#------------------------------------------------------------------------------ #$Date: 2024-11-06 03:58:44 +0100 (Wed, 06 Nov 2024) $ #$Revision: 295791 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/33/2023303.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023303 loop_ _publ_author_name 'Eder, Felix' 'Weil, Matthias' _publ_section_title ; The cadmium oxidotellurates(IV) Cd5(TeO3)4(NO3)2 and Cd4Te5O14 ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E Crystallographic Communications' _journal_paper_doi 10.1107/S2056989024010387 _journal_volume 80 _journal_year 2024 _chemical_formula_iupac 'Cd4 Te5 O14' _chemical_formula_moiety 'Cd4 O14 Te5' _chemical_formula_sum 'Cd4 O14 Te5' _chemical_formula_weight 1311.60 _chemical_name_systematic ; Pentacadmium tetrakis[oxidotellurate(IV)] dinitrate ; _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _audit_creation_method SHELXL-2016/6 _cell_angle_alpha 90 _cell_angle_beta 113.6290(10) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 11.9074(3) _cell_length_b 14.3289(3) _cell_length_c 8.7169(2) _cell_measurement_reflns_used 8153 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 36.599 _cell_measurement_theta_min 2.3465 _cell_volume 1362.58(6) _computing_cell_refinement ; SAINT (Bruker, 2016) ; _computing_data_collection ; APEX3 (Bruker, 2016) ; _computing_data_reduction ; SAINT (Bruker, 2016) ; _computing_molecular_graphics ; ATOMS (Dowty, 2006) ; _computing_publication_material ; publCIF (Westrip, 2010) ; _computing_structure_refinement ; SHELXL (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 296(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Bruker APEXII CCD' _diffrn_measurement_method '\w- and \f-scan' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0274 _diffrn_reflns_av_unetI/netI 0.0196 _diffrn_reflns_limit_h_max 19 _diffrn_reflns_limit_h_min -19 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_k_min -23 _diffrn_reflns_limit_l_max 14 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 18799 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 36.620 _diffrn_reflns_theta_min 2.843 _exptl_absorpt_coefficient_mu 16.726 _exptl_absorpt_correction_T_max 0.7471 _exptl_absorpt_correction_T_min 0.5952 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 6.394 _exptl_crystal_description fragment _exptl_crystal_F_000 2256 _exptl_crystal_size_max 0.090 _exptl_crystal_size_mid 0.070 _exptl_crystal_size_min 0.060 _refine_diff_density_max 1.099 _refine_diff_density_min -1.525 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.208 _refine_ls_hydrogen_treatment undef _refine_ls_matrix_type full _refine_ls_number_parameters 106 _refine_ls_number_reflns 3373 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.208 _refine_ls_R_factor_all 0.0264 _refine_ls_R_factor_gt 0.0219 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0070P)^2^+7.0237P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0392 _refine_ls_wR_factor_ref 0.0401 _reflns_number_gt 3084 _reflns_number_total 3373 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file pk2712.cif _cod_data_source_block Cd4Te5O14 _cod_original_sg_symbol_H-M 'C 2/c' _cod_database_code 2023303 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.314 _shelx_estimated_absorpt_t_max 0.434 _shelx_hkl_file ; 2 0 0 63.29 1.80 2 0 0 66.69 1.90 2 0 0 65.39 1.90 2 0 0 67.79 2.20 -2 0 0 68.09 2.20 -2 0 0 66.19 2.20 -2 0 0 68.69 1.90 -4 0 0 137.49 4.50 4 0 0 149.49 3.90 -4 0 0 148.69 4.00 -4 0 0 139.29 4.40 4 0 0 138.89 4.40 -6 0 0 8870.71 175.38 6 0 0 8233.88 174.98 -6 0 0 9091.89 174.38 -6 0 0 8639.24 175.18 6 0 0 8977.50 174.28 -8 0 0 152.08 6.00 8 0 0 142.29 4.70 -8 0 0 142.29 4.90 -8 0 0 123.19 5.50 -8 0 0 145.49 5.70 -10 0 0 41.00 3.00 -10 0 0 39.00 3.90 -10 0 0 38.90 3.70 -10 0 0 38.00 3.90 10 0 0 40.10 2.70 -12 0 0 1698.53 39.80 -12 0 0 1784.82 38.10 -12 0 0 1728.03 40.40 -12 0 0 1762.52 40.40 12 0 0 1763.22 37.70 -14 0 0 293.27 11.40 -14 0 0 267.97 11.40 -14 0 0 294.07 11.40 -16 0 0 0.40 2.80 -16 0 0 5.80 3.10 -16 0 0 5.10 3.00 -18 0 0 248.48 12.40 -18 0 0 222.68 11.30 3 -1 0 2.40 0.70 -3 -1 0 1.40 0.90 -3 -1 0 2.70 0.50 3 -1 0 2.50 0.80 -3 -1 0 3.60 0.90 -3 -1 0 3.40 0.70 -3 -1 0 2.20 0.80 -3 1 0 1.50 0.80 3 1 0 2.50 0.60 -3 1 0 3.10 1.00 3 1 0 1.40 0.80 -3 1 0 1.60 0.60 -5 -1 0 478.65 10.70 -5 -1 0 458.75 11.50 -5 -1 0 484.65 11.40 -5 -1 0 470.65 11.50 5 -1 0 499.25 11.00 5 -1 0 468.95 11.50 -5 1 0 470.45 11.70 5 1 0 472.75 11.40 -5 1 0 474.95 11.50 5 1 0 484.95 10.70 -5 1 0 482.25 11.00 -7 -1 0 41.30 3.10 7 -1 0 40.70 2.30 -7 -1 0 42.50 2.40 -7 -1 0 38.30 3.00 -7 -1 0 40.80 3.10 7 1 0 45.40 2.20 -7 1 0 42.90 2.60 -7 1 0 36.10 3.00 -7 1 0 42.40 3.10 -9 -1 0 2.20 1.70 -9 -1 0 0.60 1.60 9 -1 0 2.90 1.20 -9 -1 0 2.70 1.80 -9 -1 0 1.90 1.20 -9 1 0 3.70 1.50 9 1 0 2.00 1.00 -9 1 0 2.10 1.80 -9 1 0 6.70 2.10 -11 -1 0 325.97 11.00 11 -1 0 315.37 9.20 -11 -1 0 319.97 11.00 -11 -1 0 328.87 9.10 -11 -1 0 306.17 10.50 -11 1 0 313.17 10.80 -11 1 0 319.97 11.00 11 1 0 328.67 8.90 -11 1 0 319.87 10.70 -11 1 0 329.07 9.70 -13 -1 0 59.99 5.60 -13 -1 0 62.29 5.70 -13 -1 0 67.99 5.50 -13 1 0 75.19 5.90 -13 1 0 73.79 5.70 -13 1 0 70.09 5.80 -13 1 0 68.79 4.40 -15 -1 0 12.40 3.50 -15 -1 0 12.60 3.60 -15 -1 0 9.60 3.50 -15 1 0 12.00 3.60 -15 1 0 16.30 3.70 -15 1 0 11.50 3.60 -17 -1 0 108.79 7.90 -17 -1 0 114.99 8.60 -17 1 0 116.19 8.40 -17 1 0 119.49 8.40 0 -2 0 2.90 0.40 0 -2 0 3.20 0.40 0 -2 0 3.40 0.40 0 2 0 2.60 0.50 0 2 0 3.50 0.50 2 -2 0 71.49 2.30 -2 -2 0 69.89 2.50 2 -2 0 72.29 2.50 -2 -2 0 74.09 2.50 -2 -2 0 76.99 1.90 -2 -2 0 72.59 2.50 2 -2 0 72.79 1.90 -2 -2 0 73.79 2.40 -2 2 0 72.49 2.50 2 2 0 66.99 1.90 2 2 0 74.69 2.50 2 2 0 71.39 1.80 -2 2 0 71.59 2.30 -4 -2 0 106.19 3.60 4 -2 0 102.39 3.70 -4 -2 0 109.89 3.90 -4 -2 0 101.39 3.70 -4 -2 0 108.29 2.70 -4 -2 0 108.49 3.00 4 -2 0 113.99 3.50 -4 -2 0 101.39 3.70 -4 2 0 109.39 3.90 -4 2 0 108.39 3.50 -4 2 0 110.49 3.70 4 2 0 105.49 3.70 -6 -2 0 4.00 0.90 6 -2 0 2.80 1.00 -6 -2 0 1.30 1.30 -6 -2 0 3.50 1.30 -6 -2 0 4.40 1.40 -6 2 0 2.40 1.00 -6 2 0 2.60 1.30 6 2 0 4.00 0.90 6 2 0 3.90 1.20 -6 2 0 3.20 1.30 -8 -2 0 11.70 2.20 -8 -2 0 9.40 2.00 8 -2 0 11.60 1.60 -8 -2 0 10.40 1.40 -8 -2 0 8.40 2.00 8 2 0 13.10 1.50 -8 2 0 11.70 2.20 -8 2 0 8.90 1.90 -8 2 0 16.40 2.00 10 -2 0 129.69 5.10 -10 -2 0 132.99 6.20 -10 -2 0 133.29 4.70 -10 -2 0 130.39 6.40 -10 -2 0 140.39 6.30 -10 2 0 125.99 6.10 -10 2 0 136.59 5.60 10 2 0 139.29 4.70 -10 2 0 142.89 6.80 -12 -2 0 21.40 3.50 12 -2 0 23.30 2.70 -12 -2 0 21.90 3.50 -12 -2 0 27.20 3.80 -12 2 0 19.20 3.30 -12 2 0 26.50 3.20 -12 2 0 17.70 3.40 -12 2 0 15.10 3.40 -14 -2 0 36.30 4.90 -14 -2 0 48.50 5.20 -14 -2 0 43.70 4.90 -14 2 0 37.50 5.00 -14 2 0 41.60 5.00 -14 2 0 40.10 5.00 -16 -2 0 42.40 8.10 -16 -2 0 38.40 5.20 -16 -2 0 34.60 5.30 -16 2 0 35.90 5.30 -16 2 0 38.30 5.30 -16 2 0 42.40 5.60 -18 -2 0 37.20 5.60 -18 2 0 31.50 5.40 -18 2 0 33.60 5.50 -1 -3 0 285.27 6.50 -1 -3 0 288.37 6.70 -1 -3 0 293.47 6.50 1 -3 0 287.27 6.80 1 -3 0 296.37 6.30 -1 3 0 281.87 6.80 -1 3 0 289.07 6.50 3 -3 0 9168.08 191.28 3 -3 0 9392.36 189.18 -3 -3 0 9836.22 189.18 -3 -3 0 9188.48 189.18 -3 -3 0 9022.00 189.38 -3 -3 0 9999.00 188.28 3 -3 0 9743.83 188.58 3 3 0 9457.15 188.98 -3 3 0 9498.45 190.08 -3 3 0 9240.67 189.28 3 3 0 9713.83 187.88 3 3 0 9976.50 188.38 -5 -3 0 17.00 1.90 5 -3 0 18.60 1.80 -5 -3 0 21.60 2.00 -5 -3 0 17.50 1.90 -5 -3 0 21.60 2.20 5 -3 0 13.70 2.10 -5 -3 0 16.50 1.30 -5 -3 0 20.00 0.90 -5 3 0 14.80 1.60 5 3 0 15.90 1.80 -5 3 0 22.10 2.00 -5 3 0 18.90 2.10 -7 -3 0 275.87 8.30 -7 -3 0 270.17 8.50 -7 -3 0 283.37 6.90 7 -3 0 275.97 7.70 -7 -3 0 271.47 8.20 -7 -3 0 280.87 6.90 -7 3 0 278.27 8.00 -7 3 0 277.17 8.20 7 3 0 285.47 7.00 -7 3 0 266.57 8.60 -9 -3 0 2628.34 55.29 9 -3 0 2594.64 54.09 -9 -3 0 2595.24 52.99 -9 -3 0 2569.94 55.59 -9 -3 0 2535.95 55.09 -9 3 0 2644.94 54.59 -9 3 0 2574.64 55.79 -9 3 0 2581.64 55.19 9 3 0 2593.44 52.99 -11 -3 0 111.89 5.90 11 -3 0 110.19 4.90 -11 -3 0 100.69 6.10 -11 -3 0 86.49 5.60 -11 3 0 107.09 6.40 -11 3 0 99.89 5.80 -11 3 0 114.99 5.50 11 3 0 97.39 4.40 13 -3 0 35.60 3.50 -13 -3 0 38.20 4.70 -13 -3 0 40.20 4.80 -13 -3 0 38.90 4.40 -13 3 0 40.80 5.00 -13 3 0 30.50 4.20 -13 3 0 38.40 4.00 -13 3 0 38.90 4.80 -15 -3 0 419.56 15.60 -15 -3 0 458.15 15.40 -15 -3 0 462.85 15.20 -15 3 0 440.26 15.90 -15 3 0 453.45 15.60 -15 3 0 453.75 15.70 -17 -3 0 103.89 8.00 -17 3 0 117.69 8.50 -17 3 0 105.59 8.40 0 -4 0 0.00 0.60 0 -4 0 1.10 0.60 0 -4 0 0.90 0.60 2 -4 0 573.14 12.40 -2 -4 0 533.25 12.40 -2 -4 0 549.45 12.20 2 -4 0 553.24 11.60 2 -4 0 538.65 12.40 -2 -4 0 566.64 12.00 -2 4 0 544.95 12.50 -2 4 0 555.74 12.00 4 -4 0 82.69 2.40 4 -4 0 78.79 3.40 -4 -4 0 79.69 3.40 -4 -4 0 76.69 3.30 4 -4 0 84.19 3.20 -4 4 0 77.09 3.40 -4 4 0 76.19 3.10 4 4 0 79.39 2.00 4 4 0 78.69 3.30 6 -4 0 11.90 1.50 -6 -4 0 11.30 1.00 -6 -4 0 12.30 2.00 -6 -4 0 11.80 1.80 6 -4 0 14.90 1.30 -6 -4 0 13.90 1.80 -6 4 0 11.30 1.90 6 4 0 9.10 1.60 -6 4 0 10.90 1.60 -6 4 0 13.30 1.90 -8 -4 0 552.44 14.50 -8 -4 0 555.14 14.90 -8 -4 0 575.84 12.50 8 -4 0 564.24 13.90 -8 -4 0 547.95 14.50 -8 4 0 561.64 15.10 -8 4 0 573.24 14.30 -8 4 0 584.14 14.60 8 4 0 549.25 12.80 -10 -4 0 0.00 1.80 -10 -4 0 0.30 1.70 -10 -4 0 0.80 0.80 -10 -4 0 0.40 1.70 10 -4 0 1.30 1.30 -10 4 0 0.20 1.80 10 4 0 0.40 0.90 -10 4 0 -0.20 1.90 -10 4 0 3.50 1.80 -12 -4 0 7.40 2.40 12 -4 0 11.20 2.20 -12 -4 0 8.90 2.80 -12 -4 0 8.60 2.60 -12 4 0 12.10 2.90 -12 4 0 11.20 2.60 -12 4 0 6.20 2.70 -14 -4 0 345.87 12.20 -14 -4 0 324.37 12.30 -14 4 0 325.17 11.40 -14 4 0 325.77 12.50 -14 4 0 314.47 12.30 -14 4 0 320.77 12.80 -16 -4 0 2.40 2.90 -16 4 0 2.30 3.00 -16 4 0 -2.00 2.90 -18 -4 0 15.00 4.20 -18 4 0 13.90 4.40 -18 4 0 12.40 4.10 -1 -5 0 5.30 0.90 -1 -5 0 6.30 1.10 1 -5 0 11.40 1.40 1 -5 0 7.40 0.90 -1 -5 0 8.70 1.10 1 -5 0 7.40 1.00 -1 5 0 7.50 1.20 -3 -5 0 15.40 1.60 3 -5 0 17.80 1.10 3 -5 0 16.50 1.70 -3 -5 0 17.90 1.80 3 -5 0 20.40 1.90 3 5 0 18.90 1.60 -3 5 0 13.30 1.60 3 5 0 18.90 1.20 -3 5 0 18.30 1.50 5 -5 0 5.40 0.80 -5 -5 0 3.70 1.20 5 -5 0 1.90 1.00 -5 -5 0 5.80 1.50 5 5 0 4.00 1.20 -5 5 0 3.00 1.30 -5 5 0 3.20 1.20 -5 5 0 2.80 1.20 7 -5 0 40.90 1.80 -7 -5 0 38.90 3.10 7 -5 0 37.10 2.70 -7 5 0 37.30 2.90 -7 5 0 37.40 3.00 -7 5 0 39.90 3.40 -9 -5 0 8.40 2.20 -9 -5 0 8.70 2.30 -9 -5 0 6.70 0.90 9 -5 0 5.90 1.70 9 -5 0 6.30 1.10 -9 -5 0 6.70 2.00 -9 5 0 9.40 2.10 9 5 0 7.80 1.30 -9 5 0 6.80 2.10 -9 5 0 2.40 1.90 -11 -5 0 7.80 2.30 -11 -5 0 8.50 2.80 -11 -5 0 8.00 2.40 11 -5 0 8.00 2.00 -11 5 0 6.70 2.30 -11 5 0 6.30 2.50 -11 5 0 6.30 2.70 -13 -5 0 7.90 2.70 13 -5 0 7.40 2.20 -13 -5 0 7.80 2.60 -13 5 0 5.50 3.00 -13 5 0 4.60 2.50 -13 5 0 9.30 2.90 -15 -5 0 0.70 2.70 -15 5 0 2.60 3.10 -15 5 0 -3.50 2.60 -15 5 0 -1.50 2.60 -15 5 0 5.10 3.40 -17 -5 0 18.20 4.00 -17 5 0 15.90 4.20 -17 5 0 16.00 4.60 0 -6 0 2235.78 45.20 0 -6 0 2196.28 44.90 0 -6 0 2189.78 45.30 -2 -6 0 576.84 13.50 2 -6 0 604.74 13.60 -2 -6 0 582.34 13.10 2 -6 0 586.14 12.70 -2 -6 0 555.14 13.10 -2 6 0 567.94 12.90 -2 6 0 592.44 13.70 4 -6 0 542.75 13.20 -4 -6 0 539.15 13.20 4 -6 0 552.64 11.80 -4 -6 0 552.54 13.10 4 6 0 527.45 12.80 -4 6 0 542.35 12.60 4 6 0 546.85 11.80 -4 6 0 530.85 13.40 -6 -6 0 1594.84 34.10 6 -6 0 1604.44 31.90 6 -6 0 1565.34 33.80 -6 -6 0 1543.55 34.10 -6 6 0 1534.35 34.00 -6 6 0 1563.64 34.50 6 6 0 1504.75 33.50 -6 6 0 1583.44 33.50 8 -6 0 9.40 1.00 8 -6 0 7.50 1.70 -8 -6 0 6.30 1.90 -8 6 0 5.40 1.80 -8 6 0 10.10 2.40 -8 6 0 10.00 2.20 10 -6 0 116.79 5.50 -10 -6 0 128.99 6.20 -10 6 0 125.89 6.10 -10 6 0 112.49 6.40 -10 6 0 124.49 6.10 -12 -6 0 271.57 10.40 12 -6 0 278.97 9.80 -12 6 0 292.97 11.60 -12 6 0 303.77 10.60 -12 6 0 309.77 11.00 -14 -6 0 -1.40 2.40 14 -6 0 1.30 1.90 -14 6 0 -1.20 2.80 -14 6 0 2.40 2.70 -14 6 0 1.20 2.50 -16 -6 0 19.40 3.90 -16 6 0 23.60 4.70 -16 6 0 28.00 5.00 -1 -7 0 282.77 7.70 1 -7 0 287.87 7.30 -1 -7 0 294.57 7.40 1 -7 0 298.07 7.40 1 -7 0 286.37 7.80 -1 -7 0 286.77 7.50 -1 7 0 289.97 7.90 3 -7 0 907.91 20.20 3 -7 0 920.41 18.90 -3 -7 0 865.91 20.10 -3 -7 0 880.71 19.70 -3 7 0 858.61 20.20 -3 7 0 888.11 19.40 -5 -7 0 230.58 7.40 5 -7 0 240.38 5.80 -5 -7 0 222.38 7.20 5 -7 0 250.47 7.40 5 7 0 219.78 6.90 -5 7 0 239.98 6.90 -5 7 0 234.78 7.70 5 7 0 228.78 5.70 -7 -7 0 8.00 1.90 -7 -7 0 6.30 1.80 7 -7 0 8.00 0.90 7 -7 0 4.50 1.60 -7 7 0 7.40 1.90 -7 7 0 5.70 1.70 -7 7 0 7.30 2.00 9 -7 0 378.76 11.00 -9 -7 0 351.76 11.20 -9 7 0 358.36 10.90 9 7 0 339.87 8.90 -9 7 0 378.56 11.40 -9 7 0 368.36 12.00 -11 -7 0 152.38 7.30 11 -7 0 161.68 6.90 -11 7 0 163.88 7.50 -11 7 0 149.39 8.00 -11 7 0 160.18 7.40 13 -7 0 0.40 1.80 -13 -7 0 -1.00 2.20 -13 7 0 0.00 2.40 -13 7 0 0.30 2.70 -13 7 0 1.90 2.40 -15 -7 0 60.49 6.00 -15 7 0 72.59 7.30 -15 7 0 67.49 6.40 -15 7 0 65.19 6.40 -17 -7 0 49.40 5.90 -17 7 0 53.29 6.30 -17 7 0 48.40 6.70 0 -8 0 308.67 7.90 0 -8 0 294.37 8.00 0 -8 0 304.47 8.20 -2 -8 0 57.39 3.10 2 -8 0 65.69 2.70 -2 -8 0 60.79 2.90 -2 -8 0 57.99 2.90 2 -8 0 65.79 3.30 -2 8 0 60.79 3.30 -2 8 0 61.29 2.70 -4 -8 0 97.89 4.50 -4 -8 0 96.69 4.20 4 -8 0 99.99 3.30 4 -8 0 105.09 4.50 4 8 0 98.39 3.40 -4 8 0 101.69 4.60 -4 8 0 103.79 3.90 -6 -8 0 194.08 6.80 6 -8 0 194.08 4.90 -6 -8 0 182.58 6.90 6 -8 0 176.68 6.60 -6 8 0 194.48 6.30 6 8 0 179.98 4.50 -6 8 0 184.48 6.90 -6 8 0 191.48 7.20 8 -8 0 9.40 1.00 8 -8 0 10.90 2.10 -8 -8 0 9.80 2.30 -8 8 0 8.20 2.20 -8 8 0 10.50 2.50 -8 8 0 10.10 2.20 10 -8 0 65.59 4.60 -10 -8 0 74.39 5.10 -10 8 0 70.89 4.90 -10 8 0 64.59 4.90 -10 8 0 63.89 5.30 -12 -8 0 74.09 5.60 12 -8 0 72.29 5.10 -12 8 0 78.19 5.80 -12 8 0 69.89 6.30 -12 8 0 66.79 5.30 -14 -8 0 7.10 2.90 14 -8 0 6.60 2.50 -14 8 0 4.70 3.40 -14 8 0 5.00 3.00 -14 8 0 5.10 3.20 -16 -8 0 38.00 5.10 -16 8 0 33.90 6.00 -16 8 0 43.50 6.50 -16 8 0 32.10 5.00 -1 -9 0 136.89 4.90 -1 -9 0 140.19 5.00 1 -9 0 128.09 5.00 1 -9 0 135.79 4.60 1 -9 0 135.59 4.60 -1 -9 0 142.29 4.70 -1 9 0 134.39 5.10 -3 -9 0 516.15 12.90 3 -9 0 524.35 13.50 3 -9 0 539.45 12.30 -3 -9 0 534.45 13.60 -3 -9 0 535.25 12.90 -3 9 0 535.75 12.70 -3 9 0 516.65 13.70 -5 -9 0 36.50 3.10 -5 -9 0 41.00 3.30 5 -9 0 41.00 2.00 5 -9 0 41.30 3.20 5 9 0 34.70 2.10 -5 9 0 40.90 3.40 -5 9 0 44.30 2.90 -7 -9 0 44.60 3.80 -7 -9 0 40.20 3.80 7 -9 0 41.90 1.90 7 -9 0 39.30 3.60 -7 9 0 37.70 3.70 -7 9 0 42.90 3.40 -9 -9 0 174.68 7.30 9 -9 0 172.08 7.30 -9 9 0 173.08 7.10 -9 9 0 164.38 7.50 -9 9 0 170.38 8.00 -11 -9 0 10.20 2.80 11 -9 0 13.80 2.80 -11 9 0 14.20 3.30 -11 9 0 16.40 3.20 -11 9 0 10.80 3.20 -13 -9 0 14.10 3.30 13 -9 0 14.50 3.10 -13 9 0 8.80 3.20 -13 9 0 10.60 3.10 -13 9 0 5.90 3.50 15 -9 0 34.80 4.50 -15 -9 0 34.10 4.80 -15 9 0 31.40 4.80 -15 9 0 31.00 5.10 0 -10 0 3284.27 66.99 0 -10 0 3304.87 66.59 0 -10 0 3178.18 67.09 0 10 0 3242.98 67.19 -2 -10 0 15.00 1.90 2 -10 0 19.30 2.50 -2 -10 0 14.10 2.00 2 -10 0 17.70 1.90 -2 -10 0 14.20 1.80 -2 10 0 16.10 1.80 -2 10 0 12.60 2.00 -4 -10 0 12.50 2.00 -4 -10 0 14.30 2.30 4 -10 0 9.00 1.80 4 -10 0 11.00 1.40 -4 10 0 10.70 1.70 -4 10 0 12.00 2.20 4 10 0 10.20 1.50 -6 -10 0 1779.92 39.00 -6 -10 0 1722.23 39.50 6 -10 0 1835.32 36.60 6 -10 0 1836.52 39.50 -6 10 0 1759.02 38.20 6 10 0 1755.72 36.50 -6 10 0 1734.93 39.80 -6 10 0 1743.33 39.50 -8 -10 0 -1.10 1.50 8 -10 0 1.60 1.80 -8 10 0 0.30 1.80 -8 10 0 1.50 1.70 -8 10 0 1.70 1.70 10 -10 0 0.50 1.70 -10 -10 0 2.40 2.00 -10 10 0 2.90 2.20 -10 10 0 0.60 2.20 -10 10 0 0.20 2.10 -12 -10 0 515.35 15.90 12 -10 0 509.75 15.80 -12 10 0 515.75 17.40 -12 10 0 554.24 17.00 -12 10 0 532.65 16.10 -14 -10 0 5.80 2.90 14 -10 0 10.60 3.00 -14 10 0 11.10 3.80 -14 10 0 6.90 3.00 -16 -10 0 10.50 3.50 -16 10 0 9.10 3.80 -16 10 0 5.50 3.90 -1 -11 0 65.59 3.60 -1 -11 0 62.99 3.50 1 -11 0 58.79 3.20 1 -11 0 58.09 3.60 -1 -11 0 59.79 3.20 1 -11 0 65.39 3.30 -1 11 0 62.49 3.70 -1 11 0 58.99 3.20 -3 -11 0 159.28 5.80 3 -11 0 154.68 6.20 -3 -11 0 146.29 5.60 3 -11 0 157.68 5.20 -3 -11 0 154.38 6.20 -3 11 0 151.78 6.30 -3 11 0 152.38 5.40 5 -11 0 5.50 1.10 5 -11 0 7.50 2.10 -5 -11 0 9.70 2.10 -5 -11 0 7.30 2.00 -5 11 0 7.00 1.70 5 11 0 8.30 1.50 -5 11 0 4.70 1.90 -7 -11 0 181.18 7.80 7 -11 0 171.28 7.30 -7 -11 0 167.08 7.10 -7 11 0 169.88 7.70 -7 11 0 169.88 7.50 -7 11 0 177.88 6.70 9 -11 0 79.39 5.50 -9 -11 0 90.79 5.60 -9 11 0 79.79 5.60 -9 11 0 78.39 5.90 -9 11 0 83.69 5.20 -11 -11 0 27.00 3.90 11 -11 0 34.50 4.40 -11 11 0 30.80 4.80 -11 11 0 26.00 3.80 -11 11 0 23.70 3.90 -13 -11 0 101.79 6.90 13 -11 0 105.89 6.90 -13 11 0 109.79 7.10 -13 11 0 117.19 7.90 -15 -11 0 22.60 4.20 15 -11 0 21.70 4.20 -15 11 0 22.90 4.30 -15 11 0 13.70 4.40 0 -12 0 228.48 7.70 0 -12 0 226.18 7.40 0 -12 0 224.78 7.10 0 12 0 229.08 7.70 2 -12 0 59.39 3.90 2 -12 0 56.89 3.20 -2 -12 0 60.99 3.50 -2 -12 0 61.89 3.90 -2 -12 0 59.99 3.70 -2 12 0 61.09 4.00 -2 12 0 59.19 3.30 -4 -12 0 20.60 2.60 4 -12 0 25.80 2.10 -4 -12 0 21.10 2.80 4 -12 0 21.60 3.00 4 12 0 19.90 2.20 -4 12 0 20.10 2.90 -4 12 0 20.00 2.40 -6 -12 0 76.09 4.70 6 -12 0 70.09 3.00 6 -12 0 68.19 4.80 -6 -12 0 70.89 5.00 -6 12 0 76.69 4.30 -6 12 0 72.59 5.00 -6 12 0 75.59 5.20 8 -12 0 5.10 2.30 -8 -12 0 3.20 2.10 -8 12 0 4.50 2.00 -8 12 0 3.80 2.40 -8 12 0 3.10 2.00 10 -12 0 2.90 2.20 -10 -12 0 3.20 2.40 -10 12 0 4.50 2.60 -10 12 0 5.00 2.60 -10 12 0 6.10 2.80 12 -12 0 65.89 5.80 -12 -12 0 65.39 5.90 -12 12 0 55.79 6.10 -12 12 0 71.69 5.80 -12 12 0 77.49 6.60 14 -12 0 1.40 2.80 -14 -12 0 -0.80 2.70 -14 12 0 -1.40 2.90 -14 12 0 1.90 2.70 1 -13 0 2.40 1.30 1 -13 0 1.80 1.50 -1 -13 0 0.50 1.10 -1 -13 0 -0.80 1.20 1 -13 0 3.60 1.40 -1 -13 0 1.70 1.40 1 13 0 1.00 1.20 -1 13 0 1.50 1.10 -1 13 0 2.40 1.40 -3 -13 0 2535.25 53.09 3 -13 0 2480.65 52.09 3 -13 0 2454.75 53.99 -3 -13 0 2491.25 52.79 -3 -13 0 2458.05 53.79 -3 13 0 2517.85 54.09 -3 13 0 2504.65 52.59 -5 -13 0 29.60 3.70 5 -13 0 26.50 3.60 -5 -13 0 25.10 3.10 5 -13 0 27.80 2.10 -5 13 0 29.10 3.70 -5 13 0 20.80 2.60 -5 13 0 25.90 3.40 5 13 0 24.50 2.40 -7 -13 0 22.10 3.50 7 -13 0 24.90 3.60 -7 -13 0 25.00 3.40 -7 13 0 28.60 3.20 -7 13 0 30.90 4.20 -7 13 0 22.80 3.40 9 -13 0 994.30 25.80 -9 -13 0 976.60 25.10 -9 13 0 996.20 26.60 -9 13 0 967.50 26.10 -9 13 0 999.60 24.40 -11 -13 0 80.89 6.10 11 -13 0 79.19 6.20 -11 13 0 79.29 7.10 -11 13 0 80.59 5.90 -11 13 0 90.79 6.90 13 -13 0 0.30 2.50 -13 -13 0 1.70 2.80 -13 13 0 -2.80 2.70 -13 13 0 2.80 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2.40 -8 8 -4 -0.70 1.70 10 -8 4 91.09 6.50 -10 -8 -4 86.69 6.00 -10 -8 -4 77.59 5.50 10 8 4 79.39 5.40 -10 8 -4 90.79 5.90 -10 8 -4 96.29 6.80 -10 8 -4 89.59 6.50 12 -8 4 18.00 3.60 -12 -8 -4 19.30 3.50 -12 8 -4 15.60 4.70 -12 8 -4 18.60 4.20 14 -8 4 6.00 3.20 -14 -8 -4 8.30 3.00 -14 8 -4 5.10 3.70 -17 -9 4 48.00 5.90 -17 9 4 52.99 6.70 -17 9 4 58.39 6.20 -15 -9 4 16.50 3.90 -15 9 4 12.10 3.60 -15 9 4 12.00 3.50 -15 9 4 13.00 4.10 13 -9 -4 49.10 4.50 -13 -9 4 46.20 5.10 13 -9 -4 51.29 3.90 -13 9 4 41.50 5.40 -13 9 4 53.69 6.20 -13 9 4 53.89 5.40 11 -9 -4 76.29 4.40 -11 -9 4 63.39 5.30 11 -9 -4 68.79 4.70 -11 9 4 72.89 5.70 -11 9 4 63.09 5.70 -11 9 4 65.99 5.60 -11 9 4 69.09 4.10 9 -9 -4 0.70 1.60 -9 -9 4 -0.90 1.70 9 -9 -4 1.40 1.50 -9 9 4 3.10 1.10 -9 9 4 1.30 2.00 -9 9 4 3.10 2.20 -9 9 4 3.50 2.40 7 -9 -4 127.79 5.50 -7 -9 4 135.39 6.20 7 -9 -4 126.09 5.90 -7 -9 4 132.19 3.70 -7 9 4 129.39 3.80 -7 9 4 123.39 6.30 -7 9 4 129.99 6.10 -7 9 4 124.59 6.30 -5 -9 4 9.30 2.00 5 -9 -4 5.00 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147.89 10.10 -10 16 7 150.08 9.50 8 -16 -7 61.19 6.10 -8 -16 7 56.39 5.80 -8 16 7 49.99 6.00 -8 16 7 71.39 7.90 -6 -16 7 3.40 2.50 6 -16 -7 9.10 3.00 6 16 -7 9.40 3.20 -6 16 7 3.90 3.50 -6 16 7 9.60 3.20 -4 -16 7 184.88 9.10 -4 -16 7 199.48 8.30 4 -16 -7 218.58 9.80 -4 16 7 203.18 10.60 -4 16 7 212.28 9.40 4 16 -7 193.28 9.70 -2 -16 7 31.00 4.00 2 -16 -7 30.60 4.40 -2 16 7 37.90 5.40 2 16 -7 25.30 4.40 2 16 -7 24.10 4.50 0 -16 7 0.00 2.00 0 -16 -7 -0.30 2.20 0 16 7 -1.20 2.40 0 16 -7 3.00 2.90 -2 -16 -7 164.48 9.30 2 -16 7 165.08 9.00 2 16 7 162.98 8.90 -2 16 -7 171.88 9.40 -4 -16 -7 28.10 4.90 4 -16 7 18.40 4.20 -4 16 -7 23.50 4.60 6 -16 7 0.50 3.10 -6 -16 -7 4.50 3.10 -6 16 -7 2.80 3.70 -13 -17 7 4.60 3.60 -13 17 7 3.40 4.10 -13 17 7 12.90 4.70 -11 -17 7 2.90 3.40 11 -17 -7 9.20 3.20 -11 17 7 3.30 4.20 -11 17 7 5.40 3.90 -9 -17 7 144.49 8.70 9 -17 -7 140.69 8.20 -9 17 7 127.79 9.00 -9 17 7 144.29 10.30 7 -17 -7 25.70 4.30 -7 -17 7 28.50 4.50 -7 17 7 36.80 5.40 -7 17 7 29.00 5.80 -5 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72.19 6.40 11 -9 -9 168.08 8.90 -11 -9 9 157.78 7.90 -11 9 9 167.58 9.60 -11 9 9 170.18 9.40 -11 9 9 167.38 8.50 9 -9 -9 24.60 4.10 -9 -9 9 23.50 3.40 -9 9 9 26.90 3.90 -9 9 9 20.40 4.30 -9 9 9 31.80 4.90 7 -9 -9 20.70 3.80 -7 -9 9 25.10 3.50 -7 -9 9 27.60 3.50 -7 -9 9 24.80 2.80 7 9 -9 26.80 3.70 -7 9 9 22.00 4.00 -7 9 9 27.40 4.70 -5 -9 9 146.59 7.50 5 -9 -9 141.39 7.40 -5 -9 9 146.79 6.60 -5 -9 9 145.29 6.50 -5 9 9 136.79 8.40 -5 9 9 135.19 7.30 5 9 -9 143.49 7.10 -3 -9 9 38.60 4.30 3 -9 -9 33.80 4.40 -3 9 9 30.50 4.60 -3 9 9 33.20 4.00 3 9 -9 39.20 4.70 3 9 -9 35.60 4.10 1 -9 -9 17.60 3.30 -1 -9 9 16.50 3.30 -1 9 9 13.40 3.60 1 9 -9 17.40 3.20 1 -9 9 4.70 2.50 -1 -9 -9 4.20 2.30 1 9 9 4.50 2.50 -1 9 -9 7.10 2.70 -1 9 -9 3.10 2.30 3 -9 9 151.28 9.00 -3 -9 -9 164.48 8.30 -3 9 -9 152.68 8.40 3 9 9 143.99 8.20 -3 9 -9 148.09 8.20 -5 -9 -9 41.10 5.00 5 -9 9 33.90 5.40 -5 9 -9 33.40 5.10 7 -9 9 10.40 4.00 -7 9 -9 7.30 3.80 7 9 9 5.00 3.50 -16 -10 9 12.50 3.80 16 -10 -9 11.20 3.80 -16 10 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0.50 2.90 -5 -11 -9 3.90 2.60 -5 11 -9 1.30 3.00 -16 -12 9 61.79 6.60 16 -12 -9 52.49 6.10 14 -12 -9 90.99 7.20 -14 -12 9 86.09 7.40 -14 12 9 85.59 8.80 -14 12 9 86.39 8.10 12 -12 -9 72.89 6.40 -12 -12 9 70.89 6.50 -12 12 9 70.29 7.70 -12 12 9 75.99 7.80 10 -12 -9 33.70 4.80 -10 -12 9 34.30 4.70 -10 12 9 32.40 5.60 -10 12 9 35.70 5.60 -8 -12 9 84.29 6.10 8 -12 -9 94.89 6.70 -8 12 9 91.19 7.20 -8 12 9 80.99 7.30 -6 -12 9 0.40 2.10 -6 -12 9 4.50 1.80 6 -12 -9 1.90 2.30 6 12 -9 2.40 2.30 -6 12 9 4.70 2.80 -6 12 9 6.90 3.40 4 -12 -9 4.30 2.30 -4 -12 9 2.70 2.20 -4 -12 9 3.90 2.00 4 12 -9 2.40 2.40 -4 12 9 6.90 3.20 -4 12 9 5.40 2.50 2 -12 -9 20.60 3.80 -2 -12 9 15.40 3.20 -2 12 9 18.30 4.10 2 12 -9 13.80 3.20 0 -12 -9 71.69 6.10 0 -12 9 49.99 5.40 0 12 -9 63.69 5.80 0 12 -9 59.89 5.90 0 12 9 64.89 6.30 -2 -12 -9 10.40 3.30 2 -12 9 8.90 3.10 2 12 9 13.10 3.50 -2 12 -9 14.70 3.70 -4 -12 -9 1.10 2.60 4 -12 9 7.00 3.40 -4 12 -9 9.20 3.70 -6 -12 -9 153.08 9.00 6 -12 9 159.88 10.40 -6 12 -9 149.69 9.80 15 -13 -9 3.20 3.00 -15 -13 9 0.90 3.10 -15 13 9 6.90 4.10 -15 13 9 4.30 3.80 -13 -13 9 7.30 3.60 13 -13 -9 14.40 3.60 -13 13 9 17.50 4.80 -13 13 9 15.60 4.70 -11 -13 9 199.48 9.80 11 -13 -9 186.78 9.70 -11 13 9 202.48 11.10 -11 13 9 203.58 11.30 -9 -13 9 21.60 3.80 9 -13 -9 22.10 4.20 -9 13 9 19.50 4.70 -9 13 9 20.50 4.30 7 -13 -9 77.69 6.30 -7 -13 9 77.19 6.00 -7 13 9 79.69 7.40 7 13 -9 76.59 6.20 -7 13 9 70.69 6.60 -5 -13 9 268.97 9.60 -5 -13 9 268.77 10.40 5 -13 -9 257.77 11.20 -5 13 9 260.47 10.70 -5 13 9 257.27 12.20 5 13 -9 263.47 11.00 3 -13 -9 74.99 6.10 -3 -13 9 74.69 5.40 -3 13 9 67.99 7.20 3 13 -9 69.89 6.00 -1 -13 9 68.49 5.80 1 -13 -9 77.39 6.30 1 13 -9 71.39 6.60 -1 13 9 79.99 6.90 1 13 -9 73.59 6.10 1 -13 9 145.89 8.50 -1 -13 -9 150.18 8.60 -1 13 -9 146.39 8.70 1 13 9 136.89 8.50 -3 -13 -9 73.39 6.80 3 -13 9 61.99 6.70 -3 13 -9 76.99 7.40 -5 -13 -9 33.60 5.00 5 -13 9 45.20 6.30 -5 13 -9 41.40 6.10 -14 -14 9 0.50 3.30 14 -14 -9 3.00 2.80 -14 14 9 0.10 3.60 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4.10 -7 15 9 12.80 3.90 -7 15 9 9.70 4.10 7 15 -9 16.20 4.00 -5 -15 9 4.00 2.50 5 -15 -9 0.40 2.20 -5 15 9 3.20 3.60 5 15 -9 2.20 2.60 -3 -15 9 10.30 3.00 3 -15 -9 10.10 3.10 3 15 -9 9.70 3.50 -3 15 9 2.70 3.40 -1 -15 9 15.40 3.40 1 -15 -9 17.20 4.10 -1 15 9 15.50 4.10 1 15 -9 17.50 4.10 1 -15 9 10.30 3.10 -1 -15 -9 14.00 3.70 1 15 9 14.50 3.90 -1 15 -9 16.90 4.00 -3 -15 -9 28.00 5.00 3 -15 9 25.40 5.00 -3 15 -9 14.00 4.10 -12 -16 9 47.10 6.00 12 -16 -9 63.49 6.70 -12 16 9 45.30 6.80 -12 16 9 60.49 7.40 -10 -16 9 7.40 3.60 10 -16 -9 13.60 3.70 -10 16 9 15.90 4.80 -10 16 9 15.70 4.40 -8 -16 9 121.39 8.10 8 -16 -9 128.79 8.30 -8 16 9 119.09 9.60 -8 16 9 134.89 8.80 8 16 -9 120.29 8.40 -6 -16 9 95.99 7.20 6 -16 -9 95.39 7.30 6 16 -9 104.49 7.70 -6 16 9 106.69 8.70 -4 -16 9 10.10 3.50 4 -16 -9 14.90 3.90 -4 16 9 20.50 4.90 4 16 -9 14.50 3.80 -2 -16 9 108.79 7.20 2 -16 -9 117.39 8.10 -2 16 9 136.39 9.20 2 16 -9 107.29 7.80 0 -16 -9 43.60 5.90 0 -16 9 34.40 5.00 0 16 -9 40.70 5.90 0 16 9 49.70 6.20 2 -16 9 9.70 3.50 -2 -16 -9 6.20 3.30 -2 16 -9 0.60 3.10 -11 -17 9 4.00 3.50 11 -17 -9 3.10 3.10 -11 17 9 2.70 4.10 -11 17 9 5.20 3.90 -9 -17 9 1.00 3.00 9 -17 -9 0.00 2.60 -9 17 9 -0.40 3.80 9 17 -9 2.50 3.20 -9 17 9 7.90 4.00 7 -17 -9 99.19 7.60 -7 -17 9 107.19 7.70 -7 17 9 105.09 11.20 -7 17 9 112.09 9.40 7 17 -9 119.49 8.50 5 -17 -9 4.20 2.80 -5 -17 9 2.00 2.80 -5 17 9 -3.40 3.10 5 17 -9 0.30 2.70 -3 -17 9 2.00 2.40 3 -17 -9 -0.40 2.40 3 17 -9 -0.70 2.80 -3 17 9 -2.50 2.90 1 -17 -9 100.09 7.80 -1 -17 9 101.79 7.30 -1 17 9 109.69 8.50 1 17 -9 102.69 8.30 -1 -17 -9 -1.70 2.60 1 -17 9 3.10 3.10 -1 17 -9 0.70 3.20 8 -18 -9 24.20 4.90 -8 -18 9 26.60 4.50 -8 18 9 30.80 6.30 -8 18 9 46.70 6.10 8 18 -9 28.00 5.30 6 -18 -9 49.80 6.50 -6 -18 9 42.40 5.50 6 18 -9 51.79 6.40 -6 18 9 46.10 6.70 4 -18 -9 39.30 5.60 4 18 -9 44.10 5.90 -4 18 9 40.50 6.20 2 -18 -9 56.39 6.90 -2 -18 9 55.49 6.10 -2 18 9 54.39 7.00 2 18 -9 51.49 6.60 -18 0 10 203.88 11.30 18 0 -10 187.98 11.10 16 0 -10 49.60 6.40 -16 0 10 45.30 6.10 14 0 -10 227.98 11.20 -14 0 10 249.18 9.70 -14 0 10 243.18 11.50 -12 0 10 1132.49 28.10 12 0 -10 1076.09 28.90 -12 0 10 1093.59 29.70 10 0 -10 135.19 7.60 -10 0 10 151.18 7.80 -10 0 10 151.88 8.60 -8 0 10 216.68 10.00 8 0 -10 228.58 9.40 -8 0 10 213.68 9.70 6 0 -10 2198.48 48.70 -6 0 10 2190.38 49.80 -6 0 10 2172.88 50.19 6 0 -10 2107.99 45.70 -4 0 10 346.57 12.10 4 0 -10 334.47 9.70 -4 0 10 323.17 12.70 4 0 -10 338.57 11.20 -2 0 10 35.50 5.10 2 0 -10 34.60 3.30 2 0 -10 42.00 4.30 0 0 -10 1828.02 41.10 0 0 10 1817.92 44.30 0 0 10 1863.11 45.00 0 0 -10 1856.71 41.20 2 0 10 101.69 7.60 -2 0 -10 99.99 6.00 2 0 10 106.89 7.80 4 0 10 1.70 2.80 4 0 10 -2.10 2.60 -4 0 -10 4.40 2.60 -6 0 -10 837.42 23.90 6 0 10 829.62 25.90 -17 -1 10 93.19 7.80 17 -1 -10 97.09 8.20 17 1 -10 91.29 8.70 -17 1 10 107.69 8.50 15 -1 -10 31.20 5.00 -15 -1 10 31.80 5.20 15 1 -10 31.50 5.60 -15 1 10 30.00 5.20 -13 -1 10 21.30 3.60 13 -1 -10 23.30 4.20 -13 -1 10 16.90 3.80 13 1 -10 21.50 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3.10 1.40 -6 -2 10 7.40 2.80 6 -2 -10 3.80 2.00 -6 -2 10 4.60 2.50 -6 -2 10 2.90 2.00 6 2 -10 2.40 1.40 -6 2 10 1.50 2.10 -6 2 10 2.00 2.30 6 2 -10 4.10 1.90 -4 -2 10 55.99 5.40 4 -2 -10 47.80 4.50 -4 -2 10 52.39 4.70 4 2 -10 57.29 4.20 4 2 -10 62.29 3.90 -4 2 10 50.49 5.60 -4 2 10 56.79 4.90 -2 -2 10 34.80 4.50 -2 -2 10 25.20 4.50 2 -2 -10 24.10 3.30 2 -2 -10 26.40 2.90 -2 2 10 35.40 5.10 2 2 -10 25.50 3.40 2 2 -10 26.50 3.30 0 -2 -10 5.10 1.90 0 -2 10 0.10 2.30 0 -2 10 5.90 3.00 0 -2 -10 1.10 1.40 0 2 -10 3.00 2.00 0 2 10 1.10 2.50 2 -2 10 5.20 2.80 -2 -2 -10 5.90 2.20 2 -2 10 2.20 2.80 2 2 10 4.10 2.90 2 2 10 1.30 2.50 -2 2 -10 3.20 2.40 4 -2 10 55.39 6.60 -4 -2 -10 65.49 5.60 4 -2 10 54.19 6.20 4 2 10 57.49 6.30 4 2 10 48.10 6.30 -4 2 -10 63.39 5.70 -6 -2 -10 6.00 2.90 6 -2 10 -2.10 2.90 6 2 10 -1.80 2.60 -6 2 -10 -0.20 2.50 6 2 10 -1.30 2.50 17 -3 -10 137.39 8.80 -17 -3 10 119.29 8.70 -17 -3 10 116.79 7.30 -17 3 10 129.79 9.50 -15 -3 10 346.97 13.70 15 -3 -10 330.97 13.30 -15 -3 10 300.07 11.20 -15 3 10 326.27 12.50 -15 3 10 308.07 13.60 -13 -3 10 172.78 9.30 -13 -3 10 172.88 9.10 -13 -3 10 151.88 7.00 13 -3 -10 162.08 8.80 -13 3 10 150.98 9.20 -13 3 10 170.88 8.90 -11 -3 10 110.59 5.50 11 -3 -10 110.39 7.20 -11 -3 10 123.09 8.00 -11 -3 10 116.89 6.60 -11 3 10 123.19 7.50 -11 3 10 104.59 7.60 11 3 -10 117.99 8.00 -9 -3 10 941.51 22.90 9 -3 -10 966.90 25.70 -9 -3 10 965.60 26.60 -9 -3 10 964.00 22.50 -9 -3 10 1005.20 25.40 -9 3 10 972.10 26.50 9 3 -10 979.70 25.80 -9 3 10 990.30 26.50 9 3 -10 996.60 23.40 -7 -3 10 310.97 12.40 7 -3 -10 313.37 11.50 -7 -3 10 320.57 11.80 -7 -3 10 281.57 10.30 -7 -3 10 320.27 10.30 7 3 -10 326.87 9.80 -7 3 10 343.57 12.30 7 3 -10 303.57 11.10 -7 3 10 308.87 12.30 -5 -3 10 52.79 5.70 -5 -3 10 46.60 4.60 5 -3 -10 54.89 4.80 -5 3 10 42.20 4.60 5 3 -10 41.60 3.50 -5 3 10 53.49 5.90 5 3 -10 43.10 4.00 3 -3 -10 1381.96 32.50 -3 -3 10 1341.87 34.50 -3 -3 10 1382.56 33.20 3 3 -10 1355.66 31.30 3 3 -10 1320.47 31.40 -3 3 10 1358.16 34.80 -3 3 10 1379.86 32.50 1 -3 -10 238.68 9.30 -1 -3 10 243.78 11.20 -1 -3 10 265.87 10.90 1 3 -10 253.27 9.10 -1 3 10 234.98 11.00 1 3 -10 243.78 8.50 -1 -3 -10 3.50 1.70 -1 -3 -10 1.80 1.80 1 -3 10 2.70 2.40 1 -3 10 2.10 2.60 1 3 10 0.30 2.50 -1 3 -10 0.10 1.90 3 -3 10 903.41 26.60 -3 -3 -10 946.71 23.80 3 -3 10 925.11 27.00 3 3 10 908.91 26.00 -3 3 -10 886.91 24.40 3 3 10 959.80 27.30 -5 -3 -10 38.10 4.60 5 -3 10 34.90 5.70 5 3 10 42.10 5.40 5 3 10 40.90 6.10 -5 3 -10 27.20 4.50 7 -3 10 9.20 3.80 -7 -3 -10 9.90 3.20 -7 3 -10 9.00 3.70 7 3 10 3.70 3.70 18 -4 -10 17.70 4.40 -18 -4 10 15.80 4.20 -18 -4 10 13.40 3.80 -18 4 10 16.60 4.60 16 -4 -10 6.30 3.30 -16 -4 10 8.50 3.50 -16 -4 10 6.80 2.90 -16 4 10 4.60 3.60 -14 -4 10 121.79 8.10 -14 -4 10 112.29 6.50 14 -4 -10 119.99 7.90 -14 4 10 104.39 7.50 -14 4 10 104.49 8.20 -12 -4 10 16.50 3.80 -12 -4 10 11.10 2.60 -12 -4 10 19.20 3.10 12 -4 -10 13.10 3.60 -12 4 10 11.50 3.40 -12 4 10 13.90 3.70 -10 -4 10 30.40 4.70 10 -4 -10 21.70 3.80 -10 -4 10 27.20 3.10 -10 -4 10 26.40 3.70 -10 4 10 30.60 4.70 -10 4 10 23.90 4.20 -8 -4 10 66.99 4.00 8 -4 -10 64.19 5.40 -8 -4 10 68.59 6.10 -8 -4 10 62.99 4.00 -8 -4 10 68.59 5.30 8 4 -10 65.99 4.30 -8 4 10 69.19 5.90 8 4 -10 74.99 5.90 -8 4 10 71.19 6.20 6 -4 -10 1.90 2.00 -6 -4 10 -1.10 2.00 -6 -4 10 3.80 1.40 -6 -4 10 3.10 1.80 -6 4 10 4.10 2.30 6 4 -10 4.20 2.10 6 4 -10 2.70 1.70 -6 4 10 4.60 2.50 4 -4 -10 106.49 6.20 -4 -4 10 115.49 6.30 -4 -4 10 94.79 6.70 -4 4 10 105.49 6.20 4 4 -10 97.69 5.40 4 4 -10 98.99 5.40 -4 4 10 94.49 7.00 -2 -4 10 0.00 1.90 2 -4 -10 1.40 1.90 -2 -4 10 1.70 2.20 2 4 -10 0.30 1.70 2 4 -10 0.80 1.40 -2 4 10 6.80 3.20 -2 4 10 0.90 1.60 0 -4 -10 5.90 2.10 0 -4 10 2.40 2.50 0 -4 10 4.00 2.60 0 4 -10 2.70 2.00 0 4 -10 1.90 1.80 0 4 10 7.50 3.20 2 -4 10 178.68 9.90 2 -4 10 173.08 9.60 -2 -4 -10 167.38 7.80 2 4 10 179.18 9.70 -2 4 -10 183.68 8.60 4 -4 10 5.30 3.30 -4 4 -10 10.30 3.20 4 4 10 7.80 3.30 4 4 10 12.70 3.80 6 -4 10 0.70 3.10 6 4 10 2.50 2.70 -6 4 -10 4.80 3.00 6 4 10 0.60 3.30 17 -5 -10 4.20 3.10 -17 -5 10 3.10 2.90 -17 -5 10 6.60 3.50 -17 5 10 6.50 3.90 -15 -5 10 4.00 3.10 -15 -5 10 0.80 2.50 15 -5 -10 7.50 3.40 -15 5 10 4.50 3.60 -15 5 10 1.90 2.80 13 -5 -10 11.80 3.40 -13 -5 10 13.30 3.80 -13 -5 10 14.10 2.90 -13 5 10 15.30 4.00 -13 5 10 9.70 3.40 11 -5 -10 5.40 2.60 -11 -5 10 3.90 2.00 -11 -5 10 5.20 2.10 -11 -5 10 5.10 3.00 -11 5 10 4.10 3.10 -11 5 10 2.90 2.70 -9 -5 10 0.90 2.10 -9 -5 10 9.00 2.10 -9 -5 10 7.80 3.20 9 -5 -10 8.50 2.70 9 5 -10 10.00 2.40 -9 5 10 2.70 2.70 -9 5 10 7.60 3.20 -7 -5 10 28.50 2.90 -7 -5 10 28.20 4.10 7 -5 -10 25.10 3.90 -7 -5 10 28.50 3.20 -7 5 10 29.90 4.60 7 5 -10 28.80 3.30 -7 5 10 27.80 4.30 7 5 -10 31.60 4.30 5 -5 -10 4.90 2.40 -5 -5 10 3.70 2.50 -5 -5 10 2.50 1.80 5 5 -10 3.10 1.80 -5 5 10 2.80 2.10 5 5 -10 3.90 1.90 -5 5 10 6.70 2.90 -3 -5 10 10.00 2.80 -3 -5 10 12.00 3.20 3 -5 -10 9.50 2.70 -3 5 10 6.90 2.80 -3 5 10 12.40 2.70 3 5 -10 8.90 2.30 3 5 -10 9.40 2.10 1 -5 -10 5.00 2.20 -1 -5 10 8.30 2.90 -1 -5 10 5.60 2.50 -1 5 10 6.10 3.10 1 5 -10 6.90 2.40 -1 -5 -10 6.70 2.40 1 -5 10 10.10 3.20 1 -5 10 10.00 3.60 1 5 10 10.40 3.50 -1 5 -10 4.10 2.40 3 -5 10 11.60 3.60 -3 -5 -10 9.60 2.80 3 5 10 11.40 3.60 -3 5 -10 9.50 3.10 5 -5 10 -1.10 2.80 5 5 10 4.20 2.80 5 5 10 1.10 2.80 -5 5 -10 -0.30 2.70 7 -5 10 3.20 3.50 -7 5 -10 1.50 2.90 7 5 10 4.50 4.00 18 -6 -10 30.90 5.50 -18 -6 10 29.30 4.70 -16 -6 10 78.49 6.50 16 -6 -10 87.89 7.30 -16 -6 10 77.29 7.20 -16 6 10 77.49 7.20 -16 6 10 83.79 8.80 14 -6 -10 7.30 3.10 -14 -6 10 6.60 2.80 -14 -6 10 2.40 3.00 -14 6 10 7.50 3.50 -14 6 10 2.60 3.20 -14 6 10 7.30 3.20 -12 -6 10 130.49 6.80 -12 -6 10 137.69 8.40 12 -6 -10 144.09 8.20 -12 6 10 149.69 9.30 -12 6 10 142.79 8.70 10 -6 -10 272.77 11.50 -10 -6 10 297.57 9.80 -10 -6 10 301.97 10.60 -10 -6 10 285.57 12.10 -10 6 10 276.67 12.10 -10 6 10 293.47 12.30 8 -6 -10 0.40 2.10 -8 -6 10 2.40 1.60 -8 -6 10 0.30 2.00 -8 -6 10 1.20 1.10 8 6 -10 1.60 1.80 -8 6 10 1.10 2.70 -8 6 10 2.20 2.50 -6 -6 10 351.96 11.30 6 -6 -10 360.36 12.80 -6 -6 10 337.47 10.40 -6 -6 10 365.46 12.90 -6 6 10 375.76 13.00 -6 6 10 360.76 13.80 6 6 -10 340.57 11.20 6 6 -10 355.66 11.90 -4 -6 10 292.47 11.90 4 -6 -10 296.87 11.30 -4 -6 10 310.27 10.90 -4 6 10 277.27 12.10 4 6 -10 300.87 10.00 4 6 -10 318.27 10.50 -4 6 10 304.47 11.00 -2 -6 10 -2.70 2.00 2 -6 -10 1.20 1.80 -2 -6 10 2.30 2.10 -2 6 10 1.80 2.40 -2 6 10 1.00 1.70 2 6 -10 0.00 1.70 0 -6 10 423.66 15.10 0 -6 -10 419.46 14.10 0 -6 10 435.56 16.10 0 6 10 452.75 16.00 0 6 -10 475.25 14.40 0 6 -10 418.16 13.90 -2 -6 -10 179.58 8.50 2 -6 10 178.08 9.70 2 6 10 192.28 10.00 -2 6 -10 193.68 8.90 4 -6 10 17.20 4.20 -4 6 -10 15.50 3.90 4 6 10 17.30 3.80 6 -6 10 162.38 10.70 6 6 10 181.88 10.40 -6 6 -10 165.28 9.60 17 -7 -10 11.10 3.90 -17 -7 10 8.40 3.50 -17 -7 10 8.90 3.30 -17 7 10 17.60 5.00 -15 -7 10 68.49 6.90 -15 -7 10 72.39 6.10 15 -7 -10 77.79 6.90 -15 7 10 78.29 8.10 -15 7 10 74.09 7.20 13 -7 -10 35.90 5.30 -13 -7 10 25.50 3.80 -13 -7 10 29.00 4.80 -13 7 10 35.00 5.50 -13 7 10 31.80 5.10 -13 7 10 39.20 5.30 -11 -7 10 19.60 3.00 -11 -7 10 19.20 3.20 11 -7 -10 27.00 4.30 -11 7 10 19.20 4.40 -11 7 10 22.00 4.70 -9 -7 10 122.79 6.00 9 -7 -10 97.99 6.90 -9 -7 10 129.59 6.80 -9 7 10 124.59 8.00 -9 7 10 112.99 8.00 7 -7 -10 103.99 6.80 -7 -7 10 105.69 5.20 -7 -7 10 105.29 6.50 -7 -7 10 105.79 5.40 7 7 -10 106.29 5.90 -7 7 10 117.19 7.20 -7 7 10 102.89 7.50 -5 -7 10 3.90 1.80 -5 -7 10 7.20 2.20 5 -7 -10 4.70 2.40 -5 -7 10 2.50 2.20 -5 7 10 6.40 2.50 5 7 -10 6.00 2.30 -5 7 10 1.10 2.80 5 7 -10 2.70 2.00 -3 -7 10 180.98 9.20 -3 -7 10 174.38 8.00 3 -7 -10 171.68 8.30 3 7 -10 172.78 7.80 -3 7 10 141.69 8.80 -3 7 10 161.68 7.30 1 -7 -10 158.78 8.00 -1 -7 10 160.38 9.20 -1 -7 10 161.88 8.40 1 7 -10 156.08 7.70 -1 7 10 168.58 9.20 1 -7 10 16.10 3.80 -1 -7 -10 10.30 2.80 1 7 10 9.90 3.40 -1 7 -10 10.80 3.10 -1 7 -10 15.70 3.40 3 -7 10 91.69 7.40 -3 -7 -10 83.09 6.00 -3 7 -10 77.09 6.30 3 7 10 80.19 6.80 5 -7 10 157.58 10.10 5 7 10 169.48 10.10 5 7 10 156.68 10.90 -5 7 -10 149.59 9.00 -16 -8 10 23.40 4.10 16 -8 -10 16.80 4.30 -16 8 10 17.40 4.50 -16 8 10 17.50 5.00 -14 -8 10 2.70 2.70 14 -8 -10 -2.10 2.50 -14 8 10 0.10 3.30 -14 8 10 3.30 3.20 12 -8 -10 48.60 5.70 -12 -8 10 50.29 4.80 -12 8 10 37.50 5.70 -12 8 10 40.70 5.60 -12 8 10 46.20 5.40 10 -8 -10 16.50 3.70 -10 -8 10 11.50 2.60 -10 -8 10 13.40 2.90 -10 8 10 14.90 4.00 -10 8 10 17.20 4.10 8 -8 -10 7.30 2.80 -8 -8 10 8.80 2.50 -8 -8 10 8.20 2.60 -8 8 10 5.00 3.10 8 8 -10 6.10 2.40 -8 8 10 7.20 3.20 -6 -8 10 83.89 6.10 -6 -8 10 86.79 5.10 6 -8 -10 84.69 6.20 -6 -8 10 86.79 5.00 -6 8 10 82.19 6.20 6 8 -10 85.19 5.80 6 8 -10 87.19 5.70 -6 8 10 72.89 6.80 -4 -8 10 8.90 2.60 4 -8 -10 10.30 3.00 -4 -8 10 6.00 2.70 -4 8 10 9.80 2.60 -4 8 10 1.00 2.80 4 8 -10 8.30 2.60 4 8 -10 9.80 2.30 2 -8 -10 9.80 2.90 -2 -8 10 7.30 2.60 -2 -8 10 8.40 3.20 2 8 -10 13.70 3.10 -2 8 10 9.70 3.50 0 -8 10 44.10 5.50 0 -8 -10 37.60 4.70 0 8 10 32.30 5.10 0 8 -10 45.20 5.40 0 8 -10 50.89 5.40 -2 -8 -10 2.90 2.40 2 -8 10 2.70 2.60 -2 8 -10 1.60 2.40 2 8 10 3.90 2.80 -2 8 -10 3.90 2.50 -4 -8 -10 24.80 4.20 4 -8 10 14.40 4.30 4 8 10 22.60 4.50 -4 8 -10 18.90 4.10 6 -8 10 18.50 4.80 6 8 10 11.70 4.20 -6 8 -10 14.90 4.30 -15 -9 10 29.30 4.60 15 -9 -10 31.50 5.20 -15 9 10 25.50 5.60 -15 9 10 27.00 5.00 -13 -9 10 35.80 4.50 13 -9 -10 35.10 5.20 -13 9 10 26.90 5.30 -13 9 10 38.20 6.00 -13 9 10 37.40 5.30 11 -9 -10 2.30 2.40 -11 -9 10 -0.90 2.20 -11 9 10 7.60 3.40 -11 9 10 6.50 3.60 -9 -9 10 59.89 5.00 -9 -9 10 60.99 5.00 9 -9 -10 54.19 5.80 -9 9 10 70.89 6.60 -9 9 10 79.49 7.20 -7 -9 10 70.49 5.50 -7 -9 10 82.09 6.00 7 -9 -10 87.19 6.30 -7 -9 10 90.79 5.50 -7 9 10 82.29 7.20 -7 9 10 86.29 6.70 7 9 -10 75.29 5.50 -5 -9 10 0.10 1.60 -5 -9 10 2.70 2.40 -5 -9 10 0.90 1.70 5 -9 -10 1.00 2.20 -5 9 10 0.70 2.80 5 9 -10 1.80 2.10 -5 9 10 1.30 2.20 5 9 -10 0.50 1.90 3 -9 -10 111.39 6.90 -3 -9 10 98.09 6.30 -3 9 10 112.59 7.90 3 9 -10 90.29 6.20 1 -9 -10 98.39 6.60 -1 -9 10 82.59 6.20 1 9 -10 99.79 6.70 1 9 -10 83.49 6.30 -1 9 10 90.49 7.30 1 -9 10 0.80 2.20 -1 -9 -10 1.20 2.20 1 9 10 -0.50 2.60 -1 9 -10 0.20 2.40 -1 9 -10 -1.00 2.30 3 -9 10 78.39 7.20 -3 -9 -10 89.69 6.50 -3 9 -10 79.09 6.80 3 9 10 73.49 6.70 5 -9 10 43.20 6.30 -5 9 -10 43.00 5.90 -16 -10 10 7.10 3.50 16 -10 -10 10.30 3.80 -16 10 10 10.30 4.40 -16 10 10 1.70 3.60 -14 -10 10 22.20 4.10 14 -10 -10 25.20 4.40 -14 10 10 17.40 4.70 -14 10 10 17.90 4.80 12 -10 -10 328.67 13.20 -12 -10 10 326.27 12.10 -12 10 10 333.07 14.20 -12 10 10 307.97 13.90 10 -10 -10 41.10 5.40 -10 -10 10 37.00 4.40 -10 10 10 47.20 6.20 -10 10 10 54.19 6.70 -8 -10 10 38.40 4.20 8 -10 -10 31.90 4.70 8 10 -10 43.90 4.80 -8 10 10 32.10 4.80 -8 10 10 28.90 5.10 -6 -10 10 620.14 16.60 -6 -10 10 605.44 16.80 6 -10 -10 583.84 18.50 -6 10 10 557.64 19.50 -6 10 10 584.34 18.20 6 10 -10 608.14 17.80 -4 -10 10 81.29 5.50 4 -10 -10 84.89 6.40 -4 10 10 95.09 6.00 4 10 -10 84.39 6.10 -4 10 10 84.29 7.30 -2 -10 10 22.70 3.80 2 -10 -10 27.10 4.30 -2 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-0.60 1.80 -6 -8 12 -0.80 2.30 6 -8 -12 1.50 2.30 -6 8 12 -0.50 2.70 6 8 -12 0.00 2.20 -6 8 12 2.60 2.50 4 -8 -12 54.29 5.90 -4 -8 12 59.59 5.50 -4 -8 12 67.29 7.30 -4 8 12 56.29 6.60 4 8 -12 68.09 6.30 -2 -8 12 3.70 2.60 2 -8 -12 4.50 2.80 -2 8 12 9.00 3.50 2 8 -12 0.60 2.40 0 -8 12 -0.60 2.50 0 -8 -12 2.60 2.70 0 8 -12 2.70 2.70 0 8 12 1.20 3.00 13 -9 -12 -1.20 2.30 -13 9 12 1.30 3.10 -13 9 12 -4.20 3.20 13 9 -12 -2.40 2.40 11 -9 -12 44.60 6.20 -11 9 12 32.60 5.50 -11 9 12 33.20 5.70 11 9 -12 35.70 5.90 11 9 -12 33.10 4.70 9 -9 -12 21.20 4.50 -9 -9 12 16.50 3.80 9 9 -12 24.50 4.40 -9 9 12 19.70 4.30 -9 9 12 21.40 4.90 9 9 -12 20.00 3.70 -7 -9 12 9.90 3.40 7 -9 -12 16.90 4.00 -7 9 12 18.90 4.00 -7 9 12 13.50 4.50 7 9 -12 15.30 3.50 5 -9 -12 69.49 6.40 -5 -9 12 56.09 5.20 -5 9 12 73.19 8.00 5 9 -12 71.09 6.00 -3 -9 12 11.50 3.20 3 -9 -12 15.50 3.80 -3 9 12 13.00 4.10 3 9 -12 8.80 3.20 -1 -9 12 18.70 4.20 1 -9 -12 16.70 3.90 1 9 -12 15.10 3.70 -1 9 12 28.10 5.30 -1 -9 -12 71.09 6.70 1 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-5 11 12 8.90 3.80 3 -11 -12 17.30 4.10 -3 -11 12 7.20 3.00 3 11 -12 7.10 3.20 -3 11 12 6.50 3.50 -1 -11 12 10.70 3.80 1 -11 -12 15.30 3.90 1 11 -12 10.70 3.80 -1 11 12 13.80 4.10 10 -12 -12 0.80 2.80 -10 -12 12 4.20 2.80 -10 12 12 8.00 3.60 -10 12 12 3.20 3.80 10 12 -12 8.90 3.40 -8 -12 12 1.20 2.30 8 -12 -12 -0.40 2.60 8 12 -12 2.00 2.70 -8 12 12 1.80 3.60 -8 12 12 -0.60 4.40 6 -12 -12 87.79 7.40 6 12 -12 84.29 7.00 -6 12 12 88.39 8.50 -4 -12 12 -0.70 2.10 4 -12 -12 6.00 3.10 -4 12 12 0.10 3.20 4 12 -12 -0.50 2.70 2 -12 -12 9.80 3.50 -2 -12 12 2.70 2.50 2 12 -12 4.00 3.10 -2 12 12 5.70 3.50 9 -13 -12 42.20 5.90 -9 -13 12 33.60 4.60 -9 13 12 49.80 7.20 -9 13 12 43.60 5.70 9 13 -12 56.39 6.20 7 -13 -12 224.48 11.60 -7 13 12 246.28 13.00 7 13 -12 226.08 11.10 5 -13 -12 14.80 3.80 5 13 -12 10.80 3.80 -5 13 12 19.50 5.20 14 0 -13 3.90 3.30 -14 0 13 1.60 3.70 -14 0 13 7.40 3.30 -12 0 13 1.10 2.90 12 0 -13 5.70 3.30 -12 0 13 -2.10 2.80 10 0 -13 0.70 2.30 -10 0 13 2.00 2.80 -10 0 13 2.80 3.00 8 0 -13 5.60 2.70 -8 0 13 -0.90 2.70 -8 0 13 3.60 2.50 -8 0 13 0.80 2.90 6 0 -13 2.30 2.10 -6 0 13 3.20 2.50 -6 0 13 0.70 2.70 4 0 -13 -0.20 1.90 -4 0 13 0.80 2.30 -4 0 13 -3.70 2.60 -2 0 13 2.70 3.20 -2 0 13 1.80 2.90 0 0 13 1.20 3.30 0 0 13 -3.70 2.30 -15 -1 13 52.89 6.70 15 -1 -13 69.29 7.90 15 1 -13 68.29 7.80 -15 1 13 66.19 7.80 -13 -1 13 16.60 4.80 -13 -1 13 18.90 4.40 13 -1 -13 18.10 4.30 -13 1 13 21.40 4.50 -13 1 13 17.40 4.50 13 1 -13 22.60 4.70 -11 -1 13 79.09 7.30 -11 -1 13 89.69 7.70 11 -1 -13 94.29 7.40 -11 1 13 104.19 8.20 -11 1 13 92.49 7.80 11 1 -13 86.99 7.30 9 -1 -13 109.59 7.60 -9 -1 13 92.29 8.10 -9 -1 13 100.99 7.70 -9 1 13 111.49 8.30 9 1 -13 109.39 7.40 -9 1 13 104.49 8.00 -7 -1 13 17.20 4.10 7 -1 -13 13.90 3.60 -7 -1 13 11.90 3.20 -7 1 13 19.70 4.30 -7 1 13 11.10 3.30 7 1 -13 14.00 3.10 -7 1 13 18.60 4.40 5 -1 -13 55.79 5.30 -5 -1 13 55.69 7.10 -5 -1 13 57.19 6.30 5 1 -13 56.59 5.80 -5 1 13 52.99 6.70 -5 1 13 69.79 7.20 -3 -1 13 95.49 7.50 -3 -1 13 101.09 8.40 3 -1 -13 90.39 6.90 -3 1 13 94.59 7.60 -3 1 13 82.39 7.90 -1 -1 13 5.30 3.60 -1 -1 13 5.90 3.20 -1 1 13 2.70 3.10 -1 1 13 2.30 3.10 1 -1 13 18.00 4.50 1 1 13 25.10 5.10 -14 -2 13 216.88 11.70 14 -2 -13 218.48 11.50 -14 2 13 196.78 10.60 -14 2 13 195.78 11.40 14 2 -13 204.78 11.20 -12 -2 13 91.89 7.20 12 -2 -13 96.09 7.60 -12 -2 13 97.69 8.20 -12 2 13 100.39 8.20 -12 2 13 97.69 7.80 12 2 -13 104.49 7.90 -10 -2 13 3.90 3.00 10 -2 -13 11.30 3.40 -10 -2 13 7.50 3.80 -10 2 13 8.60 3.50 10 2 -13 14.90 3.70 -10 2 13 9.90 3.80 8 -2 -13 339.37 13.50 -8 -2 13 345.37 14.30 -8 -2 13 360.46 12.70 8 2 -13 343.27 13.10 -8 2 13 316.07 14.10 -8 2 13 328.57 13.70 6 -2 -13 117.69 7.30 -6 -2 13 128.29 7.90 -6 -2 13 124.89 8.80 -6 2 13 139.99 9.20 6 2 -13 120.19 7.30 -6 2 13 128.89 8.10 -4 -2 13 5.60 2.90 4 -2 -13 7.10 2.70 -4 -2 13 -1.10 2.70 -4 2 13 6.40 3.00 -4 2 13 -3.40 2.60 -2 -2 13 261.57 13.30 -2 -2 13 270.17 12.60 -2 2 13 271.47 12.70 -2 2 13 235.18 12.80 0 -2 13 75.69 8.50 0 -2 13 73.59 8.30 0 2 13 68.79 8.20 0 2 13 68.79 8.20 -15 -3 13 8.50 3.80 15 -3 -13 10.80 3.80 15 3 -13 2.40 3.00 -15 3 13 6.80 3.90 -13 -3 13 1.60 3.40 13 -3 -13 3.30 3.00 -13 -3 13 -2.50 2.70 -13 3 13 4.00 3.30 13 3 -13 2.40 2.90 -13 3 13 1.00 3.50 -11 -3 13 40.70 5.70 -11 -3 13 26.50 5.40 11 -3 -13 32.70 5.30 -11 3 13 39.70 6.10 11 3 -13 46.40 5.90 -11 3 13 38.80 5.80 9 -3 -13 16.40 3.90 -9 -3 13 17.10 4.30 9 3 -13 25.30 4.40 -9 3 13 27.00 4.80 -9 3 13 22.90 4.90 -7 -3 13 4.00 2.40 -7 -3 13 5.70 3.30 7 -3 -13 5.30 2.70 -7 3 13 7.60 3.50 7 3 -13 3.60 2.30 -7 3 13 4.80 3.00 5 -3 -13 9.20 3.20 -5 -3 13 15.90 4.30 -5 -3 13 14.80 3.60 -5 3 13 8.30 3.70 -3 -3 13 12.20 4.10 -3 -3 13 20.60 4.10 3 -3 -13 14.50 3.50 -3 3 13 12.70 4.10 -1 -3 13 8.60 3.60 -1 -3 13 6.50 4.10 -1 3 13 14.70 4.20 -1 3 13 11.10 4.10 -14 -4 13 67.69 7.60 14 -4 -13 75.59 8.10 -14 4 13 71.09 7.30 14 4 -13 77.89 8.40 -14 4 13 77.89 8.40 12 -4 -13 4.10 2.90 -12 -4 13 5.10 3.60 -12 -4 13 6.40 2.90 -12 4 13 7.50 3.80 -12 4 13 5.60 3.40 12 4 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20.30 -5 -5 13 690.43 22.40 -5 5 13 676.23 22.60 -3 -5 13 96.89 7.40 -3 -5 13 92.39 8.40 3 -5 -13 90.69 6.70 -3 5 13 90.59 8.00 -1 -5 13 12.20 3.70 -1 -5 13 7.30 3.60 1 5 -13 14.80 4.00 -1 5 13 15.80 4.70 14 -6 -13 64.39 7.40 14 6 -13 76.99 8.30 12 -6 -13 11.00 4.00 -12 6 13 9.00 3.90 -12 6 13 7.20 3.80 12 6 -13 4.90 3.20 10 -6 -13 16.30 4.00 -10 -6 13 26.00 4.50 -10 6 13 18.20 4.50 10 6 -13 38.10 5.30 -10 6 13 26.30 5.00 8 -6 -13 29.20 5.10 -8 -6 13 29.10 4.90 8 6 -13 40.40 5.10 -8 6 13 30.60 5.10 -8 6 13 28.10 5.10 -6 -6 13 5.20 3.10 6 -6 -13 8.10 3.40 -6 -6 13 8.50 2.70 -6 6 13 4.00 2.60 -6 6 13 11.50 4.10 4 -6 -13 2.30 2.50 -4 -6 13 -0.40 2.70 -4 -6 13 3.80 2.50 -4 6 13 1.60 3.00 4 6 -13 -2.10 2.20 2 -6 -13 -0.30 2.40 -2 -6 13 3.00 2.70 -2 -6 13 0.10 2.60 2 6 -13 -0.60 2.50 -2 6 13 -5.30 2.70 13 -7 -13 28.90 5.40 13 7 -13 25.50 5.10 -13 7 13 35.90 6.00 -13 7 13 28.80 5.50 -11 -7 13 43.70 5.50 11 -7 -13 57.79 6.70 -11 7 13 58.89 7.10 11 7 -13 49.99 6.30 -11 7 13 50.69 6.80 9 -7 -13 48.40 6.30 -9 -7 13 32.50 5.20 -9 7 13 41.50 5.70 -9 7 13 36.60 5.80 9 7 -13 54.19 6.00 -7 -7 13 13.70 3.90 7 -7 -13 10.60 3.30 -7 7 13 19.60 4.20 7 7 -13 8.60 2.90 -7 7 13 10.00 3.90 -5 -7 13 13.10 4.00 5 -7 -13 14.70 3.90 -5 -7 13 8.90 3.10 5 7 -13 7.20 3.20 -5 7 13 9.50 3.90 -3 -7 13 63.29 7.30 3 -7 -13 65.89 6.80 -3 -7 13 75.09 7.60 3 7 -13 72.49 6.70 -3 7 13 72.49 8.00 -1 -7 13 0.60 2.70 1 -7 -13 -1.90 2.40 1 7 -13 -0.60 2.50 12 -8 -13 99.99 8.00 -12 8 13 116.09 9.00 12 8 -13 111.29 8.60 -12 8 13 103.79 8.50 10 -8 -13 62.79 7.00 -10 -8 13 62.69 6.10 10 8 -13 69.39 6.60 10 8 -13 52.19 7.50 -10 8 13 76.79 8.30 -10 8 13 57.79 6.60 -8 -8 13 403.26 15.30 8 -8 -13 398.96 15.40 -8 8 13 404.46 15.10 8 8 -13 393.16 13.80 -8 8 13 387.56 16.50 6 -8 -13 161.78 9.20 -6 -8 13 147.19 9.20 -6 8 13 131.39 9.60 6 8 -13 145.99 8.20 4 -8 -13 22.10 4.20 -4 -8 13 16.40 3.80 -4 8 13 25.00 5.30 4 8 -13 20.20 4.00 2 -8 -13 435.26 15.90 -2 -8 13 460.75 16.70 -2 8 13 434.46 17.40 2 8 -13 440.36 15.20 11 -9 -13 20.10 4.40 -11 9 13 24.10 5.00 11 9 -13 25.80 4.30 -11 9 13 14.70 4.40 11 9 -13 23.10 4.70 9 -9 -13 12.30 3.40 9 9 -13 5.40 3.00 9 9 -13 12.70 4.50 -9 9 13 7.40 3.80 -9 9 13 8.20 3.50 7 -9 -13 32.90 5.10 7 9 -13 30.50 4.40 -7 9 13 38.20 6.60 5 -9 -13 3.00 2.80 -5 -9 13 1.10 2.40 -5 9 13 -2.50 2.80 5 9 -13 -0.60 2.60 3 -9 -13 5.00 3.10 -3 -9 13 1.40 2.60 -3 9 13 6.40 3.60 3 9 -13 2.80 3.00 10 -10 -13 31.40 5.20 -10 10 13 43.00 6.40 10 10 -13 31.60 5.00 10 10 -13 28.70 4.60 8 -10 -13 10.40 3.40 8 10 -13 7.30 3.10 -8 10 13 6.20 3.70 6 -10 -13 84.69 7.20 -6 10 13 95.39 8.80 6 10 -13 80.79 6.70 4 -10 -13 22.90 4.60 -4 -10 13 14.60 3.50 4 10 -13 15.60 3.90 7 -11 -13 10.80 3.60 -12 0 14 32.10 5.80 12 0 -14 34.70 5.70 -12 0 14 22.60 5.10 -10 0 14 6.50 3.80 10 0 -14 9.20 3.20 -10 0 14 1.80 3.30 8 0 -14 263.77 11.70 -8 0 14 256.37 12.80 -8 0 14 264.17 11.40 -6 0 14 4.40 3.00 -6 0 14 3.00 3.10 6 0 -14 -0.60 2.20 -4 0 14 0.60 3.00 -4 0 14 -1.60 2.50 -11 -1 14 45.00 6.50 11 -1 -14 54.39 6.70 -11 -1 14 53.49 6.60 11 1 -14 61.09 6.90 -11 1 14 54.79 6.90 -11 1 14 40.40 5.90 -9 -1 14 17.20 4.60 9 -1 -14 29.00 5.00 9 1 -14 24.40 4.70 -9 1 14 23.30 5.00 -9 1 14 18.40 5.70 -9 1 14 24.40 5.30 -7 -1 14 23.20 4.50 -7 -1 14 25.40 5.00 7 -1 -14 30.80 4.80 7 1 -14 29.10 4.50 -7 1 14 33.60 5.80 -7 1 14 29.50 4.70 -5 -1 14 20.90 4.70 5 -1 -14 34.20 4.50 -5 -1 14 25.20 4.90 -5 1 14 22.60 4.90 -5 1 14 27.10 4.60 -3 -1 14 8.60 3.60 -3 -1 14 7.80 3.70 -3 1 14 12.60 4.30 -3 1 14 6.30 3.50 -12 -2 14 63.59 7.50 -12 -2 14 70.29 7.20 12 -2 -14 76.79 7.30 -12 2 14 76.59 7.90 12 2 -14 78.69 7.30 -12 2 14 84.99 7.80 10 -2 -14 53.49 6.80 -10 -2 14 43.50 6.10 10 2 -14 46.50 5.70 -10 2 14 44.50 5.90 -10 2 14 41.70 6.10 8 -2 -14 25.30 4.60 -8 -2 14 26.70 5.20 -8 2 14 31.80 5.20 8 2 -14 25.50 4.40 -8 2 14 29.30 5.60 -8 2 14 21.40 4.20 6 -2 -14 15.10 3.60 -6 -2 14 18.30 4.60 -6 -2 14 17.90 4.00 -6 2 14 15.80 4.20 -6 2 14 14.20 4.40 -4 -2 14 105.59 8.70 -4 -2 14 94.49 7.80 -4 2 14 91.69 7.60 -4 2 14 89.99 8.50 -11 -3 14 61.89 6.80 11 -3 -14 62.09 7.40 -11 3 14 56.19 7.00 -11 3 14 57.19 6.80 11 3 -14 54.99 6.50 9 -3 -14 4.00 2.80 -9 -3 14 5.30 3.20 -9 3 14 7.80 3.50 -9 3 14 7.70 3.50 9 3 -14 -0.50 2.40 -7 -3 14 3.20 3.20 7 -3 -14 3.10 2.60 -7 -3 14 1.60 2.60 7 3 -14 1.00 2.30 -7 3 14 2.20 3.00 -7 3 14 6.20 2.90 -5 -3 14 122.19 8.40 -5 -3 14 119.29 9.00 5 -3 -14 128.09 7.90 -5 3 14 124.59 9.40 -5 3 14 115.29 8.40 -3 -3 14 0.80 2.70 -3 3 14 2.20 2.90 12 -4 -14 29.40 5.20 12 4 -14 38.10 5.60 10 -4 -14 6.20 3.20 -10 -4 14 6.50 3.40 -10 4 14 4.40 3.20 -10 4 14 4.80 3.70 10 4 -14 4.30 2.70 -8 -4 14 69.69 7.50 8 -4 -14 63.09 6.80 -8 4 14 69.49 7.20 -8 4 14 67.59 7.80 8 4 -14 69.89 6.20 -6 -4 14 1.00 3.10 6 -4 -14 4.10 2.80 -6 -4 14 0.50 2.50 -6 4 14 1.00 2.90 -4 -4 14 7.80 3.30 -4 -4 14 12.70 4.00 4 -4 -14 7.40 3.10 -4 4 14 0.40 3.10 11 -5 -14 32.80 5.30 11 5 -14 30.70 5.10 -9 -5 14 4.10 3.10 9 -5 -14 6.50 3.10 -9 5 14 7.00 3.20 -9 5 14 8.30 3.70 9 5 -14 5.70 2.70 7 -5 -14 37.10 5.00 -7 -5 14 40.60 5.80 -7 5 14 52.29 7.10 -7 5 14 44.00 6.30 -5 -5 14 24.40 5.20 5 -5 -14 18.80 4.00 -5 -5 14 32.70 5.40 -5 5 14 19.40 4.80 10 -6 -14 -2.50 2.40 10 6 -14 5.70 3.10 8 -6 -14 0.70 2.40 -8 -6 14 1.30 3.10 -8 6 14 3.90 3.20 -8 6 14 3.80 3.40 6 -6 -14 6.40 3.20 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 89883 _shelx_res_file ; TITL monoC_a.res in C2/c monoC_a.res created by SHELXL-2016/6 at 09:51:20 on 10-Dec-2020 REM Old TITL monoC in C2/c REM SHELXT solution in C2/c REM R1 0.093, Rweak 0.003, Alpha 0.021, Orientation as input REM Formula found by SHELXT: Cd6 O14 Te3 CELL 0.71073 11.9074 14.3289 8.7169 90.000 113.629 90.000 ZERR 8.000 0.0003 0.0003 0.0002 0.000 0.001 0.000 LATT 7 SYMM -X, Y, 1/2-Z SFAC CD Te O UNIT 16 20 56 TEMP 23 SIZE 0.06 0.07 0.09 L.S. 10 LIST 6 acta FMAP 2 PLAN 20 WGHT 0.007000 7.023700 FVAR 0.08198 TE1 2 0.150626 0.028835 0.049510 11.00000 0.00891 0.00993 = 0.00892 -0.00049 0.00293 -0.00007 TE2 2 0.158579 0.339851 0.155820 11.00000 0.00967 0.01489 = 0.01080 0.00439 0.00397 0.00058 TE3 2 0.000000 0.762236 0.250000 10.50000 0.01272 0.00968 = 0.01572 0.00000 0.00719 0.00000 CD1 1 0.321861 0.146075 0.440681 11.00000 0.01052 0.01416 = 0.00843 -0.00161 0.00347 -0.00111 CD2 1 0.000000 0.154383 0.250000 10.50000 0.00833 0.01007 = 0.01683 0.00000 0.00370 0.00000 CD3 1 0.000000 0.527052 0.250000 10.50000 0.01015 0.01016 = 0.02670 0.00000 0.00435 0.00000 O1 3 0.018172 0.413290 0.072187 11.00000 0.01116 0.01506 = 0.02047 0.00002 0.00054 0.00152 O2 3 0.061796 0.082421 0.519403 11.00000 0.01735 0.01335 = 0.01680 0.00455 0.00837 0.00574 O3 3 0.070030 0.239077 0.011295 11.00000 0.02430 0.01484 = 0.00947 -0.00134 0.00296 -0.00624 O4 3 0.152882 0.267665 0.333973 11.00000 0.01415 0.01046 = 0.00848 0.00098 0.00430 -0.00140 O5 3 0.163807 0.058978 0.266163 11.00000 0.01119 0.01297 = 0.00970 -0.00274 0.00354 -0.00097 O6 3 0.195375 0.461662 0.366160 11.00000 0.00996 0.01634 = 0.01366 0.00176 0.00239 -0.00347 O7 3 0.381432 0.171775 0.231633 11.00000 0.01934 0.03014 = 0.01474 -0.00117 0.00698 -0.01317 HKLF 4 REM monoC_a.res in C2/c REM R1 = 0.0219 for 3084 Fo > 4sig(Fo) and 0.0264 for all 3373 data REM 106 parameters refined using 0 restraints END WGHT 0.0070 7.0246 REM Highest difference peak 1.099, deepest hole -1.525, 1-sigma level 0.249 Q1 1 0.0000 0.4821 0.2500 10.50000 0.05 1.10 Q2 1 0.1170 0.3109 0.1558 11.00000 0.05 1.06 Q3 1 0.2269 0.3823 0.1774 11.00000 0.05 1.04 Q4 1 0.3462 0.2129 0.2077 11.00000 0.05 1.02 Q5 1 0.0015 0.2413 -0.0824 11.00000 0.05 0.92 Q6 1 0.0631 0.1060 0.6012 11.00000 0.05 0.84 Q7 1 0.2872 0.0800 0.1991 11.00000 0.05 0.82 Q8 1 0.0487 -0.0059 -0.1654 11.00000 0.05 0.81 Q9 1 0.4553 0.1863 0.3171 11.00000 0.05 0.81 Q10 1 0.2509 0.4151 0.3382 11.00000 0.05 0.81 Q11 1 0.4283 0.1722 0.1010 11.00000 0.05 0.80 Q12 1 0.1434 0.0286 -0.0475 11.00000 0.05 0.79 Q13 1 0.0984 0.0687 -0.0301 11.00000 0.05 0.78 Q14 1 0.2668 0.3507 0.3338 11.00000 0.05 0.77 Q15 1 0.2359 0.0480 0.2970 11.00000 0.05 0.76 Q16 1 0.1042 0.3042 0.2577 11.00000 0.05 0.75 Q17 1 0.0248 0.2781 -0.0045 11.00000 0.05 0.75 Q18 1 0.4362 0.2267 0.5251 11.00000 0.05 0.75 Q19 1 0.0996 0.4720 0.1841 11.00000 0.05 0.74 Q20 1 0.1760 0.5090 0.3982 11.00000 0.05 0.74 ; _shelx_res_checksum 78741 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cd Cd1 0.32186(2) 0.14608(2) 0.44068(2) 0.01114(4) Uani d 1 . . Cd Cd2 0.000000 0.15438(2) 0.250000 0.01217(5) Uani d 1 . . Cd Cd3 0.000000 0.52705(2) 0.250000 0.01663(6) Uani d 1 . . Te Te1 0.15063(2) 0.02884(2) 0.04951(2) 0.00946(4) Uani d 1 . . Te Te2 0.15858(2) 0.33985(2) 0.15582(2) 0.01183(4) Uani d 1 . . Te Te3 0.000000 0.76224(2) 0.250000 0.01223(5) Uani d 1 . . O O1 0.0182(2) 0.41329(16) 0.0722(3) 0.0174(4) Uani d 1 . . O O2 0.0618(2) 0.08242(15) 0.5194(3) 0.0153(4) Uani d 1 . . O O3 0.0700(2) 0.23908(16) 0.0113(3) 0.0174(4) Uani d 1 . . O O4 0.15288(19) 0.26766(14) 0.3340(2) 0.0111(3) Uani d 1 . . O O5 0.16381(18) 0.05898(15) 0.2662(2) 0.0115(4) Uani d 1 . . O O6 0.19537(19) 0.46166(16) 0.3662(3) 0.0141(4) Uani d 1 . . O O7 0.3814(2) 0.17177(19) 0.2316(3) 0.0214(5) Uani d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Cd1 0.01052(8) 0.01416(9) 0.00843(8) -0.00111(7) 0.00347(6) -0.00161(6) Cd2 0.00833(11) 0.01007(12) 0.01683(13) 0.000 0.00370(10) 0.000 Cd3 0.01015(12) 0.01016(12) 0.02670(16) 0.000 0.00435(11) 0.000 Te1 0.00891(7) 0.00993(7) 0.00892(7) -0.00007(6) 0.00293(5) -0.00049(6) Te2 0.00967(7) 0.01489(8) 0.01080(7) 0.00058(6) 0.00397(6) 0.00439(6) Te3 0.01272(11) 0.00968(10) 0.01572(11) 0.000 0.00719(9) 0.000 O1 0.0112(9) 0.0151(10) 0.0205(10) 0.0015(8) 0.0005(8) 0.0000(8) O2 0.0174(10) 0.0133(9) 0.0168(10) 0.0057(8) 0.0084(8) 0.0045(8) O3 0.0243(11) 0.0148(10) 0.0095(9) -0.0062(9) 0.0030(8) -0.0013(8) O4 0.0142(9) 0.0105(8) 0.0085(8) -0.0014(7) 0.0043(7) 0.0010(7) O5 0.0112(8) 0.0130(9) 0.0097(8) -0.0010(7) 0.0035(7) -0.0027(7) O6 0.0100(8) 0.0163(10) 0.0137(9) -0.0035(7) 0.0024(7) 0.0018(8) O7 0.0193(11) 0.0301(13) 0.0147(10) -0.0132(10) 0.0070(9) -0.0012(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Cd Cd -0.8075 1.2024 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Te Te -0.5308 1.6751 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O7 Cd1 O5 . . 89.60(8) ? O4 Cd1 O5 7_556 . 132.70(7) ? O7 Cd1 O1 . 8_556 82.92(9) ? O4 Cd1 O1 7_556 8_556 90.83(8) ? O5 Cd1 O1 . 8_556 122.23(8) ? O7 Cd1 O6 . 7_556 147.00(9) ? O4 Cd1 O6 7_556 7_556 75.74(7) ? O5 Cd1 O6 . 7_556 80.31(7) ? O1 Cd1 O6 8_556 7_556 76.40(8) ? O7 Cd1 O4 . . 92.99(8) ? O4 Cd1 O4 7_556 . 75.55(8) ? O5 Cd1 O4 . . 78.97(7) ? O1 Cd1 O4 8_556 . 158.20(7) ? O6 Cd1 O4 7_556 . 115.38(7) ? O4 Cd2 O4 2 . 91.55(10) ? O4 Cd2 O5 2 2 81.98(7) ? O4 Cd2 O5 . 2 162.69(7) ? O4 Cd2 O5 2 . 162.69(7) ? O4 Cd2 O5 . . 81.98(7) ? O5 Cd2 O5 2 . 108.48(10) ? O4 Cd2 O2 2 2 95.61(7) ? O4 Cd2 O2 . 2 120.19(7) ? O5 Cd2 O2 2 2 76.60(7) ? O5 Cd2 O2 . 2 74.25(7) ? O4 Cd2 O2 2 . 120.19(7) ? O4 Cd2 O2 . . 95.61(7) ? O5 Cd2 O2 2 . 74.24(7) ? O5 Cd2 O2 . . 76.60(7) ? O2 Cd2 O2 2 . 128.99(11) ? O1 Cd3 O1 2 . 90.65(12) ? O1 Cd3 O6 2 2 70.32(8) ? O1 Cd3 O6 . 2 76.77(8) ? O1 Cd3 O6 2 . 76.77(8) ? O1 Cd3 O6 . . 70.32(8) ? O6 Cd3 O6 2 . 132.57(11) ? O1 Cd3 O7 2 4 138.48(8) ? O1 Cd3 O7 . 4 115.36(8) ? O6 Cd3 O7 2 4 143.97(8) ? O6 Cd3 O7 . 4 82.22(8) ? O1 Cd3 O7 2 3_455 115.35(8) ? O1 Cd3 O7 . 3_455 138.48(8) ? O6 Cd3 O7 2 3_455 82.22(8) ? O6 Cd3 O7 . 3_455 143.97(8) ? O7 Cd3 O7 4 3_455 66.35(10) ? O2 Te1 O5 6 . 98.70(9) ? O2 Te1 O6 6 4_545 91.48(10) ? O5 Te1 O6 . 4_545 92.74(9) ? O2 Te1 O2 6 2 76.42(10) ? O5 Te1 O2 . 2 80.70(8) ? O6 Te1 O2 4_545 2 165.07(9) ? O1 Te2 O4 . . 108.01(10) ? O1 Te2 O3 . . 89.85(10) ? O4 Te2 O3 . . 86.37(9) ? O1 Te2 O6 . . 75.66(9) ? O4 Te2 O6 . . 80.14(8) ? O3 Te2 O6 . . 155.89(9) ? O7 Te3 O7 3_455 4 92.57(17) ? O7 Te3 O3 3_455 6_566 92.56(10) ? O7 Te3 O3 4 6_566 86.72(9) ? O7 Te3 O3 3_455 5_565 86.72(9) ? O7 Te3 O3 4 5_565 92.56(10) ? O3 Te3 O3 6_566 5_565 178.97(13) ? O7 Cd1 O4 . 7_556 130.55(8) ? Te2 O1 Cd1 . 8_455 123.87(11) ? Te2 O1 Cd3 . . 116.49(11) ? Cd1 O1 Cd3 8_455 . 104.08(9) ? Te1 O2 Cd2 6_556 . 115.99(10) ? Te1 O2 Te1 6_556 2 103.58(10) ? Cd2 O2 Te1 . 2 90.75(7) ? Te2 O3 Te3 . 5_565 126.44(11) ? Te2 O4 Cd1 . 7_556 112.50(10) ? Te2 O4 Cd2 . . 113.86(9) ? Cd1 O4 Cd2 7_556 . 118.33(9) ? Te2 O4 Cd1 . . 113.10(9) ? Cd1 O4 Cd1 7_556 . 104.45(8) ? Cd2 O4 Cd1 . . 92.39(7) ? Te1 O5 Cd1 . . 120.92(10) ? Te1 O5 Cd2 . . 109.97(9) ? Cd1 O5 Cd2 . . 99.61(8) ? Te1 O6 Cd3 4 . 126.44(11) ? Te1 O6 Cd1 4 7_556 113.29(9) ? Cd3 O6 Cd1 . 7_556 102.51(8) ? Te1 O6 Te2 4 . 119.89(10) ? Cd3 O6 Te2 . . 96.53(7) ? Cd1 O6 Te2 7_556 . 91.58(8) ? Te3 O7 Cd1 3_545 . 121.22(12) ? Te3 O7 Cd3 3_545 3_545 100.54(11) ? Cd1 O7 Cd3 . 3_545 99.69(10) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Cd1 O7 . 2.235(2) y Cd1 O4 7_556 2.237(2) y Cd1 O5 . 2.262(2) y Cd1 O1 8_556 2.314(2) y Cd1 O6 7_556 2.353(2) y Cd1 O4 . 2.539(2) y Cd2 O4 2 2.327(2) y Cd2 O4 . 2.327(2) y Cd2 O5 2 2.339(2) y Cd2 O5 . 2.339(2) y Cd2 O2 2 2.395(2) y Cd2 O2 . 2.395(2) y Cd2 O3 . 2.809(2) y Cd2 O3 2 2.809(2) y Cd3 O1 2 2.318(2) y Cd3 O1 . 2.318(2) y Cd3 O6 2 2.330(2) y Cd3 O6 . 2.330(2) y Cd3 O7 4 2.478(3) y Cd3 O7 3_455 2.478(3) y Cd3 O1 6_566 2.860(2) y Cd3 O1 5_565 2.860(2) y Te1 O2 6 1.873(2) y Te1 O5 . 1.882(2) y Te1 O6 4_545 1.936(2) y Te1 O2 2 2.476(2) y Te2 O1 . 1.859(2) y Te2 O4 . 1.890(2) y Te2 O3 . 1.928(2) y Te2 O6 . 2.441(2) y Te3 O7 3_455 1.876(2) y Te3 O7 4 1.876(2) y Te3 O3 6_566 2.088(2) y Te3 O3 5_565 2.088(2) y