#------------------------------------------------------------------------------ #$Date: 2024-05-06 06:23:16 +0200 (Mon, 06 May 2024) $ #$Revision: 291733 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/30/2023051.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023051 loop_ _publ_author_name 'Upmann, Daniel' 'Bockfeld, Dirk' 'Jones, Peter G.' 'Târcoveanu, Eliza' _publ_section_title ; Crystal structures of ten phosphane chalcogenide complexes of gold(III) chloride and bromide. ; _journal_coeditor_code YZ2051 _journal_issue 'Pt 4' _journal_name_full 'Acta crystallographica. Section E, Crystallographic communications' _journal_page_first 355 _journal_page_last 369 _journal_paper_doi 10.1107/S2056989024002032 _journal_volume 80 _journal_year 2024 _chemical_formula_iupac '[Au Cl3 (C10 H23 P S)]' _chemical_formula_moiety 'C10 H23 Au Cl3 P S' _chemical_formula_sum 'C10 H23 Au Cl3 P S' _chemical_formula_weight 509.63 _chemical_name_systematic ; (tert-Butyldipropan-2-ylphosphane sulfide-\kS)trichloridogold(III) ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2019/3 _cell_angle_alpha 90 _cell_angle_beta 94.525(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 8.4533(2) _cell_length_b 17.0563(4) _cell_length_c 11.4826(3) _cell_measurement_reflns_used 16512 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 30.7885 _cell_measurement_theta_min 2.1384 _cell_volume 1650.42(7) _computing_cell_refinement ; CrysAlisPro, Version 1.171.35.11 (Rigaku OD, 2020) ; _computing_data_collection ; CrysAlisPro, Version 1.171.35.11 (Rigaku OD, 2020) ; _computing_data_reduction ; CrysAlisPro, Version 1.171.35.11 (Rigaku OD, 2020) ; _computing_molecular_graphics ; Bruker XP, Version 5.1 (Bruker, 1998) ; _computing_publication_material ; SHELXL-2019/3 (Sheldrick, 2015) ; _computing_structure_refinement ; SHELXL-2019/3 (Sheldrick, 2015) ; _computing_structure_solution ; SHELXS-97 (Sheldrick, 2008) ; _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean 16.1419 _diffrn_measured_fraction_theta_full 0.983 _diffrn_measured_fraction_theta_max 0.934 _diffrn_measurement_device_type 'Oxford Diffraction Xcalibur, Eos' _diffrn_measurement_method '\w scan' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0400 _diffrn_reflns_av_unetI/netI 0.0242 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_k_min -24 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_number 40041 _diffrn_reflns_theta_full 30.000 _diffrn_reflns_theta_max 30.857 _diffrn_reflns_theta_min 2.388 _diffrn_source 'Enhance (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 9.599 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.19206 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (CrysAlisPro; Rigaku OD, 2020) ; _exptl_crystal_colour 'dichroic red / orange' _exptl_crystal_density_diffrn 2.051 _exptl_crystal_density_method 'not measured' _exptl_crystal_description plate _exptl_crystal_F_000 976 _exptl_crystal_size_max 0.3 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.02 _refine_diff_density_max 2.152 _refine_diff_density_min -1.414 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.071 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 152 _refine_ls_number_reflns 4863 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.071 _refine_ls_R_factor_all 0.0247 _refine_ls_R_factor_gt 0.0210 _refine_ls_shift/su_max 0.004 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0188P)^2^+1.7957P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0442 _refine_ls_wR_factor_ref 0.0456 _reflns_number_gt 4483 _reflns_number_total 4863 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file yz2051.cif _cod_data_source_block 10a _cod_depositor_comments 'Adding full bibliography for 2023050--2023062.cif.' _cod_original_cell_volume 1650.43(7) _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 2023051 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.161 _shelx_estimated_absorpt_t_max 0.831 _shelx_hkl_file ; 0 0 2 656480. 13531.0 6 0 0 2 648112. 13655.6 11 0 0 -2 628888. 13518.0 6 0 0 2 630127. 13527.2 10 0 0 2 645848. 13660.2 5 0 0 -2 635178. 13644.7 5 0 0 -2 656265. 13577.0 4 0 0 -2 643413. 13654.9 8 0 0 -2 627830. 13641.6 11 0 0 2 645768. 13562.3 4 0 0 2 631777. 13625.1 8 0 0 3 123.396 82.4128 6 0 0 3 269.865 106.093 10 0 0 3 139.066 118.906 5 0 0 3 229.258 145.914 8 0 0 3 97.8629 90.0792 11 0 0 -3 114.052 99.3623 8 0 0 -3-32.6837 114.029 11 0 0 -3-5.63075 77.2420 4 0 0 -3 73.7674 100.309 5 0 0 -3 69.8489 81.1466 6 0 0 3 93.2232 94.7098 4 0 0 -4 19560.1 963.703 11 0 0 4 20718.3 958.141 8 0 0 4 18716.8 818.538 10 0 0 -4 18898.7 823.117 6 0 0 -4 19282.1 955.991 5 0 0 -5 186.800 228.538 11 0 0 5 641.152 235.616 10 0 0 5 487.415 222.818 8 0 0 -5 1051.56 329.510 5 0 0 -6 6505.41 674.248 11 0 0 6 5921.88 511.950 10 0 0 -6 6815.32 655.590 5 0 0 6 5986.66 607.148 8 0 0 7 356.023 203.080 8 0 0 -7 410.720 274.345 5 0 0 -7 736.129 337.598 11 0 0 7 605.336 224.217 10 0 0 -8 34265.7 1809.34 5 0 0 8 32597.1 1705.36 8 0 0 8 34163.5 1530.97 10 0 0 -8 33507.1 1830.74 11 0 0 9-297.911 214.000 10 0 0 -9 118.538 262.074 11 0 0 9 237.833 263.678 8 0 0 -9 80.8363 217.073 5 0 0 -10 91310.4 3673.98 5 0 0 -10 92422.7 3752.41 11 0 0 10 93942.4 3206.18 10 0 0 10 94417.9 3567.52 8 0 0 11 203.905 193.125 10 0 0 -11 99.5354 411.630 11 0 0 11 256.027 270.964 8 0 0 -11-33.5383 296.897 5 0 0 -12 87787.9 4052.91 11 0 0 12 91503.6 3383.16 10 0 0 12 89575.6 3785.02 8 0 0 -12 91775.1 4008.18 5 0 0 -13 445.765 469.707 5 0 0 13 1026.35 406.292 10 0 0 -13 360.352 466.599 11 0 0 13 1259.35 573.346 8 0 0 14 21816.7 1893.12 8 0 0 -14 21068.8 1970.50 5 0 0 -14 16592.6 1821.86 11 0 0 15 840.077 556.694 8 0 0 15 794.212 468.716 9 0 0 -15 795.227 727.472 11 0 0 15 631.250 462.975 12 0 0 -15 475.109 612.399 5 0 1 -1 67913.6 1597.96 6 0 1 -2 1933.28 178.195 6 0 -1 -2 2022.34 217.335 8 0 1 -2 2360.03 207.511 8 0 -1 2 2181.44 189.382 6 0 1 -2 1994.65 208.740 11 0 1 2 2172.84 213.619 11 0 -1 2 2041.06 151.897 10 0 -1 -2 2119.85 223.921 5 0 -1 2 1993.13 206.367 11 0 -1 2 1836.38 185.075 8 0 -1 -2 2230.31 204.574 4 0 1 -2 2185.12 165.394 10 0 1 2 2280.75 230.190 8 0 1 2 2179.88 193.664 4 0 1 -2 2063.47 201.982 5 0 -1 2 2097.16 211.733 5 0 -1 -2 2266.92 221.992 11 0 1 2 2195.27 220.333 5 0 -1 3 353594. 7710.55 10 0 -1 -3 351639. 7988.26 11 0 -1 3 352522. 7894.78 8 0 1 3 365457. 8031.38 5 0 -1 3 366894. 7846.18 6 0 -1 -3 361114. 8060.35 8 0 1 3 347775. 8021.81 8 0 1 -3 345949. 7988.99 11 0 1 -3 346500. 7805.29 6 0 -1 3 360551. 7989.22 5 0 1 3 361380. 8007.73 11 0 1 -3 366889. 7885.30 4 0 -1 -3 345762. 8006.57 5 0 1 3 355695. 7804.54 6 0 -1 3 364269. 8000.60 11 0 1 -3 353691. 7949.87 5 0 -1 -3 361003. 7883.21 4 0 1 3 342519. 7864.90 4 0 1 -3 358735. 7952.61 8 0 1 -4 481.028 130.220 6 0 1 4 592.090 152.334 4 0 1 4 296.329 152.364 8 0 -1 -4 556.992 182.981 11 0 -1 -4 457.223 154.974 5 0 1 4 393.656 118.437 10 0 -1 4 499.025 183.996 8 0 1 -4 433.778 141.624 11 0 1 -4 654.303 194.740 5 0 -1 4 500.839 127.804 10 0 1 5 237670. 5724.14 10 0 -1 -5 235255. 5962.07 5 0 1 -5 236150. 5880.04 5 0 1 5 228662. 5735.90 4 0 1 5 239727. 5944.05 8 0 -1 5 244056. 5830.02 8 0 -1 5 237139. 5532.21 10 0 1 -5 235625. 5642.77 6 0 1 -5 230957. 5949.95 11 0 -1 -5 235791. 5938.29 11 0 1 6 3799.81 467.841 4 0 -1 6 3226.45 359.400 10 0 1 -6 2874.83 467.996 11 0 1 6 2860.50 446.421 8 0 -1 6 3120.49 423.046 8 0 -1 -6 3328.11 472.912 5 0 -1 -6 3227.89 484.848 11 0 1 6 3066.61 388.611 10 0 1 -6 2998.54 379.040 6 0 1 -6 2845.39 427.623 5 0 -1 7 35287.4 1615.10 8 0 1 -7 33142.3 1696.28 11 0 1 -7 36404.3 1498.11 6 0 1 7 35138.6 1684.69 8 0 -1 7 35818.3 1403.00 10 0 -1 -7 34002.8 1713.10 11 0 1 -7 34698.5 1663.81 5 0 1 7 35016.0 1511.67 10 0 -1 -7 35253.1 1736.36 5 0 -1 8 6749.24 731.714 8 0 -1 -8 5415.75 717.241 5 0 1 8 6298.66 637.319 10 0 -1 -8 7532.97 850.088 11 0 -1 8 5966.09 570.993 10 0 1 8 6324.47 746.407 8 0 1 -8 5878.61 779.779 11 0 1 -8 5488.44 686.664 5 0 1 9 10222.7 1005.08 8 0 -1 -9 9301.58 981.386 5 0 -1 9 11096.9 993.472 8 0 -1 -9 10020.9 1036.73 11 0 1 -9 12178.7 1156.39 11 0 1 -9 9324.26 966.791 5 0 -1 9 11614.9 853.845 10 0 1 9 11188.1 903.194 10 0 1 -10-64.6708 255.630 5 0 1 10 149.811 193.814 10 0 1 10-8.87844 248.709 8 0 -1 10 257.987 214.593 10 0 -1 -10 168.084 304.415 5 0 -1 -10-4.32728 299.003 11 0 -1 10 322.072 324.326 8 0 1 -10 697.171 451.008 11 0 1 -11 6699.56 933.897 5 0 1 11 7651.37 831.123 10 0 -1 11 7062.34 753.970 10 0 -1 -11 7950.70 1043.33 5 0 -1 11 8149.73 963.575 8 0 1 -11 8087.01 1078.54 11 0 -1 -11 7581.73 1026.94 11 0 1 11 8512.76 1032.85 8 0 1 -12 2777.07 709.802 11 0 -1 12 3329.53 555.201 10 0 1 12 3292.50 563.365 10 0 -1 12 3301.63 692.987 8 0 1 12 4104.81 760.456 8 0 1 -12 2916.11 735.857 5 0 -1 -12 3034.30 770.453 5 0 -1 -12 3817.26 840.768 11 0 -1 -13 49099.8 3045.45 11 0 -1 13 53243.4 2423.45 10 0 -1 -13 52781.7 3082.12 5 0 -1 13 55388.0 2911.33 8 0 1 13 51319.9 2542.63 10 0 1 13 55970.6 3001.34 8 0 1 -13 51801.4 3164.75 11 0 -1 13 53803.5 2744.92 12 0 1 -13 52576.5 3026.58 5 0 -1 13 50938.3 2683.94 9 0 1 14 3398.93 801.048 8 0 -1 14 2061.35 627.048 9 0 1 -14 2551.40 782.604 5 0 -1 -14 1891.26 750.658 5 0 -1 14 2381.18 664.732 8 0 -1 14 2268.55 649.125 12 0 1 -14 2382.85 827.903 11 0 -1 -14 4194.47 1018.86 11 0 1 14 1944.13 531.759 10 0 -1 15 60818.4 3261.61 12 0 -1 -15 61293.2 3806.16 11 0 -1 -15 61912.2 3733.64 5 0 -1 15 62678.8 3293.93 9 0 1 15 62512.3 3515.16 8 0 1 -15 60448.2 3618.86 5 0 1 -15 67198.7 4016.36 11 0 2 0 349197. 7670.25 2 0 -2 0 351581. 8122.18 9 0 -2 0 357384. 8137.32 12 0 -2 0 335049. 7989.38 4 0 2 0 353810. 8306.18 3 0 -2 1 27577.3 747.962 5 0 -2 1 27489.9 789.149 2 0 -2 1 27753.2 871.538 6 0 2 1 26968.3 819.447 5 0 2 1 27350.8 838.267 11 0 -2 1 26232.4 838.246 9 0 -2 -1 27823.0 909.101 8 0 2 -1 27523.8 842.502 9 0 2 1 26437.7 859.458 2 0 -2 -1 27276.2 823.507 5 0 2 -1 28402.3 849.925 12 0 2 -1 25925.8 850.253 6 0 -2 -1 26979.1 862.629 2 0 -2 -1 27755.2 836.605 4 0 2 -1 26582.6 785.014 2 0 -2 1 26413.9 839.641 12 0 2 1 26631.7 897.449 8 0 2 -1 28001.3 747.016 5 0 2 -1 25941.2 820.795 11 0 -2 1 26509.1 816.877 11 0 2 1 26558.1 827.912 4 0 -2 2 179019. 3985.25 5 0 2 -2 174200. 3964.09 5 0 2 2 167577. 3995.49 4 0 -2 -2 168093. 4071.21 5 0 -2 2 175366. 4047.70 11 0 -2 2 175049. 3755.40 10 0 -2 -2 169727. 4035.04 11 0 -2 -2 177049. 4160.63 8 0 -2 2 172162. 3985.39 12 0 2 -2 172825. 3982.22 6 0 2 -2 171656. 3857.12 1 0 -2 2 174510. 3990.23 9 0 2 -2 172133. 4049.69 11 0 2 -2 171879. 3988.89 12 0 2 2 173276. 4060.56 5 0 -2 2 178294. 3994.94 6 0 2 -2 175076. 3961.76 8 0 2 -2 173198. 3994.84 9 0 2 -2 173281. 3764.33 10 0 2 2 166844. 4135.42 8 0 2 2 173795. 4054.05 11 0 -2 -2 177665. 4009.96 4 0 2 -3 104044. 2657.93 5 0 2 -3 102548. 2334.86 1 0 2 -3 100748. 2438.15 10 0 -2 -3 99732.0 2763.73 5 0 2 3 97457.6 2629.27 4 0 2 -3 99966.6 2583.47 6 0 -2 3 102827. 2397.36 10 0 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42555.0 1769.86 5 0 2 6 43868.2 1887.23 8 0 2 -6 42975.2 1633.70 6 0 -2 6 40945.5 1688.77 8 0 -2 -7 4833.45 647.281 5 0 2 7 5209.66 654.092 8 0 2 -7 5002.68 599.367 5 0 2 -7 4444.90 500.174 6 0 -2 7 4218.10 527.284 8 0 2 7 4434.01 530.570 4 0 2 7 5029.69 558.173 10 0 -2 7 3952.24 406.680 10 0 2 -7 3747.24 572.832 11 0 -2 -7 5159.97 663.536 11 0 2 -8 54086.4 2087.19 6 0 -2 -8 50704.1 2338.88 11 0 2 8 48896.1 2278.65 8 0 2 8 51439.8 2124.86 10 0 -2 8 52332.2 1878.30 10 0 -2 -8 49844.0 2345.30 5 0 2 -8 55734.1 2312.61 5 0 -2 8 52764.9 2187.76 8 0 2 -8 48762.4 2335.83 11 0 -2 9 17392.1 999.068 10 0 2 9 17920.4 1184.85 10 0 2 -9 18003.7 1400.30 11 0 -2 -9 15337.7 1286.58 5 0 -2 9 17691.4 1223.23 8 0 -2 -9 16227.6 1322.20 11 0 2 -9 17693.8 1272.31 5 0 2 9 15254.0 1229.79 8 0 2 -10 103679. 3885.99 5 0 -2 10 112467. 3854.16 8 0 2 10 105894. 3657.07 10 0 2 -10 101769. 4072.50 11 0 -2 10 108666. 3351.65 10 0 2 10 109475. 4032.34 8 0 -2 -10 99408.0 4025.15 5 0 -2 -10 104251. 4062.93 11 0 -2 11 13957.7 1196.35 12 0 2 11 15535.7 1240.68 10 0 -2 11 15156.4 1267.53 9 0 2 11 14796.6 1358.77 8 0 -2 11 14710.6 1292.37 8 0 -2 11 14869.0 1048.66 10 0 -2 -11 14176.0 1428.43 5 0 2 -11 15247.9 1355.95 5 0 2 -11 14841.0 1450.16 11 0 -2 -11 17656.7 1557.78 11 0 -2 12 62899.3 2886.53 9 0 -2 12 60181.8 2832.81 12 0 -2 -12 64443.0 3354.47 5 0 -2 -12 61114.9 3252.05 11 0 2 12 61922.9 3134.79 8 0 -2 12 63976.8 2553.14 10 0 2 -12 62230.6 3138.88 5 0 2 -12 63802.2 3372.15 11 0 2 12 66099.7 2890.35 10 0 -2 12 63747.6 3004.38 8 0 -2 -13 1188.12 555.390 11 0 -2 -13 1487.75 656.565 5 0 2 -13 2004.80 631.115 5 0 2 13 1758.23 610.268 8 0 -2 13 1184.85 496.328 9 0 2 -13 1124.20 549.571 11 0 -2 13 1048.73 454.972 12 0 2 13 1056.16 446.414 10 0 2 -14 7349.89 1300.01 11 0 -2 -14 8443.49 1310.30 11 0 2 14 9007.12 1275.57 8 0 -2 14 9146.40 1156.44 12 0 2 -14 10054.6 1295.53 5 0 2 14 9990.40 1142.35 10 0 -2 -14 9154.81 1363.71 5 0 -2 14 6851.77 1045.12 9 0 2 -15 8467.99 1307.24 5 0 -2 15 7722.20 1135.28 12 0 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2706.34 12 0 3 2 105288. 2740.62 11 0 3 -2 104730. 2399.33 10 0 -3 -2 110509. 2727.92 4 0 3 -2 110005. 2598.81 5 0 3 2 105457. 2864.07 8 0 3 2 109109. 2790.42 2 0 3 -2 111010. 2727.91 12 0 -3 2 108546. 2712.81 9 0 3 -2 106667. 2737.42 6 0 -3 2 106784. 2723.45 11 0 -3 2 108613. 2401.71 10 0 3 2 106580. 2713.56 4 0 3 2 106984. 2725.65 5 0 3 -2 106065. 2736.70 11 0 -3 2 113134. 2770.44 6 0 -3 -2 102308. 2710.97 11 0 -3 2 108884. 2607.45 5 0 -3 -2 104598. 2744.62 5 0 -3 -3 16305.9 802.084 11 0 3 3 17133.7 820.973 5 0 3 3 16366.9 884.048 8 0 -3 3 16069.9 751.342 12 0 -3 3 17407.0 777.855 6 0 3 -3 16478.4 644.407 1 0 3 -3 17297.6 745.584 5 0 -3 3 16370.6 755.859 9 0 -3 3 16714.9 756.796 5 0 3 3 16311.0 774.049 4 0 3 -3 16304.9 569.869 10 0 3 -3 16513.1 758.365 6 0 3 -3 17047.6 832.106 11 0 -3 3 17271.9 808.229 11 0 -3 3 16791.4 555.724 10 0 3 -3 17328.5 750.918 8 0 -3 -3 15430.0 814.047 5 0 3 3 17286.8 823.901 11 0 3 4 53192.1 1937.51 8 0 3 -4 54180.0 1749.41 5 0 -3 4 54386.9 1739.34 9 0 -3 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97784.9 3557.34 8 0 -11 -3 95781.6 2965.87 5 0 11 -3 87394.1 2809.58 10 0 -11 3 93802.1 2541.25 5 0 -11 3 89490.3 3685.49 9 0 -11 3 90562.3 3705.34 12 0 -11 -3 92599.3 3907.57 3 0 11 -4 5564.26 881.457 6 0 -11 -4 5207.10 825.902 3 0 11 4 6141.67 827.943 8 0 11 4 3802.08 260.462 7 0 -11 4 3579.25 633.176 12 0 11 4 4254.16 284.235 7 0 11 -4 5334.43 650.406 11 0 -11 -4 4512.46 572.826 5 0 11 4 5015.52 666.200 4 0 -11 4 4369.25 675.548 9 0 11 -4 5040.15 418.280 10 0 -11 4 4430.50 585.741 2 0 11 -4 5038.46 489.865 5 0 -11 -5 243644. 6500.77 5 0 11 -5 240824. 6646.09 11 0 -11 5 237534. 6407.93 2 0 -11 5 242819. 6873.68 9 0 11 -5 227176. 5372.76 10 0 11 5 240852. 7073.28 8 0 -11 5 244556. 6876.17 12 0 11 -5 240863. 5956.78 5 0 11 -5 237702. 7015.86 6 0 11 5 247054. 6737.50 4 0 -11 6 4914.95 639.080 2 0 11 6 4322.37 682.212 4 0 11 6 3761.87 741.621 8 0 11 -6 4403.34 697.674 11 0 -11 6 4249.19 725.097 9 0 -11 6 3769.81 661.230 12 0 11 -6 3585.07 482.902 5 0 -11 -6 3583.27 613.866 5 0 11 -6 2994.24 586.156 6 0 -11 7 183404. 5272.87 2 0 11 -7 183521. 5789.52 6 0 11 7 190563. 6268.89 8 0 11 7 182995. 5730.10 4 0 -11 7 177741. 5642.98 9 0 11 -7 190804. 5153.73 5 0 -11 -7 183906. 5739.61 5 0 11 -7 185183. 5883.88 11 0 -11 7 181611. 5651.02 12 0 11 8 356.783 510.334 8 0 -11 8 186.833 304.216 12 0 -11 8 442.012 256.531 2 0 -11 -8 1357.34 544.157 5 0 11 -8 223.983 191.400 5 0 11 8 523.134 508.798 10 0 11 -8 311.938 323.648 6 0 11 -8-68.4747 333.373 11 0 -11 8 1564.16 503.576 9 0 11 8 944.033 450.108 4 0 11 9 8836.45 1180.69 10 0 -11 -9 10621.9 1191.72 5 0 -11 9 8762.58 1030.44 12 0 11 -9 9668.25 951.851 5 0 11 -9 8098.93 1113.99 11 0 11 9 9564.62 1084.87 4 0 11 9 9497.21 1308.23 8 0 11 -9 9700.85 1074.19 6 0 -11 9 9982.28 1091.84 9 0 -11 9 9277.87 911.244 2 0 11 -10 2315.72 529.827 5 0 11 10 1548.97 571.247 4 0 -11 10 1761.48 530.200 12 0 11 -10 2308.65 710.160 11 0 11 10 2657.89 764.339 8 0 -11 10 1777.99 597.960 9 0 -11 10 2008.32 493.928 2 0 -11 -10 2576.34 746.931 5 0 11 -10 1990.26 570.434 6 0 11 10 1444.90 576.438 10 0 11 11 10972.5 1317.78 4 0 11 -11 10344.1 1406.13 11 0 11 -11 11005.2 1257.67 6 0 -11 -11 10199.7 1325.07 5 0 11 -11 11809.4 1170.60 5 0 -11 11 10447.6 1223.72 9 0 11 11 10970.2 1411.55 10 0 11 11 12140.2 1554.89 8 0 -11 11 9517.78 1180.93 12 0 -11 12 1753.80 577.021 12 0 11 12 1619.13 614.938 10 0 -11 -12 1820.57 644.037 5 0 11 -12 2075.48 715.052 11 0 11 12 1353.63 550.581 8 0 11 -12 1295.71 532.379 6 0 -11 12 1308.75 456.420 9 0 11 12 1706.21 663.088 4 0 11 -13 28499.2 2181.78 6 0 -11 -13 26755.7 2428.22 5 0 11 13 26154.8 2472.89 8 0 11 13 27392.5 2415.34 10 0 -11 13 28935.9 2193.98 12 0 -11 13 28815.3 2201.70 9 0 11 -13 24548.0 2423.53 11 0 11 13 28944.5 2326.20 4 0 11 -14 4811.39 918.013 6 0 -12 0 40296.9 2505.68 3 0 12 0 35471.5 1839.59 8 0 -12 0 34627.9 2326.00 13 0 -12 0 33935.6 2268.93 12 0 -12 0 34777.7 2299.47 9 0 -12 0 33196.2 1837.67 2 0 12 0 33303.2 1975.47 4 0 -12 0 32060.1 1205.41 5 0 -12 0 37095.9 1484.11 5 0 12 -1 233.677 297.740 4 0 -12 1-178.104 348.605 9 0 -12 1 335.490 292.273 2 0 12 -1 617.284 237.416 8 0 12 1 360.396 213.816 4 0 12 1 356.500 260.852 8 0 -12 1 367.313 370.994 3 0 -12 -1 350.325 450.424 13 0 -12 -1 248.686 111.226 5 0 -12 -1 594.231 365.949 3 0 12 -1 208.718 201.648 11 0 -12 1 110.150 93.9904 5 0 -12 -1 59.7159 242.754 2 0 -12 1-84.0157 289.280 13 0 -12 1-256.251 351.805 12 0 -12 2 62699.7 3156.14 12 0 -12 2 62852.2 3143.49 3 0 12 2 63598.3 2773.96 4 0 12 -2 63643.0 3046.30 4 0 12 -2 55038.6 3196.24 6 0 -12 2 62755.2 2654.65 2 0 -12 2 62879.9 1851.16 5 0 -12 -2 65302.5 2815.68 2 0 12 -2 66896.8 2500.04 11 0 -12 -2 65363.6 2148.84 5 0 -12 2 61334.7 3121.88 9 0 12 2 68963.5 2823.38 8 0 -12 -2 55799.3 3149.68 3 0 12 3 7750.30 879.556 4 0 -12 3 7856.16 1029.33 9 0 12 -3 7249.44 1067.71 6 0 12 -3 8538.36 818.412 11 0 -12 3 9140.26 1085.32 12 0 -12 -3 8291.58 704.857 5 0 12 3 8321.39 937.975 8 0 -12 3 8960.82 542.647 5 0 -12 -3 9713.20 1200.90 3 0 -12 3 8031.51 856.027 2 0 -12 4 14269.8 1326.51 9 0 -12 -4 16085.7 1072.88 5 0 -12 -4 16529.3 1527.72 3 0 12 4 13162.2 597.064 7 0 12 -4 13396.1 837.320 5 0 12 -4 13839.9 1405.03 6 0 -12 4 12090.6 1058.53 2 0 12 4 14641.7 1312.60 8 0 12 -4 14268.7 1103.79 11 0 12 4 14465.7 1192.57 4 0 -12 4 13380.5 1277.31 12 0 12 5 893.580 370.366 4 0 12 -5 800.496 538.039 6 0 -12 -5 841.446 551.148 3 0 -12 5 132.614 325.450 9 0 12 -5 738.550 367.148 11 0 -12 5 583.303 226.469 2 0 12 5 999.726 443.462 8 0 12 -5 988.336 248.233 5 0 -12 -5 1064.02 376.126 5 0 -12 5 68.7890 273.737 12 0 12 6 17837.9 1421.65 4 0 12 -6 20768.5 1494.96 11 0 12 -6 17904.3 1073.06 5 0 -12 6 17661.9 1442.07 9 0 12 -6 15739.0 1414.27 6 0 -12 6 19619.7 1515.02 12 0 -12 6 19169.0 1293.09 2 0 12 6 18435.7 1599.97 8 0 -12 -6 18312.4 1345.34 5 0 -12 7 786.162 405.137 12 0 12 -7 171.575 205.172 5 0 12 -7 370.428 344.209 11 0 -12 7 453.530 368.611 9 0 -12 7 756.168 341.548 2 0 12 7 926.969 434.224 4 0 12 -7 199.290 307.005 6 0 -12 -7 727.652 423.189 5 0 12 7 173.108 386.413 8 0 12 -8 135443. 4139.01 5 0 12 8 125204. 4663.46 4 0 12 -8 124370. 4676.16 6 0 -12 8 128843. 4655.13 9 0 -12 8 126139. 4598.11 12 0 -12 8 132894. 4265.18 2 0 12 8 134411. 5094.17 10 0 -12 -8 128090. 4697.67 5 0 12 8 126983. 5127.43 8 0 12 -8 131665. 4883.18 11 0 -12 9 933.336 474.486 12 0 -12 -9 1337.41 536.099 5 0 12 9 658.752 482.083 10 0 12 -9 435.642 292.873 5 0 12 -9 1142.83 469.359 6 0 12 -9 119.304 364.827 11 0 12 9 1118.69 501.331 8 0 12 9 1524.39 522.523 4 0 -12 9 1675.33 447.608 2 0 -12 9 754.417 374.956 9 0 -12 10 110148. 3971.16 2 0 12 10 105771. 4489.69 4 0 12 10 111842. 5012.28 8 0 -12 10 118985. 4516.64 9 0 -12 -10 108275. 4634.77 5 0 12 -10 109386. 4419.37 6 0 -12 10 118138. 4516.98 12 0 12 -10 109529. 4779.35 11 0 12 10 114674. 4907.24 10 0 12 11 1198.14 458.099 4 0 12 -11 857.078 526.127 11 0 12 -11 731.608 362.182 6 0 12 11 1329.82 569.849 8 0 12 11 1696.66 623.749 10 0 -12 -11 1246.06 571.663 5 0 -12 11 1770.53 610.741 9 0 -12 11 1246.70 534.509 12 0 12 12 33706.5 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4453.88 689.421 5 -1 -6 10 5734.19 570.520 10 1 6 -10 4772.22 699.514 6 -1 6 10 4879.95 767.586 10 1 6 -9 13577.1 1119.28 6 -1 -6 9 12212.4 1032.71 9 -1 6 9 11654.1 1133.90 10 -1 -6 9 12161.6 803.566 10 1 -6 -9 12253.8 1223.72 5 1 6 -9 11534.9 1177.77 11 -1 6 9 11878.9 1093.28 4 1 -6 -9 11536.9 1165.56 11 1 6 -9 12768.2 1111.59 5 -1 6 9 14077.3 1378.91 8 -1 -6 9 13496.8 1080.98 12 1 6 -8 21649.8 1519.48 11 -1 6 8 23442.8 1716.46 8 -1 -6 8 24556.8 1414.04 9 -1 -6 8 21623.0 1332.33 12 1 -6 -8 23206.7 1578.19 11 1 6 -8 22496.4 1415.41 5 -1 6 8 21862.9 1402.10 4 1 6 -8 23006.4 1420.93 6 1 -6 -8 23851.2 1608.46 5 -1 6 8 25034.0 1570.51 10 -1 -6 8 23732.1 1103.56 10 -1 -6 7 32351.9 1519.92 2 1 6 -7 31038.4 1703.90 11 1 6 -7 33089.7 1169.08 1 1 -6 -7 32306.3 1767.75 5 -1 6 7 30008.8 1669.48 10 -1 -6 7 32879.9 1531.61 12 -1 6 7 31736.4 1923.47 8 -1 -6 7 33463.8 1245.20 10 -1 6 7 33788.9 1618.44 4 -1 -6 7 34009.6 1551.78 9 1 6 -7 33926.1 1648.35 6 1 6 -7 31909.5 1597.48 5 1 6 -6 154151. 4331.46 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425.346 5 -1 6 3 3781.89 468.470 10 1 6 -3 3370.01 353.226 11 -1 6 3 4380.09 600.954 8 -1 6 3 3801.78 224.096 7 1 6 -3 3975.73 486.141 6 -1 -6 3 4459.18 445.196 12 -1 -6 3 4461.34 388.818 11 1 6 -3 4096.57 301.186 8 -1 -6 3 4072.98 452.290 2 1 6 -3 3554.02 338.975 10 1 6 -3 3876.38 425.159 5 -1 -6 2 109006. 3123.42 12 -1 6 2 99546.3 3570.75 8 -1 6 2 110525. 2879.70 4 1 6 -2 108083. 2943.48 10 1 -6 -2 105250. 3491.73 3 -1 6 2 108348. 2738.47 5 -1 -6 2 110283. 3215.14 2 1 6 -2 106933. 3173.29 13 1 -6 -2 110506. 2804.94 5 -1 6 2 107777. 3086.53 10 -1 6 2 109446. 2628.26 7 1 6 -2 104279. 3039.67 5 1 -6 -2 106093. 2885.57 4 1 6 -2 108063. 2754.11 11 -1 -6 2 106585. 3103.66 5 -1 -6 2 105687. 3098.65 9 -1 -6 2 111062. 2767.67 11 1 6 -2 102550. 3279.66 6 1 6 -1 51588.8 2112.74 3 -1 6 1 50656.6 2270.64 8 1 6 -1 48631.4 2126.31 6 -1 6 1 52145.5 1607.95 4 1 6 -1 49625.6 1487.57 8 1 6 -1 52203.8 2029.90 12 -1 6 1 50424.1 1352.09 5 1 -6 -1 50077.7 2466.92 3 1 6 -1 53592.7 2045.23 9 1 -6 -1 50711.6 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5637.55 6 -1 6 -4 225336. 6020.99 11 1 -6 4 229091. 5253.54 2 1 -6 4 223702. 5808.82 9 1 6 4 221364. 5855.23 4 1 6 5 849.221 269.973 4 -1 6 -5 1156.64 218.794 5 1 -6 5 1147.89 219.940 2 1 -6 5 582.568 221.074 12 -1 -6 -5 812.052 104.359 7 -1 -6 -5 789.023 227.215 11 -1 -6 -5 694.897 275.657 5 -1 6 -5 956.655 313.162 11 1 6 5 1154.84 285.296 8 1 -6 5 797.586 261.512 9 -1 6 -5 599.226 190.076 6 -1 -6 -6 204426. 5389.50 11 -1 -6 -6 201543. 5817.44 5 1 6 6 195778. 5522.37 4 -1 -6 -6 201589. 4419.33 7 -1 6 -6 206310. 5299.53 6 1 6 6 203590. 5745.51 8 -1 6 -6 204799. 5814.54 11 -1 6 -6 203376. 5156.74 5 1 -6 6 203436. 5465.24 9 1 -6 6 202480. 5455.56 12 1 -6 6 191935. 4364.35 10 -1 6 -7-97.9393 217.842 11 1 6 7 511.411 293.267 8 -1 -6 -7 246.612 84.3806 7 -1 6 -7 291.452 193.320 5 1 -6 7 129.366 189.767 12 -1 -6 -7 231.934 221.796 11 -1 6 -7-173.307 241.017 6 1 6 7-161.309 261.723 4 -1 -6 -7 312.936 301.672 5 1 -6 7-0.39501 195.970 9 1 -6 7 193.628 85.6702 10 1 -6 8 69379.3 2717.78 12 1 -6 8 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1896.19 575.823 10 1 21 -3 4292.07 924.512 4 1 -21 -3 2932.78 870.575 3 1 21 -3 2148.56 924.742 6 1 -21 -3 2879.04 945.366 13 1 -21 -2 13507.3 1752.34 13 1 21 -2 15432.8 1962.79 6 1 21 -2 11183.8 1398.56 4 -1 -21 2 13104.4 1397.81 2 1 -21 -2 14424.1 1724.14 3 1 -21 -1 17189.4 1905.55 13 -1 -21 1 16800.7 1612.66 2 1 -21 -1 18273.9 1958.79 3 -1 -21 1 15751.1 1684.74 3 1 21 -1 14076.7 1551.02 4 1 21 -1 14247.6 1838.45 6 -1 -21 0 20228.4 1897.01 3 1 21 0 23454.4 1986.65 4 -1 -21 0 22868.6 1891.94 2 -1 21 0 19446.4 2128.13 6 1 -21 0 24111.8 2211.76 3 1 21 0 22408.4 2285.50 6 -1 -21 -1 15926.4 1700.02 3 1 -21 1 14012.7 1711.49 3 -1 -21 -1 17131.6 1658.63 2 -1 21 -1 20169.7 2136.97 6 -1 -21 -1 18430.4 1898.87 13 1 21 1 17328.3 1703.33 4 -1 -21 -2 10909.0 1519.13 13 -1 -21 -2 11248.9 1367.05 2 -1 21 -2 9545.69 1536.35 6 -1 -21 -2 10594.0 1365.38 3 1 21 2 10913.5 1362.31 4 1 21 3 14461.2 1589.20 4 1 -21 3 14399.5 1812.05 9 -1 -21 -3 13864.5 1658.05 3 -1 -21 -3 15885.6 1883.57 13 1 -21 3 17077.3 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13 1 22 5 23790.2 2135.64 4 -1 -22 -5 21549.4 2269.63 3 -1 -22 -6 6712.45 1330.89 3 1 22 6 5862.09 1149.88 4 -1 -22 -7 16689.6 2104.01 3 1 -23 -3 2091.83 843.674 3 1 -23 -2 38998.5 3079.56 13 1 -23 -2 43828.3 3158.73 3 1 -23 -1 7114.87 1283.17 3 -1 23 0 62762.4 4005.42 6 1 -23 0 62872.2 3794.10 3 -1 -23 0 59129.9 3502.99 3 1 -23 1 4336.05 1073.14 3 -1 23 -1 4145.99 1058.45 6 -1 -23 -1 3878.01 946.798 13 -1 -23 -1 4905.67 926.405 2 -1 -23 -1 4418.05 984.522 3 -1 -23 -2 28962.3 2533.97 13 -1 -23 -2 25619.7 2271.47 3 -1 23 -2 28359.1 2676.43 6 -1 -23 -3 1786.21 599.964 13 -1 -23 -3 1676.93 730.059 3 -1 -23 -4 1910.58 668.194 3 -1 -23 -4 3437.53 1021.48 13 -1 -23 -5 2012.22 792.566 3 -1 -24 0 1630.04 663.601 3 -1 -24 -1 1229.67 619.551 3 -1 -24 -2 2587.43 903.847 13 -2 0 15 355.861 291.173 10 -2 0 15 314.892 336.217 8 2 0 -15 459.664 400.641 5 2 0 -15 835.219 564.435 11 -2 0 14 1813.58 538.659 10 2 0 -14 2309.33 750.074 5 -2 0 14 2889.77 697.978 8 2 0 -14 2379.84 781.141 11 -2 0 13 396.869 313.156 10 2 0 -13-206.556 440.090 5 -2 0 13-331.039 431.623 8 2 0 -13 406.749 358.049 11 -2 0 12 1446.69 419.351 10 2 0 -12 2147.33 736.959 11 2 0 -12 934.741 426.735 5 -2 0 12 1730.55 526.817 8 2 0 -11-47.3995 300.964 5 -2 0 11 300.073 316.598 8 -2 0 11 110.906 232.604 10 2 0 -11 161.408 319.405 11 -2 0 10 32748.0 1721.51 10 -2 0 10 31124.7 1847.05 8 2 0 -10 28359.5 1996.97 11 2 0 -10 29269.8 1956.48 5 2 0 -9 821.644 426.715 5 -2 0 9 341.508 272.556 8 -2 0 9 531.903 302.368 10 2 0 -9 1109.75 525.685 11 2 0 -8 137728. 4570.74 5 -2 0 8 144628. 4417.94 8 -2 0 8 142912. 4182.08 10 2 0 -8 139676. 4675.20 11 2 0 -7 315.234 319.493 11 -2 0 7 630.038 341.557 8 2 0 -7 451.365 352.296 5 -2 0 7 1029.44 341.562 10 2 0 -6 156439. 4682.86 11 -2 0 6 159542. 4510.40 8 -2 0 6 163993. 4351.56 10 2 0 -6 159623. 4663.85 5 2 0 -6 160012. 4304.26 6 2 0 -5 1053.98 378.275 5 2 0 -5 1768.60 369.233 11 -2 0 5 1687.45 333.745 10 2 0 -5 1142.57 272.634 6 2 0 -5 1099.70 143.287 1 -2 0 5 1571.38 343.993 8 -2 0 4 31501.4 1276.59 10 2 0 -4 33095.0 1459.24 5 -2 0 4 33785.7 1403.79 8 2 0 -4 31126.6 1444.09 11 2 0 -4 33136.9 956.702 1 2 0 -4 32001.0 1231.72 6 2 0 -3 3047.38 524.979 5 -2 0 3 2594.81 478.262 8 2 0 -3 1728.02 460.272 8 -2 0 3 3161.47 379.187 10 2 0 -3 1357.08 306.889 7 2 0 -2 108487. 2797.71 10 -2 0 2 103995. 2767.99 10 2 0 -2 106606. 2560.62 1 2 0 -2 108145. 2792.04 7 -2 0 2 102813. 2822.20 7 -2 0 2 104484. 2592.18 6 -2 0 2 99046.7 3043.01 8 -2 0 2 109325. 2978.62 5 2 0 -2 104972. 2994.00 5 2 0 -2 106473. 2599.19 6 2 0 -1 1309.08 225.780 13 2 0 -1 451.754 193.011 10 -2 0 1 594.584 220.673 5 -2 0 1 352.648 265.553 9 -2 0 1 338.355 239.671 2 2 0 -1 138.011 79.2628 6 -2 0 1 288.212 248.650 12 -2 0 1 519.263 119.147 6 -2 0 1 314.672 340.126 10 2 0 -1 1318.78 513.494 5 2 0 -1 1338.30 282.921 7 -2 0 0 129527. 3249.11 10 -2 0 0 146567. 3515.53 3 2 0 0 135831. 3247.49 10 2 0 0 128540. 3203.89 9 2 0 0 138024. 3214.04 3 2 0 0 111610. 3750.29 4 -2 0 0 130207. 3004.83 9 -2 0 0 130443. 3237.24 7 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410.639 2 2 -6 0 6457.66 797.658 13 -2 6 0 6521.58 324.503 4 -2 6 0 6603.76 454.044 10 -2 6 0 6701.68 289.975 5 2 6 0 8777.75 812.100 12 2 -6 0 7182.52 990.157 12 2 6 0 7791.43 702.122 3 2 6 0 9967.87 1169.88 4 2 -6 1 279022. 6450.83 1 2 -6 1 263338. 7456.59 3 2 -6 1 255820. 7197.97 9 -2 6 -1 267458. 5916.00 10 -2 -6 -1 279124. 6052.20 8 -2 -6 -1 275875. 6706.42 3 2 6 1 269501. 6026.92 8 -2 6 -1 258727. 5685.88 5 -2 6 -1 265518. 5644.18 5 -2 -6 -1 272293. 7351.74 2 2 -6 1 256540. 7192.17 12 -2 6 -1 247671. 6070.44 2 2 6 1 247223. 7437.96 4 -2 6 -1 255726. 6132.50 4 2 6 1 261112. 6363.84 9 -2 6 -1 261762. 6475.27 7 2 6 1 258734. 6351.26 12 2 -6 2 3971.84 609.699 3 -2 -6 -2 2505.31 481.118 2 2 -6 2 3282.85 510.532 9 2 -6 2 2767.94 434.616 12 -2 6 -2 3328.33 583.042 11 2 6 2 3328.08 366.213 8 2 -6 2 3046.89 201.813 2 -2 -6 -2 3327.77 250.027 11 2 6 2 3410.78 344.540 7 2 6 2 3012.97 526.006 4 2 -6 2 2929.95 360.602 1 -2 6 -2 3139.60 217.335 5 -2 6 -2 3191.51 223.856 10 -2 6 -2 3449.21 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5400.23 8 -3 -6 4 154328. 3537.23 8 -3 -6 4 160203. 3935.80 12 -3 6 4 156945. 4496.64 10 -3 6 4 155992. 4100.01 7 3 6 -4 159301. 3815.61 13 3 6 -4 153987. 4791.34 5 3 6 -4 156894. 4460.93 6 3 6 -4 160191. 4293.96 11 -3 -6 4 162156. 3944.43 9 -3 -6 4 157085. 4641.84 2 -3 -6 3 579.988 222.890 10 -3 -6 3 687.373 270.450 2 3 6 -3 771.486 310.728 5 -3 6 3 795.136 283.321 10 -3 -6 3 765.861 183.931 9 -3 6 3 555.371 391.910 8 3 -6 -3 443.854 308.724 3 -3 6 3 383.792 145.376 7 -3 -6 3 776.298 197.598 12 3 -6 -3 621.689 229.782 5 3 -6 -3 570.574 141.997 4 3 6 -3 775.943 261.920 6 -3 -6 3 673.192 148.578 11 3 -6 -2 278387. 6934.45 5 3 -6 -2 275379. 6868.02 1 3 6 -2 287723. 6206.68 12 3 6 -2 287244. 6207.77 9 3 -6 -2 267228. 7990.47 3 -3 -6 2 265834. 6667.98 9 3 6 -2 271273. 7587.96 5 -3 6 2 273888. 6688.07 7 -3 -6 2 260734. 6653.81 12 3 -6 -2 286886. 6239.01 4 -3 6 2 278285. 6848.91 10 3 6 -2 280339. 7061.25 6 -3 -6 2 289759. 6223.96 11 -3 -6 2 287732. 7413.89 2 3 6 -2 288734. 6565.88 3 3 -6 -2 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1559.93 10 -3 6 -14 15473.6 1596.04 5 -3 6 -14 13189.4 1622.01 7 -3 -6 -14 12505.7 1546.44 11 -3 6 -15 432.197 479.883 5 -3 6 -15 568.590 443.992 7 -3 -7 15 8726.97 1144.99 12 -3 -7 15 10658.2 1260.72 9 -3 -7 15 8061.78 1193.95 2 -3 -7 14 261.673 391.938 2 -3 7 14 448.899 503.888 10 3 7 -14 416.743 423.700 5 -3 -7 14-184.131 435.759 9 3 7 -14 456.488 456.623 6 -3 7 14 1822.94 771.032 8 -3 -7 14-200.803 380.984 12 3 -7 -14 715.644 591.909 5 3 7 -14-154.726 459.977 11 3 7 -13 285.807 353.647 6 3 7 -13-86.2528 346.606 5 -3 -7 13 495.261 380.658 9 3 -7 -13 402.215 505.917 5 -3 7 13 78.4122 415.789 8 -3 7 13 700.679 474.969 10 -3 -7 13-93.9939 295.673 12 3 7 -13 271.829 564.042 11 -3 -7 13 488.568 407.348 2 -3 7 12 1159.46 539.595 10 -3 -7 12 405.511 246.361 9 3 -7 -12 735.888 368.585 5 3 7 -12 829.316 527.259 11 -3 7 12 936.967 672.312 8 -3 -7 12 1763.69 490.679 12 -3 -7 12 1523.70 526.435 2 3 7 -12 1004.64 532.382 5 3 7 -12 1707.96 591.371 6 -3 -7 11 10984.9 969.832 10 -3 7 11 13764.6 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433.168 11 -3 -7 7 180537. 4976.33 10 -3 -7 7 179485. 5396.48 2 3 7 -7 180101. 5595.21 5 3 -7 -7 185245. 5619.18 5 -3 -7 7 184855. 4912.21 9 -3 7 7 164480. 6183.78 8 -3 7 7 179682. 5533.61 10 -3 -7 7 190305. 4936.69 12 3 7 -7 182100. 5473.29 11 3 7 -7 183868. 5427.79 6 -3 -7 6 1083.51 293.969 10 3 7 -6 1306.51 402.507 6 -3 7 6 1522.97 447.900 10 3 7 -6 1842.92 451.296 5 3 -7 -6 1341.12 354.361 5 -3 -7 6 1460.92 311.122 9 3 7 -6 1300.07 265.957 8 3 7 -6 1360.87 346.638 11 -3 7 6 1717.66 655.946 8 -3 -7 6 1809.12 324.996 12 -3 -7 6 1641.88 405.757 2 3 -7 -6 1449.49 205.442 7 -3 -7 5 162081. 4796.44 2 -3 7 5 152574. 4697.67 10 3 7 -5 157907. 4920.38 5 3 -7 -5 155137. 4635.93 5 3 7 -5 164978. 4527.48 11 3 7 -5 155762. 3954.39 8 3 7 -5 164937. 4032.37 13 -3 7 5 150157. 4167.77 7 -3 -7 5 160296. 4152.25 9 -3 -7 5 159405. 4146.57 12 -3 -7 5 159488. 4384.51 10 -3 7 5 142664. 5573.79 8 3 7 -5 158846. 4680.02 6 3 7 -4 547.315 171.915 13 -3 -7 4 281.828 186.333 10 -3 7 4 386.385 204.624 10 -3 -7 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12 3 10 -1 115188. 4528.64 6 -3 10 0 1775.44 310.677 10 -3 -10 0 1783.73 359.409 3 3 -10 0 1949.08 660.121 9 3 -10 0 1694.61 633.079 3 -3 -10 0 2339.26 527.951 2 -3 10 0 1717.16 288.777 2 3 10 0 1777.63 208.883 8 3 -10 0 1347.72 518.188 13 -3 10 0 1563.26 351.766 7 3 -10 0 3644.27 809.979 12 3 10 0 2454.69 677.615 4 -3 10 0 2191.67 209.671 4 3 -10 1 83024.3 3983.31 3 -3 10 -1 73308.8 2312.31 10 3 10 1 85296.6 3948.75 4 -3 10 -1 82906.8 2612.41 2 -3 -10 -1 82078.7 3051.04 3 3 -10 1 69426.6 3625.05 9 -3 -10 -1 73019.3 2320.54 8 3 10 1 75003.3 2232.69 8 -3 10 -1 74499.5 2869.28 7 -3 10 -1 74340.3 2014.20 4 3 -10 1 67030.4 3594.28 12 -3 -10 -1 77281.7 3516.36 2 -3 10 -2 32219.6 1025.08 2 3 -10 2 30467.1 2228.84 3 -3 10 -2 39987.9 1421.30 4 3 -10 2 32397.1 2245.14 9 -3 10 -2 33867.7 1230.43 10 -3 10 -2 32467.1 1838.05 7 -3 -10 -2 36657.9 2300.21 2 3 10 2 34918.2 2391.48 4 3 10 2 33026.4 1414.58 8 -3 10 -2 32903.0 2276.41 11 -3 10 -2 32576.4 2058.82 6 3 -10 2 33158.5 2266.44 12 -3 -10 -2 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2200.28 8 -4 -4 9 54522.9 2156.35 12 4 4 -9 53956.7 2844.17 11 4 4 -9 52785.9 2434.06 6 -4 -4 8 4291.87 601.804 10 -4 4 8 4552.95 696.353 10 4 4 -8 4168.84 369.613 1 4 4 -8 3996.15 700.437 5 4 -4 -8 3190.97 678.629 5 -4 4 8 3455.39 725.491 8 -4 -4 8 3137.22 456.235 8 4 4 -8 3161.12 622.425 11 4 4 -8 3931.50 629.173 6 -4 -4 8 2928.03 572.524 2 -4 -4 7 64164.2 2483.04 10 -4 4 7 60432.8 2603.46 10 -4 -4 7 65042.3 2675.25 2 4 4 -7 60781.5 2860.74 5 4 -4 -7 59120.5 2789.88 5 -4 4 7 61110.3 3076.34 8 -4 -4 7 63831.9 2220.93 8 4 4 -7 62915.5 2485.89 6 4 4 -6 3366.18 495.036 6 -4 -4 6 2826.70 461.068 10 -4 4 6 3379.66 529.847 10 4 4 -6 2688.11 553.215 5 -4 -4 6 3240.66 372.143 9 4 -4 -6 3362.62 596.057 5 4 -4 -6 3939.39 458.858 1 -4 4 6 1958.09 555.727 8 -4 -4 6 3026.87 375.726 8 -4 -4 6 2989.21 356.784 12 -4 -4 6 3275.54 553.164 2 -4 -4 5 46053.6 2100.11 2 -4 -4 5 46962.7 1501.75 12 -4 4 5 44640.0 2021.43 10 4 4 -5 44594.8 2311.38 5 4 -4 -5 44323.5 2183.27 5 -4 -4 5 47978.1 1513.09 9 4 -4 -5 48515.2 1796.18 1 -4 4 5 44528.0 2615.19 8 -4 -4 5 47802.4 1661.35 8 -4 -4 5 46690.4 1977.19 10 -4 4 5 44050.4 1951.18 7 4 4 -5 47536.9 1903.59 6 -4 -4 4 2010.19 370.231 10 4 4 -4 2478.54 550.422 5 -4 4 4 1635.67 356.201 10 4 -4 -4 2489.53 510.884 5 -4 -4 4 1739.25 200.538 9 -4 4 4 1461.85 536.566 8 -4 -4 4 2033.17 274.866 8 4 -4 -4 2584.07 367.789 1 -4 4 4 1477.98 311.284 7 -4 -4 4 1603.17 193.663 12 -4 -4 4 1779.85 387.411 2 4 4 -4 1920.65 326.259 6 4 4 -3 13326.9 1202.14 5 -4 4 3 11880.8 884.201 10 4 -4 -3 13900.2 1112.73 5 -4 -4 3 13181.5 946.470 10 -4 -4 3 12987.0 473.549 9 4 -4 -3 13062.6 1091.77 3 -4 4 3 11239.7 1385.49 8 -4 -4 3 13090.7 728.500 8 4 -4 -3 13905.9 848.057 1 -4 -4 3 13141.6 476.087 12 -4 4 3 11892.5 846.638 7 4 4 -3 12471.0 803.439 6 4 -4 -3 11481.2 1184.71 13 -4 -4 3 12998.0 1013.04 2 4 -4 -2 5053.66 504.832 1 4 4 -2 5622.45 840.226 5 -4 -4 2 5082.87 593.849 10 -4 4 2 5127.09 557.150 10 4 -4 -2 5437.78 718.289 5 4 -4 -2 4837.80 781.180 3 4 -4 -2 5523.67 342.369 4 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2969.26 10 -4 -6 9 63876.2 2942.24 2 4 6 -9 64037.5 3165.37 5 -4 -6 9 70111.0 2551.30 12 4 -6 -9 69074.3 3318.72 5 -4 -6 9 68043.6 2526.77 9 -4 6 9 65629.4 3548.38 8 -4 -6 9 68618.0 2387.26 8 4 6 -9 63379.3 3146.71 11 4 6 -9 67312.4 2919.77 6 -4 -6 8 2085.59 439.991 10 -4 6 8 1688.33 461.993 10 4 6 -8 3237.87 649.406 5 4 -6 -8 2332.81 563.275 5 -4 -6 8 1893.24 337.814 9 -4 -6 8 1909.22 457.694 2 -4 6 8 2296.25 733.953 8 -4 -6 8 2102.52 342.575 8 -4 -6 8 2103.39 370.045 12 4 6 -8 2055.91 486.108 11 4 6 -8 1947.98 448.611 6 -4 -6 7 186231. 5273.27 10 -4 6 7 177022. 5584.37 10 -4 -6 7 188221. 5647.07 2 4 6 -7 181154. 5892.14 5 -4 -6 7 190141. 4855.88 9 4 -6 -7 183759. 5810.24 5 -4 6 7 171110. 6426.84 8 -4 -6 7 186901. 4667.14 8 -4 -6 7 192349. 4867.01 12 4 6 -7 182126. 5688.16 11 4 6 -7 186088. 5450.39 6 -4 -6 6 1012.34 273.876 10 -4 -6 6 814.112 209.665 12 -4 6 6 195.926 239.319 10 4 6 -6 1094.03 395.168 5 4 -6 -6 1117.62 378.784 5 -4 -6 6 873.631 225.516 9 -4 6 6-74.2591 478.913 8 -4 -6 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829.541 3 -4 -6 0 5186.72 371.572 8 -4 -6 0 4777.70 771.639 2 -4 6 0 5369.22 592.091 7 4 6 0 5227.64 408.097 12 4 -6 0 5431.97 575.510 1 -4 -6 0 5228.25 615.834 7 4 -6 0 5687.94 952.769 12 -4 -6 0 5216.97 335.547 11 -4 6 -1 186069. 4589.45 10 4 -6 1 172231. 5609.85 3 -4 -6 -1 180650. 4033.84 11 -4 -6 -1 160734. 3981.55 3 4 -6 1 172564. 5818.50 9 4 -6 1 176389. 4768.31 1 -4 6 -1 174398. 4923.26 7 -4 -6 -1 180414. 4838.03 7 4 6 1 164839. 6113.40 4 -4 -6 -1 180251. 6019.00 2 4 -6 1 168578. 5787.09 12 4 -6 2 15815.7 1251.36 3 -4 -6 -2 16741.2 723.403 11 -4 6 -2 15752.4 771.429 6 4 -6 2 15448.6 1266.68 9 4 6 2 15308.9 1420.21 4 -4 -6 -2 17612.2 784.585 3 4 -6 2 15273.7 1002.12 1 -4 6 -2 14671.8 1083.90 7 -4 -6 -2 15728.2 1007.77 7 -4 -6 -2 17329.0 1595.35 2 4 -6 2 15180.3 1270.20 12 -4 6 -2 15583.1 893.680 10 4 -6 3 207825. 4873.52 10 -4 6 -3 190159. 6726.98 11 4 -6 3 208544. 6083.61 9 4 -6 3 201061. 5476.19 1 -4 6 -3 212891. 4897.12 6 -4 6 -3 208306. 5892.63 7 -4 -6 -3 193608. 6595.11 2 -4 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65694.1 3351.36 11 4 7 -10 67446.6 3086.30 6 -4 -7 9 52.0756 196.870 10 -4 7 9 42.9760 295.024 10 4 7 -9 105.853 319.581 5 4 -7 -9 407.141 415.422 5 -4 -7 9 155.835 213.828 9 -4 7 9 62.9349 416.476 8 4 7 -9 1064.90 518.921 11 -4 -7 9 385.010 224.087 12 -4 -7 9 479.237 284.928 2 4 7 -9-393.239 386.510 6 -4 -7 8 21835.6 1590.22 2 -4 7 8 23839.9 1676.84 10 4 7 -8 22869.9 1722.45 5 4 -7 -8 22459.2 1709.69 5 -4 -7 8 24348.0 1290.36 9 -4 7 8 21045.4 1975.25 8 -4 -7 8 23188.5 1098.33 8 -4 -7 8 22911.5 1417.57 10 4 7 -8 22460.1 1645.71 11 4 7 -8 22935.1 1558.88 6 -4 -7 8 22218.2 1239.98 12 -4 -7 7 1.60325 185.623 10 -4 7 7 202.343 295.410 10 4 7 -7 20.2567 339.846 5 4 -7 -7 289.728 306.733 5 -4 -7 7 228.799 143.156 9 -4 7 7 246.773 599.802 8 -4 -7 7 240.603 126.148 8 -4 -7 7 530.155 200.413 12 -4 -7 7-27.9350 274.758 2 4 7 -7 315.326 308.342 11 4 7 -7 426.076 286.554 6 -4 -7 6 15875.8 1103.51 10 4 7 -6 16710.4 1435.89 5 -4 7 6 15209.0 1245.73 10 4 -7 -6 16774.1 1306.37 5 -4 -7 6 17705.6 938.020 9 -4 -7 6 17324.6 734.906 8 -4 7 6 14158.9 1611.70 8 -4 7 6 16346.1 1124.89 7 -4 -7 6 17716.0 937.153 12 4 7 -6 15839.6 1205.57 11 4 7 -6 15253.4 1172.33 6 -4 -7 6 16911.6 1303.57 2 -4 -7 5 2347.93 448.068 10 4 7 -5 2058.90 532.212 5 -4 7 5 1913.33 479.682 10 4 -7 -5 2091.16 481.349 5 -4 -7 5 2724.97 328.428 9 -4 -7 5 2805.77 218.221 8 -4 -7 5 2197.32 294.934 12 -4 7 5 2000.88 652.021 8 4 7 -5 2376.47 453.254 6 -4 7 5 2719.67 455.887 7 -4 -7 5 1957.29 442.448 2 4 7 -4 128923. 4685.43 5 -4 7 4 131710. 4189.42 10 4 -7 -4 132142. 4291.96 5 -4 -7 4 141102. 3559.27 9 4 -7 -4 130206. 4820.43 3 -4 7 4 138568. 5636.46 8 -4 -7 4 135348. 4495.02 2 4 7 -4 136360. 4189.71 6 -4 7 4 139777. 3983.01 7 4 -7 -4 131971. 5386.61 13 -4 -7 4 138511. 3547.60 12 -4 -7 4 132174. 4100.33 10 4 7 -3 5622.22 851.099 5 4 7 -3 5890.23 494.150 3 -4 7 3 5737.77 642.389 10 4 -7 -3 6596.71 728.648 5 -4 -7 3 5639.95 493.415 9 4 -7 -3 6045.07 644.805 1 -4 7 3 7068.53 1124.95 8 4 -7 -3 5621.54 886.943 3 4 -7 -3 6130.43 413.514 4 -4 -7 3 5805.29 495.202 12 -4 -7 3 6399.41 803.615 2 4 -7 -3 5704.77 952.805 13 -4 7 3 5826.92 595.104 7 4 7 -3 5239.96 639.383 6 -4 -7 3 5716.76 421.141 11 -4 -7 3 5662.21 638.205 10 4 -7 -2 222349. 6213.60 5 -4 7 2 221559. 5858.80 10 4 7 -2 225601. 6067.86 6 4 -7 -2 217483. 5882.77 1 4 7 -2 222979. 5618.96 3 -4 7 2 223565. 5816.40 7 4 -7 -2 228491. 5014.25 4 4 -7 -2 200025. 6939.02 13 -4 -7 2 217613. 6535.21 2 -4 -7 2 229297. 5052.61 11 4 -7 -2 194157. 7228.21 3 4 -7 -1 10142.3 945.521 5 4 -7 -1 8903.49 777.598 1 4 7 -1 8535.27 359.899 9 4 -7 -1 10137.4 1337.46 9 4 -7 -1 9646.36 1331.83 12 4 -7 -1 12225.3 1480.54 3 -4 -7 1 8340.68 379.973 8 4 7 -1 10683.2 1388.69 4 -4 7 1 8515.40 747.951 7 -4 -7 1 10130.2 713.120 13 4 -7 -1 8263.03 1038.55 13 4 7 -1 8014.69 351.910 12 4 7 -1 9009.40 836.800 6 -4 -7 1 9579.45 1047.02 2 -4 -7 1 8851.87 368.531 11 -4 7 1 8655.20 717.442 10 -4 7 0 187446. 4801.68 10 4 -7 0 203083. 6838.23 9 4 -7 0 201550. 6695.05 3 4 -7 0 179189. 4983.72 1 4 7 0 214382. 4705.11 9 -4 -7 0 183889. 4253.40 8 -4 7 0 190384. 4179.92 2 -4 7 0 186555. 5097.09 7 4 7 0 223706. 7285.87 4 4 7 0 215012. 4706.58 12 -4 -7 0 175900. 5938.43 2 4 -7 0 204688. 6860.62 12 4 7 0 180145. 5321.20 6 -4 7 0 193357. 4520.96 5 -4 -7 0 176233. 3928.60 11 -4 7 -1 709.178 204.557 10 -4 7 -1 639.971 153.807 5 4 -7 1 247.588 316.531 3 4 -7 1 443.813 332.259 9 4 7 1 668.273 188.818 9 -4 -7 -1 487.767 145.763 3 -4 -7 -1 555.155 316.906 2 -4 7 -1 822.554 297.199 7 4 -7 1-25.1893 220.994 1 -4 -7 -1 297.219 204.841 7 4 7 1 887.410 207.092 12 -4 -7 -1 573.248 88.7116 11 4 -7 1 371.278 352.040 12 4 7 1 1082.96 500.940 4 -4 7 -2 39485.1 1531.61 10 -4 7 -2 40560.7 1610.75 5 4 -7 2 40172.6 2207.66 3 -4 -7 -2 40672.2 1538.40 3 4 -7 2 36738.4 2190.09 9 4 -7 2 38842.0 1763.43 1 -4 7 -2 38518.9 1899.04 7 -4 -7 -2 38403.1 1695.47 7 4 7 2 34519.7 2333.10 4 -4 -7 -2 41042.4 2547.44 2 4 -7 2 35173.5 2153.73 12 -4 7 -2 38541.5 1531.65 6 -4 -7 -2 40339.8 1208.54 11 4 -7 3 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1801.60 664.690 6 -4 10 13 537.149 658.606 8 -4 -10 13 1150.10 531.971 2 4 10 -13 2189.53 635.702 11 -4 10 12-10.6932 446.691 10 4 10 -12-6.70765 457.432 5 4 -10 -12 504.811 430.646 5 -4 10 12 221.360 549.821 8 -4 -10 12 201.298 356.582 2 4 10 -12-367.439 545.850 11 4 10 -12 260.357 445.866 6 -4 10 11 2856.14 718.978 10 4 10 -11 2871.40 707.654 5 4 -10 -11 3232.14 763.212 5 -4 10 11 5112.49 1210.96 8 -4 -10 11 3321.63 714.051 2 4 10 -11 3384.01 845.723 11 4 10 -11 2780.16 660.497 6 4 10 -10 30418.1 2221.20 5 -4 10 10 29152.0 2215.42 10 4 -10 -10 34651.6 2381.10 5 -4 -10 10 32104.4 1813.47 9 -4 10 10 29958.4 2747.90 8 4 10 -10 32127.2 2199.15 6 -4 -10 10 33427.5 1848.31 12 4 10 -10 35641.9 2377.06 11 -4 -10 10 32214.4 2165.21 2 -4 -10 9 638.696 296.876 10 4 10 -9 847.419 396.940 5 4 -10 -9 1081.09 501.240 5 -4 -10 9 524.426 233.284 9 -4 10 9 328.229 534.912 8 -4 10 9 487.751 344.303 10 -4 -10 9 697.479 403.327 2 4 10 -9 907.347 371.974 11 -4 -10 9 635.600 210.609 12 4 10 -9 1490.12 499.847 6 4 10 -8 90259.4 3934.37 5 -4 10 8 97261.7 4044.36 10 4 -10 -8 93204.6 3866.21 5 -4 -10 8 98368.8 3293.13 9 -4 10 8 88215.1 4754.66 8 -4 -10 8 95382.1 3260.46 12 4 10 -8 96474.2 3797.16 11 4 10 -8 91356.6 3804.30 6 -4 -10 8 92363.4 3853.32 2 -4 -10 8 97503.0 3397.34 10 4 10 -7 12753.4 1306.44 5 -4 10 7 12398.5 1258.01 10 4 -10 -7 14525.2 1289.03 5 -4 -10 7 14241.8 1022.08 9 -4 10 7 12316.3 1631.68 8 -4 -10 7 13962.7 1010.62 12 4 10 -7 14536.6 1303.30 6 4 10 -7 13468.8 1178.25 11 -4 -10 7 12565.7 1250.94 2 -4 -10 7 11913.7 1010.62 10 4 10 -6 130754. 4814.70 5 -4 10 6 129736. 4622.76 10 4 -10 -6 130788. 4412.58 5 -4 -10 6 132460. 3976.13 9 4 -10 -6 127943. 5182.93 3 -4 10 6 129932. 5757.91 8 -4 -10 6 135157. 3999.40 12 -4 10 6 124029. 3974.37 7 4 10 -6 127391. 4548.75 6 4 10 -6 135394. 4224.93 11 -4 -10 6 128313. 4667.85 2 4 10 -5 6532.48 917.328 5 -4 10 5 6433.58 826.766 10 4 -10 -5 6920.01 790.225 5 -4 -10 5 6582.96 674.390 9 -4 10 5 7896.15 1261.41 8 4 -10 -5 6294.60 1052.10 3 -4 -10 5 8313.49 1018.60 2 4 -10 -5 6270.50 1167.62 13 -4 10 5 6267.47 679.552 7 -4 -10 5 6683.36 685.839 12 4 10 -5 6093.95 818.690 6 4 10 -4 52950.9 2780.79 5 -4 10 4 52965.7 2470.02 10 4 -10 -4 61122.7 2437.21 5 4 -10 -4 52276.4 3191.10 3 -4 -10 4 48816.1 2160.85 9 -4 10 4 59917.2 3559.98 8 -4 10 4 58806.0 2235.09 7 4 -10 -4 54972.8 3426.98 13 -4 -10 4 51838.7 2220.26 12 4 10 -4 53724.4 2603.24 6 -4 -10 4 54777.5 2774.45 2 -4 10 3 5640.62 727.316 10 4 -10 -3 5682.08 646.917 5 -4 -10 3 6756.78 682.040 9 4 -10 -3 3798.10 842.206 3 -4 10 3 5685.56 1075.55 8 -4 -10 3 5849.45 658.885 12 -4 -10 3 5801.02 880.293 2 -4 10 3 5534.72 615.366 7 4 -10 -3 6707.81 1125.71 13 4 10 -3 6444.09 847.201 6 4 10 -2 4410.91 402.906 12 4 -10 -2 3428.75 375.056 4 4 10 -2 4543.48 921.343 4 4 -10 -2 4669.73 564.251 5 -4 10 2 3929.43 582.005 10 4 10 -2 4445.53 403.481 9 4 -10 -2 4254.07 920.323 3 -4 -10 2 4103.08 705.587 2 4 -10 -2 5624.96 1045.82 13 4 10 -2 3947.51 700.273 6 -4 10 2 3418.76 497.651 7 -4 10 1 26297.2 1410.34 10 4 10 -1 24216.1 1744.16 6 4 -10 -1 29961.2 2439.43 3 4 10 -1 24214.5 1158.01 9 4 10 -1 24735.0 1165.31 12 4 -10 -1 28826.9 2391.98 9 -4 10 1 26747.5 947.236 5 -4 -10 1 32436.2 1665.48 13 -4 10 1 24136.8 1446.90 7 4 -10 -1 21274.5 1911.87 13 4 10 -1 26081.5 2246.10 4 -4 -10 1 25085.6 1908.59 2 4 -10 -1 28123.9 2358.57 12 -4 -10 0 15043.8 1491.89 2 4 -10 0 17863.8 1807.04 9 -4 10 0 15217.3 581.440 5 -4 -10 0 14413.4 676.426 8 -4 10 0 15688.1 1177.54 7 4 -10 0 15936.1 1716.81 3 -4 10 0 14947.4 809.615 2 -4 10 0 13828.4 944.569 10 4 10 0 18375.3 1846.57 4 4 -10 0 18430.1 1834.12 12 4 10 0 13966.4 1339.81 6 -4 10 -1 26014.7 1273.10 10 4 -10 1 29034.6 2248.82 3 -4 -10 -1 30529.7 1426.06 3 -4 10 -1 26569.1 782.051 5 4 -10 1 29653.5 2309.79 9 -4 10 -1 27280.9 801.755 5 -4 10 -1 27238.6 1648.70 7 -4 -10 -1 28037.7 2109.09 2 4 10 1 31909.2 2405.95 4 4 -10 1 29394.6 2274.36 12 -4 10 -2 72302.4 2328.17 10 4 -10 2 68393.6 3578.31 3 -4 -10 -2 78939.8 2882.87 3 4 -10 2 70019.9 3619.83 9 -4 10 -2 74231.9 1795.53 5 4 10 2 72097.9 3800.86 4 -4 10 -2 69123.1 2981.47 7 -4 -10 -2 71532.4 3630.16 2 4 -10 2 68366.8 3601.47 12 -4 10 -2 65717.2 2992.16 6 -4 10 -2 79070.1 4036.41 11 -4 -10 -3 21161.1 1373.30 3 4 -10 3 21210.2 1791.39 9 -4 10 -3 21482.3 1366.46 6 -4 10 -3 23571.5 797.408 5 -4 10 -3 21834.8 1577.55 7 -4 -10 -3 25353.4 2050.99 2 4 -10 3 18579.2 1708.66 12 4 10 3 20780.8 1909.44 4 -4 10 -3 18960.3 835.853 4 -4 10 -3 21183.6 1990.50 11 -4 10 -3 21244.9 1009.89 10 4 -10 4 121684. 4833.46 9 -4 -10 -4 132147. 4087.13 3 -4 10 -4 125540. 3899.21 6 -4 10 -4 134852. 3236.96 5 4 10 4 128524. 4026.19 8 -4 10 -4 125991. 4596.33 7 -4 -10 -4 117144. 5055.02 2 4 10 4 123401. 5139.01 4 -4 -10 -4 126379. 3273.95 11 -4 10 -4 119607. 5216.20 11 4 -10 4 120809. 4814.48 12 4 -10 5 16792.6 1529.00 9 -4 10 -5 16892.5 843.459 5 4 10 5 14931.5 1194.15 8 -4 10 -5 15732.0 1469.52 7 -4 -10 -5 15128.8 1584.59 2 4 10 5 16565.9 1625.18 4 -4 10 -5 17664.6 1099.00 6 -4 -10 -5 15922.1 892.476 11 -4 10 -5 14411.2 1624.51 11 4 -10 5 14490.4 1425.08 12 4 -10 6 45530.9 2621.29 12 4 -10 6 44786.9 2607.16 9 -4 10 -6 45849.1 2960.60 11 4 10 6 48962.5 2396.69 8 -4 -10 -6 48133.1 2856.81 5 -4 -10 -6 42382.7 2757.78 2 -4 10 -6 47666.3 2713.59 7 4 10 6 46542.1 2833.76 4 -4 10 -6 49340.2 2027.05 6 -4 -10 -6 49503.2 1909.62 11 -4 10 -7 2557.19 468.892 6 4 -10 7 2553.85 696.142 9 -4 -10 -7 2080.41 622.642 5 4 10 7 2516.80 569.454 8 -4 10 -7 2525.56 684.208 7 4 -10 7 3057.35 720.268 12 4 10 7 2443.33 616.570 4 -4 -10 -7 2773.68 455.655 11 -4 10 -7 1486.13 635.036 11 4 -10 8 1122.69 553.709 9 -4 -10 -8 1408.42 699.614 5 4 10 8 436.171 301.142 8 -4 10 -8 408.358 426.799 7 4 -10 8 539.226 482.365 12 4 10 8 613.903 507.400 4 -4 -10 -8 630.736 341.654 11 -4 10 -8 165.302 428.555 11 -4 10 -8 385.342 184.143 6 4 -10 9 5377.29 949.905 9 -4 -10 -9 5987.67 1160.58 5 4 10 9 6092.13 928.828 8 -4 10 -9 6756.15 1142.68 7 4 -10 9 4805.06 888.234 12 4 10 9 5543.31 1023.75 4 -4 10 -9 6876.22 1210.71 11 4 -10 10 23120.0 1981.17 9 -4 -10 -10 24351.7 2301.16 5 4 10 10 23289.4 1968.24 8 -4 10 -10 25900.5 2275.04 7 4 10 10 23611.6 2076.82 4 4 -10 10 24950.6 2037.30 12 -4 10 -10 22733.0 2270.47 11 4 -10 11 5731.60 1017.54 9 -4 -10 -11 6091.42 1160.36 5 -4 10 -11 7213.78 1252.11 7 4 -10 11 7668.91 1185.37 12 4 10 11 5060.16 918.838 4 -4 10 -11 6312.74 1288.02 11 4 -10 12 31511.8 2443.82 9 4 -10 12 31176.1 2431.57 12 -4 -10 -12 28146.2 2683.39 5 4 10 12 30051.3 2463.61 4 -4 10 -12 29535.0 2585.27 7 -4 10 -12 23515.1 2489.45 11 4 11 -13 27387.3 2385.61 5 4 -11 -13 34487.5 2749.52 5 -4 -11 13 28512.1 2283.09 2 -4 11 12 437.026 575.730 10 4 11 -12 115.287 431.618 5 4 -11 -12 1361.48 615.314 5 -4 11 12 335.934 558.213 8 -4 -11 12 98.3446 366.639 2 4 11 -12 542.127 458.494 11 4 11 -12 1262.82 551.239 6 -4 11 11 43585.5 2897.51 10 4 -11 -11 47705.8 3015.60 5 -4 11 11 43879.7 3486.28 8 4 11 -11 49479.4 3027.39 11 4 11 -11 47572.1 2873.98 6 4 11 -11 46770.5 2918.77 5 -4 -11 11 48844.9 2856.50 2 4 11 -10 3676.90 766.268 5 -4 11 10 2762.44 689.880 10 4 -11 -10 3535.91 784.292 5 -4 11 10 4195.21 1053.89 8 -4 -11 10 2815.28 669.293 2 4 11 -10 3034.89 715.991 11 4 11 -10 4338.86 795.893 6 4 11 -9 28053.8 2069.04 5 -4 11 9 23806.0 1957.28 10 4 -11 -9 27469.3 2016.06 5 -4 -11 9 27775.8 1640.10 9 -4 11 9 19985.8 2276.68 8 -4 -11 9 28753.8 1670.00 12 4 11 -9 28031.7 1963.85 11 4 11 -9 27469.0 2017.68 6 -4 -11 9 24184.2 1883.20 2 -4 -11 9 27992.1 1646.27 10 4 11 -8 7965.77 1083.25 5 -4 11 8 8836.97 1168.30 10 4 -11 -8 7210.96 955.057 5 -4 -11 8 7068.70 801.886 9 -4 11 8 7294.59 1351.95 8 4 11 -8 7990.09 1071.07 6 -4 -11 8 8807.23 1093.71 2 -4 -11 8 8317.97 869.397 12 4 11 -8 8480.61 1015.94 11 -4 -11 8 7573.92 823.324 10 4 11 -7 698.769 361.155 5 -4 11 7 303.273 328.903 10 4 -11 -7 509.674 290.492 5 -4 -11 7 765.629 323.467 9 -4 -11 7 974.713 304.917 12 -4 11 7 1028.51 528.045 8 4 -11 -7 1019.31 623.102 3 -4 -11 7 640.831 407.831 2 4 11 -7 569.326 296.390 11 4 11 -7 170.662 329.007 6 4 11 -6 462.491 357.777 5 -4 11 6-79.7767 296.947 10 4 -11 -6 556.660 325.328 5 -4 -11 6-54.9586 224.613 9 -4 11 6 765.833 628.315 8 4 -11 -6 1221.77 642.645 3 -4 -11 6 157.395 300.246 2 -4 -11 6 135.927 198.857 12 4 11 -6 617.104 202.809 11 4 11 -6 534.342 390.143 6 4 11 -5 68330.2 3282.73 5 -4 11 5 72133.6 3123.41 10 -4 -11 5 70981.1 2802.76 9 4 -11 -5 70682.7 3850.34 3 -4 11 5 78421.6 4210.85 8 4 -11 -5 74731.6 2906.40 5 -4 11 5 73526.7 2674.58 7 -4 -11 5 67962.4 2763.37 12 4 11 -5 68029.6 3159.77 6 -4 -11 5 74347.5 3369.31 2 4 -11 -5 72353.4 4090.90 13 4 11 -4 4807.10 828.584 5 -4 11 4 6280.33 822.300 10 4 -11 -4 6571.24 718.368 5 -4 -11 4 5386.71 666.038 9 -4 11 4 4590.91 1027.68 8 4 -11 -4 4194.45 963.313 3 -4 -11 4 4875.36 801.894 2 4 -11 -4 6260.23 1128.36 13 -4 11 4 5436.50 622.307 7 -4 -11 4 5449.50 658.148 12 4 11 -4 6843.13 949.673 6 -4 11 3 109066. 3822.51 10 4 -11 -3 118334. 3626.51 5 4 -11 -3 90477.0 4773.87 3 -4 -11 3 122536. 3727.63 9 -4 11 3 119549. 5205.83 8 -4 11 3 106652. 3528.14 7 4 -11 -3 118325. 5196.17 13 -4 -11 3 119125. 3707.28 12 4 11 -3 97970.6 4832.60 4 4 11 -3 101154. 4171.47 6 -4 -11 3 101089. 4300.02 2 4 -11 -2 7227.31 650.201 5 4 11 -2 8315.39 1258.51 4 -4 11 2 7077.51 773.593 10 -4 11 2 6666.41 1068.67 8 4 -11 -2 5835.63 1146.97 3 -4 -11 2 5632.50 937.086 2 -4 11 2 6385.48 709.145 7 4 -11 -2 7135.29 1170.75 13 4 11 -2 6064.17 887.561 6 -4 11 1 89568.0 3167.04 10 4 -11 -1 100169. 4754.66 3 4 -11 -1 98817.0 4769.81 9 -4 11 1 89878.6 3319.41 7 4 -11 -1 88615.9 4301.62 13 -4 -11 1 112060. 3653.88 13 -4 -11 1 90603.0 4060.72 2 4 -11 -1 106883. 4922.85 12 4 11 -1 92280.5 3963.90 6 4 11 -1 103257. 4777.57 4 -4 -11 0 2191.72 374.061 3 -4 11 0 1535.86 330.913 10 4 -11 0 2307.20 704.723 9 4 -11 0 1399.34 582.649 3 -4 -11 0 980.798 489.001 2 4 11 0 1916.57 658.176 4 -4 11 0 1617.06 419.085 7 4 -11 0 2510.74 800.889 12 4 11 0 1613.71 467.612 6 -4 11 -1 37386.9 1620.66 10 4 11 1 47306.6 3001.94 4 4 -11 1 42065.8 2845.94 3 -4 -11 -1 40484.6 1821.50 3 4 -11 1 40785.4 2794.47 9 -4 11 -1 37797.8 2062.90 7 -4 -11 -1 39401.2 2561.91 2 4 -11 1 37992.3 2699.75 12 -4 11 -2 885.472 227.571 10 4 -11 2 1313.41 537.480 3 -4 -11 -2-332.198 367.957 2 4 -11 2 483.427 384.850 9 -4 -11 -2 919.785 307.560 3 -4 11 -2 87.2205 258.780 7 4 -11 2 110.127 342.568 12 -4 11 -2 287.377 272.234 6 -4 11 -2 819.603 487.751 11 4 11 2 1052.03 592.613 4 -4 -11 -3 1331.30 582.623 2 4 -11 3 1353.29 480.309 9 -4 -11 -3 2356.14 488.409 3 4 11 3 1978.41 368.690 8 -4 11 -3 2413.05 579.708 7 -4 11 -3 2392.63 520.638 6 4 -11 3 1034.62 338.947 12 4 11 3 2680.36 786.309 4 -4 11 -3 1170.89 561.402 11 -4 -11 -4 717.924 572.710 2 4 -11 4-270.123 582.076 9 -4 -11 -4 266.210 198.075 3 4 11 4 154.155 203.085 8 -4 11 -4 464.272 433.379 7 -4 11 -4 682.086 487.144 11 4 -11 4-57.3058 455.246 12 4 11 4 861.923 523.697 4 -4 11 -4 745.198 316.367 6 4 -11 5 63432.6 3297.33 9 -4 -11 -5 69863.0 2770.30 3 4 11 5 62774.6 2683.83 8 -4 11 -5 62546.1 3158.19 7 -4 -11 -5 62560.7 3511.44 2 4 -11 5 58442.7 3189.20 12 4 11 5 60901.6 3461.64 4 -4 11 -5 63780.2 2522.47 6 -4 11 -5 61792.5 3542.59 11 4 -11 6 1513.21 577.172 9 -4 -11 -6 2351.40 660.564 5 -4 -11 -6 3074.95 816.357 2 4 11 6 1885.21 511.206 8 4 -11 6 2338.24 627.070 12 -4 11 -6 2646.30 458.799 6 -4 11 -6 2052.39 596.832 7 4 11 6 2694.61 730.602 4 -4 11 -6 1514.45 513.690 11 4 -11 7 174464. 6215.66 9 -4 -11 -7 177188. 6502.90 5 4 11 7 178854. 5827.12 8 -4 11 -7 175956. 6412.68 7 4 11 7 180715. 6605.95 4 -4 11 -7 187036. 5265.62 6 -4 11 -7 171464. 6734.73 11 4 -11 7 178380. 6245.11 12 4 -11 8 9970.32 1269.21 9 4 11 8 12675.6 1317.48 8 -4 -11 -8 10037.5 1371.20 5 -4 11 -8 10317.0 1362.93 7 4 -11 8 9983.46 1277.90 12 -4 11 -8 11266.4 996.554 6 4 11 8 10426.8 1380.49 4 -4 11 -8 11254.9 1533.92 11 4 -11 9 118689. 5011.11 9 -4 -11 -9 125187. 5503.14 5 4 11 9 130911. 5044.52 8 -4 11 -9 127388. 5467.77 7 4 11 9 122349. 5271.19 4 -4 11 -9 118239. 5557.54 11 4 -11 9 125948. 5093.28 12 4 -11 10 5716.22 1065.83 9 -4 -11 -10 4427.79 1006.65 5 4 11 10 3836.39 842.289 8 -4 11 -10 3326.87 942.150 7 4 -11 10 4219.05 881.196 12 4 11 10 3731.02 905.593 4 -4 11 -10 2917.94 871.623 11 4 -11 11 11399.8 1478.86 12 -4 11 -11 15103.4 1980.70 11 4 -11 11 13409.2 1588.52 9 -4 -11 -11 13568.4 1747.14 5 4 11 11 14167.9 1652.19 8 -4 11 -11 11233.6 1619.92 7 4 11 11 10959.8 1496.82 4 -4 11 -12 691.422 512.039 7 4 12 -13-603.367 533.395 5 4 -12 -13 765.098 549.844 5 -4 -12 13-417.062 525.578 2 4 12 -12 1346.17 637.473 5 -4 12 12 1958.82 606.600 10 4 -12 -12 883.175 479.510 5 -4 12 12 1475.86 649.036 8 -4 -12 12 2001.00 660.065 2 4 12 -12 867.375 505.676 6 4 12 -11 783.164 519.580 5 -4 12 11 1184.39 623.762 10 4 -12 -11 766.421 429.786 5 -4 12 11 1442.48 799.466 8 -4 -12 11-3.44430 316.328 2 4 12 -11 255.522 480.929 6 4 12 -10 28931.0 2192.42 5 -4 12 10 26626.5 2199.38 10 4 -12 -10 31602.3 2263.84 5 4 12 -10 28468.9 2194.96 6 -4 -12 10 25357.6 2028.29 2 4 12 -9 1161.11 531.725 5 -4 12 9 849.066 492.234 10 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1307.45 381.981 12 4 12 -5 781.159 415.167 6 -4 12 4 24400.5 1683.41 10 4 -12 -4 27513.5 1505.46 5 4 -12 -4 22618.8 2236.30 3 4 -12 -4 29101.9 2447.26 13 -4 -12 4 25866.4 1592.20 9 -4 12 4 28167.0 2401.62 8 -4 -12 4 25574.8 1584.61 12 -4 12 4 25189.4 1429.77 7 4 12 -4 23351.4 1841.00 6 -4 -12 4 22775.6 1846.49 2 4 12 -3 297.884 432.222 4 -4 12 3 297.626 272.415 10 4 -12 -3 89.0350 457.920 3 4 -12 -3 394.979 199.821 5 -4 12 3 763.965 503.653 8 4 -12 -3 403.895 366.171 13 -4 -12 3-125.738 426.000 2 -4 12 3 522.107 259.400 7 4 12 -3 189.157 264.983 6 -4 12 2 767.372 276.840 7 -4 12 2 727.211 294.226 10 4 -12 -2 649.972 448.586 3 -4 12 2-252.280 583.468 8 4 -12 -2 848.713 501.459 13 -4 -12 2 1265.79 492.715 2 4 12 -2 802.081 558.180 4 4 12 -2 290.396 351.570 6 4 12 -1 255.263 390.299 4 -4 12 1 47.4891 195.565 10 4 -12 -1 1238.10 681.292 3 -4 -12 1 372.756 387.020 2 -4 12 1 6.60709 254.623 7 -4 -12 1 174.267 244.616 13 4 12 -1 396.259 293.227 6 4 -12 -1 829.997 496.624 13 -4 -12 0 32612.4 1592.14 3 4 -12 0 37788.8 2764.07 3 4 -12 0 37307.6 2770.88 9 -4 12 0 32876.9 1884.90 7 -4 -12 0 34096.2 1952.91 13 -4 12 0 34236.4 1634.84 10 -4 -12 0 31237.4 2276.34 2 4 12 0 32559.1 2532.96 4 4 -12 0 37428.6 2749.60 12 4 12 0 30985.6 2249.83 6 -4 12 -1 1326.98 315.727 10 4 -12 1 1063.29 514.543 3 -4 -12 -1 503.331 262.529 3 4 -12 1 759.429 576.788 9 -4 -12 -1 749.102 452.884 2 -4 12 -1 708.185 330.828 7 4 -12 1 887.211 633.434 12 4 12 1 1266.99 600.800 4 4 -12 2 83268.9 4360.92 12 4 -12 2 93932.0 4568.98 3 -4 -12 -2 107822. 3635.24 3 4 -12 2 88801.7 4486.77 9 -4 12 -2 94074.5 2882.78 10 -4 12 -2 93833.4 3763.97 7 -4 -12 -2 102893. 4487.22 2 4 12 2 102873. 4738.20 4 -4 12 -2 91111.7 4055.18 6 -4 12 -2 106110. 4704.42 11 -4 -12 -3 2251.07 744.708 2 4 -12 3 1094.68 579.604 9 -4 -12 -3 691.613 302.160 3 4 12 3 1095.31 329.682 8 -4 12 -3 708.240 364.490 7 4 -12 3 773.427 359.853 12 -4 12 -3 1218.24 459.433 6 4 12 3 809.022 537.422 4 -4 12 -3 398.136 379.758 11 -4 -12 -4 190473. 5970.50 3 4 -12 4 185266. 6853.12 9 4 12 4 208109. 5662.64 8 -4 12 -4 198637. 6465.32 7 -4 -12 -4 194796. 7019.95 2 4 12 4 184950. 7070.14 4 4 -12 4 181398. 6797.90 12 -4 12 -4 199672. 7129.04 11 -4 12 -4 193578. 5885.63 6 -4 -12 -5 2218.47 847.725 2 4 -12 5 1211.97 331.578 9 -4 12 -5 1168.00 368.261 6 -4 -12 -5 1771.89 791.828 3 -4 -12 -5 1304.68 648.870 5 4 12 5 955.512 440.364 8 -4 12 -5 738.357 494.943 7 4 -12 5 154.758 424.089 12 4 12 5 458.006 449.910 4 -4 12 -5 1551.24 638.034 11 -4 -12 -6 75381.1 3141.76 3 4 -12 6 74246.6 3751.67 9 4 12 6 82662.0 3318.08 8 -4 -12 -6 78526.8 3783.82 5 -4 -12 -6 71016.1 3878.61 2 -4 12 -6 72102.1 3691.84 7 4 12 6 70845.4 3923.80 4 4 -12 6 74573.3 3763.18 12 -4 12 -6 75987.5 2962.60 6 -4 12 -6 73060.7 3983.57 11 4 -12 7 328.135 465.964 9 -4 -12 -7 77.6003 329.148 5 4 12 7 831.416 483.378 8 -4 12 -7-306.581 404.076 7 -4 12 -7 224.416 389.213 11 4 -12 7 322.081 435.753 12 4 12 7 176.844 432.720 4 -4 12 -7 897.198 355.379 6 4 -12 8 995.458 536.911 9 -4 -12 -8 1405.98 644.114 5 4 12 8 1532.18 537.979 8 -4 12 -8 999.220 618.426 7 4 -12 8 400.832 331.674 12 4 12 8 1379.72 630.617 4 -4 12 -8 754.598 568.995 11 4 -12 9 20.4400 376.446 9 -4 -12 -9 801.022 568.580 5 4 12 9 295.448 368.345 8 4 -12 9 153.345 370.129 12 -4 12 -9 264.532 527.367 7 4 12 9 1106.26 619.398 4 -4 12 -9-403.168 561.180 11 4 -12 10 21908.6 2044.90 9 -4 -12 -10 25534.0 2353.77 5 4 -12 10 23418.8 2080.12 12 4 12 10 21940.2 1972.65 8 -4 12 -10 21248.3 2166.58 7 4 12 10 23282.5 2200.71 4 -4 12 -10 21389.8 2281.48 11 4 -12 11 540.424 528.152 9 -4 -12 -11 359.219 485.370 5 4 12 11 1009.82 570.703 8 -4 12 -11 1226.15 707.796 7 4 -12 11 553.982 428.505 12 4 12 11 303.690 423.642 4 -4 12 -11 599.019 539.044 11 4 -13 -13 23269.3 2280.20 5 4 13 -12 386.422 401.100 5 -4 -13 12 1344.97 608.427 2 4 -13 -12 142.373 467.702 5 4 13 -11 38915.9 2688.10 5 -4 13 11 44705.4 3009.01 10 4 -13 -11 46259.0 2902.38 5 -4 13 11 34948.4 3233.73 8 4 13 -11 38785.5 2736.53 6 -4 -13 11 35553.6 2540.88 2 4 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41065.6 3103.93 3 -4 -13 5 41952.9 2255.06 9 -4 -13 5 42406.2 2264.62 12 -4 13 5 52208.6 3412.71 8 4 13 -5 40280.8 2567.89 6 4 -13 -5 49132.6 3383.73 13 -4 -13 5 41262.2 2597.56 2 4 13 -4 2342.60 656.725 4 -4 13 4 3337.81 641.375 10 -4 -13 4 4480.67 680.345 9 4 -13 -4 3198.71 787.991 3 -4 13 4 3516.30 936.547 8 -4 -13 4 3012.65 712.046 2 4 -13 -4 4413.54 1039.28 13 -4 13 4 3089.40 498.380 7 -4 -13 4 4054.24 645.983 12 4 13 -4 3721.44 824.200 6 -4 13 3 57859.0 2650.48 10 4 13 -3 54516.2 3528.13 4 4 -13 -3 54440.1 3617.48 3 -4 13 3 63168.3 3639.12 8 -4 13 3 55759.4 2385.06 7 4 -13 -3 65901.5 3791.26 13 -4 -13 3 59024.3 3211.07 2 4 13 -3 54762.1 3098.49 6 4 13 -2 1368.24 537.209 4 -4 13 2 2157.84 487.823 10 4 13 -2 1424.45 521.475 6 4 -13 -2 1614.07 677.516 3 -4 13 2 2771.13 777.086 8 4 -13 -2 1751.41 668.421 13 -4 -13 2 1672.44 558.273 2 -4 13 2 930.485 296.011 7 -4 13 1 45130.2 2108.92 10 4 13 -1 42064.1 2729.83 6 4 -13 -1 50620.6 3267.02 3 4 -13 -1 46912.0 3110.60 13 -4 13 1 43452.5 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122550. 4209.53 6 -4 13 -7 114026. 5324.49 11 4 -13 8 5627.45 1036.58 9 -4 -13 -8 7543.18 1231.76 5 4 13 8 6393.13 993.034 8 -4 13 -8 4415.61 994.302 7 4 -13 8 3267.70 856.471 12 4 13 8 6979.47 1288.61 4 -4 13 -8 7491.14 1287.55 11 4 -13 9 58448.6 3442.20 9 -4 -13 -9 53749.8 3410.86 5 4 13 9 56551.9 3149.17 8 -4 13 -9 57362.0 3613.88 7 4 13 9 54997.1 3541.42 4 4 -13 9 53479.2 3352.92 12 -4 13 -9 53646.3 3616.43 11 4 -13 10 1758.84 757.105 9 -4 -13 -10 501.918 460.281 5 4 13 10 1893.71 639.000 8 -4 13 -10 564.916 448.013 7 4 -13 10 1608.85 665.306 12 4 13 10 2127.05 835.388 4 -4 13 -10 1020.84 510.092 11 -4 -13 -11 3708.39 950.232 5 -4 13 -11 5734.06 1270.11 11 4 13 11 3926.89 911.519 8 -4 -14 12-348.451 387.232 2 -4 14 11 2546.79 770.382 10 -4 14 11 2930.67 1134.53 8 4 -14 -11 2350.54 879.030 3 -4 -14 11 2309.95 735.477 2 4 14 -11 1950.65 674.282 6 4 14 -10 10817.2 1459.45 6 4 14 -10 8705.25 1229.87 5 -4 14 10 9994.19 1439.34 10 -4 14 10 9262.29 1650.60 8 4 -14 -10 10334.4 1581.64 3 -4 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982.550 7 5 11 -4 8690.06 1016.23 6 5 11 -3 8.08279 430.926 4 5 -11 -3 625.143 369.919 5 -5 11 3 763.246 314.953 10 5 -11 -3-247.607 557.494 3 -5 11 3 786.767 708.260 8 -5 -11 3-66.4838 517.289 2 5 -11 -3 732.973 511.855 13 5 11 -3 1101.74 495.064 6 -5 11 3 663.188 316.334 7 5 -11 -2 594.835 243.349 5 5 11 -2 704.772 484.245 4 5 -11 -2 851.557 517.635 13 -5 11 2 426.630 268.540 10 5 -11 -2 561.223 409.733 3 -5 -11 2 544.930 415.983 2 -5 11 2 326.553 232.478 7 5 11 -2 537.378 325.971 6 5 -11 -1 573.466 575.349 12 5 11 -1 362.546 587.482 4 -5 11 1 211.702 174.868 10 5 -11 -1 208.831 481.594 9 5 -11 -1-411.863 425.516 3 -5 -11 1 405.546 328.534 2 -5 11 1 180.860 246.075 7 5 11 -1 676.152 423.516 6 -5 11 0 18827.1 1236.59 10 5 -11 0 20131.0 1995.09 3 5 -11 0 20248.4 2065.62 9 -5 11 0 19566.3 1454.84 7 -5 -11 0 20604.6 1904.76 2 5 11 0 22571.2 2173.77 4 5 -11 0 20411.2 2071.67 12 5 11 0 17987.5 1588.32 6 -5 11 -1 3825.16 539.842 10 5 -11 1 3697.77 930.960 3 5 -11 1 2899.63 800.897 9 -5 -11 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78800.5 3792.31 7 5 11 6 77991.8 4119.00 4 5 -11 6 73949.4 3797.18 12 -5 11 -6 70805.9 4180.89 11 5 -11 7 291.204 413.767 9 -5 -11 -7 550.175 477.182 5 -5 11 -7 677.869 512.234 7 5 -11 7 815.701 489.097 12 5 11 7 756.500 515.379 4 -5 11 -7-389.738 550.858 11 5 -11 8 1024.71 625.999 9 -5 -11 -8 243.598 376.880 5 5 -11 8 97.4114 394.343 12 -5 11 -8 415.432 463.385 11 -5 11 -8 84.0304 388.490 7 5 11 8 762.272 621.299 4 5 -11 9-10.5844 350.604 9 -5 -11 -9 311.706 497.839 5 -5 11 -9-109.201 399.577 7 5 -11 9 564.065 541.330 12 5 11 9 390.807 362.719 4 -5 11 -9 485.739 637.054 11 5 -11 10 18216.9 1884.53 9 -5 -11 -10 16717.9 2006.33 5 5 11 10 15670.3 1799.73 4 -5 11 -10 16410.3 1860.68 7 5 -11 10 15104.0 1717.28 12 -5 11 -10 17637.4 2156.11 11 5 -11 11 1075.35 590.448 9 -5 -11 -11 501.714 575.492 5 -5 11 -11 531.497 547.906 7 5 -11 11 545.859 400.723 12 5 11 11 343.830 452.499 4 -5 11 -11 327.005 646.711 11 5 -12 -13 22741.0 2308.12 5 5 12 -12 866.333 607.550 5 5 -12 -12 775.711 508.945 5 -5 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3570.99 823.802 10 8 5 -9 2656.37 772.878 5 -8 5 9 2091.10 608.564 10 8 -5 -9 2565.11 796.873 5 -8 5 9 3922.65 1083.37 8 8 -5 -9 2659.01 774.839 3 -8 -5 9 2585.73 684.440 2 -8 -5 8 48558.6 2805.07 10 -8 5 8 47485.1 2891.85 10 8 5 -8 50327.5 3521.96 5 8 -5 -8 49469.8 3432.38 5 -8 5 8 48552.0 2742.55 2 8 -5 -8 50235.4 3298.77 3 -8 5 8 52411.1 3803.03 8 8 5 -8 51446.1 2519.99 6 -8 -5 8 47440.0 2952.45 2 8 5 -7 1611.88 700.654 5 -8 -5 7 717.051 482.392 10 8 -5 -7 1104.26 608.502 5 -8 5 7 1175.59 438.845 10 -8 5 7 969.880 706.160 8 8 -5 -7 311.314 436.021 3 8 -5 -7 711.554 338.859 1 -8 -5 7 967.745 483.933 2 8 5 -7 1320.45 440.209 1 -8 5 7 386.296 306.852 2 8 5 -7 556.760 252.331 6 -8 -5 6 12941.8 1352.26 10 -8 5 6 14387.0 1438.75 10 -8 5 6 13621.8 1307.55 2 8 5 -6 15783.1 1948.27 5 8 -5 -6 14943.8 1866.56 5 8 5 -6 13897.3 1180.06 1 8 -5 -6 12913.8 1164.91 1 -8 5 6 12508.6 1961.16 8 8 -5 -6 12526.7 1718.33 3 -8 5 6 12228.5 1413.13 7 8 5 -6 12479.2 1070.09 6 -8 -5 6 14592.8 1564.92 2 8 5 -5 217.038 490.219 5 8 -5 -5 379.446 560.091 5 -8 -5 5 519.317 371.264 10 -8 5 5-162.901 352.257 10 8 -5 -5-302.047 657.705 3 -8 5 5-373.724 811.939 8 -8 -5 5 158.400 434.629 2 -8 5 5-145.651 337.031 7 8 -5 -5 50.8704 238.616 1 -8 5 5-28.4310 251.817 2 8 5 -5 353.283 266.626 6 8 5 -4 1296.40 483.044 4 8 -5 -4 213.197 541.305 5 -8 -5 4-194.970 364.984 10 -8 5 4-405.379 373.223 10 8 -5 -4 645.718 560.105 3 -8 5 4-511.691 891.308 8 -8 -5 4-123.599 418.337 2 -8 5 4-170.427 406.608 7 -8 5 4 258.134 218.798 2 8 -5 -4-85.0509 252.655 1 8 5 -4 176.622 210.079 6 8 5 -3 1511.31 789.137 4 8 -5 -3 866.488 392.101 1 -8 -5 3 1462.35 546.298 10 -8 5 3 1874.41 591.045 10 8 -5 -3 1473.07 551.411 3 -8 -5 3 1673.58 600.826 2 -8 5 3 1808.52 536.498 7 -8 5 3 1164.83 384.315 2 8 5 -3 1199.43 296.026 6 -8 5 2 49632.1 2654.01 10 8 -5 -2 45762.4 2794.44 3 8 -5 -2 45674.4 2352.42 1 -8 5 2 47974.7 2613.28 7 -8 -5 2 47858.5 2725.01 7 8 5 -2 57499.0 3930.52 4 -8 -5 2 52208.2 3171.05 2 -8 5 2 49675.6 2504.68 2 -8 5 1 2065.98 521.756 10 8 -5 -1 2048.64 495.619 1 8 -5 -1 2014.31 524.569 3 -8 -5 1 1276.13 547.564 2 -8 5 1 2206.03 608.214 7 -8 -5 1 2125.32 631.525 7 8 5 -1 1574.23 629.672 4 -8 5 0 146848. 5238.96 10 8 -5 0 144719. 4898.53 3 8 -5 0 162508. 6040.66 9 8 -5 0 148889. 4971.37 1 -8 5 0 154925. 5302.49 7 -8 -5 0 143667. 5257.87 7 8 5 0 142884. 6039.80 4 -8 -5 0 159230. 6509.51 2 8 -5 0 159895. 6002.57 12 -8 -5 0 151056. 4722.21 11 -8 5 -1 8120.46 997.369 10 8 -5 1 8105.43 963.898 1 8 -5 1 9412.30 1379.13 9 -8 -5 -1 8387.84 1405.02 2 -8 5 -1 8432.49 1053.43 7 -8 -5 -1 7595.05 1007.04 7 8 -5 1 8117.26 1239.16 12 -8 -5 -1 7950.09 825.045 11 8 5 1 6377.07 1065.03 4 8 -5 2 148280. 6214.52 9 8 -5 2 147677. 5004.08 1 -8 5 -2 144909. 5242.46 7 -8 -5 -2 142785. 5113.16 7 -8 -5 -2 168008. 7035.18 2 8 5 2 137483. 5459.66 4 8 -5 2 155381. 6346.50 12 -8 -5 -2 152970. 4602.95 11 -8 5 -2 151508. 6903.60 11 8 -5 3 9185.07 1054.94 1 -8 -5 -3 9737.80 1490.40 2 8 -5 3 10145.7 1430.28 9 -8 5 -3 10268.6 1187.01 7 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1320.63 1 8 -5 8 11658.2 1215.48 1 -8 5 -8 11415.3 1269.47 5 -8 -5 -8 13171.7 1899.95 5 -8 -5 -8 11927.6 1225.03 7 -8 5 -8 12077.3 1469.78 7 8 -5 8 11264.6 1388.34 12 8 5 8 11096.6 1268.65 4 -8 5 -8 12174.2 1678.86 11 8 -5 9 7535.13 1209.12 9 -8 -5 -9 9766.68 1717.96 5 8 5 9 7743.73 1049.85 1 -8 5 -9 9493.06 1300.91 7 8 -5 9 8667.70 1264.61 12 8 5 9 8920.37 1162.07 4 8 -5 9 8753.95 1068.55 1 -8 5 -9 8023.73 1392.97 11 8 5 10 27819.1 2004.88 1 8 -5 10 27398.8 2358.40 9 8 5 10 25769.1 2072.91 4 8 -5 10 27084.7 2326.07 12 -8 -6 12 728.094 490.064 10 -8 6 12-492.958 865.233 8 -8 -6 11 21335.9 1897.58 10 8 -6 -11 20200.3 2257.33 5 -8 6 11 22251.7 2460.24 8 8 6 -11 22014.1 1834.90 6 8 6 -10 989.136 447.195 6 -8 -6 10 466.602 370.333 10 8 6 -10-482.294 576.603 5 -8 6 10 1244.20 557.701 10 8 -6 -10 2354.90 917.710 5 -8 6 10 1826.02 902.470 8 8 -6 -10 2238.86 855.660 3 -8 -6 10 354.266 383.726 2 -8 -6 9 427.544 391.247 10 8 6 -9 2314.75 864.160 5 -8 6 9 856.212 496.815 10 8 -6 -9 1554.04 676.385 5 -8 6 9 717.665 774.662 8 8 -6 -9 1369.11 695.885 3 -8 -6 9 410.016 401.764 2 8 6 -9 623.482 321.319 6 -8 6 8 423.830 402.209 2 8 6 -8 479.482 531.213 5 -8 -6 8 927.076 443.006 10 -8 6 8 694.516 432.666 10 8 -6 -8 1741.04 759.318 5 8 -6 -8 520.812 333.167 1 -8 6 8 1547.64 845.337 8 8 -6 -8 2433.12 832.729 3 -8 -6 8 371.448 442.762 2 8 6 -8 840.300 385.725 6 -8 -6 7 28219.9 2078.31 10 8 6 -7 28092.9 2653.56 5 -8 6 7 29312.6 2169.32 10 8 -6 -7 29910.6 2617.36 5 -8 6 7 31744.6 2095.70 2 8 -6 -7 29356.4 1861.05 1 8 -6 -7 24715.8 2439.60 3 8 6 -7 31405.4 1807.17 1 -8 6 7 29854.0 3077.64 8 -8 6 7 36706.4 2583.23 7 8 6 -7 32031.0 1891.32 6 -8 -6 7 27140.1 2204.65 2 8 6 -6 1878.46 797.679 5 -8 -6 6 2661.51 652.523 10 8 -6 -6 3579.63 1038.33 5 -8 6 6 4210.99 784.189 10 -8 6 6 3808.75 1237.97 8 8 -6 -6 2930.63 905.628 3 8 -6 -6 3718.87 659.063 1 -8 -6 6 3412.92 793.231 2 -8 6 6 4013.44 810.792 7 -8 6 6 4016.02 723.029 2 8 6 -6 3558.40 601.022 6 8 6 -5 106185. 5498.38 5 -8 6 5 107074. 4410.51 10 8 -6 -5 121219. 5670.43 5 -8 6 5 108352. 4102.60 2 8 -6 -5 98973.2 5407.43 3 8 -6 -5 104635. 3950.84 1 -8 6 5 126626. 6800.27 8 -8 6 5 115440. 4709.05 7 8 6 -5 113873. 3804.90 6 -8 -6 5 111252. 4831.51 2 -8 -6 5 109823. 4436.55 10 8 6 -4 3577.37 1079.01 4 8 -6 -4 2368.29 796.518 5 -8 -6 4 2426.41 601.711 10 -8 6 4 2080.25 584.496 10 8 -6 -4 2713.01 841.650 3 -8 6 4 3809.88 1167.21 8 -8 -6 4 1270.47 499.668 2 -8 6 4 3106.21 697.743 7 8 -6 -4 2511.16 525.025 1 -8 6 4 2103.02 496.780 2 8 6 -4 2274.27 450.389 6 -8 6 3 93994.4 4016.60 10 8 -6 -3 116969. 5296.53 3 8 -6 -3 98094.4 3773.85 1 -8 6 3 95664.0 4074.64 7 8 6 -3 113879. 5905.31 4 -8 -6 3 97144.5 4596.57 2 8 6 -3 106873. 3385.29 6 -8 6 3 99172.2 3756.59 2 8 6 -2 3568.77 1033.78 4 -8 6 2 1523.56 439.994 10 8 -6 -2 1980.82 599.847 3 -8 -6 2 1355.08 561.236 2 -8 6 2 3240.24 700.350 7 8 -6 -2 2348.45 535.363 1 8 6 -2 2266.88 413.567 6 -8 6 1 34549.8 2190.92 10 8 -6 -1 36774.1 2364.66 3 8 -6 -1 35248.3 2059.88 1 -8 6 1 31747.2 2109.70 7 -8 -6 1 36480.5 2307.51 7 8 6 -1 42948.7 3235.26 4 -8 -6 1 36787.2 2805.84 2 8 -6 0 69.7407 302.858 1 -8 6 0 505.427 407.866 10 8 -6 0 259.295 293.380 3 8 -6 0 317.687 476.176 9 -8 -6 0 1097.74 652.838 2 -8 6 0 121.100 310.200 7 -8 -6 0 242.356 287.930 7 8 -6 0 97.1289 486.225 12 8 6 0 323.126 454.970 4 -8 6 -1 88.1470 290.711 10 8 -6 1 695.777 345.048 1 8 -6 1 352.908 404.972 9 -8 -6 -1 17.8474 372.919 2 -8 6 -1 427.144 318.606 7 -8 -6 -1 446.083 319.403 7 8 -6 1 4.58615 401.879 12 8 6 1 314.586 335.842 4 8 -6 2 305.507 293.832 1 8 -6 2 597.658 433.576 9 -8 -6 -2 1284.82 859.492 2 -8 6 -2 1454.43 545.958 7 -8 -6 -2 1438.41 443.311 7 8 -6 2 2467.94 735.290 12 8 6 2 1489.00 576.679 4 -8 6 -2-114.217 753.429 11 8 -6 3 22191.8 2167.19 9 8 -6 3 24791.5 1720.86 1 -8 6 -3 22706.1 1809.54 7 -8 -6 -3 24125.2 2456.28 2 -8 -6 -3 23026.4 1694.44 7 8 6 3 21935.1 1923.44 4 8 -6 3 23329.2 2192.29 12 -8 6 -3 24561.9 2564.44 11 8 -6 4 794.639 408.958 1 -8 -6 -4-230.643 432.103 2 8 -6 4-563.723 738.616 9 -8 6 -4-110.894 345.989 7 -8 -6 -4 832.153 431.428 7 8 -6 4-214.997 613.113 12 8 6 4 544.065 426.954 4 -8 6 -4 442.303 522.091 11 8 -6 5 73153.1 3888.45 9 8 -6 5 73797.3 3251.76 1 -8 -6 -5 68333.2 4030.47 2 -8 6 -5 75367.4 3610.38 7 8 6 5 70303.6 3512.10 4 -8 -6 -5 71825.9 3227.75 7 8 -6 5 77377.4 3995.59 12 -8 6 -5 77756.4 4554.61 11 -8 -6 -6 1197.89 586.332 2 8 -6 6 756.070 555.478 9 -8 6 -6 292.312 235.528 5 -8 6 -6 1149.78 556.795 7 -8 -6 -6 1320.59 418.028 7 8 -6 6 669.393 399.528 12 8 6 6 4.80938 331.451 4 -8 6 -6 300.120 477.640 11 8 -6 6 1084.69 446.511 1 8 -6 7 75860.6 3988.92 9 8 -6 7 78327.7 3443.62 1 -8 6 -7 86192.6 4022.75 7 8 6 7 71751.6 3615.76 4 -8 -6 -7 81609.2 3469.21 7 8 -6 7 83825.7 4147.77 12 -8 6 -7 81840.9 4653.48 11 8 -6 8 2515.81 759.943 9 -8 -6 -8 1065.83 552.202 5 -8 6 -8 3209.55 798.826 7 -8 -6 -8 2563.69 589.653 7 8 -6 8 3172.07 837.641 12 8 6 8 3698.02 785.191 4 8 -6 8 3012.73 658.908 1 -8 6 -8 2188.92 818.841 11 8 -6 9 22238.1 2091.39 9 8 6 9 18416.0 1635.81 1 8 -6 9 19822.6 1639.18 1 -8 -6 -9 17593.2 2318.61 5 8 6 9 21305.0 1875.53 4 -8 6 -9 21863.8 2035.59 7 8 -6 9 20545.9 1997.42 12 -8 6 -9 19551.4 2253.41 11 8 -6 10 3099.76 830.284 9 8 6 10 3471.02 724.961 1 8 -6 10 3017.12 765.829 12 8 6 10 3348.82 771.798 4 8 7 -11 175.421 410.145 6 -8 -7 11-17.6320 408.277 10 8 -7 -11 231.828 475.998 5 -8 7 11 1776.05 877.427 8 8 -7 -11 691.830 664.175 3 -8 -7 10 37389.6 2538.39 10 -8 7 10 42202.7 2883.81 10 8 7 -10 38360.3 3177.30 5 8 -7 -10 39563.5 3149.55 5 8 -7 -10 41694.7 3196.32 3 -8 7 10 42426.2 3640.20 8 8 7 -10 46207.7 2646.95 6 -8 -7 10 42091.9 2929.20 2 8 7 -9 134.834 413.078 5 -8 -7 9 442.092 379.494 10 -8 7 9 483.744 364.971 10 8 -7 -9 761.348 572.392 5 -8 7 9 155.238 600.606 8 8 -7 -9 329.801 532.421 3 -8 -7 9 727.900 537.490 2 8 7 -9 249.693 330.010 6 -8 -7 8 77101.1 3678.28 10 8 7 -8 77495.6 4567.43 5 -8 7 8 80622.5 3935.21 10 8 -7 -8 78240.5 4406.19 5 8 -7 -8 75150.7 4449.74 3 -8 7 8 86338.2 5408.76 8 8 7 -8 78813.3 3412.73 6 -8 -7 8 80720.9 4080.79 2 -8 7 7 1139.97 547.300 2 8 7 -7 1827.40 741.594 5 -8 -7 7 1307.92 532.965 10 8 -7 -7 2536.00 866.954 5 -8 7 7 1736.42 590.832 10 8 -7 -7 887.531 371.039 1 -8 7 7 2280.54 1000.97 8 8 -7 -7 952.948 655.055 3 8 -7 -7 1446.19 573.409 13 -8 -7 7 943.073 462.472 2 -8 7 7 1810.54 596.592 7 8 7 -7 1520.87 415.818 6 8 7 -6 52573.5 3710.74 5 -8 7 6 56153.5 3051.97 10 8 -7 -6 57891.3 3693.30 5 -8 7 6 53168.2 2720.81 2 8 -7 -6 57038.5 2744.63 1 8 -7 -6 49186.5 3703.04 3 -8 7 6 57860.7 4514.36 8 -8 7 6 58049.0 3300.49 7 8 -7 -6 59407.3 3198.39 13 8 7 -6 56958.5 2610.24 6 -8 -7 6 54124.6 3256.80 2 -8 -7 6 52957.1 2918.31 10 8 7 -5 1247.32 715.469 4 8 -7 -5 1732.27 755.871 5 -8 -7 5 589.826 412.947 10 -8 7 5 1724.78 590.627 10 8 -7 -5 736.535 560.885 3 -8 7 5 1504.29 793.298 8 8 -7 -5 478.990 334.993 1 -8 -7 5 2460.32 761.083 2 -8 7 5 990.307 446.231 7 -8 7 5 1164.11 488.390 2 8 7 -5 1249.28 366.996 6 8 7 -4 675.508 634.542 4 8 -7 -4-618.309 782.692 5 -8 7 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3129.43 3 -8 14 5 30478.1 3129.18 8 8 14 -5 30298.7 3159.50 4 -8 -14 5 28032.6 2695.57 2 8 14 -5 27179.4 2167.08 6 -8 14 4 31281.1 2378.46 10 8 -14 -4 35427.1 3163.05 3 -8 14 4 41673.9 3634.27 8 8 14 -4 33653.0 3213.21 4 -8 -14 4 33458.6 2918.13 2 8 14 -4 32697.0 2358.59 6 8 14 -3 12574.7 1900.81 4 8 -14 -3 13738.8 1936.66 3 -8 14 3 12863.6 1994.14 8 -8 -14 3 12505.2 1732.28 2 8 14 -3 10168.8 1303.55 6 8 -14 -2 17674.2 2135.68 3 -8 14 2 15433.4 2139.88 8 -8 -14 2 17159.6 2068.58 2 -8 14 2 15771.1 1660.04 7 8 14 -2 15077.2 1541.40 6 8 14 -2 18414.6 2263.63 4 8 -14 -1-46.1759 459.225 3 -8 -14 1 164.545 514.529 2 -8 14 1 623.657 382.826 7 8 14 -1-137.243 407.961 6 8 14 -1 98.0156 432.139 4 8 -14 0 3726.96 1061.83 3 -8 -14 0 3330.08 946.748 2 -8 14 0 1532.12 487.913 7 8 14 0 3443.68 952.392 4 8 -14 1 1.28551 408.899 3 -8 -14 -1 458.387 599.972 2 8 -14 1 1119.91 723.944 9 -8 14 -1 327.390 351.755 7 8 14 1 1527.21 812.800 4 -8 14 -1 442.946 475.976 11 -8 -14 -2 6155.44 1218.04 2 8 -14 2 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6951.43 1508.36 12 -8 16 6 9865.03 1457.11 10 8 16 -5 45666.2 3063.40 6 8 -16 -4 9616.12 1699.01 3 8 16 -4 10028.3 1398.05 6 8 -16 -3 34413.1 3076.17 3 8 16 -3 35630.1 2664.53 6 8 -16 -2 3689.24 927.766 3 -8 16 2 4290.50 1275.01 8 8 16 -2 1617.46 569.102 6 8 16 -2 5404.26 1285.57 4 8 -16 -1 6156.27 1224.69 3 -8 -16 1 7967.11 1483.96 2 -8 16 1 6193.20 1114.54 7 8 16 -1 7373.95 1204.67 6 8 16 -1 7440.58 1492.87 4 8 -16 0-139.783 473.214 3 -8 -16 0-455.885 591.311 2 -8 16 0 537.169 499.153 7 8 16 0 450.940 622.975 4 -8 16 -1 324.669 469.343 7 -8 16 -1 1954.46 820.780 11 8 -16 2 4383.83 1144.41 9 -8 16 -2 2297.93 719.161 7 8 -16 2 4633.92 1221.14 12 -8 16 -3 9590.38 1473.82 7 8 17 -4-252.467 535.375 6 8 17 -3 26.4739 465.694 6 8 17 -2 8893.65 1362.26 6 8 -17 -1 984.308 666.232 3 8 17 -1 3404.99 923.161 6 8 -17 0 40339.6 3271.60 3 -8 17 0 33058.3 2601.86 7 -8 17 -1 1621.02 651.244 7 -8 17 -2 38905.3 2956.62 7 8 18 -2 3273.22 846.309 6 8 18 -1 26061.8 2418.30 6 -8 18 -1 1061.96 637.185 7 -9 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-2-890.363 649.932 7 11 0 2-90.9483 378.146 1 -11 1 8 16116.6 1904.69 2 -11 -1 7 4.92394 465.758 2 11 -1 -6 1750.44 568.691 1 11 1 -6 1234.04 468.725 1 -11 -1 6-78.4204 464.596 2 -11 1 5-40.6096 404.453 10 11 -1 -5 588.269 361.677 1 11 1 -5 214.940 364.616 1 -11 -1 5-521.606 550.705 2 -11 1 5 228.582 599.414 7 -11 -1 4 11850.6 1551.43 10 -11 1 4 12989.3 1615.56 10 11 -1 -4 13458.2 1406.64 1 -11 1 4 11500.9 1595.71 7 -11 -1 4 14562.8 1782.14 7 11 1 -4 14311.4 1472.39 1 -11 1 3 929.269 591.699 10 11 -1 -3 2384.21 608.839 1 -11 1 3 560.015 474.329 7 -11 -1 3 2100.07 744.502 7 11 1 -3 1755.32 539.926 1 -11 -1 3 178.689 389.687 10 -11 1 2 18281.2 1950.50 7 11 -1 -2 18400.8 1684.12 1 -11 -1 2 18772.3 1965.08 7 11 1 -2 18922.5 1714.27 1 -11 1 2 18588.5 1937.08 10 11 1 -1 2231.75 614.268 1 11 -1 -1 1966.27 570.369 1 -11 1 1 719.404 485.343 7 -11 -1 1 1055.33 467.735 7 -11 -1 0 18104.6 1948.69 7 11 -1 0 17115.4 1622.46 1 -11 1 0 17852.4 1893.41 7 11 1 0 17957.9 1705.92 1 -11 1 0 16592.3 2000.55 11 11 1 1 1994.92 580.558 1 11 -1 1 1617.85 594.186 1 -11 1 -1 2090.29 727.676 7 -11 -1 -1 1242.57 701.299 7 -11 1 -1 1931.02 669.083 11 11 1 2 7635.50 1131.59 1 11 -1 2 5935.76 993.850 1 -11 1 -2 7244.79 1227.91 7 -11 -1 -2 7472.44 1209.03 7 -11 1 -2 5280.08 1030.06 11 -11 1 -3 975.806 586.917 11 -11 1 -4 2843.93 813.838 11 -11 -2 7 53423.2 3652.59 2 11 -2 -6 3747.41 772.670 1 11 2 -6 4372.94 803.572 1 -11 -2 6 3736.79 962.614 2 -11 2 5 27763.7 2387.74 10 11 -2 -5 25226.1 1967.88 1 -11 2 5 26166.1 2455.67 7 11 2 -5 24124.4 1933.84 1 -11 -2 5 27701.4 2617.22 2 -11 -2 4 2061.12 716.833 10 -11 2 4 1624.08 662.434 10 11 -2 -4 1837.33 538.201 1 -11 2 4 2177.54 957.531 8 -11 -2 4 1003.95 635.949 2 -11 2 4 1329.85 615.482 7 11 2 -4 1631.77 586.252 1 -11 2 3 3976.91 885.579 10 11 2 -3 2255.54 634.653 1 11 -2 -3 4329.24 851.228 1 -11 2 3 857.451 504.550 7 -11 -2 3 2154.03 770.266 7 -11 2 2-188.961 480.794 10 11 2 -2 649.391 454.734 1 11 -2 -2 603.022 481.702 1 -11 2 2-273.208 427.680 7 -11 -2 2-95.2012 515.730 7 11 2 -1 1168.38 524.850 1 11 -2 -1 1406.02 496.571 1 -11 2 1 2180.60 734.226 7 -11 -2 1 1512.42 636.734 7 11 2 0 10681.2 1309.60 1 11 -2 0 8951.70 1220.50 1 -11 2 0 9312.31 1421.04 7 -11 -2 0 11391.2 1509.50 7 -11 2 0 8604.21 1457.91 11 -11 2 -1 22668.4 2147.45 7 -11 -2 -1 24107.6 2193.09 7 11 -2 1 21169.8 1866.26 1 -11 2 -1 21351.0 2297.28 11 11 2 1 21712.8 1902.09 1 -11 -2 -2 39468.8 2796.45 7 -11 2 -2 34465.3 2890.94 11 -11 2 -3 52606.8 3561.55 11 -11 2 -4 21449.6 2186.62 11 -11 2 -5 43520.2 3177.81 11 -11 -3 7 422.975 582.264 2 -11 -3 6 320.984 413.193 2 11 3 -6 815.661 430.903 1 11 -3 -6 431.365 370.726 1 11 -3 -5 5393.35 938.740 1 -11 3 5 6461.33 1193.66 10 -11 3 5 7929.56 1769.08 8 -11 -3 5 4889.33 1091.64 2 -11 3 5 6274.30 1249.85 7 11 3 -5 6171.26 998.907 1 -11 3 4 14382.4 1714.26 10 11 3 -4 12008.4 1325.81 1 -11 3 4 17151.3 2577.74 8 11 -3 -4 14107.2 1469.05 1 -11 -3 4 15180.9 1968.81 2 -11 3 4 13222.0 1723.79 7 -11 -3 4 14204.4 1691.60 10 -11 -3 3 19645.7 2313.25 2 11 -3 -3 21101.7 1824.23 1 -11 3 3 22934.1 2243.21 7 -11 -3 3 20982.3 2106.29 7 11 3 -3 19652.3 1770.99 1 -11 3 3 19340.8 1994.53 10 11 -3 -2 27236.1 2085.20 1 -11 3 2 28387.9 2430.61 7 -11 -3 2 24416.0 2304.09 7 11 3 -2 22450.6 1921.19 1 -11 3 2 26720.8 2369.01 10 11 3 -1 26177.0 2083.81 1 11 -3 -1 27922.0 2125.14 1 -11 3 1 28184.7 2405.97 7 -11 -3 1 26625.1 2344.29 7 -11 3 1 28217.0 2428.38 10 11 3 0 17918.6 1716.46 1 11 -3 0 17679.0 1687.49 1 -11 -3 0 17171.4 1874.08 7 -11 3 0 15858.0 1766.17 7 -11 3 0 15810.1 2146.84 11 11 3 1 15372.7 1595.29 1 11 -3 1 18288.6 1728.67 1 -11 3 -1 17632.7 1897.13 7 -11 -3 -1 15860.2 1779.68 7 -11 3 -1 18530.1 2225.47 11 -11 -3 -2 2434.48 791.203 7 -11 3 -2 2675.23 921.945 11 -11 3 -3-103.929 607.175 11 -11 3 -4 1791.43 702.382 11 -11 3 -5 18172.6 2116.26 11 11 -4 -6 32979.1 2288.58 1 -11 4 6 31135.2 2803.85 7 -11 -4 6 34438.8 2953.41 2 11 4 -6 28906.3 2147.01 1 -11 4 5 13426.4 1726.41 10 11 4 -5 12347.0 1362.45 1 -11 4 5 13977.5 2349.75 8 -11 -4 5 11741.8 1758.73 2 -11 4 5 11948.6 1657.84 7 11 -4 -5 11482.5 1337.43 1 -11 4 4 21351.6 2132.14 10 11 -4 -4 23011.9 1898.04 1 -11 4 4 22465.8 3010.16 8 -11 4 4 21421.9 2176.32 7 -11 -4 4 23717.7 2527.48 2 11 4 -4 24351.7 1958.01 1 -11 4 3 2794.65 795.100 10 11 -4 -3 2722.54 691.986 1 -11 -4 3 2977.06 966.840 2 11 4 -3 2029.60 620.256 1 -11 4 3 3335.48 842.870 7 -11 4 2 1939.46 761.059 10 11 -4 -2 2978.64 743.251 1 -11 -4 2 3297.69 1083.39 2 -11 4 2 2562.86 789.020 7 -11 -4 2 3738.70 975.648 7 11 4 -2 2337.24 660.833 1 11 4 -1 2062.76 616.619 1 11 -4 -1 2333.21 635.666 1 -11 4 1 4572.60 1029.01 7 -11 -4 1 2361.17 773.803 7 -11 4 1 3235.83 847.417 10 11 4 0 6434.15 1088.03 1 11 -4 0 7558.91 1126.09 1 -11 4 0 4761.89 1018.49 7 -11 -4 0 6362.22 1152.69 7 -11 4 0 5178.75 1227.29 11 11 4 1 22501.1 1959.15 1 -11 4 -1 26356.4 2353.49 7 -11 -4 -1 25349.4 2254.47 7 -11 4 -1 29373.2 2947.14 11 -11 -4 -2 43038.0 2935.94 7 -11 4 -2 38067.5 3338.03 11 -11 4 -3 17481.7 2151.29 11 -11 4 -4 33554.2 3022.09 11 -11 5 7 2245.26 982.077 8 11 5 -6 2575.53 641.610 1 -11 5 6 4845.39 1393.19 8 -11 -5 6 4441.68 1079.02 2 11 -5 -6 3468.41 815.383 1 -11 5 6 3331.67 942.185 7 -11 5 5 9141.78 1934.27 8 -11 -5 5 6367.19 1296.06 2 11 5 -5 5566.08 967.375 1 -11 5 5 8184.82 1390.32 7 11 -5 -5 5819.10 978.367 1 -11 5 4 779.266 606.488 10 -11 5 4 726.453 1069.35 8 -11 -5 4-75.3968 527.000 2 -11 5 4-227.752 505.656 7 11 -5 -4 222.598 392.777 1 11 5 -4 709.691 413.176 1 -11 5 3 32521.9 2620.90 10 11 5 -3 28649.9 2166.89 1 11 -5 -3 29760.4 2221.50 1 -11 5 3 29306.3 2542.70 7 -11 -5 3 34266.7 3140.22 2 -11 5 2 3761.43 908.692 10 11 5 -2 3760.20 827.838 1 -11 -5 2 5423.85 1320.33 2 -11 5 2 2936.86 831.661 7 11 -5 -2 3864.83 841.737 1 11 5 -1 48581.1 2959.23 1 11 -5 -1 52426.3 3043.46 1 -11 5 1 50932.3 3371.98 7 -11 -5 1 57668.5 3523.21 7 -11 -5 1 62000.9 4342.27 2 -11 5 1 51950.4 3423.06 10 11 -5 0 686.203 322.108 1 -11 5 0 134.110 416.330 7 -11 -5 0 714.010 450.002 7 11 5 0 970.489 491.594 1 -11 5 0 345.728 555.297 11 -11 -5 -1 28921.9 2413.10 7 -11 5 -1 28948.6 3018.04 11 -11 5 -2 3891.31 1019.18 11 -11 5 -3 808.828 484.872 11 11 6 -6 39054.7 2536.82 1 11 -6 -6 39668.7 2604.62 1 -11 6 6 46787.8 4397.31 8 -11 6 6 43894.9 3389.55 7 11 6 -5 983.587 495.456 1 -11 6 5 1559.46 722.242 8 -11 -6 5 1093.40 507.904 2 11 -6 -5 1275.64 473.881 1 -11 6 5 2271.77 841.926 7 -11 6 4 25947.9 2373.60 10 11 6 -4 23448.5 1949.21 1 11 -6 -4 25621.6 2057.24 1 -11 6 4 29428.0 3576.99 8 -11 6 4 23256.2 2320.25 7 -11 -6 4 26066.0 2716.62 2 -11 6 3 1378.98 581.592 10 -11 6 3-602.539 1233.46 8 -11 -6 3 1164.81 582.775 2 -11 6 3 965.869 434.113 7 11 -6 -3 909.056 506.200 1 11 6 -3 1225.80 533.235 1 -11 6 2 481.510 403.350 10 11 6 -2 712.619 483.969 1 -11 -6 2-52.8456 708.631 2 -11 6 2 1472.64 623.465 7 11 -6 -2 920.160 462.435 1 -11 6 1 850.432 587.093 10 -11 -6 1 1936.42 836.703 2 11 6 -1 654.678 451.508 1 -11 6 1 282.887 515.060 7 -11 -6 0 12289.7 1960.76 2 -11 6 0 9345.93 1881.08 11 -11 6 -1 9939.27 1785.91 11 -11 6 -2 26380.0 2958.79 11 11 7 -6 15658.9 2404.64 4 -11 7 6 12768.8 1862.89 7 11 7 -5 8929.60 1791.48 4 11 7 -5 6530.55 1075.65 1 -11 7 5 5791.20 1277.85 7 11 7 -4 9230.79 1763.75 4 -11 7 4 10455.0 1492.09 10 11 7 -4 7980.35 1174.32 1 -11 -7 4 9478.61 1664.23 2 -11 7 4 7748.81 1407.67 7 -11 7 3 28984.8 2509.19 10 11 7 -3 27247.9 2187.79 1 -11 7 3 32367.3 3682.73 8 -11 7 3 27119.9 2491.09 7 11 7 -3 33743.7 3192.04 4 -11 -7 3 27300.6 2887.98 2 -11 7 2 4037.13 1005.71 10 -11 -7 2 3361.05 982.998 2 -11 7 2 4350.61 1054.55 7 -11 -7 1 29071.2 3013.98 2 -11 7 1 26696.3 2431.13 10 -11 -7 0 2056.72 924.793 2 -11 7 0 4934.85 1541.39 11 -11 -7 -1 12691.1 1994.00 2 11 8 -5 3348.48 1101.09 4 -11 8 5 3386.74 920.010 7 -11 8 4 6391.34 1227.59 10 -11 8 4 5514.73 1101.19 7 -11 8 3 500.142 565.126 10 -11 -8 3-375.787 581.066 2 -11 8 3 731.545 460.113 7 11 8 -3-168.697 597.259 4 -11 8 2 2405.74 842.842 10 -11 -8 2 1098.56 605.931 2 11 8 -2 1497.76 768.297 4 -11 -8 1 1503.24 785.393 2 11 8 -1 1011.15 557.921 4 -11 -8 0 18819.3 2425.22 2 11 8 0 17780.6 2155.02 4 -11 -8 -1 9277.89 1687.78 2 -11 9 5 9731.55 1556.00 7 -11 9 3 21709.2 2211.53 10 11 9 -3 24813.0 2827.59 4 11 9 -2 39590.4 3476.59 4 -11 -9 1 20392.7 2519.76 2 11 9 -1 21047.8 2429.13 4 -11 -9 0 24108.8 2747.35 2 11 9 0 17517.2 2204.64 4 -11 -9 -1 3962.79 1161.46 2 11 9 1 3151.24 938.015 4 -11 -9 -2 1915.08 948.836 2 11 9 2 3047.71 963.590 4 -12 3 1-222.377 706.900 11 -12 3 0-38.1807 478.687 11 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 63791 _shelx_res_file ; TITL Philip in P2(1)/n shelx.res created by SHELXL-2019/3 at 11:28:53 on 03-Nov-2023 CELL 0.71073 8.453325 17.056295 11.482596 90.0000 94.5250 90.0000 ZERR 4.00 0.0002 0.0004 0.0003 0.0000 0.002 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H P S Cl Au UNIT 40.00 92.00 4.00 4.00 12.00 4.00 L.S. 6 FMAP 2 PLAN 10 OMIT 0 1 1 OMIT 2 1 1 TEMP -173 SIZE 0.3 0.2 0.02 ACTA 60 CONF 2.35 BOND $H HTAB C32 CL3 HTAB C3 CL3 HTAB C13 CL3 EQIV $1 -1+x,y,z HTAB C13 CL2_$1 EQIV $2 0.5-x,0.5+y,1.5-z HTAB C31 CL1_$2 EQIV $3 1-x,1-y,1-z RTAB CONT CL3 S1_$3 WGHT 0.018800 1.795700 FVAR 2.12691 AU1 6 0.537318 0.458112 0.698923 11.00000 0.01036 0.01403 = 0.01301 -0.00017 -0.00001 -0.00005 CL1 5 0.601481 0.330067 0.743755 11.00000 0.02115 0.01696 = 0.02570 0.00290 -0.00093 0.00271 CL2 5 0.781179 0.495710 0.779455 11.00000 0.01171 0.02626 = 0.02005 0.00025 -0.00237 -0.00191 CL3 5 0.294109 0.415919 0.623957 11.00000 0.01409 0.01678 = 0.02697 -0.00096 -0.00454 -0.00167 S1 4 0.495528 0.588415 0.644059 11.00000 0.01236 0.01516 = 0.01916 0.00194 0.00322 -0.00095 P1 3 0.295781 0.632896 0.710793 11.00000 0.01107 0.01231 = 0.01240 -0.00049 -0.00107 -0.00069 C1 1 0.284481 0.610533 0.869795 11.00000 0.01447 0.02658 = 0.01101 0.00000 -0.00194 0.00183 C2 1 0.318620 0.739387 0.690648 11.00000 0.01572 0.01367 = 0.02441 -0.00232 -0.00158 -0.00176 AFIX 13 H2 2 0.225743 0.765191 0.723585 11.00000 -1.20000 AFIX 0 C3 1 0.113618 0.598931 0.626738 11.00000 0.01199 0.01539 = 0.01278 -0.00077 -0.00226 -0.00196 AFIX 13 H3 2 0.086801 0.546807 0.659853 11.00000 -1.20000 AFIX 0 C11 1 0.191582 0.675957 0.927128 11.00000 0.02905 0.04451 = 0.01700 -0.00505 0.00144 0.01554 AFIX 137 H11A 2 0.087035 0.681955 0.884754 11.00000 -1.50000 H11B 2 0.250247 0.725398 0.924447 11.00000 -1.50000 H11C 2 0.178412 0.662105 1.008626 11.00000 -1.50000 AFIX 0 C12 1 0.452247 0.605259 0.931553 11.00000 0.01963 0.02609 = 0.01649 -0.00117 -0.00406 0.00130 AFIX 137 H12A 2 0.444865 0.599219 1.015825 11.00000 -1.50000 H12B 2 0.511144 0.653237 0.916622 11.00000 -1.50000 H12C 2 0.507673 0.559959 0.901581 11.00000 -1.50000 AFIX 0 C13 1 0.200177 0.532278 0.884624 11.00000 0.02573 0.03474 = 0.01570 0.00744 -0.00062 -0.00601 AFIX 137 H13A 2 0.251077 0.491559 0.840353 11.00000 -1.50000 H13B 2 0.088482 0.537125 0.855490 11.00000 -1.50000 H13C 2 0.206934 0.517989 0.967533 11.00000 -1.50000 AFIX 0 C21 1 0.468554 0.772421 0.757012 11.00000 0.02217 0.01801 = 0.03918 -0.00497 -0.00592 -0.00551 AFIX 137 H21A 2 0.562457 0.747474 0.728384 11.00000 -1.50000 H21B 2 0.465404 0.761735 0.840654 11.00000 -1.50000 H21C 2 0.473607 0.829162 0.744403 11.00000 -1.50000 AFIX 0 C22 1 0.314425 0.762659 0.561398 11.00000 0.02874 0.01935 = 0.02840 0.00585 0.00265 -0.00536 AFIX 137 H22A 2 0.327366 0.819562 0.555111 11.00000 -1.50000 H22B 2 0.212447 0.747082 0.521601 11.00000 -1.50000 H22C 2 0.400784 0.736199 0.524910 11.00000 -1.50000 AFIX 0 C31 1 -0.029476 0.652836 0.641597 11.00000 0.01190 0.02044 = 0.02142 -0.00292 -0.00200 0.00110 AFIX 137 H31A 2 -0.008746 0.704791 0.609683 11.00000 -1.50000 H31B 2 -0.046308 0.657606 0.724769 11.00000 -1.50000 H31C 2 -0.124461 0.630425 0.599796 11.00000 -1.50000 AFIX 0 C32 1 0.137478 0.585310 0.497126 11.00000 0.01853 0.01813 = 0.01235 -0.00047 -0.00260 -0.00026 AFIX 137 H32A 2 0.038294 0.566233 0.456976 11.00000 -1.50000 H32B 2 0.221306 0.546296 0.490133 11.00000 -1.50000 H32C 2 0.168064 0.634707 0.461534 11.00000 -1.50000 AFIX 0 HKLF 4 REM Philip in P2(1)/n REM wR2 = 0.0456, GooF = S = 1.071, Restrained GooF = 1.071 for all data REM R1 = 0.0210 for 4483 Fo > 4sig(Fo) and 0.0247 for all 4863 data REM 152 parameters refined using 0 restraints END WGHT 0.0188 1.7955 REM Highest difference peak 2.152, deepest hole -1.414, 1-sigma level 0.135 Q1 1 0.5423 0.4578 0.7729 11.00000 0.05 2.15 Q2 1 0.5347 0.4584 0.6235 11.00000 0.05 2.11 Q3 1 0.5843 0.4924 0.6986 11.00000 0.05 1.00 Q4 1 0.5810 0.4201 0.6959 11.00000 0.05 1.00 Q5 1 0.5017 0.5151 0.7494 11.00000 0.05 0.84 Q6 1 0.5042 0.4022 0.7549 11.00000 0.05 0.83 Q7 1 0.5731 0.5119 0.6419 11.00000 0.05 0.80 Q8 1 0.4657 0.4093 0.6483 11.00000 0.05 0.65 Q9 1 0.5034 0.5181 0.6542 11.00000 0.05 0.56 Q10 1 0.5971 0.3335 0.6612 11.00000 0.05 0.56 ; _shelx_res_checksum 14168 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Au Au1 0.53732(2) 0.45811(2) 0.69892(2) 0.01252(3) Uani d 1 . . Cl Cl1 0.60148(8) 0.33007(4) 0.74376(6) 0.02142(13) Uani d 1 . . Cl Cl2 0.78118(7) 0.49571(4) 0.77945(6) 0.01953(13) Uani d 1 . . Cl Cl3 0.29411(8) 0.41592(4) 0.62396(6) 0.01961(13) Uani d 1 . . S S1 0.49553(7) 0.58842(4) 0.64406(6) 0.01545(12) Uani d 1 . . P P1 0.29578(8) 0.63290(4) 0.71079(5) 0.01203(12) Uani d 1 . . C C1 0.2845(3) 0.61053(17) 0.8698(2) 0.0175(5) Uani d 1 . . C C2 0.3186(3) 0.73939(16) 0.6906(2) 0.0181(5) Uani d 1 . . H H2 0.225743 0.765191 0.723585 0.022 Uiso calc 1 . . C C3 0.1136(3) 0.59893(16) 0.6267(2) 0.0136(5) Uani d 1 . . H H3 0.086801 0.546807 0.659853 0.016 Uiso calc 1 . . C C11 0.1916(4) 0.6760(2) 0.9271(3) 0.0302(7) Uani d 1 . . H H11A 0.087035 0.681955 0.884754 0.045 Uiso calc 1 . . H H11B 0.250247 0.725398 0.924447 0.045 Uiso calc 1 . . H H11C 0.178412 0.662105 1.008626 0.045 Uiso calc 1 . . C C12 0.4522(3) 0.60526(18) 0.9316(2) 0.0210(6) Uani d 1 . . H H12A 0.444865 0.599219 1.015825 0.032 Uiso calc 1 . . H H12B 0.511144 0.653237 0.916622 0.032 Uiso calc 1 . . H H12C 0.507673 0.559959 0.901581 0.032 Uiso calc 1 . . C C13 0.2002(4) 0.53228(19) 0.8846(3) 0.0255(7) Uani d 1 . . H H13A 0.251077 0.491559 0.840353 0.038 Uiso calc 1 . . H H13B 0.088482 0.537125 0.855490 0.038 Uiso calc 1 . . H H13C 0.206934 0.517989 0.967533 0.038 Uiso calc 1 . . C C21 0.4686(4) 0.77242(18) 0.7570(3) 0.0269(7) Uani d 1 . . H H21A 0.562457 0.747474 0.728384 0.040 Uiso calc 1 . . H H21B 0.465404 0.761735 0.840654 0.040 Uiso calc 1 . . H H21C 0.473607 0.829162 0.744403 0.040 Uiso calc 1 . . C C22 0.3144(4) 0.76266(18) 0.5614(3) 0.0255(6) Uani d 1 . . H H22A 0.327366 0.819562 0.555111 0.038 Uiso calc 1 . . H H22B 0.212447 0.747082 0.521601 0.038 Uiso calc 1 . . H H22C 0.400784 0.736199 0.524910 0.038 Uiso calc 1 . . C C31 -0.0295(3) 0.65284(17) 0.6416(2) 0.0181(5) Uani d 1 . . H H31A -0.008746 0.704791 0.609683 0.027 Uiso calc 1 . . H H31B -0.046308 0.657606 0.724769 0.027 Uiso calc 1 . . H H31C -0.124461 0.630425 0.599796 0.027 Uiso calc 1 . . C C32 0.1375(3) 0.58531(16) 0.4971(2) 0.0165(5) Uani d 1 . . H H32A 0.038294 0.566233 0.456976 0.025 Uiso calc 1 . . H H32B 0.221306 0.546296 0.490133 0.025 Uiso calc 1 . . H H32C 0.168064 0.634707 0.461534 0.025 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Au1 0.01036(5) 0.01403(6) 0.01301(5) -0.00005(4) -0.00001(3) -0.00017(3) Cl1 0.0212(3) 0.0170(3) 0.0257(3) 0.0027(3) -0.0009(2) 0.0029(3) Cl2 0.0117(3) 0.0263(4) 0.0201(3) -0.0019(3) -0.0024(2) 0.0002(3) Cl3 0.0141(3) 0.0168(3) 0.0270(3) -0.0017(2) -0.0045(2) -0.0010(3) S1 0.0124(3) 0.0152(3) 0.0192(3) -0.0010(2) 0.0032(2) 0.0019(2) P1 0.0111(3) 0.0123(3) 0.0124(3) -0.0007(2) -0.0011(2) -0.0005(2) C1 0.0145(12) 0.0266(15) 0.0110(11) 0.0018(11) -0.0019(9) 0.0000(10) C2 0.0157(12) 0.0137(13) 0.0244(13) -0.0018(10) -0.0016(10) -0.0023(10) C3 0.0120(11) 0.0154(12) 0.0128(11) -0.0020(10) -0.0023(9) -0.0008(9) C11 0.0291(16) 0.045(2) 0.0170(13) 0.0155(15) 0.0014(11) -0.0051(13) C12 0.0196(13) 0.0261(15) 0.0165(12) 0.0013(12) -0.0041(10) -0.0012(11) C13 0.0257(15) 0.0347(18) 0.0157(13) -0.0060(13) -0.0006(11) 0.0074(12) C21 0.0222(15) 0.0180(14) 0.0392(17) -0.0055(12) -0.0059(12) -0.0050(13) C22 0.0287(16) 0.0194(15) 0.0284(15) -0.0054(13) 0.0026(12) 0.0058(12) C31 0.0119(12) 0.0204(14) 0.0214(13) 0.0011(11) -0.0020(9) -0.0029(10) C32 0.0185(13) 0.0181(13) 0.0124(11) -0.0003(11) -0.0026(9) -0.0005(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag Cl3 Au1 Cl2 . . 177.46(2) y Cl3 Au1 Cl1 . . 88.54(2) y Cl2 Au1 Cl1 . . 89.23(3) y Cl3 Au1 S1 . . 94.93(2) y Cl2 Au1 S1 . . 87.39(2) y Cl1 Au1 S1 . . 174.30(2) y P1 S1 Au1 . . 111.29(3) y C2 P1 C3 . . 109.58(12) y C2 P1 C1 . . 109.67(13) y C3 P1 C1 . . 109.94(12) y C2 P1 S1 . . 102.70(10) y C3 P1 S1 . . 111.45(9) y C1 P1 S1 . . 113.25(9) y C13 C1 C12 . . 108.6(2) ? C13 C1 C11 . . 109.1(3) ? C12 C1 C11 . . 109.1(2) ? C13 C1 P1 . . 110.25(18) ? C12 C1 P1 . . 110.19(19) ? C11 C1 P1 . . 109.59(19) ? C21 C2 C22 . . 109.9(2) ? C21 C2 P1 . . 113.0(2) ? C22 C2 P1 . . 112.4(2) ? C21 C2 H2 . . 107.0 ? C22 C2 H2 . . 107.0 ? P1 C2 H2 . . 107.0 ? C32 C3 C31 . . 111.2(2) ? C32 C3 P1 . . 112.74(18) ? C31 C3 P1 . . 112.65(18) ? C32 C3 H3 . . 106.6 ? C31 C3 H3 . . 106.6 ? P1 C3 H3 . . 106.6 ? C1 C11 H11A . . 109.5 ? C1 C11 H11B . . 109.5 ? H11A C11 H11B . . 109.5 ? C1 C11 H11C . . 109.5 ? H11A C11 H11C . . 109.5 ? H11B C11 H11C . . 109.5 ? C1 C12 H12A . . 109.5 ? C1 C12 H12B . . 109.5 ? H12A C12 H12B . . 109.5 ? C1 C12 H12C . . 109.5 ? H12A C12 H12C . . 109.5 ? H12B C12 H12C . . 109.5 ? C1 C13 H13A . . 109.5 ? C1 C13 H13B . . 109.5 ? H13A C13 H13B . . 109.5 ? C1 C13 H13C . . 109.5 ? H13A C13 H13C . . 109.5 ? H13B C13 H13C . . 109.5 ? C2 C21 H21A . . 109.5 ? C2 C21 H21B . . 109.5 ? H21A C21 H21B . . 109.5 ? C2 C21 H21C . . 109.5 ? H21A C21 H21C . . 109.5 ? H21B C21 H21C . . 109.5 ? C2 C22 H22A . . 109.5 ? C2 C22 H22B . . 109.5 ? H22A C22 H22B . . 109.5 ? C2 C22 H22C . . 109.5 ? H22A C22 H22C . . 109.5 ? H22B C22 H22C . . 109.5 ? C3 C31 H31A . . 109.5 ? C3 C31 H31B . . 109.5 ? H31A C31 H31B . . 109.5 ? C3 C31 H31C . . 109.5 ? H31A C31 H31C . . 109.5 ? H31B C31 H31C . . 109.5 ? C3 C32 H32A . . 109.5 ? C3 C32 H32B . . 109.5 ? H32A C32 H32B . . 109.5 ? C3 C32 H32C . . 109.5 ? H32A C32 H32C . . 109.5 ? H32B C32 H32C . . 109.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Au1 Cl3 . 2.2818(6) y Au1 Cl2 . 2.2837(6) y Au1 Cl1 . 2.2989(7) y Au1 S1 . 2.3294(7) y S1 P1 . 2.0538(9) y P1 C2 . 1.843(3) y P1 C3 . 1.845(2) y P1 C1 . 1.875(3) y C1 C13 . 1.529(4) ? C1 C12 . 1.537(4) ? C1 C11 . 1.542(4) ? C2 C21 . 1.534(4) ? C2 C22 . 1.534(4) ? C2 H2 . 1.0000 ? C3 C32 . 1.535(3) ? C3 C31 . 1.540(4) ? C3 H3 . 1.0000 ? C11 H11A . 0.9800 ? C11 H11B . 0.9800 ? C11 H11C . 0.9800 ? C12 H12A . 0.9800 ? C12 H12B . 0.9800 ? C12 H12C . 0.9800 ? C13 H13A . 0.9800 ? C13 H13B . 0.9800 ? C13 H13C . 0.9800 ? C21 H21A . 0.9800 ? C21 H21B . 0.9800 ? C21 H21C . 0.9800 ? C22 H22A . 0.9800 ? C22 H22B . 0.9800 ? C22 H22C . 0.9800 ? C31 H31A . 0.9800 ? C31 H31B . 0.9800 ? C31 H31C . 0.9800 ? C32 H32A . 0.9800 ? C32 H32B . 0.9800 ? C32 H32C . 0.9800 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C32 H32B Cl3 . 0.98 2.75 3.452(3) 129.5 yes C3 H3 Cl3 . 1.00 2.89 3.476(3) 118.3 yes C13 H13A Cl3 . 0.98 2.85 3.729(3) 149.9 yes C13 H13B Cl2 1_455 0.98 2.77 3.704(3) 160.3 yes C31 H31A Cl1 2_556 0.98 2.87 3.372(3) 112.9 yes C13 H13C Cl2 3_667 0.98 2.91 3.878(3) 170.1 yes C32 H32A Cl3 3_566 0.98 2.91 3.800(3) 152.3 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag Cl3 Au1 S1 P1 . . . . 56.17(4) y Cl2 Au1 S1 P1 . . . . -122.80(4) y Au1 S1 P1 C2 . . . . 165.31(9) y Au1 S1 P1 C3 . . . . -77.45(10) y Au1 S1 P1 C1 . . . . 47.12(11) y C2 P1 C1 C13 . . . . 156.8(2) ? C3 P1 C1 C13 . . . . 36.3(2) ? S1 P1 C1 C13 . . . . -89.1(2) ? C2 P1 C1 C12 . . . . -83.3(2) ? C3 P1 C1 C12 . . . . 156.11(19) ? S1 P1 C1 C12 . . . . 30.7(2) ? C2 P1 C1 C11 . . . . 36.8(2) ? C3 P1 C1 C11 . . . . -83.8(2) ? S1 P1 C1 C11 . . . . 150.83(18) ? C3 P1 C2 C21 . . . . -179.5(2) ? C1 P1 C2 C21 . . . . 59.7(2) ? S1 P1 C2 C21 . . . . -60.9(2) ? C3 P1 C2 C22 . . . . -54.4(2) ? C1 P1 C2 C22 . . . . -175.1(2) ? S1 P1 C2 C22 . . . . 64.2(2) ? C2 P1 C3 C32 . . . . 81.7(2) ? C1 P1 C3 C32 . . . . -157.68(19) ? S1 P1 C3 C32 . . . . -31.3(2) ? C2 P1 C3 C31 . . . . -45.2(2) ? C1 P1 C3 C31 . . . . 75.4(2) ? S1 P1 C3 C31 . . . . -158.18(16) ?