#------------------------------------------------------------------------------ #$Date: 2024-05-06 06:23:16 +0200 (Mon, 06 May 2024) $ #$Revision: 291733 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/30/2023060.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023060 loop_ _publ_author_name 'Upmann, Daniel' 'Bockfeld, Dirk' 'Jones, Peter G.' 'Târcoveanu, Eliza' _publ_section_title ; Crystal structures of ten phosphane chalcogenide complexes of gold(III) chloride and bromide. ; _journal_coeditor_code YZ2051 _journal_issue 'Pt 4' _journal_name_full 'Acta crystallographica. Section E, Crystallographic communications' _journal_page_first 355 _journal_page_last 369 _journal_paper_doi 10.1107/S2056989024002032 _journal_volume 80 _journal_year 2024 _chemical_formula_iupac '[Au Br3 (C11 H25 P S)]' _chemical_formula_moiety 'C11 H25 Au Br3 P S' _chemical_formula_sum 'C11 H25 Au Br3 P S' _chemical_formula_weight 657.04 _chemical_name_systematic ; Tribromido[di-tert-butyl(propan-2-yl)phosphane sulfide-\kS]gold(III) ; _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2019/3 _cell_angle_alpha 77.873(10) _cell_angle_beta 70.257(10) _cell_angle_gamma 71.867(10) _cell_formula_units_Z 2 _cell_length_a 8.6067(8) _cell_length_b 10.1161(12) _cell_length_c 11.5123(12) _cell_measurement_reflns_used 29495 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 30.7729 _cell_measurement_theta_min 2.5994 _cell_volume 890.37(18) _computing_cell_refinement ; CrysAlisPro, Version 1.171.35.21 (Rigaku OD, 2020) ; _computing_data_collection ; CrysAlisPro, Version 1.171.35.21 (Rigaku OD, 2020) ; _computing_data_reduction ; CrysAlisPro, Version 1.171.35.21 (Rigaku OD, 2020) ; _computing_molecular_graphics ; Bruker XP, Version 5.1 (Bruker, 1998) ; _computing_publication_material ; SHELXL-2019/3 (Sheldrick, 2015) ; _computing_structure_refinement ; SHELXL-2019/3 (Sheldrick, 2015) ; _computing_structure_solution ; SHELXS-97 (Sheldrick, 2008) ; _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean 16.1419 _diffrn_measured_fraction_theta_full 0.988 _diffrn_measured_fraction_theta_max 0.945 _diffrn_measurement_device_type 'Oxford Diffaction Xcalibur, Eos' _diffrn_measurement_method '\w scan' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0375 _diffrn_reflns_av_unetI/netI 0.0184 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_number 65025 _diffrn_reflns_theta_full 30.000 _diffrn_reflns_theta_max 30.848 _diffrn_reflns_theta_min 2.605 _diffrn_source 'Enhance (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 15.181 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.44703 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (CrysAlisPro; Rigaku OD, 2020) ; _exptl_crystal_colour red-brown _exptl_crystal_density_diffrn 2.451 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 612 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.2 _refine_diff_density_max 1.077 _refine_diff_density_min -1.426 _refine_ls_extinction_coef 0.00557(11) _refine_ls_extinction_expression 'F~c~^*^ = kF~c~[1 + 0.001 F~c~^2^\l^3^/sin(2\q)]^-1/4^' _refine_ls_extinction_method ; SHELXL-2019/3 (Sheldrick, 2015) ; _refine_ls_goodness_of_fit_ref 1.135 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 163 _refine_ls_number_reflns 5297 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.135 _refine_ls_R_factor_all 0.0192 _refine_ls_R_factor_gt 0.0174 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0122P)^2^+1.1802P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0357 _refine_ls_wR_factor_ref 0.0362 _reflns_number_gt 5057 _reflns_number_total 5297 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file yz2051.cif _cod_data_source_block 11b _cod_depositor_comments 'Adding full bibliography for 2023050--2023062.cif.' _cod_database_code 2023060 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.151 _shelx_estimated_absorpt_t_max 0.151 _shelx_hkl_file ; 0 0 -2 640414. 16274.0 29 0 0 -2 663301. 16260.5 27 0 0 2 710348. 16120.8 19 0 0 -2 649759. 16091.2 19 0 0 -2 666683. 16258.7 26 0 0 -2 657860. 16258.5 24 0 0 -2 709797. 16056.6 2 0 0 2 735937. 16383.7 29 0 0 2 721151. 16331.9 24 0 0 -2 641312. 16283.0 31 0 0 2 744355. 16081.9 2 0 0 -2 707438. 16229.8 1 0 0 -2 727648. 15945.5 4 0 0 2 732134. 16088.4 18 0 0 -2 664888. 16260.2 25 0 0 2 756682. 15973.8 7 0 0 -2 638809. 15872.1 23 0 0 2 795064. 15984.5 23 0 0 2 716816. 16318.7 25 0 0 -2 647403. 16317.6 21 0 0 2 738825. 15931.6 4 0 0 2 730502. 16408.8 21 0 0 2 735566. 16245.4 1 0 0 2 717572. 16332.9 30 0 0 -2 735055. 16076.4 18 0 0 2 722911. 16329.1 27 0 0 -2 656560. 16255.3 30 0 0 2 741994. 16391.3 31 0 0 2 712955. 16314.8 26 0 0 -3 82726.4 2437.84 18 0 0 3 79405.7 2724.21 31 0 0 -3 79458.0 2693.94 25 0 0 3 79609.2 2400.60 2 0 0 -3 83105.6 2705.43 26 0 0 3 74296.9 2426.79 19 0 0 3 80475.9 2672.47 25 0 0 3 80601.1 2679.86 27 0 0 3 80307.4 2278.90 23 0 0 3 80785.0 2261.22 4 0 0 -3 83203.7 2287.22 4 0 0 -3 81116.3 2607.92 1 0 0 3 80340.4 2676.17 26 0 0 -3 80664.0 2697.69 24 0 0 -3 84317.0 2740.73 29 0 0 -3 72114.1 2461.11 19 0 0 -3 80707.9 2212.85 23 0 0 3 79207.1 2674.48 30 0 0 -3 78896.5 2675.65 30 0 0 -3 80355.4 2412.12 2 0 0 -3 76518.6 2726.67 21 0 0 3 79131.7 2413.49 18 0 0 3 79544.6 2577.31 1 0 0 -3 79491.7 2712.17 31 0 0 3 83563.0 2760.38 29 0 0 3 82112.6 2308.99 7 0 0 3 85490.3 2795.90 21 0 0 3 80262.5 2684.27 24 0 0 -3 81171.6 2700.28 27 0 0 -4 236819. 6143.29 18 0 0 -4 233917. 6545.67 24 0 0 4 227041. 6370.31 1 0 0 -4 225769. 6601.92 21 0 0 4 234092. 5898.02 4 0 0 -4 236043. 6541.24 26 0 0 4 244676. 6652.89 29 0 0 4 245189. 5917.85 23 0 0 -4 235870. 6547.69 30 0 0 -4 244754. 5928.83 4 0 0 -4 234128. 6316.66 9 0 0 4 236340. 5935.85 7 0 0 4 245054. 6654.76 31 0 0 -4 234725. 6111.84 2 0 0 4 230386. 6185.45 19 0 0 -4 231020. 5770.92 23 0 0 -4 234944. 6250.80 19 0 0 -4 228207. 6524.65 25 0 0 -4 237924. 6565.26 27 0 0 -5 158937. 4746.68 9 0 0 5 156318. 4323.24 4 0 0 -5 160149. 5036.62 25 0 0 5 154638. 4623.16 19 0 0 -5 161372. 5028.01 27 0 0 5 156055. 4240.21 23 0 0 -5 152185. 4546.51 18 0 0 -5 154968. 4520.08 2 0 0 -5 148964. 5060.33 21 0 0 -5 158748. 4298.98 4 0 0 5 153939. 4823.48 1 0 0 -5 155977. 4990.25 24 0 0 -5 158021. 4086.90 23 0 0 5 152891. 4297.82 7 0 0 5 166793. 5145.31 29 0 0 -5 157748. 5001.58 30 0 0 -5 154620. 4957.69 26 0 0 5 159582. 5076.08 31 0 0 6 81559.7 2723.98 4 0 0 -6 83560.2 3351.81 27 0 0 -6 77292.0 3046.15 9 0 0 6 76490.7 2667.92 7 0 0 -6 83789.8 3366.58 26 0 0 6 77713.4 3167.72 1 0 0 -6 80018.8 2902.37 2 0 0 -6 79188.9 2613.25 4 0 0 -6 78684.8 3290.41 24 0 0 6 77601.5 2941.37 19 0 0 -6 78235.8 2396.73 23 0 0 6 79345.8 2586.71 23 0 0 6 80836.6 3383.86 29 0 0 -6 77117.5 3398.28 21 0 0 -6 80702.4 2955.83 18 0 0 -6 80046.0 3308.39 30 0 0 6 84856.4 3434.47 31 0 0 -6 83676.3 3372.72 25 0 0 7 199605. 6003.02 19 0 0 -7 201957. 6489.89 25 0 0 -7 210221. 6555.02 26 0 0 7 191576. 5559.40 7 0 0 -7 205878. 6536.74 24 0 0 7 207458. 5664.89 4 0 0 7 208379. 6640.18 31 0 0 7 199884. 6328.72 1 0 0 -7 196728. 6648.36 21 0 0 -7 200389. 5915.87 2 0 0 -7 203668. 5989.85 18 0 0 -7 190335. 5135.12 23 0 0 -7 204924. 6517.83 30 0 0 7 203902. 6614.04 29 0 0 -7 204176. 6167.53 9 0 0 -7 206566. 6530.85 27 0 0 8 157474. 5706.98 31 0 0 -8 147627. 4159.81 23 0 0 8 156528. 4701.69 4 0 0 -8 160279. 5141.66 18 0 0 -8 153199. 5783.16 21 0 0 -8 157057. 5628.91 24 0 0 -8 156853. 5062.19 2 0 0 -8 166996. 5731.88 27 0 0 -8 159535. 5647.27 25 0 0 8 155682. 5478.88 1 0 0 -8 156936. 5621.59 26 0 0 8 153335. 5088.69 19 0 0 -8 160278. 5315.44 9 0 0 8 150721. 4693.43 7 0 0 9 181851. 6438.41 1 0 0 -9 199225. 6741.70 27 0 0 -9 194726. 6699.37 24 0 0 9 185197. 5471.23 4 0 0 -9 185929. 6579.69 26 0 0 -9 188417. 6860.81 21 0 0 9 180057. 5580.92 7 0 0 9 184723. 6038.51 19 0 0 -9 194490. 6121.37 18 0 0 -9 194785. 6332.25 9 0 0 -9 191343. 6041.54 2 0 0 -9 192054. 6656.81 25 0 0 -10 83190.0 4009.96 27 0 0 -10 78299.3 3493.54 18 0 0 10 77304.6 3930.11 17 0 0 10 77933.9 3138.94 7 0 0 -10 81262.1 3960.25 26 0 0 -10 77539.8 3900.92 28 0 0 10 76196.6 3826.61 1 0 0 -10 81591.7 4007.94 24 0 0 10 75726.8 3418.86 19 0 0 -10 81431.5 3524.60 2 0 0 -10 83992.9 4019.85 25 0 0 -10 80892.5 4172.25 21 0 0 -10 80820.8 3697.90 9 0 0 -11 95230.9 4490.50 26 0 0 -11 91834.9 4430.88 25 0 0 11 85202.2 4327.02 17 0 0 -11 93441.7 4472.97 27 0 0 11 88487.1 3543.66 7 0 0 -11 91709.3 4698.04 21 0 0 -11 93733.7 4192.66 9 0 0 -11 95932.2 4504.04 28 0 0 -11 86350.4 3707.85 3 0 0 11 91589.7 4379.52 1 0 0 -11 89120.4 3923.11 2 0 0 -11 93574.2 4026.20 18 0 0 11 88737.9 3879.61 19 0 0 -11 93117.4 4475.70 24 0 0 -12 11327.7 1430.66 9 0 0 12 7712.04 1315.13 17 0 0 -12 9778.49 1601.53 21 0 0 -12 12596.9 1434.39 2 0 0 12 10371.8 1603.88 10 0 0 -12 11179.2 1566.71 25 0 0 12 11869.9 1179.86 7 0 0 -12 12067.2 1599.36 27 0 0 -12 12354.9 1592.91 26 0 0 12 11310.4 1307.82 19 0 0 -12 13382.9 1494.24 18 0 0 -12 9298.52 1091.68 3 0 0 -12 14521.9 1850.64 15 0 0 12 11474.9 1554.17 1 0 0 -12 11121.0 1516.86 28 0 0 -12 10973.4 1570.88 24 0 0 -13 30302.5 2675.87 27 0 0 -13 34626.2 2846.59 25 0 0 -13 28262.7 2603.86 26 0 0 -13 33622.3 2996.73 21 0 0 13 29189.2 2600.09 17 0 0 -13 36555.1 3041.88 15 0 0 13 36127.4 2982.90 10 0 0 -13 34295.4 2488.40 2 0 0 -13 32510.1 2740.29 28 0 0 -13 38346.9 2693.92 9 0 0 13 39243.1 2949.98 1 0 0 -13 34426.1 2842.80 24 0 0 -13 34816.0 2519.43 18 0 0 -14 347.690 677.381 26 0 0 -14 176.027 638.155 24 0 0 14 533.472 743.005 12 0 0 -14 50.2393 765.813 27 0 0 -14-537.291 702.275 25 0 0 -14-78.8376 586.451 15 0 0 -14-446.128 689.635 21 0 0 -14-544.284 664.248 18 0 0 -14-1029.48 704.392 28 0 0 14 1394.63 955.688 10 0 0 14 165.251 536.765 17 0 0 15 10419.7 1673.01 12 0 -1 15 14800.0 1995.91 12 0 1 -14 17977.9 2168.89 27 0 1 -14 14484.1 1729.68 2 0 1 -14 17569.2 1892.90 18 0 1 -14 15142.0 1983.80 24 0 -1 14 15603.3 1883.66 1 0 -1 14 14569.4 1924.15 17 0 1 -14 12929.9 1791.78 25 0 1 -14 16019.0 2094.21 28 0 1 -14 15606.8 2194.25 21 0 -1 14 18422.5 2266.60 10 0 1 -14 15665.2 2017.22 26 0 1 -14 17958.4 2239.13 15 0 1 -13 19021.9 2126.93 27 0 1 -13 18523.5 2121.54 25 0 1 -13 21530.3 1986.72 2 0 1 -13 19313.8 2243.87 21 0 -1 13 17221.8 2029.90 17 0 1 -13 19285.0 2201.79 15 0 1 -13 19071.8 1880.33 18 0 1 -13 19669.0 2188.56 24 0 1 -13 20109.8 2183.04 28 0 -1 13 17427.9 2117.64 10 0 -1 13 19066.5 2029.17 1 0 1 -13 17987.9 2078.23 26 0 1 -12 6643.72 1101.65 2 0 1 -12 5953.36 1229.87 24 0 -1 12 8324.83 1361.88 1 0 1 -12 6519.12 1067.61 9 0 1 -12 8544.01 1450.99 15 0 -1 12 7050.13 1393.44 10 0 1 -12 6309.53 1126.71 18 0 1 -12 8175.97 1480.63 21 0 1 -12 7446.77 1352.19 27 0 1 -12 6911.74 1250.71 25 0 -1 12 8324.40 1172.45 19 0 1 -12 6041.35 1191.83 26 0 -1 11 9023.95 1173.33 19 0 1 -11 11478.6 1540.23 25 0 1 -11 8745.52 1203.57 2 0 1 -11 8913.43 1357.11 27 0 -1 11 11159.1 1597.27 10 0 1 -11 11483.0 1507.72 24 0 1 -11 8452.68 1345.22 26 0 1 -11 11985.4 1624.85 15 0 1 -11 8780.11 1408.73 21 0 -1 11 11355.2 1124.11 7 0 1 -11 12070.1 1328.94 9 0 -1 11 10358.3 1361.22 1 0 1 -11 10990.4 1308.58 18 0 -1 11 10878.4 1513.31 31 0 1 -10 85221.0 4127.28 30 0 1 -10 79147.4 4233.14 21 0 1 -10 87252.8 4154.24 26 0 -1 10 79885.5 3692.22 19 0 -1 10 83523.6 4204.11 31 0 1 -10 85510.8 3704.97 2 0 1 -10 81906.8 3695.72 18 0 1 -10 87606.4 4169.26 27 0 -1 10 79813.7 3250.62 7 0 1 -10 78122.4 3993.83 24 0 -1 10 77601.0 4077.73 29 0 -1 10 82568.7 3893.89 1 0 1 -10 82257.6 4061.81 25 0 1 -10 89512.0 3751.72 9 0 1 -9 5530.97 1019.56 30 0 -1 9 6222.33 788.244 7 0 1 -9 5765.26 1027.30 24 0 1 -9 4075.65 876.732 26 0 -1 9 5437.08 532.854 4 0 1 -9 5950.90 959.984 2 0 1 -9 5782.73 1022.97 27 0 -1 9 5999.33 1050.51 29 0 -1 9 4540.81 825.970 19 0 1 -9 5883.35 863.106 9 0 1 -9 7348.67 1197.72 21 0 -1 9 4460.70 861.966 1 0 1 -9 6314.42 952.454 18 0 1 -9 4154.56 895.253 25 0 -1 9 5349.17 1028.02 31 0 -1 8 328649. 9946.06 31 0 1 -8 356643. 9213.92 9 0 -1 8 337850. 8210.20 4 0 1 -8 329690. 9197.27 18 0 1 -8 344563. 9870.38 26 0 -1 8 335907. 8682.07 7 0 1 -8 302678. 7532.78 22 0 1 -8 348443. 9915.04 27 0 -1 8 333780. 9970.25 29 0 1 -8 345617. 9898.75 30 0 1 -8 338814. 9873.39 24 0 1 -8 330083. 10003.2 21 0 -1 8 345960. 9533.77 1 0 -1 8 339520. 9370.19 19 0 1 -8 334868. 9826.53 25 0 1 -8 336018. 9177.57 2 0 -1 7 1603.28 283.420 4 0 1 -7 469.597 486.357 30 0 1 -7-67.2331 406.434 27 0 1 -7 318.055 315.708 9 0 -1 7 577.912 444.409 19 0 1 -7-463.857 512.844 25 0 1 -7-75.2883 326.488 2 0 1 -7 491.641 422.528 18 0 -1 7 707.606 410.274 29 0 1 -7 465.195 455.128 24 0 -1 7 46.6607 243.723 7 0 -1 7 230.695 291.730 1 0 1 -7 703.265 590.010 21 0 1 -7 221.886 475.067 26 0 1 -7 675.843 233.429 14 0 -1 7-86.3086 365.819 31 0 1 -6 518515. 13663.3 27 0 1 -6 554736. 13091.9 9 0 -1 6 520824. 12671.9 7 0 1 -6 526858. 13855.4 21 0 1 -6 508297. 13645.2 30 0 1 -6 546383. 12598.7 14 0 1 -6 503637. 12668.2 23 0 -1 6 545349. 12362.6 4 0 1 -6 518476. 13658.8 25 0 -1 6 536252. 13418.1 19 0 1 -6 509089. 13648.5 24 0 1 -6 520220. 13653.7 26 0 -1 6 507447. 13785.9 29 0 -1 6 530013. 13326.7 1 0 -1 6 489508. 13713.9 31 0 1 -6 532312. 13160.7 2 0 1 -6 517729. 13116.3 18 0 1 -5 15455.6 1040.39 2 0 -1 5 15926.7 737.835 4 0 1 -5 14774.4 1251.59 21 0 -1 5 13342.1 1213.39 29 0 -1 5 14699.3 1110.67 19 0 1 -5 13884.1 1157.58 25 0 1 -5 14050.8 1026.00 18 0 1 -5 15612.4 854.601 14 0 -1 5 15511.6 1091.74 1 0 1 -5 13238.1 1127.72 26 0 1 -5 15709.6 1216.35 27 0 1 -5 14187.0 1148.19 30 0 1 -5 14139.7 904.017 23 0 1 -5 14774.5 1170.77 24 0 1 -5 16174.9 1010.24 9 0 -1 5 16522.0 900.818 7 0 -1 5 15342.4 1258.76 31 0 -1 4 275732. 6683.86 4 0 1 -4 285906. 7654.71 24 0 -1 4 290063. 7770.30 29 0 1 -4 275333. 7317.09 1 0 1 -4 296862. 6975.18 7 0 1 -4 274003. 7117.26 23 0 1 -4 287840. 7645.49 26 0 1 -4 281410. 7616.41 25 0 -1 4 275254. 7330.57 1 0 -1 4 289319. 7763.79 31 0 1 -4 287447. 7647.78 27 0 1 -4 290083. 7333.66 2 0 -1 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498.005 609.516 24 0 -10 -3-68.4257 582.832 31 0 -10 -3-151.560 736.587 27 0 -10 -3 747.917 539.645 26 0 10 3 2197.83 826.864 4 0 -10 -3 740.368 590.173 3 0 10 4 129664. 5194.70 6 0 -10 -4 136849. 6136.41 31 0 -10 -4 141352. 6202.91 28 0 -10 -4 139664. 5447.82 3 0 10 4 139745. 5893.97 17 0 -10 -4 138943. 5444.03 11 0 -10 -4 144445. 6266.94 29 0 10 4 150743. 5596.80 12 0 -10 -4 142742. 6226.86 26 0 10 4 137811. 5840.50 30 0 10 4 140125. 5872.15 24 0 10 4 158991. 6354.56 4 0 -10 -4 137885. 5632.88 8 0 -10 -4 141034. 6221.69 27 0 10 4 143632. 5862.68 13 0 -10 -5 365.280 588.682 27 0 10 5-165.888 449.460 12 0 10 5 910.761 725.138 30 0 10 5 592.440 590.039 24 0 -10 -5 592.998 439.787 3 0 10 5 73.2791 597.374 17 0 -10 -5 109.962 520.496 28 0 10 5 732.008 676.597 4 0 -10 -5 631.925 562.128 29 0 10 5-199.666 482.305 13 0 -10 -5-545.678 606.776 11 0 10 5 419.966 511.970 6 0 -10 -5-238.650 532.234 31 0 -10 -5 194.654 566.703 26 0 -10 -6 50622.7 2953.54 3 0 10 6 52860.1 3293.58 12 0 10 6 49991.2 3285.14 30 0 -10 -6 52451.8 3558.71 28 0 -10 -6 50883.6 3504.17 26 0 -10 -6 49436.9 2948.56 11 0 10 6 49936.0 3284.41 24 0 10 6 50037.1 2899.82 6 0 -10 -6 51769.1 3527.20 27 0 -10 -6 49680.6 3457.81 29 0 10 6 46020.8 3132.53 13 0 -10 -6 51841.0 3529.69 31 0 10 6 50546.8 3323.54 17 0 10 6 54957.2 3657.30 4 0 -10 -7 17743.6 2106.21 26 0 -10 -7 17253.3 2101.18 31 0 -10 -7 16606.4 1650.91 3 0 -10 -7 16341.6 2082.67 9 0 -10 -7 14584.6 1585.25 11 0 -10 -7 18268.6 2124.42 27 0 -10 -7 17359.3 2036.81 28 0 10 7 16798.4 1878.55 13 0 10 7 17494.2 1966.02 30 0 10 7 15376.9 1845.69 24 0 10 7 14109.7 1527.44 6 0 10 7 17460.0 1916.89 12 0 10 7 16291.5 1889.25 17 0 10 7 17819.0 2139.56 4 0 -10 -7 17366.3 2064.74 29 0 10 8 11698.0 1605.34 13 0 10 8 15502.1 1906.61 24 0 10 8 15456.8 1565.11 23 0 -10 -8 16516.0 2022.20 27 0 10 8 13255.4 1911.38 4 0 10 8 11995.1 1743.93 12 0 10 8 15728.1 1917.48 17 0 -10 -8 12953.4 1482.41 3 0 -10 -8 15624.6 1673.51 11 0 -10 -8 14309.6 1937.17 26 0 -10 -8 17812.7 2118.44 31 0 10 8 15325.7 1885.67 30 0 -10 -8 12582.2 1959.30 9 0 -10 -8 11807.3 1759.72 28 0 -10 -8 16259.8 2018.28 29 0 -10 -9 40285.4 3281.48 29 0 10 9 43172.2 3444.90 4 0 -10 -9 40473.2 3288.93 28 0 10 9 38928.8 3083.93 24 0 -10 -9 42682.0 3369.89 27 0 -10 -9 41538.4 3628.70 9 0 10 9 38036.3 3250.43 12 0 10 9 42560.6 2594.62 23 0 10 9 36397.8 2905.16 13 0 -10 -9 37734.2 2711.45 11 0 10 9 37523.2 3023.55 30 0 10 9 38805.0 3094.39 17 0 -10 -9 44184.1 3446.44 31 0 -10 -9 40612.5 3295.42 26 0 10 10 27494.4 2869.08 12 0 -10 -10 28326.9 2802.76 26 0 10 10 24697.5 2652.33 4 0 -10 -10 28844.8 2817.93 29 0 10 10 23061.1 2437.66 17 0 -10 -10 25819.6 2701.16 27 0 -10 -10 27062.9 2807.25 28 0 -10 -10 28555.7 2398.72 11 0 10 10 27577.6 2666.63 30 0 -10 -10 25455.8 2951.38 9 0 -10 -11 65272.8 3927.88 11 0 11 -6 30734.3 2921.90 30 0 11 -6 29022.4 2830.06 24 0 11 -6 27860.4 2678.85 13 0 11 -6 27738.0 2652.13 2 0 11 -6 29376.6 2835.80 25 0 -11 6 30928.5 3076.70 28 0 -11 6 25957.6 2816.39 19 0 11 -6 30500.9 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13 0 11 -3 874.173 644.844 30 0 11 -3 1803.46 901.904 2 0 -11 3-279.411 656.081 29 0 11 -3 273.068 704.038 17 0 11 -2 49862.6 3145.53 6 0 11 -2 50078.4 3211.45 2 0 -11 2 54650.6 3759.22 28 0 -11 2 50310.7 3640.05 31 0 -11 2 47974.1 3556.66 19 0 -11 2 50092.1 3616.05 29 0 -11 2 49829.4 3117.09 14 0 11 -2 55887.6 3549.60 24 0 -11 2 49967.5 3434.58 8 0 -11 2 50625.1 3659.03 27 0 11 -2 57371.6 3589.20 30 0 11 -2 52021.0 3416.43 25 0 11 -2 53731.6 3485.95 17 0 11 -2 50158.6 3289.15 13 0 11 -1 1975.91 819.856 24 0 11 -1 1027.31 688.622 13 0 11 -1 1325.75 649.902 17 0 11 -1 2046.72 755.249 6 0 -11 1 2689.18 1000.45 31 0 -11 1 2664.54 1011.76 28 0 11 -1 2421.50 867.302 25 0 -11 1 1439.63 679.969 14 0 -11 1 1821.05 782.707 8 0 11 -1 2193.49 766.781 2 0 -11 1 994.319 660.647 29 0 -11 1 2665.34 1001.81 27 0 11 -1 3134.64 990.063 30 0 -11 1 2849.08 964.992 19 0 -11 0 16149.0 1868.94 8 0 11 0 13938.1 1697.50 17 0 -11 0 12314.0 1551.54 14 0 11 0 15416.8 1764.89 24 0 -11 0 13224.1 1713.75 19 0 -11 0 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2011.40 4 0 -11 -2 25213.0 2248.62 14 0 11 2 23477.7 2145.62 13 0 11 3 53159.5 3304.75 13 0 -11 -3 52683.1 3593.06 27 0 11 3 59139.3 3580.00 4 0 -11 -3 48150.6 2989.27 11 0 -11 -3 44460.3 3102.14 8 0 -11 -3 51859.1 3543.80 29 0 11 3 54150.8 3383.27 24 0 -11 -3 47646.0 3418.36 31 0 11 3 49524.0 3268.88 30 0 -11 -3 46867.8 3006.64 3 0 11 3 48705.1 2904.24 6 0 11 3 46458.5 3179.13 17 0 -11 -3 47929.3 3459.67 28 0 -11 -3 46503.6 3230.77 14 0 11 4 58370.6 3535.69 13 0 -11 -4 50012.7 3606.76 28 0 -11 -4 51699.6 3645.61 29 0 -11 -4 54071.0 3761.64 27 0 11 4 54439.8 3077.72 12 0 -11 -4 51693.1 3672.77 26 0 11 4 63393.1 3841.13 4 0 -11 -4 53722.4 3195.39 11 0 -11 -4 46313.3 3472.38 31 0 11 4 53624.5 3496.43 30 0 -11 -4 58078.9 3638.98 14 0 -11 -4 48453.1 3217.95 8 0 11 4 53044.9 3464.72 24 0 -11 -4 52832.5 3212.15 3 0 11 4 52462.0 3459.72 17 0 11 4 51192.1 3047.19 6 0 11 5 102831. 4721.25 12 0 11 5 101356. 4913.93 13 0 -11 -5 93571.7 4492.38 11 0 -11 -5 97971.1 4586.43 3 0 11 5 113136. 5480.14 4 0 11 5 94441.8 4921.48 17 0 11 5 96644.6 4956.64 24 0 -11 -5 94211.1 5212.92 29 0 -11 -5 104561. 5411.79 28 0 -11 -5 102105. 5366.32 31 0 -11 -5 105548. 5368.63 9 0 11 5 90104.3 4333.67 6 0 -11 -5 99245.1 5297.42 26 0 -11 -5 93910.4 5178.13 27 0 11 5 101194. 5058.68 30 0 -11 -6 35239.9 3051.38 29 0 -11 -6 35712.8 2595.74 3 0 -11 -6 31232.9 2917.32 28 0 -11 -6 36203.9 3133.49 9 0 -11 -6 34127.8 2978.96 26 0 11 6 28169.2 2614.47 30 0 11 6 34482.7 2866.02 24 0 11 6 31129.1 2646.63 13 0 11 6 32799.7 2910.37 4 0 -11 -6 34246.1 3016.58 27 0 11 6 30213.3 2678.31 17 0 -11 -6 32650.1 2480.96 11 0 -11 -6 34741.6 3046.22 31 0 11 6 32309.8 2414.53 6 0 11 6 33648.9 2670.15 12 0 -11 -7 92953.0 5249.29 27 0 -11 -7 89580.6 5258.21 9 0 -11 -7 94842.8 5287.21 29 0 11 7 93581.3 5002.54 24 0 -11 -7 90039.2 5182.36 31 0 -11 -7 89827.5 4457.36 11 0 -11 -7 83753.0 4301.49 3 0 11 7 94250.4 5007.82 30 0 11 7 94265.7 5034.62 17 0 11 7 93494.6 4851.83 13 0 -11 -7 87323.7 5125.91 26 0 11 7 91668.9 4844.26 12 0 11 7 99105.5 5382.08 4 0 -11 -7 85659.5 5056.47 28 0 -11 -8 9100.83 1331.38 3 0 11 8 8722.89 1538.25 12 0 -11 -8 9723.64 1719.25 26 0 -11 -8 9917.40 1741.12 27 0 11 8 9534.19 1526.26 13 0 -11 -8 9742.35 1416.98 11 0 -11 -8 5959.68 1342.71 28 0 -11 -8 9531.82 1700.80 29 0 -11 -8 8802.72 1605.93 31 0 11 8 9542.53 1708.19 4 0 -11 -8 7475.93 1535.67 9 0 11 8 6808.48 1360.08 17 0 11 8 11599.8 1739.22 24 0 11 8 9013.55 1622.36 30 0 11 8 8707.26 1275.45 23 0 -11 -9 33126.5 2645.27 11 0 11 9 38199.3 3271.17 12 0 -11 -9 36209.4 3438.90 9 0 -11 -10 2951.16 928.551 11 0 11 10 1269.34 979.833 12 0 12 -5 899.156 823.571 2 0 12 -4 5601.72 1287.08 25 0 -12 4 3693.87 1110.97 28 0 -12 4 3480.21 1124.37 31 0 12 -4 6271.22 1379.42 30 0 12 -4 4452.18 1178.35 26 0 12 -4 6798.37 1409.61 24 0 -12 4 5781.74 1358.56 29 0 -12 4 4647.53 1256.04 8 0 12 -4 5167.84 1226.18 17 0 12 -4 4102.85 1061.86 2 0 -12 4 4329.31 1299.95 19 0 -12 3 31754.4 3014.74 28 0 -12 3 24378.0 2667.19 31 0 12 -3 29986.9 2674.55 13 0 -12 3 26381.2 2354.12 14 0 12 -3 30313.0 2726.63 30 0 -12 3 29246.3 2908.75 19 0 -12 3 30456.2 2928.01 29 0 -12 3 24785.9 2582.25 8 0 12 -3 25172.7 2519.54 17 0 12 -3 26194.0 2384.66 2 0 12 -3 29228.3 2698.34 24 0 12 -3 27009.4 2461.82 6 0 12 -3 31007.6 2748.18 25 0 -12 2 16507.9 2163.71 31 0 12 -2 18514.3 2096.41 30 0 12 -2 13270.4 1782.11 17 0 12 -2 15766.4 1829.34 2 0 -12 2 16191.2 2147.11 29 0 -12 2 12956.9 1891.73 19 0 12 -2 15920.8 1960.93 24 0 12 -2 10675.4 1566.53 6 0 12 -2 14857.5 1832.94 13 0 -12 2 15402.0 1991.20 8 0 -12 2 13280.4 1934.20 27 0 -12 2 14731.4 1993.99 28 0 -12 2 13659.0 1670.50 14 0 12 -2 16733.6 1976.19 25 0 -12 1 32596.0 2961.18 27 0 12 -1 36992.5 2905.01 13 0 -12 1 31756.0 2894.46 29 0 12 -1 37238.0 2913.50 24 0 12 -1 33879.7 2807.85 17 0 12 -1 34266.8 2791.51 25 0 12 -1 32477.5 2569.58 2 0 -12 1 31686.0 2893.79 19 0 -12 1 32450.3 2609.09 14 0 -12 1 32926.0 2808.87 8 0 -12 1 30795.4 2880.91 31 0 12 -1 29591.3 2460.37 6 0 12 -1 32895.6 2775.68 30 0 -12 1 24695.9 2586.19 28 0 -12 0 14791.7 1904.32 8 0 12 0 17003.0 1843.12 2 0 12 0 17088.2 1939.43 17 0 -12 0 14167.4 1921.95 31 0 -12 0 17478.0 2152.11 28 0 -12 0 13674.1 1855.91 27 0 12 0 16559.6 1925.44 24 0 -12 0 15314.0 1965.07 19 0 12 0 17588.3 1956.91 25 0 12 0 16192.7 1884.85 13 0 12 0 20470.2 2131.88 30 0 -12 0 16790.9 2070.29 29 0 -12 0 18383.6 1962.45 14 0 12 0 14111.1 1647.96 6 0 -12 -1 16186.6 2004.96 29 0 -12 -1 17633.3 2036.61 19 0 12 1 18631.3 1984.34 13 0 -12 -1 15774.6 1988.41 27 0 12 1 18661.3 1977.42 24 0 12 1 18555.3 1945.94 2 0 12 1 16783.3 1762.60 6 0 12 1 19582.8 2054.97 25 0 -12 -1 16403.2 2078.13 31 0 -12 -1 15647.8 1730.14 11 0 -12 -1 15089.6 1838.86 14 0 12 1 18525.5 1995.96 30 0 -12 -1 14491.4 1922.37 28 0 -12 -1 16331.0 1972.63 8 0 12 1 18339.3 1997.10 17 0 12 2 6689.22 1232.50 24 0 -12 -2 6287.87 1161.91 11 0 12 2 7411.44 1173.96 6 0 12 2 7843.42 1398.52 17 0 12 2 10076.6 1555.76 30 0 12 2 8912.80 1408.12 25 0 12 2 7787.82 1219.97 2 0 -12 -2 7662.85 1431.32 27 0 -12 -2 7689.25 1445.46 31 0 -12 -2 8707.57 1531.17 29 0 -12 -2 10404.8 1556.35 14 0 -12 -2 10958.3 1611.54 8 0 12 2 7255.55 1333.50 13 0 -12 -2 7472.57 1448.09 28 0 -12 -3 4855.52 1070.56 28 0 -12 -3 3904.34 1045.29 29 0 12 3 3849.20 1013.86 24 0 -12 -3 3142.87 1159.27 31 0 12 3 4281.06 957.669 6 0 12 3 3323.24 935.705 17 0 12 3 3948.36 1135.27 13 0 -12 -3 3579.15 1069.30 14 0 -12 -3 3779.78 1124.03 27 0 -12 -3 3612.74 983.892 8 0 -12 -3 2809.45 835.234 11 0 12 3 4088.28 1116.21 4 0 12 3 4853.91 1085.62 30 0 12 4 1591.38 942.971 4 0 12 4 2557.73 835.746 6 0 12 4 2949.00 956.852 24 0 -12 -4 1249.41 594.881 31 0 -12 -4 323.041 592.108 29 0 -12 -4 230.442 508.552 11 0 -12 -4 2765.94 1005.99 14 0 -12 -4 1532.93 884.816 27 0 -12 -4 1538.02 815.382 8 0 12 4 354.341 596.681 30 0 12 4 1558.42 741.235 17 0 12 4 1065.80 730.142 13 0 -12 -4 202.242 579.641 28 0 -12 -5 31690.8 3040.85 27 0 12 5 34912.2 2927.51 24 0 12 5 30271.6 2645.56 13 0 -12 -5 33573.0 3071.68 26 0 -12 -5 30983.0 2507.26 11 0 -12 -5 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1570.78 31 -2 8 -1 9358.77 1125.48 12 2 -8 1 8126.69 1145.88 3 2 -8 1 9759.44 1483.98 29 -2 8 -2 69412.9 3767.11 24 -2 8 -2 63152.1 2576.30 18 2 -8 2 66687.4 3951.48 28 -2 8 -2 68573.6 3757.25 30 2 -8 2 63590.9 3874.02 29 2 -8 2 64557.7 3416.35 11 2 -8 2 61450.4 2680.87 10 2 -8 2 63591.3 3861.06 27 -2 8 -2 64661.5 3271.14 6 -2 8 -2 66388.2 3710.31 25 -2 8 -2 59214.2 3293.81 13 2 -8 2 62842.7 3247.47 3 -2 8 -2 72682.4 3173.80 12 2 -8 2 60504.8 3412.71 8 2 -8 2 63651.1 3101.43 20 -2 8 -2 71621.4 3856.64 17 2 -8 2 64289.9 3899.88 31 -2 8 -2 64315.8 3092.57 2 -2 8 -3 613.073 549.248 24 2 -8 3-743.473 646.950 27 2 -8 3-423.950 664.407 8 2 -8 3-69.7024 557.196 28 -2 8 -3 409.749 333.091 18 2 -8 3 15.2040 468.470 14 -2 8 -3 412.156 517.498 25 2 -8 3 178.653 515.285 29 -2 8 -3 132.901 485.912 17 -2 8 -3 3.55187 474.337 13 -2 8 -3 699.989 683.893 30 2 -8 3 450.161 660.191 31 -2 8 -3-410.095 547.148 6 2 -8 3 637.393 339.717 10 2 -8 3 425.349 377.746 20 -2 8 -3 52.1137 381.379 2 -2 8 -4 8582.11 942.728 18 2 -8 4 8674.39 1039.63 14 -2 8 -4 7995.46 1372.08 17 2 -8 4 8383.45 1497.01 28 2 -8 4 7379.23 1415.21 31 -2 8 -4 7929.15 1325.57 30 2 -8 4 7099.66 1184.68 8 -2 8 -4 8572.25 1250.35 13 -2 8 -4 10279.9 1483.33 25 -2 8 -4 8016.93 1353.01 24 2 -8 4 6900.25 1380.98 29 2 -8 4 8442.56 1093.37 10 2 -8 4 8018.04 1129.31 20 2 -8 4 5501.64 1175.10 27 -2 8 -4 7743.71 1068.69 2 -2 8 -5 15070.0 1918.34 30 2 -8 5 11943.0 1521.66 8 2 -8 5 12378.4 1444.14 10 2 -8 5 15384.7 2031.85 29 2 -8 5 14475.7 1902.36 28 -2 8 -5 11985.4 1676.24 24 -2 8 -5 12956.0 1227.23 18 -2 8 -5 14455.7 1678.52 13 2 -8 5 15145.3 1343.02 14 2 -8 5 16534.0 1463.69 1 -2 8 -5 14255.8 1783.17 25 2 -8 5 13583.3 1893.81 31 -2 8 -5 12187.4 1718.48 17 2 -8 5 13549.7 1499.03 20 -2 8 -5 12771.7 1395.61 2 -2 8 -5 12261.9 1676.57 26 -2 8 -6 20821.4 2273.39 25 2 -8 6 15997.6 1905.53 8 2 -8 6 21484.3 2421.74 31 2 -8 6 19110.8 2232.73 29 -2 8 -6 20458.2 2223.40 26 2 -8 6 18603.7 1860.38 10 2 -8 6 18416.1 2201.51 28 -2 8 -6 18972.9 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26 2 -7 -4 22460.4 1627.08 20 2 -7 -4 23085.4 2039.34 26 -2 7 4 23454.4 2001.45 24 -2 7 4 22947.5 1956.12 17 2 -7 -4 22151.0 1999.03 31 2 -7 -4 25827.9 2157.35 29 -2 7 4 19767.1 1602.17 6 -2 7 4 22607.8 1692.91 13 -2 7 4 19590.3 1562.24 23 2 -7 -4 19995.3 1870.77 27 2 -7 -4 19566.1 1555.71 3 -2 7 4 19532.3 1809.59 12 -2 7 4 22195.4 1990.86 4 2 -7 -4 19675.8 1610.79 21 -2 7 4 21514.3 1914.73 30 2 -7 -4 19790.6 1669.28 11 2 -7 -4 21934.1 1984.18 28 2 -7 -3 27094.0 2215.77 27 -2 7 3 27584.0 2125.40 17 2 -7 -3 24071.0 2094.85 26 -2 7 3 24977.7 2054.64 24 2 -7 -3 28668.3 2265.72 29 -2 7 3 23056.4 1973.81 30 -2 7 3 28164.4 1902.21 6 2 -7 -3 24410.1 1602.11 8 -2 7 3 27747.8 1870.80 13 2 -7 -3 28881.2 2276.65 31 2 -7 -3 22118.3 1991.81 28 2 -7 -3 25784.9 1780.29 3 -2 7 3 26479.6 2044.64 12 -2 7 3 31424.1 2283.15 4 2 -7 -3 27036.6 1762.80 20 2 -7 -3 26352.2 1811.93 21 2 -7 -3 25612.6 1870.22 11 -2 7 2 1528.30 570.845 17 -2 7 2 1358.92 481.434 30 2 -7 -2 1073.44 598.364 31 2 -7 -2 1931.33 570.344 20 2 -7 -2 1654.88 463.285 8 2 -7 -2 1951.35 767.785 28 2 -7 -2 2114.32 683.077 27 2 -7 -2 1213.69 593.133 29 2 -7 -2 1550.28 672.483 26 -2 7 2 1025.90 519.068 13 -2 7 2 1202.30 448.933 24 -2 7 2 1600.84 599.967 12 -2 7 2 2020.18 545.613 6 2 -7 -2 2506.71 651.975 11 2 -7 -2 1204.58 457.153 3 2 -7 -1 82970.8 4090.25 31 -2 7 1 89137.6 4016.33 17 2 -7 -1 82032.6 3541.15 8 -2 7 1 82584.5 3890.87 30 2 -7 -1 81123.7 4067.03 27 2 -7 -1 86240.0 4144.45 28 2 -7 -1 75634.0 3497.74 11 -2 7 1 80353.9 3525.66 13 -2 7 1 73266.2 3361.85 6 2 -7 -1 84357.6 4124.81 26 2 -7 -1 77442.1 3426.47 3 -2 7 1 86312.1 3721.03 12 -2 7 1 80941.8 3862.38 24 2 -7 -1 74990.8 3217.35 20 2 -7 -1 88330.1 4186.71 29 2 -7 0 17565.6 1538.47 11 -2 7 0 18475.8 1540.11 12 2 -7 0 15544.5 1435.47 8 2 -7 0 17186.0 1365.33 20 -2 7 0 15717.0 743.524 16 2 -7 0 18531.7 1808.17 31 2 -7 0 16210.1 1737.55 27 -2 7 0 15274.6 1425.73 13 -2 7 0 16976.5 1098.90 18 -2 7 0 17570.2 1645.79 30 2 -7 0 15788.8 1421.13 3 -2 7 0 17053.3 1657.40 24 -2 7 0 15012.9 1369.48 6 2 -7 0 16936.0 1727.81 28 -2 7 0 18595.5 1419.77 2 -2 7 0 18140.8 1711.90 17 2 -7 0 18998.8 1853.03 29 2 -7 0 17264.8 918.414 10 2 -7 1 76246.8 2803.58 10 -2 7 -1 80051.0 2865.26 18 -2 7 -1 87210.1 4078.02 25 -2 7 -1 80326.1 3525.37 6 2 -7 1 80779.4 3723.46 8 2 -7 1 84772.8 4260.93 28 2 -7 1 74734.9 3579.23 11 -2 7 -1 89652.8 3646.08 12 2 -7 1 81023.2 4162.14 31 -2 7 -1 76624.1 3564.46 13 2 -7 1 83028.1 3563.82 3 2 -7 1 82559.4 4181.73 29 -2 7 -1 83924.4 3397.64 2 -2 7 -1 86594.6 4072.44 24 -2 7 -1 90502.5 4129.13 17 2 -7 1 85134.3 3458.41 20 -2 7 -1 85720.7 4048.19 30 2 -7 1 89769.7 4364.39 27 -2 7 -2 62221.9 2591.45 15 -2 7 -2 62940.2 3440.45 30 2 -7 2 63271.0 3680.58 27 2 -7 2 55281.5 2880.40 3 2 -7 2 59553.4 3565.76 29 2 -7 2 54515.7 2436.28 10 2 -7 2 63555.7 3657.25 31 2 -7 2 56542.9 2782.82 20 2 -7 2 54523.9 3017.60 8 -2 7 -2 53163.7 2247.37 18 -2 7 -2 62759.0 3478.58 17 -2 7 -2 61041.0 2802.11 2 -2 7 -2 65469.0 3507.25 25 2 -7 2 59071.9 3548.21 28 -2 7 -2 51674.2 2898.86 13 -2 7 -2 59512.2 3372.77 24 -2 7 -2 66121.5 2946.89 12 -2 7 -2 55892.7 2896.27 6 2 -7 2 60086.4 3116.95 11 -2 7 -3 50598.3 3145.60 17 2 -7 3 47953.6 3228.95 29 2 -7 3 48062.0 3220.70 31 2 -7 3 46754.3 3206.44 28 -2 7 -3 52801.6 2530.93 12 -2 7 -3 49149.4 3111.33 24 2 -7 3 50616.1 3316.82 27 -2 7 -3 52050.0 3172.06 25 -2 7 -3 49496.1 2354.24 15 -2 7 -3 45546.2 2109.42 18 -2 7 -3 45930.3 2467.32 2 -2 7 -3 45999.3 2720.21 13 -2 7 -3 50850.8 3143.55 30 2 -7 3 44948.4 2350.49 10 2 -7 3 49485.4 2607.87 20 2 -7 3 49186.8 2863.20 11 2 -7 3 41927.6 2690.52 8 -2 7 -4 62952.9 2822.82 15 2 -7 4 61085.2 3307.65 8 -2 7 -4 63764.2 3684.13 17 2 -7 4 61678.5 3800.26 28 -2 7 -4 60922.3 3602.33 30 -2 7 -4 60232.2 2992.29 2 -2 7 -4 63297.7 3659.68 24 -2 7 -4 66464.5 3714.47 25 2 -7 4 61214.0 3768.67 31 2 -7 4 61525.3 2821.97 14 -2 7 -4 57151.5 3198.88 13 -2 7 -4 60260.9 2641.98 18 2 -7 4 65970.9 3188.53 20 2 -7 4 59039.4 3726.11 29 2 -7 4 60867.9 3785.57 27 2 -7 4 61959.8 2998.84 10 2 -7 5 18320.6 1657.13 10 2 -7 5 18132.3 1395.10 14 2 -7 5 20878.8 2148.51 28 2 -7 5 21420.9 2197.45 29 -2 7 -5 19564.7 1991.13 26 2 -7 5 16707.4 1931.49 31 -2 7 -5 20980.3 2073.96 17 -2 7 -5 18902.3 1630.76 2 2 -7 5 20031.8 1835.43 8 -2 7 -5 21672.8 1905.92 13 -2 7 -5 17322.3 1888.97 25 -2 7 -5 19401.1 1984.22 24 -2 7 -5 17879.5 1441.79 15 2 -7 5 18134.7 1510.32 1 -2 7 -5 17481.4 1402.01 18 -2 7 -5 19199.1 1977.62 30 2 -7 5 17033.1 1649.49 20 2 -7 6 9517.23 1283.52 10 2 -7 6 8958.41 1522.31 29 2 -7 6 11405.9 1089.30 14 2 -7 6 9820.29 1554.51 28 -2 7 -6 11727.3 1383.05 2 -2 7 -6 9428.75 1464.39 26 -2 7 -6 8506.34 1370.12 17 2 -7 6 9315.62 1388.47 8 -2 7 -6 12378.2 1657.14 24 -2 7 -6 10317.2 1528.42 30 2 -7 6 11299.8 1699.35 31 2 -7 6 10612.6 1144.73 1 2 -7 6 9424.62 1236.86 20 -2 7 -6 11758.4 1615.77 25 -2 7 -6 9406.45 1087.28 18 2 -7 7 19500.7 1921.21 10 -2 7 -7 24101.4 2331.06 17 -2 7 -7 21074.7 1896.51 2 -2 7 -7 18155.5 1606.52 18 2 -7 7 23761.3 2447.44 28 2 -7 7 20174.1 2243.99 31 -2 7 -7 21731.1 2264.24 24 2 -7 7 22382.4 2133.23 8 -2 7 -7 26720.9 2461.32 25 2 -7 7 19096.2 1961.41 20 -2 7 -7 24422.5 2393.11 26 2 -7 7 24807.4 2323.63 19 2 -7 7 23802.2 2457.12 29 -2 7 -7 22472.8 2295.03 30 2 -7 7 22278.2 1696.90 1 2 -7 8 1459.13 872.523 19 -2 7 -8 3281.39 981.470 24 -2 7 -8 854.759 689.942 17 -2 7 -8 774.255 817.989 30 -2 7 -8 1727.51 761.702 26 2 -7 8 1866.12 688.047 10 2 -7 8 1436.17 730.895 20 2 -7 8 891.714 771.911 8 2 -7 8 1246.37 899.525 31 -2 7 -8 2034.02 829.788 25 2 -7 8 424.634 670.784 28 -2 7 -8 1010.20 554.422 2 2 -7 8 1219.53 766.188 29 -2 7 -8 1095.85 587.365 18 -2 7 -9 95721.5 5332.05 30 2 -7 9 94016.3 5422.38 28 2 -7 9 92301.7 4950.60 8 -2 7 -9 98768.8 5411.49 24 2 -7 9 87834.5 5254.37 31 -2 7 -9 98708.5 5380.18 25 -2 7 -9 96322.9 5362.91 17 -2 7 -9 97508.6 5362.90 26 2 -7 9 92745.2 5360.35 29 -2 7 -9 78754.7 4021.90 18 -2 7 -9 81612.0 4396.54 2 2 -7 9 86892.8 4680.57 10 2 -7 9 84234.1 4916.78 19 2 -7 10 1710.43 951.171 19 2 -7 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8244.75 1409.04 2 -2 3 -14 7398.77 1302.44 18 2 -3 14 11189.0 1670.37 19 -2 2 14 31271.4 2486.79 7 2 -2 -14 33562.6 3059.68 9 -2 2 13 11394.5 1467.82 7 2 -2 -13 12747.0 1877.42 27 2 -2 -13 14481.7 2013.23 28 2 -2 -13 13139.1 1590.28 18 2 -2 -13 16283.0 2087.15 26 -2 2 13 15137.0 1947.11 17 2 -2 -13 14615.8 1947.59 25 2 -2 -13 13675.0 1936.66 9 2 -2 -13 12520.9 2080.79 21 -2 2 13 14466.3 2048.10 12 2 -2 -13 14494.5 2010.87 11 -2 2 12 9658.08 1532.95 17 2 -2 -12 11293.6 1744.28 9 2 -2 -12 8508.86 1486.80 28 2 -2 -12 10520.9 1653.04 26 2 -2 -12 9778.64 1614.18 27 2 -2 -12 9712.20 1605.40 25 -2 2 12 7942.91 1167.15 7 -2 2 12 9476.36 1577.05 12 -2 2 12 8709.53 1419.30 10 2 -2 -12 9172.56 1247.20 3 2 -2 -12 11850.6 1422.25 18 2 -2 -12 10953.3 1871.17 21 2 -2 -12 9742.77 1549.46 11 2 -2 -11 9867.73 1239.75 3 -2 2 11 11056.8 1535.86 10 2 -2 -11 9392.44 1449.75 28 2 -2 -11 8095.83 1368.02 9 2 -2 -11 9855.33 1532.57 27 2 -2 -11 9894.81 1463.15 26 2 -2 -11 10893.2 1544.07 25 2 -2 -11 10039.7 1464.95 24 -2 2 11 9339.00 1230.30 7 -2 2 11 8123.93 1267.01 17 2 -2 -11 10954.5 1294.72 18 -2 2 11 7018.02 1341.68 12 2 -2 -11 7202.45 1312.35 11 2 -2 -11 8433.48 1512.83 21 -2 2 10-12.1903 479.970 10 2 -2 -10 475.383 531.484 24 2 -2 -10-295.501 577.493 27 2 -2 -10 476.043 517.513 3 2 -2 -10 865.372 605.074 26 2 -2 -10 687.851 404.535 18 2 -2 -10 478.336 476.091 25 2 -2 -10-443.670 709.446 11 -2 2 10-589.281 618.549 17 -2 2 10 832.013 658.855 12 2 -2 -10 178.178 678.561 21 -2 2 10 342.036 419.878 7 2 -2 -10 77.8586 543.170 28 -2 2 10 446.552 339.792 19 -2 2 9 20841.2 1907.39 10 2 -2 -9 24477.7 2041.11 28 2 -2 -9 23099.6 1983.12 27 2 -2 -9 23673.8 2029.37 26 2 -2 -9 22336.4 2009.58 25 2 -2 -9 24383.0 2067.98 24 -2 2 9 22459.9 1613.05 23 -2 2 9 25603.5 1859.98 7 -2 2 9 23318.1 2131.78 12 2 -2 -9 21482.4 2198.81 21 2 -2 -9 22319.6 1709.58 3 2 -2 -9 26629.4 2173.19 11 2 -2 -9 28322.5 1855.96 18 -2 2 9 26221.7 1679.84 19 -2 2 9 17859.7 1755.86 17 2 -2 -8 1587.40 505.221 18 2 -2 -8 1316.98 590.019 26 2 -2 -8 898.887 473.205 11 -2 2 8 2189.33 551.741 4 2 -2 -8 1480.04 625.416 24 -2 2 8 693.121 314.203 23 2 -2 -8 754.871 533.872 25 2 -2 -8 337.618 446.285 27 2 -2 -8 1684.76 557.168 3 -2 2 8 250.513 524.118 12 -2 2 8 860.581 481.938 17 -2 2 8 1033.96 437.106 10 2 -2 -8-17.2301 708.653 21 -2 2 8 1260.67 497.848 7 2 -2 -8 1078.25 568.610 28 -2 2 8 1342.27 356.467 19 -2 2 7 123951. 5009.42 12 2 -2 -7 123875. 4606.72 28 -2 2 7 119495. 4500.00 17 -2 2 7 120945. 4595.48 10 2 -2 -7 119762. 5062.69 21 2 -2 -7 123503. 4615.69 27 2 -2 -7 126315. 4216.80 18 -2 2 7 122456. 3281.93 22 -2 2 7 120971. 4264.11 4 2 -2 -7 126409. 4660.92 25 -2 2 7 128917. 4522.48 7 -2 2 7 115716. 3443.59 13 2 -2 -7 124435. 4630.15 26 -2 2 7 119321. 4082.07 23 2 -2 -7 123993. 4340.02 3 2 -2 -7 124796. 4727.61 11 -2 2 7 117789. 3981.80 19 2 -2 -6 1557.39 454.891 28 2 -2 -6 2081.09 540.871 3 2 -2 -6 2256.71 614.394 21 -2 2 6 1720.82 504.301 17 2 -2 -6 2437.40 579.292 25 -2 2 6 2372.52 500.340 23 2 -2 -6 1293.03 480.437 27 -2 2 6 1465.62 260.450 13 2 -2 -6 1167.56 467.783 26 -2 2 6 1316.84 475.793 7 -2 2 6 1270.83 407.194 10 -2 2 6 2119.07 305.069 22 -2 2 6 1796.97 537.934 12 2 -2 -6 945.756 369.742 18 -2 2 6 2452.04 538.949 4 2 -2 -6 2163.50 566.968 11 -2 2 6 1902.29 399.843 19 -2 2 5 136605. 4335.58 10 2 -2 -5 141264. 4542.66 25 -2 2 5 134061. 4423.83 30 -2 2 5 134663. 4433.24 17 2 -2 -5 141273. 4528.02 29 -2 2 5 131969. 4832.25 12 2 -2 -5 137436. 4565.24 11 2 -2 -5 142745. 4534.90 28 2 -2 -5 140649. 4946.94 21 -2 2 5 141165. 4617.16 7 -2 2 5 130351. 4437.05 4 -2 2 5 138390. 3705.80 13 2 -2 -5 137501. 4500.38 27 2 -2 -5 138630. 4509.57 26 -2 2 5 137307. 4172.50 23 2 -2 -5 136194. 4143.66 18 -2 2 5 136894. 3701.56 22 2 -2 -5 140991. 4395.43 3 -2 2 5 135491. 4029.66 19 2 -2 -4 4289.28 563.681 29 2 -2 -4 3558.26 555.389 28 2 -2 -4 3456.78 426.491 18 -2 2 4 3986.67 558.607 17 -2 2 4 3951.10 638.870 7 -2 2 4 3569.98 649.657 12 -2 2 4 4350.06 580.260 30 2 -2 -4 3837.12 522.278 3 2 -2 -4 4030.81 596.582 25 2 -2 -4 3187.66 521.485 26 -2 2 4 3876.57 499.362 23 -2 2 4 4293.83 631.670 4 2 -2 -4 3317.24 534.496 27 -2 2 4 3600.58 362.074 13 -2 2 4 3355.49 369.494 22 2 -2 -4 3781.53 662.134 21 -2 2 4 3773.93 445.503 19 2 -2 -4 6027.07 699.960 11 -2 2 4 3003.26 423.366 10 2 -2 -3 3340.58 463.677 3 2 -2 -3 4706.34 582.373 26 -2 2 3 4424.60 393.095 2 2 -2 -3 3690.72 497.028 27 -2 2 3 4295.80 537.496 17 2 -2 -3 3694.67 379.261 18 2 -2 -3 3637.37 504.167 28 2 -2 -3 2691.34 499.671 25 2 -2 -3 4318.70 571.506 29 -2 2 3 4629.45 620.128 7 -2 2 3 3670.35 359.030 13 -2 2 3 3436.89 498.603 30 -2 2 3 3807.22 294.702 8 -2 2 3 2681.53 436.438 23 -2 2 3 4400.78 411.278 10 -2 2 3 4254.18 419.270 22 -2 2 3 3561.39 648.244 12 2 -2 -3 4378.70 644.246 21 -2 2 3 3658.57 519.888 6 2 -2 -3 3873.68 533.873 11 2 -2 -2 45781.1 1440.15 18 2 -2 -2 46558.3 1868.59 29 2 -2 -2 45675.2 1399.16 16 -2 2 2 44801.5 1538.75 13 2 -2 -2 43489.9 1484.57 10 -2 2 2 46846.1 1956.99 7 2 -2 -2 48959.7 1669.38 13 -2 2 2 44252.3 1386.41 8 -2 2 2 46398.2 1829.63 30 2 -2 -2 47135.5 1875.04 26 -2 2 2 47475.6 2181.43 12 2 -2 -2 45821.1 1862.32 27 2 -2 -2 45156.3 1862.18 25 -2 2 2 46995.7 1766.20 23 -2 2 2 45777.6 1566.11 18 -2 2 2 47486.2 1697.77 22 -2 2 2 46577.8 1407.09 2 2 -2 -2 44734.7 2013.42 21 2 -2 -2 45780.4 1760.00 3 -2 2 2 44771.5 1828.91 6 2 -2 -2 47785.5 1882.29 28 2 -2 -2 45382.8 1844.95 11 -2 2 2 44962.8 1827.12 17 -2 2 2 47196.5 1407.31 10 2 -2 -1 42006.4 1169.58 18 2 -2 -1 40837.0 1764.93 26 2 -2 -1 42056.4 1781.68 27 2 -2 -1 40492.6 1159.45 16 2 -2 -1 41703.7 1775.57 31 2 -2 -1 42047.1 1281.11 8 -2 2 1 39359.5 1442.42 13 2 -2 -1 41249.0 1771.99 29 -2 2 1 42363.7 1628.92 22 -2 2 1 42078.5 1749.16 30 2 -2 -1 43776.2 1613.06 13 2 -2 -1 38911.1 1327.52 10 -2 2 1 43846.4 1777.26 24 -2 2 1 41811.4 1613.30 23 -2 2 1 42745.9 2026.33 12 -2 2 1 41052.0 1633.94 6 -2 2 1 40291.7 1269.74 8 2 -2 -1 40916.8 1575.97 3 2 -2 -1 43008.5 1789.60 28 -2 2 1 43090.6 1764.66 17 2 -2 -1 42301.1 1666.16 11 -2 2 1 40874.6 1249.47 18 -2 2 1 41952.4 1707.81 7 2 -2 0 31643.0 1656.00 31 -2 2 0 33485.2 1622.33 30 -2 2 0 34129.1 1640.02 17 2 -2 0 33318.2 1675.91 29 2 -2 0 35450.6 1717.42 26 2 -2 0 32397.7 1660.77 27 -2 2 0 32390.1 1694.86 15 -2 2 0 34204.9 1442.84 22 2 -2 0 32525.0 1315.43 3 2 -2 0 30105.0 1607.89 28 -2 2 0 33738.9 1304.06 13 2 -2 0 31334.2 1296.38 13 2 -2 0 32938.7 1237.41 8 -2 2 0 32205.8 1589.06 24 -2 2 0 30621.9 1334.86 23 -2 2 0 33199.1 1703.85 12 -2 2 0 31640.5 1359.77 6 2 -2 0 32513.8 1416.46 11 2 -2 0 31232.8 1426.86 20 -2 2 0 32363.5 1013.72 16 -2 2 -1 11085.1 889.137 25 -2 2 -1 12516.9 965.004 17 2 -2 1 13862.7 1046.05 29 2 -2 1 12718.5 867.555 20 2 -2 1 13332.7 1036.08 27 2 -2 1 13128.2 710.792 8 -2 2 -1 11379.3 943.937 12 -2 2 -1 12862.4 572.535 2 2 -2 1 11673.5 973.686 31 -2 2 -1 13187.2 969.221 24 -2 2 -1 13350.4 795.929 13 -2 2 -1 12957.6 602.447 16 -2 2 -1 12930.1 973.330 30 2 -2 1 13031.5 770.543 3 -2 2 -1 11704.0 795.881 6 2 -2 1 14053.1 908.028 11 2 -2 1 14475.6 1065.37 28 -2 2 -1 13519.0 990.987 15 2 -2 2 44770.0 1993.43 31 2 -2 2 43096.2 1985.65 27 2 -2 2 46173.0 1717.16 3 -2 2 -2 44151.5 1908.56 12 -2 2 -2 44605.6 1770.62 9 -2 2 -2 44219.7 1884.44 15 -2 2 -2 45227.8 1486.22 2 -2 2 -2 45852.3 1403.33 7 -2 2 -2 43027.1 1917.57 24 2 -2 2 44326.1 1533.37 2 -2 2 -2 42842.2 1917.84 30 -2 2 -2 44227.9 1320.50 18 2 -2 2 46194.2 1907.01 11 -2 2 -2 41288.4 1896.33 17 2 -2 2 49380.7 1953.76 20 2 -2 2 42642.1 1964.25 28 -2 2 -2 44055.7 1914.51 25 2 -2 2 43502.1 1974.98 29 2 -2 2 43849.8 1322.11 18 2 -2 3 54942.5 2305.81 31 -2 2 -3 51972.9 1414.37 7 -2 2 -3 56064.3 2282.00 30 2 -2 3 54154.7 1730.20 18 -2 2 -3 55324.1 2085.68 9 2 -2 3 56555.0 2062.68 3 -2 2 -3 55511.9 2107.23 15 -2 2 -3 55571.0 1890.62 2 2 -2 3 53438.2 2290.30 28 2 -2 3 54353.2 2203.72 11 -2 2 -3 55075.1 1755.01 18 -2 2 -3 56768.6 2287.81 24 -2 2 -3 56598.6 2308.80 17 2 -2 3 55803.4 2248.08 20 2 -2 3 52055.8 2257.37 29 -2 2 -3 54432.9 2241.60 25 2 -2 4 39759.2 2008.05 29 -2 2 -4 41467.6 1984.37 25 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1153.47 30 2 -2 6 10500.9 1132.36 29 -2 2 -6 12258.6 1006.93 2 -2 2 -6 10959.6 1157.29 17 -2 2 -6 10877.8 1085.29 21 2 -2 6 11241.4 1014.45 1 -2 2 -6 12076.8 949.955 18 -2 2 -7 8335.03 740.278 22 -2 2 -7 7807.65 849.759 9 -2 2 -7 6039.15 959.254 25 -2 2 -7 7794.59 941.793 15 -2 2 -7 7819.06 1063.74 26 -2 2 -7 7671.81 1044.90 30 -2 2 -7 8059.11 1101.18 24 2 -2 7 8037.66 921.371 1 2 -2 7 7572.69 1056.24 29 -2 2 -7 7859.41 836.618 18 -2 2 -7 7223.73 845.473 2 -2 2 -7 7462.86 1017.77 21 2 -2 7 7857.56 1007.73 20 2 -2 7 9552.58 1198.51 31 2 -2 8 3387.94 725.243 19 -2 2 -8 2832.28 776.206 21 2 -2 8 2531.53 724.152 31 2 -2 8 3036.63 638.915 1 -2 2 -8 3003.00 718.981 15 2 -2 8 2577.75 445.170 4 -2 2 -8 3160.36 631.884 18 -2 2 -8 2906.95 762.154 26 2 -2 8 2414.44 694.598 29 -2 2 -8 2477.11 519.312 9 2 -2 8 2736.31 274.453 7 -2 2 -8 3252.50 794.473 25 -2 2 -8 2925.17 763.466 30 -2 2 -8 3472.78 485.850 22 -2 2 -8 2429.52 579.194 2 -2 2 -8 2220.61 678.577 27 -2 2 -8 3030.48 758.095 24 2 -2 9 864.531 511.877 19 -2 2 -9 1016.63 604.326 25 2 -2 9 1506.11 582.345 1 -2 2 -9 350.860 572.781 24 -2 2 -9 658.214 541.001 26 -2 2 -9 528.497 454.080 15 -2 2 -9-608.508 702.055 27 -2 2 -9 1390.85 517.609 18 2 -2 9 941.987 351.772 4 -2 2 -9 1113.41 666.958 21 -2 2 -9 1094.41 475.125 9 -2 2 -9 1291.45 350.747 22 -2 2 -9 721.171 485.856 2 2 -2 9 186.263 619.605 31 -2 2 -9 1079.94 593.383 30 2 -2 9 332.793 555.554 29 2 -2 10 16266.8 1676.23 19 -2 2 -10 15162.7 1654.43 15 -2 2 -10 19402.3 1970.57 27 -2 2 -10 19039.4 1980.91 26 2 -2 10 20053.1 2056.16 29 -2 2 -10 16723.7 1841.91 25 -2 2 -10 18228.3 1902.90 24 -2 2 -10 18535.7 1553.37 18 2 -2 10 16488.1 1824.49 31 -2 2 -10 17059.0 1838.87 30 -2 2 -10 18916.8 1584.70 2 2 -2 10 16155.5 1581.57 1 -2 2 -10 15085.0 1738.78 21 -2 2 -10 20466.2 1669.84 9 2 -2 11 118.307 555.854 31 -2 2 -11 372.720 620.764 27 2 -2 11 1182.77 576.917 1 -2 2 -11 1463.15 692.203 2 -2 2 -11 1271.64 708.790 24 -2 2 -11 739.683 718.276 30 -2 2 -11-184.904 681.002 15 -2 2 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68123.1 4660.72 31 -2 2 -14 79279.6 4894.65 27 2 -2 14 73101.1 4298.23 1 -2 2 -14 77178.3 4850.19 24 2 -2 14 74541.8 4815.02 29 -2 2 -14 74333.9 4033.14 2 -2 2 -14 73654.0 4760.16 30 -2 2 -14 71892.0 4672.68 26 -2 2 -14 71323.8 4692.42 21 -2 2 -15 456.944 793.773 15 -2 1 14 5992.72 1473.17 12 -2 1 13 120563. 6104.23 10 -2 1 13 117196. 5681.34 17 -2 1 13 109977. 4941.49 7 2 -1 -13 113662. 5172.13 18 2 -1 -13 122419. 5886.46 28 2 -1 -13 122514. 5891.93 26 2 -1 -13 123198. 5902.33 25 2 -1 -13 120395. 5881.30 24 2 -1 -13 124662. 5806.97 9 -2 1 13 115209. 6032.02 12 2 -1 -13 119944. 6480.79 21 2 -1 -13 120042. 5854.47 27 2 -1 -13 119806. 6050.81 11 2 -1 -12 858.990 774.958 26 2 -1 -12-67.4682 623.328 28 2 -1 -12 262.160 526.998 24 2 -1 -12-633.175 622.621 25 2 -1 -12 248.668 513.792 27 2 -1 -12 286.123 581.481 11 -2 1 12-144.942 561.384 7 2 -1 -12 468.062 496.965 3 -2 1 12 539.788 580.622 17 2 -1 -12 30.6211 511.470 18 -2 1 12 1547.78 915.395 12 2 -1 -12 106.031 728.118 21 2 -1 -12 1183.99 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636.878 30 3 -8 6 1413.82 627.720 10 3 -8 6 1126.34 818.086 31 -3 8 -6 181.866 720.652 17 3 -8 6 1082.58 727.724 28 3 -8 6 387.117 673.823 8 -3 8 -6-155.374 778.839 26 -3 8 -6 1393.59 813.545 25 3 -8 6 1310.60 751.684 29 3 -8 6 1061.66 591.248 1 -3 8 -6 254.935 583.218 24 -3 8 -6 1126.12 560.823 2 3 -8 6 269.662 477.064 20 -3 8 -7 4125.15 1196.74 24 -3 8 -7 4237.22 1144.10 30 3 -8 7 4766.50 1262.91 29 -3 8 -7 2953.39 947.095 17 3 -8 7 4320.98 1121.16 8 -3 8 -7 2772.99 1016.52 26 3 -8 7 3458.41 891.201 10 -3 8 -7 3465.74 1033.76 25 3 -8 7 3599.01 1240.38 28 -3 8 -7 3819.14 850.366 2 3 -8 7 3143.57 945.733 20 3 -8 7 3373.07 1118.13 31 3 -8 8 18813.7 2228.26 19 -3 8 -8 20610.2 2473.06 25 3 -8 8 17962.7 2000.88 10 3 -8 8 21359.2 2683.13 29 3 -8 8 18646.3 2455.45 28 -3 8 -8 23388.0 2655.75 26 -3 8 -8 22363.3 2612.87 30 3 -8 8 21467.2 2349.70 8 -3 8 -8 22042.6 2578.66 24 3 -8 8 21435.7 2647.76 31 -3 8 -8 17977.5 1911.04 2 3 -8 8 18575.3 2091.55 20 -3 8 -8 20838.5 2537.82 17 3 -8 9 187.088 660.860 19 -3 8 -9-89.4522 825.277 26 3 -8 9 2017.97 1027.56 31 3 -8 9 1754.22 957.196 29 -3 8 -9 1034.69 923.993 17 -3 8 -9 2067.37 1011.60 24 3 -8 9 2701.44 1232.34 28 -3 8 -9 1084.98 958.229 30 -3 8 -9 601.982 747.812 25 3 -8 9 752.610 802.007 8 -3 8 -9-802.961 836.831 22 3 -8 9 1669.09 761.775 10 -3 8 -9-508.836 655.881 2 3 -8 9 324.614 771.938 20 3 -8 10 27327.2 2619.52 10 -3 8 -10 21744.7 2248.47 2 3 -7 -11 5257.29 1096.66 3 -3 7 10 39113.0 3227.62 30 -3 7 10 40353.1 3284.46 17 3 -7 -10 42935.4 3535.76 28 3 -7 -10 43847.9 3580.39 29 3 -7 -10 46318.0 3642.83 27 3 -7 -10 44701.8 3610.78 26 -3 7 10 39825.6 3094.57 7 3 -7 -10 36211.0 2702.65 3 -3 7 10 39251.5 3611.98 12 3 -7 -10 41392.8 3554.14 21 3 -7 -10 40371.5 3165.04 11 3 -7 -9 1397.08 644.891 3 3 -7 -9 1494.89 805.839 29 3 -7 -9 2854.28 1025.70 28 -3 7 9 1674.78 756.975 17 3 -7 -9 2752.57 984.521 27 -3 7 9 1940.05 881.351 7 3 -7 -9 2157.37 957.732 26 -3 7 9 1257.38 556.747 23 -3 7 9 2241.64 968.216 12 -3 7 9 2526.96 944.958 30 3 -7 -9 3983.51 1223.13 21 3 -7 -9 3717.04 1076.95 11 -3 7 8 95712.1 4925.22 30 -3 7 8 94602.6 4908.50 17 3 -7 -8 108407. 5369.70 29 3 -7 -8 95892.6 5106.65 28 3 -7 -8 105346. 5345.18 27 -3 7 8 100521. 5538.08 12 -3 7 8 95636.2 4865.92 7 3 -7 -8 102446. 5267.52 26 -3 7 8 88821.8 4141.37 23 3 -7 -8 96227.1 4391.92 3 3 -7 -8 110675. 5503.01 21 3 -7 -8 92717.4 4637.52 11 3 -7 -7 580.561 627.787 3 -3 7 7-183.818 544.765 30 3 -7 -7 337.483 644.983 29 3 -7 -7 1070.75 779.439 27 3 -7 -7 795.823 743.226 28 3 -7 -7 922.703 741.692 26 -3 7 7-451.973 582.381 17 -3 7 7-610.131 635.882 7 -3 7 7 519.193 463.724 23 -3 7 7 517.194 556.142 24 3 -7 -7 864.383 586.276 11 -3 7 7 599.920 759.958 12 3 -7 -7 41.1317 572.276 31 3 -7 -7 874.365 653.940 21 3 -7 -7-415.738 516.078 20 3 -7 -6 98882.0 4856.12 31 -3 7 6 81721.5 3756.81 23 -3 7 6 89236.5 4495.37 30 -3 7 6 87433.1 4459.93 17 3 -7 -6 88937.8 4652.23 29 3 -7 -6 86695.4 4599.96 27 3 -7 -6 96301.8 4809.58 26 -3 7 6 83275.0 4283.98 7 3 -7 -6 89884.1 4635.95 28 -3 7 6 87916.4 4471.24 24 3 -7 -6 88783.9 3939.84 3 -3 7 6 83119.3 4604.61 12 -3 7 6 85253.8 3564.71 22 3 -7 -6 97652.7 4626.09 21 -3 7 6 83868.5 4059.48 6 3 -7 -6 81207.5 4039.67 11 3 -7 -6 85066.2 4005.06 20 3 -7 -5 5537.35 877.485 3 -3 7 5 4829.64 1028.00 30 -3 7 5 5453.62 1123.62 24 3 -7 -5 5162.63 1116.42 26 -3 7 5 4929.37 1026.02 17 3 -7 -5 3444.74 927.310 27 3 -7 -5 4939.96 1070.41 31 3 -7 -5 5633.99 1199.97 29 -3 7 5 6006.58 869.137 13 -3 7 5 4296.79 843.137 23 -3 7 5 5488.41 851.522 22 -3 7 5 4333.62 1026.92 12 3 -7 -5 4000.02 885.083 21 -3 7 5 4665.56 915.470 6 3 -7 -5 6294.06 1020.08 20 3 -7 -5 6244.18 1073.75 11 3 -7 -5 5938.87 1196.66 28 3 -7 -4 9655.63 1403.29 31 3 -7 -4 9283.29 1384.49 28 3 -7 -4 10828.5 1559.52 27 3 -7 -4 7926.08 1308.67 26 -3 7 4 8532.69 1059.74 13 -3 7 4 8132.84 1254.40 24 -3 7 4 7988.97 1031.40 23 -3 7 4 6909.08 979.629 22 -3 7 4 7949.20 1262.32 17 -3 7 4 6404.81 1145.83 12 3 -7 -4 9969.33 1381.86 29 3 -7 -4 8729.96 1154.65 21 -3 7 4 7913.87 1078.06 6 -3 7 4 7650.25 1161.52 30 3 -7 -4 8147.07 1075.45 20 3 -7 -4 7559.87 1152.23 11 3 -7 -4 7086.19 980.700 3 -3 7 3 14876.4 1657.62 30 -3 7 3 14906.6 1646.02 17 3 -7 -3 17535.1 1867.34 28 3 -7 -3 16052.3 1825.37 27 3 -7 -3 15130.2 1128.40 8 3 -7 -3 12404.9 1572.33 26 -3 7 3 14468.0 1354.01 13 3 -7 -3 14583.2 1703.84 31 -3 7 3 15579.8 1718.16 24 -3 7 3 12340.0 1309.62 23 -3 7 3 17456.5 1790.30 12 3 -7 -3 15844.2 1551.30 21 -3 7 3 14448.7 1426.98 6 3 -7 -3 14924.2 1395.66 20 3 -7 -3 14624.5 1494.83 11 3 -7 -3 14489.6 1703.22 29 3 -7 -3 13159.9 1338.39 3 -3 7 2 845.621 530.208 30 -3 7 2 1100.18 587.743 6 3 -7 -2 221.487 578.350 26 3 -7 -2 1271.59 432.861 8 -3 7 2 694.354 429.394 13 -3 7 2 720.921 597.277 17 -3 7 2 1107.53 633.248 24 3 -7 -2 1389.43 686.686 29 3 -7 -2-67.0798 551.506 28 -3 7 2 1005.93 577.208 23 -3 7 2 916.378 534.115 12 3 -7 -2 473.130 481.794 31 3 -7 -2 830.876 535.990 11 3 -7 -2 554.140 450.500 20 3 -7 -2 627.867 483.595 27 3 -7 -2 932.422 457.340 3 3 -7 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3214.14 13 -3 7 -1 67911.3 2876.29 2 3 -7 1 60421.9 3130.65 3 -3 7 -1 73780.4 3809.58 24 3 -7 1 72156.8 4003.95 27 3 -7 1 66698.9 3450.59 11 3 -7 1 66244.4 3178.31 20 -3 7 -1 65203.5 3264.80 6 -3 7 -1 74967.4 3536.44 12 3 -7 2 29721.3 1596.67 10 -3 7 -2 28642.5 2336.24 30 3 -7 2 33127.7 2725.78 27 3 -7 2 26593.7 2424.50 29 -3 7 -2 27648.9 1359.27 16 3 -7 2 25556.1 2012.03 8 -3 7 -2 31527.1 1963.80 15 -3 7 -2 31214.1 2472.05 25 -3 7 -2 26262.8 1677.02 2 -3 7 -2 23012.3 1901.03 13 3 -7 2 27038.8 1978.39 3 -3 7 -2 30099.8 2407.60 24 -3 7 -2 30387.7 2100.76 12 3 -7 2 27996.3 2487.37 28 -3 7 -2 28097.3 2016.18 6 -3 7 -2 28138.5 2345.13 17 3 -7 2 26256.1 2060.30 11 3 -7 2 28012.0 1981.62 20 3 -7 2 28152.5 2492.63 31 3 -7 3 25112.7 1646.00 10 3 -7 3 23971.3 2359.36 28 -3 7 -3 25440.7 2255.54 30 3 -7 3 23686.6 1954.89 8 3 -7 3 25122.5 2410.90 29 -3 7 -3 31765.4 2001.27 15 3 -7 3 30439.3 2644.77 27 -3 7 -3 22218.4 2118.38 17 -3 7 -3 22987.8 1620.34 2 -3 7 -3 25078.8 2267.78 25 3 -7 3 23483.6 2319.25 31 -3 7 -3 23768.9 1975.20 13 3 -7 3 23803.7 1852.12 3 -3 7 -3 29351.5 2408.83 24 -3 7 -3 27833.9 1979.38 12 -3 7 -3 25165.9 1960.14 6 3 -7 3 28644.9 2175.59 11 3 -7 3 20471.5 1769.98 20 3 -7 4 500.134 347.186 10 -3 7 -4-319.276 680.681 30 3 -7 4 2053.94 879.728 31 3 -7 4-644.210 742.573 28 3 -7 4 1183.02 820.630 29 3 -7 4 363.021 664.464 27 3 -7 4-779.594 714.754 8 -3 7 -4 647.262 356.277 15 -3 7 -4 777.203 555.801 13 -3 7 -4 518.278 636.188 25 3 -7 4 657.894 433.671 3 -3 7 -4 1386.49 731.326 17 -3 7 -4 246.612 582.078 24 -3 7 -4-118.888 561.192 6 3 -7 4 449.383 521.326 20 -3 7 -4 1290.60 494.916 2 3 -7 5 2043.15 726.688 1 3 -7 5 1712.51 589.223 8 3 -7 5 2373.80 827.393 29 -3 7 -5 2474.38 810.472 17 -3 7 -5 1307.68 456.198 15 3 -7 5 1670.62 754.649 31 3 -7 5 3710.02 664.304 14 -3 7 -5 2017.68 848.089 25 -3 7 -5 1954.06 760.754 24 3 -7 5 2114.50 604.404 10 3 -7 5 739.031 692.531 28 3 -7 5 3360.94 842.344 20 -3 7 -5 2073.45 527.396 2 -3 7 -5 2380.78 852.908 30 3 -7 6 5030.01 925.123 10 -3 7 -6 8772.26 1472.08 30 3 -7 6 6506.86 1411.97 28 -3 7 -6 5353.90 1218.87 24 -3 7 -6 7943.83 1461.82 25 3 -7 6 6381.20 1154.50 8 -3 7 -6 5902.49 1204.16 17 -3 7 -6 7743.85 1395.37 26 3 -7 6 8220.95 1463.99 29 3 -7 6 4889.85 940.643 1 3 -7 6 8586.64 1552.27 31 -3 7 -6 6071.50 973.739 2 3 -7 6 5864.19 1080.20 20 -3 7 -6 6812.88 1032.05 15 -3 7 -7 193.348 764.755 30 -3 7 -7 1361.58 893.878 26 -3 7 -7 771.816 880.652 17 3 -7 7 293.702 652.277 28 3 -7 7 642.647 806.008 31 3 -7 7-108.749 692.203 29 -3 7 -7 180.454 691.918 25 3 -7 7 119.382 537.336 8 -3 7 -7-571.156 863.785 24 3 -7 7 742.123 459.776 10 3 -7 7 156.037 403.559 1 -3 7 -7-49.0581 492.857 2 3 -7 7 406.391 520.701 20 3 -7 8 14874.3 2135.98 31 3 -7 8 14022.5 1986.27 29 3 -7 8 14687.5 1730.08 10 3 -7 8 13033.4 1703.40 20 -3 7 -8 14161.4 1953.47 30 -3 7 -8 15274.4 2075.47 17 -3 7 -8 17942.8 2223.72 26 -3 7 -8 13974.2 1911.16 25 3 -7 8 14818.8 1837.64 8 -3 7 -8 17013.0 2125.61 24 -3 7 -8 13027.6 1553.29 2 3 -7 8 18978.5 2349.91 28 3 -7 9 21471.3 2316.01 19 3 -7 9 15460.5 1849.59 10 -3 7 -9 16899.5 2232.28 30 -3 7 -9 14564.8 2078.33 17 3 -7 9 14319.3 1946.59 8 -3 7 -9 19383.9 2398.69 26 3 -7 9 15074.2 2142.80 28 -3 7 -9 16979.2 2265.41 24 3 -7 9 16396.0 2260.67 31 -3 7 -9 17085.1 2242.91 25 -3 7 -9 12436.8 1582.24 22 -3 7 -9 14766.2 1698.01 2 3 -7 9 14441.2 1870.19 20 3 -7 9 17149.1 2317.50 29 3 -7 10 1365.85 756.519 19 3 -7 10 2848.28 979.997 10 -3 7 -10 1294.13 943.075 30 3 -7 10 784.230 832.883 29 -3 7 -10 2199.33 958.722 17 3 -7 10 4064.19 1318.78 28 -3 7 -10 3436.50 1277.69 25 3 -7 10 1867.35 1016.05 31 3 -7 10 682.132 775.528 8 -3 7 -10 1467.72 830.491 26 -3 7 -10 3997.05 1500.45 24 -3 7 -10 1839.05 752.032 22 -3 7 -10 2581.44 879.980 2 3 -7 10 2956.63 1063.33 20 3 -7 11 30772.8 2806.55 10 -3 7 -11 31203.1 2684.04 2 3 -7 11 29514.1 2946.78 19 3 -6 -12 63139.1 4892.93 21 3 -6 -11 2461.95 1074.86 25 3 -6 -11 899.608 817.025 27 3 -6 -11 1023.78 790.460 28 3 -6 -11 1150.13 966.984 29 3 -6 -11 337.424 751.605 26 3 -6 -11 11.9770 555.711 3 -3 6 11 1372.56 793.520 30 -3 6 11 821.172 644.448 7 3 -6 -11 600.048 950.432 21 -3 6 11 1152.30 758.684 17 3 -6 -11 2176.45 911.710 11 -3 6 10 24459.9 2422.43 30 3 -6 -10 26854.8 2200.45 3 3 -6 -10 28391.1 2698.26 29 -3 6 10 21566.6 2308.77 17 3 -6 -10 27900.9 2713.83 28 3 -6 -10 25596.5 2616.14 27 3 -6 -10 27383.7 2665.02 26 -3 6 10 28201.6 2496.04 7 3 -6 -10 24418.3 2593.15 25 -3 6 10 24452.4 2779.58 12 3 -6 -10 23163.6 2685.14 21 3 -6 -10 25709.9 2469.47 11 3 -6 -9 25441.9 2448.08 28 -3 6 9 19550.2 2076.12 30 3 -6 -9 17856.8 1785.14 3 3 -6 -9 19975.9 2193.07 27 3 -6 -9 22810.5 2337.36 26 3 -6 -9 21095.3 2268.32 25 3 -6 -9 22967.0 2322.10 29 -3 6 9 21071.9 2126.40 7 -3 6 9 21381.6 1760.58 23 -3 6 9 21456.0 2485.08 12 3 -6 -9 20062.2 2388.27 21 3 -6 -9 21662.2 2099.56 11 -3 6 9 22991.2 2216.10 17 -3 6 8 43484.7 2946.76 30 -3 6 8 42849.4 2960.16 17 3 -6 -8 44563.4 3127.90 28 3 -6 -8 39383.4 2951.90 26 -3 6 8 44116.7 2975.84 7 3 -6 -8 41964.8 3018.22 27 3 -6 -8 46779.4 3191.50 29 3 -6 -8 39068.9 2961.08 25 -3 6 8 41065.4 2454.86 23 -3 6 8 44186.8 3405.36 12 3 -6 -8 41341.6 2603.02 3 3 -6 -8 44138.4 2908.38 11 3 -6 -8 44135.6 3337.21 21 3 -6 -7 100706. 4864.47 27 -3 6 7 101467. 4726.62 17 -3 6 7 93513.3 4012.63 23 -3 6 7 100427. 4688.63 7 -3 6 7 105846. 5247.93 12 3 -6 -7 98872.6 4229.07 3 3 -6 -7 103458. 4882.73 28 3 -6 -7 106097. 4972.40 26 3 -6 -7 106062. 5124.96 21 3 -6 -7 98276.3 4448.55 11 3 -6 -7 106187. 4930.34 29 -3 6 7 103708. 4754.11 30 -3 6 6 53767.8 3197.02 30 -3 6 6 55936.0 3241.61 17 3 -6 -6 56522.1 3346.05 27 3 -6 -6 59124.5 3433.91 29 -3 6 6 52948.4 3163.38 7 3 -6 -6 57212.4 3378.34 26 -3 6 6 50360.2 2668.91 23 3 -6 -6 52070.7 2793.84 3 -3 6 6 56772.0 3554.26 12 -3 6 6 57410.0 2572.83 22 3 -6 -6 58906.2 3481.09 21 3 -6 -6 59269.1 3125.77 11 3 -6 -6 62004.6 3485.11 28 3 -6 -5 158310. 6002.55 29 -3 6 5 149708. 5781.28 17 3 -6 -5 155668. 5971.71 28 3 -6 -5 159517. 6046.08 27 3 -6 -5 159385. 6044.89 31 -3 6 5 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1303.03 282.379 14 -3 4 -6 1256.05 566.292 25 -3 4 -6 1735.43 641.100 26 -3 4 -6 397.832 435.628 24 -3 4 -6 1572.24 471.904 15 -3 4 -6 1633.80 623.360 30 -3 4 -6 814.441 448.189 22 -3 4 -6 1672.48 430.259 18 -3 4 -6 1129.64 408.065 2 3 -4 6 1257.79 497.750 20 -3 4 -7 67178.3 3597.90 30 -3 4 -7 72092.7 2964.37 9 3 -4 7 67617.9 3665.27 29 -3 4 -7 72344.9 3715.87 24 -3 4 -7 65720.4 2991.40 2 -3 4 -7 71261.5 3664.24 26 -3 4 -7 70679.2 3656.05 25 -3 4 -7 64017.6 3086.91 15 -3 4 -7 68943.8 3106.46 22 -3 4 -7 68922.1 2858.50 18 3 -4 7 68101.3 3466.22 20 3 -4 7 68464.2 3682.46 28 3 -4 7 67091.4 3654.61 31 -3 4 -7 74351.7 3756.76 17 3 -4 7 73542.3 3331.24 1 -3 4 -8 24227.7 2121.65 30 -3 4 -8 25380.4 2198.81 17 -3 4 -8 23162.7 1606.71 9 3 -4 8 23599.2 2142.18 28 -3 4 -8 19132.4 1667.04 15 -3 4 -8 23661.6 2080.82 26 -3 4 -8 21057.6 1553.36 18 -3 4 -8 25992.9 2216.30 24 3 -4 8 22004.3 2089.64 31 -3 4 -8 21361.0 1645.25 2 -3 4 -8 19941.9 1570.29 22 3 -4 8 22293.1 1978.97 20 3 -4 8 21157.1 2053.52 29 3 -4 8 22902.7 1833.13 1 -3 4 -8 27146.7 2252.21 25 3 -4 9 28792.8 2551.27 31 -3 4 -9 30822.6 1986.24 18 3 -4 9 26973.7 2490.84 29 -3 4 -9 30924.8 1967.81 9 -3 4 -9 26533.3 2074.95 15 -3 4 -9 32908.1 2655.62 26 -3 4 -9 30810.5 2604.86 30 -3 4 -9 30835.2 2062.19 2 -3 4 -9 31536.8 2642.70 25 -3 4 -9 28895.4 2509.98 24 -3 4 -9 31343.9 1947.66 22 3 -4 9 25909.2 2092.16 1 3 -4 9 30223.6 2442.45 20 3 -4 10 12256.5 1639.43 19 -3 4 -10 12667.8 1213.03 22 -3 4 -10 14421.5 1417.61 18 -3 4 -10 14753.2 1932.06 30 3 -4 10 11927.6 1815.40 29 -3 4 -10 15529.5 1959.30 26 3 -4 10 11378.2 1483.49 1 3 -4 10 12256.8 1829.59 31 -3 4 -10 14732.5 1889.67 25 -3 4 -10 12954.9 1418.17 2 -3 4 -10 11927.0 1463.52 15 -3 4 -10 14440.4 1870.37 24 3 -4 11 7922.06 1395.70 19 3 -4 11 9307.66 1704.69 31 -3 4 -11 7941.78 1528.49 30 -3 4 -11 7451.90 1475.16 25 3 -4 11 9265.68 1644.69 29 -3 4 -11 11357.2 1763.27 27 -3 4 -11 9523.78 1418.49 15 -3 4 -11 12253.9 1900.35 26 3 -4 11 9721.38 1362.68 1 -3 4 -11 7833.39 1484.80 24 -3 4 -11 9117.58 1308.35 2 -3 4 -11 11371.3 1344.98 18 3 -4 12 1779.77 815.714 19 -3 4 -12 658.167 488.326 18 3 -4 12 1765.03 672.870 1 3 -4 12 835.215 854.035 29 -3 4 -12 46.4234 736.567 30 -3 4 -12 343.852 696.971 27 -3 4 -12 2116.22 841.192 15 -3 4 -12-168.858 668.180 26 -3 4 -12 19.0596 924.134 25 -3 4 -12 1077.81 968.492 24 -3 4 -12 1421.56 769.733 2 3 -4 12-338.990 727.000 31 3 -4 13 3416.41 1268.91 31 3 -4 13 2107.05 919.162 8 -3 4 -13 1618.34 762.168 2 -3 4 -13 1687.48 1021.17 27 -3 4 -13 791.123 608.806 15 -3 4 -13 2640.95 1189.71 26 -3 4 -13 793.003 876.511 25 3 -4 13 1289.72 1002.17 29 -3 4 -13 1121.02 864.480 24 -3 4 -13 931.223 632.948 18 -3 4 -13 839.962 761.971 30 3 -4 13 795.079 635.157 19 -3 4 -14-1050.65 725.644 18 -3 4 -14-60.3317 703.212 15 3 -4 14-399.066 803.378 19 3 -3 -13 12952.1 1631.28 18 -3 3 13 14259.5 1959.31 17 3 -3 -13 14884.6 2238.21 9 3 -3 -13 11392.0 1915.83 29 3 -3 -13 10375.5 1736.75 28 3 -3 -13 12896.2 1932.94 27 -3 3 13 14194.4 1923.06 30 3 -3 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27940.9 2330.68 28 4 -4 -8 26733.6 2292.11 27 4 -4 -8 27402.8 2306.38 26 4 -4 -8 26052.8 2267.73 25 -4 4 8 28868.1 2326.56 7 -4 4 8 25147.0 1956.54 23 -4 4 8 25742.5 2652.74 12 4 -4 -8 27791.3 2180.47 3 4 -4 -8 25329.6 2634.56 21 4 -4 -8 25919.7 2268.38 11 4 -4 -7 21904.8 1516.30 18 -4 4 7 21782.4 1881.74 30 -4 4 7 23351.6 1946.86 17 4 -4 -7 22603.2 1991.98 29 4 -4 -7 23147.7 2021.00 28 4 -4 -7 23733.9 2025.94 27 4 -4 -7 19365.7 1863.32 26 4 -4 -7 19071.0 1888.89 25 -4 4 7 21987.1 1978.78 7 -4 4 7 22187.6 1751.96 23 4 -4 -7 22372.4 1909.47 3 -4 4 7 22616.2 2294.19 12 4 -4 -7 22627.4 2361.04 21 4 -4 -7 22702.3 1988.28 11 4 -4 -6 35250.2 1791.35 18 -4 4 6 30341.5 2162.71 30 -4 4 6 29808.6 2165.48 17 4 -4 -6 27791.3 2160.94 29 4 -4 -6 33944.0 2358.45 27 4 -4 -6 34525.0 2379.17 26 4 -4 -6 29380.5 2251.13 25 -4 4 6 30251.8 2289.62 7 4 -4 -6 33426.4 2344.71 28 -4 4 6 31496.6 2023.47 23 -4 4 6 30762.2 2606.92 12 -4 4 6 32623.1 1743.48 22 4 -4 -6 28392.8 2039.59 3 4 -4 -6 32366.4 2647.06 21 4 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4 -4 -3 599.653 481.067 26 4 -4 -3 450.735 424.297 27 -4 4 3 875.589 322.591 13 -4 4 3 722.739 458.419 7 -4 4 3 395.377 362.314 24 -4 4 3 158.385 351.722 23 -4 4 3 844.890 395.368 22 -4 4 3 1599.58 736.019 12 4 -4 -3 1196.11 619.015 21 -4 4 3 277.203 385.323 6 4 -4 -3 492.091 371.923 20 4 -4 -3 1276.64 559.443 11 4 -4 -2 356135. 10325.6 31 -4 4 2 334236. 10021.6 17 -4 4 2 342938. 10056.9 30 4 -4 -2 346546. 10238.0 29 -4 4 2 361263. 10017.8 7 4 -4 -2 356313. 10309.4 28 4 -4 -2 344516. 10253.1 27 4 -4 -2 345539. 10265.4 26 -4 4 2 356526. 9144.96 13 -4 4 2 336457. 10018.2 24 -4 4 2 356436. 9661.84 23 -4 4 2 372449. 10769.1 12 4 -4 -2 350650. 9554.80 3 -4 4 2 363777. 9599.74 22 -4 4 2 352518. 9749.98 6 4 -4 -2 359814. 9861.04 11 4 -4 -2 345280. 9871.32 20 4 -4 -1 10695.5 1220.17 29 -4 4 1 10811.0 1233.31 24 -4 4 1 11423.3 510.263 2 4 -4 -1 13555.5 1422.80 28 4 -4 -1 11108.7 1264.09 27 4 -4 -1 10045.3 694.398 8 -4 4 1 11405.4 1231.13 17 4 -4 -1 10779.0 1283.77 26 4 -4 -1 9622.32 1004.77 3 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57792.2 2221.87 16 4 -4 3 58661.7 3190.11 27 4 -4 3 54710.4 2484.84 8 -4 4 -3 57035.5 3050.10 15 -4 4 -3 58824.7 2108.13 2 4 -4 3 56572.3 3127.78 28 -4 4 -3 57001.2 2162.17 7 -4 4 -3 57396.8 3025.33 25 -4 4 -3 57958.5 3041.25 24 4 -4 3 59163.1 2616.95 3 -4 4 -3 59076.0 2641.47 23 -4 4 -3 58336.1 3057.92 12 -4 4 -3 55801.9 2698.83 6 -4 4 -3 56835.8 2821.34 22 4 -4 3 59170.4 2937.79 11 4 -4 3 58492.3 2869.84 20 -4 4 -4 37293.5 1263.31 18 4 -4 4 38405.3 2494.21 31 -4 4 -4 35441.5 2382.24 17 4 -4 4 36145.9 2469.43 29 4 -4 4 37690.4 2490.00 28 -4 4 -4 34580.6 1744.33 16 4 -4 4 36265.5 1992.17 8 -4 4 -4 35452.3 1675.27 2 -4 4 -4 37705.4 2363.01 15 -4 4 -4 36442.1 2376.34 25 -4 4 -4 35987.8 1413.98 7 -4 4 -4 38320.2 2442.55 24 4 -4 4 34852.9 1980.42 3 -4 4 -4 35071.4 1981.70 23 -4 4 -4 36642.8 2140.21 6 -4 4 -4 33700.2 2163.01 22 4 -4 4 36785.3 2341.80 11 4 -4 4 40457.8 2375.36 20 -4 4 -4 40552.2 2517.94 30 -4 4 -5 161031. 4429.80 18 -4 4 -5 156354. 4940.43 2 -4 4 -5 166863. 6044.54 30 -4 4 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935.149 30 4 -4 10 1291.13 882.376 29 -4 4 -10 1362.70 879.357 25 -4 4 -10 2438.38 713.453 15 -4 4 -10 753.397 663.763 26 -4 4 -10 1958.08 610.411 18 -4 4 -10 1729.09 894.565 24 4 -4 10 1837.63 704.090 1 -4 4 -10 2221.95 771.631 2 -4 4 -10 1206.76 491.519 22 4 -4 10 1588.10 678.297 20 -4 4 -11 23282.8 1857.34 18 -4 4 -11 23719.3 2234.78 15 -4 4 -11 24944.8 2636.92 30 4 -4 11 19681.6 2405.36 29 -4 4 -11 25263.9 2076.91 2 -4 4 -11 25911.1 2650.53 27 -4 4 -11 29296.1 2816.55 26 4 -4 11 22988.5 2587.47 31 -4 4 -11 21196.4 2414.99 25 -4 4 -11 25901.8 2706.36 24 4 -4 11 21973.0 2177.69 1 4 -4 11 23810.2 2490.99 20 4 -4 11 25304.6 2433.56 19 4 -4 12 12238.5 1796.60 19 -4 4 -12 8451.15 1655.62 30 -4 4 -12 7715.49 1381.50 15 4 -4 12 9045.90 1467.64 1 -4 4 -12 12078.8 2027.51 27 -4 4 -12 10435.6 1860.12 26 -4 4 -12 7493.22 1578.52 25 -4 4 -12 9453.10 1748.23 24 -4 4 -12 9294.91 1323.54 2 4 -4 12 7571.61 1662.16 31 4 -4 12 11263.5 1953.78 29 -4 4 -12 10968.2 1366.19 18 4 -4 13 12373.4 1885.91 19 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631.542 24 -8 4 -2 341.989 745.388 23 -8 4 -2-64.5553 763.106 12 -8 4 -2 998.090 781.093 22 -8 4 -2 545.271 474.614 6 8 -4 2-665.376 685.516 11 8 -4 2-183.162 633.912 20 8 -4 3 118525. 5412.24 31 -8 4 -3 117181. 5232.53 30 -8 4 -3 116776. 5237.59 17 8 -4 3 122614. 5472.09 29 8 -4 3 121101. 5448.53 28 -8 4 -3 126702. 6268.49 15 -8 4 -3 119128. 5215.44 25 -8 4 -3 119598. 5260.72 24 8 -4 3 111925. 4892.39 3 -8 4 -3 129121. 6176.90 12 -8 4 -3 118470. 5319.91 23 -8 4 -3 123471. 5535.80 22 -8 4 -3 109802. 4994.47 6 8 -4 3 123155. 5437.51 11 8 -4 3 112653. 5452.87 20 8 -4 4 1279.84 585.165 31 -8 4 -4 171.531 469.826 30 8 -4 4 659.554 557.699 29 -8 4 -4 1951.30 736.473 17 8 -4 4 1943.98 796.143 28 -8 4 -4 3951.52 1128.47 15 -8 4 -4 705.361 574.980 25 -8 4 -4 1106.90 584.957 24 -8 4 -4 410.924 788.424 12 -8 4 -4 947.489 570.579 23 -8 4 -4 2676.51 934.750 22 -8 4 -4 860.931 684.493 6 8 -4 4 2013.10 784.406 11 8 -4 4 327.676 629.833 20 8 -4 4 1922.52 684.232 3 8 -4 5 184376. 7182.17 31 -8 4 -5 185599. 7080.11 30 -8 4 -5 185547. 7109.39 17 8 -4 5 180846. 7197.20 29 8 -4 5 183373. 7171.83 28 -8 4 -5 183199. 7930.89 15 -8 4 -5 181402. 6987.56 26 -8 4 -5 175135. 6923.60 25 -8 4 -5 183561. 7047.07 24 8 -4 5 185236. 6639.43 3 -8 4 -5 179310. 6935.67 23 -8 4 -5 171028. 7137.17 22 -8 4 -5 178569. 6734.02 6 8 -4 5 201180. 7509.81 11 8 -4 5 191673. 7546.11 20 8 -4 6 6692.02 1244.82 31 -8 4 -6 7163.52 1279.50 30 8 -4 6 6022.79 1202.00 29 -8 4 -6 5337.12 1154.94 17 8 -4 6 6454.11 1229.35 28 8 -4 6 4238.15 1182.98 1 -8 4 -6 4037.32 1198.17 15 -8 4 -6 5055.90 1008.15 26 -8 4 -6 5065.57 1079.84 25 -8 4 -6 6084.71 1212.42 24 -8 4 -6 5775.19 1203.45 23 -8 4 -6 4584.19 1111.64 22 -8 4 -6 5165.44 1060.76 6 8 -4 6 4105.47 1073.33 20 8 -4 6 3864.50 837.632 3 8 -4 7 108929. 5289.16 31 -8 4 -7 108955. 5201.62 30 -8 4 -7 107940. 5191.19 17 8 -4 7 109292. 5317.85 29 8 -4 7 108867. 5293.31 28 -8 4 -7 99461.4 4351.93 16 8 -4 7 102219. 5793.18 1 -8 4 -7 97108.1 5541.53 15 -8 4 -7 112322. 5220.49 26 -8 4 -7 105487. 5101.25 25 8 -4 7 97064.5 4539.22 3 -8 4 -7 101401. 5041.56 24 -8 4 -7 96808.8 4750.13 23 -8 4 -7 110270. 5343.91 22 -8 4 -7 98077.9 4731.22 6 8 -4 7 108118. 5541.89 20 8 -4 8 15916.8 1946.40 31 -8 4 -8 14827.3 1842.21 30 8 -4 8 14203.7 1811.96 29 -8 4 -8 17724.2 2062.86 17 8 -4 8 17561.9 2048.19 28 -8 4 -8 15324.4 1600.98 16 -8 4 -8 13256.4 2021.22 15 -8 4 -8 17296.0 1966.29 26 -8 4 -8 18003.1 2034.72 25 8 -4 8 13129.2 2100.80 1 -8 4 -8 14567.5 1825.51 24 -8 4 -8 15388.9 1922.23 22 -8 4 -8 13529.0 1651.50 6 8 -4 8 16694.5 2129.29 20 8 -4 9 22758.9 2399.98 31 -8 4 -9 24702.9 2470.95 30 8 -4 9 22306.6 2405.08 29 -8 4 -9 21314.8 2315.53 17 8 -4 9 24176.8 2518.47 28 -8 4 -9 20496.3 1916.08 16 8 -4 9 21185.3 2156.32 8 -8 4 -9 23006.8 2361.24 26 -8 4 -9 23510.2 2606.56 15 -8 4 -9 22899.2 2373.92 25 -8 4 -9 19716.3 2226.38 24 -8 4 -9 24084.2 2245.71 6 -8 4 -9 24795.7 2414.92 22 8 -4 9 23823.1 2551.58 20 8 -4 9 22922.4 2625.18 1 8 -4 10 51376.6 3833.24 31 8 -4 10 42401.2 3724.89 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3807.76 15 -11 -1 -5 37886.1 3332.17 23 -11 -1 -5 42367.0 3452.88 22 11 1 5 48918.5 3661.34 20 11 1 6 73578.8 4545.54 1 -11 -1 -6 67137.2 3998.80 16 -11 -1 -6 74076.4 5081.72 15 -11 -1 -6 67184.8 4423.84 23 -11 -1 -6 65027.6 4418.56 22 11 1 6 77519.9 4721.45 20 11 1 7 52484.9 3834.61 1 -11 -1 -7 53308.7 3486.43 16 -11 -1 -7 49927.7 3674.21 23 -11 -1 -7 49699.5 3825.33 22 11 1 7 56774.7 4017.31 20 -11 -1 -8 15388.3 1844.30 16 11 1 8 11235.1 1788.45 20 -11 -1 -9 47523.7 3357.21 16 11 1 9 52035.0 3888.46 20 11 1 10 877.036 813.846 20 -11 -2 1 43778.0 3291.07 12 11 2 -1 39266.3 3279.06 20 -11 -2 0 33324.0 3025.43 7 -11 -2 0 32632.8 2807.34 12 11 2 0 30778.1 2570.75 3 11 2 0 31227.2 2831.94 20 -11 -2 -1 52795.4 3701.05 7 -11 -2 -1 55283.7 3657.87 12 -11 -2 -1 46730.4 3794.90 23 -11 -2 -1 46574.5 3445.95 22 11 2 1 46362.6 3483.74 21 11 2 1 43247.0 2967.20 3 11 2 1 47639.3 3572.18 20 11 2 2 4640.35 968.883 3 -11 -2 -2 6726.29 1377.36 7 -11 -2 -2 3731.21 1061.21 23 -11 -2 -2 5698.51 1261.70 22 11 2 2 6277.40 1332.74 20 11 2 3 86058.6 4626.70 1 -11 -2 -3 90581.1 5585.13 15 -11 -2 -3 80700.2 4431.90 7 -11 -2 -3 81529.3 5050.59 23 -11 -2 -3 77903.9 4684.47 22 11 2 3 76745.2 3841.01 3 11 2 3 84900.3 4798.87 20 -11 -2 -4-287.232 841.332 15 11 2 4-993.610 739.898 1 -11 -2 -4 326.943 598.780 7 -11 -2 -4-51.8921 849.850 23 -11 -2 -4 208.834 709.777 22 11 2 4 863.310 739.596 20 11 2 5 140893. 6255.22 1 -11 -2 -5 132224. 5947.32 16 -11 -2 -5 134212. 7008.97 15 -11 -2 -5 124869. 6414.13 23 -11 -2 -5 124734. 6322.28 22 11 2 5 141083. 6488.06 20 -11 -2 -6 2459.88 983.686 16 11 2 6 3015.85 1042.32 1 -11 -2 -6 1108.29 722.838 15 -11 -2 -6 2106.98 911.927 23 -11 -2 -6 1945.73 926.994 22 11 2 6 456.516 602.418 20 11 2 7 158750. 6951.37 1 -11 -2 -7 161875. 7211.97 9 -11 -2 -7 155117. 6530.63 16 -11 -2 -7 153442. 7752.73 15 -11 -2 -7 144081. 6733.54 23 -11 -2 -7 145360. 7045.60 22 11 2 7 165925. 7111.85 20 -11 -2 -8 7349.82 1559.14 9 -11 -2 -8 8164.27 1397.22 16 -11 -2 -8 9449.39 1791.76 15 11 2 8 9419.73 1624.98 1 -11 -2 -8 7596.83 1571.27 22 11 2 8 6142.37 1324.86 20 -11 -2 -9 80588.9 4433.36 16 -11 -2 -9 82506.6 5045.63 22 11 3 -1 57598.0 3882.46 20 11 3 0 4056.91 1020.15 3 -11 -3 0 3698.39 1124.10 7 11 3 0 3756.03 1097.50 21 11 3 0 5319.17 1264.23 20 -11 -3 -1 88692.5 4957.66 7 -11 -3 -1 83533.2 5225.03 23 11 3 1 88417.7 4891.99 21 11 3 1 84138.9 4342.97 3 11 3 1 99195.2 5101.96 20 11 3 2 10603.9 1492.57 1 11 3 2 8863.59 1250.05 3 -11 -3 -2 11559.8 1650.13 7 -11 -3 -2 10190.6 1793.86 23 11 3 2 9286.41 1509.10 21 11 3 2 9829.27 1522.55 20 11 3 3 42597.9 3023.62 1 -11 -3 -3 44655.8 3750.60 15 -11 -3 -3 40851.0 3060.94 7 -11 -3 -3 41084.1 3505.17 23 -11 -3 -3 42521.7 3321.05 22 11 3 3 40109.6 2616.23 3 11 3 3 45364.0 3317.19 20 -11 -3 -4 15771.2 2209.66 15 -11 -3 -4 16608.6 1911.21 7 -11 -3 -4 16005.5 2152.37 23 -11 -3 -4 17088.5 2135.20 22 11 3 4 17406.8 1926.87 1 11 3 4 18737.7 2099.63 20 11 3 5 20940.3 2162.58 1 -11 -3 -5 18339.2 2065.77 16 -11 -3 -5 23801.6 2742.39 15 -11 -3 -5 22509.0 2137.80 7 -11 -3 -5 17733.4 2245.08 23 -11 -3 -5 21841.4 2462.46 22 11 3 5 19912.3 2163.26 20 11 3 6 45596.3 3271.32 1 -11 -3 -6 48256.1 3570.32 9 -11 -3 -6 47042.9 3224.44 16 -11 -3 -6 45677.3 3862.69 15 -11 -3 -6 41617.2 3343.93 23 -11 -3 -6 41156.7 3457.55 22 -11 -3 -7 12273.7 1851.90 9 -11 -3 -7 13298.3 1725.80 16 -11 -3 -7 12075.6 2008.82 15 11 3 7 14388.6 1915.78 1 -11 -3 -7 11158.8 1641.97 23 -11 -3 -7 12239.3 1877.01 22 11 3 8 102852. 5327.24 1 -11 -3 -8 102994. 5536.20 9 -11 -3 -8 91685.8 4833.85 16 -11 -3 -8 91505.4 5751.91 15 -11 -3 -8 97763.5 5513.56 22 11 3 9 14009.4 1976.19 1 -11 -3 -9 12069.4 1664.56 16 -11 -3 -9 16343.8 2406.68 15 -11 -3 -9 15799.0 2118.86 22 -11 -3 -10 94133.2 5440.06 22 -11 -4 0 64594.9 4243.83 7 11 4 0 56432.3 3711.87 21 11 4 0 53417.1 3514.88 3 11 4 1 3890.16 971.303 3 -11 -4 -1 5282.17 1250.58 7 -11 -4 -1 5054.67 1450.58 23 11 4 1 5458.64 1275.21 21 -11 -4 -2 101517. 5180.39 7 -11 -4 -2 90058.9 5420.61 23 11 4 2 97591.7 4922.07 21 11 4 2 89045.9 4324.72 3 11 4 3 1247.31 631.684 3 -11 -4 -3 2118.14 1069.05 15 -11 -4 -3 2217.57 924.735 7 -11 -4 -3 1295.20 786.157 23 11 4 3 1327.43 660.002 1 11 4 4 99766.0 4725.15 1 -11 -4 -4 86054.1 5288.69 15 -11 -4 -4 97447.4 4858.03 7 -11 -4 -4 86898.6 5244.05 23 -11 -4 -5 10206.9 1684.68 9 -11 -4 -5 9647.70 1780.43 15 -11 -4 -5 7798.49 1462.50 23 11 4 5 8881.86 1356.16 1 11 4 6 50756.2 3372.95 1 -11 -4 -6 52514.6 3698.56 9 -11 -4 -6 49447.6 3368.86 16 -11 -4 -6 45117.8 3808.65 15 -11 -4 -6 47608.1 3576.99 23 11 4 7 34404.2 2812.20 1 -11 -4 -7 41330.8 3310.46 9 -11 -4 -7 35204.4 2822.46 16 11 4 7 36316.7 3186.81 4 -11 -4 -7 32185.1 3220.94 15 -11 -4 -7 34405.7 2912.62 23 -11 -4 -8 40176.3 3338.90 9 -11 -4 -8 34262.3 2814.45 16 11 4 8 39025.5 3352.42 4 -11 -4 -8 39995.4 3637.11 15 11 4 8 41758.8 3193.43 1 -11 -4 -9 65372.4 4447.53 9 -11 -4 -9 65859.9 3974.74 16 11 4 9 68190.5 4586.55 4 -11 -4 -9 71146.5 4937.19 15 11 4 9 70028.7 4366.08 1 11 4 10 31721.2 2988.39 1 11 5 -1 4331.30 1065.75 21 11 5 0 21449.6 2190.88 21 11 5 0 21952.0 2231.33 3 11 5 1 23422.7 2318.79 4 -11 -5 -1 21742.9 2381.74 7 -11 -5 -1 23263.4 2671.52 23 11 5 1 20793.8 2169.80 21 11 5 1 20402.7 2085.31 3 11 5 2 26416.5 2525.99 4 -11 -5 -2 29955.5 2702.07 7 -11 -5 -2 27619.6 2881.00 23 11 5 2 27716.0 2384.05 21 11 5 2 25246.7 2152.74 3 11 5 3 82958.8 4789.54 4 -11 -5 -3 82658.9 4617.71 7 -11 -5 -3 82916.3 5110.26 23 11 5 3 90443.3 4573.16 21 11 5 4 45169.5 3413.93 4 -11 -5 -4 42842.1 3485.10 15 -11 -5 -4 42697.0 3548.24 23 11 5 5 98236.0 4708.27 1 -11 -5 -5 100348. 5305.13 9 11 5 5 98842.3 5372.57 4 -11 -5 -5 104536. 5682.77 15 -11 -5 -5 92127.2 5317.11 23 -11 -5 -6 25634.2 2537.37 9 -11 -5 -6 17557.0 2026.25 16 -11 -5 -6 22266.1 2560.61 15 11 5 6 22367.1 2489.67 4 -11 -5 -6 18629.2 2211.76 23 11 5 6 21189.8 2056.55 1 -11 -5 -7 65826.9 4275.93 9 -11 -5 -7 63037.5 3871.12 16 11 5 7 63329.6 4307.87 4 -11 -5 -7 63783.2 4508.56 15 -11 -5 -7 63622.6 4008.43 23 11 5 7 70123.4 4001.16 1 -11 -5 -8 520.624 635.962 9 -11 -5 -8 1619.17 821.051 16 -11 -5 -8-101.445 893.252 15 11 5 8 756.003 753.680 4 11 5 8-350.867 546.847 1 -11 -5 -9 59313.1 4155.21 9 -11 -5 -9 50218.6 3465.75 16 11 5 9 54331.8 4058.48 4 -11 -5 -9 60679.0 4457.19 15 11 5 9 53493.7 3736.52 1 -11 -5 -10 5421.05 1394.75 15 11 5 10 5413.56 1354.04 1 11 6 -1 18954.1 2123.67 21 11 6 0-44.8977 634.640 3 11 6 0-797.161 714.899 21 11 6 1 11766.3 1564.19 3 11 6 1 12781.1 1659.20 21 11 6 2 2913.99 885.369 3 11 6 2 738.000 649.050 4 -11 -6 -2 989.035 721.017 7 -11 -6 -2 1331.28 900.805 23 11 6 2 374.627 535.803 21 11 6 3 35089.3 2968.07 4 -11 -6 -3 33544.5 3120.58 23 11 6 3 36514.2 2698.80 21 -11 -6 -4 3649.35 1013.22 9 -11 -6 -4 4286.64 1104.84 15 11 6 4 3858.34 1157.66 4 -11 -6 -4 5664.79 1470.64 23 11 6 4 2938.64 816.515 21 -11 -6 -5 60238.3 4002.11 9 11 6 5 60303.1 4085.18 4 -11 -6 -5 59971.3 4083.48 15 -11 -6 -5 64004.2 4230.71 23 -11 -6 -6 31233.8 2825.09 9 11 6 6 31643.3 2953.17 4 -11 -6 -6 27224.6 2770.40 15 11 6 6 33254.7 2376.13 13 11 6 6 32921.0 2559.10 1 -11 -6 -7 84868.3 4873.51 9 -11 -6 -7 71814.3 4275.65 16 11 6 7 80619.3 4902.70 4 -11 -6 -7 75826.5 4812.01 15 11 6 7 74173.4 4170.82 1 -11 -6 -8 47277.1 3643.51 9 -11 -6 -8 44005.8 3237.61 16 11 6 8 48490.8 3735.18 4 -11 -6 -8 46552.2 3776.30 15 11 6 8 45262.6 3290.35 1 -11 -6 -9 21924.7 2506.01 9 -11 -6 -9 19275.1 2479.37 15 11 6 9 21659.1 2357.74 1 -11 -6 -10 42312.3 3733.41 15 11 6 10 47320.5 3581.71 1 11 7 0 30450.7 2705.38 3 11 7 1 21823.8 2131.45 18 11 7 1 21031.4 2163.63 3 11 7 2 26393.7 2334.22 18 11 7 3-49.8675 688.181 18 -11 -7 -3 2164.17 1094.90 5 11 7 3 3227.34 1089.93 4 -11 -7 -4 37516.4 3546.76 5 11 7 4 36354.5 2818.46 18 -11 -7 -4 33041.6 2887.14 9 11 7 4 35037.2 3041.62 4 -11 -7 -4 39064.0 3047.45 15 11 7 5 1897.77 709.850 18 -11 -7 -5 1906.72 1091.14 5 -11 -7 -5 3944.06 1150.53 9 -11 -7 -5 2435.95 817.052 15 11 7 5 3681.57 1176.76 4 -11 -7 -6 79767.4 5316.61 5 -11 -7 -6 78470.2 4649.86 9 11 7 6 79549.3 4875.27 4 -11 -7 -6 71972.6 4518.26 15 11 7 6 79698.7 3987.42 13 -11 -7 -7 650.782 729.659 5 -11 -7 -7 3201.70 1105.00 9 -11 -7 -7-534.530 848.661 16 -11 -7 -7 1646.64 918.427 15 11 7 7 320.076 895.839 4 11 7 7 1320.89 694.436 13 -11 -7 -8 109755. 6242.81 5 -11 -7 -8 107282. 5720.92 9 11 7 8 98658.0 5705.43 4 -11 -7 -8 98481.3 5580.50 15 11 7 8 101098. 4826.67 13 11 7 8 97655.9 5022.91 1 -11 -7 -9 6216.28 1526.49 9 -11 -7 -9 5115.11 1361.15 15 11 7 9 5576.28 1182.69 1 -11 -7 -10 87291.5 5335.70 15 11 7 10 80494.3 4813.03 1 11 8 1 3044.73 948.341 18 11 8 1 2170.54 744.264 3 11 8 2 41740.4 3102.24 18 11 8 3 5704.75 1181.39 18 11 8 3 4954.84 1179.65 4 11 8 4 39757.0 3066.48 18 -11 -8 -4 42763.0 3187.70 9 11 8 4 32347.0 2982.77 4 11 8 5 6925.94 1289.00 18 -11 -8 -5 8104.31 1420.15 9 11 8 5 8182.72 1562.29 4 11 8 6 7021.28 1420.82 4 11 8 6 9691.70 1348.50 13 -11 -8 -7 26366.6 2681.80 9 11 8 7 24271.5 2685.73 4 11 8 7 20503.9 1990.52 13 -11 -8 -8 9663.28 1683.99 9 -11 -8 -8 7732.93 1474.52 15 11 8 8 8326.42 1358.80 13 -11 -8 -9 72892.3 4590.74 15 11 8 9 69949.5 4078.31 13 -11 -8 -10 9213.81 1657.03 15 11 8 11 73198.4 4673.63 1 11 9 3 39142.1 3089.17 18 11 9 4 2303.57 956.956 18 11 9 4 1637.30 874.895 4 11 9 5 44640.5 3451.34 18 11 9 5 38384.0 3396.72 4 -11 -9 -6 1767.59 882.963 9 11 9 6 1244.43 714.776 4 11 9 6 1739.96 818.110 13 -11 -9 -7 26972.1 2760.23 9 11 9 7 23433.5 2207.89 13 -11 -9 -8 19298.5 2348.90 9 11 9 8 14538.9 1771.76 13 11 10 5 17484.6 2240.60 4 11 10 6 40403.2 2986.08 13 -12 -1 -6 15873.0 1986.31 16 12 2 3 8233.39 1577.73 20 12 2 4 4601.03 1205.94 20 -12 -2 -6 2312.64 1043.45 23 12 3 3 1650.01 812.433 1 -12 -3 -3 1263.37 871.025 7 12 3 4 2304.79 926.335 1 12 3 5 370.336 573.603 1 -12 -3 -5-129.635 825.999 23 -12 -3 -6 10494.7 1819.87 23 12 3 6 14086.6 1913.22 1 -12 -4 -4 3931.25 1090.01 7 -12 -4 -5 1134.33 692.895 23 12 4 5 2148.23 876.544 1 12 4 6-87.7167 497.417 1 -12 -4 -6 910.953 633.844 23 12 4 7 2980.20 939.531 1 12 5 3 11701.7 1832.46 4 12 5 3 12483.7 1755.65 21 12 5 4 2104.93 936.520 21 -12 -5 -5 10170.8 1873.02 23 12 5 6 4617.75 1098.88 1 -12 -5 -6 3725.77 1173.43 23 12 5 7 5246.26 1218.69 1 12 5 8 1074.24 830.897 1 12 6 3 1997.02 833.924 4 12 6 3 1937.30 762.197 21 12 6 4 1956.90 893.399 4 12 6 4 2637.18 901.242 21 -12 -6 -5 9219.33 1720.40 15 -12 -6 -6 1950.24 865.192 15 12 6 8 5545.67 1225.68 1 -12 -7 -5 2683.59 1050.29 15 -12 -7 -6 3898.77 1166.73 15 -12 -7 -7-564.476 859.486 15 12 7 8 8316.47 1294.42 13 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 77560 _shelx_res_file ; TITL Kiwi in P-1 shelx.res created by SHELXL-2019/3 at 11:28:49 on 07-Nov-2023 CELL 0.71073 8.6067 10.1161 11.5123 77.873 70.257 71.867 ZERR 2.00 0.0008 0.0012 0.0012 0.010 0.010 0.010 LATT 1 SFAC C H P S BR AU UNIT 22 50 2 2 6 2 TEMP -173 SIZE 0.2 0.2 0.2 ACTA 60 CONF 2.3 BOND $H FMAP 2 PLAN 10 L.S. 6 OMIT 2 3 1 HTAB C13 AU1 HTAB C21 S1 HTAB C12 S1 HTAB C3 BR3 HTAB C12 BR2 EQIV $1 1-x,1-y,1-z HTAB C13 BR2_$1 EQIV $2 1-x,1-y,-z RTAB CONT S1 S1_$2 WGHT 0.012200 1.180200 EXTI 0.005567 FVAR 3.38176 AU1 6 0.464119 0.357945 0.234398 11.00000 0.01042 0.00647 = 0.00921 -0.00260 -0.00286 -0.00031 BR1 5 0.533500 0.123217 0.343922 11.00000 0.02234 0.00864 = 0.01814 0.00053 -0.00895 -0.00152 BR2 5 0.749927 0.375896 0.207486 11.00000 0.01064 0.01396 = 0.01718 -0.00448 -0.00497 -0.00019 BR3 5 0.195290 0.322209 0.239359 11.00000 0.01402 0.01009 = 0.02811 -0.00517 -0.00674 -0.00327 P1 3 0.215041 0.722997 0.245170 11.00000 0.00736 0.00623 = 0.00721 -0.00103 -0.00218 -0.00126 S1 4 0.407915 0.586004 0.131114 11.00000 0.01131 0.00841 = 0.00755 -0.00185 -0.00086 -0.00064 C1 1 0.252736 0.705908 0.399635 11.00000 0.01173 0.01002 = 0.00743 -0.00192 -0.00404 -0.00063 C2 1 0.227126 0.896083 0.150269 11.00000 0.01341 0.00730 = 0.00947 0.00008 -0.00265 -0.00294 C3 1 0.009474 0.683388 0.271495 11.00000 0.01001 0.00837 = 0.01424 0.00093 -0.00531 -0.00331 AFIX 13 H3 2 0.027169 0.582577 0.306905 11.00000 -1.20000 AFIX 0 C11 1 0.148090 0.835302 0.469035 11.00000 0.01509 0.01321 = 0.01337 -0.00585 -0.00316 -0.00117 AFIX 137 H11A 2 0.188266 0.917296 0.422652 11.00000 -1.50000 H11B 2 0.162709 0.818416 0.552175 11.00000 -1.50000 H11C 2 0.026852 0.852351 0.476344 11.00000 -1.50000 AFIX 0 C12 1 0.442562 0.686946 0.384564 11.00000 0.01105 0.01854 = 0.01457 -0.00429 -0.00622 -0.00033 AFIX 137 H12A 2 0.512084 0.606051 0.339530 11.00000 -1.50000 H12B 2 0.459923 0.671395 0.466740 11.00000 -1.50000 H12C 2 0.476683 0.771305 0.337815 11.00000 -1.50000 AFIX 0 C13 1 0.201000 0.574820 0.478079 11.00000 0.01808 0.01032 = 0.00912 -0.00005 -0.00400 -0.00166 AFIX 137 H13A 2 0.227809 0.559330 0.556900 11.00000 -1.50000 H13B 2 0.264247 0.493282 0.432585 11.00000 -1.50000 H13C 2 0.077974 0.588312 0.494739 11.00000 -1.50000 AFIX 0 C21 1 0.260157 0.884650 0.012171 11.00000 0.02168 0.01193 = 0.01069 0.00087 -0.00542 -0.00534 AFIX 137 H21A 2 0.373120 0.821183 -0.019419 11.00000 -1.50000 H21B 2 0.256084 0.977510 -0.035458 11.00000 -1.50000 H21C 2 0.172280 0.847983 0.003539 11.00000 -1.50000 AFIX 0 C22 1 0.058077 1.008076 0.194436 11.00000 0.01592 0.00766 = 0.01799 -0.00076 -0.00527 -0.00095 AFIX 137 H22A 2 0.070696 1.100103 0.150803 11.00000 -1.50000 H22B 2 0.029741 1.009738 0.284121 11.00000 -1.50000 H22C 2 -0.033703 0.985600 0.176468 11.00000 -1.50000 AFIX 0 C23 1 0.375685 0.942156 0.160093 11.00000 0.01670 0.01274 = 0.01701 -0.00026 -0.00405 -0.00768 AFIX 137 H23A 2 0.386915 1.028408 0.104086 11.00000 -1.50000 H23B 2 0.481998 0.868304 0.136720 11.00000 -1.50000 H23C 2 0.353000 0.959173 0.245746 11.00000 -1.50000 AFIX 0 C31 1 -0.031481 0.690612 0.150039 11.00000 0.01858 0.01797 = 0.02102 0.00109 -0.01253 -0.00806 AFIX 137 H31A 2 -0.071273 0.788820 0.117928 11.00000 -1.50000 H31B 2 -0.121040 0.642829 0.166014 11.00000 -1.50000 H31C 2 0.071737 0.644795 0.088671 11.00000 -1.50000 AFIX 0 C32 1 -0.147391 0.762100 0.367497 11.00000 0.00840 0.01440 = 0.02175 -0.00064 -0.00237 -0.00233 AFIX 137 H32A 2 -0.246278 0.727637 0.377566 11.00000 -1.50000 H32B 2 -0.172299 0.862586 0.338601 11.00000 -1.50000 H32C 2 -0.123437 0.746175 0.447427 11.00000 -1.50000 AFIX 0 HKLF 4 REM Kiwi in P-1 REM wR2 = 0.0362, GooF = S = 1.135, Restrained GooF = 1.135 for all data REM R1 = 0.0174 for 5057 Fo > 4sig(Fo) and 0.0192 for all 5297 data REM 163 parameters refined using 0 restraints END WGHT 0.0122 1.1801 REM Highest difference peak 1.077, deepest hole -1.426, 1-sigma level 0.126 Q1 1 0.3843 0.4034 0.2325 11.00000 0.05 1.08 Q2 1 0.5608 0.3043 0.2352 11.00000 0.05 0.84 Q3 1 0.6052 0.3625 0.2311 11.00000 0.05 0.81 Q4 1 0.3070 0.3586 0.2461 11.00000 0.05 0.77 Q5 1 0.5970 0.3435 0.1459 11.00000 0.05 0.77 Q6 1 0.6572 0.4203 0.2117 11.00000 0.05 0.73 Q7 1 0.4164 0.2837 0.2488 11.00000 0.05 0.73 Q8 1 0.5117 0.4219 0.2187 11.00000 0.05 0.72 Q9 1 0.6342 0.1371 0.3503 11.00000 0.05 0.66 Q10 1 0.2177 0.3509 0.1783 11.00000 0.05 0.63 ; _shelx_res_checksum 17185 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Au Au1 0.46412(2) 0.35795(2) 0.23440(2) 0.00889(3) Uani d 1 . . Br Br1 0.53350(3) 0.12322(2) 0.34392(2) 0.01652(5) Uani d 1 . . Br Br2 0.74993(3) 0.37590(2) 0.20749(2) 0.01400(5) Uani d 1 . . Br Br3 0.19529(3) 0.32221(2) 0.23936(2) 0.01676(5) Uani d 1 . . P P1 0.21504(7) 0.72300(6) 0.24517(5) 0.00701(10) Uani d 1 . . S S1 0.40792(7) 0.58600(6) 0.13111(5) 0.00991(10) Uani d 1 . . C C1 0.2527(3) 0.7059(2) 0.3996(2) 0.0098(4) Uani d 1 . . C C2 0.2271(3) 0.8961(2) 0.1503(2) 0.0104(4) Uani d 1 . . C C3 0.0095(3) 0.6834(2) 0.2715(2) 0.0105(4) Uani d 1 . . H H3 0.027169 0.582577 0.306905 0.013 Uiso calc 1 . . C C11 0.1481(3) 0.8353(2) 0.4690(2) 0.0141(5) Uani d 1 . . H H11A 0.188266 0.917296 0.422652 0.021 Uiso calc 1 . . H H11B 0.162709 0.818416 0.552175 0.021 Uiso calc 1 . . H H11C 0.026852 0.852351 0.476344 0.021 Uiso calc 1 . . C C12 0.4426(3) 0.6869(3) 0.3846(2) 0.0146(5) Uani d 1 . . H H12A 0.512084 0.606051 0.339530 0.022 Uiso calc 1 . . H H12B 0.459923 0.671395 0.466740 0.022 Uiso calc 1 . . H H12C 0.476683 0.771305 0.337815 0.022 Uiso calc 1 . . C C13 0.2010(3) 0.5748(2) 0.4781(2) 0.0132(4) Uani d 1 . . H H13A 0.227809 0.559330 0.556900 0.020 Uiso calc 1 . . H H13B 0.264247 0.493282 0.432585 0.020 Uiso calc 1 . . H H13C 0.077974 0.588312 0.494739 0.020 Uiso calc 1 . . C C21 0.2602(3) 0.8846(2) 0.0122(2) 0.0147(5) Uani d 1 . . H H21A 0.373120 0.821183 -0.019419 0.022 Uiso calc 1 . . H H21B 0.256084 0.977510 -0.035458 0.022 Uiso calc 1 . . H H21C 0.172280 0.847983 0.003539 0.022 Uiso calc 1 . . C C22 0.0581(3) 1.0081(2) 0.1944(2) 0.0144(5) Uani d 1 . . H H22A 0.070696 1.100103 0.150803 0.022 Uiso calc 1 . . H H22B 0.029741 1.009738 0.284121 0.022 Uiso calc 1 . . H H22C -0.033703 0.985600 0.176468 0.022 Uiso calc 1 . . C C23 0.3757(3) 0.9422(2) 0.1601(2) 0.0150(5) Uani d 1 . . H H23A 0.386915 1.028408 0.104086 0.023 Uiso calc 1 . . H H23B 0.481998 0.868304 0.136720 0.023 Uiso calc 1 . . H H23C 0.353000 0.959173 0.245746 0.023 Uiso calc 1 . . C C31 -0.0315(3) 0.6906(3) 0.1500(2) 0.0172(5) Uani d 1 . . H H31A -0.071273 0.788820 0.117928 0.026 Uiso calc 1 . . H H31B -0.121040 0.642829 0.166014 0.026 Uiso calc 1 . . H H31C 0.071737 0.644795 0.088671 0.026 Uiso calc 1 . . C C32 -0.1474(3) 0.7621(3) 0.3675(2) 0.0158(5) Uani d 1 . . H H32A -0.246278 0.727637 0.377566 0.024 Uiso calc 1 . . H H32B -0.172299 0.862586 0.338601 0.024 Uiso calc 1 . . H H32C -0.123437 0.746175 0.447427 0.024 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Au1 0.01042(5) 0.00647(4) 0.00921(4) -0.00031(3) -0.00286(3) -0.00260(3) Br1 0.02234(13) 0.00864(10) 0.01814(11) -0.00152(9) -0.00895(9) 0.00053(8) Br2 0.01064(11) 0.01396(10) 0.01718(11) -0.00019(8) -0.00497(8) -0.00448(8) Br3 0.01402(11) 0.01009(10) 0.02811(13) -0.00327(8) -0.00674(10) -0.00517(9) P1 0.0074(2) 0.0062(2) 0.0072(2) -0.00126(19) -0.00218(19) -0.00103(18) S1 0.0113(3) 0.0084(2) 0.0075(2) -0.00064(19) -0.00086(19) -0.00185(18) C1 0.0117(10) 0.0100(9) 0.0074(9) -0.0006(8) -0.0040(8) -0.0019(7) C2 0.0134(11) 0.0073(9) 0.0095(10) -0.0029(8) -0.0026(8) 0.0001(7) C3 0.0100(10) 0.0084(9) 0.0142(10) -0.0033(8) -0.0053(8) 0.0009(8) C11 0.0151(11) 0.0132(10) 0.0134(11) -0.0012(9) -0.0032(9) -0.0058(8) C12 0.0110(11) 0.0185(11) 0.0146(11) -0.0003(9) -0.0062(9) -0.0043(9) C13 0.0181(12) 0.0103(10) 0.0091(10) -0.0017(9) -0.0040(8) -0.0001(8) C21 0.0217(12) 0.0119(10) 0.0107(10) -0.0053(9) -0.0054(9) 0.0009(8) C22 0.0159(11) 0.0077(10) 0.0180(11) -0.0010(8) -0.0053(9) -0.0008(8) C23 0.0167(12) 0.0127(10) 0.0170(11) -0.0077(9) -0.0040(9) -0.0003(9) C31 0.0186(12) 0.0180(11) 0.0210(12) -0.0081(10) -0.0125(10) 0.0011(9) C32 0.0084(11) 0.0144(11) 0.0217(12) -0.0023(9) -0.0024(9) -0.0006(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag S1 Au1 Br3 . . 93.532(19) y S1 Au1 Br2 . . 87.959(19) y Br3 Au1 Br2 . . 172.720(9) y S1 Au1 Br1 . . 177.293(16) y Br3 Au1 Br1 . . 89.099(14) y Br2 Au1 Br1 . . 89.510(14) y C3 P1 C2 . . 112.57(10) y C3 P1 C1 . . 108.53(11) y C2 P1 C1 . . 113.56(10) y C3 P1 S1 . . 109.09(8) y C2 P1 S1 . . 101.70(7) y C1 P1 S1 . . 111.23(7) y P1 S1 Au1 . . 111.56(3) y C12 C1 C13 . . 108.27(19) ? C12 C1 C11 . . 107.87(19) ? C13 C1 C11 . . 109.49(19) ? C12 C1 P1 . . 111.22(15) ? C13 C1 P1 . . 107.83(15) ? C11 C1 P1 . . 112.09(15) ? C23 C2 C21 . . 107.46(19) ? C23 C2 C22 . . 109.62(19) ? C21 C2 C22 . . 108.69(19) ? C23 C2 P1 . . 110.46(16) ? C21 C2 P1 . . 110.21(15) ? C22 C2 P1 . . 110.34(16) ? C31 C3 C32 . . 110.81(19) ? C31 C3 P1 . . 112.74(17) ? C32 C3 P1 . . 117.05(16) ? C31 C3 H3 . . 105.0 ? C32 C3 H3 . . 105.0 ? P1 C3 H3 . . 105.0 ? C1 C11 H11A . . 109.5 ? C1 C11 H11B . . 109.5 ? H11A C11 H11B . . 109.5 ? C1 C11 H11C . . 109.5 ? H11A C11 H11C . . 109.5 ? H11B C11 H11C . . 109.5 ? C1 C12 H12A . . 109.5 ? C1 C12 H12B . . 109.5 ? H12A C12 H12B . . 109.5 ? C1 C12 H12C . . 109.5 ? H12A C12 H12C . . 109.5 ? H12B C12 H12C . . 109.5 ? C1 C13 H13A . . 109.5 ? C1 C13 H13B . . 109.5 ? H13A C13 H13B . . 109.5 ? C1 C13 H13C . . 109.5 ? H13A C13 H13C . . 109.5 ? H13B C13 H13C . . 109.5 ? C2 C21 H21A . . 109.5 ? C2 C21 H21B . . 109.5 ? H21A C21 H21B . . 109.5 ? C2 C21 H21C . . 109.5 ? H21A C21 H21C . . 109.5 ? H21B C21 H21C . . 109.5 ? C2 C22 H22A . . 109.5 ? C2 C22 H22B . . 109.5 ? H22A C22 H22B . . 109.5 ? C2 C22 H22C . . 109.5 ? H22A C22 H22C . . 109.5 ? H22B C22 H22C . . 109.5 ? C2 C23 H23A . . 109.5 ? C2 C23 H23B . . 109.5 ? H23A C23 H23B . . 109.5 ? C2 C23 H23C . . 109.5 ? H23A C23 H23C . . 109.5 ? H23B C23 H23C . . 109.5 ? C3 C31 H31A . . 109.5 ? C3 C31 H31B . . 109.5 ? H31A C31 H31B . . 109.5 ? C3 C31 H31C . . 109.5 ? H31A C31 H31C . . 109.5 ? H31B C31 H31C . . 109.5 ? C3 C32 H32A . . 109.5 ? C3 C32 H32B . . 109.5 ? H32A C32 H32B . . 109.5 ? C3 C32 H32C . . 109.5 ? H32A C32 H32C . . 109.5 ? H32B C32 H32C . . 109.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Au1 S1 . 2.3477(6) y Au1 Br3 . 2.4310(3) y Au1 Br2 . 2.4330(3) y Au1 Br1 . 2.4399(4) y P1 C3 . 1.847(2) y P1 C2 . 1.872(2) y P1 C1 . 1.877(2) y P1 S1 . 2.0640(8) y C1 C12 . 1.537(3) ? C1 C13 . 1.538(3) ? C1 C11 . 1.543(3) ? C2 C23 . 1.535(3) ? C2 C21 . 1.541(3) ? C2 C22 . 1.541(3) ? C3 C31 . 1.536(3) ? C3 C32 . 1.540(3) ? C3 H3 . 1.0000 ? C11 H11A . 0.9800 ? C11 H11B . 0.9800 ? C11 H11C . 0.9800 ? C12 H12A . 0.9800 ? C12 H12B . 0.9800 ? C12 H12C . 0.9800 ? C13 H13A . 0.9800 ? C13 H13B . 0.9800 ? C13 H13C . 0.9800 ? C21 H21A . 0.9800 ? C21 H21B . 0.9800 ? C21 H21C . 0.9800 ? C22 H22A . 0.9800 ? C22 H22B . 0.9800 ? C22 H22C . 0.9800 ? C23 H23A . 0.9800 ? C23 H23B . 0.9800 ? C23 H23C . 0.9800 ? C31 H31A . 0.9800 ? C31 H31B . 0.9800 ? C31 H31C . 0.9800 ? C32 H32A . 0.9800 ? C32 H32B . 0.9800 ? C32 H32C . 0.9800 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C13 H13B Au1 . 0.98 2.69 3.607(2) 156.1 yes C21 H21A S1 . 0.98 2.63 3.109(2) 110.2 yes C12 H12A S1 . 0.98 2.89 3.417(2) 114.4 yes C3 H3 Br3 . 1.00 2.71 3.546(2) 140.9 yes C12 H12A Br2 . 0.98 2.89 3.863(2) 173.6 yes C13 H13A Br2 2_666 0.98 3.00 3.931(2) 159.1 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C3 P1 S1 Au1 . . . . -70.82(8) y C2 P1 S1 Au1 . . . . 170.07(8) y C1 P1 S1 Au1 . . . . 48.86(9) y Br3 Au1 S1 P1 . . . . 70.22(3) y Br2 Au1 S1 P1 . . . . -116.91(3) y C3 P1 C1 C12 . . . . 160.43(16) ? C2 P1 C1 C12 . . . . -73.58(18) ? S1 P1 C1 C12 . . . . 40.42(17) ? C3 P1 C1 C13 . . . . 41.86(17) ? C2 P1 C1 C13 . . . . 167.86(15) ? S1 P1 C1 C13 . . . . -78.15(15) ? C3 P1 C1 C11 . . . . -78.73(18) ? C2 P1 C1 C11 . . . . 47.3(2) ? S1 P1 C1 C11 . . . . 161.26(14) ? C3 P1 C2 C23 . . . . 164.85(15) ? C1 P1 C2 C23 . . . . 41.03(19) ? S1 P1 C2 C23 . . . . -78.55(15) ? C3 P1 C2 C21 . . . . -76.56(18) ? C1 P1 C2 C21 . . . . 159.61(16) ? S1 P1 C2 C21 . . . . 40.03(17) ? C3 P1 C2 C22 . . . . 43.48(19) ? C1 P1 C2 C22 . . . . -80.34(18) ? S1 P1 C2 C22 . . . . 160.08(15) ? C2 P1 C3 C31 . . . . 54.96(19) ? C1 P1 C3 C31 . . . . -178.47(16) ? S1 P1 C3 C31 . . . . -57.14(17) ? C2 P1 C3 C32 . . . . -75.32(19) ? C1 P1 C3 C32 . . . . 51.24(19) ? S1 P1 C3 C32 . . . . 172.58(15) ?