.97 18.80
-11 4 0 304.07 21.40
-11 4 0 269.67 21.00
-12 -4 0 -22.70 11.60
-12 -4 0 28.50 14.50
-12 -4 0 22.80 10.90
-12 4 0 30.90 13.50
-12 4 0 -12.10 11.80
-13 -4 0 -10.10 13.30
-13 -4 0 -37.80 14.30
-13 4 0 11.30 14.50
-13 4 0 29.90 16.90
0 -5 0 -1.00 1.00
0 -5 0 -4.50 1.50
0 5 0 0.00 1.00
0 5 0 -0.30 1.70
-1 -5 0 61.39 3.90
-1 -5 0 47.10 3.70
1 -5 0 50.29 4.40
1 5 0 52.39 3.70
1 5 0 60.59 3.90
-1 5 0 57.69 4.60
2 -5 0 1465.25 44.90
-2 -5 0 1461.65 42.90
-2 -5 0 1435.56 44.10
2 5 0 1358.16 43.90
-2 5 0 1466.75 45.00
-2 5 0 1487.65 41.80
2 5 0 1410.66 43.50
3 -5 0 71.19 6.00
-3 -5 0 63.19 5.60
3 -5 0 66.09 3.90
-3 -5 0 63.89 4.00
3 5 0 60.09 5.50
-3 5 0 61.29 5.60
3 5 0 66.19 4.10
4 -5 0 58.29 4.40
-4 -5 0 51.39 5.80
-4 -5 0 59.09 4.40
4 -5 0 62.59 6.40
4 5 0 58.59 5.70
-4 5 0 60.29 4.70
-4 5 0 61.69 6.60
5 -5 0 -1.50 2.50
5 -5 0 -0.20 3.60
-5 -5 0 -2.90 3.20
-5 -5 0 -1.60 2.30
5 5 0 -5.00 3.60
-5 5 0 4.10 3.00
-5 5 0 -1.20 3.30
6 -5 0 45.40 6.60
-6 -5 0 27.30 5.60
6 -5 0 32.20 4.90
-6 -5 0 47.70 5.10
-6 -5 0 37.40 4.70
-6 5 0 33.00 5.10
6 5 0 32.80 6.00
-6 5 0 33.50 6.20
-7 -5 0 6.30 5.50
7 -5 0 4.40 4.80
-7 -5 0 12.80 4.00
-7 -5 0 11.50 4.60
7 -5 0 8.80 5.50
7 5 0 4.90 5.40
-7 5 0 6.00 5.40
-7 5 0 7.60 4.20
-8 -5 0 897.01 30.60
-8 -5 0 902.21 35.20
8 -5 0 847.62 32.50
-8 -5 0 907.11 31.50
8 -5 0 955.50 35.00
-8 5 0 874.11 34.50
-8 5 0 886.91 32.90
8 5 0 854.91 34.80
9 -5 0 25.80 8.50
-9 -5 0 28.10 7.10
-9 -5 0 29.00 8.80
-9 -5 0 30.30 6.40
-9 5 0 31.70 8.10
-9 5 0 33.30 8.00
9 5 0 29.40 9.50
10 -5 0 18.10 9.70
-10 -5 0 1.50 6.50
-10 -5 0 1.40 8.20
-10 -5 0 -0.30 7.70
-10 5 0 10.60 8.60
-10 5 0 17.60 9.80
-11 -5 0 5.30 8.20
11 -5 0 -12.20 11.60
-11 -5 0 -18.10 9.60
-11 -5 0 -3.80 10.60
-11 5 0 29.40 11.60
-11 5 0 -5.60 9.50
-12 -5 0 -25.90 13.10
-12 -5 0 -9.40 14.20
-12 -5 0 11.90 10.90
-12 5 0 3.60 13.50
-12 5 0 3.40 12.30
-13 -5 0 -7.20 13.40
-13 5 0 14.90 17.70
-13 5 0 18.10 14.90
0 -6 0 488.45 17.10
0 -6 0 497.05 15.40
0 6 0 499.65 15.40
0 6 0 500.65 17.30
-1 -6 0 1113.29 34.20
-1 -6 0 1091.59 33.80
1 -6 0 1108.29 35.20
1 6 0 1100.29 34.20
1 6 0 1113.99 33.80
-1 6 0 1131.69 35.40
2 -6 0 92.39 6.80
-2 -6 0 105.49 5.30
-2 -6 0 88.79 5.90
2 6 0 101.39 5.40
2 6 0 97.99 6.10
-2 6 0 112.09 7.30
-3 -6 0 819.22 25.70
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1 -1 22 30.60 17.50
1 1 22 76.49 19.20
-1 1 -22 8.50 19.40
-5 -2 22 17.90 14.80
-5 2 22 -10.90 15.50
-4 -2 22 124.69 18.00
-4 2 22 99.19 17.90
-3 -2 22 33.20 14.40
-3 2 22 26.50 15.70
2 -2 -22 -6.00 15.00
-2 -2 22 17.60 14.80
-2 2 22 53.39 17.50
-1 -2 22 68.69 17.60
1 -2 -22 15.40 17.30
-1 2 22 44.10 16.00
1 2 -22 37.10 17.70
0 -2 -22 22.80 17.00
0 -2 22 18.00 16.30
0 2 22 16.90 16.20
0 2 -22 -6.60 16.20
-1 -2 -22 12.50 18.90
1 -2 22 3.80 16.70
1 2 22 -4.50 17.30
-5 -3 22 38.10 15.30
-5 3 22 9.00 17.50
-4 -3 22 34.90 14.70
-4 3 22 41.00 16.70
-3 -3 22 11.60 14.70
-3 3 22 11.30 16.50
2 -3 -22 -12.40 14.50
-2 -3 22 16.10 15.60
-2 3 22 -4.60 15.20
1 -3 -22 65.09 18.60
-1 -3 22 64.29 17.70
1 3 -22 57.59 17.40
-1 3 22 32.10 18.10
0 -3 -22 29.60 18.00
0 -3 22 3.70 16.50
0 3 -22 35.20 17.20
0 3 22 76.99 17.10
-1 -3 -22 -5.60 18.70
1 3 22 18.80 28.40
-4 -4 22 27.60 15.80
-4 4 22 27.80 18.00
-3 -4 22 219.68 26.10
3 -4 -22 130.59 21.00
-3 4 22 144.19 21.80
-2 -4 22 10.50 14.90
2 -4 -22 -1.90 17.30
-2 4 22 12.40 17.80
1 -4 -22 10.60 16.10
-1 4 22 11.90 16.90
1 4 -22 19.40 20.00
0 -4 -22 68.79 20.90
0 4 22 48.70 28.90
0 0 0 0.00 0.00
_computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)'
;
_shelx_hkl_checksum 49347
_shelx_res_file
;
TITL tpculfur_0m_a.res in P2(1)/n
tpculfur_0m.res
created by SHELXL-2018/3 at 12:37:17 on 29-Oct-2024
REM Old TITL tpCuLfur_0m in P2(1)/n
REM SHELXT solution in P2(1)/n
REM R1 0.109, Rweak 0.006, Alpha 0.029, Orientation as input
REM Formula found by SHELXT: C17 N5 O2 S2 Cl2 Cu
CELL 0.71073 10.229 13.0681 16.9601 90 98.377 90
ZERR 2 0.0009 0.001 0.0015 0 0.003 0
LATT 1
SYMM 0.5-X,0.5+Y,0.5-Z
SFAC C H Cl Cu N O S
UNIT 68 96 8 4 16 12 8
EQIV $1 1-X,1-Y,1-Z
EQIV $2 0.5+X,0.5-Y,-0.5+Z
EQIV $3 -0.5+X,0.5-Y,-0.5+Z
L.S. 30
PLAN 5
SIZE 0.054 0.076 0.135
TEMP -133(2)
CONF
HTAB C30 O10
HTAB C4 Cl2B_$3
HTAB C4 Cl2A_$3
HTAB C30 O10_$1
HTAB C14 Cl1_$2
BOND $H
BOND
list 4
MORE -1
fmap 2
acta
REM
REM
REM
WGHT 0.029200 0.966900
FVAR 0.31786 0.61640
CU1 4 0.845171 0.554254 0.439775 11.00000 0.01290 0.02103 =
0.01530 -0.00410 0.00497 -0.00403
S20 7 -0.027635 0.360022 0.504701 11.00000 0.01409 0.01841 =
0.02314 -0.00438 0.00688 -0.00343
S10 7 0.921898 0.551373 0.321243 11.00000 0.02143 0.02666 =
0.01914 -0.00417 0.00957 -0.00827
CL1 3 0.519550 0.244050 0.504942 11.00000 0.03498 0.02371 =
0.03009 0.00356 0.01364 0.00118
PART 1
CL2A 3 0.684461 0.354577 0.635096 21.00000 0.04094 0.04526 =
0.02753 0.01734 -0.00449 0.00630
PART 0
O1 6 0.437489 0.415300 0.375899 11.00000 0.01194 0.02073 =
0.01270 -0.00446 0.00463 -0.00326
O20 6 0.248198 0.424894 0.469615 11.00000 0.01580 0.02737 =
0.01843 -0.01063 0.00736 -0.00863
O10 6 0.679994 0.490141 0.394623 11.00000 0.01353 0.03793 =
0.01992 -0.01177 0.00672 -0.00809
N20 5 0.120967 0.306011 0.385490 11.00000 0.01247 0.01773 =
0.01813 -0.00286 0.00231 -0.00293
N10 5 0.720452 0.410786 0.275867 11.00000 0.01558 0.02000 =
0.01685 -0.00207 0.00629 -0.00096
N21 5 -0.069632 0.220958 0.390370 11.00000 0.01329 0.01721 =
0.02169 -0.00215 0.00217 -0.00299
N11 5 0.900070 0.403679 0.212770 11.00000 0.01501 0.02400 =
0.01662 -0.00212 0.00684 0.00017
C20 1 0.222763 0.366772 0.409721 11.00000 0.01418 0.01738 =
0.01462 -0.00076 0.00141 -0.00151
C21 1 0.013995 0.293789 0.422450 11.00000 0.01244 0.01339 =
0.01842 0.00185 0.00099 0.00054
C10 1 0.650931 0.435975 0.332751 11.00000 0.01444 0.01630 =
0.01292 0.00192 0.00180 0.00133
C5 1 0.324319 0.359624 0.356515 11.00000 0.01235 0.01767 =
0.01655 -0.00245 0.00097 -0.00321
C2 1 0.518887 0.388963 0.321830 11.00000 0.01408 0.02036 =
0.01143 -0.00118 0.00458 0.00290
C11 1 0.841686 0.448897 0.269096 11.00000 0.01555 0.01986 =
0.01414 0.00261 0.00223 0.00119
C4 1 0.333070 0.299701 0.292140 11.00000 0.01734 0.02751 =
0.02315 -0.00973 0.00357 -0.00660
AFIX 43
H4 2 0.267641 0.253875 0.267244 11.00000 -1.20000
AFIX 0
C12 1 1.031952 0.434850 0.195441 11.00000 0.01335 0.03200 =
0.02239 -0.00270 0.00784 0.00279
AFIX 23
H12A 2 1.076331 0.374578 0.175901 11.00000 -1.20000
H12B 2 1.085855 0.457912 0.245532 11.00000 -1.20000
AFIX 0
C14 1 0.832532 0.319708 0.164204 11.00000 0.02301 0.02505 =
0.02218 -0.00455 0.00839 0.00301
AFIX 23
H14A 2 0.784256 0.276870 0.198538 11.00000 -1.20000
H14B 2 0.899900 0.276039 0.144445 11.00000 -1.20000
AFIX 0
C3 1 0.458653 0.318685 0.269224 11.00000 0.02011 0.02795 =
0.01894 -0.00923 0.00788 -0.00383
AFIX 43
H3 2 0.493828 0.288489 0.225885 11.00000 -1.20000
AFIX 0
C22 1 -0.190608 0.194302 0.423373 11.00000 0.01417 0.02415 =
0.03308 -0.00220 0.00437 -0.00858
AFIX 23
H22A 2 -0.255015 0.163290 0.380844 11.00000 -1.20000
H22B 2 -0.230516 0.257583 0.441381 11.00000 -1.20000
AFIX 0
C30 1 0.568683 0.365467 0.546936 11.00000 0.02732 0.02330 =
0.02224 0.00425 0.00282 0.00316
PART 1
AFIX 23
H30A 2 0.608215 0.406292 0.507265 21.00000 -1.20000
H30B 2 0.489631 0.402474 0.559208 21.00000 -1.20000
AFIX 23
PART 2
H30C 2 0.620516 0.402930 0.511272 -21.00000 -1.20000
H30D 2 0.489701 0.406736 0.553233 -21.00000 -1.20000
AFIX 0
PART 0
C24 1 -0.036681 0.158162 0.323063 11.00000 0.02209 0.02572 =
0.02150 -0.00798 0.00130 -0.00860
AFIX 23
H24A 2 -0.002603 0.203498 0.283944 11.00000 -1.20000
H24B 2 -0.118227 0.125169 0.296061 11.00000 -1.20000
AFIX 0
C23 1 -0.164597 0.120064 0.492957 11.00000 0.03132 0.02340 =
0.04579 0.00460 0.01649 -0.00427
AFIX 137
H23A 2 -0.122811 0.057995 0.475893 11.00000 -1.50000
H23B 2 -0.248397 0.102117 0.511037 11.00000 -1.50000
H23C 2 -0.105823 0.152244 0.536775 11.00000 -1.50000
AFIX 0
C15 1 0.736461 0.357096 0.093913 11.00000 0.02999 0.03819 =
0.03031 -0.00644 -0.00038 -0.00258
AFIX 137
H15A 2 0.784371 0.396006 0.057839 11.00000 -1.50000
H15B 2 0.670058 0.401186 0.112873 11.00000 -1.50000
H15C 2 0.692659 0.298337 0.065448 11.00000 -1.50000
AFIX 0
C13 1 1.027210 0.520059 0.133978 11.00000 0.02514 0.04742 =
0.03030 0.00887 0.01082 -0.00673
AFIX 137
H13A 2 0.975577 0.497390 0.083784 11.00000 -1.50000
H13B 2 1.117258 0.536891 0.125049 11.00000 -1.50000
H13C 2 0.985739 0.580787 0.153507 11.00000 -1.50000
AFIX 0
C25 1 0.065787 0.075849 0.349588 11.00000 0.03887 0.02420 =
0.03923 -0.00697 0.01057 0.00122
AFIX 137
H25A 2 0.087206 0.038988 0.302800 11.00000 -1.50000
H25B 2 0.030115 0.027765 0.385352 11.00000 -1.50000
H25C 2 0.145957 0.107842 0.377676 11.00000 -1.50000
AFIX 0
PART 2
CL2B 3 0.665609 0.345999 0.640725 -21.00000 0.05570 0.04327 =
0.02677 0.01749 -0.01633 -0.02110
HKLF 4
REM tpculfur_0m_a.res in P2(1)/n
REM wR2 = 0.0760, GooF = S = 1.030, Restrained GooF = 1.030 for all data
REM R1 = 0.0376 for 4232 Fo > 4sig(Fo) and 0.0713 for all 5809 data
REM 276 parameters refined using 0 restraints
END
WGHT 0.0292 0.9669
REM Highest difference peak 0.498, deepest hole -0.445, 1-sigma level 0.086
Q1 1 0.0844 0.3028 0.4059 11.00000 0.05 0.50
Q2 1 0.4011 0.3033 0.2898 11.00000 0.05 0.46
Q3 1 0.1043 0.3035 0.3454 11.00000 0.05 0.45
Q4 1 0.7719 0.4226 0.2779 11.00000 0.05 0.41
Q5 1 0.7336 0.5238 0.3948 11.00000 0.05 0.40
;
_shelx_res_checksum 12355
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Cu Cu1 0.84517(2) 0.55425(2) 0.43977(2) 0.01612(8) Uani d 1 . .
S S20 -0.02763(5) 0.36002(4) 0.50470(3) 0.01813(12) Uani d 1 . .
S S10 0.92190(5) 0.55137(4) 0.32124(3) 0.02175(13) Uani d 1 . .
Cl Cl1 0.51955(6) 0.24405(4) 0.50494(4) 0.02871(14) Uani d 1 . .
Cl Cl2A 0.6845(12) 0.3546(8) 0.6351(5) 0.0389(13) Uani d 0.62(6) A 1
O O1 0.43749(13) 0.41530(10) 0.37590(8) 0.0148(3) Uani d 1 . .
O O20 0.24820(14) 0.42489(11) 0.46961(9) 0.0201(3) Uani d 1 . .
O O10 0.67999(14) 0.49014(12) 0.39462(9) 0.0234(4) Uani d 1 . .
N N20 0.12097(16) 0.30601(13) 0.38549(10) 0.0161(4) Uani d 1 . .
N N10 0.72045(17) 0.41079(13) 0.27587(11) 0.0171(4) Uani d 1 . .
N N21 -0.06963(17) 0.22096(13) 0.39037(11) 0.0174(4) Uani d 1 . .
N N11 0.90007(17) 0.40368(13) 0.21277(11) 0.0181(4) Uani d 1 . .
C C20 0.2228(2) 0.36677(15) 0.40972(12) 0.0155(4) Uani d 1 . .
C C21 0.01399(19) 0.29379(15) 0.42245(12) 0.0149(4) Uani d 1 . .
C C10 0.6509(2) 0.43597(15) 0.33275(12) 0.0146(4) Uani d 1 . .
C C5 0.3243(2) 0.35962(15) 0.35652(13) 0.0156(4) Uani d 1 . .
C C2 0.5189(2) 0.38896(16) 0.32183(12) 0.0150(4) Uani d 1 . .
C C11 0.8417(2) 0.44890(16) 0.26910(12) 0.0165(4) Uani d 1 . .
C C4 0.3331(2) 0.29970(17) 0.29214(14) 0.0226(5) Uani d 1 . .
H H4 0.267641 0.253875 0.267244 0.027 Uiso calc 1 . .
C C12 1.0320(2) 0.43485(17) 0.19544(14) 0.0221(5) Uani d 1 . .
H H12A 1.076331 0.374578 0.175901 0.026 Uiso calc 1 . .
H H12B 1.085855 0.457912 0.245532 0.026 Uiso calc 1 . .
C C14 0.8325(2) 0.31971(17) 0.16420(13) 0.0229(5) Uani d 1 . .
H H14A 0.784256 0.276870 0.198538 0.027 Uiso calc 1 . .
H H14B 0.899900 0.276039 0.144445 0.027 Uiso calc 1 . .
C C3 0.4587(2) 0.31868(17) 0.26922(13) 0.0218(5) Uani d 1 . .
H H3 0.493828 0.288489 0.225885 0.026 Uiso calc 1 . .
C C22 -0.1906(2) 0.19430(17) 0.42337(14) 0.0237(5) Uani d 1 . .
H H22A -0.255015 0.163290 0.380844 0.028 Uiso calc 1 . .
H H22B -0.230516 0.257583 0.441381 0.028 Uiso calc 1 . .
C C30 0.5687(2) 0.36547(17) 0.54694(14) 0.0244(5) Uani d 1 . .
H H30A 0.608215 0.406292 0.507265 0.029 Uiso calc 0.62(6) A 1
H H30B 0.489631 0.402474 0.559208 0.029 Uiso calc 0.62(6) A 1
H H30C 0.620516 0.402930 0.511272 0.029 Uiso calc 0.38(6) A 2
H H30D 0.489701 0.406736 0.553233 0.029 Uiso calc 0.38(6) A 2
C C24 -0.0367(2) 0.15816(17) 0.32306(14) 0.0233(5) Uani d 1 . .
H H24A -0.002603 0.203498 0.283944 0.028 Uiso calc 1 . .
H H24B -0.118227 0.125169 0.296061 0.028 Uiso calc 1 . .
C C23 -0.1646(3) 0.12006(18) 0.49296(16) 0.0324(6) Uani d 1 . .
H H23A -0.122811 0.057995 0.475893 0.049 Uiso calc 1 . .
H H23B -0.248397 0.102117 0.511037 0.049 Uiso calc 1 . .
H H23C -0.105823 0.152244 0.536775 0.049 Uiso calc 1 . .
C C15 0.7365(3) 0.3571(2) 0.09391(15) 0.0333(6) Uani d 1 . .
H H15A 0.784371 0.396006 0.057839 0.050 Uiso calc 1 . .
H H15B 0.670058 0.401186 0.112873 0.050 Uiso calc 1 . .
H H15C 0.692659 0.298337 0.065448 0.050 Uiso calc 1 . .
C C13 1.0272(3) 0.5201(2) 0.13398(16) 0.0336(6) Uani d 1 . .
H H13A 0.975577 0.497390 0.083784 0.050 Uiso calc 1 . .
H H13B 1.117258 0.536891 0.125049 0.050 Uiso calc 1 . .
H H13C 0.985739 0.580787 0.153507 0.050 Uiso calc 1 . .
C C25 0.0658(3) 0.07585(18) 0.34959(17) 0.0336(6) Uani d 1 . .
H H25A 0.087206 0.038988 0.302800 0.050 Uiso calc 1 . .
H H25B 0.030115 0.027765 0.385352 0.050 Uiso calc 1 . .
H H25C 0.145957 0.107842 0.377676 0.050 Uiso calc 1 . .
Cl Cl2B 0.6656(19) 0.3460(10) 0.6407(9) 0.044(2) Uani d 0.38(6) A 2
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Cu1 0.01290(13) 0.02103(14) 0.01530(14) -0.00403(10) 0.00497(10) -0.00410(11)
S20 0.0141(3) 0.0184(3) 0.0231(3) -0.0034(2) 0.0069(2) -0.0044(2)
S10 0.0214(3) 0.0267(3) 0.0191(3) -0.0083(2) 0.0096(2) -0.0042(2)
Cl1 0.0350(3) 0.0237(3) 0.0301(3) 0.0012(2) 0.0136(3) 0.0036(2)
Cl2A 0.041(2) 0.045(2) 0.0275(12) 0.006(2) -0.0045(13) 0.0173(14)
O1 0.0119(7) 0.0207(7) 0.0127(8) -0.0033(6) 0.0046(6) -0.0045(6)
O20 0.0158(7) 0.0274(8) 0.0184(8) -0.0086(6) 0.0074(6) -0.0106(6)
O10 0.0135(8) 0.0379(9) 0.0199(9) -0.0081(7) 0.0067(6) -0.0118(7)
N20 0.0125(9) 0.0177(9) 0.0181(10) -0.0029(7) 0.0023(7) -0.0029(7)
N10 0.0156(9) 0.0200(9) 0.0168(10) -0.0010(7) 0.0063(8) -0.0021(7)
N21 0.0133(9) 0.0172(9) 0.0217(10) -0.0030(7) 0.0022(7) -0.0021(7)
N11 0.0150(9) 0.0240(9) 0.0166(10) 0.0002(7) 0.0068(8) -0.0021(8)
C20 0.0142(10) 0.0174(10) 0.0146(11) -0.0015(8) 0.0014(9) -0.0008(8)
C21 0.0124(10) 0.0134(10) 0.0184(11) 0.0005(8) 0.0010(9) 0.0019(8)
C10 0.0144(10) 0.0163(10) 0.0129(11) 0.0013(8) 0.0018(8) 0.0019(8)
C5 0.0124(10) 0.0177(10) 0.0165(11) -0.0032(8) 0.0010(8) -0.0025(8)
C2 0.0141(10) 0.0204(11) 0.0114(11) 0.0029(8) 0.0046(8) -0.0012(8)
C11 0.0156(10) 0.0199(10) 0.0141(11) 0.0012(9) 0.0022(8) 0.0026(9)
C4 0.0173(11) 0.0275(12) 0.0232(13) -0.0066(9) 0.0036(10) -0.0097(10)
C12 0.0134(11) 0.0320(12) 0.0224(12) 0.0028(9) 0.0078(9) -0.0027(10)
C14 0.0230(12) 0.0251(12) 0.0222(13) 0.0030(10) 0.0084(10) -0.0045(9)
C3 0.0201(11) 0.0279(12) 0.0189(12) -0.0038(9) 0.0079(10) -0.0092(9)
C22 0.0142(11) 0.0241(12) 0.0331(14) -0.0086(9) 0.0044(10) -0.0022(10)
C30 0.0273(13) 0.0233(12) 0.0222(13) 0.0032(10) 0.0028(10) 0.0042(9)
C24 0.0221(12) 0.0257(12) 0.0215(12) -0.0086(10) 0.0013(10) -0.0080(9)
C23 0.0313(14) 0.0234(13) 0.0458(17) -0.0043(11) 0.0165(12) 0.0046(11)
C15 0.0300(14) 0.0382(15) 0.0303(15) -0.0026(11) -0.0004(11) -0.0064(11)
C13 0.0251(13) 0.0474(16) 0.0303(15) -0.0067(12) 0.0108(11) 0.0089(12)
C25 0.0389(15) 0.0242(13) 0.0392(16) 0.0012(11) 0.0106(13) -0.0070(11)
Cl2B 0.056(4) 0.043(2) 0.027(3) -0.021(3) -0.016(3) 0.0175(18)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
S20 Cu1 S10 3_666 . 90.35(2) ?
O20 Cu1 S20 3_666 3_666 94.14(4) ?
O20 Cu1 S10 3_666 . 168.29(5) ?
O10 Cu1 S20 . 3_666 175.25(5) ?
O10 Cu1 S10 . . 92.12(5) ?
O10 Cu1 O20 . 3_666 82.68(6) ?
C21 S20 Cu1 . 3_666 107.20(7) ?
C11 S10 Cu1 . . 105.37(7) ?
C5 O1 C2 . . 106.35(15) ?
C20 O20 Cu1 . 3_666 130.70(13) ?
C10 O10 Cu1 . . 130.91(13) ?
C20 N20 C21 . . 125.52(18) ?
C10 N10 C11 . . 124.50(18) ?
C21 N21 C22 . . 122.38(18) ?
C21 N21 C24 . . 120.11(17) ?
C22 N21 C24 . . 117.34(17) ?
C11 N11 C12 . . 122.41(18) ?
C11 N11 C14 . . 120.30(17) ?
C12 N11 C14 . . 117.29(17) ?
O20 C20 N20 . . 131.98(19) ?
O20 C20 C5 . . 116.66(17) ?
N20 C20 C5 . . 111.33(18) ?
N20 C21 S20 . . 128.46(16) ?
N21 C21 S20 . . 117.42(15) ?
N21 C21 N20 . . 114.12(18) ?
O10 C10 N10 . . 131.22(19) ?
O10 C10 C2 . . 116.03(17) ?
N10 C10 C2 . . 112.72(18) ?
O1 C5 C20 . . 117.82(17) ?
C4 C5 O1 . . 110.36(17) ?
C4 C5 C20 . . 131.58(19) ?
O1 C2 C10 . . 116.58(17) ?
C3 C2 O1 . . 110.28(18) ?
C3 C2 C10 . . 133.07(19) ?
N10 C11 S10 . . 127.42(16) ?
N11 C11 S10 . . 118.44(15) ?
N11 C11 N10 . . 114.05(18) ?
C5 C4 H4 . . 126.6 ?
C5 C4 C3 . . 106.76(19) ?
C3 C4 H4 . . 126.6 ?
N11 C12 H12A . . 108.9 ?
N11 C12 H12B . . 108.9 ?
N11 C12 C13 . . 113.50(19) ?
H12A C12 H12B . . 107.7 ?
C13 C12 H12A . . 108.9 ?
C13 C12 H12B . . 108.9 ?
N11 C14 H14A . . 108.9 ?
N11 C14 H14B . . 108.9 ?
N11 C14 C15 . . 113.34(19) ?
H14A C14 H14B . . 107.7 ?
C15 C14 H14A . . 108.9 ?
C15 C14 H14B . . 108.9 ?
C2 C3 C4 . . 106.24(19) ?
C2 C3 H3 . . 126.9 ?
C4 C3 H3 . . 126.9 ?
N21 C22 H22A . . 109.1 ?
N21 C22 H22B . . 109.1 ?
N21 C22 C23 . . 112.59(19) ?
H22A C22 H22B . . 107.8 ?
C23 C22 H22A . . 109.1 ?
C23 C22 H22B . . 109.1 ?
Cl1 C30 H30A . . 109.1 ?
Cl1 C30 H30B . . 109.1 ?
Cl1 C30 H30C . . 110.0 ?
Cl1 C30 H30D . . 110.0 ?
Cl2A C30 Cl1 . . 112.4(4) ?
Cl2A C30 H30A . . 109.1 ?
Cl2A C30 H30B . . 109.1 ?
H30A C30 H30B . . 107.9 ?
H30C C30 H30D . . 108.3 ?
Cl2B C30 Cl1 . . 108.7(5) ?
Cl2B C30 H30C . . 110.0 ?
Cl2B C30 H30D . . 110.0 ?
N21 C24 H24A . . 109.0 ?
N21 C24 H24B . . 109.0 ?
N21 C24 C25 . . 112.76(19) ?
H24A C24 H24B . . 107.8 ?
C25 C24 H24A . . 109.0 ?
C25 C24 H24B . . 109.0 ?
C22 C23 H23A . . 109.5 ?
C22 C23 H23B . . 109.5 ?
C22 C23 H23C . . 109.5 ?
H23A C23 H23B . . 109.5 ?
H23A C23 H23C . . 109.5 ?
H23B C23 H23C . . 109.5 ?
C14 C15 H15A . . 109.5 ?
C14 C15 H15B . . 109.5 ?
C14 C15 H15C . . 109.5 ?
H15A C15 H15B . . 109.5 ?
H15A C15 H15C . . 109.5 ?
H15B C15 H15C . . 109.5 ?
C12 C13 H13A . . 109.5 ?
C12 C13 H13B . . 109.5 ?
C12 C13 H13C . . 109.5 ?
H13A C13 H13B . . 109.5 ?
H13A C13 H13C . . 109.5 ?
H13B C13 H13C . . 109.5 ?
C24 C25 H25A . . 109.5 ?
C24 C25 H25B . . 109.5 ?
C24 C25 H25C . . 109.5 ?
H25A C25 H25B . . 109.5 ?
H25A C25 H25C . . 109.5 ?
H25B C25 H25C . . 109.5 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Cu1 S20 3_666 2.2612(6) ?
Cu1 S10 . 2.2624(6) ?
Cu1 O20 3_666 1.9431(14) ?
Cu1 O10 . 1.9406(15) ?
S20 C21 . 1.746(2) ?
S10 C11 . 1.743(2) ?
Cl1 C30 . 1.781(2) ?
Cl2A C30 . 1.773(8) ?
O1 C5 . 1.366(2) ?
O1 C2 . 1.369(2) ?
O20 C20 . 1.265(2) ?
O10 C10 . 1.265(2) ?
N20 C20 . 1.326(3) ?
N20 C21 . 1.347(3) ?
N10 C10 . 1.321(3) ?
N10 C11 . 1.357(3) ?
N21 C21 . 1.341(3) ?
N21 C22 . 1.472(3) ?
N21 C24 . 1.484(3) ?
N11 C11 . 1.336(3) ?
N11 C12 . 1.479(3) ?
N11 C14 . 1.481(3) ?
C20 C5 . 1.475(3) ?
C10 C2 . 1.471(3) ?
C5 C4 . 1.357(3) ?
C2 C3 . 1.363(3) ?
C4 H4 . 0.9500 ?
C4 C3 . 1.417(3) ?
C12 H12A . 0.9900 ?
C12 H12B . 0.9900 ?
C12 C13 . 1.521(3) ?
C14 H14A . 0.9900 ?
C14 H14B . 0.9900 ?
C14 C15 . 1.511(3) ?
C3 H3 . 0.9500 ?
C22 H22A . 0.9900 ?
C22 H22B . 0.9900 ?
C22 C23 . 1.521(3) ?
C30 H30A . 0.9900 ?
C30 H30B . 0.9900 ?
C30 H30C . 0.9900 ?
C30 H30D . 0.9900 ?
C30 Cl2B . 1.766(13) ?
C24 H24A . 0.9900 ?
C24 H24B . 0.9900 ?
C24 C25 . 1.523(3) ?
C23 H23A . 0.9800 ?
C23 H23B . 0.9800 ?
C23 H23C . 0.9800 ?
C15 H15A . 0.9800 ?
C15 H15B . 0.9800 ?
C15 H15C . 0.9800 ?
C13 H13A . 0.9800 ?
C13 H13B . 0.9800 ?
C13 H13C . 0.9800 ?
C25 H25A . 0.9800 ?
C25 H25B . 0.9800 ?
C25 H25C . 0.9800 ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
C30 H30A O10 . 0.99 2.41 3.388(3) 170.5 yes
C30 H30B O10 3_666 0.99 2.45 3.428(3) 170.5 yes
C14 H14B Cl1 4_665 0.99 2.83 3.627(2) 138.0 yes
C4 H4 Cl2A 4_565 0.95 2.68 3.506(8) 145.2 yes
C4 H4 Cl2B 4_565 0.95 2.60 3.446(12) 148.9 yes
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
Cu1 S20 C21 N20 3_666 . . . -14.0(2) ?
Cu1 S20 C21 N21 3_666 . . . 166.21(14) ?
Cu1 S10 C11 N10 . . . . 29.0(2) ?
Cu1 S10 C11 N11 . . . . -154.56(15) ?
Cu1 O20 C20 N20 3_666 . . . 5.2(4) ?
Cu1 O20 C20 C5 3_666 . . . -172.26(14) ?
Cu1 O10 C10 N10 . . . . -5.1(3) ?
Cu1 O10 C10 C2 . . . . 172.61(14) ?
O1 C5 C4 C3 . . . . -0.2(3) ?
O1 C2 C3 C4 . . . . -0.4(3) ?
O20 C20 C5 O1 . . . . 0.3(3) ?
O20 C20 C5 C4 . . . . 174.1(2) ?
O10 C10 C2 O1 . . . . 5.2(3) ?
O10 C10 C2 C3 . . . . -171.6(2) ?
N20 C20 C5 O1 . . . . -177.58(17) ?
N20 C20 C5 C4 . . . . -3.8(3) ?
N10 C10 C2 O1 . . . . -176.69(17) ?
N10 C10 C2 C3 . . . . 6.5(3) ?
C20 N20 C21 S20 . . . . 6.1(3) ?
C20 N20 C21 N21 . . . . -174.10(19) ?
C20 C5 C4 C3 . . . . -174.3(2) ?
C21 N20 C20 O20 . . . . 0.9(4) ?
C21 N20 C20 C5 . . . . 178.46(19) ?
C21 N21 C22 C23 . . . . -82.9(2) ?
C21 N21 C24 C25 . . . . 76.7(2) ?
C10 N10 C11 S10 . . . . -11.0(3) ?
C10 N10 C11 N11 . . . . 172.43(19) ?
C10 C2 C3 C4 . . . . 176.6(2) ?
C5 O1 C2 C10 . . . . -177.26(17) ?
C5 O1 C2 C3 . . . . 0.3(2) ?
C5 C4 C3 C2 . . . . 0.4(3) ?
C2 O1 C5 C20 . . . . 175.01(18) ?
C2 O1 C5 C4 . . . . 0.0(2) ?
C11 N10 C10 O10 . . . . -6.7(4) ?
C11 N10 C10 C2 . . . . 175.57(19) ?
C11 N11 C12 C13 . . . . -88.5(3) ?
C11 N11 C14 C15 . . . . 83.8(2) ?
C12 N11 C11 S10 . . . . 2.4(3) ?
C12 N11 C11 N10 . . . . 179.34(18) ?
C12 N11 C14 C15 . . . . -95.6(2) ?
C14 N11 C11 S10 . . . . -176.94(15) ?
C14 N11 C11 N10 . . . . 0.0(3) ?
C14 N11 C12 C13 . . . . 90.9(2) ?
C22 N21 C21 S20 . . . . -1.7(3) ?
C22 N21 C21 N20 . . . . 178.48(18) ?
C22 N21 C24 C25 . . . . -98.7(2) ?
C24 N21 C21 S20 . . . . -176.80(15) ?
C24 N21 C21 N20 . . . . 3.4(3) ?
C24 N21 C22 C23 . . . . 92.4(2) ?