#------------------------------------------------------------------------------
#$Date: 2024-05-06 06:23:16 +0200 (Mon, 06 May 2024) $
#$Revision: 291733 $
#$URL: svn://www.crystallography.net/cod/cif/2/02/30/2023052.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2023052
loop_
_publ_author_name
'Upmann, Daniel'
'Bockfeld, Dirk'
'Jones, Peter G.'
'Târcoveanu, Eliza'
_publ_section_title
;
 Crystal structures of ten phosphane chalcogenide complexes of gold(III)
 chloride and bromide.
;
_journal_coeditor_code           YZ2051
_journal_issue                   'Pt 4'
_journal_name_full
'Acta crystallographica. Section E, Crystallographic communications'
_journal_page_first              355
_journal_page_last               369
_journal_paper_doi               10.1107/S2056989024002032
_journal_volume                  80
_journal_year                    2024
_chemical_formula_iupac          '[Au Cl3 (C10 H23 P S)]'
_chemical_formula_moiety         'C10 H23 Au Cl3 P S'
_chemical_formula_sum            'C10 H23 Au Cl3 P S'
_chemical_formula_weight         509.63
_chemical_name_systematic
;
(<i>tert</i>-Butyldipropan-2-ylphosphane sulfide-\k<i>S</i>)trichloridogold(III)
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-2019/3
_cell_angle_alpha                90
_cell_angle_beta                 91.774(3)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   7.9363(3)
_cell_length_b                   14.4096(4)
_cell_length_c                   14.2851(4)
_cell_measurement_reflns_used    14677
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      30.3880
_cell_measurement_theta_min      2.8240
_cell_volume                     1632.85(9)
_computing_cell_refinement
;
CrysAlisPro, Version 1.171.36.24a (Rigaku OD, 2020)
;
_computing_data_collection
;
CrysAlisPro, Version 1.171.36.24a (Rigaku OD, 2020)
;
_computing_data_reduction
;
CrysAlisPro, Version 1.171.36.24a (Rigaku OD, 2020)
;
_computing_molecular_graphics
;
Bruker XP, Version 5.1 (Bruker, 1998)
;
_computing_publication_material
;
SHELXL-2019/3 (Sheldrick, 2015)
;
_computing_structure_refinement
;
SHELXL-2019/3 (Sheldrick, 2015)
;
_computing_structure_solution
;
SHELXS-97 (Sheldrick, 2008)
;
_diffrn_ambient_temperature      100(2)
_diffrn_detector_area_resol_mean 16.1419
_diffrn_measured_fraction_theta_full 0.990
_diffrn_measured_fraction_theta_max 0.949
_diffrn_measurement_device_type  'Oxford Diffraction Xcalibur, Eos'
_diffrn_measurement_method       '\w scan'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0455
_diffrn_reflns_av_unetI/netI     0.0307
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            42542
_diffrn_reflns_theta_full        30.000
_diffrn_reflns_theta_max         30.835
_diffrn_reflns_theta_min         2.827
_diffrn_source                   'Enhance (Mo) X-ray Source'
_exptl_absorpt_coefficient_mu    9.702
_exptl_absorpt_correction_T_max  0.2471
_exptl_absorpt_correction_T_min  0.1589
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
(CrysAlisPro; Rigaku OD, 2020)
;
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    2.073
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             976
_exptl_crystal_size_max          0.3
_exptl_crystal_size_mid          0.2
_exptl_crystal_size_min          0.2
_refine_diff_density_max         2.523
_refine_diff_density_min         -1.501
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.123
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     152
_refine_ls_number_reflns         4881
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.123
_refine_ls_R_factor_all          0.0339
_refine_ls_R_factor_gt           0.0251
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0115P)^2^+2.5557P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0424
_refine_ls_wR_factor_ref         0.0450
_reflns_number_gt                4296
_reflns_number_total             4881
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            yz2051.cif
_cod_data_source_block           10aa
_cod_depositor_comments
'Adding full bibliography for 2023050--2023062.cif.'
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               2023052
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.159
_shelx_estimated_absorpt_t_max   0.247
_shelx_hkl_file
;
   0   0   2 82441.4 1685.80   6
   0   0   2 78195.5 1348.68  10
   0   0  -2 82142.3 1369.14  10
   0   0   2 79478.3 1518.43   1
   0   0  -2 77691.2 1698.91  14
   0   0  -2 80321.3 1635.94   6
   0   0   2 83599.4 1754.57  14
   0   0   2 79479.8 1782.58   7
   0   0  -2 79404.0 1882.43   3
   0   0  -2 79570.9 1540.82   1
   0   0   2 80675.9 1683.35  13
   0   0   2 85670.6 1903.50   3
   0   0  -2 79038.9 1672.57  13
   0   0  -3 1598.81 529.411   3
   0   0  -3 1334.69 486.195  14
   0   0  -3 830.252 425.481   6
   0   0   3 1964.84 498.678   7
   0   0   3 1139.06 541.698   3
   0   0   3 1104.67 474.716  13
   0   0   3 1008.11 358.264   6
   0   0   3 1476.21 409.019  14
   0   0  -3 931.314 304.013  10
   0   0  -3 1813.30 440.396  13
   0   0   3 1111.76 285.105  10
   0   0  -3 970.147 375.823   1
   0   0  -3 1442.40 423.846   7
   0   0   3 453.486 383.647   1
   0   0   4 16414.5 899.612  10
   0   0   4 19185.0 1190.01   6
   0   0   4 17690.3 1225.89  13
   0   0   4 16460.1 1087.26   1
   0   0  -4 16271.1 925.016  10
   0   0  -4 16847.7 1189.50   6
   0   0   4 18547.9 1197.58  14
   0   0  -4 15523.2 1187.83  14
   0   0   4 18222.3 1343.03   3
   0   0  -4 16814.0 1185.14   7
   0   0   4 17899.1 1300.20   7
   0   0  -4 15957.8 725.705   2
   0   0  -4 16112.4 1267.74   3
   0   0  -4 16038.1 1143.66  13
   0   0  -4 16442.7 1062.49   1
   0   0   5 1825.79 688.684   3
   0   0   5 307.683 584.011  13
   0   0   5-123.234 518.666   1
   0   0  -5 405.620 357.097  10
   0   0  -5 365.984 257.141   2
   0   0   5 319.886 296.815  10
   0   0  -5 422.941 582.377  14
   0   0  -5-57.6501 387.679   1
   0   0  -5-49.6415 542.491   6
   0   0  -6 909005. 6297.09   2
   0   0   6 882383. 8915.37   1
   0   0   6 884877. 10412.2   3
   0   0  -6 864364. 9486.63   6
   0   0   6 906958. 10014.4  13
   0   0  -6 920467. 10306.3  14
   0   0   6 939140. 8080.83  10
   0   0  -7 358.077 263.830   2
   0   0  -7 898.394 729.639   6
   0   0   7 205.676 689.342   3
   0   0   7 1397.57 816.304  13
   0   0  -7 28.2839 723.897  14
   0   0   7 782.310 693.577   1
   0   0   8 295480. 6619.37   4
   0   0   8 295786. 6759.86  13
   0   0  -8 284477. 6436.74   6
   0   0   8 287835. 5982.38   1
   0   0   8 287903. 6843.97   3
   0   0  -8 294023. 4102.04   2
   0   0  -8 299369. 6911.05  14
   0   0  -9 738.715 974.871   6
   0   0   9 494.554 797.462   3
   0   0   9 450.137 742.682   4
   0   0  -9 245.371 232.903   2
   0   0   9 719.805 877.114  13
   0   0  -9 217.374 905.796  14
   0   0   9 266.846 712.353   1
   0   0 -10 38653.3 1622.48   2
   0   0  10 44429.3 3058.49   3
   0   0 -10 42637.9 1720.65   8
   0   0 -10 40711.5 2870.23   6
   0   0  10 45676.4 2930.83   4
   0   0 -10 36036.2 2854.91  14
   0   0  10 41101.4 2678.61   1
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   0   0  11 149.708 651.213   4
   0   0  11 643.945 841.182   1
   0   0 -11 367.258 946.828   6
   0   0 -11 467.419 248.926   2
   0   0 -11-219.014 233.325   8
   0   0 -11-632.632 1005.17  14
   0   0  11 12.6176 814.012  13
   0   0 -12 142563. 3300.10   8
   0   0  12 142898. 5594.25   4
   0   0 -12 138889. 6105.52  14
   0   0 -12 134881. 5729.16   6
   0   0  12 127937. 5592.70   3
   0   0  12 124561. 5714.11  13
   0   0  12 135104. 5238.83   1
   0   0  13 327.936 912.378  13
   0   0  13-149.307 643.675   4
   0   0  13 368.461 803.219   3
   0   0 -13-729.704 984.602   6
   0   0 -13 417.013 1028.57  14
   0   0  13 16.4487 938.522   1
   0   0  14 252582. 7909.17   4
   0   0  14 233867. 7607.56   1
   0   0 -14 239157. 8805.76  14
   0   0 -14 236449. 8305.57   6
   0   0  14 236633. 8654.23  13
   0   0  14 223607. 7976.76   3
   0   0 -15 546.298 846.979  14
   0   0  15 1497.90 641.676   4
   0   0  15 299.480 837.780   1
   0   0  15 174.178 685.030  13
   0   0  15-51.5513 579.619   3
   0   0 -15 1580.98 1070.04   6
   0   0 -16 38689.4 3925.87  14
   0   0  16 38696.1 3438.17   1
   0   0  16 43998.2 4132.44  13
   0   0  16 34467.7 3419.69   3
   0   0 -16 35900.2 3627.57   6
   0   0  17-1874.69 1145.57  13
   0   0  17 397.468 378.642   3
   0   0 -17 401.874 582.762  14
   0   0  17-228.927 906.121   1
   0   0 -17 497.074 528.657   6
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   0   0  18 5602.42 1582.04   1
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   0   0  18 10308.2 2309.17  13
   0   0 -18 11194.3 2186.19   6
   0   0  19-1140.45 1162.12   3
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   0   0  19-716.948 1410.17  13
   0   0 -19 1691.00 1313.86   6
   0  -1   2 129038. 2197.09   1
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   0   1   3 305401. 2521.45   2
   0  -1   3 309959. 4189.83   6
   0  -1  -3 287656. 4300.78  14
   0   1   3 292898. 4785.04   3
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   0  -1  -3 301397. 3159.84   8
   0   1   3 293354. 3533.12   1
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   0  -1   3 298140. 3735.60   3
   0   1  -3 306721. 3979.72   1
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   0   1   3 304024. 3850.40  13
   0   1  -3 297537. 4095.71   6
   0   1   3 305206. 4070.39   6
   0   1  -4 69853.4 1209.50  16
   0   1  -4 73288.3 1720.01  10
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   0  -1  -4 71605.8 1686.01   8
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   0  -1   5 436743. 6696.41  13
   0   1   5 418999. 5438.42   1
   0   1  -5 443926. 4698.55  10
   0   1   5 418537. 7081.57   3
   0  -1  -5 436186. 3770.31   2
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   0   1   7 1813.12 867.553   3
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   0  -1  -7 1366.05 388.433   8
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   0   1   7 1553.39 722.633   1
   0  -1   7 1154.51 738.062   3
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   0   1   7 1008.31 195.750  16
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   0  -1  -8 48387.0 2946.21  14
   0   1   8 49090.6 2543.06   4
   0   1   8 43273.9 2869.35   3
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   0  -1  10 13733.2 1708.05   1
   0  -1 -10 18543.7 1218.90   8
   0   1  10 16657.3 1760.22   1
   0   1  10 17119.3 1737.93   4
   0  -1  10 14180.2 1732.06   3
   0   1  10 17779.0 2010.05  13
   0   1 -10 16879.1 1958.37   6
   0   1 -10 17846.7 2065.00  14
   0  -1  10 19706.1 2124.73   4
   0  -1  10 16449.0 2077.92  13
   0  -1 -10 16724.3 996.395   2
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   0  -1  11 163665. 5582.42   1
   0  -1  11 166527. 6367.17  13
   0   1  11 167514. 5417.16   1
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   0   1 -12 52475.3 3625.17   6
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   2   1   3 20903.4 1730.87   3
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   2   1   4 38668.6 1582.83  12
   2   1   4 36533.7 2322.20   3
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   2  -1   4 36315.9 1121.99   8
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   2   1   4 35710.6 1402.43   8
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   2   1   4 38358.4 1162.58   2
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   2  -1   4 37830.4 1554.61   2
   2   1   4 35805.9 1872.53  13
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   2  -1   4 38527.0 2110.01   3
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   2   1   5 157819. 4998.65   3
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   2   1   5 153398. 2883.82  16
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   2  -1   5 157742. 4222.41  12
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   2  -1   5 156267. 4374.50   1
   2   1   5 154832. 4215.99  13
   2   1   5 152501. 2033.65   2
   2  -1   5 164951. 3161.55   2
   2   1   5 152741. 2600.19   8
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   2   1   5 163160. 3377.20  12
   2   1   6 7310.67 870.236  12
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   2  -1   6 7651.26 1106.92  12
   2   1   6 6740.10 1371.38   3
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   2  -1   6 6600.82 467.947  10
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   2   1   6 6738.85 1101.86  13
   2   1   6 6599.97 442.612   8
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   2  -1   7 35716.5 2303.84  12
   2   1   7 34636.1 1233.65  16
   2  -1   7 34382.4 1146.16  10
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   2  -1   7 34768.7 2477.05   1
   2  -1   7 37775.7 2572.28   3
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   2   1   7 35632.4 2776.03   3
   2  -1   7 37702.1 2734.94  13
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   2   1   7 31685.2 2353.93   1
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   2   1   7 37773.4 2474.99  13
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   2  -1   8 175.229 95.6019  10
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   2  -1   8-291.671 883.908  13
   2  -1   8 596.657 969.102   1
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   2  -1   8 558.598 828.116   3
   2   1   8 1121.41 990.451   1
   2   1   8-216.667 1011.45   3
   2   1   8 156.472 636.554  13
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   2   1   9 6023.32 1566.82   3
   2  -1   9 4455.90 1259.19   3
   2  -1   9 6150.96 1429.01   1
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   2   1   9 6429.05 1446.05   1
   2   1   9 5157.01 1160.67  13
   2  -1   9 5936.70 1413.60  13
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   2  -1  10 20124.4 2388.02  13
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   2  -1  10 20338.3 2277.48   1
   2   1  10 21266.3 2558.95   3
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   2   1  10 22730.1 2387.15   1
  -2   1 -10 20302.3 2324.35  14
   2  -1  10 20718.8 2281.38   3
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   2   1  10 21836.6 2291.97  13
   2  -1  11 58456.3 4091.84  13
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   2  -2   1 181825. 4207.49  12
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   2   2   1 194927. 3825.31   5
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   2  -2   1 191811. 2857.57  10
   2   2   1 187056. 3731.93  16
   2  -2   1 203446. 4021.74   2
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   2   2   1 200941. 4043.75  14
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   2   2   1 195548. 3250.12   6
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   2  -2   2 36256.2 1079.66  10
   2   2   2 37443.9 1947.80   5
   2   2   2 32473.7 2126.99   3
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   2  -2   2 36437.6 1717.02   1
   2  -2   2 38275.0 1559.11   8
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   2   2   2 39239.0 1810.81   8
   2  -2   2 35437.4 2010.70  12
   2  -2   2 38450.3 1781.70   2
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   2   2   2 36814.5 1681.84  16
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   2   2   2 37064.7 1618.76   6
   2   2   3 1721.97 852.699   5
   2  -2   3 2538.45 752.456  12
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   2   2   3 2726.00 967.391   3
   2  -2   3 2014.38 741.060   1
   2   2   3 2100.88 477.194   8
   2   2   3 2068.00 391.018   2
   2  -2   3 2435.23 656.900   3
   2  -2   3 1943.50 497.762   2
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   2  -2   3 1666.59 432.983   8
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   2   2   3 1924.01 578.716  16
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   2   2   4 606.897 321.364  12
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   2  -2   4 945.224 758.697   1
   2   2   4 529.069 836.702   3
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   2  -2   4 821.194 565.404   3
   2   2   4 736.934 450.764  16
   2  -2   4 1270.85 707.272  12
   2  -2   4 473.845 286.605   8
   2  -2   4 1068.01 447.753   2
   2   2   4 480.707 257.022   8
   2   2   4 738.522 253.908   2
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   2   2   4 744.466 442.943  13
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   2  -2   4 270.244 243.416  14
   2   2   5 7610.63 1429.68   3
   2   2   5 5916.02 592.208  12
  -2   2  -5 6618.78 1286.92   6
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   2   3  -3 3759.23 584.956  13
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   2   3  -1 4185.32 877.743  16
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   2  -3  -1 4196.95 905.231  12
  -2  -3   1 4224.71 482.337  13
  -2   3   0 105522. 2515.25  10
   2  -3   0 100061. 2194.26   1
   2   3   0 94716.6 2960.53  16
   2  -3   0 105200. 2525.89   3
   2   3   0 100300. 2758.83   5
   2  -3   0 96914.0 2478.66  10
   2   3   0 97585.9 1802.39   6
   2  -3   0 101377. 1993.06   9
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   2   4  -5 138886. 2725.78   6
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   2  -6   2 152507. 5342.70  12
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   2  -6   2 152704. 2788.45   3
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   2   7 -13 6282.18 1084.79  10
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   2  -7  -9 203886. 5591.88  12
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   2   7  -9 180867. 6018.10  16
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   2   7  -9 196270. 6284.22   5
   2  -7  -9 195039. 6701.63   8
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   2  -7  -9 191926. 6316.76   6
   2  -7  -9 187611. 6635.98  14
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   2   7  -9 190336. 5306.17   6
   2   7  -8 3518.88 768.462   6
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   2  -7  -7 6535.40 1383.83   6
   2   7  -7 5349.29 1348.44  16
   2  -7  -7 6380.82 1250.58  14
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   3   4   9 7759.81 1871.17   3
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   3 -11   3 104017. 5720.20   8
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   3  11   3 103515. 5771.87  16
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   4   4   5 2430.09 1572.04   3
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   4   4   6 3562.10 1529.36   3
   4  -4   6 5067.70 1078.89   3
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   4   4   6 3942.17 1000.04  16
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   4   4   7 150198. 6845.20   3
   4  -4   7 144022. 5977.91  12
   4   4   7 144214. 3395.83  12
   4  -4   7 143409. 5136.02   3
   4  -4   7 133447. 5382.44   1
   4  -4   7 146197. 4033.84   8
   4   4   7 146998. 4535.36  16
   4   4   7 145953. 3192.17   2
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   4   7 -11 33844.4 3105.00   5
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   4   7   5 85812.8 4672.90   5
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   4  -7   7 84675.3 5294.47  12
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   4   7   8 2250.25 1389.63   3
   4  -7   8 1102.04 393.632   3
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   4   7   8 338.470 829.521  16
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   4   7   9 12929.6 2717.30   3
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   4   7   9 12081.2 1701.11  16
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   4  -7  10 10438.0 2047.86  12
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   4   7  11 49706.6 5031.18   3
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   4  -7  11 45558.3 3964.21   1
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   4   7  12 1247.45 1572.17   3
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   4   7  13 52772.9 4340.90   1
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   4   7  13 58770.6 5597.33   3
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   4   7  16-73.3507 886.030   3
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   4  -8 -14 26369.7 3223.36   8
   4  -8 -14 26011.4 3285.94  14
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   4   8  -8 16875.6 2499.00  16
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   4  -8  -3 20692.6 2473.79   8
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   5  -4   2 2779.13 864.077   8
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   5   4   3 13126.9 1893.71   5
   5   4   3 14329.2 2176.77   3
  -5  -4  -3 10481.3 1744.34   9
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   5  -4   4 136601. 4652.06   8
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   5   4   4 133772. 4960.06  16
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   5  -4   8 18300.8 2177.36   3
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   5  -4   8 15391.0 2294.35   1
   5   4   8 12094.7 2316.91   3
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   5   4   8 18612.4 1858.52  16
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   5  -4  10 29365.6 2859.19   3
   5  -4  10 21816.8 2790.18   1
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   5  -4  12 53794.4 4317.96  12
   5  -4  12 44813.4 4086.94   1
   5   4  12 52934.1 4332.13   1
   5  -4  12 60884.4 4377.44   3
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   5   4  12 51614.8 4936.57   3
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   5   4  13 398.066 1182.59   3
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   5  -4  14 31066.4 3657.87   1
   5   4  14 37580.4 3918.77   1
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   5   4  14 36661.3 4378.87   3
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   5   4  15 1618.55 983.585   3
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   5  -4  16 686.901 1121.53   1
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   5   5 -17 12001.3 2470.69  10
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   5   5 -14 8577.49 1844.54   5
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   5  -5 -14 9728.91 1645.86   5
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   5   5 -12 20998.6 2614.81   5
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   5  -5  -2 15266.5 1748.60  10
   5  -5  -2 14856.7 1937.67   8
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   5   5  -2 13290.8 2099.69  16
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   5  -5  -1 5243.24 1495.33  12
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   5  -5  -1 4949.13 644.140   5
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   5  -5   0 19076.6 2287.52  12
   5   5   0 20447.5 2360.48  16
   5  -5   0 17810.3 1526.55   1
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   5  -5   0 17204.5 1655.03  10
   5   5   0 15431.6 1921.01   5
   5  -5   0 19955.8 2128.42   8
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   5  -5   0 19469.6 1127.26  14
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   5  -5   1 106650. 5092.38  12
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   5  -5   1 102327. 3699.97  10
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   5  -5   1 97061.1 4354.62   8
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   5   5   1 98642.5 4584.03  16
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   5  -5   2 80532.1 4485.48  12
   5   5   2 77594.3 4045.99   5
   5  -5   2 74455.6 3412.18   1
   5   5   2 82889.2 4823.65   3
   5  -5   2 75622.5 3033.85  10
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   5  -5   2 73847.7 3728.27   8
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   5   5   2 73497.9 3931.21  16
   5  -5   2 71549.3 2175.05  14
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   5  -5   3 23872.3 2599.54  12
   5   5   3 21710.8 2387.92   5
   5   5   3 23994.6 2849.43   3
   5  -5   3 19512.5 1962.58   1
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   5  -5   3 20572.6 1987.92   8
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   5   5   3 23182.6 2336.48  16
   5  -5   3 19332.0 1182.85  14
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   5  -5   4 68456.3 4316.13  12
   5   5   4 68822.1 4101.93   5
   5   5   4 76537.0 4918.11   3
   5  -5   4 69524.5 3664.29   1
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   5  -5   4 69637.4 3538.94   8
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   5   5   4 73912.5 3865.29  16
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   5  -5   5 4049.71 1359.28  12
   5  -5   5 3188.57 1173.81   1
   5   5   5 1816.27 1481.20   3
   5   5   5 2767.94 1236.34   5
  -5   5  -5 3769.25 967.686   9
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   5  -5   5 3323.21 1017.50   3
   5  -5   5 3234.68 838.094   8
   5   5   5 4777.89 1316.49  16
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   5  -5   6 2197.38 1243.74   1
   5   5   6 1575.70 1239.33   5
   5  -5   6 1070.14 843.760  12
   5   5   6 2714.10 615.558  12
   5   5   6 2538.84 1408.20   3
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   5  -5   6 2773.13 1016.38   3
   5  -5   6 1519.39 536.039   8
   5   5   6 1373.71 1053.14  16
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   5  -5   7 23536.7 2691.05  12
   5   5   7 23441.2 1542.28  12
   5  -5   7 20748.2 2159.41   3
   5  -5   7 21886.0 2512.45   1
   5   5   7 21192.5 2984.11   3
   5  -5   7 21135.2 1860.55   8
  -5   5  -7 21581.7 2097.17   2
   5   5   7 20769.1 2128.50  16
  -5   5  -7 23980.1 1838.48  14
  -5  -5  -7 21447.7 2706.19  14
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   5  -5   8 51638.8 3996.79  12
   5  -5   8 47009.5 3283.11   3
   5  -5   8 41354.6 3404.46   1
  -5   5  -8 45648.7 3889.40   6
   5   5   8 48761.0 3044.28  16
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   6   1  12 19633.6 2894.46   1
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   6  -6  11 5691.43 1729.44  12
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   6   6  11 12361.6 2711.28   3
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   6  -6  13 1147.75 1582.25  12
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   6   6  14 18316.9 3333.55   3
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   6   7 -16 1113.40 1674.92  10
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   6   7 -11 10890.4 1989.95   5
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   7   2 -12 2656.08 1167.89  10
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   7   2 -11-2.39308 690.032  10
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   7  -2 -11 1889.26 957.950  14
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   7   2 -10 6719.59 1703.37  10
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   7   2  -9 59919.4 3915.24   5
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   7   2  -9 58660.0 4456.64  16
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   7  -2  -8 141394. 5175.54   5
   7   2  -8 138014. 5728.65   5
   7  -2  -8 120739. 6274.55  10
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   7   2  -8 131445. 6568.72  16
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   7  -2  -7 69346.3 3527.37   5
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   7  -3   7 28014.1 2991.52  12
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   7   3   7 17157.4 2841.52   3
   7  -3   7 21177.5 2707.12   3
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   7   3   7 17247.9 2120.73  16
   7  -3   7 21676.8 2774.92   1
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   7   3   8 566.378 1258.46   3
   7  -3   8 928.368 888.586   3
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   7  -3   8 602.960 1321.72   1
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   7   3   9 87885.4 6239.82   3
   7  -3   9 84984.9 5419.21   3
   7  -3   9 77997.1 5171.00   1
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   7  -3  10 8032.55 2007.43   1
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   7  -3  11 63523.1 5074.97   1
   7   3  11 59184.9 4903.87   1
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   7   4  -5 268.227 778.845   5
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   7   4   2 14809.7 2178.06   5
   7   4   2 19090.8 2799.03   3
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   7  -4   3 1347.94 717.426   8
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   7  -4   4 55671.8 4159.49  12
   7   4   4 51951.1 3979.67   5
   7   4   4 52525.2 4505.17   3
   7  -4   4 53809.3 2762.33  10
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   7  -4   4 53100.7 3431.40   8
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   7   4   4 58538.8 3985.40  16
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   7   4   5 2777.86 1354.53  16
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   7  -4   6 114529. 6076.75  12
   7   4   6 122367. 4899.00  12
   7   4   6 128268. 7172.36   3
   7  -4   6 119129. 5950.98   3
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   7  -4   6 118630. 4870.07   8
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   7   4   6 126126. 5663.13  16
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   7   4   7 6299.14 2123.07   3
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   7  -4   8 55960.4 4382.20  12
   7   4   8 52232.1 4875.42   3
   7  -4   8 52257.4 4087.58   3
   7  -4   8 48972.8 4062.40   1
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   7   4   8 47661.4 3407.94  16
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   7  -4   9 1207.42 1290.91   1
   7   4   9 1769.18 1191.25   3
   7  -4   9 785.313 768.637   3
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   7  -4  10 1801.31 1152.67  12
   7  -4  10 1597.59 1413.96   1
   7   4  10 4875.23 1825.77   3
   7  -4  10 2066.22 859.893   3
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   7  -4  11 2306.19 1492.34  12
   7   4  11 3158.91 1523.63   3
   7  -4  11 2565.25 977.400   3
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   7   4  11 1103.76 1449.39   1
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   7  -4  12 57889.9 4967.04   1
   7   4  12 53653.5 4811.57   1
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  -7   4 -12 51437.6 4753.84   6
   7   4  12 55600.9 5445.99   3
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   7   4  13 8576.70 2141.89   3
   7  -4  13 10131.0 2381.78   1
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   7   4  13 8575.98 2239.70   1
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   7   4  14 44493.1 5116.61   3
   7  -5 -15-96.2422 1710.07   8
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   7  -5 -15 1483.97 1804.16  14
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   7   5 -14 1917.91 1288.62  10
   7   5 -14 2910.87 1102.64   5
   7  -5 -14 1719.18 1406.26   8
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   7  -5 -14 3673.64 1726.10  14
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   7   5 -13 20531.5 3056.29  10
   7   5 -13 18178.1 2621.62   5
   7  -5 -13 25347.5 3421.99   8
   7   5 -13 13051.9 2126.78  16
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  -7   5  13 22052.4 2940.77   7
   7  -5 -13 21819.2 3053.47  14
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   7   5 -12 24268.2 2962.81   5
   7  -5 -12 28277.8 3470.43   8
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   7   5 -12 20876.1 2798.10  16
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   7  -5 -12 25536.1 3135.51  14
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   7   5 -11 50518.4 4122.33   5
   7  -5 -11 57116.0 4813.79  10
   7  -5 -11 52347.4 4650.72   8
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   7   5 -11 47051.2 4264.71  16
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   7  -5 -11 54812.5 4312.70  14
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   7   5 -10 44912.6 3766.40   5
   7  -5 -10 47383.8 4249.08  10
   7  -5 -10 39386.7 3984.41   8
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   7   5 -10 31264.6 3538.38  16
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   7  -5 -10 42634.3 3654.57  14
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   7   5  -9 28295.9 2960.69   5
   7  -5  -9 26335.5 3138.21  10
   7  -5  -9 30737.4 3474.04   8
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  -7   5   9 29431.4 2798.87   7
   7   5  -9 35711.1 3729.22  16
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   7  -5  -9 32514.8 3048.09  14
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   7  -5  -8-1465.07 896.897  10
   7  -5  -8 655.081 957.279   8
   7   5  -8-79.8067 941.742   5
   7   5  -8 2791.29 1668.75  16
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   7  -5  -8 92.9269 624.871  14
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   7  -5  -7 8751.18 1820.34  10
   7   5  -7 7378.76 1604.33   5
   7   5  -7 13192.5 2487.23  16
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  -7   5   7 10212.3 1572.52   7
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   7  -5  -7 9665.11 1502.80  14
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  -7  -5   6 37030.8 2889.54  11
   7   5  -6 35028.1 3061.98   5
   7  -5  -6 34981.8 3325.80  10
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   7  -5   9 51732.5 4350.84   1
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   7   6   8 23529.5 3535.78   3
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   7   6   8 22843.3 2533.63  16
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   7  -6  10 3041.14 1456.27  12
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   7   6  11 18617.5 3287.63   3
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   7   7   3 1342.00 1205.74   3
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   7   7   8 42790.0 4681.18   3
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   7  -7   8 36883.6 3661.56   1
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   7   8   4 2685.11 1316.57   3
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   7   8   5 24161.8 3094.71   5
   7   8   5 23852.8 3431.92   3
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   7  -8   5 22422.7 2652.48   8
   7   8   5 19836.4 2749.79  16
   7  -8   5 21843.0 2591.15   1
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   7  -8   6 10606.0 2132.48  12
   7   8   6 8620.95 2228.46   3
   7   8   6 11873.1 2284.50   5
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   7  -8   6 8463.70 1793.84   1
   7   8   6 9562.12 2109.43  16
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   7   8   7 74894.1 6211.31   3
   7  -8   7 72863.1 5661.13  12
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   7   8   7 67880.7 4677.77  16
   7  -8   7 69941.9 4816.42   1
   7  -8   8 7450.26 1968.29  12
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   7   8   8 8531.71 2191.60   3
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   7  -8   8 9654.17 2172.84   1
   7   8   8 8621.14 1949.33  16
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   7  -8   9 6455.78 2007.87  12
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   7   8   9 8258.40 2247.52   3
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   7  -8   9 2670.18 1530.93   1
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   7  -8  10 1145.06 1563.49  12
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   7  -8  10 31.1232 946.116   1
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   7  -8  11 3802.80 2220.96  12
   7   8  11 4998.72 1867.00   3
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   7  -8  11 8559.42 2176.69   1
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   7  -8  12 8633.72 2726.97  12
   7  -8  12 5253.09 1911.59   1
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   7  -8  13 32486.4 4574.50  12
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  -7  -9  13 4062.38 1611.91  11
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   7  -9 -12 14773.5 2852.36  12
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   7  -9 -12 15872.9 3005.27   8
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   7  -9 -11 56756.8 5131.54  12
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   7   9 -11 54804.6 4583.61   5
   7  -9 -11 64093.9 5672.13   8
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   7   9 -11 60948.5 5310.82  16
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   8   1  -4 14337.4 1914.06   5
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   8   1  -2 18054.1 2184.31   5
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   8   1  -2 16738.6 2479.50  16
   8  -1  -1 116723. 5068.83   5
   8   1  -1 116029. 5313.51   5
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   8   1  -1 109060. 5838.59  16
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   8  -1   0 8654.47 1507.89   5
   8   1   0 12771.1 1883.52   5
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   8   1   0 11366.8 2010.57  16
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   8  -1   1 33727.9 2876.00   5
   8   1   1 31002.2 2888.27   5
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   8  -1   2 14232.1 2100.30  12
   8  -1   2 14178.4 1924.70   5
   8   1   2 15330.2 2155.96   5
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   8   1   2 12946.0 2033.14  16
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   8  -1   3-960.223 726.503   5
   8  -1   3 717.351 595.313  12
   8   1   3-131.280 250.789  12
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   8   1   4 2029.24 734.408  12
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   8   1   4 3072.77 1397.69   3
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   8  -1   4 2646.81 1432.86   1
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   8  -1   5 47931.7 3800.18  12
   8   1   5 56988.8 3946.99  12
   8   1   5 55766.8 4714.15   3
   8  -1   5 52090.2 4420.48   3
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   8  -1   6 11403.8 1884.55  12
   8   1   6 12003.9 1857.65  12
   8   1   6 8841.37 2101.00   3
   8  -1   6 8559.00 2072.88   3
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   8  -1   6 11260.8 2252.77   1
   8  -1   7 56618.8 4235.87  12
   8   1   7 57730.9 4023.53  12
   8   1   7 57320.4 4875.13   3
   8  -1   7 52517.2 4547.79   3
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  -8   1  -7 45786.5 3956.30   9
   8  -1   7 55358.2 4380.05   1
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  -8   1  -8 11337.1 1993.75   6
   8  -1   8 10135.3 1951.33  12
   8   1   8 9735.18 2185.97   3
   8  -1   8 8487.40 1960.78   3
  -8  -1  -8 8967.11 1929.67   9
  -8   1  -8 8657.34 1777.36   9
   8   1   8 11490.1 2316.75   1
   8  -1   8 13282.1 2465.24   1
  -8  -1  -9 5644.07 1565.94   6
  -8   1  -9 4799.14 1466.13   6
   8  -1   9 6797.88 1934.99   1
   8   1   9 4424.54 1556.86   3
   8  -1   9 5998.54 1733.83   3
  -8  -1  -9 5802.57 1489.73   9
  -8   1  -9 3957.40 1263.74   9
   8   1   9 3841.69 1817.12   1
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  -8   1 -10-1295.16 702.602   6
   8   1  10 1702.14 1060.84   3
   8  -1  10 3188.66 952.294   3
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  -8  -1 -10 2439.49 1200.88   9
   8   1  10 215.594 1288.71   1
   8  -1  10 820.322 1430.42   1
  -8  -1 -11 11234.3 2162.06   6
  -8   1 -11 10400.8 2033.97   6
   8   1  11 8334.55 1989.99   3
   8  -1  11 7666.75 1796.26   3
  -8   1 -11 12343.3 2442.42   9
  -8  -1 -11 9012.91 2013.22   9
   8   1  11 9601.04 2296.28   1
   8  -1  11 10365.4 2368.92   1
  -8  -1 -12 3948.45 1323.27   6
  -8   1 -12 2106.58 1125.43   6
   8   1  12 7659.14 2230.51   1
   8   1  12 3495.19 1509.44   3
   8  -1  12 5177.34 1775.14   3
  -8   1 -12 3850.06 1714.53   9
  -8  -1 -12 1883.55 1269.26   9
   8  -1  12 4875.58 1864.14   1
   8   1  13 36942.1 4446.45   3
   8  -1  13 30999.1 4022.79   3
  -8   1 -13 30442.2 4091.48   9
  -8  -1 -13 29292.4 3717.54   6
   8   2 -14-996.076 1078.26   5
  -8   2  14 2056.79 1464.81   7
   8  -2 -14-209.497 1633.25  14
  -8  -2  14-716.219 1890.31  13
   8   2 -13 9011.44 2224.87  10
   8   2 -13 11249.1 2035.75   5
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  -8   2  13 8891.43 2036.91   7
   8  -2 -13 9302.29 2431.84  14
  -8  -2  13 5029.55 1925.88  13
  -8   2  13 7894.28 2153.57  13
   8   2 -12 15439.8 2744.33  10
   8  -2 -12 17707.2 2861.45  10
   8   2 -12 16547.9 2365.70   5
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  -8   2  12 15309.1 2471.71   7
  -8   2  12 15780.6 2399.12  15
   8  -2 -12 16609.7 2731.03  14
  -8  -2  12 16553.9 2690.49  13
  -8   2  12 16722.9 2727.24  13
   8   2 -11 16194.2 2696.83  10
   8  -2 -11 21435.2 3018.33  10
   8   2 -11 16892.0 2336.00   5
  -8  -2  11 17563.1 2612.85   7
  -8   2  11 12724.1 2179.43   7
  -8   2  11 21315.4 2676.44  15
   8  -2 -11 19105.9 2761.44  14
  -8  -2  11 21257.9 2811.73  13
  -8   2  11 19391.9 2782.07  13
   8   2 -10 18629.9 2774.48  10
   8  -2 -10 18366.9 2765.48  10
   8   2 -10 16094.3 2233.29   5
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   8  -2  -9 41831.9 3066.67   5
   8   2  -9 42065.5 3461.23   5
   8   2  -9 43212.0 4237.72  10
   8  -2  -9 37702.5 3834.91  10
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   8   2  -9 33423.4 3628.09  16
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   8  -2  -8 5077.14 1349.83  10
   8  -2  -8 5610.08 1137.86   5
   8   2  -8 5587.06 1382.18   5
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   8  -2  -7 713.980 726.888  10
   8  -2  -7 1066.80 497.006   5
   8   2  -7 2354.19 974.070   5
   8   2  -7 1767.52 1210.98  16
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   8  -2  -6 10935.6 2010.88  10
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   8  -2  -5 15740.3 1799.40   5
   8   2  -5 19656.9 2300.13   5
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   8  -2  -3 64233.6 3569.70   5
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   8   2  -1 11972.9 1934.69   5
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   8   2  -1 11393.1 2035.80  16
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   8   2   0 1085.57 947.624   5
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   8   2   0-1099.69 1493.18  16
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   8  -2   1 12265.2 1984.72  12
   8  -2   1 10646.7 1541.87  10
   8  -2   1 11830.3 1684.47   5
   8   2   1 11829.0 1925.02   5
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   8   2   1 9575.68 1948.14  16
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   8  -2   2 39936.3 3562.52  12
   8  -2   2 38397.1 3041.88   5
   8   2   2 48468.2 3763.93   5
   8  -2   2 43464.2 3047.87  10
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   8  -2   2 39860.2 3257.41   1
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   8   2   2 42881.9 3617.22  16
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   8  -2   3 44538.0 3733.94  12
   8   2   3 38831.7 3448.84   5
   8  -2   3 46886.1 3076.78  10
   8   2   3 43425.3 4196.23   3
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   8  -2   3 43579.1 3496.17   1
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   8   2   3 38997.3 3493.27  16
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   8  -2   4 26223.8 2868.51  12
   8   2   4 26648.4 2676.05  12
   8   2   4 27851.7 3003.46   5
   8   2   4 29116.0 3502.32   3
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   8  -2   4 27785.9 2978.41   1
   8   2   4 27780.7 2968.81  16
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   8  -2   5 56155.0 4232.51  12
   8   2   5 54398.5 3762.84  12
   8   2   5 50310.0 4587.01   3
   8  -2   5 54678.6 4473.58   3
  -8  -2  -5 45268.9 3902.07   9
  -8   2  -5 50512.3 3914.02   9
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   8  -2   5 49063.1 3893.55   1
   8   2   5 44864.7 3613.85  16
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   8  -2   6 9360.34 1794.73  12
   8   2   6 8538.45 1540.60  12
   8   2   6 8006.35 2037.04   3
   8  -2   6 9549.19 2045.82   3
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   8  -2   6 7509.41 1870.68   1
   8   2   6 4789.33 1403.98  16
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   8  -2   7 2078.11 1098.28  12
   8  -2   7 1224.70 1348.65   1
   8   2   7 2230.37 1245.98   3
   8  -2   7 2474.26 1288.15   3
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   8   2   7-1716.08 927.581  16
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   8  -2   8 20202.4 2687.52  12
   8   2   8 14328.1 2657.26   3
   8  -2   8 14657.9 2412.10   3
  -8  -2  -8 16138.2 2546.54   9
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   8  -2   8 13825.9 2442.43   1
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   8  -2   9 20071.2 2721.51  12
   8   2   9 19475.6 3142.80   3
   8  -2   9 13201.2 2348.33   3
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  -8   2  -9 12963.7 2219.88   9
   8  -2   9 17896.4 2756.92   1
   8   2   9 20328.0 2980.10   1
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  -8   2 -10 15977.9 2601.78   6
   8   2  10 14098.8 2615.47   3
   8  -2  10 20074.5 2889.55   3
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   8   2  10 15181.7 2764.79   1
   8  -2  10 22505.6 3150.34   1
   8  -2  11 38257.8 4105.04   1
  -8   2 -11 40124.5 4190.88   9
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   8   2  11 31962.2 3855.15   1
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   8   2  11 37404.2 4327.26   3
   8  -2  11 45563.3 4436.93   3
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   8   2  12 19386.6 3273.19   3
   8  -2  12 20030.6 3091.92   3
   8  -2  12 19918.3 3192.62   1
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   8   2  13 831.337 1279.25   3
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   8   3 -13 2498.38 1057.40   5
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   8   3 -12 13396.0 2616.61  10
   8  -3 -12 11012.3 2344.76  10
   8   3 -12 12168.4 2079.43   5
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   8  -3 -12 10902.1 2388.19  14
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   8   3 -11-53.3548 674.434  10
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   8   3 -10 8091.96 1897.98  10
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   8  -3  -9 13925.7 2342.96  10
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   8   3  -8 50542.8 3803.74   5
   8  -3  -8 52420.2 4404.26  10
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   8   3  -8 42387.5 4118.74  16
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   8  -3  -7 2263.01 946.402  10
   8   3  -7 3062.08 1004.82   5
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   8   3  -6 76106.7 4492.33   5
   8  -3  -6 76383.9 5047.48  10
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   8   3  -6 78658.5 5429.75  16
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   8  -3  -5 1223.78 774.704  10
   8   3  -5 110.062 828.736   5
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   8  -3  -4-853.273 732.250  10
   8  -3  -4 967.178 601.639   5
   8   3  -4 503.680 730.945   5
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   8   3  -4-943.004 1641.09  16
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   8  -3  -3 16604.3 1771.97   5
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   8  -3  -3 15881.2 2199.43  10
   8   3  -3 17601.5 2271.75   5
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   8   3  -3 14731.7 2392.18  16
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   8  -3  -2 27789.2 2301.40   5
   8   3  -2 29848.7 2860.92   5
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   8  -3  -2 30321.6 2882.55  10
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   8   3  -2 26086.6 3066.32  16
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   8  -3  -1 6465.83 1343.44  10
   8  -3  -1 5194.93 1070.22   5
   8   3  -1 6336.26 1500.90   5
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   8   3  -1 2751.23 1363.70  16
   8  -3  -1 5603.78 1186.19   1
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   8  -3   0 124957. 6407.23  12
   8  -3   0 115410. 4855.41   5
   8   3   0 120178. 5724.83   5
   8  -3   0 111187. 5146.99  10
  -8   3   0 109236. 5713.00   2
   8  -3   0 117342. 4951.86   1
  -8  -3   0 110647. 5585.82   7
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   8   3   0 112762. 5948.47  16
   8  -3   1 2714.19 1085.79   1
   8  -3   1 2310.13 894.935  12
   8  -3   1 3381.04 882.219  10
   8   3   1 2025.89 1100.19   5
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   8  -3   2 11421.1 1973.84  12
   8  -3   2 12430.2 1648.52  10
   8   3   2 9972.36 1870.33   5
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   8   3   2 9116.23 1804.73  16
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   8  -3   2 9544.04 1753.47   1
   8  -3   3 6703.27 1498.25  12
   8  -3   3 6393.30 1147.01  10
   8   3   3 5205.48 1548.35   5
   8   3   3 8816.31 2132.27   3
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   8  -3   3 8197.36 1744.24   1
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   8   3   3 5305.66 1440.81  16
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   8  -3   4 4709.45 1249.00  12
   8   3   4 328.851 381.994  12
   8   3   4 2630.82 1248.49   5
   8   3   4 3545.91 1620.72   3
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   8  -3   4 2888.44 1451.40   1
  -8   3  -4 1263.67 564.602   7
   8   3   4 743.948 1099.34  16
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   8   3   5 6631.44 1703.34   5
   8  -3   5 5391.93 1360.73  12
   8   3   5 8104.92 1492.70  12
   8  -3   5 5577.82 1600.23   1
   8   3   5 6922.29 2019.83   3
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   8  -3   5 7238.80 1791.52   3
   8  -3   5 6244.34 1312.86   8
   8   3   5 2850.39 1096.47  16
  -8   3  -5 3214.52 1101.11   2
   8  -3   6 94606.1 5677.88  12
   8   3   6 105104. 6744.47   3
   8  -3   6 104695. 6071.35   3
   8  -3   6 100731. 5637.82   1
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  -8   3  -6 86337.7 5137.02   9
  -8   3  -6 94961.4 4893.33   2
   8   3   6 98821.3 5348.88  16
  -8  -3  -6 103717. 5232.75   6
  -8   3  -6 101383. 5948.57   6
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  -8   3  -7 2502.58 1150.99   6
   8  -3   7 4749.65 1464.93  12
   8   3   7 7488.90 2005.47   3
   8  -3   7 4285.06 1416.90   3
  -8  -3  -7 3412.04 1276.81   9
  -8   3  -7 4578.62 1205.00   9
   8   3   7 1282.24 713.470  16
   8  -3   7 4598.19 1533.37   1
   8  -3   8 30224.5 3340.52  12
  -8   3  -8 22316.4 2908.11   6
   8  -3   8 28228.4 3260.93   3
   8   3   8 26204.7 3606.15   3
   8  -3   8 29432.0 3400.89   1
  -8  -3  -8 26856.2 3265.11   9
  -8   3  -8 22147.0 2804.40   9
   8   3   8 20592.9 2404.32  16
  -8  -3  -8 25868.2 2818.79   6
  -8   3  -9 2542.05 1062.12   6
   8  -3   9 1128.73 1362.32  12
   8   3   9-259.556 972.254   3
   8  -3   9-133.293 479.943   3
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   8   3  10 6754.42 1896.80   3
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   8   3  10 3615.75 1799.10   1
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   8   3  11 10190.7 2291.56   3
   8  -3  11 8985.99 2010.03   3
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   8   3  12 42746.6 4805.94   3
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   8   4   3 80375.2 5115.79   5
   8   4   3 79576.5 5759.02   3
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   8   4   5 44393.0 3301.40  12
   8   4   5 38716.6 3749.79   5
   8   4   5 40682.0 4305.93   3
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   8   4   7 42.4986 970.589   3
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   8   4   9 50376.7 5002.22   3
   8  -4   9 47300.7 4204.49   3
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   8   4  10-67.5639 362.758   3
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   8   4  11 50356.4 4727.04   1
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   8   4  11 55969.5 5487.71   3
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   8  -5   1 33683.5 2764.53  10
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   8  -5   3 19368.4 2345.94   1
   8   5   3 18407.5 2605.73   5
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   8  -5   4 50519.5 4340.99  12
   8   5   4 49315.4 4188.92   5
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   8   5   5 1929.13 1083.76   5
   8   5   5 1783.93 1342.10   3
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   8  -5   5 1982.89 1022.59   3
   8  -5   5 2683.99 1024.16   8
   8   5   5 4737.06 1596.50  16
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   8  -5   6 29903.7 3420.67  12
   8   5   6 26064.8 3219.89   5
   8  -5   6 30293.6 3188.35   3
   8  -5   6 26581.4 2999.81   1
   8   5   6 25834.2 3630.71   3
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   8   5   7 46256.2 4803.68   3
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   8   5   7 37698.7 3399.97  16
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   8   5   8 33500.6 4164.72   3
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   8   5   9 20091.7 3329.41   3
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   8   6   2 40243.8 4262.62   3
   8  -6   2 38741.9 3438.18   8
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   8   6   3 36059.6 3639.59   5
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   8   6   3 35335.5 4001.28   3
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   8   6   4 59625.4 5225.42   3
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   8   6   5 171.776 972.176   5
   8   6   5-2040.31 1144.40   3
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   8   6   5 6669.74 1746.73  16
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   8  -6   5 418.294 933.515   1
   8   6   6 2379.81 1176.62   5
   8  -6   6 7742.56 1873.63  12
   8   6   6 3559.39 1609.94   3
   8  -6   6 5928.49 1401.32   3
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   8  -6   7-814.301 1250.74  12
   8   6   7 271.905 1146.41   3
   8  -6   7-77.7719 270.012   3
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   8  -6   7-928.009 1113.20   1
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   8  -6   8 4709.51 1709.19  12
   8   6   8 3511.75 1430.58   3
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   8  -6   8 6052.21 1796.77   1
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   8  -6   9 31894.6 4030.09  12
   8  -6   9 26407.6 3338.07   1
   8   6   9 31709.0 4145.68   3
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   8  -6  10 45272.3 4730.34  12
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   8   7  -9 37700.5 3713.86   5
   8  -7  -9 39086.6 4327.83   8
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   8   7  -9 39792.5 4425.97  16
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   8  -7  -7 45504.6 4388.37  12
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   8   7  -7 44021.2 4483.71  16
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   8   7  -5 39505.6 3623.73   5
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   8  -7  -1 51698.0 4547.49  12
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   8   7  -1 61954.9 4868.76  16
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   8   7   1 76263.1 5820.99   3
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   8   7   1 78739.6 5323.65  16
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   8  -7   2 11459.2 2149.65  12
   8   7   2 17024.6 2623.08   5
   8   7   2 16316.1 2801.76   3
   8  -7   2 14155.6 2152.75   8
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   8   7   2 20587.5 2909.35  16
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   8  -7   3 7152.73 1721.44  12
   8   7   3 3236.83 1377.85   5
   8   7   3 5213.18 1772.77   3
   8  -7   3 5849.34 1490.68   8
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   8  -7   4 4777.90 1543.81  12
   8   7   4 5656.07 1698.80   5
   8   7   4 4903.98 1713.90   3
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   8  -7   4 6171.27 1553.91   8
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   8  -7   4 5067.22 1350.98   1
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   8  -7   5 29753.7 3551.07  12
   8  -7   5 30341.5 3078.18   1
   8   7   5 35219.7 4226.41   3
   8   7   5 29514.7 3494.05   5
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   8  -7   5 31882.8 3144.44   3
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   8   7   5 40293.1 3737.69  16
   8  -7   6 804.743 982.280  12
   8   7   6 2655.20 1220.16   3
   8   7   6-1067.00 1034.13   5
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   8  -7   6-251.094 905.661   1
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   8  -7   7 66054.2 5446.73  12
   8   7   7 68827.3 5983.82   3
   8  -7   7 65473.0 4795.20   1
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   8   7   7 70663.7 4828.48  16
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   8  -7   8 2833.84 1667.94  12
   8   7   8 1611.55 1124.08   3
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   8  -7   8 2683.95 1413.41   1
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   8  -7   9 30569.6 3911.95  12
   8   7   9 26019.3 3817.92   3
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   8  -7   9 25051.5 3283.35   1
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   8  -7  10 7280.04 2346.35  12
   8  -7  10 3879.21 1557.51   1
   8  -7  11 8465.71 2854.34  12
   8  -7  11 4021.81 1543.42   1
   8  -8 -12 43852.3 4847.91  12
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   8   8 -12 36485.0 4376.67  16
   8  -8 -11 5666.99 2198.43  12
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   8  -8 -10 43250.0 4516.86  12
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   8   8 -10 35020.1 3668.23   5
   8  -8 -10 37458.0 4389.24   8
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   8  -8  -9 16873.6 2870.55  12
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   8   8  -9 12644.9 2238.24   5
   8  -8  -9 12939.3 2624.54   8
   8   8  -9 21177.9 3329.06  16
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   8  -8  -8 2963.36 1320.68  12
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   8   8  -8 818.107 886.378   5
   8  -8  -8-511.879 865.410   8
   8   8  -8 3349.05 1853.81  16
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   8  -8  -7 2235.56 1086.09  12
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   8   8  -7 1728.44 1121.17   5
   8  -8  -7-2.82522 408.513   8
  -8  -8   7 1051.01 748.089   7
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   8   9   5 16225.4 2965.52   3
   8   9   5 14285.5 2504.76   5
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   8   9   5 15579.3 2796.54  16
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   8  -9   6 15622.9 2917.86  12
   8   9   6 23202.3 3540.83   3
   8   9   6 15269.2 2672.58   5
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   8   9   8 39795.3 3782.86  16
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   8   9   8 38439.7 4855.05   3
   8  -9   9 954.665 1978.74  12
   8  -9   9 2569.87 1411.28   1
   8  -9  10 7507.00 2917.63  12
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   8 -10 -10 4816.54 2274.74  12
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   8 -10  -9 12905.6 2715.76  12
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   8 -10  -7-264.074 852.690   8
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   8  10   1 16173.0 2629.82   5
   8 -10   1 18932.2 2864.91   8
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   8 -10   2 10898.0 2405.00  12
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   8  10   2 13762.4 2615.36   3
   8  10   2 10270.0 2210.68   5
   8 -10   2 12045.2 2284.55   8
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   8  10   2 11105.5 2690.81  16
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   8 -10   3 49840.2 5047.88  12
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   8 -10   3 51686.9 4572.97   8
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   8 -10   4 2192.81 1482.76   8
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   8 -10   5 26608.4 3800.02  12
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   8  10   5 23809.9 3292.56   5
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   8  10   5 28521.9 3729.73  16
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   8  10   6 2955.26 1914.72  16
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   8 -10   7 467.195 1751.79  12
   8 -10   7 884.631 763.291   1
   8  10   7-264.287 1213.26   3
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   8  10   7-265.206 1412.33  16
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   8 -10   8 7634.02 2514.08  12
   8 -10   8 4096.84 1415.81   1
   8  10   8 7564.56 1989.08  16
   8 -10   9 23069.2 3196.22   1
   8 -11  -9-627.159 1864.31  12
   8 -11  -8 29382.4 4036.43  12
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   8 -11  -7 2921.60 1742.63  12
  -8 -11   7 543.072 893.244  11
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   8 -11  -6 48253.8 5019.20  12
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   8  11  -6 45564.5 4285.09   5
   8 -11  -6 48373.5 5139.97   8
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   8  11  -6 47460.1 5212.53  16
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   9  -1  -2 35607.4 3409.76  10
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   9  -1   2 10699.8 2001.41  12
   9  -1   2 11673.9 1815.83   5
   9   1   2 11830.4 1955.19   5
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   9  -1   3 9432.37 1876.18  12
   9   1   3 9256.89 1806.88  12
   9   1   3 7163.75 1546.63   5
   9   1   3 11214.0 2353.15   3
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   9  -2   0 25043.6 2545.00   5
   9   2   0 34495.5 3267.33   5
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   9   2   5 11376.4 2015.96  12
   9   2   5 13376.4 2595.00   3
   9  -2   5 16410.2 2692.83   3
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   9   2   5 5038.72 1321.36  16
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   9   2   7-29.3957 724.970   3
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   9  -3  -1 23405.9 3033.14  12
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   9  -3  -1 14875.7 2175.09  10
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   9   3  -1 12950.7 2447.77  16
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   9  -3   0 276.806 873.231  12
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   9   3   0 2958.55 1155.26   5
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   9  -3   1 17718.5 2604.70  12
   9  -3   1 22904.4 2530.93  10
   9   3   1 18344.1 2482.98   5
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   9  -3   1 16828.5 2183.74   1
   9   3   1 15143.4 2383.89  16
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   9  -3   2 623.087 797.057  12
   9   3   2 918.256 801.193   5
   9   3   2-166.551 1270.47   3
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   9  -3   3 18194.6 2742.56  12
   9   3   3 19792.4 2662.63   5
   9   3   3 18243.0 3004.10   3
   9  -3   3 19407.2 2505.80   1
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   9   3   3 14233.5 2307.98  16
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   9  -3   4 3032.49 1419.65  12
   9   3   4 2134.36 1156.49  12
   9  -3   4 3491.71 1329.40   1
   9   3   4 3806.23 1357.29   5
   9   3   4 2602.22 1199.26   3
   9  -3   4 3479.67 1197.41   8
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   9   3   4-1158.93 886.994  16
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   9  -3   5 37851.9 3810.26  12
   9   3   5 40911.7 4458.15   3
   9  -3   5 38209.7 3930.55   3
   9  -3   5 42765.8 3843.09   1
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   9   3   5 34992.1 3485.53  16
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   9  -3   6 2756.22 1450.91  12
   9   3   6 2686.33 1550.37   3
   9  -3   6 4230.09 1356.60   3
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   9  -3   6 1933.72 1277.06   1
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   9  -3   7 2293.35 1664.03  12
   9   3   7 592.870 735.151   3
   9  -3   7 2674.89 1098.98   3
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   9  -3   7 2612.41 1483.99   1
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   9  -3   8-948.906 1659.18  12
   9   3   8 904.059 979.344   3
   9  -3   8-1377.41 816.236   3
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   9  -3   8 824.341 1259.12   1
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   9   3   9 7824.64 2134.49   1
   9   3   9 3053.76 1424.76   3
   9  -3   9 9301.52 2081.84   3
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   9  -3   9 3234.87 1464.96   1
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   9  -3  10 2813.62 1445.77   3
   9  -3  10 5346.18 1935.93   1
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   9   4 -11-832.961 893.353   5
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   9   4 -10 2404.68 986.806   5
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   9  -4  -9 237.041 1214.89  10
   9   4  -9-23.5539 195.570   5
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  -9   4   9 1740.69 1271.05   7
  -9   4   9 1657.06 1047.07  15
   9   4  -8 32229.4 3301.07   5
   9  -4  -8 36139.1 4034.78  10
  -9   4   8 31928.3 3922.40   2
  -9  -4   8 33964.5 3573.35   7
  -9   4   8 28256.3 3174.55   7
   9   4  -8 30024.6 3734.12  16
  -9   4   8 29846.7 3327.25  15
   9  -4  -7 13959.3 2454.67  10
   9   4  -7 13043.7 2117.39   5
   9   4  -7 12899.4 2496.66  16
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  -9   4   7 15590.4 2278.21   7
  -9   4   7 16470.4 2420.87  15
  -9   4   7 13695.9 2578.62   2
   9   4  -6 32569.4 3244.15   5
   9  -4  -6 29708.4 3433.80  10
  -9   4   6 39327.2 4217.44   2
  -9  -4   6 35733.7 3540.70   7
  -9   4   6 37351.3 3393.75   7
   9   4  -6 34290.8 3924.13  16
  -9   4   6 33506.3 3399.57  15
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   9  -4  -5 848.041 899.179  10
   9   4  -5 1439.61 911.581   5
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   9   4  -5-395.406 1804.98  16
  -9   4   5 504.595 802.700   7
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  -9   4   5-407.501 450.785  15
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   9  -4  -4-1190.60 830.285  10
   9   4  -4 698.037 824.230   5
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   9  -4  -3 8243.03 1930.19  12
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   9  -4  -3 6408.06 1528.40  10
   9   4  -3 5089.62 1374.55   5
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   9   4  -3 4166.95 1387.19  16
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  -9   4   3 8766.21 2020.61   2
   9  -4  -2 23546.0 3083.27  12
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   9  -4  -2 19437.0 2530.69  10
   9   4  -2 18680.2 2518.69   5
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   9   4  -2 11394.1 2329.27  16
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  -9   4   2 21329.5 2926.33   2
   9  -4  -1 11671.5 2252.17  12
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   9  -4  -1 10908.0 1834.81  10
   9   4  -1 13102.1 2189.42   5
  -9  -4   1 10342.8 1934.66   7
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   9   4  -1 11114.2 2257.34  16
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  -9   4   1 13769.4 2482.93   2
   9  -4   0 45114.6 4259.94  12
   9   4   0 48342.4 4002.53   5
  -9  -4   0 40296.6 3467.76  11
   9  -4   0 52077.4 3834.04  10
  -9   4   0 45804.8 4090.39   2
  -9  -4   0 40750.9 3740.22   7
  -9   4   0 43022.8 3362.85   7
   9   4   0 37855.9 3825.75  16
   9  -4   1 2.45009 867.178  12
   9  -4   1 1489.93 893.439  10
   9   4   1 67.3168 534.282   5
   9  -4   1 196.145 585.866   8
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   9   4   1-4843.74 1667.84  16
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   9  -4   2 6008.15 1683.63  12
   9   4   2 7610.76 1683.26   5
   9   4   2 10030.9 2228.33   3
   9  -4   2 7779.29 1679.97   8
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   9   4   2 3822.35 1115.51  16
   9  -4   2 8386.70 1650.55   1
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   9  -4   3 9776.82 2060.51  12
   9   4   3 6374.70 1683.98   5
   9   4   3 12882.9 2709.84   3
   9  -4   3 12679.5 2054.78   8
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  -9   4  -3 7606.88 1539.19   7
   9   4   3 5008.86 1396.11  16
   9  -4   3 7398.36 1671.78   1
  -9   4  -3 9754.13 1900.82   2
  -9   4  -4 3130.23 1068.81   6
   9  -4   4 518.758 1441.93  12
   9   4   4 2235.03 1188.44  12
   9   4   4-472.362 637.244   5
   9   4   4 1606.72 1380.17   3
   9  -4   4-547.046 870.033   8
   9  -4   4 494.943 993.745   1
  -9  -4  -4 1530.47 787.040   7
  -9   4  -4 678.704 826.538   7
  -9   4  -4 1538.74 1047.77   2
  -9   4  -5 4629.79 1457.18   6
   9   4   5 6067.57 1670.66   5
   9  -4   5 4221.05 1548.81  12
   9   4   5 4877.45 1846.17   3
   9  -4   5 4599.33 1471.30   3
  -9  -4  -5 1383.24 888.268   9
   9  -4   5 4178.31 1591.62   1
  -9   4  -5 6814.38 1555.59   7
   9   4   5 615.212 1037.43  16
  -9   4  -5 3144.18 1002.88   2
   9  -4   6 30760.2 3674.70  12
   9   4   6 43856.8 4714.13   3
   9  -4   6 33414.8 3621.50   3
   9  -4   6 30558.9 3384.42   1
  -9  -4  -6 33732.6 3699.51   9
  -9   4  -6 35162.7 3495.70   9
  -9   4  -6 36615.1 3298.83   2
   9   4   6 29504.6 3155.96  16
  -9   4  -6 33374.6 3670.37   6
  -9   4  -7 226.080 605.269   6
   9  -4   7 3093.38 1673.41  12
   9   4   7 1134.40 751.074   3
   9  -4   7 3207.98 1270.26   3
  -9  -4  -7 2080.64 1062.32   9
  -9   4  -7 2134.86 1230.57   9
   9  -4   7 1791.19 1231.78   1
  -9   4  -8 16806.0 2766.46   6
   9  -4   8 15385.0 2825.67  12
   9   4   8 20625.0 3399.54   3
   9  -4   8 16333.2 2672.67   1
   9  -4   8 18993.1 2833.12   3
  -9  -4  -8 16302.1 2711.28   9
  -9   4  -8 21742.6 3050.61   9
  -9   4  -9 4102.50 1653.07   6
   9  -4   9 1405.94 1673.60  12
   9  -4   9 1027.85 1246.64   1
   9   4   9 2426.80 1133.11   3
   9  -4   9 2845.88 1452.84   3
  -9   4  -9 2445.22 1516.15   9
  -9   4 -10 3806.67 1532.75   6
   9  -4  10 557.019 1069.72   1
  -9   4 -10 2547.50 1779.42   9
  -9   4 -11 417.759 1682.66   9
   9   5 -11 18273.0 2961.81  16
   9   5 -10 6680.56 1626.26   5
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   9  -5  -9 10999.4 2358.88  10
   9   5  -9 13232.4 2229.26   5
  -9   5   9 19920.8 3094.77   2
   9  -5  -9 17746.8 3029.36   8
   9   5  -9 9535.62 2081.79  16
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  -9   5   9 16130.9 2569.71  15
   9  -5  -8 5266.68 1739.13  10
   9  -5  -8 5562.57 1717.40   8
   9   5  -8 2818.01 1147.98   5
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  -9   5   8 3447.77 1262.57  15
  -9   5   8 4075.72 1621.02   2
   9  -5  -7 427.326 917.001  10
   9  -5  -7 8.46362 748.144   8
   9   5  -7 90.3386 445.022   5
  -9  -5   7 888.316 589.393   7
  -9   5   7 77.9356 734.830  15
  -9   5   7-170.200 1022.39   2
  -9  -5   6 11829.8 1840.35  11
   9  -5  -6 10261.1 2080.79  10
   9  -5  -6 12127.9 2396.75   8
   9   5  -6 17837.1 2561.81   5
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   9   5  -6 6734.12 1886.08  16
  -9   5   6 16120.8 2436.99  15
  -9   5   6 11489.0 2472.66   2
  -9  -5   5 13164.4 1923.10  11
   9  -5  -5 15128.9 2511.26  10
   9  -5  -5 13574.8 2390.26   8
   9   5  -5 9624.02 1837.49   5
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   9   5  -5 8162.31 2071.69  16
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   9  -5  -4 11501.0 2227.84  12
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   9  -5  -4 8785.43 1852.96  10
   9   5  -4 8364.16 1769.20   5
   9  -5  -4 11491.0 2167.12   8
  -9  -5   4 13143.6 2222.95   7
   9   5  -4 5332.96 1746.93  16
  -9  -5   4 6088.26 1324.54  15
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  -9   5   4 11493.3 2374.14   2
   9  -5  -3 34334.3 3845.02  12
   9   5  -3 30731.2 3211.89   5
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   9  -5  -3 33984.2 3392.33  10
   9  -5  -3 37664.1 3890.02   8
  -9   5   3 38044.9 3996.52   2
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   9   5  -3 35794.7 3893.76  16
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   9  -5  -2 17396.5 2766.55  12
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   9  -5  -2 17871.1 2423.54  10
   9   5  -2 16573.8 2400.92   5
   9  -5  -2 21000.0 2849.75   8
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   9   5  -2 14856.3 2674.51  16
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   9  -5  -1 7111.48 1778.48  12
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   9  -5  -1 7707.09 1609.11  10
   9   5  -1 7639.17 1789.63   5
   9  -5  -1 8631.78 1810.37   8
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   9   5  -1 10321.6 2306.43  16
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  -9   5   1 6635.07 1906.15   2
   9  -5   0 4146.02 1413.60  12
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   9  -5   0 7278.42 1539.15  10
   9   5   0 6026.92 1568.50   5
   9  -5   0 6983.51 1568.97   8
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   9   5   0 7359.84 2184.46  16
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   9  -5   1 1307.96 1078.90  12
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   9   5   1 2958.32 1282.21   5
   9   5   1 1477.15 1067.28   3
   9  -5   1 1007.95 872.534   8
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   9   5   1 3796.96 1748.14  16
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   9  -5   2 4487.72 1516.43  12
   9   5   2 4452.82 1450.57   5
   9   5   2 5169.02 1683.35   3
   9  -5   2 5176.91 1452.73   8
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   9   5   2 4256.33 1383.21  16
  -9   5  -2 4536.47 1514.42   2
   9  -5   3 46931.1 4469.34  12
   9   5   3 52472.8 4491.27   5
   9   5   3 52297.5 4952.36   3
   9  -5   3 50953.8 3854.27   1
   9  -5   3 48088.9 4029.53   8
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   9   5   3 46984.1 4197.99  16
   9  -5   4 18080.9 2851.18  12
   9  -5   4 15500.4 2328.67   1
   9   5   4 17710.7 2727.09   5
   9   5   4 16492.0 3021.92   3
   9  -5   4 17976.1 2465.72   8
  -9  -5  -4 10194.7 2085.38   7
   9   5   4 11489.3 2134.59  16
  -9   5  -4 16060.1 2445.57   2
  -9   5  -5 9677.29 1950.81   6
   9  -5   5 7267.79 1978.35  12
   9  -5   5 9885.97 2004.75   1
   9   5   5 8595.71 1905.53   5
   9   5   5 6389.03 1992.20   3
   9  -5   5 10614.1 2042.63   3
  -9  -5  -5 7886.22 1774.49   9
  -9  -5  -5 8210.22 1836.49   7
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  -9   5  -6 1407.32 904.003   6
   9  -5   6 2757.87 1641.10  12
   9  -5   6 1704.20 1372.87   1
   9   5   6 1744.30 1232.35   3
   9  -5   6 2221.00 1003.04   3
  -9  -5  -6-664.354 649.056   9
  -9   5  -6 222.705 377.468   2
  -9   5  -7 343.369 659.275   6
   9  -5   7 1530.34 1476.93  12
   9  -5   7 1971.18 1311.61   1
   9   5   7 2318.84 1257.91   3
   9  -5   7 1538.44 986.028   3
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  -9   5  -7 945.926 1153.21   9
   9  -5   8 3028.67 1534.46   1
  -9   5  -8 3650.95 1494.95   6
   9  -5   8 1931.25 1765.47  12
   9   5   8 4814.60 1604.60   3
  -9  -5  -8-200.315 877.847   9
  -9   5  -9 21851.6 3262.86   6
   9  -5   9 24459.1 3718.90  12
   9  -5   9 20860.3 3062.43   1
   9   6 -10-4253.15 1448.89  16
   9   6  -9 14030.1 2300.84   5
  -9   6   9 17333.3 2789.40  15
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   9  -6  -8 2813.88 1516.26  10
   9   6  -8 1742.73 862.008   5
   9  -6  -8 3590.55 1625.19   8
   9   6  -8 245.665 1177.52  16
  -9  -6   8 913.322 805.805   7
  -9   6   8 5376.34 1632.59  15
  -9   6   8 253.926 1117.94   2
  -9  -6   7 33351.5 3272.35  11
   9   6  -7 32457.5 3446.35   5
   9  -6  -7 30834.3 3653.98  10
   9  -6  -7 32055.2 3911.43   8
  -9   6   7 33087.4 3996.70   2
  -9  -6   7 34597.7 3640.93   7
   9   6  -7 32383.1 3998.45  16
  -9   6   7 37524.7 3768.82  15
   9  -6  -6 10273.1 2259.17  12
  -9  -6   6 8375.86 1672.89  11
   9  -6  -6 8644.65 1978.83  10
   9   6  -6 8922.47 1828.89   5
   9  -6  -6 12279.5 2348.11   8
   9   6  -6 10633.3 2565.17  16
  -9  -6   6 6357.28 1538.08   7
  -9   6   6 10661.1 1993.76  15
  -9   6   6 12615.0 2628.88   2
   9  -6  -5 36215.5 4076.01  12
   9   6  -5 30855.5 3318.58   5
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   9  -6  -5 33765.2 3708.96  10
   9  -6  -5 33446.4 3884.71   8
  -9   6   5 33885.7 3877.49   2
  -9  -6   5 34543.3 3561.34   7
   9   6  -5 33622.4 3980.46  16
  -9   6   5 34321.1 3580.61  15
   9  -6  -4 1107.67 971.321  12
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   9  -6  -4 1438.15 983.896  10
   9   6  -4 2391.34 1304.23   5
   9  -6  -4 3461.59 1286.22   8
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   9   6  -4 3919.52 1887.95  16
  -9   6   4 2455.88 1048.95  15
  -9   6   4 708.824 1084.84   2
   9  -6  -3 3496.43 1291.94  12
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   9  -6  -3 3712.39 1301.31  10
   9   6  -3 2530.28 1170.84   5
   9  -6  -3 6106.51 1702.92   8
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   9   6  -3 7269.95 2278.92  16
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   9  -6  -2 7519.65 1898.53  12
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   9  -6  -2 5253.38 1436.66  10
   9   6  -2 7346.91 1728.52   5
   9  -6  -2 7362.87 1754.77   8
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   9   6  -2 10505.9 2570.43  16
  -9   6   2 8559.26 1808.51  15
  -9   6   2 7093.10 1962.06   2
   9  -6  -1 29269.5 3612.36  12
   9   6  -1 27203.8 3148.99   5
  -9  -6   1 26317.8 2903.73  11
   9  -6  -1 23556.7 2752.24  10
   9  -6  -1 28264.4 3366.33   8
   9   6  -1 29839.0 3663.33  16
  -9  -6   1 19441.5 2739.46   7
  -9   6   1 24361.5 3043.81  15
  -9   6   1 26206.5 3262.01   2
   9  -6   0-82.5913 999.118  12
  -9  -6   0 5672.46 1471.31  11
   9   6   0 4137.08 1462.42   5
   9   6   0 2720.81 1255.22   3
   9  -6   0 2435.32 1100.69   8
  -9  -6   0 1130.09 1008.22   7
   9   6   0 6727.73 2021.98  16
  -9   6   0 2602.39 1022.11  15
  -9   6   0 3495.31 1515.75   2
   9  -6   1 51854.1 4753.33  12
   9   6   1 52760.8 4410.01   5
  -9  -6  -1 54337.9 4289.26  11
   9   6   1 56649.8 5185.48   3
   9  -6   1 61161.0 4750.41   8
  -9   6  -1 53312.0 4523.46   2
  -9  -6  -1 49618.1 4301.13   7
   9   6   1 63970.1 5080.78  16
   9  -6   2 10835.7 2348.40  12
  -9  -6  -2 9323.08 1886.11  11
   9   6   2 7470.82 1848.61   5
   9   6   2 8500.31 2075.66   3
   9  -6   2 8245.13 1786.69   8
  -9  -6  -2 8724.20 1932.12   7
  -9   6  -2 9156.57 1975.01   2
   9  -6   3 3209.23 1537.45  12
   9   6   3 1739.05 1047.48   5
   9   6   3 4907.72 1524.83   3
   9  -6   3 3400.74 1345.82   8
  -9  -6  -3-1474.65 1024.44   7
   9   6   3 4108.02 1711.93  16
  -9   6  -3 3014.63 1192.94   2
   9  -6   4 7694.28 2050.28  12
   9   6   4 2052.66 1129.33   5
   9   6   4 9572.20 2301.33   3
  -9  -6  -4 6058.58 1562.19   7
   9   6   4 13151.7 2424.80  16
  -9   6  -4 7528.08 1712.14   2
   9  -6   5 8278.41 2219.98  12
   9   6   5 9184.14 1929.18   5
   9   6   5 5935.76 1845.96   3
   9  -6   5 12594.8 2159.54   3
  -9  -6  -5 7194.89 1719.52   7
   9   6   5 11371.3 2235.07  16
  -9   6  -5 11277.3 2032.50   2
   9  -6   5 9445.68 1932.45   1
  -9   6  -6 2646.79 1218.72   6
   9  -6   6 1655.89 1818.49  12
   9   6   6 1027.83 742.166   3
   9  -6   6 335.706 683.022   3
  -9  -6  -6 2004.76 1032.43   9
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   9  -6   7 31034.5 3909.13  12
   9  -6   7 32422.5 3575.53   1
   9   6   7 37358.6 4578.24   3
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   9   6   7 28365.4 3155.19  16
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   9  -6   8 13634.6 2971.14  12
   9  -6   8 11450.8 2312.86   1
   9  -6   9 16749.1 3244.53  12
   9  -6   9 14902.5 2653.40   1
   9  -6  10 1720.13 2364.31  12
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   9  -8  -5 30102.4 3936.72  12
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   9  11  -6-1174.10 1913.66   3
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   9 -11   0-1774.83 1903.61   8
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   9 -11   2 949.781 1768.48   8
   9  12  -4 5123.37 2488.85   3
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   9 -12   1 13690.1 3392.27   8
   9 -12   2 25741.4 3997.60   8
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  10   0  -7 744.128 1192.65  10
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  10   0  -5 840.297 1167.19  10
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 -10   4  -5 39867.2 4196.23   6
 -10   4  -6 890.876 1360.54   6
  10  -4   6 1612.79 1954.92  12
  10  -4   6 3657.97 1458.91   3
  10  -4   6 3250.61 1454.89   1
 -10   4  -7 690.473 1347.64   6
  10  -4   7 2445.41 2181.25  12
  10  -4   7 2073.64 1258.84   1
  10  -4   7 1949.24 1454.51   3
  10   5  -7 28924.4 3381.67   5
  10   5  -6 40380.1 3941.92   5
  10  -5  -6 38491.7 4195.75  10
  10  -5  -5 9256.46 2342.79  10
  10   5  -5 6877.18 1577.53   5
  10  -5  -5 7289.84 2066.85   8
 -10  -5   5 4626.93 1421.91   7
 -10   5   5 11176.8 2321.23  15
  10  -5  -4 7222.22 2282.98  12
  10  -5  -4 6983.60 1918.74  10
  10   5  -4 8273.13 1767.78   5
  10  -5  -4 7289.83 1999.49   8
 -10  -5   4 6217.88 1605.05   7
  10   5  -4 3460.10 1397.26  16
 -10   5   4 6817.40 1838.87  15
 -10   5   4 3734.52 1188.41   2
  10  -5  -3-709.509 1370.36  12
 -10  -5   3-349.444 820.528  11
  10  -5  -3 204.380 1193.53  10
  10   5  -3 2804.34 1072.01   5
  10  -5  -3 1539.29 1244.33   8
 -10  -5   3 1532.11 794.408   7
 -10   5   3-629.819 1218.26  15
 -10   5   3 703.497 890.432   2
  10  -5  -2 497.013 1178.93  12
 -10  -5   2 1059.74 945.999  11
  10  -5  -2 666.919 1231.14  10
  10   5  -2 2033.46 869.707   5
  10  -5  -2 1864.19 1287.52   8
 -10  -5   2 1156.47 677.249   7
  10   5  -2-2070.85 1337.13  16
 -10   5   2 3489.47 1625.14  15
 -10   5   2 2506.44 1281.00   2
  10  -5  -1 34129.6 4104.88  12
  10   5  -1 40616.3 3990.78   5
 -10  -5   1 32974.8 3473.13  11
  10  -5  -1 38576.6 4146.73   8
 -10   5   1 37383.6 4031.04   2
 -10  -5   1 38189.7 3878.48   7
  10   5  -1 30972.9 3695.28  16
 -10   5   1 36088.6 4054.23  15
  10  -5   0 35747.7 4201.19  12
  10   5   0 32158.0 3592.58   5
 -10  -5   0 31195.8 3388.53  11
  10  -5   0 38376.1 4062.83   8
  10   5   0 25916.2 3679.84   3
  10   5   0 30034.5 3628.72  16
 -10  -5   0 27390.4 3294.62   7
 -10   5   0 29507.7 3768.72  15
 -10   5   0 28311.7 3542.21   2
  10  -5   1 11292.7 2556.72  12
 -10  -5  -1 9723.45 2048.50  11
  10   5   1 10707.2 2103.97   5
  10   5   1 15016.5 2854.06   3
  10  -5   1 10375.9 2264.49   8
 -10  -5  -1 8242.96 1823.76   7
  10   5   1 5475.01 1552.56  16
 -10   5  -1 13072.6 2483.64  15
 -10   5  -1 9082.70 2028.31   2
  10   5   2 29774.8 3554.29   5
  10  -5   2 29927.1 3864.18  12
 -10  -5  -2 29642.1 3446.19  11
  10   5   2 30618.7 3995.86   3
 -10   5  -2 28607.8 3368.73   2
  10  -5   2 25576.4 3225.72   8
 -10  -5  -2 19876.3 2894.72   7
  10   5   2 25313.9 3299.83  16
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  10  -5   3 5351.89 1915.23  12
  10   5   3 3576.58 1235.71   5
  10   5   3 6946.82 1989.10   3
 -10  -5  -3 2780.36 1225.61   7
 -10   5  -3 6266.76 1528.92   2
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  10  -5   4 819.980 1472.51  12
  10   5   4-609.253 711.274   5
  10  -5   4 1919.32 1112.47   3
 -10  -5  -4 1738.12 1148.40   7
 -10   5  -4 223.932 718.335   2
 -10   5  -5 15006.3 2737.01   6
  10   5   5 16816.7 2843.12   5
  10  -5   5 20270.9 3343.12  12
  10  -5   5 17409.3 2816.35   3
  10   5   5 8407.77 1769.95  16
 -10   5  -6 10568.6 2411.62   6
  10  -5   6 8653.12 2448.06  12
  10  -5   6 11106.9 2314.41   3
  10  -5   7 11753.7 2293.55   1
 -10   5  -7 14035.9 2827.37   6
  10  -5   7 17413.0 3489.35  12
  10  -5   8 23335.2 3922.60  12
  10  -6  -6 3769.94 1875.60  10
  10  -6  -5 5540.82 2076.65  10
  10   6  -5 4479.45 1399.19   5
  10   6  -4 42149.3 4072.35   5
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  10  -6  -4 43044.1 4220.25  10
  10  -6  -4 40870.2 4577.14   8
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  10  -6  -3 10249.7 2231.36  10
  10   6  -3 9543.59 1982.83   5
  10  -6  -3 12850.6 2619.87   8
 -10  -6   3 11399.3 2161.79   7
 -10   6   3 13249.5 2468.00  15
 -10   6   3 12370.1 2468.00   2
  10  -6  -2 35084.0 4300.11  12
 -10  -6   2 26419.1 3120.19  11
  10  -6  -2 22616.9 3022.12  10
  10   6  -2 21830.8 2943.30   5
  10  -6  -2 29196.8 3705.28   8
 -10  -6   2 24375.7 3124.35   7
  10   6  -2 20473.4 3051.93  16
 -10   6   2 24788.8 3358.51  15
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  10  -6  -1 15395.1 2973.75  12
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  10   6  -1 13012.3 2332.46   5
  10  -6  -1 9477.63 2198.86   8
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  10   6  -1 6667.37 1813.48  16
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 -10   6   1 14733.1 2638.38   2
  10  -6   0-1227.12 1434.63  12
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  10   6   0 2558.88 1042.40   5
  10   6   0 5693.58 1832.91   3
  10  -6   0 264.166 1138.02   8
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  10   6   1 1270.69 1052.00   3
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  10  -6   2 34707.8 3774.39   8
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  10   6   2 23571.5 3165.88  16
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  10  -6   3 9386.27 2507.66  12
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  10   6   3 7691.17 1885.57   5
  10   6   3 2984.75 1159.11  16
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  10   6   4 19884.1 3027.75   5
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  10   7  -1 21802.8 3033.20   5
  10   7  -1 21593.2 3503.38   3
  10  -7  -1 24144.9 3483.79   8
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  10   7   0 1323.08 806.946   5
  10  -7   0 3520.97 1821.28   8
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  10   7   1 74533.8 5700.71   5
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  10  -7   1 68941.2 5547.19   8
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  10  -7   2-583.982 1602.59   8
  10   7   2 2877.72 1178.49  16
 -10   7  -2-298.684 413.356   2
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 -10   7  -3 4750.29 1503.65   2
  10   7   4-3880.45 1304.89  16
 -10   7  -4 1158.66 926.050   2
 -10   7  -5 4336.50 1928.62   6
 -10   7  -5 5720.88 1836.69   2
 -10  -8   6 745.247 1465.24  11
 -10  -8   5 10256.1 2229.06  11
 -10  -8   4 30907.0 3650.15  11
 -10  -8   3 2006.47 1299.45  11
 -10  -8   2 23837.7 3149.54  11
 -10  -8   1-201.563 1194.55  11
  10  -8  -1-441.765 1329.57   8
 -10  -8   0 3692.25 1554.60  11
  10  -8   0 2094.67 1698.29   8
 -10  -8  -1 5621.56 1810.63  11
  10  -8   1 6281.54 2338.64   8
  10  -8   2 14223.4 2980.62   8
 -10   8  -2 15347.9 2650.48   2
 -10   8  -3 3754.69 1411.52   2
 -10   8  -4 28025.3 3576.19   2
 -10   8  -5 4160.88 1619.57   2
  10  -9   1 17897.3 3252.27   8
  10  -9   2 10576.9 2765.10   8
 -11   0   5 36094.5 4085.59   7
 -11   0   4-1545.96 1363.24   7
  11   0  -3 5987.15 2076.49  10
 -11   0   3 3269.54 1676.20   7
  11   0  -2-490.891 1575.34  10
 -11   0   2-557.963 1338.87   7
  11   0  -1 25792.2 3402.07  10
 -11   0   1 25856.8 3356.51   7
  11   0   0 5408.53 2387.50  12
 -11   0   0-157.823 1206.43   7
  11   0   1 46180.6 4831.39  12
 -11   0  -1 44778.7 4427.23   7
  11   0   2-331.049 1848.55  12
 -11   0  -2-1243.65 1444.02   7
  11   0   3 20853.3 3468.75  12
 -11   0  -3 16157.2 2832.46   7
  11   0   4 428.769 1906.83  12
  11   0   4 1458.21 984.543   1
 -11   0  -4-789.913 1754.38   7
 -11   1   6 1708.68 1691.05   7
 -11   1   5 6300.99 2093.34   7
 -11  -1   5 4492.42 1878.95  15
 -11   1   4 30929.8 3750.05   7
 -11  -1   4 32831.1 3866.78  15
  11   1  -3 4280.47 1919.22  10
  11  -1  -3 6157.67 2219.52  10
 -11  -1   3 3087.21 1589.77   7
 -11   1   3 1186.39 1423.38   7
 -11  -1   3 1104.57 1531.12  15
  11   1  -2 67851.1 5504.60  10
  11  -1  -2 61151.2 5167.67  10
 -11  -1   2 56201.3 4974.65   7
 -11   1   2 58935.9 5018.11   7
 -11  -1   2 58563.0 5129.93  15
  11   1  -1 10473.9 2450.54  10
  11  -1  -1 11478.3 2482.06  10
 -11  -1   1 11257.6 2348.66   7
 -11   1   1 8605.90 2255.71   7
 -11  -1   1 9235.35 2360.96  15
  11   1   0 9337.80 2673.00  12
 -11  -1   0 4742.83 1693.12   7
 -11   1   0 4861.56 1816.30   7
 -11  -1  -1 141.907 1074.64   7
 -11   1  -1-186.910 1287.66   7
  11  -1   2 9749.39 2595.98  12
  11   1   2 14248.2 2906.43  12
 -11  -1  -2 9106.37 2213.98   7
 -11   1  -2 10100.5 2263.44   7
  11  -1   3 1703.79 2227.18  12
  11   1   3 421.155 1670.41  12
 -11   1  -3 1126.73 1488.86   7
  11  -1   4 55345.3 5401.27  12
  11   1   4 53884.9 4794.38   1
 -11   1  -4 51441.4 4700.97   7
 -11   1  -5 15938.6 2990.99   7
 -11  -2   4 17260.6 2923.51  15
  11  -2  -3 1604.57 1706.75  10
 -11  -2   3 362.111 1404.65  15
  11  -2  -2 575.677 1521.52  10
 -11  -2   2-352.724 1527.51  15
  11   2  -1 9803.25 2107.08   5
  11   2   0 31794.0 3634.56   5
  11   2   1 21755.8 3437.96  12
  11   2   1 14020.1 2536.25   5
  11   2   2 22345.5 3416.41  12
  11   2   2 12773.4 2576.34   5
  11   2   3 8414.25 2228.92   5
  11   3  -5 1154.54 1460.72   5
  11   3  -4 9003.71 2176.61   5
  11   3  -3 62572.1 5099.88   5
  11  -3  -3 69876.5 5563.84  10
 -11  -3   3 68818.7 5331.53  15
  11   3  -2 1440.37 1237.44   5
 -11  -3   2 1628.69 1720.83  15
  11   3  -1 27451.6 3535.73   5
  11   3   0-733.158 1222.04   5
  11   3   1-1655.74 1574.65   5
  11  -3   1-796.484 1795.23   8
  11   3   2 5643.24 1939.20   5
  11  -4  -3 2983.14 1937.15  10
  11   4  -2 3781.68 1601.32   5
  11   4  -1 87.9772 1162.24   5
  11   4   0 34115.6 3913.68   5
  11  -4   0 35349.0 4177.81   8
  11  -4   1 782.394 1693.08   8
 -11  -4  -2 35902.0 3994.10  11
 -11   4  -3 10612.8 2269.39   2
 -11  -5  -1 1515.58 1854.54  11
  11  -5   1 2230.96 2025.16   8
   0   0   0    0.00    0.00   0
TITL cherie in P2(1)/n
REM P2(1)/n (#14 in standard setting)
CELL 0.71073   7.936343  14.409605  14.285058  90.0000  91.7745  90.0000
ZERR    5.00   0.000121   0.000220   0.000220   0.0000   0.0014   0.0000
LATT  1
SYMM -x+1/2, y+1/2,-z+1/2
SFAC C H P S Cl Au
UNIT 55.00 105.00 5.00 5.00 15.00 5.00
TREF
HKLF 4
END
;
_shelx_hkl_checksum              58802
_shelx_res_file
;
TITL cherie in P2(1)/n
    shelx.res
    created by SHELXL-2019/3 at 10:13:56 on 06-Nov-2023
CELL 0.71073   7.936343  14.409605  14.285058  90.0000  91.7745  90.0000
ZERR    4.00   0.0003   0.0004   0.0004   0.0000   0.003   0.0000
LATT  1
SYMM -x+1/2, y+1/2,-z+1/2
SFAC C H P S Cl Au
UNIT 40.00 92.00 4.00 4.00 12.00 4.00
L.S. 6
FMAP 2
PLAN 10
TEMP -173
ACTA 60
CONF 2.35
SIZE 0.3 0.2 0.2
BOND $H
HTAB C3 CL3
EQIV $1 1+x,y,z
HTAB C3 CL2_$1
EQIV $2 0.5+x, 0.5-y, 0.5+z
HTAB C21 CL2_$2
HTAB C22 CL2_$2
EQIV $3 1.5-x,0.5+y,0.5-z
HTAB C13 CL3_$3
EQIV $4 -1+x,y,z
RTAB CONT CL2 CL3_$4
RTAB ANGL AU1 CL2 CL3_$4
RTAB ANGL CL2 CL3_$4 AU1_$4
EQIV $5 1-x,-y,1-z
RTAB CONT S1 S1_$5
WGHT    0.011500    2.555700
FVAR       2.34519
AU1   6    0.471368    0.070447    0.321567    11.00000    0.01406    0.01090 =
         0.01491   -0.00097    0.00199   -0.00074
CL1   5    0.433698    0.016057    0.170125    11.00000    0.02667    0.02495 =
         0.01657   -0.00396   -0.00173    0.00035
CL2   5    0.188065    0.097624    0.326078    11.00000    0.01408    0.02796 =
         0.02738   -0.00095    0.00080    0.00116
CL3   5    0.750813    0.033766    0.318624    11.00000    0.01580    0.02160 =
         0.02320   -0.00774    0.00246    0.00248
S1    4    0.491649    0.123263    0.475522    11.00000    0.01980    0.01385 =
         0.01542   -0.00160    0.00549   -0.00496
P1    3    0.654821    0.233970    0.488212    11.00000    0.01174    0.01043 =
         0.01322   -0.00070    0.00175    0.00053
C1    1    0.611294    0.326712    0.399074    11.00000    0.02667    0.01256 =
         0.01407    0.00238    0.00258    0.00066
C2    1    0.612517    0.274873    0.607150    11.00000    0.01710    0.01859 =
         0.01361   -0.00489    0.00306    0.00010
AFIX  13
H2    2    0.701534    0.321315    0.624880    11.00000   -1.20000
AFIX   0
C3    1    0.875493    0.197112    0.480772    11.00000    0.01620    0.02292 =
         0.02606   -0.00794   -0.00004    0.00466
AFIX  13
H3    2    0.889522    0.177394    0.414348    11.00000   -1.20000
AFIX   0
C11   1    0.677796    0.420474    0.436752    11.00000    0.02676    0.01257 =
         0.02873    0.00097    0.00689   -0.00348
AFIX 137
H11A  2    0.664136    0.467885    0.387920    11.00000   -1.50000
H11B  2    0.797448    0.414501    0.454791    11.00000   -1.50000
H11C  2    0.614084    0.438648    0.491501    11.00000   -1.50000
AFIX   0
C12   1    0.423365    0.334934    0.375886    11.00000    0.03606    0.02022 =
         0.03972    0.00522   -0.01832    0.00302
AFIX 137
H12A  2    0.363374    0.349423    0.433018    11.00000   -1.50000
H12B  2    0.381545    0.276083    0.349810    11.00000   -1.50000
H12C  2    0.404201    0.384591    0.329903    11.00000   -1.50000
AFIX   0
C13   1    0.703365    0.301569    0.308867    11.00000    0.06373    0.01708 =
         0.01918    0.00363    0.01395    0.00205
AFIX 137
H13A  2    0.669156    0.239351    0.288111    11.00000   -1.50000
H13B  2    0.825429    0.302658    0.321490    11.00000   -1.50000
H13C  2    0.673948    0.346738    0.259745    11.00000   -1.50000
AFIX   0
C21   1    0.442118    0.322060    0.616713    11.00000    0.02995    0.02407 =
         0.02050    0.00225    0.00938    0.00745
AFIX 137
H21A  2    0.351900    0.277980    0.600347    11.00000   -1.50000
H21B  2    0.434612    0.375598    0.574483    11.00000   -1.50000
H21C  2    0.430237    0.342953    0.681460    11.00000   -1.50000
AFIX   0
C22   1    0.624455    0.195027    0.679381    11.00000    0.03575    0.03255 =
         0.01519    0.00093    0.00054    0.01041
AFIX 137
H22A  2    0.612684    0.220219    0.742566    11.00000   -1.50000
H22B  2    0.734042    0.164198    0.675259    11.00000   -1.50000
H22C  2    0.534206    0.150064    0.666093    11.00000   -1.50000
AFIX   0
C31   1    1.004156    0.275813    0.498415    11.00000    0.01678    0.04586 =
         0.07730   -0.03695   -0.00069   -0.00111
AFIX 137
H31A  2    0.987941    0.302640    0.560531    11.00000   -1.50000
H31B  2    0.987610    0.323988    0.450586    11.00000   -1.50000
H31C  2    1.118712    0.250844    0.495347    11.00000   -1.50000
AFIX   0
C32   1    0.921004    0.112357    0.540482    11.00000    0.03165    0.05428 =
         0.03097    0.00612    0.00322    0.02899
AFIX 137
H32A  2    1.025232    0.084618    0.518326    11.00000   -1.50000
H32B  2    0.829555    0.066760    0.535428    11.00000   -1.50000
H32C  2    0.937441    0.131286    0.606022    11.00000   -1.50000
AFIX   0
HKLF 4
REM  cherie in P2(1)/n
REM wR2 = 0.0450, GooF = S = 1.123, Restrained GooF = 1.123 for all data
REM R1 = 0.0251 for 4296 Fo > 4sig(Fo) and 0.0339 for all 4881 data
REM 152 parameters refined using 0 restraints
END
WGHT      0.0115      2.5555
REM Highest difference peak  2.523,  deepest hole -1.501,  1-sigma level  0.161
Q1    1   0.4964  0.0348  0.3538  11.00000  0.05    2.52
Q2    1   0.4160  0.0415  0.2904  11.00000  0.05    1.37
Q3    1   0.4491 -0.0290  0.1993  11.00000  0.05    1.02
Q4    1   0.4201  0.1228  0.2828  11.00000  0.05    1.00
Q5    1   0.5192  0.0743  0.3019  11.00000  0.05    0.91
Q6    1   0.5083  0.0841  0.3222  11.00000  0.05    0.77
Q7    1   0.4357  0.0909  0.3359  11.00000  0.05    0.72
Q8    1   0.5344  0.0828  0.4012  11.00000  0.05    0.69
Q9    1   0.2154  0.0501  0.3419  11.00000  0.05    0.66
Q10   1   0.9534  0.2463  0.5421  11.00000  0.05    0.66
;
_shelx_res_checksum              93399
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au Au1 0.47137(2) 0.07045(2) 0.32157(2) 0.01326(4) Uani d 1 . .
Cl Cl1 0.43370(11) 0.01606(6) 0.17013(5) 0.02278(17) Uani d 1 . .
Cl Cl2 0.18806(10) 0.09762(6) 0.32608(6) 0.02314(17) Uani d 1 . .
Cl Cl3 0.75081(10) 0.03377(6) 0.31862(6) 0.02016(16) Uani d 1 . .
S S1 0.49165(10) 0.12326(5) 0.47552(5) 0.01625(16) Uani d 1 . .
P P1 0.65482(10) 0.23397(5) 0.48821(5) 0.01177(15) Uani d 1 . .
C C1 0.6113(4) 0.3267(2) 0.3991(2) 0.0177(7) Uani d 1 . .
C C2 0.6125(4) 0.2749(2) 0.6072(2) 0.0164(6) Uani d 1 . .
H H2 0.701534 0.321315 0.624880 0.020 Uiso calc 1 . .
C C3 0.8755(4) 0.1971(2) 0.4808(2) 0.0217(7) Uani d 1 . .
H H3 0.889522 0.177394 0.414348 0.026 Uiso calc 1 . .
C C11 0.6778(4) 0.4205(2) 0.4368(2) 0.0226(7) Uani d 1 . .
H H11A 0.664136 0.467885 0.387920 0.034 Uiso calc 1 . .
H H11B 0.797448 0.414501 0.454791 0.034 Uiso calc 1 . .
H H11C 0.614084 0.438648 0.491501 0.034 Uiso calc 1 . .
C C12 0.4234(5) 0.3349(3) 0.3759(3) 0.0324(9) Uani d 1 . .
H H12A 0.363374 0.349423 0.433018 0.049 Uiso calc 1 . .
H H12B 0.381545 0.276083 0.349810 0.049 Uiso calc 1 . .
H H12C 0.404201 0.384591 0.329903 0.049 Uiso calc 1 . .
C C13 0.7034(6) 0.3016(2) 0.3089(2) 0.0331(9) Uani d 1 . .
H H13A 0.669156 0.239351 0.288111 0.050 Uiso calc 1 . .
H H13B 0.825429 0.302658 0.321490 0.050 Uiso calc 1 . .
H H13C 0.673948 0.346738 0.259745 0.050 Uiso calc 1 . .
C C21 0.4421(5) 0.3221(2) 0.6167(2) 0.0247(8) Uani d 1 . .
H H21A 0.351900 0.277980 0.600347 0.037 Uiso calc 1 . .
H H21B 0.434612 0.375598 0.574483 0.037 Uiso calc 1 . .
H H21C 0.430237 0.342953 0.681460 0.037 Uiso calc 1 . .
C C22 0.6245(5) 0.1950(3) 0.6794(2) 0.0278(8) Uani d 1 . .
H H22A 0.612684 0.220219 0.742566 0.042 Uiso calc 1 . .
H H22B 0.734042 0.164198 0.675259 0.042 Uiso calc 1 . .
H H22C 0.534206 0.150064 0.666093 0.042 Uiso calc 1 . .
C C31 1.0042(5) 0.2758(3) 0.4984(4) 0.0467(13) Uani d 1 . .
H H31A 0.987941 0.302640 0.560531 0.070 Uiso calc 1 . .
H H31B 0.987610 0.323988 0.450586 0.070 Uiso calc 1 . .
H H31C 1.118712 0.250844 0.495347 0.070 Uiso calc 1 . .
C C32 0.9210(5) 0.1124(3) 0.5405(3) 0.0389(11) Uani d 1 . .
H H32A 1.025232 0.084618 0.518326 0.058 Uiso calc 1 . .
H H32B 0.829555 0.066760 0.535428 0.058 Uiso calc 1 . .
H H32C 0.937441 0.131286 0.606022 0.058 Uiso calc 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Au1 0.01406(6) 0.01090(6) 0.01491(6) -0.00074(5) 0.00199(4) -0.00097(4)
Cl1 0.0267(4) 0.0249(4) 0.0166(4) 0.0004(3) -0.0017(3) -0.0040(3)
Cl2 0.0141(4) 0.0280(4) 0.0274(4) 0.0012(3) 0.0008(3) -0.0010(3)
Cl3 0.0158(4) 0.0216(4) 0.0232(4) 0.0025(3) 0.0025(3) -0.0077(3)
S1 0.0198(4) 0.0138(4) 0.0154(4) -0.0050(3) 0.0055(3) -0.0016(3)
P1 0.0117(4) 0.0104(4) 0.0132(4) 0.0005(3) 0.0017(3) -0.0007(3)
C1 0.0267(17) 0.0126(15) 0.0141(15) 0.0007(13) 0.0026(13) 0.0024(12)
C2 0.0171(15) 0.0186(16) 0.0136(14) 0.0001(12) 0.0031(12) -0.0049(12)
C3 0.0162(16) 0.0229(18) 0.0261(18) 0.0047(13) 0.0000(13) -0.0079(14)
C11 0.0268(18) 0.0126(16) 0.0287(18) -0.0035(13) 0.0069(14) 0.0010(13)
C12 0.036(2) 0.0202(19) 0.040(2) 0.0030(16) -0.0183(18) 0.0052(16)
C13 0.064(3) 0.0171(18) 0.0192(17) 0.0021(18) 0.0139(18) 0.0036(14)
C21 0.0299(19) 0.0241(18) 0.0205(17) 0.0074(15) 0.0094(15) 0.0023(14)
C22 0.036(2) 0.033(2) 0.0152(16) 0.0104(17) 0.0005(15) 0.0009(15)
C31 0.0168(19) 0.046(3) 0.077(3) -0.0011(18) -0.001(2) -0.037(2)
C32 0.032(2) 0.054(3) 0.031(2) 0.029(2) 0.0032(17) 0.0061(19)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
Cl3 Au1 Cl2 . . 176.43(3) y
Cl3 Au1 Cl1 . . 90.10(3) y
Cl2 Au1 Cl1 . . 89.18(3) y
Cl3 Au1 S1 . . 93.11(3) y
Cl2 Au1 S1 . . 87.51(3) y
Cl1 Au1 S1 . . 176.43(3) y
P1 S1 Au1 . . 111.18(4) y
C3 P1 C2 . . 110.36(15) y
C3 P1 C1 . . 108.88(16) y
C2 P1 C1 . . 111.39(14) y
C3 P1 S1 . . 111.66(12) y
C2 P1 S1 . . 101.38(11) y
C1 P1 S1 . . 113.03(11) y
C12 C1 C11 . . 109.3(3) ?
C12 C1 C13 . . 108.8(3) ?
C11 C1 C13 . . 109.3(3) ?
C12 C1 P1 . . 111.3(2) ?
C11 C1 P1 . . 109.5(2) ?
C13 C1 P1 . . 108.6(2) ?
C21 C2 C22 . . 108.0(3) ?
C21 C2 P1 . . 114.4(2) ?
C22 C2 P1 . . 111.6(2) ?
C21 C2 H2 . . 107.5 ?
C22 C2 H2 . . 107.5 ?
P1 C2 H2 . . 107.5 ?
C32 C3 C31 . . 110.7(3) ?
C32 C3 P1 . . 114.1(3) ?
C31 C3 P1 . . 113.9(2) ?
C32 C3 H3 . . 105.8 ?
C31 C3 H3 . . 105.8 ?
P1 C3 H3 . . 105.8 ?
C1 C11 H11A . . 109.5 ?
C1 C11 H11B . . 109.5 ?
H11A C11 H11B . . 109.5 ?
C1 C11 H11C . . 109.5 ?
H11A C11 H11C . . 109.5 ?
H11B C11 H11C . . 109.5 ?
C1 C12 H12A . . 109.5 ?
C1 C12 H12B . . 109.5 ?
H12A C12 H12B . . 109.5 ?
C1 C12 H12C . . 109.5 ?
H12A C12 H12C . . 109.5 ?
H12B C12 H12C . . 109.5 ?
C1 C13 H13A . . 109.5 ?
C1 C13 H13B . . 109.5 ?
H13A C13 H13B . . 109.5 ?
C1 C13 H13C . . 109.5 ?
H13A C13 H13C . . 109.5 ?
H13B C13 H13C . . 109.5 ?
C2 C21 H21A . . 109.5 ?
C2 C21 H21B . . 109.5 ?
H21A C21 H21B . . 109.5 ?
C2 C21 H21C . . 109.5 ?
H21A C21 H21C . . 109.5 ?
H21B C21 H21C . . 109.5 ?
C2 C22 H22A . . 109.5 ?
C2 C22 H22B . . 109.5 ?
H22A C22 H22B . . 109.5 ?
C2 C22 H22C . . 109.5 ?
H22A C22 H22C . . 109.5 ?
H22B C22 H22C . . 109.5 ?
C3 C31 H31A . . 109.5 ?
C3 C31 H31B . . 109.5 ?
H31A C31 H31B . . 109.5 ?
C3 C31 H31C . . 109.5 ?
H31A C31 H31C . . 109.5 ?
H31B C31 H31C . . 109.5 ?
C3 C32 H32A . . 109.5 ?
C3 C32 H32B . . 109.5 ?
H32A C32 H32B . . 109.5 ?
C3 C32 H32C . . 109.5 ?
H32A C32 H32C . . 109.5 ?
H32B C32 H32C . . 109.5 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Au1 Cl3 . 2.2815(8) y
Au1 Cl2 . 2.2851(8) y
Au1 Cl1 . 2.3116(8) y
Au1 S1 . 2.3281(8) y
S1 P1 . 2.0592(11) y
P1 C3 . 1.836(3) y
P1 C2 . 1.839(3) y
P1 C1 . 1.871(3) y
C1 C12 . 1.522(5) ?
C1 C11 . 1.541(4) ?
C1 C13 . 1.544(4) ?
C2 C21 . 1.524(4) ?
C2 C22 . 1.546(5) ?
C2 H2 . 1.0000 ?
C3 C32 . 1.527(5) ?
C3 C31 . 1.542(5) ?
C3 H3 . 1.0000 ?
C11 H11A . 0.9800 ?
C11 H11B . 0.9800 ?
C11 H11C . 0.9800 ?
C12 H12A . 0.9800 ?
C12 H12B . 0.9800 ?
C12 H12C . 0.9800 ?
C13 H13A . 0.9800 ?
C13 H13B . 0.9800 ?
C13 H13C . 0.9800 ?
C21 H21A . 0.9800 ?
C21 H21B . 0.9800 ?
C21 H21C . 0.9800 ?
C22 H22A . 0.9800 ?
C22 H22B . 0.9800 ?
C22 H22C . 0.9800 ?
C31 H31A . 0.9800 ?
C31 H31B . 0.9800 ?
C31 H31C . 0.9800 ?
C32 H32A . 0.9800 ?
C32 H32B . 0.9800 ?
C32 H32C . 0.9800 ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
C3 H3 Cl3 . 1.00 2.70 3.427(3) 130.1 yes
C3 H3 Cl2 1_655 1.00 2.95 3.665(3) 129.1 yes
C21 H21C Cl2 4_666 0.98 2.99 3.706(4) 131.1 yes
C22 H22A Cl2 4_666 0.98 2.94 3.675(4) 132.9 yes
C13 H13C Cl3 2_655 0.98 2.99 3.832(4) 145.3 yes
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
Cl3 Au1 S1 P1 . . . . 61.27(5) y
Cl2 Au1 S1 P1 . . . . -122.25(5) y
Au1 S1 P1 C3 . . . . -73.62(13) y
Au1 S1 P1 C2 . . . . 168.88(11) y
Au1 S1 P1 C1 . . . . 49.55(12) y
C3 P1 C1 C12 . . . . 158.8(2) ?
C2 P1 C1 C12 . . . . -79.2(3) ?
S1 P1 C1 C12 . . . . 34.1(3) ?
C3 P1 C1 C11 . . . . -80.2(2) ?
C2 P1 C1 C11 . . . . 41.7(3) ?
S1 P1 C1 C11 . . . . 155.07(19) ?
C3 P1 C1 C13 . . . . 39.1(3) ?
C2 P1 C1 C13 . . . . 161.0(2) ?
S1 P1 C1 C13 . . . . -85.6(3) ?
C3 P1 C2 C21 . . . . 170.2(2) ?
C1 P1 C2 C21 . . . . 49.1(3) ?
S1 P1 C2 C21 . . . . -71.3(2) ?
C3 P1 C2 C22 . . . . -66.8(3) ?
C1 P1 C2 C22 . . . . 172.2(2) ?
S1 P1 C2 C22 . . . . 51.7(2) ?
C2 P1 C3 C32 . . . . 65.5(3) ?
C1 P1 C3 C32 . . . . -172.0(3) ?
S1 P1 C3 C32 . . . . -46.5(3) ?
C2 P1 C3 C31 . . . . -63.0(3) ?
C1 P1 C3 C31 . . . . 59.6(3) ?
S1 P1 C3 C31 . . . . -174.9(3) ?