#------------------------------------------------------------------------------ #$Date: 2024-08-02 03:53:16 +0200 (Fri, 02 Aug 2024) $ #$Revision: 293633 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/32/2023226.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023226 loop_ _publ_author_name 'Loukopoulos, Edward' 'Papatriantafyllopoulou, Constantina' 'Moushi, Eleni' 'Kitos, Alexandros A.' 'Tasiopoulos, Anastasios J.' 'Perlepes, Spyros P.' 'Nastopoulos, Vassilios' _publ_section_title ; Solvatomorphism in a series of copper(II) complexes with the 5-phenylimidazole/perchlorate system as ligands ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B Structural Science, Crystal Engineering and Materials' _journal_page_first 347 _journal_page_last 359 _journal_paper_doi 10.1107/S2052520624005948 _journal_volume 80 _journal_year 2024 _chemical_formula_moiety 'C36 H32 Cl2 Cu N8 O8, 2(C3 H8 O)' _chemical_formula_sum 'C42 H48 Cl2 Cu N8 O10' _chemical_formula_weight 959.32 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 103.496(6) _cell_angle_beta 94.562(5) _cell_angle_gamma 105.229(6) _cell_formula_units_Z 1 _cell_length_a 9.1329(6) _cell_length_b 10.0787(7) _cell_length_c 13.0825(8) _cell_measurement_reflns_used 4307 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 29.3780 _cell_measurement_theta_min 6.5150 _cell_volume 1117.04(14) _computing_cell_refinement 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_molecular_graphics 'PLATON v.270519 (Spek, 2009); MERCURY v.2020.3.0 (Macrae et al., 2020)' _computing_publication_material 'WINGX v.2018.3 (Farrugia, 2012); OLEX2 v.1.3.0 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT-2018/2 (Sheldrick, 2015); SIR92 (Altomare et al., 1994)' _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean 10.4223 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.990 _diffrn_measurement_device_type 'Oxford Diffraction SuperNova with Atlas CCD detector' _diffrn_measurement_method '\w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0253 _diffrn_reflns_av_unetI/netI 0.0351 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.990 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 10056 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.990 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.000 _diffrn_reflns_theta_min 3.023 _diffrn_source 'SuperNova (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 0.674 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.803 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour purple _exptl_crystal_density_diffrn 1.426 _exptl_crystal_density_method 'not measured' _exptl_crystal_description prism _exptl_crystal_F_000 499 _exptl_crystal_size_max 0.21 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.11 _refine_diff_density_max 0.382 _refine_diff_density_min -0.456 _refine_diff_density_rms 0.064 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.074 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 296 _refine_ls_number_reflns 4829 _refine_ls_number_restraints 3 _refine_ls_restrained_S_all 1.074 _refine_ls_R_factor_all 0.0470 _refine_ls_R_factor_gt 0.0362 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0337P)^2^+1.0475P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0861 _refine_ls_wR_factor_ref 0.0940 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4106 _reflns_number_total 4829 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file aw5090sup1.cif _cod_data_source_block 4 _cod_original_cell_volume 1117.04(13) _cod_database_code 2023226 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.871 _shelx_estimated_absorpt_t_max 0.930 _shelx_res_file ; 04.res created by SHELXL-2014/7 TITL EL50D in P-1 CELL 0.71073 9.1329 10.0787 13.0825 103.496 94.562 105.229 ZERR 1 0.0006 0.0007 0.0008 0.006 0.005 0.006 LATT 1 SFAC C H N O CL CU UNIT 42 48 8 10 2 1 MERG 2 FMAP 2 OMIT -2 54 SIZE 0.21 0.15 0.11 TEMP -173 ACTA LIST 4 MORE -3 PLAN 10 BOND BOND $H HTAB L.S. 7 WGHT 0.033700 1.047500 FVAR 4.78925 CU 6 0.000000 0.000000 0.000000 10.50000 0.01325 0.01377 = 0.01510 0.00377 0.00192 0.00413 DFIX 0.86 0.01 N1A H1A N1B H1B N1A 3 -0.222603 -0.341095 0.105770 11.00000 0.01948 0.01644 = 0.02552 0.00851 0.00421 0.00686 H1A 2 -0.223539 -0.422272 0.115503 11.00000 -1.50000 N1B 3 -0.344540 -0.124838 -0.258640 11.00000 0.01615 0.02476 = 0.01958 0.00485 -0.00028 0.00937 H1B 2 -0.432907 -0.126812 -0.287486 11.00000 -1.50000 C2A 1 -0.104573 -0.259370 0.073407 11.00000 0.01818 0.01946 = 0.02358 0.00717 0.00289 0.00689 AFIX 43 H2A 2 -0.009751 -0.279684 0.064786 11.00000 -1.20000 AFIX 0 C2B 1 -0.282483 -0.055242 -0.158121 11.00000 0.01898 0.01951 = 0.01960 0.00365 0.00359 0.00839 AFIX 43 H2B 2 -0.332533 -0.005491 -0.108163 11.00000 -1.20000 AFIX 0 N3A 3 -0.138015 -0.146951 0.055169 11.00000 0.01532 0.01568 = 0.01829 0.00390 0.00175 0.00361 N3B 3 -0.142075 -0.064839 -0.137430 11.00000 0.01544 0.01761 = 0.01672 0.00538 0.00205 0.00502 C4A 1 -0.285444 -0.158492 0.075919 11.00000 0.01620 0.01683 = 0.02082 0.00396 0.00220 0.00606 AFIX 43 H4A 2 -0.340410 -0.092127 0.069471 11.00000 -1.20000 AFIX 0 C4B 1 -0.114327 -0.144216 -0.230544 11.00000 0.01521 0.01915 = 0.01844 0.00442 0.00489 0.00678 AFIX 43 H4B 2 -0.021329 -0.167676 -0.240369 11.00000 -1.20000 AFIX 0 C5A 1 -0.340836 -0.280323 0.107297 11.00000 0.01759 0.01710 = 0.01676 0.00287 0.00091 0.00582 C5B 1 -0.239828 -0.184312 -0.306693 11.00000 0.01648 0.01767 = 0.01895 0.00599 0.00462 0.00505 C6A 1 -0.490027 -0.343847 0.135854 11.00000 0.01828 0.02190 = 0.01534 0.00633 0.00105 0.00234 C6B 1 -0.271099 -0.276522 -0.415004 11.00000 0.01920 0.02109 = 0.01901 0.00529 0.00387 0.00464 C7A 1 -0.539349 -0.488410 0.131221 11.00000 0.02528 0.02041 = 0.01579 0.00359 0.00189 0.00213 AFIX 43 H7A 2 -0.475446 -0.547252 0.109525 11.00000 -1.20000 AFIX 0 C7B 1 -0.398078 -0.287529 -0.485789 11.00000 0.02539 0.02572 = 0.02014 0.00420 0.00264 0.00981 AFIX 43 H7B 2 -0.466201 -0.233004 -0.464484 11.00000 -1.20000 AFIX 0 C8A 1 -0.681528 -0.546789 0.158192 11.00000 0.02943 0.02763 = 0.02159 0.00655 0.00180 -0.00593 AFIX 43 H8A 2 -0.713835 -0.645221 0.155801 11.00000 -1.20000 AFIX 0 C8B 1 -0.425781 -0.377988 -0.587614 11.00000 0.02913 0.03494 = 0.01987 0.00383 -0.00262 0.01043 AFIX 43 H8B 2 -0.513157 -0.385422 -0.635534 11.00000 -1.20000 AFIX 0 C9A 1 -0.776152 -0.463080 0.188401 11.00000 0.01904 0.04468 = 0.02275 0.00774 0.00303 -0.00454 AFIX 43 H9A 2 -0.873655 -0.503534 0.206441 11.00000 -1.20000 AFIX 0 C9B 1 -0.327480 -0.456925 -0.619546 11.00000 0.04097 0.03390 = 0.01866 -0.00137 0.00172 0.01405 AFIX 43 H9B 2 -0.346276 -0.518069 -0.689476 11.00000 -1.20000 AFIX 0 C10A 1 -0.728108 -0.319454 0.192289 11.00000 0.02135 0.04311 = 0.02569 0.00559 0.00407 0.01155 AFIX 43 H10A 2 -0.793130 -0.261368 0.212898 11.00000 -1.20000 AFIX 0 C10B 1 -0.201378 -0.446739 -0.549357 11.00000 0.03646 0.04305 = 0.02741 -0.00213 0.00367 0.02171 AFIX 43 H10B 2 -0.133650 -0.501518 -0.571114 11.00000 -1.20000 AFIX 0 C11A 1 -0.585935 -0.260035 0.166331 11.00000 0.02168 0.02647 = 0.02624 0.00711 0.00286 0.00728 AFIX 43 H11A 2 -0.553842 -0.161386 0.169392 11.00000 -1.20000 AFIX 0 C11B 1 -0.172883 -0.357394 -0.447603 11.00000 0.02573 0.03576 = 0.02534 0.00203 0.00031 0.01516 AFIX 43 H11B 2 -0.085921 -0.351257 -0.399823 11.00000 -1.20000 AFIX 0 CL 5 0.229778 -0.256013 -0.122658 11.00000 0.01777 0.01928 = 0.02351 0.00534 0.00553 0.00990 O1 4 0.154301 -0.165117 -0.061703 11.00000 0.03428 0.02823 = 0.02540 0.00259 0.00769 0.02060 O2 4 0.176072 -0.281638 -0.233948 11.00000 0.03155 0.04108 = 0.02217 0.00183 0.00573 0.01668 O3 4 0.390809 -0.191367 -0.101169 11.00000 0.01620 0.08360 = 0.04401 0.02323 0.00465 0.00837 O4 4 0.190870 -0.388206 -0.094205 11.00000 0.07067 0.02349 = 0.05652 0.01670 0.01242 0.02330 DFIX 0.85 0.01 O5 H5 C12 1 0.676538 0.000080 0.372252 11.00000 0.03042 0.04177 = 0.03467 0.00605 0.00049 0.01337 AFIX 23 H12A 2 0.690688 -0.064870 0.306732 11.00000 -1.20000 H12B 2 0.593140 -0.054911 0.402996 11.00000 -1.20000 AFIX 0 C13 1 0.822222 0.049402 0.450256 11.00000 0.02754 0.04914 = 0.03609 0.01589 0.00122 0.01387 AFIX 23 H13A 2 0.849640 -0.034985 0.462417 11.00000 -1.20000 H13B 2 0.906182 0.103066 0.419182 11.00000 -1.20000 AFIX 0 C14 1 0.809502 0.142162 0.554860 11.00000 0.05104 0.08274 = 0.03165 0.00164 -0.00133 0.01091 AFIX 137 H14A 2 0.906706 0.169628 0.602880 11.00000 -1.50000 H14B 2 0.726867 0.089579 0.586286 11.00000 -1.50000 H14C 2 0.786613 0.227942 0.543825 11.00000 -1.50000 AFIX 0 O5 4 0.630907 0.113745 0.344738 11.00000 0.02465 0.05719 = 0.03990 0.02474 0.00820 0.02051 H5 2 0.694984 0.163874 0.315658 11.00000 -1.50000 HKLF 4 REM EL50D in P-1 REM R1 = 0.0362 for 4106 Fo > 4sig(Fo) and 0.0470 for all 4829 data REM 296 parameters refined using 3 restraints END WGHT 0.0326 1.1077 REM Instructions for potential hydrogen bonds EQIV $1 -x, -y-1, -z HTAB N1A O4_$1 EQIV $2 -x, -y, -z HTAB N1B O5_$2 HTAB C2A O1 HTAB C2B O1_$2 HTAB C4B O2 EQIV $3 -x+1, -y, -z HTAB O5 Cl_$3 HTAB O5 O2_$3 REM Highest difference peak 0.382, deepest hole -0.456, 1-sigma level 0.064 Q1 1 0.2822 -0.3668 -0.0794 11.00000 0.05 0.38 Q2 1 -0.4302 -0.3111 0.1159 11.00000 0.05 0.38 Q3 1 -0.0741 -0.0846 0.0358 11.00000 0.05 0.38 Q4 1 -0.1224 -0.1019 -0.1815 11.00000 0.05 0.37 Q5 1 -0.5253 -0.4073 0.1257 11.00000 0.05 0.32 Q6 1 -0.2594 -0.2317 -0.3647 11.00000 0.05 0.31 Q7 1 -0.1580 -0.1415 -0.2881 11.00000 0.05 0.31 Q8 1 -0.1869 -0.0225 -0.1592 11.00000 0.05 0.30 Q9 1 0.7811 0.2058 0.5174 11.00000 0.05 0.29 Q10 1 -0.3167 -0.2504 -0.4595 11.00000 0.05 0.29 ; _shelx_res_checksum 11141 _shelx_hkl_file ; 0 0 3 116752. 1977.03 3 0 0 3 116473. 1966.05 4 0 0 4 117793. 2044.24 3 0 0 4 116092. 2035.75 4 0 0 5 7634.39 316.477 3 0 0 6 10952.1 426.432 3 0 0 7 15691.1 558.376 3 0 0 8 15030.1 579.855 3 0 0 -9 24310.9 767.981 4 0 0 9 24244.4 808.618 3 0 0 10 773.032 170.149 3 0 0 11 936.192 146.268 6 0 0 11 1235.45 202.246 3 0 0 12 536.886 164.971 3 0 0 13 2153.85 226.684 2 0 0 13 3101.99 338.599 3 0 0 14 2058.87 301.039 3 0 0 14 1654.87 210.469 2 0 0 15 2656.86 360.364 3 0 0 15 2104.25 247.622 2 0 0 16 8339.03 503.329 2 0 -1 16-86.8012 134.195 3 0 -1 15 1001.46 216.909 3 0 -1 15 726.495 146.508 2 0 -1 14 2040.30 212.975 2 0 -1 14 2103.82 301.213 3 0 -1 13 5031.35 323.010 2 0 -1 13 5097.60 429.971 3 0 -1 12 1301.46 211.135 3 0 -1 12 1435.09 173.740 6 0 -1 12 1460.85 170.970 2 0 -1 11 5102.64 294.068 2 0 -1 11 5465.73 396.610 3 0 -1 11 5196.02 313.527 6 0 -1 10 7093.74 426.207 3 0 -1 10 6867.95 345.875 6 0 -1 9 21260.9 633.903 6 0 1 -9 21740.8 708.282 4 0 -1 9 21134.6 734.047 3 0 -1 8-14.4394 57.9945 6 0 -1 8-34.1416 95.9870 3 0 -1 8-152.902 109.559 4 0 -1 7 4313.36 267.286 3 0 -1 7 4238.26 262.419 4 0 -1 7 4576.92 230.231 6 0 -1 6 2094.23 143.265 6 0 -1 6 2393.56 186.362 3 0 -1 6 2238.59 179.322 4 0 -1 5 5698.34 220.846 6 0 -1 5 5727.07 257.740 4 0 -1 5 5653.78 257.036 3 0 -1 4 67652.3 1265.75 4 0 -1 4 70996.8 1280.65 3 0 -1 4 67520.4 1205.51 6 0 -1 3 66231.3 1118.69 6 0 -1 3 63622.5 1162.68 4 0 -1 3 67137.5 1171.45 3 0 1 2 23600.0 505.407 3 0 1 3 162628. 2705.88 3 0 1 4 28931.6 689.197 3 0 1 5 625.669 109.311 3 0 1 6 44369.4 1046.02 3 0 1 7 18465.4 626.038 3 0 -1 -8 12017.7 496.704 4 0 1 8 12008.2 516.930 3 0 1 9 2522.13 255.524 3 0 -1 -9 2313.42 227.264 4 0 1 10 12067.1 587.852 3 0 1 11 670.801 164.179 3 0 1 12 8994.78 563.063 3 0 1 13 5632.86 466.668 3 0 1 14 8269.93 588.153 3 0 1 14 6279.10 432.195 2 0 1 15 1606.34 238.398 2 0 1 15 1769.31 309.305 3 0 1 16 4025.04 366.733 2 0 -2 16-234.148 181.764 3 0 -2 15 743.170 197.105 3 0 -2 15 1028.24 149.335 2 0 -2 14 790.716 203.632 3 0 -2 14 1101.55 148.048 2 0 -2 13 12405.9 654.725 3 0 -2 13 11770.6 462.333 2 0 -2 12 3393.48 254.132 6 0 -2 12 3169.28 223.595 2 0 -2 12 2879.55 303.777 3 0 -2 11 20451.7 650.443 6 0 -2 11 20910.6 592.325 2 0 -2 11 18774.2 755.553 3 0 -2 10 993.885 127.727 6 0 -2 10 855.718 151.559 4 0 -2 10 965.136 170.009 3 0 -2 10 885.197 107.182 2 0 2 -10 1032.78 155.490 4 0 -2 9 1206.30 128.798 6 0 -2 9 1182.27 173.158 3 0 -2 9 1015.19 101.686 2 0 -2 9 1117.81 160.284 4 0 2 -9 1333.27 163.348 4 0 -2 8 3659.91 210.645 6 0 -2 8 3360.44 251.894 3 0 -2 8 3813.89 180.223 2 0 -2 8 3079.83 238.660 4 0 -2 7 10584.8 418.945 4 0 -2 7 11123.6 432.609 3 0 -2 7 11016.2 362.216 6 0 -2 7 11110.1 307.230 2 0 -2 6 56506.9 979.633 2 0 -2 6 54831.3 1064.03 6 0 -2 6 53435.2 1154.36 4 0 -2 6 56464.9 1168.47 3 0 -2 5 28066.3 587.529 6 0 -2 5 29327.0 670.414 3 0 -2 5 29565.0 677.900 4 0 2 -4 9399.75 252.713 6 0 -2 4 9844.18 304.127 3 0 -2 4 8948.06 247.650 6 0 -2 4 9274.98 304.547 4 0 -2 3 19889.8 464.454 4 0 -2 3 20504.5 443.381 3 0 2 -3 20610.2 409.076 6 0 -2 2 11847.0 293.532 4 0 -2 1 40131.8 716.281 1 0 -2 0 24233.3 482.188 1 0 2 0 23646.5 435.687 3 0 -2 -1 176416. 2861.67 5 0 2 1 176735. 2822.77 3 0 2 2 1570.76 108.954 3 0 2 3 53267.4 1054.95 3 0 2 4 6705.76 295.380 3 0 2 5 137887. 2485.22 3 0 2 6 60449.8 1336.95 3 0 -2 -7 31914.4 884.855 4 0 -2 -7 32372.7 892.460 3 0 2 7 32742.5 911.283 3 0 -2 -8 1407.39 176.655 3 0 -2 -8 1530.12 180.525 4 0 2 8 1587.75 195.873 3 0 2 9 710.336 157.443 3 0 2 10 465.297 140.938 3 0 2 11 9024.70 546.301 3 0 2 12 1505.27 260.042 3 0 2 13 7844.34 558.877 3 0 2 14 4019.76 373.052 2 0 2 14 5369.38 490.458 3 0 2 15 1583.14 296.708 3 0 2 15 1458.78 235.538 2 0 2 16-27.3470 113.862 2 0 -3 16 1631.77 272.674 3 0 -3 15 5452.69 470.849 3 0 -3 14 10188.1 611.068 3 0 -3 14 9572.84 370.752 2 0 -3 13 1665.03 182.349 6 0 -3 13 1597.56 145.049 2 0 -3 13 1709.73 251.859 3 0 -3 12 4600.39 286.003 6 0 -3 12 4060.71 343.519 4 0 -3 12 4540.68 225.850 2 0 -3 12 4444.96 363.777 3 0 -3 11 1944.98 138.000 2 0 -3 11 1901.15 172.304 6 0 -3 11 1593.16 209.647 4 0 -3 11 1737.47 224.108 3 0 -3 10 570.349 127.414 4 0 3 -10 727.759 132.227 4 0 -3 10 709.866 138.711 3 0 -3 10 894.711 89.3592 2 0 -3 10 943.011 121.583 6 0 -3 9 17931.4 637.794 3 0 3 -9 18362.8 632.204 4 0 -3 9 16480.5 613.930 4 0 -3 9 17866.6 525.338 6 0 -3 9 16939.1 407.889 2 0 -3 8 35656.3 908.159 3 0 3 -8 36748.6 914.787 4 0 -3 8 34596.4 901.781 4 0 -3 8 34346.8 770.238 6 0 3 -7 71411.6 1319.76 4 0 -3 7 70587.8 1306.23 3 0 -3 7 66133.3 1146.65 6 0 -3 7 67608.0 1299.84 4 0 3 -6 21060.8 589.270 4 0 3 -6 20798.3 497.059 6 0 -3 6 20830.3 496.721 6 0 -3 6 20987.3 584.437 4 0 -3 6 21554.0 582.016 3 0 3 -5 7075.01 231.550 6 0 3 -5 7065.98 286.258 4 0 -3 5 7098.64 288.532 4 0 -3 5 7545.27 280.410 3 0 -3 4 5131.75 223.540 4 0 3 -4 4844.90 217.538 4 0 3 -4 4720.49 172.177 6 0 -3 4 5016.81 200.063 3 0 3 -3 18677.1 452.812 1 0 -3 3 20185.7 474.860 4 0 3 -3 19817.1 475.550 4 0 3 -2 70528.1 1264.80 1 0 -3 2 74772.5 1282.99 4 0 -3 1 2545.12 128.697 1 0 3 -1 2739.13 134.151 1 0 -3 0 1029.00 92.2804 1 0 -3 0 1051.71 67.5080 3 0 -3 -1 125.943 41.3725 3 0 3 1 31.8491 34.4521 3 0 -3 -1 111.247 44.6316 5 0 3 2 2896.92 158.151 3 0 -3 -2 3042.49 172.872 5 0 -3 -2 2821.22 152.251 3 0 3 3 1190.89 119.055 3 0 -3 -3 966.970 104.254 3 0 3 4 970.686 118.042 3 0 -3 -4 803.301 103.732 3 0 3 5 28774.1 780.045 3 0 -3 -6 7765.44 373.955 3 0 3 6 7998.33 392.810 3 0 3 7 3094.39 262.738 3 0 -3 -7 3004.02 248.874 3 0 -3 -7 3334.72 259.345 4 0 3 8 17471.6 683.702 3 0 -3 -8 18002.5 669.382 3 0 -3 -8 17984.7 663.306 4 0 3 9 13415.9 621.646 3 0 3 10 31960.9 1069.54 3 0 3 11 20509.5 864.632 3 0 3 12 1600.26 243.987 3 0 3 13 152.568 160.352 3 0 3 14 430.869 177.842 3 0 3 14 311.402 129.131 2 0 3 15 121.099 138.741 2 0 -4 16 9784.32 662.652 3 0 -4 15 1588.77 280.617 3 0 -4 14 373.526 159.005 3 0 -4 13-29.4986 116.196 3 0 -4 13-16.4800 31.9773 2 0 -4 13 58.0838 111.292 4 0 -4 13-29.9477 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48.2485 34.2655 2 -2 6 -5 17.6772 40.5182 1 2 -6 6 10419.3 443.150 4 -2 6 -6 7936.36 196.367 6 2 -6 7 33996.4 945.444 4 2 -6 8 105038. 2156.26 4 2 -6 9 26263.4 814.452 3 2 -6 9 26744.6 864.566 4 2 -6 10 10491.6 506.988 3 2 -6 10 10899.8 541.099 4 2 -6 11 226.815 120.403 4 2 -6 11 166.567 92.2263 3 2 -6 12 129.768 109.899 4 2 -6 12 247.928 121.458 3 2 -6 13-130.668 136.463 4 2 -6 13-153.627 123.191 3 2 -6 14 2330.86 302.942 4 2 -6 14 2112.08 287.309 3 2 -6 15 3902.75 412.728 4 2 -6 15 3573.70 381.357 3 2 -6 16 2282.50 322.124 3 -2 5 13 158.074 129.347 3 -2 5 13 257.129 147.017 2 -2 5 12 4336.52 424.006 3 -2 5 12 4279.39 409.465 2 -2 5 11 3019.93 346.785 3 -2 5 11 2812.95 331.996 2 -2 5 10 6454.58 465.440 2 -2 5 10 6626.57 489.000 3 -2 5 9 3402.32 330.325 3 -2 5 9 3769.64 351.647 2 -2 5 8 1686.28 224.928 2 -2 5 8 2035.27 243.911 3 -2 5 7 76.0035 116.841 2 2 -5 -7 172.899 83.4008 3 -2 5 7 99.0695 86.1313 3 -2 5 6 578.805 135.477 2 -2 5 6 470.595 120.109 3 2 -5 -6 735.511 128.326 5 2 -5 -6 660.650 130.225 3 -2 5 5 9218.46 468.214 2 2 -5 -5 9659.32 399.398 5 -2 5 5 9840.43 458.682 3 2 -5 -5 9695.89 452.024 3 -2 5 4 768.530 131.562 3 2 -5 -4 807.223 109.732 5 -2 5 4 803.017 151.048 2 -2 5 3 12634.4 499.156 2 2 -5 -3 12573.2 419.919 5 2 -5 -2 47269.4 1074.97 3 -2 5 2 46910.2 1096.25 2 2 -5 -1 58156.6 1205.81 3 -2 5 1 58824.2 1232.20 2 -2 5 1 55758.9 1116.53 5 2 -5 0 2642.11 124.685 1 -2 5 0 2433.14 151.521 5 -2 5 0 3086.55 202.598 2 2 -5 0 2567.44 183.320 3 2 -5 1 257.621 44.7736 1 -2 5 -1 511.726 94.1294 2 -2 5 -2 4847.54 221.511 2 -2 5 -3 127.267 50.2107 2 -2 5 -3 80.7650 27.0524 1 2 -5 4 35657.6 867.822 4 -2 5 -4 34833.6 682.227 2 -2 5 -4 34760.1 681.295 1 2 -5 5 18526.0 579.240 4 -2 5 -5 17397.4 371.684 2 2 -5 6 11488.9 460.253 4 2 -5 7 50930.6 1215.58 4 2 -5 8 461.346 125.556 4 -2 5 -8 386.721 118.197 4 2 -5 9-37.2350 107.742 4 2 -5 9-61.4647 95.4349 3 2 -5 10 389.611 121.067 4 2 -5 10 579.746 142.204 3 2 -5 11 2987.09 287.323 3 2 -5 11 2710.69 287.284 4 2 -5 12 13487.9 642.296 3 2 -5 12 14340.4 681.583 4 2 -5 13 163.010 127.577 4 2 -5 13-62.7985 120.048 3 2 -5 14 4523.98 417.100 3 2 -5 14 5398.37 457.645 4 2 -5 15 7174.26 552.364 4 2 -5 15 7400.48 547.827 3 2 -5 16 3610.39 406.913 3 -2 4 14 3059.51 390.003 3 -2 4 14 2762.21 346.652 2 -2 4 13 3135.87 372.686 3 -2 4 13 3346.40 365.859 2 -2 4 12 9766.82 587.710 2 -2 4 12 9877.05 635.605 3 -2 4 11 10992.3 636.603 3 -2 4 11 10422.1 586.593 2 -2 4 10 292.371 123.345 3 -2 4 10 314.361 118.024 2 -2 4 9-162.091 141.547 2 -2 4 9-16.2644 123.696 3 -2 4 8 20.1027 107.823 3 -2 4 8 8.76323 98.1823 2 -2 4 7 85.9393 89.4876 2 -2 4 7 227.739 106.510 3 2 -4 -7 313.133 92.1708 3 2 -4 -6 16858.0 625.653 3 -2 4 6 15780.2 609.838 2 -2 4 6 16810.9 626.111 3 -2 4 5 12174.3 501.416 2 2 -4 -5 12234.2 502.319 3 -2 4 5 12464.5 499.772 3 -2 4 4 13508.2 506.817 2 -2 4 4 13003.9 487.504 3 2 -4 -3 45958.0 1064.85 3 2 -4 -3 45953.1 944.135 5 -2 4 3 48719.3 1082.58 3 -2 4 3 45700.3 1066.88 2 2 -4 -2 39564.3 920.639 3 -2 4 2 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465.765 3 2 -4 13 14553.3 703.326 3 2 -4 13 14775.2 716.925 4 2 -4 14 6806.46 507.660 4 2 -4 14 6389.85 491.928 3 2 -4 15 7849.68 572.818 3 2 -4 15 8506.49 597.587 4 2 -4 16-13.7888 127.208 3 -2 3 16 6053.21 494.868 2 -2 3 15 4992.56 445.553 2 -2 3 14 2128.20 286.521 2 -2 3 14 2277.24 338.994 3 -2 3 13 1834.51 284.258 3 -2 3 13 859.941 190.905 2 -2 3 12-170.481 149.768 2 -2 3 12 32.4160 116.853 3 -2 3 11 6817.06 487.389 3 -2 3 11 5792.07 411.778 2 -2 3 10 1618.06 218.708 2 -2 3 10 1714.16 238.301 3 -2 3 9 9399.00 487.797 2 -2 3 9 9116.76 520.584 3 2 -3 -8 30879.1 945.785 3 -2 3 8 30197.0 954.006 3 -2 3 8 29062.2 900.382 2 -2 3 7 18470.9 679.962 3 -2 3 7 18181.9 651.163 2 2 -3 -7 19619.4 688.426 3 -2 3 6 30370.3 850.339 2 -2 3 6 31271.7 884.087 3 -2 3 5 6496.84 339.484 3 -2 3 5 6566.54 333.041 2 -2 3 4 43509.1 1007.09 2 -2 3 4 43274.9 1009.94 3 -2 3 3 41191.4 941.867 3 -2 3 3 39957.9 920.994 2 2 -3 -2 13017.5 324.268 5 -2 3 2 13554.4 426.911 2 -2 3 1 12905.8 394.008 2 -2 3 0 12374.3 361.582 2 -2 3 -1 21762.4 495.383 2 2 -3 1 21376.2 502.195 2 -2 3 -2 22146.8 468.104 2 2 -3 2 23212.8 485.512 2 2 -3 3 29998.3 593.466 2 2 -3 3 30387.1 704.547 4 -2 3 -3 29912.9 583.949 2 2 -3 4 27963.9 680.778 4 2 -3 4 26584.8 535.138 2 2 -3 5 38.7288 64.9847 4 2 -3 5 45.3007 28.8840 2 2 -3 6 19629.4 593.680 4 2 -3 6 17979.6 385.556 6 2 -3 6 18991.8 420.019 2 2 -3 7 620.363 119.040 4 2 -3 7 550.985 62.8412 6 2 -3 8 2040.67 128.850 6 2 -3 8 2114.47 206.510 4 2 -3 8 2036.70 204.005 3 2 -3 9 5068.29 339.294 4 2 -3 9 4516.97 320.638 3 2 -3 9 4565.32 216.048 6 -2 3 -9 4789.45 317.100 4 2 -3 10 9322.30 348.808 6 2 -3 10 9706.89 497.429 3 2 -3 10 9947.26 502.472 4 2 -3 11 3631.17 321.806 3 2 -3 11 3107.34 206.262 6 2 -3 11 3841.76 332.467 4 2 -3 12 1903.82 253.928 3 2 -3 12 1689.82 160.983 6 2 -3 12 1787.50 245.385 4 2 -3 13 3686.74 250.889 6 2 -3 13 4147.73 384.229 4 2 -3 13 3965.08 370.599 3 2 -3 14 6130.26 489.913 3 2 -3 14 5763.58 473.987 4 2 -3 15 1584.59 269.886 3 -2 2 16 41.5958 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1761.66 4 2 -1 7 10110.8 425.751 4 2 -1 7 9891.16 437.521 3 2 -1 8 290.144 100.285 3 -2 1 -8 140.484 59.6021 4 2 -1 8 395.993 107.021 4 -2 1 -9 313.516 86.0906 4 2 -1 9 282.320 115.723 4 2 -1 9 405.518 121.830 3 2 -1 10 1108.73 187.166 3 2 -1 10 1008.14 175.016 4 2 -1 11 15791.1 701.754 3 2 -1 11 15550.7 686.807 4 2 -1 12 8882.34 542.546 3 2 -1 13 6357.46 486.440 3 2 -1 14 607.723 183.415 3 2 -1 15-221.406 160.445 3 -2 0 16 47.3063 86.7689 2 -2 0 16-106.701 163.201 3 -2 0 15 3454.02 309.107 2 -2 0 15 4361.67 446.849 3 -2 0 14 12561.8 724.349 3 -2 0 14 10576.1 526.493 2 -2 0 13 2975.29 344.075 3 -2 0 13 2472.31 241.337 2 -2 0 12 21013.8 721.294 2 -2 0 12 19886.1 855.314 3 -2 0 11 6903.60 375.150 2 -2 0 11 6399.94 448.601 3 -2 0 10 13392.4 551.044 6 -2 0 10 12515.5 598.793 3 -2 0 10 13236.9 515.995 2 -2 0 9 139.699 79.5822 2 2 0 -9 394.921 109.425 3 -2 0 9 380.451 125.071 3 -2 0 9 345.510 105.319 6 2 0 -9 550.598 116.553 4 2 0 -8 3829.49 276.200 3 2 0 -8 4724.95 302.005 4 -2 0 8 4139.75 248.127 2 -2 0 8 4025.88 293.414 3 -2 0 8 4345.85 274.911 6 -2 0 7-18.5923 66.6950 2 -2 0 7 156.795 74.0777 6 -2 0 7 12.3100 81.7732 3 -2 0 6 41483.6 902.109 2 -2 0 6 40680.9 990.126 3 -2 0 6 41482.4 952.775 6 2 0 -5 483.895 90.7808 2 -2 0 5 443.945 83.6205 2 -2 0 5 487.333 96.0583 6 -2 0 5 519.411 107.899 3 -2 0 4 50727.6 1033.16 6 -2 0 4 51067.9 996.883 2 -2 0 4 51819.9 1059.47 3 2 0 -4 52036.5 1008.97 2 -2 0 3 84305.5 1524.45 6 -2 0 3 84462.3 1492.36 2 -2 0 3 89677.1 1557.26 3 2 0 -3 84976.9 1500.39 2 -2 0 2 24674.1 542.158 6 -2 0 2 24773.4 528.731 2 -2 0 1 1265.17 89.1995 1 -2 0 1 1164.19 87.8830 2 -2 0 0 275958. 4332.73 5 -2 0 0 277287. 4366.16 1 2 0 1 3467.99 124.410 4 -2 0 -1 3345.85 157.532 1 2 0 2 143371. 2336.65 4 -2 0 -3 43935.6 870.404 4 2 0 3 46432.0 879.402 4 -2 0 -4 58222.4 1156.42 4 2 0 4 62894.3 1177.93 4 -2 0 -5 101338. 1874.29 4 2 0 5 104884. 1894.96 4 2 0 6 24869.6 685.259 4 2 0 6 23600.9 693.013 3 2 0 7 15916.5 560.847 4 -2 0 -7 15938.7 540.194 4 2 0 7 15515.6 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7 5800.92 420.683 3 -3 7 7 6175.90 452.745 2 3 -7 -7 6185.95 380.749 5 -3 7 6 29811.8 1034.32 2 3 -7 -6 31415.0 898.863 5 3 -7 -5 31491.3 984.485 3 -3 7 5 31080.0 1024.68 2 3 -7 -5 32114.3 876.458 5 3 -7 -4 4830.78 340.324 3 -3 7 4 4512.41 357.656 2 -3 7 3 51.8741 98.7505 2 3 -7 -3 102.600 68.7494 3 3 -7 -2 2002.21 207.772 3 -3 7 2 2108.44 223.674 2 3 -7 -1 335.345 68.2764 1 -3 7 1 176.071 95.1926 2 3 -7 0 106.203 43.1948 1 -3 7 0 121.999 62.1932 5 -3 7 0 118.844 85.7283 2 3 -7 1 2605.84 113.935 1 -3 7 -1 2682.62 217.373 2 -3 7 -1 2790.67 191.704 5 -3 7 -2 25817.0 711.726 2 -3 7 -3 17852.8 538.970 2 3 -7 4 6035.59 353.633 4 -3 7 -4 6352.59 274.064 2 3 -7 5 12302.2 527.807 4 -3 7 -5 12796.3 376.611 2 -3 7 -5 11763.4 311.910 1 3 -7 6 9590.16 468.741 4 -3 7 -6 9401.70 297.913 1 -3 7 -6 9376.11 282.852 2 3 -7 7 2595.62 259.028 4 3 -7 8 5881.36 384.739 4 3 -7 9 142.724 104.155 4 3 -7 10 6411.21 432.836 4 3 -7 11 18135.3 768.087 4 3 -7 11 16615.2 703.960 3 3 -7 12 8482.12 529.329 4 3 -7 12 7921.49 496.750 3 3 -7 13 85.4991 121.081 4 3 -7 13 178.505 142.019 3 3 -7 14 656.162 186.159 4 3 -7 14 958.599 203.697 3 3 -7 15 1227.20 236.839 3 -3 6 12 3364.13 406.871 3 -3 6 12 3505.78 397.647 2 -3 6 11-7.84416 146.372 2 -3 6 11 193.751 127.782 3 -3 6 10 4.49236 119.819 2 -3 6 10 235.369 157.278 3 -3 6 9 1790.13 267.168 2 -3 6 9 2020.60 272.713 3 -3 6 8 5630.52 425.259 3 -3 6 8 5230.71 416.368 2 3 -6 -8 5999.84 368.875 5 -3 6 7 19014.4 783.380 3 -3 6 7 18474.4 773.527 2 3 -6 -7 19043.6 657.502 5 -3 6 6 3956.97 328.040 3 3 -6 -6 3580.98 256.053 5 -3 6 6 3698.35 331.016 2 3 -6 -5 37336.2 1071.41 3 -3 6 5 35386.3 1068.92 2 3 -6 -5 36747.9 919.108 5 -3 6 4 51.0092 92.6157 2 3 -6 -4 143.940 69.0697 5 3 -6 -4 155.386 78.1176 3 3 -6 -3 15856.7 606.333 3 -3 6 3 15927.1 614.766 2 -3 6 2 99.4158 85.4274 2 -3 6 1 200.409 90.3590 2 -3 6 0 810.857 96.6632 5 3 -6 0 724.801 62.5567 1 -3 6 0 748.010 119.439 2 -3 6 -1 945.422 126.391 2 -3 6 -2 44925.1 992.921 2 -3 6 -3 6565.13 278.704 2 3 -6 4 72.7225 88.4193 4 -3 6 -4 66.3631 27.6359 1 -3 6 -4 61.7978 54.8258 2 3 -6 5 702.539 136.078 4 -3 6 -5 858.332 85.1461 2 3 -6 6 2402.91 234.902 4 3 -6 7 1685.68 198.895 4 3 -6 8 12025.6 547.883 4 3 -6 9 10951.7 542.013 4 3 -6 10 15855.1 682.465 4 3 -6 11 30767.0 1028.32 4 3 -6 11 29304.0 988.849 3 3 -6 12 2886.54 305.123 3 3 -6 12 3122.62 327.235 4 3 -6 13 1290.69 228.173 4 3 -6 13 1420.03 228.930 3 3 -6 14 1348.40 241.158 4 3 -6 14 1334.74 234.604 3 3 -6 15 7.20100 150.199 4 3 -6 15-6.48281 141.703 3 -3 5 13 112.857 127.287 2 -3 5 13 20.1881 141.596 3 -3 5 12-61.3197 166.952 2 -3 5 12-252.428 175.019 3 -3 5 11 1053.98 211.618 3 -3 5 11 1115.44 210.077 2 -3 5 10 10007.0 601.436 3 -3 5 10 9849.62 580.491 2 -3 5 9 23395.4 912.464 3 -3 5 9 22970.0 894.514 2 -3 5 8 20228.3 806.585 3 -3 5 8 19106.7 778.784 2 -3 5 7 153.768 107.159 3 -3 5 7-53.0133 109.890 2 -3 5 6 5700.33 382.823 3 3 -5 -6 6440.92 395.686 3 -3 5 6 5701.27 379.316 2 -3 5 5 3999.07 297.393 3 3 -5 -5 4639.75 321.882 3 -3 5 5 4184.05 307.891 2 3 -5 -5 4470.08 242.788 5 -3 5 4 87.9657 100.289 2 3 -5 -4-15.7318 76.1190 3 3 -5 -4 28.7692 48.0506 5 -3 5 3 2583.04 229.374 2 3 -5 -3 2545.20 156.936 5 -3 5 2 5256.36 310.900 2 -3 5 1 66017.6 1371.70 2 3 -5 -1 63854.9 1388.08 3 -3 5 0 14492.4 467.083 2 -3 5 0 13177.9 346.618 5 -3 5 -1 30879.1 748.728 2 -3 5 -2 17027.0 479.361 2 3 -5 2 16194.7 484.647 2 3 -5 3 31.6224 41.8347 2 -3 5 -3 74.0976 27.9355 6 -3 5 -3 139.256 54.3160 2 3 -5 4 451.662 73.2567 2 -3 5 -4 371.743 64.0229 2 3 -5 4 325.059 89.6636 4 3 -5 5 583.254 73.8431 2 3 -5 5 536.052 113.576 4 -3 5 -5 470.440 63.5847 2 3 -5 6 1345.03 168.267 4 3 -5 6 1508.59 107.957 2 3 -5 7 16955.7 622.619 4 3 -5 7 17105.1 417.520 2 3 -5 8 33077.1 947.187 4 3 -5 8 30042.7 629.792 2 3 -5 9 8495.66 456.073 4 3 -5 9 7193.77 236.861 2 3 -5 10 4202.31 334.811 4 3 -5 10 3511.05 159.264 2 3 -5 11 196.387 129.050 4 3 -5 11 384.007 56.1457 2 3 -5 11 291.736 123.749 3 3 -5 12 5744.84 434.033 4 3 -5 12 5552.79 416.978 3 3 -5 13 3645.89 370.040 4 3 -5 13 3529.28 353.143 3 3 -5 14 7338.21 533.373 3 3 -5 14 7570.17 549.300 4 3 -5 15 9358.76 628.966 3 3 -5 15 8382.73 611.435 4 -3 4 14-165.283 168.050 2 -3 4 14 81.5434 121.714 3 -3 4 13 644.792 173.237 2 -3 4 13 821.470 206.319 3 -3 4 12 1023.75 196.614 2 -3 4 12 1004.49 213.074 3 -3 4 11 7786.97 512.644 2 -3 4 11 7158.41 520.944 3 -3 4 10 27306.9 1013.49 3 -3 4 10 27539.4 981.684 2 -3 4 9 16869.8 743.852 3 -3 4 9 17171.6 724.044 2 -3 4 8 1485.34 208.733 2 -3 4 8 988.587 186.577 3 -3 4 7 5832.20 387.988 3 -3 4 7 5943.32 384.309 2 3 -4 -7 6675.83 411.878 3 -3 4 6 6242.70 379.857 3 3 -4 -6 6341.24 387.714 3 -3 4 6 5982.43 370.539 2 3 -4 -5 3567.99 272.202 3 -3 4 5 3035.15 251.239 2 -3 4 5 3003.36 260.867 3 -3 4 4 15015.8 558.200 3 -3 4 4 15209.7 553.517 2 3 -4 -3 15478.1 395.805 5 -3 4 3 15593.0 535.526 2 -3 4 2 99920.4 1903.35 2 -3 4 1 56798.0 1190.65 2 3 -4 0 77265.9 1493.95 2 -3 4 0 74580.1 1400.11 6 3 -4 1 612.651 89.4958 2 -3 4 -1 488.417 86.0101 2 -3 4 -1 555.795 67.5138 6 -3 4 -2 52159.5 1021.12 2 3 -4 2 53007.7 1049.98 2 -3 4 -2 51173.8 909.505 6 3 -4 3 749.883 116.558 4 3 -4 3 649.910 90.0849 2 -3 4 -3 588.866 82.1837 2 -3 4 -4 24317.7 544.440 2 3 -4 4 24651.6 682.212 4 3 -4 4 23572.0 557.893 2 3 -4 5 6935.86 341.123 4 3 -4 5 6691.16 245.586 2 3 -4 6 37561.3 955.429 4 3 -4 6 36720.8 759.073 2 3 -4 7 446.439 107.435 4 3 -4 7 404.864 63.8370 2 3 -4 8 393.257 41.6422 6 3 -4 8 530.366 129.052 4 -3 4 -8 774.759 135.038 4 3 -4 8 592.960 74.8941 2 3 -4 9 3021.81 271.606 4 3 -4 9 2891.63 164.169 2 3 -4 9 2900.99 137.796 6 3 -4 10 17.8767 35.2788 6 3 -4 10 113.498 96.1645 4 3 -4 10 80.1231 50.6821 2 3 -4 10-40.0838 91.8788 3 3 -4 11 892.156 181.798 4 3 -4 11 659.623 89.2718 2 3 -4 11 739.416 89.1165 6 3 -4 11 520.123 149.538 3 3 -4 12 405.184 75.5694 2 3 -4 12 671.643 179.701 4 3 -4 12 516.332 85.2244 6 3 -4 12 488.441 154.386 3 3 -4 13 17850.7 813.505 3 3 -4 13 18993.7 839.880 4 3 -4 14 9004.80 587.361 3 3 -4 14 8927.02 600.762 4 3 -4 15 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66035.7 1357.16 5 -4 -2 -1 62652.0 1379.53 1 -4 -2 -2 1704.47 180.767 1 -4 -2 -2 1953.80 176.477 5 -4 -2 -3 11860.1 344.228 4 -4 -2 -3 12414.4 508.893 1 -4 -2 -3 13062.8 485.992 5 -4 -2 -4 25676.3 626.406 4 -4 -2 -4 26116.3 821.012 1 -4 -2 -4 27221.1 781.040 5 -4 -2 -5 4245.18 230.625 4 -4 -2 -5 4094.34 317.311 1 -4 -2 -5 4119.64 289.249 5 4 2 6 24416.6 778.835 3 -4 -2 -7 23826.9 716.164 4 4 2 7 23791.9 805.793 3 -4 -2 -8 463.549 104.090 4 4 2 8 366.910 132.633 3 4 2 9 763.848 174.641 3 4 2 10 10569.6 592.304 3 4 2 11 4565.57 408.617 3 4 2 12 6084.35 501.005 3 4 2 13 1914.75 310.937 3 -4 -3 16 1144.30 230.318 3 -4 -3 15 6401.81 513.233 3 -4 -3 14 5369.87 305.291 2 -4 -3 14 4845.22 427.234 3 -4 -3 13 510.219 102.130 2 -4 -3 13 477.887 152.488 3 -4 -3 12 577.612 110.876 2 -4 -3 12 644.590 168.009 3 -4 -3 11 138.481 72.9584 2 -4 -3 11 11.0268 88.9430 3 4 3 -11 84.3250 95.8356 6 4 3 -10-26.5183 58.3049 2 4 3 -10 18.3509 66.9462 4 -4 -3 10-16.0456 91.8435 3 4 3 -10-15.2052 91.9048 6 -4 -3 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477.195 1 4 3 -1 12120.8 469.053 5 -4 -3 0 50941.3 1204.55 1 4 3 0 51797.7 1186.84 5 -4 -3 -1 69503.3 1531.18 1 -4 -3 -1 70758.3 1497.28 5 -4 -3 -2 15797.2 592.744 1 -4 -3 -2 17104.0 582.882 5 -4 -3 -3 10036.9 304.546 4 -4 -3 -3 10329.1 486.447 1 -4 -3 -3 11147.9 478.142 5 -4 -3 -4 1287.97 115.801 4 -4 -3 -4 1113.44 156.464 5 -4 -3 -4 1181.54 182.097 1 4 3 4 1331.40 154.687 3 -4 -3 -5 498.083 82.4470 4 -4 -3 -5 991.584 187.124 1 4 3 5 796.570 126.410 3 -4 -3 -6 4148.81 347.590 1 4 3 6 3676.13 287.934 3 -4 -3 -7 967.701 135.894 4 -4 -3 -7 1069.58 201.890 1 4 3 7 1155.94 175.490 3 -4 -3 -8 5015.65 323.107 4 4 3 8 5224.14 376.681 3 4 3 9 16768.6 736.578 3 4 3 10 2373.86 286.221 3 4 3 11-27.9081 109.422 3 4 3 12 1995.67 297.308 3 -4 -4 16 3791.17 404.719 3 -4 -4 15 5983.28 489.774 3 -4 -4 14 3837.81 375.279 3 -4 -4 13 258.878 129.874 3 -4 -4 12 1507.41 218.715 3 4 4 -12 1206.42 198.944 6 4 4 -11 273.895 78.3129 2 -4 -4 11 330.257 122.344 3 4 4 -11 154.993 106.786 6 4 4 -10 5239.49 334.335 4 -4 -4 10 4778.96 330.904 3 4 4 -10 4625.40 271.198 2 4 4 -10 4839.18 320.297 3 4 4 -10 4771.48 351.820 6 4 4 -9 3558.35 259.837 4 -4 -4 9 3535.91 270.117 3 4 4 -9 3850.10 235.645 2 4 4 -9 3223.17 277.725 6 4 4 -9 3399.55 248.796 3 4 4 -8 7475.46 347.420 4 4 4 -8 7246.33 343.549 3 4 4 -8 7037.98 323.320 2 -4 -4 8 7087.23 358.867 3 4 4 -8 6816.30 390.248 6 4 4 -7 4884.25 251.695 4 4 4 -7 4694.06 258.034 2 4 4 -7 4772.95 255.595 3 4 4 -7 4796.21 318.918 6 4 4 -6 1186.98 108.951 4 4 4 -6 1282.85 134.826 2 4 4 -6 1342.95 173.961 1 4 4 -6 1338.66 127.314 3 4 4 -6 1220.49 165.280 6 4 4 -5 10761.8 470.659 6 4 4 -5 10608.7 408.399 2 4 4 -5 10523.1 310.356 4 4 4 -5 10740.0 350.623 3 4 4 -5 10889.2 482.326 1 4 4 -4 1591.96 156.678 2 4 4 -4 1589.15 116.607 3 4 4 -4 1584.15 183.896 1 4 4 -3 5372.30 286.326 2 4 4 -3 5178.32 323.929 1 -4 -4 3 5346.46 327.404 1 4 4 -3 4540.15 192.047 3 4 4 -3 5111.37 322.611 5 4 4 -2 6263.26 361.889 1 4 4 -2 6175.34 225.469 3 -4 -4 2 6119.19 350.579 1 4 4 -2 6492.91 363.741 5 4 4 -1 8014.15 419.444 1 -4 -4 1 7540.74 396.612 1 4 4 -1 8068.57 406.789 5 -4 -4 0 42443.2 1099.48 1 4 4 0 42268.6 1087.80 5 -4 -4 -1 27732.4 854.900 1 -4 -4 -2 2508.40 249.804 1 -4 -4 -2 1926.68 97.7220 4 4 4 2 2506.97 175.706 3 -4 -4 -2 2376.06 221.614 5 -4 -4 -3 1336.07 100.852 4 -4 -4 -3 1180.83 186.844 1 4 4 3 1277.75 143.784 3 -4 -4 -4 1772.20 135.556 4 -4 -4 -4 1968.22 238.895 1 4 4 4 1760.70 176.184 3 -4 -4 -5 466.674 76.8286 4 -4 -4 -5 564.423 156.460 1 4 4 5 693.331 130.076 3 -4 -4 -6 5008.08 404.025 1 4 4 6 4687.94 324.734 3 -4 -4 -7 2838.99 228.797 4 4 4 7 2767.09 271.329 3 -4 -4 -7 3319.00 343.050 1 4 4 8 8271.53 502.296 3 -4 -4 -8 9308.62 603.049 1 -4 -4 -9 2922.11 351.284 1 4 4 9 3005.42 314.062 3 4 4 10 7.47500 113.058 3 4 4 11 1100.42 228.026 3 4 4 12 217.995 154.136 3 -4 -5 17 110.983 115.292 3 -4 -5 16 304.444 139.943 3 -4 -5 15 1441.14 224.887 3 -4 -5 14 887.133 192.145 3 -4 -5 13 6465.84 442.354 3 4 5 -13 6427.14 441.236 6 4 5 -12 9569.56 531.984 6 -4 -5 12 9902.01 520.970 3 -4 -5 11 5285.31 355.101 3 4 5 -11 5372.63 277.538 2 4 5 -11 4986.16 373.699 6 4 5 -10 3092.75 251.985 4 -4 -5 10 3052.09 260.050 3 4 5 -10 2910.38 205.190 2 4 5 -10 3056.81 284.604 6 4 5 -10 3543.39 257.286 3 4 5 -9 2004.25 191.952 4 -4 -5 9 1750.98 184.774 3 4 5 -9 1804.17 159.688 2 4 5 -9 1827.71 171.385 3 4 5 -9 1549.32 196.656 6 4 5 -8 35.2390 50.7834 4 4 5 -8-79.7473 116.283 6 4 5 -8 83.0117 55.8135 2 4 5 -8 35.7375 54.6467 3 4 5 -7 9365.74 354.149 4 4 5 -7 8842.40 367.548 2 4 5 -7 9316.20 463.218 6 4 5 -7 9331.32 340.445 3 4 5 -6 64.0662 42.9757 4 4 5 -6 218.755 106.434 6 4 5 -6 131.468 69.6134 2 4 5 -6 66.7620 43.8409 3 4 5 -5 243.295 77.2589 2 4 5 -5 179.457 43.8124 3 4 5 -4 51437.8 1112.48 2 4 5 -4 51748.2 1256.56 1 4 5 -3 104812. 1944.38 1 -4 -5 3 103492. 1899.97 1 4 5 -3 107547. 1945.01 5 4 5 -2 40344.5 1058.16 1 -4 -5 2 40389.8 1024.05 1 4 5 -2 41387.2 1059.34 5 4 5 -1 9196.42 465.468 5 -4 -5 1 9533.88 467.506 1 4 5 -1 8725.74 248.819 3 4 5 0 443.530 66.0808 3 4 5 0 407.758 118.154 5 4 5 1 4633.59 217.278 3 -4 -5 -1 4651.85 335.235 1 -4 -5 -2 2327.16 245.370 1 -4 -5 -2 1914.25 98.9198 4 4 5 2 2473.68 174.183 3 -4 -5 -3 938.882 89.4363 4 -4 -5 -3 962.378 183.543 1 4 5 3 987.141 128.533 3 -4 -5 -4 19849.2 535.724 4 -4 -5 -4 20947.5 815.339 1 4 5 4 21088.7 658.720 3 -4 -5 -5 1986.24 260.481 1 4 5 5 2211.27 219.442 3 -4 -5 -6 9531.26 406.725 4 -4 -5 -6 11487.8 628.251 1 4 5 6 10729.4 509.881 3 -4 -5 -7 3649.86 381.522 1 4 5 7 3373.95 301.738 3 -4 -5 -8 2556.58 329.062 1 4 5 8 2213.91 261.148 3 -4 -5 -9 900.153 225.740 1 4 5 9 619.685 165.609 3 4 5 10-13.7664 101.450 3 4 5 11 887.915 209.613 3 -4 -6 15 3145.75 336.879 3 -4 -6 14 2745.44 297.539 3 4 6 -14 2719.45 307.821 6 -4 -6 13 11652.5 584.354 3 4 6 -13 11363.5 604.158 6 -4 -6 12 4929.15 358.154 3 4 6 -12 4426.98 362.097 6 -4 -6 11 310.388 109.435 3 4 6 -11 127.988 110.536 6 4 6 -10-205.188 98.1713 4 4 6 -10-97.1334 111.901 6 4 6 -9-80.5674 79.0345 4 4 6 -9-85.5110 134.150 6 4 6 -8 1685.48 156.354 4 4 6 -8 1751.51 161.543 2 4 6 -8 1387.38 194.207 6 4 6 -7 19312.8 596.585 2 4 6 -7 19805.5 725.611 6 4 6 -6 19216.6 604.858 2 4 6 -6 19164.4 705.908 6 4 6 -5 10813.5 443.115 2 -4 -6 4 1914.46 228.422 1 4 6 -4 1593.16 225.088 5 4 6 -4 1542.49 166.377 2 -4 -6 3 2934.33 275.814 1 4 6 -3 2946.86 285.582 5 -4 -6 2 506.856 131.301 1 4 6 -2 225.451 121.920 5 -4 -6 1 4912.51 353.377 1 4 6 -1 5116.98 368.948 5 4 6 0 13040.3 331.569 3 -4 -6 0 15218.6 637.420 1 4 6 1 3653.06 183.818 3 -4 -6 -1 3467.37 313.655 1 -4 -6 -2 370.050 48.3246 4 4 6 2 657.176 98.7427 3 -4 -6 -2 490.533 145.670 1 -4 -6 -3 17013.6 723.391 1 4 6 3 16324.8 524.252 3 -4 -6 -4 875.637 191.650 1 4 6 4 617.173 122.471 3 -4 -6 -5 1457.41 240.955 1 4 6 5 1390.19 177.464 3 -4 -6 -6 61.6871 117.839 1 4 6 6 211.040 101.727 3 -4 -6 -7 256.656 127.642 1 4 6 7 220.126 105.967 3 -4 -6 -8 2092.72 327.309 1 4 6 8 1949.75 254.269 3 4 6 9 1383.17 225.139 3 4 7 -14 2185.98 281.782 6 4 7 -13 57.9633 100.153 6 4 7 -12-94.0372 132.314 6 4 7 -11-392.817 161.343 6 4 7 -10 8666.72 494.011 6 4 7 -9 15882.2 670.489 6 4 7 -8 8888.57 376.067 2 4 7 -8 8945.99 489.038 6 4 7 -7 18220.0 597.498 2 4 7 -7 19298.9 738.195 6 4 7 -6 4839.40 291.961 2 4 7 -5 4203.52 281.391 2 4 7 -5 5303.77 398.618 5 -4 -7 4 747.844 162.153 1 4 7 -4 744.817 168.039 5 4 7 -3 4610.72 379.386 5 -4 -7 3 5139.86 373.445 1 -4 -7 2 1881.98 229.747 1 4 7 -2 1791.29 242.675 5 -4 -7 1 307.635 124.567 1 4 7 -1 183.850 128.233 5 -4 -7 0 412.382 135.769 1 4 7 1 5301.36 199.739 3 -4 -7 -1 7352.26 464.714 1 4 7 2 18474.7 521.074 3 -4 -7 -2 21044.6 822.919 1 4 7 3 16150.1 534.015 3 -4 -7 -3 18797.8 792.019 1 -4 -7 -4 451.631 153.952 1 4 7 4 411.409 104.998 3 -4 -7 -5-180.943 136.362 1 -4 -7 -6-4.04698 135.421 1 -4 -7 -7 2157.72 316.801 1 4 8 -14 854.683 190.857 6 4 8 -13-93.4296 127.660 6 4 8 -12 144.812 130.476 6 4 8 -11 1456.92 215.495 6 4 8 -10 11101.3 579.438 6 4 8 -9 1367.09 207.076 6 4 8 -8 18057.2 742.326 6 4 8 -7 1087.89 185.124 6 4 8 -6 1875.38 189.910 2 4 8 -6 2709.12 305.695 5 4 8 -5-248.591 145.349 5 -4 -8 4 639.366 163.077 1 4 8 -4 650.310 197.447 5 -4 -8 3 4179.01 365.401 1 4 8 -3 5292.13 421.519 5 -4 -8 2 11280.9 591.403 1 4 8 -2 12190.0 644.819 5 -4 -8 1 9346.28 548.815 1 4 8 -1 9807.85 584.497 5 -4 -8 0-226.923 119.522 1 -4 -8 -1 228.300 135.230 1 -4 -8 -2 165.625 118.967 1 -4 -8 -3 211.598 141.565 1 -4 -8 -4 102.134 120.421 1 -4 -8 -5 3001.95 340.949 1 4 9 -13 338.801 144.803 6 4 9 -12 815.465 179.557 6 4 9 -11 2541.72 283.360 6 4 9 -10 1860.60 255.918 6 4 9 -9 3627.44 339.888 6 4 9 -8 758.583 174.409 6 4 9 -7-56.3383 117.803 6 4 9 -7 90.2785 147.057 5 4 9 -6 26.1622 134.458 5 4 9 -5 29.0425 140.561 5 4 9 -4 8078.11 561.605 5 -4 -9 3 8949.08 557.976 1 4 9 -3 9629.12 606.404 5 -4 -9 2 25520.3 970.688 1 4 9 -2 25906.2 1021.07 5 -4 -9 1 2792.84 318.561 1 -4 -9 0 266.290 130.317 1 -4 -9 -1 872.988 192.137 1 -4 -9 -2-225.607 154.121 1 -4 -9 -3-361.943 166.527 1 4 10 -11 5.31924 105.377 6 4 10 -10 356.978 137.301 6 4 10 -9 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2 -8 24880.4 755.244 4 7 2 -7 33640.2 1013.89 3 7 2 -7 34930.6 1100.73 6 7 2 -7 32748.2 858.128 4 7 2 -6 12604.1 553.242 3 7 2 -6 11821.9 589.980 6 7 2 -6 11440.5 417.508 4 7 2 -5 72.0213 50.1945 4 7 2 -5 152.789 76.1442 3 7 2 -5 173.937 107.159 6 7 2 -5-118.229 103.287 5 7 2 -4 4136.29 299.227 3 7 2 -4 4273.42 343.096 6 7 2 -4 4170.65 295.546 5 7 2 -4 4244.46 192.158 4 7 2 -3 6627.37 369.660 3 7 2 -3 6055.61 395.624 6 7 2 -3 6841.18 368.357 5 7 2 -3 5877.80 198.218 4 7 2 -2 1757.35 222.389 6 -7 -2 2 1929.70 221.761 1 7 2 -2 1142.38 57.3560 4 -7 -2 1 4873.45 353.377 1 -7 -2 0 12765.9 590.915 1 -7 -2 -1 13470.6 613.445 1 -7 -2 -2 3864.91 329.481 1 -7 -2 -3 5633.49 407.951 1 -7 -2 -4 3833.70 346.947 1 -7 -2 -5 291.565 136.706 1 -7 -2 -6 2459.73 304.205 1 -7 -2 -7 5975.17 480.928 1 7 2 7 5899.31 438.326 3 -7 -2 -8 938.461 220.074 1 7 2 8 481.729 168.501 3 -7 -2 -9 8923.10 628.392 1 7 2 9 8502.03 569.434 3 7 2 10 12.5860 130.887 3 7 3 -13 1983.87 294.874 6 7 3 -12-7.48462 135.967 6 7 3 -11 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7574.50 364.133 1 8 -4 -2 25436.6 719.556 1 -8 4 2 26270.6 880.237 2 8 -4 -2 24693.3 834.342 6 -8 4 1 18197.1 703.369 2 8 -4 -1 16729.7 551.471 1 8 -4 -1 17647.0 661.113 6 -8 4 0 6469.75 401.989 2 8 -4 0 6906.25 384.312 6 -8 4 -1 2723.10 263.633 2 8 -4 1 2806.80 235.168 6 8 -4 2 9191.12 462.878 4 -8 4 -2 9744.55 390.509 1 8 -4 2 9378.50 422.468 6 -8 4 -2 9942.37 325.167 5 8 -4 3 1063.25 165.759 4 -8 4 -3 1005.90 130.167 1 -8 4 -3 1071.02 113.831 5 -8 4 -4 164.667 84.8016 1 8 -4 4 136.463 97.4649 4 8 -4 5 1170.07 176.242 4 -8 4 -5 1251.42 156.586 1 8 -4 6 3395.63 300.776 4 -8 4 -6 3120.96 248.660 1 -8 4 -7 25894.7 818.598 1 8 -4 7 25008.4 891.075 4 8 -4 8 3979.21 348.483 4 -8 4 -8 4242.63 322.729 1 8 -4 9 1321.75 211.560 4 -8 4 -9 1861.00 230.077 1 8 -4 10 2762.08 307.228 4 -8 4 -10 3311.89 319.682 1 8 -4 11-44.1130 132.859 4 -8 4 -11 269.242 134.523 1 8 -4 12 2612.89 332.094 4 -8 4 -12 2233.91 297.746 1 -8 3 13 2083.27 305.553 2 -8 3 12 5864.74 478.910 2 -8 3 11 7547.04 527.661 2 -8 3 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7180.94 354.118 6 -8 3 -5 7909.75 406.779 1 8 -3 6 27510.6 882.122 4 8 -3 6 25321.2 741.219 6 -8 3 -6 27443.5 857.933 1 8 -3 7 4800.19 352.060 4 -8 3 -7 4472.48 341.063 1 8 -3 7 4626.24 279.220 6 8 -3 8-79.8121 112.138 4 -8 3 -8 17.6840 95.9540 1 -8 3 -9 27.1806 103.083 1 8 -3 9 77.7945 117.391 4 8 -3 10 953.654 184.331 4 -8 3 -10 1229.82 218.348 1 8 -3 11 717.632 185.930 4 -8 3 -11 912.775 205.462 1 8 -3 12 2426.24 319.990 4 -8 3 -12 2423.15 326.144 1 -8 2 13 2159.50 299.732 2 -8 2 12 400.721 164.512 2 -8 2 11 163.846 151.080 2 -8 2 10 549.582 169.516 2 -8 2 9 712.604 159.217 2 -8 2 8 5258.28 402.924 2 8 -2 -8 5269.18 426.924 6 -8 2 7 3371.14 321.661 2 8 -2 -7 3686.36 346.654 6 -8 2 6 30963.7 996.895 2 8 -2 -6 30001.9 1016.60 6 8 -2 -6 28808.9 650.634 5 -8 2 5 25240.3 881.162 2 8 -2 -5 25771.1 912.833 6 -8 2 4 7965.26 464.091 2 8 -2 -4 8652.69 491.122 6 8 -2 -4 9259.88 453.314 1 -8 2 3 63.9043 107.851 2 8 -2 -3 181.965 101.301 6 8 -2 -3 215.520 89.1130 1 -8 2 2 5470.93 367.669 2 8 -2 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440.554 6 9 -2 1 326.343 98.2986 4 9 -2 1 395.152 122.699 6 -9 2 -1 297.553 111.308 1 9 -2 2 26.7231 78.1705 4 9 -2 2 30.0652 82.1407 6 -9 2 -2-15.1107 92.7159 1 -9 2 -3 186.700 100.099 1 9 -2 3 150.477 92.9954 4 9 -2 3-40.5467 84.9030 6 -9 2 -3 86.6339 70.9607 5 9 -2 4 13476.6 553.727 4 9 -2 4 12851.5 556.297 6 -9 2 -4 13347.8 591.369 1 9 -2 5 32789.7 954.468 4 9 -2 5 30286.3 926.814 6 -9 2 -5 33456.5 1028.77 1 9 -2 6 4895.41 343.567 4 9 -2 6 4648.62 324.596 6 -9 2 -6 4788.14 375.678 1 9 -2 7 137.402 115.851 4 -9 2 -7 74.0923 107.469 1 -9 2 -8 18.0667 126.583 1 9 -2 8 120.229 98.3415 4 -9 2 -9 2827.14 330.593 1 9 -2 9 3259.82 321.146 4 -9 2 -10 492.525 168.339 1 -9 1 13 5997.53 485.945 2 -9 1 12 1162.98 212.556 2 -9 1 11-187.702 132.859 2 -9 1 10 145.495 123.752 2 9 -1 -10 264.467 143.481 6 -9 1 9 151.107 117.094 2 9 -1 -9 129.835 141.049 6 -9 1 8 1152.08 210.185 2 9 -1 -8 1591.89 255.440 6 -9 1 7 2696.23 297.318 2 9 -1 -7 2628.51 318.066 6 9 -1 -7 2306.43 178.501 5 -9 1 6 1334.70 212.909 2 9 -1 -6 1076.34 203.335 6 9 -1 -6 1269.91 131.872 5 -9 1 5 9997.55 558.664 2 9 -1 -5 10796.8 598.013 6 9 -1 -4 14026.5 674.357 6 9 -1 -3 9360.18 527.618 6 9 -1 -2 230.700 111.992 6 9 -1 -1 424.155 137.815 6 9 -1 0 492.384 100.215 4 -9 1 0 561.166 146.162 1 9 -1 0 713.945 163.456 6 9 -1 1 1616.54 168.009 4 9 -1 1 1297.86 191.134 6 -9 1 -1 1452.07 208.417 1 -9 1 -2 477.167 135.343 1 9 -1 2 823.673 120.889 4 9 -1 2 533.092 145.153 6 9 -1 3 2571.28 213.523 4 -9 1 -3 2172.84 247.381 1 9 -1 3 2084.40 232.358 6 9 -1 4 9472.25 492.982 6 -9 1 -4 10007.6 541.937 1 9 -1 5 723.324 135.244 4 -9 1 -5 1099.69 205.166 1 9 -1 6 718.369 130.073 4 -9 1 -6 632.188 161.940 1 -9 1 -7 1626.61 253.598 1 9 -1 7 2449.27 250.981 4 -9 1 -8 2846.85 331.474 1 -9 1 -9 2195.41 298.125 1 -9 0 13-116.785 158.677 2 -9 0 12 319.635 129.840 2 -9 0 11 1268.26 230.265 2 9 0 -11 1541.33 273.288 6 -9 0 10 4885.50 414.147 2 9 0 -10 4751.25 445.561 6 -9 0 9 2317.07 286.112 2 9 0 -9 2215.32 314.818 6 -9 0 8 11906.7 629.169 2 9 0 -8 12108.4 688.096 6 9 0 -8 12748.3 496.861 5 -9 0 7 1371.32 220.914 2 9 0 -7 1172.59 228.759 6 9 0 -7 1391.64 163.775 5 9 0 -6 1129.23 209.604 6 9 0 -6 827.529 126.376 5 9 0 -5 1973.49 260.499 6 9 0 -4 154.106 111.439 6 9 0 -3 713.403 171.589 6 9 0 -2 542.850 156.831 6 9 0 -1 9957.45 369.785 4 -9 0 1 10116.0 538.755 1 9 0 -1 9414.01 525.404 6 9 0 0 6683.80 292.806 4 -9 0 0 6860.51 437.892 1 9 0 0 6386.71 424.214 6 9 0 1 6519.29 293.712 4 -9 0 -1 6098.53 415.718 1 9 0 1 5700.43 399.563 6 9 0 2 2130.02 167.769 4 -9 0 -2 2098.34 251.910 1 9 0 2 2074.57 243.403 6 9 0 3 4116.00 246.088 4 9 0 3 3981.20 329.862 6 -9 0 -3 4263.64 363.379 1 -9 0 -4 142.117 126.104 1 -9 0 -5 25.7776 113.961 1 -9 0 -6 835.002 191.393 1 -9 0 -7 5374.85 454.793 1 -9 0 -8 7948.15 573.224 1 -9 -1 13 206.681 141.619 2 -9 -1 12-230.415 141.156 2 -9 -1 11 2700.44 314.584 2 9 1 -10 5710.76 489.880 6 -9 -1 10 5225.12 426.467 2 9 1 -9 10831.3 672.224 6 9 1 -9 11126.0 511.173 5 9 1 -8 11083.0 658.760 6 9 1 -8 10994.3 504.187 5 9 1 -7-240.501 164.551 6 9 1 -7 17.5129 91.5859 5 9 1 -6 36.9123 121.027 6 9 1 -6 94.3580 79.5245 5 9 1 -5-67.6445 156.638 6 9 1 -5 139.909 94.7249 5 9 1 -4 2540.64 292.660 6 9 1 -3 163.110 53.0166 4 9 1 -3 349.876 142.120 6 9 1 -2 8604.19 516.742 6 -9 -1 1 1177.47 205.949 1 9 1 -1 1581.31 234.640 6 9 1 0 48.0927 96.7029 6 -9 -1 0 35.1451 126.165 1 -9 -1 -1-55.2656 120.274 1 9 1 1-3.78841 97.8143 6 -9 -1 -2-163.031 142.652 1 -9 -1 -3 13661.7 682.074 1 -9 -1 -4 5085.38 429.278 1 -9 -1 -5 8525.27 566.869 1 -9 -1 -6 3745.61 387.803 1 -9 -1 -7 342.711 154.954 1 9 2 -10 4196.78 435.841 6 9 2 -9 958.695 219.926 6 9 2 -9 927.871 170.540 5 9 2 -8-211.925 162.329 6 9 2 -8-1.89279 100.816 5 9 2 -7 3070.63 343.200 6 9 2 -7 3768.41 311.410 5 9 2 -6 590.507 180.214 6 9 2 -6 397.786 118.895 5 9 2 -5 16754.9 789.228 6 9 2 -5 17514.7 676.556 5 9 2 -4 2759.78 316.390 6 9 2 -3 11026.8 613.002 6 -9 -2 2 2336.84 290.996 1 9 2 -2 2040.09 274.037 6 -9 -2 1 3045.44 321.207 1 9 2 -1 2727.93 300.627 6 9 2 0 63.8477 100.348 6 -9 -2 0-63.9274 133.422 1 -9 -2 -1 483.871 173.573 1 -9 -2 -2 496.540 158.399 1 -9 -2 -3 1110.37 215.965 1 -9 -2 -4 3891.70 387.449 1 -9 -2 -5 3977.10 410.759 1 9 2 7 208.104 136.469 3 9 2 8 1635.41 258.067 3 9 3 -10 565.044 157.668 5 9 3 -9 90.5424 129.939 6 9 3 -9 228.578 129.016 5 9 3 -8 319.909 164.470 6 9 3 -8 280.661 112.949 5 9 3 -7-32.7673 124.936 6 9 3 -7 75.5676 102.176 5 9 3 -6 8537.32 576.986 6 9 3 -6 9242.75 517.015 5 9 3 -5 8896.45 571.281 6 9 3 -5 9451.99 523.387 5 9 3 -4 519.350 166.373 6 9 3 -3 6834.99 500.544 6 -9 -3 2 1477.33 254.884 1 9 3 -2 1139.48 211.993 6 9 3 -1 273.987 150.064 6 -9 -3 1 738.704 197.000 1 -9 -3 0 61.6081 111.060 1 -9 -3 -1 5086.76 442.020 1 -9 -3 -2 9108.25 600.572 1 -9 -3 -3 7952.31 563.280 1 -9 -3 -4 25.8282 147.196 1 9 4 -10 2186.00 277.867 5 9 4 -9 2237.22 288.709 5 9 4 -8 660.573 186.650 6 9 4 -8 687.171 174.590 5 9 4 -7 2484.70 329.193 6 9 4 -7 1709.21 246.562 5 9 4 -6 9602.29 620.349 6 9 4 -6 9786.15 568.940 5 9 4 -5 206.003 135.969 6 9 4 -5-71.5277 130.995 5 9 4 -4-25.8643 115.978 6 9 4 -3 2249.30 300.644 6 -9 -4 2 2008.14 290.010 1 9 4 -2 1609.64 264.306 6 -9 -4 1 3222.25 354.399 1 9 4 -1 3677.66 378.401 6 -9 -4 0 5512.20 475.568 1 -9 -4 -1 7425.45 552.966 1 9 5 -11 1078.73 226.738 5 9 5 -10 1629.78 258.446 5 9 5 -9 739.630 193.085 5 9 5 -8 36.6724 142.181 5 9 5 -7 976.678 202.208 5 9 5 -6 231.762 141.528 5 9 5 -5 364.736 163.016 5 9 6 -7 79.1526 118.894 5 9 6 -6 548.234 185.228 5 9 6 -5 3054.08 373.356 5 -10 11 -2 3266.95 363.085 2 -10 11 -3 8089.08 535.673 2 -10 10 0 1816.89 280.973 2 -10 10 -1 548.171 164.989 2 -10 10 -2 821.281 189.547 2 -10 10 -3 340.351 146.619 2 -10 10 -4 71.2316 96.1498 2 -10 9 2 6852.00 521.490 2 -10 9 1 1703.54 264.312 2 -10 9 0 155.765 123.004 2 -10 9 -1 142.408 123.367 2 -10 9 -2 806.084 193.851 2 10 -9 3 1207.77 245.937 4 -10 9 -3 1514.45 240.253 2 10 -9 4 3201.16 368.218 4 -10 8 4 7766.01 557.290 2 -10 8 3-171.675 145.714 2 -10 8 2-74.4983 123.716 2 -10 8 1 257.927 150.740 2 -10 8 0 376.363 168.040 2 -10 8 -1 5451.12 437.878 2 -10 8 -2 2738.56 321.327 2 -10 8 -3 12592.1 654.959 2 10 -8 3 13047.2 716.537 4 10 -8 4 6010.37 489.593 4 10 -8 5 2302.49 310.724 4 10 -8 6 1129.91 220.889 4 -10 7 5 2636.07 326.043 2 -10 7 4-37.7528 144.175 2 -10 7 3 2301.11 292.839 2 -10 7 2 1325.12 238.038 2 -10 7 1 1420.05 247.803 2 -10 7 0 9860.50 593.346 2 -10 7 -1 2213.91 280.896 2 -10 7 -2 3976.59 370.905 2 10 -7 2 3621.64 362.821 4 10 -7 3 219.881 121.503 4 10 -7 4 55.1232 110.919 4 10 -7 5 33.3683 115.375 4 10 -7 6 2195.03 297.323 4 10 -7 7 2091.18 292.067 4 10 -7 8 5901.15 482.917 4 -10 6 6 212.378 132.863 2 -10 6 5 15.2041 109.259 2 -10 6 4 312.511 155.893 2 -10 6 3 1694.10 269.894 2 -10 6 2 13114.1 684.721 2 -10 6 1 2863.37 317.524 2 -10 6 0 565.014 168.952 2 -10 6 -1 980.593 207.338 2 10 -6 2 46.3382 105.073 4 10 -6 3 8.44524 112.703 4 10 -6 4 397.247 143.102 4 10 -6 5 2319.84 286.933 4 10 -6 6 2617.56 308.684 4 10 -6 7 11839.8 659.360 4 10 -6 8 4054.79 394.802 4 10 -6 9 3788.13 386.077 4 -10 5 7 249.213 129.027 2 -10 5 6 281.748 153.673 2 -10 5 5 1837.56 273.389 2 -10 5 4 3093.24 340.454 2 -10 5 3 12067.7 650.235 2 -10 5 2 13499.1 685.974 2 -10 5 1 548.715 157.068 2 10 -5 -1 172.438 100.892 6 -10 5 0 50.3603 108.368 2 10 -5 0-108.967 129.718 6 10 -5 1 59.3885 97.2646 6 10 -5 2-104.843 125.387 4 10 -5 2-198.916 129.860 6 10 -5 3 712.719 157.304 4 10 -5 3 525.779 110.944 6 10 -5 4 2568.55 286.819 4 10 -5 5 1897.73 244.608 4 10 -5 6 1242.49 215.870 4 10 -5 7 1544.53 240.530 4 10 -5 8 2174.45 283.890 4 10 -5 9 4434.83 406.757 4 -10 4 8 637.382 186.765 2 -10 4 7 553.416 168.583 2 -10 4 6 4816.20 423.448 2 -10 4 5 6073.42 467.940 2 -10 4 4 3969.52 375.810 2 10 -4 -4 3923.68 365.125 6 -10 4 3 564.121 153.824 2 10 -4 -3 316.295 136.163 6 -10 4 2 914.419 186.328 2 10 -4 -2 778.983 163.799 6 -10 4 1-33.0742 113.276 2 10 -4 -1-180.188 141.571 6 10 -4 0 1627.95 225.008 6 10 -4 1 5151.63 377.337 4 10 -4 1 5745.42 392.403 6 10 -4 2 1750.62 232.233 4 10 -4 2 1742.76 214.946 6 10 -4 3 7884.70 463.123 4 -10 4 -3 8356.12 427.808 1 10 -4 3 7894.34 438.347 6 10 -4 4 17003.1 711.460 4 -10 4 -4 17704.4 652.453 1 10 -4 4 17077.3 653.614 6 -10 4 -5 427.002 114.007 1 10 -4 5 700.204 164.053 4 -10 4 -6 338.474 126.703 1 10 -4 6 47.4776 104.089 4 10 -4 7 988.696 179.089 4 10 -4 8 514.091 151.470 4 10 -4 9 545.714 160.631 4 -10 3 9 5201.67 460.560 2 -10 3 8 7494.57 540.088 2 -10 3 7 6217.18 486.947 2 10 -3 -7 6827.25 524.787 6 -10 3 6 1235.51 224.648 2 10 -3 -6 1127.43 222.192 6 -10 3 5 186.721 124.510 2 10 -3 -5 227.479 136.259 6 -10 3 4 226.846 124.316 2 10 -3 -4 139.442 122.632 6 -10 3 3 230.676 117.943 2 10 -3 -3 93.2327 108.057 6 10 -3 -2 378.435 140.543 6 10 -3 -1 357.155 163.051 6 10 -3 0 20816.4 747.801 4 10 -3 0 19210.4 772.488 6 10 -3 1 12392.9 555.974 4 10 -3 1 11148.9 558.993 6 10 -3 2 6659.37 394.765 4 -10 3 -2 5969.36 379.943 1 10 -3 2 5842.47 385.326 6 10 -3 3 3932.31 307.178 4 -10 3 -3 4346.10 326.856 1 10 -3 3 3834.41 310.583 6 10 -3 4 273.495 111.772 4 10 -3 4 150.578 104.086 6 -10 3 -4-18.4318 101.362 1 -10 3 -5-121.038 113.251 1 10 -3 5-30.5074 101.202 4 10 -3 6 5132.70 370.932 4 -10 3 -6 4313.02 357.618 1 10 -3 7 4702.25 368.082 4 -10 3 -7 4369.23 368.355 1 -10 3 -8 4220.61 376.149 1 -10 2 10 741.243 207.393 2 -10 2 9 3221.78 362.747 2 -10 2 8 198.193 125.216 2 10 -2 -8 79.3340 134.441 6 -10 2 7 1916.77 271.805 2 10 -2 -7 2310.96 310.529 6 -10 2 6 71.6146 113.411 2 10 -2 -6 6.98416 138.431 6 -10 2 5 1036.21 208.545 2 10 -2 -5 779.511 182.538 6 10 -2 -4 4265.59 392.515 6 -10 2 4 4232.28 389.314 2 10 -2 -3 12376.7 644.985 6 10 -2 -2 6306.42 444.425 6 10 -2 -1 2577.83 291.257 6 10 -2 0 4629.46 308.010 4 10 -2 0 3908.08 340.037 6 10 -2 1 189.498 90.9899 4 -10 2 -1 164.832 96.0592 1 10 -2 1 92.8595 97.2486 6 10 -2 2 100.524 86.5850 4 10 -2 2 135.432 113.569 6 -10 2 -2-185.017 129.287 1 10 -2 3 683.708 140.040 4 10 -2 3 486.398 134.439 6 -10 2 -3 656.341 144.805 1 10 -2 4 3169.93 261.300 4 -10 2 -4 2834.24 293.544 1 10 -2 4 2401.47 251.589 6 -10 2 -5 1806.63 235.679 1 10 -2 5 1630.07 207.385 6 10 -2 6 7793.25 452.569 6 -10 2 -6 8497.94 520.495 1 -10 2 -7 3807.06 367.728 1 -10 2 -8 181.630 140.693 1 -10 2 -9 4942.77 445.408 1 -10 1 10 6406.72 501.148 2 -10 1 9 2095.39 297.043 2 10 -1 -9 2182.29 327.150 6 -10 1 8-37.8931 132.488 2 10 -1 -8-36.0963 134.801 6 -10 1 7 1086.73 210.233 2 10 -1 -7 927.488 211.965 6 10 -1 -6 318.939 153.958 6 -10 1 6 441.250 154.171 2 10 -1 -5 6564.56 493.737 6 10 -1 -4 10856.8 624.585 6 10 -1 -3 13181.3 674.174 6 10 -1 -2 105.646 137.641 6 10 -1 -1 5388.15 309.444 4 10 -1 -1 5615.58 416.363 6 -10 1 0 1004.62 183.316 1 10 -1 0 653.587 113.958 4 10 -1 0 1042.22 204.717 6 10 -1 1 60.2959 106.921 6 -10 1 -1-178.264 131.469 1 10 -1 2 1172.43 201.507 6 -10 1 -2 1469.82 218.054 1 -10 1 -3 1651.49 237.842 1 10 -1 3 1441.77 213.169 6 10 -1 4 2649.19 279.991 6 -10 1 -4 3110.13 323.193 1 -10 1 -5 1822.94 260.314 1 10 -1 5 1560.39 217.109 6 10 -1 6 2183.55 251.456 6 -10 1 -6 2894.83 324.376 1 -10 1 -7-12.9957 115.742 1 -10 1 -8-29.6941 126.228 1 -10 0 11-102.356 130.936 2 -10 0 10 41.2892 112.047 2 10 0 -9 398.190 163.767 6 -10 0 9 529.185 174.716 2 10 0 -8-176.911 170.605 6 10 0 -7 3966.66 402.998 6 10 0 -6 5867.89 483.302 6 10 0 -5 5277.32 450.365 6 10 0 -4 4324.52 396.639 6 10 0 -3 5284.47 434.433 6 10 0 -2 2007.73 264.774 6 10 0 -1 711.905 176.647 6 -10 0 0 1553.91 227.393 1 10 0 0 1428.86 220.603 6 10 0 1 1506.98 226.640 6 -10 0 -1 1376.35 222.036 1 -10 0 -2 5506.67 418.437 1 10 0 2 4571.60 387.269 6 -10 0 -3 7114.91 499.826 1 10 0 3 5570.74 417.985 6 -10 0 -4 1857.89 270.089 1 10 0 4 1454.75 219.840 6 -10 0 -5 611.133 180.357 1 -10 0 -6 328.823 168.778 1 10 1 -8-20.4217 130.535 6 10 1 -7 3299.12 377.424 6 10 1 -6 1913.38 291.770 6 10 1 -5 3865.54 393.481 6 10 1 -4-66.2623 142.162 6 10 1 -3 288.024 152.862 6 10 1 -2 1751.73 267.580 6 -10 -1 1 1035.19 213.058 1 10 1 -1 1464.55 231.502 6 10 1 0 146.640 118.690 6 -10 -1 0 241.786 146.436 1 -10 -1 -1 3134.61 341.336 1 10 1 1 3267.88 332.207 6 -10 -1 -2 5948.07 462.732 1 10 1 2 4959.99 416.881 6 -10 -1 -3-99.7781 134.575 1 10 1 3 84.1995 108.222 6 -10 -1 -4 219.819 145.335 1 -10 -1 -5-25.0236 145.768 1 10 2 -7 798.139 233.941 6 10 2 -7 1017.05 178.106 5 10 2 -6-214.616 157.397 6 10 2 -6-49.7994 92.8588 5 10 2 -5 1112.60 225.038 6 10 2 -4 230.057 138.798 6 10 2 -3 7721.23 538.303 6 10 2 -2 7400.31 525.332 6 -10 -2 1 3228.05 353.130 1 10 2 -1 3100.00 343.894 6 10 2 0 183.003 127.254 6 -10 -2 0 251.186 163.085 1 10 2 1 1231.51 224.370 6 -10 -2 -1 1467.61 257.199 1 -10 -2 -2 154.153 122.706 1 10 2 2 36.6198 120.656 6 -10 -2 -3-168.961 151.643 1 10 3 -7 330.392 126.757 5 10 3 -6 4446.18 369.211 5 10 3 -4 9628.34 625.494 6 10 3 -3 4168.95 410.488 6 10 3 -2 450.802 180.546 6 -10 -3 1-11.6959 130.541 1 10 3 -1 33.4200 114.795 6 10 3 0-91.8600 115.937 6 -10 -3 0 86.5109 133.774 1 10 4 -8 86.0208 108.205 5 10 4 -7 11773.2 643.201 5 10 4 -6 6242.56 475.261 5 10 5 -7 784.843 208.282 5 -11 9 -2-86.0751 141.326 2 -11 8 0 1435.10 252.787 2 -11 8 -1 63.5771 112.900 2 11 -8 2 978.458 222.680 4 -11 8 -2 611.366 168.076 2 11 -8 3 1286.56 247.242 4 -11 7 2-42.6575 140.809 2 -11 7 1 1808.65 279.203 2 -11 7 0 1666.27 260.651 2 -11 7 -1 358.677 154.735 2 11 -7 2 2049.62 300.196 4 11 -7 3 4482.98 419.435 4 11 -7 4 1287.26 247.042 4 11 -7 5 1211.98 215.386 4 11 -7 6 989.417 218.772 4 -11 6 3 1920.87 285.851 2 -11 6 2 761.321 193.369 2 -11 6 1 6306.91 495.053 2 -11 6 0 1955.51 288.801 2 11 -6 1 5547.77 444.566 4 11 -6 2 2092.33 279.390 4 11 -6 3 334.898 126.939 4 11 -6 4 566.204 154.407 4 11 -6 5 66.6928 126.208 4 11 -6 6-60.7285 118.354 4 11 -6 7 5444.10 456.254 4 -11 5 4 5715.14 480.451 2 -11 5 3 3125.08 362.766 2 -11 5 2 12096.1 680.015 2 11 -5 -2 11185.0 624.973 6 11 -5 -1 2029.98 263.618 6 -11 5 1 2082.45 279.626 2 11 -5 0 561.977 141.040 6 11 -5 1-246.991 134.212 4 11 -5 1-37.0589 98.5725 6 11 -5 2 470.315 147.221 4 11 -5 2 388.505 123.489 6 11 -5 3 1294.96 217.679 4 11 -5 4 254.343 105.058 4 11 -5 5 956.231 192.386 4 11 -5 6 5655.44 448.173 4 11 -5 7 9265.90 576.301 4 -11 4 5 849.301 211.301 2 11 -4 -5 384.742 179.029 6 -11 4 4 6331.27 497.100 2 11 -4 -4 5199.79 447.458 6 -11 4 3 2381.06 311.416 2 11 -4 -3 1693.96 260.510 6 11 -4 -2 2982.46 321.892 6 11 -4 -1 1022.90 196.148 6 11 -4 0-57.3501 103.641 4 11 -4 0-252.490 134.355 6 11 -4 1 502.673 145.752 4 11 -4 1 610.540 143.711 6 11 -4 2 261.068 129.289 4 11 -4 2 179.662 115.699 6 11 -4 3 4034.29 343.215 4 11 -4 3 4186.59 332.523 6 11 -4 4 2897.77 296.886 4 11 -4 5 4752.68 379.925 4 11 -3 -7 1293.21 260.472 6 11 -3 -6 2141.10 302.600 6 -11 3 5 6712.68 513.076 2 11 -3 -5 6806.40 523.222 6 11 -3 -4 3404.72 360.098 6 -11 3 4 3238.99 361.714 2 11 -3 -3-250.132 182.034 6 11 -3 -2-175.321 150.943 6 11 -3 -1 36.0043 87.7047 4 11 -3 -1 131.790 113.915 6 11 -3 0 924.552 160.817 4 11 -3 0 710.271 168.894 6 11 -3 1 4052.17 318.802 4 11 -3 1 3060.30 311.835 6 11 -3 2 4793.31 380.940 6 -11 3 -3 4556.91 361.865 1 11 -3 3 4572.40 354.553 6 -11 3 -4 4075.34 339.155 1 11 -2 -7 1041.94 219.914 6 11 -2 -6 342.249 142.102 6 -11 2 6 352.228 162.640 2 11 -2 -5-90.6379 132.021 6 11 -2 -4-219.238 165.376 6 11 -2 -3 774.666 184.638 6 11 -2 -2 6164.53 474.035 6 11 -2 -1 8153.71 528.712 6 11 -2 0 3628.96 351.585 6 11 -2 1 2341.06 275.571 6 -11 2 -2 2190.34 261.741 1 11 -2 2 2182.14 267.624 6 11 -2 3 519.027 140.930 6 -11 2 -3 455.117 140.394 1 11 -2 4 130.067 109.551 6 -11 2 -4-157.264 121.369 1 -11 2 -5 143.828 107.690 1 -11 2 -6 2716.85 310.874 1 11 -1 -6-95.9422 181.450 6 11 -1 -5 1344.43 254.216 6 11 -1 -4 1674.40 266.340 6 11 -1 -3 664.815 183.050 6 11 -1 -2 6056.89 472.196 6 11 -1 -1 2011.45 284.820 6 11 -1 0 2873.23 329.055 6 -11 1 -1 2189.30 279.411 1 11 -1 1 2288.90 283.235 6 11 -1 2 158.148 129.095 6 -11 1 -2-170.137 138.421 1 11 -1 3 99.8580 93.0285 6 -11 1 -3 68.5329 122.228 1 -11 1 -4 1780.57 261.623 1 11 -1 4 1396.90 218.603 6 -11 1 -5 2397.03 311.535 1 11 -1 5 2406.48 288.250 6 11 0 -5 5379.47 479.568 6 11 0 -4 4962.70 446.279 6 11 0 -3 4119.41 404.427 6 11 0 -2 975.938 206.072 6 11 0 -1 291.172 141.392 6 11 0 0 198.341 140.386 6 -11 0 -1 98.5318 141.579 1 11 0 1 144.061 120.977 6 11 0 2 1308.62 233.303 6 -11 0 -2 1928.64 276.405 1 -11 0 -3 3162.78 356.217 1 11 0 3 3497.98 355.763 6 -11 0 -4 11337.9 670.675 1 11 0 4 10082.8 603.634 6 11 0 5 4137.85 383.648 6 11 1 -3 290.870 165.521 6 11 1 -2 90.6925 112.748 6 11 1 -1 176.876 131.051 6 -11 -1 0 1254.18 240.408 1 11 1 0 1161.92 222.618 6 11 1 1 516.524 163.407 6 -11 -1 -1 283.519 156.210 1 11 1 2 3094.10 354.204 6 12 -7 1 512.701 167.304 4 12 -6 0 276.166 162.546 4 12 -6 1 419.435 159.830 4 12 -6 2 260.924 138.443 4 12 -6 3 2796.39 328.355 4 12 -5 -2 4517.64 420.241 6 12 -5 -1 4504.19 398.575 6 12 -5 0 8161.57 538.525 4 12 -5 1 3289.18 339.765 4 12 -4 -4 566.284 194.496 6 12 -4 -3 11346.7 678.190 6 12 -4 -2 2254.96 306.532 6 12 -4 -1 2775.72 322.090 6 12 -4 0 524.227 140.566 6 12 -3 -4 7343.92 556.133 6 12 -3 -3 731.492 194.769 6 12 -3 -2-208.660 160.473 6 12 -3 -1-262.944 169.026 6 12 -3 0 427.332 148.026 6 12 -3 1-62.0229 110.898 6 12 -2 -3-264.267 197.708 6 12 -2 -2 380.723 131.504 6 12 -2 -1-63.2337 156.886 6 12 -2 0 382.006 146.151 6 12 -2 1 5263.98 434.159 6 12 -2 2 4493.39 398.500 6 12 -1 -1 3778.42 388.660 6 12 -1 0 2515.89 316.495 6 12 -1 1 1459.37 240.544 6 -12 1 -2 0.35439 123.983 1 12 -1 2 305.043 135.866 6 0 0 0 0.00 0.00 0 TITL exp_4358-ms in P-1 REM P-1 (#2 in standard setting) CELL 0.71073 9.132924 10.078694 13.082540 103.4960 94.5620 105.2285 ZERR 5.00 0.000575 0.000671 0.000786 0.0054 0.0050 0.0056 LATT 1 SFAC C H N O UNIT 55.00 50.00 5.00 5.00 TREF HKLF 4 END ; _shelx_hkl_checksum 24352 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu Cu 0.0000 0.0000 0.0000 0.01401(10) Uani 1 2 d S . P . . N1A N -0.2226(2) -0.34109(18) 0.10577(14) 0.0196(4) Uani 1 1 d D . . . . H1A H -0.224(3) -0.4223(16) 0.116(2) 0.029 Uiso 1 1 d D U . . . N1B N -0.34454(19) -0.12484(19) -0.25864(14) 0.0198(4) Uani 1 1 d D . . . . H1B H -0.4329(16) -0.127(3) -0.2875(19) 0.030 Uiso 1 1 d D U . . . C2A C -0.1046(2) -0.2594(2) 0.07341(17) 0.0199(4) Uani 1 1 d . . . . . H2A H -0.0098 -0.2797 0.0648 0.024 Uiso 1 1 calc R U . . . C2B C -0.2825(2) -0.0552(2) -0.15812(16) 0.0190(4) Uani 1 1 d . . . . . H2B H -0.3325 -0.0055 -0.1082 0.023 Uiso 1 1 calc R U . . . N3A N -0.13802(18) -0.14695(17) 0.05517(13) 0.0168(3) Uani 1 1 d . . . . . N3B N -0.14208(18) -0.06484(17) -0.13743(13) 0.0164(3) Uani 1 1 d . . . . . C4A C -0.2854(2) -0.1585(2) 0.07592(16) 0.0179(4) Uani 1 1 d . . . . . H4A H -0.3404 -0.0921 0.0695 0.021 Uiso 1 1 calc R U . . . C4B C -0.1143(2) -0.1442(2) -0.23054(16) 0.0172(4) Uani 1 1 d . . . . . H4B H -0.0213 -0.1677 -0.2404 0.021 Uiso 1 1 calc R U . . . C5A C -0.3408(2) -0.2803(2) 0.10730(16) 0.0174(4) Uani 1 1 d . . . . . C5B C -0.2398(2) -0.1843(2) -0.30669(16) 0.0174(4) Uani 1 1 d . . . . . C6A C -0.4900(2) -0.3438(2) 0.13585(16) 0.0190(4) Uani 1 1 d . . . . . C6B C -0.2711(2) -0.2765(2) -0.41500(16) 0.0199(4) Uani 1 1 d . . . . . C7A C -0.5393(2) -0.4884(2) 0.13122(16) 0.0217(4) Uani 1 1 d . . . . . H7A H -0.4754 -0.5473 0.1095 0.026 Uiso 1 1 calc R U . . . C7B C -0.3981(3) -0.2875(2) -0.48579(17) 0.0236(4) Uani 1 1 d . . . . . H7B H -0.4662 -0.2330 -0.4645 0.028 Uiso 1 1 calc R U . . . C8A C -0.6815(3) -0.5468(3) 0.15819(18) 0.0291(5) Uani 1 1 d . . . . . H8A H -0.7138 -0.6452 0.1558 0.035 Uiso 1 1 calc R U . . . C8B C -0.4258(3) -0.3780(3) -0.58761(18) 0.0287(5) Uani 1 1 d . . . . . H8B H -0.5132 -0.3854 -0.6355 0.034 Uiso 1 1 calc R U . . . C9A C -0.7762(3) -0.4631(3) 0.18840(18) 0.0317(5) Uani 1 1 d . . . . . H9A H -0.8737 -0.5035 0.2064 0.038 Uiso 1 1 calc R U . . . C9B C -0.3275(3) -0.4569(3) -0.61955(19) 0.0322(5) Uani 1 1 d . . . . . H9B H -0.3463 -0.5181 -0.6895 0.039 Uiso 1 1 calc R U . . . C10A C -0.7281(3) -0.3195(3) 0.19229(19) 0.0302(5) Uani 1 1 d . . . . . H10A H -0.7931 -0.2614 0.2129 0.036 Uiso 1 1 calc R U . . . C10B C -0.2014(3) -0.4467(3) -0.5494(2) 0.0357(6) Uani 1 1 d . . . . . H10B H -0.1337 -0.5015 -0.5711 0.043 Uiso 1 1 calc R U . . . C11A C -0.5859(2) -0.2600(2) 0.16633(18) 0.0248(5) Uani 1 1 d . . . . . H11A H -0.5538 -0.1614 0.1694 0.030 Uiso 1 1 calc R U . . . C11B C -0.1729(3) -0.3574(3) -0.44760(19) 0.0290(5) Uani 1 1 d . . . . . H11B H -0.0859 -0.3513 -0.3998 0.035 Uiso 1 1 calc R U . . . Cl Cl 0.22978(5) -0.25601(5) -0.12266(4) 0.01921(12) Uani 1 1 d . . . . . O1 O 0.15430(19) -0.16512(17) -0.06170(12) 0.0276(4) Uani 1 1 d . . . . . O2 O 0.17607(19) -0.28164(19) -0.23395(13) 0.0314(4) Uani 1 1 d . . . . . O3 O 0.39081(19) -0.1914(2) -0.10117(16) 0.0480(5) Uani 1 1 d . . . . . O4 O 0.1909(3) -0.38821(19) -0.09421(17) 0.0471(5) Uani 1 1 d . . . . . C12 C 0.6765(3) 0.0001(3) 0.3723(2) 0.0360(6) Uani 1 1 d . . . . . H12A H 0.6907 -0.0649 0.3067 0.043 Uiso 1 1 calc R U . . . H12B H 0.5931 -0.0549 0.4030 0.043 Uiso 1 1 calc R U . . . C13 C 0.8222(3) 0.0494(3) 0.4503(2) 0.0365(6) Uani 1 1 d . . . . . H13A H 0.8496 -0.0350 0.4624 0.044 Uiso 1 1 calc R U . . . H13B H 0.9062 0.1031 0.4192 0.044 Uiso 1 1 calc R U . . . C14 C 0.8095(4) 0.1422(4) 0.5549(2) 0.0596(9) Uani 1 1 d . . . . . H14A H 0.9067 0.1696 0.6029 0.089 Uiso 1 1 calc R U . . . H14B H 0.7269 0.0896 0.5863 0.089 Uiso 1 1 calc R U . . . H14C H 0.7866 0.2279 0.5438 0.089 Uiso 1 1 calc R U . . . O5 O 0.63091(19) 0.1137(2) 0.34474(14) 0.0366(4) Uani 1 1 d D . . . . H5 H 0.695(3) 0.164(3) 0.316(2) 0.055 Uiso 1 1 d D U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu 0.01325(17) 0.01377(17) 0.01510(18) 0.00377(13) 0.00192(12) 0.00413(13) N1A 0.0195(8) 0.0164(8) 0.0255(9) 0.0085(7) 0.0042(7) 0.0069(7) N1B 0.0161(8) 0.0248(9) 0.0196(9) 0.0048(7) -0.0003(7) 0.0094(7) C2A 0.0182(10) 0.0195(10) 0.0236(11) 0.0072(8) 0.0029(8) 0.0069(8) C2B 0.0190(10) 0.0195(10) 0.0196(10) 0.0036(8) 0.0036(8) 0.0084(8) N3A 0.0153(8) 0.0157(8) 0.0183(8) 0.0039(7) 0.0017(6) 0.0036(7) N3B 0.0154(8) 0.0176(8) 0.0167(8) 0.0054(7) 0.0021(6) 0.0050(7) C4A 0.0162(9) 0.0168(9) 0.0208(10) 0.0040(8) 0.0022(8) 0.0061(8) C4B 0.0152(9) 0.0191(10) 0.0184(10) 0.0044(8) 0.0049(8) 0.0068(8) C5A 0.0176(9) 0.0171(9) 0.0168(10) 0.0029(8) 0.0009(8) 0.0058(8) C5B 0.0165(9) 0.0177(10) 0.0189(10) 0.0060(8) 0.0046(8) 0.0050(8) C6A 0.0183(10) 0.0219(10) 0.0153(10) 0.0063(8) 0.0010(8) 0.0023(8) C6B 0.0192(10) 0.0211(10) 0.0190(10) 0.0053(8) 0.0039(8) 0.0046(8) C7A 0.0253(11) 0.0204(10) 0.0158(10) 0.0036(8) 0.0019(8) 0.0021(9) C7B 0.0254(11) 0.0257(11) 0.0201(11) 0.0042(9) 0.0026(9) 0.0098(9) C8A 0.0294(12) 0.0276(12) 0.0216(11) 0.0066(9) 0.0018(9) -0.0059(10) C8B 0.0291(12) 0.0349(13) 0.0199(11) 0.0038(10) -0.0026(9) 0.0104(10) C9A 0.0190(11) 0.0447(14) 0.0227(12) 0.0077(10) 0.0030(9) -0.0045(10) C9B 0.0410(14) 0.0339(13) 0.0187(11) -0.0014(10) 0.0017(10) 0.0141(11) C10A 0.0213(11) 0.0431(14) 0.0257(12) 0.0056(10) 0.0041(9) 0.0115(10) C10B 0.0365(13) 0.0431(15) 0.0274(13) -0.0021(11) 0.0037(10) 0.0217(12) C11A 0.0217(11) 0.0265(11) 0.0262(12) 0.0071(9) 0.0029(9) 0.0073(9) C11B 0.0257(11) 0.0358(13) 0.0253(12) 0.0020(10) 0.0003(9) 0.0152(10) Cl 0.0178(2) 0.0193(2) 0.0235(3) 0.00534(19) 0.00553(19) 0.00990(19) O1 0.0343(9) 0.0282(8) 0.0254(8) 0.0026(7) 0.0077(7) 0.0206(7) O2 0.0316(9) 0.0411(10) 0.0222(8) 0.0018(7) 0.0057(7) 0.0167(8) O3 0.0162(8) 0.0836(16) 0.0440(11) 0.0232(11) 0.0047(8) 0.0084(9) O4 0.0707(14) 0.0235(9) 0.0565(13) 0.0167(9) 0.0124(10) 0.0233(9) C12 0.0304(13) 0.0418(15) 0.0347(14) 0.0060(11) 0.0005(10) 0.0134(11) C13 0.0275(12) 0.0491(16) 0.0361(14) 0.0159(12) 0.0012(10) 0.0139(12) C14 0.0510(19) 0.083(2) 0.0316(16) 0.0016(16) -0.0013(13) 0.0109(18) O5 0.0246(9) 0.0572(12) 0.0399(10) 0.0247(9) 0.0082(7) 0.0205(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N3A Cu N3A 180.0 . 2 ? N3A Cu N3B 90.47(7) . . ? N3A Cu N3B 89.53(7) 2 . ? N3A Cu N3B 89.53(7) . 2 ? N3A Cu N3B 90.47(7) 2 2 ? N3B Cu N3B 180.0 . 2 ? C2A N1A C5A 108.71(17) . . ? C2A N1A H1A 122.8(17) . . ? C5A N1A H1A 128.0(17) . . ? C2B N1B C5B 108.31(17) . . ? C2B N1B H1B 124.4(18) . . ? C5B N1B H1B 127.2(18) . . ? N3A C2A N1A 110.58(18) . . ? N3A C2A H2A 124.7 . . ? N1A C2A H2A 124.7 . . ? N3B C2B N1B 110.96(18) . . ? N3B C2B H2B 124.5 . . ? N1B C2B H2B 124.5 . . ? C2A N3A C4A 106.34(16) . . ? C2A N3A Cu 124.63(14) . . ? C4A N3A Cu 128.94(13) . . ? C2B N3B C4B 105.65(16) . . ? C2B N3B Cu 129.79(14) . . ? C4B N3B Cu 124.28(13) . . ? C5A C4A N3A 109.54(17) . . ? C5A C4A H4A 125.2 . . ? N3A C4A H4A 125.2 . . ? C5B C4B N3B 110.00(17) . . ? C5B C4B H4B 125.0 . . ? N3B C4B H4B 125.0 . . ? C4A C5A N1A 104.83(17) . . ? C4A C5A C6A 131.69(18) . . ? N1A C5A C6A 123.46(18) . . ? C4B C5B N1B 105.06(17) . . ? C4B C5B C6B 130.88(18) . . ? N1B C5B C6B 123.96(18) . . ? C11A C6A C7A 119.03(19) . . ? C11A C6A C5A 119.88(19) . . ? C7A C6A C5A 121.07(19) . . ? C7B C6B C11B 119.0(2) . . ? C7B C6B C5B 121.69(19) . . ? C11B C6B C5B 119.25(19) . . ? C8A C7A C6A 120.2(2) . . ? C8A C7A H7A 119.9 . . ? C6A C7A H7A 119.9 . . ? C8B C7B C6B 120.2(2) . . ? C8B C7B H7B 119.9 . . ? C6B C7B H7B 119.9 . . ? C9A C8A C7A 120.5(2) . . ? C9A C8A H8A 119.8 . . ? C7A C8A H8A 119.8 . . ? C9B C8B C7B 120.4(2) . . ? C9B C8B H8B 119.8 . . ? C7B C8B H8B 119.8 . . ? C8A C9A C10A 119.5(2) . . ? C8A C9A H9A 120.2 . . ? C10A C9A H9A 120.2 . . ? C8B C9B C10B 119.6(2) . . ? C8B C9B H9B 120.2 . . ? C10B C9B H9B 120.2 . . ? C9A C10A C11A 120.4(2) . . ? C9A C10A H10A 119.8 . . ? C11A C10A H10A 119.8 . . ? C9B C10B C11B 120.5(2) . . ? C9B C10B H10B 119.7 . . ? C11B C10B H10B 119.7 . . ? C10A C11A C6A 120.3(2) . . ? C10A C11A H11A 119.8 . . ? C6A C11A H11A 119.8 . . ? C10B C11B C6B 120.2(2) . . ? C10B C11B H11B 119.9 . . ? C6B C11B H11B 119.9 . . ? O3 Cl O1 109.91(12) . . ? O3 Cl O4 110.66(13) . . ? O1 Cl O4 107.82(11) . . ? O3 Cl O2 109.92(11) . . ? O1 Cl O2 109.30(10) . . ? O4 Cl O2 109.19(12) . . ? O5 C12 C13 113.6(2) . . ? O5 C12 H12A 108.9 . . ? C13 C12 H12A 108.9 . . ? O5 C12 H12B 108.9 . . ? C13 C12 H12B 108.9 . . ? H12A C12 H12B 107.7 . . ? C14 C13 C12 113.0(2) . . ? C14 C13 H13A 109.0 . . ? C12 C13 H13A 109.0 . . ? C14 C13 H13B 109.0 . . ? C12 C13 H13B 109.0 . . ? H13A C13 H13B 107.8 . . ? C13 C14 H14A 109.5 . . ? C13 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? C13 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? C12 O5 H5 115(2) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu N3A 1.9915(16) . ? Cu N3A 1.9916(16) 2 ? Cu N3B 1.9946(16) . ? Cu N3B 1.9946(16) 2 ? N1A C2A 1.337(3) . ? N1A C5A 1.374(3) . ? N1A H1A 0.855(10) . ? N1B C2B 1.336(3) . ? N1B C5B 1.375(3) . ? N1B H1B 0.857(10) . ? C2A N3A 1.315(3) . ? C2A H2A 0.9500 . ? C2B N3B 1.323(3) . ? C2B H2B 0.9500 . ? N3A C4A 1.375(3) . ? N3B C4B 1.374(3) . ? C4A C5A 1.369(3) . ? C4A H4A 0.9500 . ? C4B C5B 1.363(3) . ? C4B H4B 0.9500 . ? C5A C6A 1.463(3) . ? C5B C6B 1.461(3) . ? C6A C11A 1.388(3) . ? C6A C7A 1.393(3) . ? C6B C7B 1.389(3) . ? C6B C11B 1.391(3) . ? C7A C8A 1.388(3) . ? C7A H7A 0.9500 . ? C7B C8B 1.389(3) . ? C7B H7B 0.9500 . ? C8A C9A 1.377(4) . ? C8A H8A 0.9500 . ? C8B C9B 1.376(3) . ? C8B H8B 0.9500 . ? C9A C10A 1.385(4) . ? C9A H9A 0.9500 . ? C9B C10B 1.380(3) . ? C9B H9B 0.9500 . ? C10A C11A 1.384(3) . ? C10A H10A 0.9500 . ? C10B C11B 1.383(3) . ? C10B H10B 0.9500 . ? C11A H11A 0.9500 . ? C11B H11B 0.9500 . ? Cl O3 1.4184(17) . ? Cl O1 1.4243(15) . ? Cl O4 1.4296(18) . ? Cl O2 1.4392(17) . ? C12 O5 1.427(3) . ? C12 C13 1.503(3) . ? C12 H12A 0.9900 . ? C12 H12B 0.9900 . ? C13 C14 1.498(4) . ? C13 H13A 0.9900 . ? C13 H13B 0.9900 . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? O5 H5 0.844(10) . ? _cod_database_fobs_code 2023226