#------------------------------------------------------------------------------ #$Date: 2024-12-07 18:11:30 +0100 (Sat, 07 Dec 2024) $ #$Revision: 296781 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/32/2023291.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023291 loop_ _publ_author_name 'Vashchenko, Oleksandr V.' 'Khomenko, Dmytro M.' 'Dyakonenko, Viktoriya V.' 'Lampeka, Rostyslav D.' _publ_section_title ; Synthesis, structures and Hirshfeld surface analyses of 2-hydroxy-N′-methylacetohydrazide and 2-hydroxy-N-methylacetohydrazide ; _journal_coeditor_code YZ2059 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E Crystallographic Communications' _journal_page_first 1170 _journal_page_last 1174 _journal_paper_doi 10.1107/S2056989024009526 _journal_volume 80 _journal_year 2024 _chemical_formula_iupac 'C3 H8 N2 O2' _chemical_formula_moiety 'C3 H8 N2 O2' _chemical_formula_sum 'C3 H8 N2 O2' _chemical_formula_weight 104.11 _chemical_name_systematic ; 2-Hydroxy-N'-methylacetohydrazide ; _space_group_crystal_system orthorhombic _space_group_IT_number 61 _space_group_name_Hall '-P 2ac 2ab' _space_group_name_H-M_alt 'P b c a' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary iterative _audit_creation_method ; Olex2 1.5 (compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 9.4484(8) _cell_length_b 7.0977(7) _cell_length_c 15.3781(14) _cell_measurement_reflns_used 3322 _cell_measurement_temperature 296.15 _cell_measurement_theta_max 29.77 _cell_measurement_theta_min 2.65 _cell_volume 1031.28(16) _computing_cell_refinement ; SAINT (Bruker, 2008) ; _computing_data_collection ; APEX2 (Bruker, 2008) ; _computing_data_reduction ; SAINT (Bruker, 2008) ; _computing_molecular_graphics ; Olex2 1.5 (Dolomanov et al., 2009) ; _computing_publication_material ; Olex2 1.5 (Dolomanov et al., 2009) ; _computing_structure_refinement ; SHELXL2019/3 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2018/2 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 296.15 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'Bruker APEXII CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0716 _diffrn_reflns_av_unetI/netI 0.0374 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 8 _diffrn_reflns_limit_k_min -8 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 10003 _diffrn_reflns_theta_full 24.997 _diffrn_reflns_theta_max 24.997 _diffrn_reflns_theta_min 2.649 _diffrn_source_current 35.0 _diffrn_source_power 1.75 _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.111 _exptl_absorpt_correction_T_max 0.7460 _exptl_absorpt_correction_T_min 0.6017 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.341 _exptl_crystal_description block _exptl_crystal_F_000 448 _exptl_crystal_size_max 0.3 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.1 _refine_diff_density_max 0.319 _refine_diff_density_min -0.346 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.339 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 77 _refine_ls_number_reflns 909 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.339 _refine_ls_R_factor_all 0.1091 _refine_ls_R_factor_gt 0.1028 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0435P)^2^+3.1357P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1957 _refine_ls_wR_factor_ref 0.1985 _reflns_number_gt 841 _reflns_number_total 909 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file yz2059.cif _cod_data_source_block 1 _cod_depositor_comments 'Adding full bibliography for 2023291--2023292.cif.' _cod_database_code 2023291 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.967 _shelx_estimated_absorpt_t_max 0.989 _shelx_hkl_file ; 0 -1 0 -10.00 0.90 0 -1 0 -10.20 1.20 0 -1 0 -9.00 1.70 0 1 0 -10.70 1.00 0 1 0 -7.40 1.80 0 1 0 -10.30 1.20 0 1 0 -9.50 0.90 0 -2 0 8510.75 234.68 0 -2 0 9999.00 253.77 0 -2 0 8488.85 293.97 0 -3 0 0.20 2.80 0 -3 0 2.10 2.60 0 -3 0 -1.20 2.20 0 -3 0 0.70 1.90 0 3 0 -0.90 1.90 0 3 0 -0.50 1.20 0 3 0 1.50 2.00 0 -4 0 130.29 7.10 0 -4 0 124.39 8.40 0 -4 0 128.39 10.50 0 -4 0 120.89 11.40 0 4 0 122.69 7.80 0 4 0 124.99 6.40 0 4 0 130.69 8.10 0 -5 0 2.10 4.80 0 -5 0 0.90 2.80 0 -5 0 -1.30 3.80 0 -5 0 -0.10 3.70 0 5 0 1.30 3.20 0 5 0 2.00 1.80 0 -6 0 3.20 6.80 0 -6 0 5.50 5.20 0 6 0 6.60 2.50 0 6 0 5.50 4.50 0 -7 0 -2.00 4.40 0 -7 0 4.20 7.30 0 7 0 7.30 4.30 0 -8 0 23.60 8.90 0 -8 0 28.00 13.20 0 8 0 27.70 7.30 0 -9 0 8.30 8.80 0 -9 0 3.20 6.30 1 -9 0 4.40 9.00 1 -9 0 -0.70 5.60 -1 8 0 8.70 4.80 1 -8 0 1.60 8.20 1 -8 0 -0.20 5.40 -1 7 0 4.00 4.40 1 -7 0 -1.50 4.10 1 -7 0 2.50 6.60 1 -7 0 -2.90 5.10 -1 6 0 2.20 2.10 -1 6 0 2.90 4.30 1 -6 0 6.90 6.60 1 -6 0 -0.90 4.40 1 -6 0 -3.50 4.80 -1 5 0 1.20 2.00 -1 5 0 -1.50 3.10 1 -5 0 0.60 3.90 1 -5 0 0.70 5.00 1 -5 0 -0.60 3.00 1 -5 0 1.00 4.00 -1 4 0 0.10 1.70 -1 4 0 -0.10 2.50 1 -4 0 0.60 2.40 1 -4 0 -2.10 3.60 1 -4 0 -0.20 2.80 1 -4 0 1.30 3.20 -1 3 0 0.50 2.00 -1 3 0 -1.20 1.70 -1 3 0 1.10 1.60 1 -3 0 -1.00 1.70 1 -3 0 2.20 2.50 1 -3 0 0.90 2.30 1 -3 0 -0.10 2.90 -1 2 0 -1.60 1.80 -1 2 0 0.90 1.80 -1 2 0 -1.00 1.30 1 -2 0 1.00 2.20 1 -2 0 -0.70 0.90 1 -2 0 -0.30 2.80 1 -2 0 0.30 2.00 1 -2 0 0.10 2.10 -1 1 0 0.20 1.00 -1 1 0 0.00 1.00 -1 1 0 -0.90 1.30 1 -1 0 0.30 1.50 1 -1 0 -0.40 1.00 1 -1 0 -0.80 0.80 1 -1 0 -0.30 1.00 1 -1 0 -0.60 1.00 -1 0 0 -0.40 0.60 -1 0 0 -0.50 0.30 1 0 0 -0.40 0.50 1 0 0 -0.70 0.40 1 0 0 -0.20 0.40 -1 -1 0 0.30 1.00 -1 -1 0 0.30 1.40 1 1 0 -0.10 0.90 1 1 0 -0.60 0.60 1 1 0 0.40 1.30 1 1 0 -0.60 0.70 -1 -2 0 -1.00 2.10 -1 -2 0 -2.30 1.10 -1 -2 0 1.80 2.70 1 2 0 0.20 1.70 1 2 0 -0.90 2.00 -1 -3 0 0.20 1.30 -1 -3 0 1.90 3.00 -1 -3 0 -0.10 2.20 1 3 0 1.00 1.50 1 3 0 -1.20 2.00 -1 -4 0 0.90 3.00 -1 -4 0 1.50 1.60 -1 -4 0 0.20 3.50 1 4 0 -1.20 1.50 1 4 0 -1.60 2.50 -1 -5 0 3.70 4.90 -1 -5 0 -1.50 3.40 -1 -5 0 2.80 1.90 1 5 0 -0.30 1.40 1 5 0 -2.00 3.00 -1 -6 0 2.20 5.80 -1 -6 0 -0.50 4.40 1 6 0 2.20 1.50 1 6 0 -2.40 3.80 -1 -7 0 4.20 7.40 -1 -7 0 0.70 4.70 1 7 0 4.10 4.30 -1 -8 0 11.50 9.10 -1 -8 0 2.40 5.70 1 8 0 10.00 4.90 -1 -9 0 12.30 8.80 -1 -9 0 1.30 5.80 2 -9 0 15.30 10.10 2 -9 0 -0.40 6.10 -2 8 0 23.40 6.10 2 -8 0 7.80 7.00 2 -8 0 13.40 9.40 2 -8 0 6.70 7.00 -2 7 0 5.80 4.20 -2 7 0 5.60 2.50 2 -7 0 0.00 4.60 2 -7 0 -2.10 5.40 2 -7 0 0.80 6.80 -2 6 0 54.89 5.70 -2 6 0 48.40 6.60 2 -6 0 59.99 11.50 2 -6 0 53.39 9.40 2 -6 0 55.79 10.80 -2 5 0 23.20 5.60 -2 5 0 24.90 5.20 2 -5 0 23.70 8.50 2 -5 0 24.60 6.30 2 -5 0 21.30 6.70 -2 4 0 456.55 17.60 -2 4 0 441.96 16.20 2 -4 0 453.05 21.50 2 -4 0 440.76 17.30 2 -4 0 452.05 18.20 2 -4 0 449.06 24.00 -2 3 0 70.29 6.00 -2 3 0 73.39 5.70 -2 3 0 71.99 5.30 2 -3 0 83.49 5.90 2 -3 0 76.99 7.40 2 -3 0 80.19 5.50 2 -3 0 74.39 8.10 2 -3 0 79.49 6.50 -2 2 0 118.49 6.90 -2 2 0 120.09 6.90 2 -2 0 128.59 8.10 2 -2 0 128.39 9.00 2 -2 0 127.59 7.20 2 -2 0 139.49 6.20 2 -2 0 129.59 7.20 -2 1 0 207.98 10.30 -2 1 0 214.08 9.10 2 -1 0 196.18 10.20 2 -1 0 201.48 8.50 2 -1 0 215.68 9.10 2 -1 0 206.78 9.10 -2 0 0 327.97 11.90 2 0 0 352.66 12.00 2 0 0 318.67 13.30 2 0 0 338.37 13.80 -2 -1 0 218.98 9.10 -2 -1 0 212.98 8.20 -2 -1 0 207.28 10.20 2 1 0 202.98 10.10 2 1 0 204.88 8.00 -2 -2 0 131.09 8.80 -2 -2 0 130.59 7.80 2 2 0 126.59 5.80 2 2 0 123.59 5.60 -2 -3 0 82.89 7.30 -2 -3 0 75.49 7.80 2 3 0 77.49 4.20 2 3 0 76.29 5.80 2 3 0 73.59 4.60 -2 -4 0 455.85 24.20 -2 -4 0 471.25 21.40 2 4 0 477.55 14.80 2 4 0 457.35 17.10 -2 -5 0 25.30 6.80 -2 -5 0 31.60 8.90 2 5 0 21.20 2.60 -2 -6 0 51.39 9.10 -2 -6 0 54.79 9.90 2 6 0 60.99 9.60 -2 -7 0 1.30 4.30 -2 -7 0 -1.20 6.10 2 7 0 6.60 4.60 -2 -8 0 2.40 5.50 -2 -8 0 25.80 11.90 2 8 0 7.30 5.60 -2 -9 0 1.00 5.50 -2 -9 0 11.50 10.00 3 -9 0 7.30 7.90 3 -9 0 -1.10 7.40 3 -9 0 3.40 7.10 3 -8 0 -1.70 6.00 3 -8 0 -0.20 7.60 3 -8 0 -0.10 5.70 -3 7 0 11.70 3.30 3 -7 0 1.40 5.70 3 -7 0 -0.60 5.10 3 -7 0 4.50 7.80 -3 6 0 4.40 2.80 3 -6 0 1.30 4.80 3 -6 0 1.80 4.70 3 -6 0 6.00 7.00 -3 5 0 0.30 2.40 3 -5 0 -2.80 5.10 3 -5 0 -1.60 3.70 3 -5 0 -1.40 4.10 -3 4 0 0.40 2.30 3 -4 0 -0.30 3.00 3 -4 0 -1.80 2.90 3 -4 0 0.60 4.10 -3 3 0 -0.40 1.80 3 -3 0 -1.10 2.40 3 -3 0 -0.10 3.50 3 -3 0 -0.40 2.40 3 -3 0 0.40 2.10 -3 2 0 -0.30 1.70 3 -2 0 0.70 2.10 3 -2 0 1.60 1.70 3 -2 0 1.10 1.90 3 -2 0 -1.10 1.80 3 -2 0 -1.40 2.50 -3 1 0 -1.90 1.50 3 -1 0 -0.40 1.50 3 -1 0 -0.40 2.20 3 -1 0 -0.30 1.60 -3 0 0 1.10 2.00 3 0 0 -1.00 1.90 3 0 0 -0.50 1.60 -3 -1 0 -0.30 1.90 -3 -1 0 -0.40 1.40 -3 -1 0 0.90 1.70 3 1 0 -0.40 1.30 -3 -2 0 1.10 2.20 -3 -2 0 0.70 1.70 3 2 0 0.20 1.40 3 2 0 -0.50 1.60 -3 -3 0 -0.50 2.10 -3 -3 0 2.60 3.10 3 3 0 1.00 1.20 3 3 0 0.10 1.90 -3 -4 0 -2.50 2.30 -3 -4 0 -1.00 3.10 3 4 0 2.80 2.50 3 4 0 0.50 2.80 3 4 0 3.00 1.30 -3 -5 0 1.40 3.70 -3 -5 0 -0.90 3.80 3 5 0 0.00 2.10 -3 -6 0 -4.40 4.10 -3 -6 0 1.90 4.20 -3 -7 0 7.00 7.60 -3 -7 0 0.90 4.30 3 7 0 1.50 4.30 -3 -8 0 2.30 7.40 -3 -8 0 0.30 4.40 3 8 0 8.30 4.80 -3 -9 0 3.40 5.90 -3 -9 0 26.10 8.90 4 -9 0 -4.70 8.20 4 -9 0 -3.10 6.10 4 -9 0 20.00 10.20 4 -8 0 -3.60 5.10 4 -8 0 -4.20 5.80 4 -8 0 0.60 7.10 4 -7 0 15.20 9.50 4 -7 0 13.40 6.90 4 -7 0 17.30 8.20 -4 6 0 9.70 3.70 4 -6 0 3.40 5.20 4 -6 0 8.80 8.20 4 -6 0 2.70 5.30 -4 5 0 36.20 5.60 4 -5 0 49.90 12.20 4 -5 0 25.40 7.50 4 -5 0 41.10 8.20 -4 4 0 7.20 3.30 4 -4 0 6.30 4.10 4 -4 0 7.00 5.40 4 -4 0 8.30 4.80 -4 3 0 22.60 5.30 4 -3 0 21.90 6.80 4 -3 0 25.10 4.60 4 -3 0 18.40 4.70 4 -3 0 18.10 5.10 -4 2 0 306.17 14.50 4 -2 0 290.87 13.50 4 -2 0 299.27 16.80 4 -2 0 307.77 15.10 -4 1 0 10.90 3.60 4 -1 0 14.70 4.70 4 -1 0 12.00 3.30 -4 0 0 1961.10 56.39 4 0 0 2004.90 56.39 4 0 0 1879.11 66.59 -4 -1 0 11.30 3.10 -4 -1 0 12.20 3.50 -4 -1 0 13.80 4.20 4 1 0 16.70 3.70 -4 -2 0 322.37 13.50 -4 -2 0 302.47 16.70 -4 -2 0 334.27 15.20 4 2 0 317.47 13.10 -4 -3 0 16.50 4.50 -4 -3 0 27.10 7.00 4 3 0 26.20 3.30 4 3 0 21.00 4.20 -4 -4 0 8.70 4.90 -4 -4 0 4.40 3.80 4 4 0 12.20 2.10 4 4 0 6.70 3.20 -4 -5 0 37.30 8.20 -4 -5 0 39.90 8.10 4 5 0 34.40 4.60 -4 -6 0 15.20 7.80 -4 -6 0 3.60 4.40 -4 -7 0 16.00 7.20 -4 -7 0 23.10 11.10 -4 -8 0 21.70 9.20 -4 -8 0 1.00 4.60 4 8 0 9.50 4.50 -4 -9 0 28.80 10.10 -4 -9 0 2.60 5.60 5 -9 0 2.60 7.70 5 -9 0 11.90 9.10 5 -8 0 -0.20 6.00 5 -8 0 7.30 7.40 5 -8 0 3.00 8.10 -5 7 0 5.10 3.80 5 -7 0 -3.80 5.70 5 -7 0 2.10 5.60 5 -7 0 8.10 8.00 -5 6 0 3.80 3.40 5 -6 0 -8.60 4.10 5 -6 0 -1.70 4.40 5 -6 0 2.30 6.30 -5 5 0 1.00 2.80 5 -5 0 -1.40 4.30 5 -5 0 1.30 4.50 5 -5 0 1.30 5.70 -5 4 0 -0.80 2.90 5 -4 0 -1.20 3.80 5 -4 0 -0.60 3.50 5 -4 0 3.50 5.70 -5 3 0 -0.40 2.40 5 -3 0 -2.00 2.70 5 -3 0 0.20 3.20 5 -3 0 -0.30 4.00 -5 2 0 1.30 2.70 5 -2 0 -0.40 2.40 5 -2 0 -1.40 3.10 5 -2 0 -1.80 2.40 -5 1 0 0.90 2.30 5 -1 0 -0.10 2.00 5 -1 0 -1.50 2.40 -5 0 0 -1.10 1.80 5 0 0 -0.80 2.30 -5 -1 0 0.20 1.90 -5 -1 0 3.30 2.60 -5 -1 0 -1.60 1.90 -5 -2 0 -0.20 2.30 -5 -2 0 -1.50 2.80 -5 -2 0 1.70 2.40 -5 -3 0 0.30 2.50 -5 -3 0 3.40 3.80 5 3 0 1.30 2.30 -5 -4 0 0.80 3.10 -5 -4 0 3.20 4.30 5 4 0 1.10 3.10 5 4 0 6.60 2.20 -5 -5 0 0.80 3.50 -5 -5 0 8.00 4.80 5 5 0 -0.90 3.20 -5 -6 0 13.50 6.90 -5 -6 0 -1.30 3.10 -5 -7 0 1.40 4.30 -5 -7 0 6.80 7.10 -5 -8 0 28.70 10.40 -5 -8 0 2.50 4.80 -5 -9 0 39.50 10.80 6 -8 0 19.60 10.70 6 -8 0 13.20 8.80 6 -8 0 8.50 8.00 -6 7 0 37.80 6.10 6 -7 0 21.10 8.80 6 -7 0 50.89 13.90 6 -7 0 24.70 8.90 -6 6 0 28.60 7.10 6 -6 0 13.10 7.30 6 -6 0 24.80 9.70 6 -6 0 9.00 6.40 -6 5 0 3.60 3.00 6 -5 0 -1.60 4.20 6 -5 0 8.30 6.00 6 -5 0 0.70 4.70 -6 4 0 74.99 8.70 6 -4 0 71.79 9.10 6 -4 0 78.39 10.30 6 -4 0 80.19 11.20 -6 3 0 129.29 10.90 6 -3 0 135.89 10.90 6 -3 0 129.49 11.90 6 -3 0 124.69 12.60 -6 2 0 54.59 7.20 6 -2 0 47.40 7.10 6 -2 0 49.30 7.90 6 -2 0 44.80 6.70 -6 1 0 181.38 12.30 6 -1 0 176.08 13.00 6 -1 0 171.48 11.80 -6 0 0 559.74 23.70 6 0 0 589.44 23.50 6 0 0 545.05 26.50 -6 -1 0 189.18 12.30 -6 -1 0 174.68 11.70 -6 -2 0 51.49 7.40 -6 -2 0 48.60 6.80 -6 -2 0 50.09 6.10 -6 -3 0 135.49 11.40 -6 -3 0 144.09 12.70 6 3 0 123.89 9.00 -6 -4 0 92.09 10.40 -6 -4 0 92.19 10.90 6 4 0 87.59 7.70 -6 -5 0 6.70 6.00 -6 -5 0 5.60 4.40 6 5 0 7.30 3.30 -6 -6 0 30.60 11.40 -6 -6 0 23.20 7.90 -6 -7 0 47.90 9.10 -6 -7 0 25.90 8.50 -6 -8 0 40.10 14.30 7 -8 0 -0.70 6.30 7 -8 0 11.40 8.30 -7 7 0 19.30 5.10 7 -7 0 13.70 8.50 7 -7 0 -1.80 5.60 7 -7 0 -5.00 6.80 -7 6 0 10.40 3.90 7 -6 0 2.80 7.00 7 -6 0 -6.20 4.50 7 -6 0 -0.30 5.30 -7 5 0 -0.10 3.40 7 -5 0 1.10 5.00 7 -5 0 2.50 6.50 7 -5 0 0.90 4.90 -7 4 0 -0.90 3.40 7 -4 0 1.40 4.10 7 -4 0 -0.40 4.10 7 -4 0 5.00 5.70 -7 3 0 2.70 3.40 7 -3 0 3.30 5.30 7 -3 0 0.80 4.00 7 -3 0 -0.40 3.60 -7 2 0 -1.50 2.70 7 -2 0 0.20 3.20 7 -2 0 0.20 4.40 7 -2 0 -0.60 3.50 -7 1 0 1.30 3.40 7 -1 0 1.50 3.40 7 -1 0 -1.50 2.50 -7 0 0 1.80 2.80 7 0 0 -0.50 2.60 7 0 0 3.00 3.90 -7 -1 0 3.70 3.70 7 1 0 1.00 4.10 -7 -2 0 0.60 3.20 -7 -2 0 0.10 2.40 -7 -2 0 3.50 4.30 -7 -3 0 1.30 3.10 -7 -3 0 -0.60 4.00 7 3 0 0.70 3.10 -7 -4 0 1.70 3.50 -7 -4 0 9.10 5.10 7 4 0 6.20 3.10 -7 -5 0 1.60 3.70 -7 -5 0 6.40 6.40 -7 -6 0 2.20 4.40 -7 -6 0 18.20 7.80 -7 -7 0 17.80 9.30 -7 -7 0 2.50 5.00 -7 -8 0 38.40 11.20 -8 7 0 33.10 7.70 8 -7 0 16.60 10.10 8 -7 0 13.10 8.50 8 -7 0 8.00 7.80 -8 6 0 13.20 4.60 8 -6 0 6.50 8.30 8 -6 0 2.00 6.10 8 -6 0 -2.20 5.20 -8 5 0 13.60 4.90 8 -5 0 5.60 5.90 8 -5 0 12.60 8.20 8 -5 0 8.60 6.10 -8 4 0 13.70 5.60 8 -4 0 9.50 5.80 8 -4 0 9.40 6.20 8 -4 0 18.80 8.30 -8 3 0 43.00 9.70 8 -3 0 32.60 7.80 8 -3 0 36.80 9.20 8 -3 0 37.40 10.20 -8 2 0 25.30 7.40 8 -2 0 27.20 7.30 8 -2 0 22.50 6.90 8 -2 0 38.10 10.00 -8 1 0 32.00 8.00 8 -1 0 19.40 6.00 8 -1 0 22.20 6.60 8 -1 0 26.80 8.40 -8 0 0 116.89 11.10 8 0 0 116.39 10.80 8 0 0 114.49 11.60 -8 -1 0 36.80 8.00 8 1 0 27.20 8.60 -8 -2 0 37.00 8.30 -8 -2 0 24.40 6.60 -8 -2 0 39.60 9.90 -8 -3 0 32.80 7.50 -8 -3 0 51.99 8.60 8 3 0 36.90 5.60 -8 -4 0 30.70 9.50 -8 -4 0 17.70 6.30 8 4 0 29.20 4.50 -8 -5 0 23.00 8.80 -8 -6 0 30.10 9.00 -8 -6 0 4.90 4.90 -8 -7 0 41.20 8.90 -8 -7 0 12.30 6.80 -9 7 0 14.90 5.10 9 -7 0 14.20 9.30 -9 6 0 14.60 5.70 9 -6 0 -2.90 5.40 9 -6 0 1.80 6.80 9 -6 0 2.10 6.10 -9 5 0 6.70 3.80 9 -5 0 4.30 5.30 9 -5 0 8.50 6.90 9 -5 0 -1.50 5.10 -9 4 0 4.00 4.90 9 -4 0 10.30 6.10 9 -4 0 -0.10 5.30 9 -4 0 -1.00 4.60 -9 3 0 4.40 3.70 9 -3 0 0.20 4.10 9 -3 0 8.40 5.90 9 -3 0 2.10 4.20 -9 2 0 1.70 3.50 9 -2 0 4.40 4.60 9 -2 0 -3.30 3.60 9 -2 0 0.90 4.10 -9 1 0 4.90 3.50 9 -1 0 2.40 4.50 9 -1 0 3.90 4.30 9 -1 0 -1.30 3.00 -9 0 0 6.00 4.10 9 0 0 1.10 3.40 9 0 0 2.70 4.30 -9 -1 0 1.70 4.20 9 1 0 5.90 4.70 9 1 0 1.30 3.30 -9 -2 0 10.00 4.70 9 2 0 2.60 4.40 -9 -3 0 12.10 7.20 9 3 0 13.80 4.40 -9 -4 0 18.80 8.60 9 4 0 26.80 4.10 -9 -5 0 22.10 8.60 -9 -5 0 2.00 4.00 -9 -7 0 52.59 9.40 -10 6 0 7.60 5.20 10 -6 0 -5.80 5.10 10 -6 0 16.00 8.70 -10 5 0 59.39 9.10 10 -5 0 58.19 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5.00 2 -5 3 40.30 8.60 -2 5 -3 38.70 4.60 -2 5 -3 36.50 5.30 2 -6 3 43.00 11.20 2 -6 3 37.90 7.60 2 -6 3 30.30 8.50 -2 6 -3 43.30 7.80 -2 6 -3 34.10 4.60 2 -7 3 0.40 4.80 2 -7 3 5.60 6.00 2 -7 3 12.70 7.90 -2 7 -3 8.40 4.70 2 -8 3 9.90 7.30 2 -8 3 19.30 9.80 2 -8 3 17.10 7.60 -2 8 -3 29.70 5.80 2 -9 3 10.30 8.50 2 -9 3 -0.80 6.10 -1 -9 -3 21.80 9.70 -1 -9 -3 0.80 5.40 1 8 3 34.70 8.70 -1 -8 -3 28.80 9.80 -1 -8 -3 51.89 15.30 1 7 3 15.50 6.10 -1 -7 -3 9.10 6.20 -1 -7 -3 8.00 8.50 1 6 3 113.99 8.50 1 6 3 107.49 9.40 -1 -6 -3 115.19 13.00 -1 -6 -3 127.39 14.50 1 5 3 88.69 8.00 1 5 3 93.99 7.40 -1 -5 -3 87.09 10.80 -1 -5 -3 111.89 7.90 -1 -5 -3 93.89 10.70 1 4 3 276.37 12.40 1 4 3 302.17 13.50 -1 -4 -3 290.47 13.00 -1 -4 -3 274.67 17.50 -1 -4 -3 283.97 16.50 1 3 3 189.68 9.90 1 3 3 176.68 8.40 1 3 3 184.18 10.20 -1 -3 -3 182.88 11.50 -1 -3 -3 176.98 12.10 1 2 3 223.18 10.60 1 2 3 234.78 8.50 -1 -2 -3 212.98 11.70 -1 -2 -3 234.48 11.60 -1 -2 -3 220.68 9.90 1 1 3 9.10 2.00 1 1 3 8.50 2.80 1 1 3 10.30 3.40 -1 -1 -3 8.60 2.80 -1 -1 -3 5.40 2.70 -1 -1 -3 3.30 2.10 1 0 3 -3.60 1.90 -1 0 -3 -2.40 1.30 -1 0 -3 -2.90 1.70 -1 0 -3 -2.30 0.90 1 -1 3 3.50 2.00 1 -1 3 6.90 2.20 1 -1 3 4.30 2.40 -1 1 -3 3.50 2.10 1 -2 3 228.78 10.80 1 -2 3 212.88 11.20 1 -2 3 221.28 8.80 1 -2 3 210.98 8.70 1 -3 3 192.68 8.10 1 -3 3 176.48 10.90 1 -3 3 187.18 12.10 -1 3 -3 177.58 8.10 1 -4 3 273.47 17.10 1 -4 3 295.77 11.00 1 -4 3 280.57 15.80 -1 4 -3 282.37 11.10 -1 4 -3 268.47 11.60 1 -5 3 101.39 11.20 1 -5 3 100.89 11.70 1 -5 3 108.59 6.20 -1 5 -3 90.09 7.40 -1 5 -3 91.79 5.90 1 -6 3 117.89 13.60 1 -6 3 113.09 12.70 -1 6 -3 117.69 9.30 1 -7 3 6.90 5.90 1 -7 3 -0.30 3.60 1 -7 3 9.50 7.40 -1 7 -3 9.60 5.30 1 -8 3 54.19 15.40 1 -8 3 26.40 9.50 -1 8 -3 48.20 9.30 1 -9 3 -5.40 4.60 1 -9 3 8.00 9.00 0 -9 -3 2.60 5.80 0 -9 -3 25.70 11.10 0 8 3 118.39 11.10 0 -8 -3 123.49 15.80 0 -8 -3 115.79 15.20 0 7 3 1.20 3.80 0 7 3 3.00 2.40 0 -7 -3 -0.10 6.50 0 -7 -3 -0.20 4.60 0 6 3 280.77 14.10 0 6 3 278.47 15.00 0 -6 -3 279.67 21.20 0 -6 -3 272.77 19.80 0 5 3 -0.80 2.90 0 5 3 0.90 2.90 0 -5 -3 5.70 5.60 0 -5 -3 -0.10 3.70 0 4 3 3.90 3.30 0 4 3 1.30 2.80 0 -4 -3 2.00 3.30 0 -4 -3 2.80 4.30 0 -4 -3 -0.30 2.60 0 3 3 0.00 2.40 0 3 3 -0.20 2.20 0 3 3 0.30 2.40 0 -3 -3 -1.70 2.20 0 -3 -3 0.00 2.70 0 -3 -3 -0.10 2.90 0 2 3 1900.21 44.90 0 2 3 1939.71 55.39 0 -2 -3 1988.30 55.49 0 -2 -3 1969.40 67.19 0 -2 -3 2088.49 58.29 0 -2 -3 2059.09 45.00 0 1 3 -1.40 1.70 0 1 3 2.70 2.70 0 1 3 -0.40 1.90 0 -1 -3 -0.90 1.50 0 -1 -3 2.10 2.40 0 -1 -3 -0.50 2.20 0 -1 -3 -0.70 1.40 0 0 3 -0.50 0.90 0 0 3 0.30 1.80 0 0 -3 -0.30 1.50 0 0 -3 -0.90 1.20 0 0 -3 -0.30 0.80 0 -1 3 0.00 1.00 0 -1 3 0.30 1.70 0 -1 3 -0.30 1.90 0 1 -3 -0.80 1.10 0 1 -3 2.60 1.30 0 1 -3 -0.20 1.60 0 -2 3 2011.50 56.79 0 -2 3 1971.70 48.60 0 -2 3 1975.00 67.09 0 -2 3 2049.70 52.49 0 -3 3 0.40 0.90 0 -3 3 2.50 3.20 0 -3 3 -0.40 1.10 0 -3 3 -0.20 1.70 0 -3 3 1.60 2.40 0 -4 3 2.70 3.30 0 -4 3 3.80 4.50 0 -4 3 1.10 2.70 0 -4 3 1.80 1.40 0 -4 3 3.10 1.40 0 4 -3 3.30 2.10 0 -5 3 1.60 4.80 0 -5 3 -1.60 1.70 0 -5 3 -1.20 3.40 0 -5 3 0.60 3.80 0 5 -3 3.50 2.40 0 -6 3 299.57 22.20 0 -6 3 289.87 15.20 0 -6 3 296.37 20.20 0 6 -3 275.47 14.50 0 -7 3 1.90 4.90 0 -7 3 1.40 6.10 0 7 -3 5.40 4.00 0 -8 3 111.39 15.00 0 -8 3 107.59 15.10 0 8 -3 116.09 10.70 0 -9 3 1.00 6.00 0 -9 3 19.90 9.00 1 -9 -3 -0.50 6.10 1 -9 -3 18.70 11.40 1 -8 -3 20.10 8.90 1 -8 -3 44.30 13.40 -1 7 3 16.90 5.70 -1 7 3 13.00 4.00 1 -7 -3 12.70 8.70 1 -7 -3 7.60 6.40 -1 6 3 124.69 9.50 -1 6 3 101.59 9.40 1 -6 -3 121.39 11.70 1 -6 -3 134.19 15.00 1 -6 -3 108.09 12.90 -1 5 3 88.39 7.90 -1 5 3 107.99 8.40 1 -5 -3 97.29 10.30 1 -5 -3 107.19 11.50 1 -5 -3 106.29 12.10 -1 4 3 278.47 13.50 -1 4 3 277.97 12.60 1 -4 -3 297.97 16.70 1 -4 -3 279.77 18.30 1 -4 -3 273.37 14.60 -1 3 3 184.98 10.10 1 -3 -3 186.78 11.50 1 -3 -3 192.78 8.80 1 -3 -3 180.08 12.90 1 -3 -3 190.48 10.30 1 -3 -3 181.58 10.60 -1 2 3 220.48 10.50 -1 2 3 231.28 10.30 1 -2 -3 233.18 10.80 1 -2 -3 238.68 10.70 1 -2 -3 232.38 8.80 1 -2 -3 220.28 12.90 1 -2 -3 225.88 11.10 -1 1 3 5.90 2.40 -1 1 3 7.90 3.00 1 -1 -3 8.90 3.20 1 -1 -3 5.60 2.10 1 -1 -3 8.30 2.90 1 -1 -3 3.90 3.10 -1 0 3 -0.90 1.50 -1 0 3 -2.30 1.70 -1 0 3 -1.50 0.90 1 0 -3 -1.10 1.70 1 0 -3 -2.60 0.70 1 0 -3 -0.60 2.10 1 0 -3 -0.40 1.60 1 0 -3 -2.20 1.90 -1 -1 3 6.00 1.50 -1 -1 3 6.40 2.90 -1 -1 3 8.30 2.30 1 1 -3 8.60 2.50 1 1 -3 5.60 1.40 -1 -2 3 224.78 12.50 -1 -2 3 229.58 7.10 -1 -2 3 224.18 9.70 1 2 -3 218.68 7.10 -1 -3 3 183.28 10.40 -1 -3 3 179.28 12.30 1 3 -3 185.88 7.00 -1 -4 3 283.37 18.20 -1 -4 3 300.97 15.90 1 4 -3 286.17 10.90 -1 -5 3 100.99 10.40 -1 -5 3 97.69 11.50 1 5 -3 109.99 7.10 -1 -6 3 121.59 13.90 -1 -6 3 106.59 12.20 -1 -7 3 7.70 6.10 -1 -7 3 13.20 8.10 1 7 -3 14.20 5.30 -1 -8 3 53.99 14.70 -1 -8 3 34.30 10.50 1 8 -3 40.40 9.20 -1 -9 3 0.80 5.90 -1 -9 3 5.10 8.40 2 -9 -3 1.60 6.30 2 -9 -3 9.60 10.40 2 -8 -3 4.80 6.80 2 -8 -3 16.10 11.50 -2 7 3 8.30 4.00 2 -7 -3 6.10 6.00 2 -7 -3 7.40 8.40 2 -7 -3 7.20 6.80 -2 6 3 30.20 5.30 2 -6 -3 42.80 9.30 2 -6 -3 29.70 8.50 2 -6 -3 42.10 12.90 -2 5 3 37.60 5.50 2 -5 -3 40.40 8.70 2 -5 -3 55.19 12.90 2 -5 -3 44.90 8.30 -2 4 3 48.60 5.90 2 -4 -3 46.80 7.40 2 -4 -3 49.30 8.30 2 -4 -3 52.89 7.30 -2 3 3 81.69 6.80 2 -3 -3 92.59 8.30 2 -3 -3 82.39 6.10 2 -3 -3 81.79 9.00 2 -3 -3 85.29 7.60 -2 2 3 652.43 22.80 -2 2 3 663.03 21.30 2 -2 -3 635.24 28.00 2 -2 -3 673.83 23.00 2 -2 -3 661.83 23.20 2 -2 -3 653.73 21.50 -2 1 3 3.60 2.10 -2 1 3 3.80 2.20 2 -1 -3 1.40 2.70 2 -1 -3 3.80 2.00 2 -1 -3 6.60 2.50 2 -1 -3 3.00 2.50 -2 0 3 22.50 1.90 -2 0 3 16.90 2.70 -2 0 3 27.90 3.60 2 0 -3 19.30 3.30 2 0 -3 19.70 2.10 2 0 -3 18.00 2.90 -2 -1 3 3.00 2.60 -2 -1 3 4.60 2.00 -2 -1 3 2.90 1.10 2 1 -3 4.40 1.30 2 1 -3 2.20 1.10 2 1 -3 3.60 2.00 -2 -2 3 650.93 27.80 -2 -2 3 700.83 21.60 -2 -2 3 644.04 19.10 2 2 -3 671.73 19.30 -2 -3 3 80.29 8.40 2 3 -3 80.39 4.20 -2 -4 3 48.60 8.00 -2 -4 3 51.89 7.10 2 4 -3 48.50 4.40 -2 -5 3 35.50 7.70 -2 -5 3 41.40 7.40 2 5 -3 40.30 5.00 -2 -6 3 33.90 8.40 -2 -6 3 42.70 11.90 -2 -7 3 4.10 5.10 -2 -7 3 6.80 7.50 -2 -8 3 13.30 7.40 -2 -8 3 25.30 10.50 2 8 -3 25.80 6.80 -2 -9 3 3.90 6.30 -2 -9 3 12.80 9.50 3 -9 -3 3.60 6.70 3 -9 -3 17.40 10.20 3 -8 -3 7.30 10.10 3 -8 -3 3.00 6.40 3 -8 -3 -3.10 6.50 -3 7 3 11.40 4.30 3 -7 -3 -5.90 5.60 3 -7 -3 3.80 5.80 3 -7 -3 12.00 9.30 -3 6 3 17.60 5.00 3 -6 -3 10.70 6.20 3 -6 -3 5.00 5.70 3 -6 -3 11.30 8.20 -3 5 3 14.00 4.90 3 -5 -3 12.10 6.00 3 -5 -3 14.20 6.10 3 -5 -3 11.70 8.00 -3 4 3 0.90 2.70 3 -4 -3 2.60 5.00 3 -4 -3 -2.10 3.10 3 -4 -3 0.70 3.60 -3 3 3 72.09 6.80 3 -3 -3 69.19 7.10 3 -3 -3 72.59 7.60 3 -3 -3 66.99 8.90 -3 2 3 50.59 5.50 3 -2 -3 55.19 6.00 3 -2 -3 51.39 7.20 3 -2 -3 53.29 5.80 -3 1 3 393.96 16.20 -3 1 3 419.66 14.80 3 -1 -3 413.26 16.50 3 -1 -3 417.16 15.20 3 -1 -3 394.76 19.80 3 -1 -3 403.56 14.80 -3 0 3 3.00 2.30 3 0 -3 1.90 1.80 3 0 -3 5.10 3.40 3 0 -3 3.00 1.50 3 0 -3 3.80 2.40 -3 -1 3 446.66 13.70 -3 -1 3 396.86 19.40 -3 -1 3 406.26 15.00 3 1 -3 400.36 13.20 3 1 -3 409.96 15.00 -3 -2 3 57.59 6.80 -3 -2 3 50.39 4.40 -3 -2 3 52.59 3.90 3 2 -3 54.19 4.10 -3 -3 3 65.69 8.10 -3 -3 3 72.99 6.40 -3 -3 3 71.69 4.00 3 3 -3 74.39 4.20 -3 -4 3 -0.20 2.60 -3 -4 3 -0.80 3.10 3 4 -3 0.30 2.10 -3 -5 3 11.80 5.20 -3 -5 3 17.40 7.70 3 5 -3 12.80 3.50 -3 -6 3 9.60 5.20 -3 -6 3 13.60 8.60 -3 -7 3 14.30 8.60 -3 -7 3 8.80 5.80 -3 -8 3 14.70 9.70 3 8 -3 16.20 5.90 -3 -9 3 4.30 6.20 -3 -9 3 26.90 11.90 4 -9 -3 8.40 10.60 4 -9 -3 6.80 7.40 4 -8 -3 7.20 7.30 4 -8 -3 8.70 8.50 4 -8 -3 27.60 12.60 -4 7 3 14.20 5.00 4 -7 -3 10.80 7.10 4 -7 -3 19.20 11.70 4 -7 -3 4.90 7.40 -4 6 3 20.10 6.00 4 -6 -3 21.90 10.50 4 -6 -3 16.00 7.40 4 -6 -3 14.00 6.90 -4 5 3 30.60 7.30 4 -5 -3 34.00 11.30 4 -5 -3 22.60 7.50 4 -5 -3 27.40 7.50 -4 4 3 2.00 3.10 4 -4 -3 -1.00 4.80 4 -4 -3 -0.30 3.80 4 -4 -3 1.20 3.90 -4 3 3 62.59 7.00 4 -3 -3 70.19 7.90 4 -3 -3 70.69 9.40 4 -3 -3 68.59 7.50 -4 2 3 83.19 7.50 4 -2 -3 91.19 7.70 4 -2 -3 90.79 9.60 4 -2 -3 92.39 7.80 -4 1 3 382.16 16.80 4 -1 -3 399.66 15.60 4 -1 -3 368.66 20.10 4 -1 -3 377.86 15.20 -4 0 3 0.10 2.00 4 0 -3 -0.80 1.80 4 0 -3 0.10 3.00 4 0 -3 -0.30 1.30 -4 -1 3 378.96 15.60 -4 -1 3 374.76 19.90 -4 -1 3 410.16 14.50 4 1 -3 401.86 15.80 -4 -2 3 92.29 6.20 -4 -2 3 104.89 6.90 -4 -2 3 94.49 9.40 4 2 -3 101.59 6.50 -4 -3 3 70.39 8.60 -4 -3 3 63.19 4.70 -4 -3 3 72.59 6.60 4 3 -3 77.09 5.10 -4 -4 3 6.70 4.50 -4 -4 3 0.60 1.10 4 4 -3 1.40 1.70 4 4 -3 -1.70 2.30 4 4 -3 3.90 1.80 -4 -5 3 23.70 6.60 -4 -5 3 31.90 10.10 -4 -6 3 24.20 9.20 -4 -6 3 24.40 7.40 -4 -7 3 13.60 6.60 -4 -7 3 24.40 10.80 -4 -8 3 42.70 12.70 -4 -9 3 28.80 10.60 5 -9 -3 1.70 6.90 5 -9 -3 14.60 11.30 5 -8 -3 14.20 8.30 5 -8 -3 25.50 12.70 5 -8 -3 -2.20 8.40 -5 7 3 10.30 4.00 5 -7 -3 3.70 7.60 5 -7 -3 -7.90 5.70 5 -7 -3 2.30 6.00 -5 6 3 37.90 8.30 5 -6 -3 32.40 12.40 5 -6 -3 26.80 8.70 5 -6 -3 22.30 8.10 -5 5 3 2.60 3.60 5 -5 -3 -1.30 4.40 5 -5 -3 1.60 4.70 5 -5 -3 6.80 6.60 -5 4 3 103.09 9.90 5 -4 -3 103.19 11.10 5 -4 -3 102.49 13.10 5 -4 -3 98.89 9.90 -5 3 3 5.40 3.80 5 -3 -3 7.40 5.90 5 -3 -3 6.60 4.10 5 -3 -3 4.40 3.80 -5 2 3 153.18 11.00 5 -2 -3 167.88 11.00 5 -2 -3 156.48 10.90 5 -2 -3 166.08 13.70 -5 1 3 82.49 7.60 5 -1 -3 81.39 7.10 5 -1 -3 74.99 8.80 5 -1 -3 76.79 6.80 -5 0 3 -1.30 1.80 5 0 -3 0.60 3.10 5 0 -3 -2.20 1.90 5 0 -3 -0.30 1.50 -5 -1 3 73.29 8.30 -5 -1 3 77.29 6.70 -5 -2 3 154.38 9.30 -5 -2 3 184.98 10.10 -5 -2 3 170.88 13.60 -5 -3 3 4.60 2.80 -5 -3 3 7.00 3.00 -5 -3 3 6.90 5.20 5 3 -3 12.10 2.90 -5 -4 3 95.49 8.80 -5 -4 3 105.79 12.10 5 4 -3 98.89 6.20 5 4 -3 113.29 6.50 -5 -5 3 1.00 3.10 -5 -5 3 6.30 5.40 -5 -6 3 50.19 13.60 -5 -6 3 25.50 7.30 -5 -7 3 16.70 7.70 -5 -7 3 2.50 4.50 -5 -8 3 34.30 12.90 -5 -8 3 17.90 7.80 -5 -9 3 2.20 5.20 -5 -9 3 17.80 7.70 6 -8 -3 12.50 8.90 6 -8 -3 35.00 14.60 -6 7 3 11.00 4.70 6 -7 -3 -5.60 5.60 6 -7 -3 -1.00 5.30 6 -7 -3 2.80 8.40 -6 6 3 29.90 7.90 6 -6 -3 21.10 8.50 6 -6 -3 45.20 14.00 6 -6 -3 29.80 9.40 -6 5 3 47.50 7.30 6 -5 -3 33.30 9.00 6 -5 -3 48.00 10.10 6 -5 -3 46.70 9.50 -6 4 3 42.00 9.00 6 -4 -3 35.30 11.30 6 -4 -3 23.20 7.20 6 -4 -3 26.60 7.40 -6 3 3 47.70 7.00 6 -3 -3 46.70 8.70 6 -3 -3 45.00 8.80 6 -3 -3 39.70 7.90 -6 2 3 197.78 13.50 6 -2 -3 213.28 13.30 6 -2 -3 214.38 13.40 6 -2 -3 198.38 16.30 -6 1 3 64.39 7.40 6 -1 -3 64.19 8.90 6 -1 -3 67.09 7.50 6 -1 -3 71.89 7.20 -6 0 3 4.40 3.50 6 0 -3 4.60 3.20 6 0 -3 2.60 2.40 6 0 -3 2.30 4.00 -6 -1 3 69.59 6.90 6 1 -3 65.99 9.00 -6 -2 3 210.68 12.10 -6 -2 3 218.08 16.60 -6 -2 3 235.28 12.60 -6 -3 3 45.60 6.30 -6 -3 3 46.30 5.30 -6 -3 3 47.20 8.50 -6 -4 3 46.00 12.10 -6 -4 3 36.70 6.60 6 4 -3 34.90 4.30 -6 -6 3 33.40 8.40 -6 -6 3 42.00 12.80 -6 -7 3 1.50 4.20 -6 -7 3 13.50 7.80 -6 -8 3 53.59 10.70 -6 -8 3 15.60 7.40 7 -8 -3 20.00 10.90 7 -8 -3 5.20 7.30 -7 7 3 13.80 5.40 7 -7 -3 1.90 6.00 7 -7 -3 10.10 9.80 7 -7 -3 -2.20 7.10 -7 6 3 19.00 5.70 7 -6 -3 0.20 6.40 7 -6 -3 2.90 5.80 7 -6 -3 19.00 9.30 -7 5 3 34.40 8.40 7 -5 -3 26.40 7.80 7 -5 -3 41.00 13.30 7 -5 -3 26.40 8.70 -7 4 3 2.00 3.40 7 -4 -3 2.30 6.00 7 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4 24.00 11.30 -1 -9 -4 8.00 7.30 -1 -9 -4 24.90 11.10 1 8 4 9.70 5.00 -1 -8 -4 -0.60 5.10 -1 -8 -4 18.50 9.70 1 7 4 19.70 5.00 1 7 4 15.20 6.00 -1 -7 -4 21.80 10.70 -1 -7 -4 10.40 6.40 1 6 4 0.80 3.20 1 6 4 2.40 4.20 -1 -6 -4 2.20 4.60 -1 -6 -4 1.50 6.00 1 5 4 21.00 5.70 1 5 4 14.70 5.30 -1 -5 -4 16.40 6.10 -1 -5 -4 27.50 8.70 1 4 4 13.60 4.40 1 4 4 14.30 4.80 -1 -4 -4 17.70 6.50 -1 -4 -4 15.10 5.10 1 3 4 21.90 5.30 1 3 4 24.10 4.50 -1 -3 -4 21.00 5.10 -1 -3 -4 23.40 6.20 -1 -3 -4 18.20 4.50 1 2 4 345.67 11.00 1 2 4 335.17 14.40 -1 -2 -4 335.27 15.10 -1 -2 -4 329.07 13.70 -1 -2 -4 329.97 15.70 1 1 4 5.90 3.40 1 1 4 4.00 2.40 -1 -1 -4 6.80 1.80 -1 -1 -4 3.60 2.70 -1 -1 -4 7.40 2.70 -1 -1 -4 2.90 2.10 1 0 4 977.00 29.10 -1 0 -4 900.41 30.10 -1 0 -4 929.41 28.40 -1 0 -4 931.81 30.40 -1 0 -4 986.90 29.20 1 -1 4 1.80 2.00 1 -1 4 3.70 2.60 1 -1 4 4.20 2.00 -1 1 -4 7.60 2.20 -1 1 -4 2.00 2.00 1 -2 4 332.37 12.60 1 -2 4 355.26 12.70 1 -2 4 338.47 15.50 1 -2 4 345.97 14.50 1 -3 4 18.40 4.50 1 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18.80 5.50 1 -7 -4 21.20 10.30 1 -7 -4 15.20 7.40 -1 6 4 2.20 3.30 1 -6 -4 0.90 4.70 1 -6 -4 0.50 6.20 -1 5 4 23.00 5.70 1 -5 -4 24.30 6.90 1 -5 -4 13.20 5.90 1 -5 -4 22.50 9.20 -1 4 4 14.50 4.60 1 -4 -4 14.30 5.10 1 -4 -4 11.40 4.80 1 -4 -4 19.30 7.20 -1 3 4 20.80 4.90 1 -3 -4 19.00 6.30 1 -3 -4 19.20 4.70 1 -3 -4 24.10 4.40 1 -3 -4 15.90 4.60 -1 2 4 327.97 14.40 1 -2 -4 334.97 17.30 1 -2 -4 341.27 13.90 1 -2 -4 364.06 15.00 1 -2 -4 358.66 11.90 1 -2 -4 342.27 14.80 -1 1 4 8.40 3.30 -1 1 4 4.90 2.60 1 -1 -4 5.50 3.30 1 -1 -4 4.30 3.40 1 -1 -4 7.60 2.80 1 -1 -4 3.80 2.00 -1 0 4 1013.10 27.20 -1 0 4 1007.00 26.00 -1 0 4 983.60 29.70 1 0 -4 928.91 35.20 1 0 -4 939.31 34.50 1 0 -4 1001.80 29.80 1 0 -4 1009.30 27.20 -1 -1 4 5.10 1.30 -1 -1 4 4.00 1.40 -1 -1 4 5.10 2.90 -1 -1 4 6.90 2.60 1 1 -4 7.90 2.80 1 1 -4 2.70 1.20 -1 -2 4 344.27 12.90 -1 -2 4 350.76 17.10 -1 -2 4 358.26 11.50 1 2 -4 330.57 11.10 -1 -3 4 19.40 5.90 -1 -3 4 11.80 3.50 -1 -4 4 16.30 5.00 -1 -4 4 22.90 7.10 -1 -5 4 28.50 8.70 -1 -5 4 15.40 5.80 1 5 -4 24.70 3.80 -1 -6 4 8.50 6.80 -1 -6 4 1.40 4.50 -1 -7 4 17.10 8.90 -1 -7 4 10.30 6.40 1 7 -4 19.40 6.40 -1 -8 4 16.10 8.80 -1 -8 4 0.80 5.00 1 8 -4 7.50 4.40 -1 -9 4 3.30 6.50 -1 -9 4 22.40 9.90 2 -9 -4 28.00 13.60 2 -8 -4 4.50 6.60 2 -8 -4 -0.70 9.60 -2 7 4 31.10 6.80 2 -7 -4 36.50 12.70 2 -7 -4 15.60 7.80 2 -7 -4 29.50 9.10 -2 6 4 47.50 6.30 2 -6 -4 41.30 9.30 2 -6 -4 44.00 9.90 2 -6 -4 62.59 11.10 -2 5 4 32.30 5.70 2 -5 -4 41.40 8.40 2 -5 -4 25.40 7.40 2 -5 -4 33.70 10.60 -2 4 4 250.67 13.80 2 -4 -4 253.67 14.80 2 -4 -4 273.17 16.30 2 -4 -4 263.47 18.40 -2 3 4 51.89 6.10 2 -3 -4 53.29 6.70 2 -3 -4 61.79 8.10 2 -3 -4 51.69 6.70 -2 2 4 31.50 4.70 -2 2 4 30.40 4.50 2 -2 -4 41.10 5.30 2 -2 -4 37.90 5.10 2 -2 -4 39.60 6.00 2 -2 -4 28.70 4.90 -2 1 4 0.70 1.90 -2 1 4 1.90 2.30 2 -1 -4 0.30 2.40 2 -1 -4 1.70 2.80 2 -1 -4 1.00 2.10 2 -1 -4 1.40 1.60 -2 0 4 314.27 12.80 -2 0 4 327.57 10.80 -2 0 4 319.57 9.60 2 0 -4 324.97 11.00 2 0 -4 302.07 15.70 2 0 -4 328.97 9.70 2 0 -4 328.87 13.10 -2 -1 4 1.30 1.80 -2 -1 4 2.10 2.40 -2 -1 4 0.30 0.60 2 1 -4 2.00 1.20 2 1 -4 2.20 2.20 -2 -2 4 37.40 3.80 -2 -2 4 33.40 5.30 -2 -2 4 34.20 3.00 2 2 -4 36.70 3.60 -2 -3 4 52.89 5.60 -2 -3 4 52.69 7.20 2 3 -4 51.29 2.60 -2 -4 4 274.97 14.70 -2 -4 4 251.67 17.50 2 4 -4 264.87 9.10 -2 -5 4 47.60 11.40 -2 -5 4 30.90 7.30 2 5 -4 35.40 4.00 -2 -6 4 48.90 9.00 -2 -6 4 49.20 8.60 -2 -7 4 29.40 8.90 -2 -7 4 44.00 13.20 -2 -8 4 2.00 5.00 -2 -8 4 10.60 8.60 2 8 -4 10.70 4.80 -2 -9 4 15.20 11.00 -2 -9 4 12.70 8.00 3 -9 -4 14.70 11.40 3 -9 -4 10.10 8.10 3 -8 -4 0.20 5.40 3 -8 -4 -4.40 6.60 3 -8 -4 3.90 9.40 -3 7 4 25.70 6.20 3 -7 -4 18.30 8.00 3 -7 -4 4.30 7.60 3 -7 -4 24.20 12.10 -3 6 4 31.50 7.40 3 -6 -4 9.80 6.70 3 -6 -4 30.20 12.10 3 -6 -4 13.00 6.60 -3 5 4 43.90 6.40 3 -5 -4 51.59 10.10 3 -5 -4 47.40 9.20 3 -5 -4 51.89 10.20 -3 4 4 217.38 13.30 3 -4 -4 209.48 14.60 3 -4 -4 216.68 13.60 3 -4 -4 211.38 17.00 -3 3 4 120.89 9.30 3 -3 -4 136.79 12.40 3 -3 -4 134.89 10.20 3 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-5 -8 4 10.30 7.30 -5 -8 4 9.00 6.10 -6 8 4 19.50 5.60 6 -8 -4 6.00 11.80 6 -8 -4 -4.60 5.80 -6 7 4 29.40 7.90 6 -7 -4 5.90 7.80 6 -7 -4 22.40 9.20 6 -7 -4 28.80 13.70 -6 6 4 53.49 8.10 6 -6 -4 52.79 11.50 6 -6 -4 62.49 13.10 6 -6 -4 64.29 12.20 -6 5 4 14.10 5.70 6 -5 -4 6.20 5.90 6 -5 -4 8.50 8.40 6 -5 -4 4.50 5.90 -6 4 4 180.28 14.00 6 -4 -4 197.38 15.40 6 -4 -4 182.08 17.70 6 -4 -4 190.58 14.10 -6 3 4 39.00 6.60 6 -3 -4 37.40 7.90 6 -3 -4 36.90 11.10 6 -3 -4 47.60 8.70 -6 2 4 32.30 5.60 6 -2 -4 32.10 6.50 6 -2 -4 36.10 10.00 6 -2 -4 26.90 6.40 -6 1 4 59.89 7.20 6 -1 -4 59.99 6.70 6 -1 -4 56.99 8.80 6 -1 -4 57.49 7.40 -6 0 4 66.89 7.30 6 0 -4 70.69 7.00 6 0 -4 55.79 8.40 6 0 -4 69.29 6.30 -6 -1 4 63.39 6.90 6 1 -4 57.09 8.80 6 1 -4 55.59 5.30 6 1 -4 59.89 6.20 -6 -2 4 32.30 4.80 -6 -2 4 31.30 4.80 -6 -2 4 32.20 7.00 -6 -3 4 38.20 10.50 -6 -3 4 42.00 5.00 -6 -3 4 42.30 6.00 -6 -4 4 196.18 10.50 -6 -4 4 217.98 13.70 -6 -4 4 203.28 18.10 -6 -5 4 20.60 9.20 -6 -5 4 12.70 5.10 -6 -7 4 44.20 9.30 -6 -7 4 29.80 8.50 -6 -8 4 38.60 7.40 7 -8 -4 0.70 6.70 7 -8 -4 13.60 10.60 7 -7 -4 38.80 13.90 7 -7 -4 15.90 9.30 7 -7 -4 17.40 8.70 -7 6 4 8.60 4.30 7 -6 -4 2.50 7.70 7 -6 -4 -2.40 5.00 7 -6 -4 -2.40 5.60 -7 5 4 69.99 9.30 7 -5 -4 75.09 13.30 7 -5 -4 70.29 10.90 7 -5 -4 67.19 10.10 -7 4 4 23.40 7.40 7 -4 -4 15.90 6.50 7 -4 -4 23.60 10.20 7 -4 -4 17.00 6.70 -7 3 4 116.19 11.50 7 -3 -4 139.99 12.40 7 -3 -4 134.19 15.10 7 -3 -4 141.09 12.50 -7 2 4 57.69 7.90 7 -2 -4 61.49 8.50 7 -2 -4 55.29 9.70 7 -2 -4 51.49 7.40 -7 1 4 39.40 6.50 7 -1 -4 49.20 12.00 7 -1 -4 46.30 8.20 7 -1 -4 41.70 6.80 -7 0 4 105.89 9.90 7 0 -4 109.99 9.40 7 0 -4 105.39 8.60 7 0 -4 100.69 11.90 -7 -1 4 39.60 5.90 7 1 -4 45.80 11.60 7 1 -4 40.50 5.50 7 1 -4 45.30 7.10 -7 -2 4 65.09 7.10 -7 -2 4 56.79 9.40 -7 -3 4 134.69 9.70 -7 -3 4 145.39 15.10 -7 -3 4 145.89 10.60 -7 -4 4 23.20 6.00 -7 -4 4 31.40 4.40 -7 -4 4 38.00 12.10 -7 -5 4 91.39 13.70 -7 -5 4 83.79 10.00 -7 -6 4 19.00 10.30 -7 -7 4 58.59 15.50 -7 -8 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3 -1 16 1.40 3.50 3 -1 16 4.00 8.50 3 -2 16 3.40 4.60 3 -2 16 1.00 7.90 3 -3 16 3.80 5.10 3 -3 16 -1.10 7.70 3 -4 16 2.00 5.70 3 -4 16 -6.60 8.10 3 -5 16 4.80 6.80 2 6 16 1.30 9.00 -2 -6 -16 4.60 6.10 2 5 16 13.60 10.10 -2 -5 -16 18.80 8.70 2 4 16 -2.10 8.10 -2 -4 -16 3.40 4.70 2 3 16 0.40 7.40 -2 -3 -16 1.30 3.90 2 2 16 9.10 9.30 -2 -2 -16 6.10 5.00 2 1 16 0.80 8.10 -2 -1 -16 2.30 3.80 2 0 16 16.00 10.30 2 -1 16 -0.10 8.10 2 -1 16 8.20 4.60 2 -2 16 4.40 3.40 2 -2 16 1.70 8.60 2 -3 16 -1.90 7.10 2 -3 16 1.80 2.70 1 6 16 10.40 8.20 -1 -6 -16 5.10 6.20 1 5 16 -6.10 6.90 -1 -5 -16 4.10 5.70 1 4 16 -1.10 7.70 -1 -4 -16 5.70 5.20 1 3 16 23.30 10.90 -1 -3 -16 27.90 8.10 1 2 16 23.80 10.10 -1 -2 -16 17.60 6.30 1 1 16 1.50 8.90 -1 -1 -16 10.80 5.10 1 0 16 36.10 11.50 1 -1 16 16.90 5.60 1 -1 16 18.00 9.20 1 -2 16 19.10 6.30 1 -2 16 19.20 10.10 1 -3 16 25.90 9.70 0 6 16 9.20 7.90 0 -6 -16 12.20 7.50 0 5 16 1.20 7.70 0 -5 -16 24.80 10.00 0 -5 -16 3.60 5.00 0 4 16 50.99 13.20 0 -4 -16 29.90 9.00 0 -4 -16 46.10 9.10 0 3 16 -2.10 7.20 0 -3 -16 15.50 6.20 0 -3 -16 3.00 4.30 0 2 16 12.40 9.40 0 -2 -16 20.60 6.30 0 1 16 1.70 6.80 0 0 16 4.90 7.00 0 -1 16 -4.50 6.20 0 -2 16 17.30 8.90 0 -3 16 -2.20 6.40 -1 6 16 12.60 7.70 1 -6 -16 5.30 5.80 1 -6 -16 33.20 11.80 -1 5 16 6.80 7.80 1 -5 -16 27.30 10.20 1 -5 -16 3.20 5.30 -1 4 16 9.70 7.80 1 -4 -16 6.80 5.20 1 -4 -16 22.10 9.20 -1 3 16 43.20 12.30 1 -3 -16 54.09 8.60 -1 2 16 16.20 8.60 1 -2 -16 17.70 5.70 -1 1 16 23.30 8.80 1 -1 -16 45.00 6.40 -1 0 16 30.10 10.50 1 0 -16 53.39 6.90 1 1 -16 50.39 6.40 -1 -2 16 23.70 9.00 1 3 -16 89.79 8.80 -1 -5 16 19.20 7.20 2 -6 -16 34.80 11.20 -2 5 16 28.30 9.40 2 -5 -16 19.40 7.80 -2 4 16 -0.20 5.40 2 -4 -16 3.40 4.30 2 -4 -16 19.90 8.00 -2 3 16 6.90 6.20 2 -3 -16 18.30 7.90 -2 2 16 9.50 7.20 2 -2 -16 37.80 7.00 -2 1 16 11.40 7.40 -2 0 16 19.40 8.30 2 0 -16 40.30 6.60 2 2 -16 41.00 6.30 -2 -5 16 47.80 8.90 -2 -6 16 13.90 8.50 3 -6 -16 25.90 12.50 -3 5 16 4.40 7.20 3 -5 -16 33.20 11.80 -3 4 16 0.70 6.10 3 -4 -16 19.60 9.00 3 -3 -16 30.80 9.70 -3 2 16 6.20 5.90 3 -2 -16 23.60 7.60 -3 1 16 3.50 5.90 3 -1 -16 35.40 7.10 3 0 -16 33.30 6.70 -3 -1 16 3.60 5.90 -3 -2 16 10.50 5.90 3 2 -16 40.90 6.60 3 3 -16 58.99 7.50 3 4 -16 66.99 8.10 -3 -5 16 42.90 8.40 -3 -6 16 24.70 9.70 4 -5 -16 47.90 10.00 4 -4 -16 48.60 9.90 -4 3 16 32.50 9.70 4 -3 -16 41.80 12.90 -4 2 16 11.90 7.60 4 -2 -16 41.80 8.20 -4 1 16 23.60 7.20 4 -1 -16 32.90 6.60 -4 0 16 34.70 9.70 4 0 -16 60.89 8.30 4 1 -16 52.99 7.00 4 2 -16 49.90 7.70 4 3 -16 48.80 7.20 4 4 -16 45.80 6.70 5 -5 -16 46.30 14.50 -5 4 16 7.00 6.40 5 -4 -16 41.10 11.90 5 -3 -16 52.89 10.00 5 -2 -16 48.90 8.30 -5 1 16 11.80 5.60 5 -1 -16 40.10 7.10 5 0 -16 42.30 7.50 -5 -1 16 22.30 6.70 5 1 -16 41.60 7.00 5 3 -16 89.59 10.10 5 4 -16 56.39 8.40 6 -4 -16 51.29 10.70 -6 2 16 9.60 6.30 6 -2 -16 43.30 8.50 -6 1 16 23.20 7.30 6 -1 -16 32.30 6.90 -6 0 16 43.20 7.00 6 0 -16 52.39 8.20 -6 -2 16 39.90 6.10 6 3 -16 75.89 10.00 6 4 -16 85.09 10.20 7 -3 -16 45.70 9.10 -7 2 16 30.60 8.00 -7 1 16 28.10 8.20 7 -1 -16 49.50 8.60 -7 0 16 31.90 7.80 -7 -1 16 24.70 6.80 7 2 -16 67.69 9.10 7 3 -16 75.69 10.90 7 4 -16 77.29 9.90 8 -2 -16 78.89 11.50 8 -1 -16 58.29 9.10 -8 0 16 71.09 9.80 8 0 -16 85.39 11.20 -8 -1 16 49.00 7.00 8 1 -16 61.89 8.80 8 2 -16 89.49 10.90 8 0 17 6.10 5.30 7 0 17 4.30 4.70 7 -1 17 2.90 5.10 7 -2 17 3.30 5.60 7 -3 17 8.40 7.20 -6 -3 -17 3.40 5.10 6 2 17 27.50 13.60 -6 -2 -17 20.00 8.00 6 1 17 -2.00 9.20 6 0 17 2.60 3.90 6 0 17 3.20 8.80 6 -1 17 4.20 8.60 6 -1 17 5.30 5.30 6 -2 17 15.50 7.60 6 -2 17 31.40 11.70 6 -3 17 -0.30 5.30 6 -3 17 9.30 9.50 6 -4 17 8.30 7.80 6 -4 17 19.90 10.50 -5 -4 -17 7.10 6.10 5 3 17 10.10 11.40 -5 -3 -17 6.10 5.60 5 2 17 4.70 10.20 -5 -2 -17 4.60 5.40 5 1 17 -7.20 8.20 5 0 17 4.70 9.20 5 -1 17 -4.80 7.80 5 -1 17 3.80 4.30 5 -2 17 4.20 9.80 5 -2 17 5.20 5.60 5 -3 17 2.70 5.90 5 -3 17 11.40 9.50 5 -4 17 1.90 6.50 5 -4 17 4.90 9.30 -4 -5 -17 8.70 6.60 4 4 17 -1.90 9.30 -4 -4 -17 1.90 4.90 4 3 17 -4.10 9.50 -4 -3 -17 5.00 5.40 4 2 17 -5.00 8.40 -4 -2 -17 2.00 4.50 4 1 17 -1.00 9.10 4 0 17 7.70 8.90 4 -1 17 1.10 8.20 4 -1 17 5.40 4.60 4 -2 17 -1.70 7.90 4 -2 17 3.70 4.80 4 -3 17 2.50 5.30 4 -3 17 1.20 8.40 4 -4 17 5.50 6.90 4 -4 17 -2.60 9.20 3 5 17 -11.80 8.00 -3 -5 -17 4.20 5.70 3 4 17 -8.70 8.10 -3 -4 -17 2.00 4.90 3 3 17 -1.60 8.30 -3 -3 -17 2.60 4.80 3 2 17 -0.70 7.90 -3 -2 -17 3.30 4.50 3 1 17 -8.10 7.70 -3 -1 -17 3.00 4.20 3 0 17 -2.00 7.50 3 -1 17 6.20 4.50 3 -1 17 4.70 8.50 3 -2 17 -8.50 7.10 3 -2 17 3.50 4.60 3 -3 17 -4.20 8.70 3 -3 17 4.80 5.20 2 5 17 3.20 8.50 -2 -5 -17 3.50 5.40 2 4 17 5.60 9.70 -2 -4 -17 10.40 6.50 2 3 17 -0.70 7.80 -2 -3 -17 2.30 4.30 2 2 17 18.10 10.10 -2 -2 -17 24.00 7.70 2 1 17 11.10 9.10 -2 -1 -17 7.00 4.80 2 0 17 -4.60 7.90 2 -1 17 8.20 10.00 2 -1 17 7.70 3.70 2 -2 17 16.00 10.10 2 -2 17 14.50 5.20 2 -3 17 8.00 8.50 1 5 17 21.20 11.50 -1 -5 -17 16.50 8.00 1 4 17 4.60 8.00 -1 -4 -17 0.80 4.30 1 3 17 8.10 8.40 -1 -3 -17 5.40 4.50 1 2 17 -1.90 6.50 -1 -2 -17 1.60 3.60 1 1 17 7.20 8.80 -1 -1 -17 8.00 4.90 1 0 17 -0.80 7.60 1 -1 17 3.40 8.20 1 -2 17 4.80 7.60 1 -3 17 17.20 10.00 0 5 17 3.10 7.10 0 -5 -17 2.10 4.80 0 4 17 16.10 9.20 0 -4 -17 12.70 6.50 0 3 17 -3.50 6.40 0 -3 -17 3.10 4.10 0 2 17 12.50 8.70 0 -2 -17 10.00 5.10 0 1 17 4.10 6.30 0 -1 -17 -0.50 3.10 0 0 17 3.90 6.10 0 -1 17 -1.30 7.20 0 -2 17 11.70 8.10 0 -3 17 3.60 6.80 -1 5 17 13.30 9.20 1 -5 -17 20.30 8.20 -1 4 17 2.60 7.50 1 -4 -17 4.70 4.90 1 -4 -17 28.90 9.50 -1 3 17 16.50 8.50 1 -3 -17 22.40 8.60 1 -3 -17 9.60 5.10 -1 2 17 7.50 7.20 1 -2 -17 36.90 6.60 -1 1 17 7.10 7.90 -1 -2 17 3.40 7.00 -1 -3 17 18.10 8.10 2 -5 -17 49.40 10.70 -2 4 17 8.80 8.10 2 -4 -17 39.60 11.50 2 -2 -17 66.89 8.70 -2 1 17 10.90 7.40 -2 0 17 8.70 7.10 2 1 -17 60.29 6.80 2 2 -17 71.89 8.00 2 3 -17 64.19 7.40 2 4 -17 96.19 9.30 3 -5 -17 59.59 10.70 -3 3 17 15.30 7.30 -3 -1 17 6.90 6.40 3 3 -17 73.59 8.30 3 4 -17 76.89 8.80 4 -5 -17 37.80 12.60 -4 4 17 4.80 7.10 4 -4 -17 41.50 12.60 -4 3 17 13.10 7.40 4 -3 -17 50.59 9.80 -4 0 17 13.60 6.40 -4 -1 17 12.00 6.70 4 2 -17 44.70 6.40 4 3 -17 74.89 9.20 4 4 -17 81.09 9.70 4 5 -17 105.59 10.90 5 -4 -17 62.99 10.90 -5 3 17 5.20 6.90 5 -3 -17 39.10 8.30 5 -2 -17 61.49 9.60 -5 -2 17 40.20 6.40 5 3 -17 89.49 10.40 5 4 -17 57.09 7.90 6 -4 -17 72.89 12.30 6 -3 -17 38.80 12.00 -6 2 17 50.19 8.30 -6 1 17 28.40 7.20 6 -1 -17 50.59 8.30 -6 0 17 23.40 6.60 -6 -1 17 35.90 8.90 6 1 -17 49.10 8.30 6 2 -17 87.99 10.60 6 3 -17 63.69 8.20 6 4 -17 78.19 10.10 7 -3 -17 79.59 12.60 7 -2 -17 44.30 8.50 -7 1 17 45.80 8.10 7 -1 -17 48.90 8.30 -7 0 17 42.80 7.00 -7 -1 17 48.20 7.50 7 2 -17 77.79 10.10 7 3 -17 78.09 10.10 8 -1 -17 83.49 11.10 8 0 -17 51.19 8.90 8 1 -17 92.69 11.60 7 0 18 5.30 4.90 7 -1 18 6.50 5.70 6 0 18 13.30 6.20 6 -1 18 2.40 4.60 6 -2 18 2.20 5.10 -5 -3 -18 1.30 4.90 5 2 18 9.40 11.50 -5 -2 -18 13.30 7.20 5 1 18 3.50 9.60 5 0 18 13.40 12.40 5 0 18 20.50 7.20 5 -1 18 -0.20 9.20 5 -1 18 4.50 4.80 5 -2 18 15.20 11.60 5 -2 18 15.40 7.60 5 -3 18 1.50 5.60 5 -3 18 -1.40 9.50 -4 -4 -18 2.30 5.30 4 3 18 0.30 9.10 -4 -3 -18 4.80 5.40 4 2 18 10.80 10.70 -4 -2 -18 3.50 5.10 4 1 18 5.50 10.10 4 0 18 -5.00 9.00 4 -1 18 5.00 4.70 4 -1 18 2.40 8.50 4 -2 18 6.20 9.90 4 -2 18 3.40 5.10 4 -3 18 -0.80 5.00 4 -3 18 -14.40 7.80 3 4 18 -4.90 9.50 -3 -4 -18 1.80 5.30 3 3 18 -6.20 8.70 -3 -3 -18 0.60 4.40 3 2 18 2.10 9.90 -3 -2 -18 0.80 4.00 3 1 18 -8.80 7.80 3 0 18 -2.10 8.60 3 -1 18 -6.90 8.00 3 -1 18 3.00 4.10 3 -2 18 0.20 10.20 3 -2 18 7.90 5.70 3 -3 18 -12.90 9.00 -2 -5 -18 9.80 6.60 2 4 18 3.60 9.50 -2 -4 -18 -0.80 4.10 2 3 18 10.80 10.00 -2 -3 -18 9.00 6.00 2 2 18 11.00 9.60 -2 -2 -18 2.50 4.10 2 1 18 0.00 8.90 2 0 18 24.60 11.90 2 -1 18 -14.20 7.60 2 -2 18 6.40 9.10 2 -3 18 16.80 10.40 -1 -5 -18 6.80 6.20 1 4 18 5.00 8.50 -1 -4 -18 1.70 4.90 1 3 18 0.00 8.90 -1 -3 -18 5.00 4.70 1 2 18 0.40 8.10 -1 -2 -18 1.80 3.90 1 1 18 2.50 8.00 1 0 18 12.00 9.20 1 -1 18 -4.10 7.70 1 -2 18 -2.80 8.40 1 -3 18 -6.00 8.10 0 -5 -18 5.80 5.50 0 4 18 33.10 12.70 0 -4 -18 28.70 9.00 0 3 18 -4.50 7.00 0 -3 -18 1.30 4.10 0 2 18 11.30 8.70 0 1 18 -4.40 7.60 0 0 18 1.30 7.10 0 -1 18 7.00 7.70 0 -2 18 5.10 8.80 0 -3 18 6.10 7.90 -1 4 18 1.30 7.80 -1 3 18 7.00 7.80 -1 2 18 8.90 8.40 -1 1 18 1.70 6.50 -1 0 18 1.20 7.80 -1 -1 18 6.60 7.70 -1 -2 18 6.90 8.10 2 -5 -18 64.19 11.50 2 -4 -18 46.70 9.50 2 -3 -18 51.69 8.50 -2 1 18 9.50 7.40 2 0 -18 66.49 7.80 -2 -2 18 13.20 7.20 3 -4 -18 26.90 9.60 3 3 -18 93.19 9.20 3 4 -18 101.29 9.60 4 -4 -18 41.50 8.20 4 -3 -18 58.09 10.30 4 -1 -18 57.69 8.40 -4 -2 18 42.30 7.40 4 2 -18 60.99 7.60 4 3 -18 85.29 9.00 4 4 -18 97.99 10.20 5 -3 -18 43.30 12.70 5 -2 -18 77.39 11.20 5 0 -18 83.19 10.20 -5 -1 18 30.20 6.90 5 2 -18 58.19 8.50 5 3 -18 105.39 9.60 6 -3 -18 57.99 10.10 6 -2 -18 87.79 10.60 6 -1 -18 51.89 7.90 -6 0 18 43.20 7.70 -6 -1 18 47.00 8.10 6 2 -18 95.19 10.80 6 3 -18 80.39 9.40 7 -1 -18 52.69 8.80 7 0 -18 77.89 10.80 7 1 -18 96.89 11.50 6 0 19 6.00 4.90 -5 -2 -19 0.80 4.60 5 0 19 5.30 4.20 5 -1 19 9.40 5.80 5 -2 19 2.20 5.10 -4 -3 -19 2.60 4.90 -4 -2 -19 1.90 4.90 4 1 19 9.50 11.60 4 0 19 -8.70 9.30 4 0 19 6.90 4.30 4 -1 19 7.00 5.10 4 -1 19 14.90 12.10 4 -2 19 5.20 5.60 4 -2 19 0.00 10.40 4 -3 19 -9.90 9.20 -3 -3 -19 1.60 5.00 3 2 19 2.90 10.70 -3 -2 -19 5.30 5.20 3 1 19 19.90 11.60 3 0 19 -0.80 9.60 3 0 19 7.40 4.20 3 -1 19 3.50 11.60 3 -2 19 -7.00 9.00 3 -3 19 -5.20 10.60 -2 -4 -19 3.10 5.20 -2 -3 -19 3.80 5.00 2 2 19 -3.70 9.20 -2 -2 -19 -0.90 3.90 2 1 19 20.10 11.80 2 0 19 -7.80 8.50 2 -1 19 7.20 11.70 2 -2 19 1.80 8.90 2 -3 19 -0.30 9.30 -1 -4 -19 6.80 5.50 1 3 19 -4.00 8.40 -1 -3 -19 4.20 4.80 1 2 19 -4.20 6.60 1 1 19 12.00 9.50 1 0 19 -12.00 6.20 1 -1 19 2.20 9.50 1 -2 19 4.40 8.70 1 -3 19 -11.50 8.40 0 3 19 -0.30 7.90 0 2 19 12.80 9.70 0 1 19 0.50 8.30 0 0 19 2.80 7.80 0 -1 19 4.30 8.10 0 -2 19 8.00 9.40 -1 3 19 -1.60 7.60 -1 2 19 7.70 7.80 -1 1 19 8.80 9.20 -1 0 19 3.70 8.20 -1 -1 19 18.90 9.60 -1 -2 19 4.60 8.10 -2 2 19 13.20 7.40 -2 1 19 17.40 9.90 -2 0 19 9.00 8.10 -2 -1 19 24.50 9.00 -2 -2 19 9.80 7.00 3 -4 -19 62.09 10.40 3 -3 -19 70.99 10.50 3 -1 -19 81.39 8.80 -3 -1 19 35.20 9.60 -3 -2 19 20.30 6.90 4 -3 -19 58.29 10.00 4 -2 -19 69.19 9.50 4 -1 -19 82.69 10.00 4 0 -19 59.39 7.40 -4 -1 19 29.10 8.70 4 2 -19 103.59 9.60 4 3 -19 122.69 10.50 5 -2 -19 96.59 10.50 5 0 -19 83.69 9.50 5 2 -19 105.39 10.60 6 0 -19 60.09 8.60 6 1 -19 65.79 9.20 4 0 20 11.50 5.30 -3 -2 -20 5.00 5.60 3 -1 20 -2.20 9.90 3 -2 20 7.70 11.20 2 0 20 -5.90 9.10 2 -1 20 0.70 10.50 2 -2 20 -8.10 9.70 1 1 20 9.30 10.90 1 0 20 19.30 11.30 1 -1 20 20.00 11.30 1 -2 20 18.30 12.00 0 1 20 10.20 9.40 0 0 20 79.99 17.60 0 -1 20 7.10 9.40 0 -2 20 16.80 11.00 -1 1 20 14.20 9.70 -1 0 20 8.70 9.90 -1 -1 20 15.40 9.90 -1 -2 20 16.20 10.50 -2 1 20 15.60 8.20 -2 0 20 12.80 8.10 -2 -1 20 20.70 8.90 -2 -2 20 17.50 8.20 -3 0 20 25.60 9.50 -3 -1 20 15.50 7.80 4 -2 -20 80.29 10.10 4 -1 -20 103.89 10.20 -4 -1 20 32.30 8.80 0 -1 21 5.80 9.30 0 -2 21 11.60 10.70 -1 -1 21 17.50 9.70 -2 -1 21 19.00 10.00 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 76437 _shelx_res_file ; TITL lamp16aa_a.res in Pbca lamp16aa.res created by SHELXL-2019/3 at 18:59:06 on 19-Sep-2024 REM Old TITL lamp16aa in Pbca REM SHELXT solution in Pbca: R1 0.197, Rweak 0.066, Alpha 0.067 REM 1.868 for 205 systematic absences, Orientation as input REM Formula found by SHELXT: H2 H1c O1 CELL 0.71073 9.4484 7.0977 15.3781 90 90 90 ZERR 8 0.0008 0.0007 0.0014 0 0 0 LATT 1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H N O UNIT 24 64 16 16 EQIV $1 1-X,-0.5+Y,1.5-Z EQIV $2 0.5+X,+Y,1.5-Z L.S. 4 PLAN 1 SIZE 0.1 0.2 0.3 TEMP 23 CONF HTAB O1 N2_$1 HTAB N1 O2_$2 list 4 MORE -1 BOND $H fmap 2 acta OMIT 0 50 REM REM REM WGHT 0.043500 3.135700 FVAR 0.55836 O1 4 0.560275 0.392638 0.888330 11.00000 0.02212 0.02910 = 0.03211 -0.00398 -0.00606 0.00358 H1 2 0.575425 0.275461 0.875012 11.00000 0.02231 O2 4 0.210692 0.480158 0.807609 11.00000 0.01285 0.07003 = 0.04152 0.00163 0.00022 0.00128 N1 3 0.420017 0.476060 0.741456 11.00000 0.00951 0.03772 = 0.02808 0.00766 0.00114 0.00329 N2 3 0.365612 0.529965 0.659377 11.00000 0.01548 0.03515 = 0.02672 0.00961 0.00056 0.00175 H2 2 0.282716 0.533984 0.669801 11.00000 0.02382 H1A 2 0.494796 0.466548 0.740597 11.00000 0.00028 C1 1 0.411541 0.411487 0.894323 11.00000 0.02403 0.04565 = 0.02550 0.00000 0.00341 -0.00009 AFIX 23 H1B 2 0.389895 0.509200 0.936369 11.00000 -1.20000 H1C 2 0.372361 0.294298 0.916087 11.00000 -1.20000 AFIX 0 C2 1 0.340210 0.459211 0.809881 11.00000 0.02243 0.02183 = 0.03098 -0.00425 0.00408 -0.00217 C3 1 0.399946 0.391073 0.592778 11.00000 0.03532 0.04798 = 0.02810 0.00138 0.00031 -0.00679 AFIX 137 H3A 2 0.352088 0.422889 0.539704 11.00000 -1.50000 H3B 2 0.370059 0.268531 0.611778 11.00000 -1.50000 H3C 2 0.500296 0.390350 0.583003 11.00000 -1.50000 AFIX 0 HKLF 4 REM lamp16aa_a.res in Pbca REM wR2 = 0.1985, GooF = S = 1.339, Restrained GooF = 1.339 for all data REM R1 = 0.1028 for 841 Fo > 4sig(Fo) and 0.1091 for all 909 data REM 77 parameters refined using 0 restraints END WGHT 0.0435 3.1357 REM Highest difference peak 0.319, deepest hole -0.346, 1-sigma level 0.093 Q1 1 0.3296 0.2979 0.5635 11.00000 0.05 0.32 ; _shelx_res_checksum 38306 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O O1 0.5603(3) 0.3926(5) 0.8883(2) 0.0278(8) Uani d 1 . . H H1 0.575(4) 0.275(7) 0.875(3) 0.022(12) Uiso d 1 . . O O2 0.2107(3) 0.4802(6) 0.8076(2) 0.0415(10) Uani d 1 . . N N1 0.4200(4) 0.4761(5) 0.7415(2) 0.0251(9) Uani d 1 . . N N2 0.3656(4) 0.5300(5) 0.6594(2) 0.0258(9) Uani d 1 . . H H2 0.283(5) 0.534(7) 0.670(3) 0.024(13) Uiso d 1 . . H H1A 0.495(5) 0.467(5) 0.741(3) 0.000(10) Uiso d 1 . . C C1 0.4115(4) 0.4115(7) 0.8943(3) 0.0317(12) Uani d 1 . . H H1B 0.389895 0.509200 0.936369 0.038 Uiso calc 1 . . H H1C 0.372361 0.294298 0.916087 0.038 Uiso calc 1 . . C C2 0.3402(4) 0.4592(6) 0.8099(3) 0.0251(10) Uani d 1 . . C C3 0.3999(5) 0.3911(7) 0.5928(3) 0.0371(13) Uani d 1 . . H H3A 0.352088 0.422889 0.539704 0.056 Uiso calc 1 . . H H3B 0.370059 0.268531 0.611778 0.056 Uiso calc 1 . . H H3C 0.500296 0.390350 0.583003 0.056 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.0221(16) 0.0291(18) 0.0321(19) 0.0036(13) -0.0061(13) -0.0040(14) O2 0.0129(16) 0.070(3) 0.042(2) 0.0013(16) 0.0002(13) 0.0016(19) N1 0.0095(19) 0.038(2) 0.028(2) 0.0033(17) 0.0011(17) 0.0077(18) N2 0.0155(18) 0.035(2) 0.027(2) 0.0017(17) 0.0006(16) 0.0096(17) C1 0.024(2) 0.046(3) 0.025(3) 0.000(2) 0.0034(19) 0.000(2) C2 0.022(2) 0.022(2) 0.031(3) -0.0022(18) 0.0041(19) -0.0043(19) C3 0.035(3) 0.048(3) 0.028(3) -0.007(2) 0.000(2) 0.001(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C1 O1 H1 . . 106(3) ? N2 N1 H1A . . 112(3) ? C2 N1 N2 . . 122.4(4) ? C2 N1 H1A . . 126(3) ? N1 N2 H2 . . 101(3) ? N1 N2 C3 . . 111.3(4) ? C3 N2 H2 . . 112(3) ? O1 C1 H1B . . 108.7 ? O1 C1 H1C . . 108.7 ? O1 C1 C2 . . 114.3(4) ? H1B C1 H1C . . 107.6 ? C2 C1 H1B . . 108.7 ? C2 C1 H1C . . 108.7 ? O2 C2 N1 . . 122.8(4) ? O2 C2 C1 . . 119.8(4) ? N1 C2 C1 . . 117.4(4) ? N2 C3 H3A . . 109.5 ? N2 C3 H3B . . 109.5 ? N2 C3 H3C . . 109.5 ? H3A C3 H3B . . 109.5 ? H3A C3 H3C . . 109.5 ? H3B C3 H3C . . 109.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag O1 H1 . 0.87(5) ? O1 C1 . 1.415(5) ? O2 C2 . 1.233(5) ? N1 N2 . 1.416(5) ? N1 H1A . 0.71(4) ? N1 C2 . 1.300(6) ? N2 H2 . 0.80(5) ? N2 C3 . 1.458(6) ? C1 H1B . 0.9700 ? C1 H1C . 0.9700 ? C1 C2 . 1.502(6) ? C3 H3A . 0.9600 ? C3 H3B . 0.9600 ? C3 H3C . 0.9600 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag O1 H1 N2 3_646 0.87(5) 1.90(5) 2.767(5) 172(4) yes N1 H1A O2 6_657 0.71(4) 2.17(4) 2.848(5) 159(4) yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag O1 C1 C2 O2 . . . . -179.6(4) ? O1 C1 C2 N1 . . . . 0.7(6) ? N2 N1 C2 O2 . . . . 3.5(7) ? N2 N1 C2 C1 . . . . -176.7(4) ? C2 N1 N2 C3 . . . . -124.1(4) ?