#------------------------------------------------------------------------------
#$Date: 2024-05-06 06:19:48 +0200 (Mon, 06 May 2024) $
#$Revision: 291718 $
#$URL: svn://www.crystallography.net/cod/cif/2/02/30/2023046.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2023046
loop_
_publ_author_name
'Hubin, Daniel J.'
'Cunningham, Blue M.'
'Hubin, Timothy J.'
'Ebel, Jonathan P.'
'Krause, Jeanette A.'
'Oliver, Allen G.'
_publ_section_title
;
The unanti-cipated oxidation of a tertiary amine in a tetra-cyclic
glyoxal-cyclam condensate yielding zinc(II) coordinated to a sterically
hindered amine oxide.
;
_journal_coeditor_code PK2704
_journal_issue 'Pt 4'
_journal_name_full
'Acta crystallographica. Section E, Crystallographic communications'
_journal_page_first 343
_journal_page_last 346
_journal_paper_doi 10.1107/S2056989024001889
_journal_volume 80
_journal_year 2024
_chemical_formula_iupac '[Zn Cl3 (C12 H23 N4 O)], H2 O'
_chemical_formula_moiety 'C12 H23 Cl3 N4 O Zn, H2 O'
_chemical_formula_sum 'C12 H25 Cl3 N4 O2 Zn'
_chemical_formula_weight 429.08
_chemical_name_systematic
;
Trichlorido(1,4,11-triaza-8-azoniatetracyclo[6.6.2.0^4,16^.0^11,15^]hexadecane
1-oxide-\kO)zinc(II) monohydrate
;
_space_group_crystal_system monoclinic
_space_group_IT_number 14
_space_group_name_Hall '-P 2yn'
_space_group_name_H-M_alt 'P 1 21/n 1'
_atom_sites_solution_hydrogens mixed
_atom_sites_solution_primary dual
_atom_sites_solution_secondary difmap
_audit_creation_method SHELXL-2019/3
_cell_angle_alpha 90
_cell_angle_beta 104.760(2)
_cell_angle_gamma 90
_cell_formula_units_Z 4
_cell_length_a 8.7253(8)
_cell_length_b 14.3482(14)
_cell_length_c 14.0718(13)
_cell_measurement_reflns_used 8725
_cell_measurement_temperature 120(2)
_cell_measurement_theta_max 28.13
_cell_measurement_theta_min 2.50
_cell_volume 1703.5(3)
_computing_cell_refinement
;
SAINT V8.40B (Bruker, 2021)
;
_computing_data_collection
;
APEX-4 (Bruker, 2021)
;
_computing_data_reduction
;
SAINT V8.40B (Bruker, 2021)
;
_computing_molecular_graphics
;
Olex2 1.5 (Dolomanov et al., 2009), Mercury (Macrae et
al.,
2020)
;
_computing_publication_material
;
Olex2 1.5 (Dolomanov et al., 2009) and PublCIF (Westrip,
2010)
;
_computing_structure_refinement
;
SHELXL2019/2 (Sheldrick, 2015b)
;
_computing_structure_solution
;
SHELXT2014/5 (Sheldrick, 2015a)
;
_diffrn_ambient_temperature 120(2)
_diffrn_detector_area_resol_mean 8.33
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type 'Bruker APEXII CCD'
_diffrn_measurement_method '\f and \w scans'
_diffrn_radiation_type MoK\a
_diffrn_radiation_wavelength 0.71073
_diffrn_reflns_av_R_equivalents 0.0437
_diffrn_reflns_av_unetI/netI 0.0248
_diffrn_reflns_limit_h_max 11
_diffrn_reflns_limit_h_min -11
_diffrn_reflns_limit_k_max 19
_diffrn_reflns_limit_k_min -19
_diffrn_reflns_limit_l_max 18
_diffrn_reflns_limit_l_min -18
_diffrn_reflns_number 32386
_diffrn_reflns_theta_full 25.242
_diffrn_reflns_theta_max 28.311
_diffrn_reflns_theta_min 2.063
_diffrn_source X-ray
_exptl_absorpt_coefficient_mu 1.923
_exptl_absorpt_correction_T_max 0.7925
_exptl_absorpt_correction_T_min 0.6991
_exptl_absorpt_correction_type numerical
_exptl_absorpt_process_details
;
(SADABS; Krause et al., 2015)
;
_exptl_crystal_colour colorless
_exptl_crystal_density_diffrn 1.673
_exptl_crystal_description block
_exptl_crystal_F_000 888
_exptl_crystal_size_max 0.214
_exptl_crystal_size_mid 0.116
_exptl_crystal_size_min 0.089
_refine_diff_density_max 0.416
_refine_diff_density_min -0.328
_refine_ls_extinction_method none
_refine_ls_goodness_of_fit_ref 1.012
_refine_ls_hydrogen_treatment mixed
_refine_ls_matrix_type full
_refine_ls_number_parameters 220
_refine_ls_number_reflns 4237
_refine_ls_number_restraints 3
_refine_ls_restrained_S_all 1.012
_refine_ls_R_factor_all 0.0335
_refine_ls_R_factor_gt 0.0237
_refine_ls_shift/su_max 0.002
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0244P)^2^+0.8924P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.0522
_refine_ls_wR_factor_ref 0.0556
_reflns_number_gt 3572
_reflns_number_total 4237
_reflns_threshold_expression 'I > 2\s(I)'
_cod_data_source_file pk2704.cif
_cod_data_source_block I
_cod_depositor_comments 'Adding full bibliography for 2023046.cif.'
_cod_original_sg_symbol_H-M 'P 21/n'
_cod_database_code 2023046
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min 0.684
_shelx_estimated_absorpt_t_max 0.847
_shelx_hkl_file
;
1 0 0 1.10 1.10
1 0 0 0.30 1.00
1 0 0 -0.60 0.90
1 0 0 0.30 0.70
1 0 0 -0.20 0.80
-1 0 0 0.40 0.80
2 0 0 582.04 11.20
2 0 0 580.94 11.10
2 0 0 561.34 12.00
2 0 0 582.94 12.30
2 0 0 586.74 11.60
-2 0 0 591.44 11.00
3 0 0 2.70 1.80
3 0 0 -0.30 1.70
3 0 0 -0.50 2.30
3 0 0 -2.20 1.90
3 0 0 0.50 2.30
4 0 0 760.22 16.40
4 0 0 762.92 17.50
4 0 0 749.23 15.70
4 0 0 728.73 17.60
4 0 0 734.03 15.40
5 0 0 -0.10 2.90
5 0 0 -0.30 1.90
5 0 0 -1.00 3.10
5 0 0 4.00 2.70
5 0 0 0.00 2.00
6 0 0 112.59 6.20
6 0 0 105.79 7.70
6 0 0 111.39 8.20
6 0 0 114.79 7.00
6 0 0 109.69 6.10
7 0 0 2.70 4.70
7 0 0 -2.70 2.50
7 0 0 2.20 3.30
7 0 0 -1.20 3.70
7 0 0 -0.90 2.60
-7 0 0 -3.10 2.70
8 0 0 943.61 26.60
8 0 0 947.01 24.50
8 0 0 968.60 27.10
9 0 0 0.60 5.40
9 0 0 -3.60 3.80
9 0 0 8.70 6.80
10 0 0 214.68 16.50
10 0 0 243.88 15.70
10 0 0 255.47 13.50
11 0 0 7.00 6.80
11 0 0 -6.10 7.30
11 0 -1 377.26 19.90
11 0 -1 288.47 19.90
10 0 -1 -4.70 7.00
10 0 -1 -2.30 5.60
9 0 -1 75.99 7.80
9 0 -1 89.59 10.40
9 0 -1 74.39 9.60
8 0 -1 -3.40 4.80
8 0 -1 1.60 5.30
8 0 -1 0.20 3.20
-7 0 1 259.17 9.40
7 0 -1 268.57 10.70
7 0 -1 255.07 12.40
7 0 -1 261.07 9.10
7 0 -1 242.08 11.70
7 0 -1 230.28 9.70
-6 0 1 0.90 2.20
6 0 -1 0.70 3.80
6 0 -1 -2.00 2.30
6 0 -1 -0.40 3.10
6 0 -1 0.70 1.90
6 0 -1 0.00 2.60
5 0 -1 69.79 4.90
5 0 -1 62.79 5.00
5 0 -1 63.19 4.10
5 0 -1 78.09 6.70
5 0 -1 70.99 6.40
-4 0 1 -1.70 1.80
4 0 -1 -0.60 1.50
4 0 -1 2.40 2.20
4 0 -1 1.60 2.80
4 0 -1 -1.30 2.00
4 0 -1 2.70 2.80
-3 0 1 5958.00 96.59
3 0 -1 5764.32 93.39
3 0 -1 5703.33 91.69
3 0 -1 5698.03 93.29
3 0 -1 5746.33 92.19
3 0 -1 5796.52 93.29
-2 0 1 -0.80 1.60
2 0 -1 0.00 1.00
2 0 -1 2.20 1.90
2 0 -1 0.50 1.50
2 0 -1 1.60 2.10
2 0 -1 -1.10 1.70
-1 0 1 119.19 3.50
1 0 -1 116.29 3.60
1 0 -1 114.79 2.80
1 0 -1 121.29 3.40
0 0 1 2.90 0.60
0 0 1 1.80 0.60
0 0 1 2.90 0.60
0 0 1 2.60 0.70
0 0 1 1.90 0.60
1 0 1 1147.09 20.30
1 0 1 1218.38 20.40
1 0 1 1174.38 19.90
1 0 1 1170.18 18.70
1 0 1 1214.18 20.20
2 0 1 0.60 1.10
2 0 1 2.40 2.10
2 0 1 0.30 1.90
2 0 1 1.60 1.80
2 0 1 -0.90 2.00
3 0 1 1750.02 30.90
3 0 1 1714.43 31.20
3 0 1 1658.93 28.80
3 0 1 1714.23 31.80
3 0 1 1773.32 31.10
4 0 1 2.40 1.70
4 0 1 1.00 2.10
4 0 1 0.10 3.10
4 0 1 -3.50 2.80
4 0 1 -0.50 2.30
5 0 1 742.13 19.20
5 0 1 694.23 15.20
5 0 1 721.43 17.10
5 0 1 727.93 18.40
5 0 1 766.12 17.90
6 0 1 0.70 2.20
6 0 1 1.30 2.60
6 0 1 -3.50 2.70
6 0 1 -4.00 3.70
6 0 1 -2.20 3.20
7 0 1 1169.68 27.20
7 0 1 1125.09 25.80
7 0 1 1148.49 29.20
7 0 1 1178.68 28.60
-7 0 -1 1150.98 26.70
8 0 1 -0.20 4.90
8 0 1 -1.30 5.70
8 0 1 -4.60 3.40
9 0 1 -2.60 4.10
9 0 1 14.10 6.60
9 0 1 -0.90 6.00
10 0 1 11.00 6.70
10 0 1 12.10 7.20
10 0 1 5.60 4.90
11 0 1 247.78 17.30
11 0 -2 7.30 6.50
11 0 -2 -19.00 6.80
10 0 -2 15.60 6.70
10 0 -2 -8.40 6.30
9 0 -2 1.80 3.70
9 0 -2 3.40 6.10
9 0 -2 -1.60 5.20
8 0 -2 720.23 19.50
8 0 -2 727.83 22.70
8 0 -2 774.02 23.30
8 0 -2 724.63 19.80
7 0 -2 4.60 4.50
7 0 -2 0.50 4.30
7 0 -2 -3.20 2.80
7 0 -2 3.60 2.90
-6 0 2 187.68 6.70
6 0 -2 208.98 8.30
6 0 -2 191.68 9.70
6 0 -2 194.78 6.50
6 0 -2 205.48 10.20
6 0 -2 199.48 8.50
-5 0 2 0.30 2.20
-5 0 2 -0.40 1.50
5 0 -2 0.40 1.40
5 0 -2 -2.50 2.70
5 0 -2 -1.90 2.30
5 0 -2 -1.40 2.00
5 0 -2 -2.20 3.20
-4 0 2 518.05 10.30
-4 0 2 522.45 12.80
4 0 -2 529.75 13.90
4 0 -2 515.85 13.80
4 0 -2 516.55 10.10
4 0 -2 496.05 11.80
4 0 -2 521.25 13.00
-3 0 2 0.50 2.10
-3 0 2 1.00 1.00
3 0 -2 0.60 0.90
3 0 -2 0.00 1.70
3 0 -2 0.30 2.40
3 0 -2 -0.40 2.10
3 0 -2 1.40 2.40
-2 0 2 387.56 9.10
2 0 -2 378.46 9.10
2 0 -2 383.86 9.50
2 0 -2 374.56 7.80
2 0 -2 374.16 9.00
-1 0 2 1.00 0.80
-1 0 2 0.70 1.60
-1 0 2 -0.20 1.40
1 0 -2 -0.20 0.90
1 0 -2 -0.30 1.30
1 0 -2 -0.30 1.20
0 0 2 5563.54 93.49
0 0 2 5427.96 90.49
0 0 2 5456.85 90.79
0 0 2 5610.34 89.49
0 0 2 5463.55 90.99
1 0 2 -2.00 1.50
1 0 2 1.60 1.70
1 0 2 0.40 1.70
1 0 2 1.10 1.70
1 0 2 0.50 0.70
2 0 2 635.64 10.80
2 0 2 621.84 13.20
2 0 2 670.03 14.10
2 0 2 644.34 13.70
2 0 2 624.04 13.90
3 0 2 0.60 2.00
3 0 2 -1.40 2.30
3 0 2 -1.60 2.00
3 0 2 3.90 2.80
3 0 2 1.80 1.40
4 0 2 2143.19 40.60
4 0 2 2092.29 35.70
4 0 2 2183.28 39.70
4 0 2 2178.58 39.70
4 0 2 2182.68 39.70
5 0 2 -1.10 1.80
5 0 2 -0.70 3.30
5 0 2 4.60 2.90
5 0 2 0.50 3.60
5 0 2 -3.10 2.40
6 0 2 43.50 6.30
6 0 2 52.19 5.80
6 0 2 45.20 6.40
7 0 2 1.40 3.40
7 0 2 1.40 4.10
7 0 2 -1.10 4.70
7 0 2 -1.30 3.50
8 0 2 754.12 23.90
8 0 2 687.33 20.30
8 0 2 733.43 22.60
8 0 2 696.63 21.40
-8 0 -2 727.43 21.40
9 0 2 -1.00 5.10
9 0 2 3.00 5.70
9 0 2 1.40 4.30
10 0 2 85.39 11.50
10 0 2 55.39 8.40
10 0 2 55.69 9.50
11 0 -3 335.67 18.30
11 0 -3 383.26 20.80
10 0 -3 -3.20 5.30
10 0 -3 -7.10 5.80
9 0 -3 -2.70 5.60
9 0 -3 1.40 4.80
9 0 -3 1.00 3.90
9 0 -3 -3.60 3.70
8 0 -3 1.50 5.10
8 0 -3 0.80 5.00
8 0 -3 -5.60 2.80
8 0 -3 2.30 3.50
7 0 -3 31.50 4.30
7 0 -3 22.10 5.60
7 0 -3 25.30 6.20
7 0 -3 25.00 4.70
-6 0 3 1.10 1.40
6 0 -3 -0.40 2.20
6 0 -3 2.50 3.90
6 0 -3 4.10 3.10
6 0 -3 -1.00 3.60
-5 0 3 133.09 6.90
-5 0 3 110.19 3.60
5 0 -3 138.09 7.90
5 0 -3 125.19 6.90
5 0 -3 130.39 7.40
5 0 -3 116.99 5.60
-4 0 3 -1.40 2.20
4 0 -3 -0.80 2.80
4 0 -3 1.00 1.90
4 0 -3 2.70 2.90
4 0 -3 0.10 2.40
-3 0 3 936.21 19.50
3 0 -3 1001.40 19.80
3 0 -3 959.30 19.90
3 0 -3 975.10 17.60
3 0 -3 951.50 20.20
-2 0 3 -3.00 1.90
-2 0 3 0.20 0.80
2 0 -3 -1.10 1.30
2 0 -3 -0.50 2.00
2 0 -3 -0.10 2.00
2 0 -3 -0.10 1.70
-1 0 3 1411.66 24.20
-1 0 3 1383.06 23.60
-1 0 3 1390.56 24.60
-1 0 3 1400.26 23.50
-1 0 3 1392.76 24.70
1 0 -3 1414.16 23.50
1 0 -3 1453.35 24.80
1 0 -3 1422.16 24.30
0 0 3 1.50 1.80
0 0 3 1.00 1.70
0 0 3 2.70 1.80
0 0 3 3.40 1.50
0 0 3 -1.70 1.60
1 0 3 118.19 5.00
1 0 3 113.69 5.00
1 0 3 119.29 4.40
1 0 3 116.99 3.20
1 0 3 118.79 5.50
2 0 3 0.10 0.70
2 0 3 2.40 2.00
2 0 3 1.90 2.20
2 0 3 -1.20 2.00
2 0 3 -5.70 2.10
3 0 3 411.46 11.70
3 0 3 420.56 11.90
3 0 3 379.46 7.20
3 0 3 403.26 11.40
3 0 3 392.16 10.80
4 0 3 0.10 2.70
4 0 3 3.00 2.70
4 0 3 -5.00 2.90
4 0 3 1.00 1.40
4 0 3 0.40 2.70
5 0 3 616.04 16.70
5 0 3 604.94 17.80
5 0 3 610.24 16.90
5 0 3 586.44 12.00
5 0 3 618.84 16.60
6 0 3 2.90 3.60
6 0 3 -5.20 3.90
6 0 3 -1.80 3.10
6 0 3 0.50 3.50
7 0 3 830.32 24.30
7 0 3 832.62 22.50
7 0 3 782.72 22.30
7 0 3 826.22 23.00
8 0 3 2.40 4.00
8 0 3 -5.40 3.80
8 0 3 10.30 5.90
8 0 3 -1.70 4.60
-8 0 -3 1.70 4.20
9 0 3 111.09 11.80
9 0 3 97.09 9.90
9 0 3 133.39 11.40
10 0 3 -4.40 4.80
10 0 3 -0.60 6.00
11 0 -4 5.70 6.30
11 0 -4 -11.60 7.00
10 0 -4 -7.80 5.60
10 0 -4 2.10 5.80
9 0 -4 0.30 4.00
9 0 -4 -3.50 4.60
9 0 -4 10.10 5.50
8 0 -4 487.65 17.00
8 0 -4 517.85 18.80
8 0 -4 519.75 19.20
8 0 -4 503.25 14.80
7 0 -4 -0.90 3.80
7 0 -4 0.90 2.60
7 0 -4 0.50 3.30
7 0 -4 0.00 3.80
-6 0 4 27.90 4.50
6 0 -4 30.80 5.50
6 0 -4 37.20 3.90
6 0 -4 26.50 5.00
6 0 -4 32.40 4.90
-5 0 4 -1.30 2.20
5 0 -4 1.10 2.90
5 0 -4 1.60 3.20
5 0 -4 -4.30 2.90
5 0 -4 -1.10 1.90
-4 0 4 1691.53 31.90
4 0 -4 1588.04 32.20
4 0 -4 1591.24 28.60
4 0 -4 1670.83 32.20
4 0 -4 1623.34 31.40
-3 0 4 0.40 2.20
3 0 -4 2.20 2.70
3 0 -4 -0.70 2.20
3 0 -4 -2.30 1.40
3 0 -4 -1.40 2.20
-2 0 4 468.65 9.20
-2 0 4 471.15 11.50
2 0 -4 481.85 11.20
2 0 -4 478.45 9.70
2 0 -4 483.15 11.70
-1 0 4 2.90 1.70
-1 0 4 -1.10 1.60
-1 0 4 4.00 2.30
-1 0 4 -1.50 1.90
-1 0 4 1.10 2.00
1 0 -4 -1.10 1.90
1 0 -4 -0.60 1.80
0 0 4 355.36 8.80
0 0 4 347.37 8.50
0 0 4 360.16 8.70
0 0 4 337.77 8.10
1 0 4 1.30 2.30
1 0 4 0.50 2.30
1 0 4 0.50 1.20
1 0 4 0.00 1.80
1 0 4 -0.90 2.00
2 0 4 389.56 11.40
2 0 4 378.46 7.00
2 0 4 378.86 10.80
2 0 4 383.46 9.70
2 0 4 380.26 10.90
3 0 4 -0.10 2.40
3 0 4 -0.30 2.80
3 0 4 0.50 2.60
3 0 4 0.90 2.70
4 0 4 1978.50 36.80
4 0 4 1961.80 38.80
4 0 4 2007.70 38.90
4 0 4 1893.51 37.90
5 0 4 5.70 3.80
5 0 4 -0.80 3.10
5 0 4 1.60 3.20
5 0 4 -1.10 3.30
6 0 4 49.70 6.50
6 0 4 41.00 5.90
6 0 4 52.29 6.90
6 0 4 56.29 6.90
7 0 4 -2.30 4.00
7 0 4 1.20 3.90
7 0 4 6.30 4.40
7 0 4 4.00 4.90
8 0 4 179.78 13.10
8 0 4 162.38 11.30
8 0 4 162.38 10.80
8 0 4 172.48 11.30
-8 0 -4 171.88 11.60
9 0 4 2.00 6.00
9 0 4 -4.30 4.60
10 0 4 11.50 6.10
10 0 4 14.10 7.40
11 0 -5 207.18 15.20
11 0 -5 233.18 17.20
10 0 -5 0.50 4.80
10 0 -5 3.40 5.90
10 0 -5 0.10 6.20
9 0 -5 129.39 11.60
9 0 -5 96.99 9.30
9 0 -5 128.49 11.40
8 0 -5 2.80 4.00
8 0 -5 1.40 3.70
8 0 -5 6.70 5.30
8 0 -5 2.80 5.20
-7 0 5 939.41 23.70
7 0 -5 947.11 25.10
7 0 -5 953.70 24.40
7 0 -5 945.81 25.60
7 0 -5 942.11 20.70
-6 0 5 0.50 2.70
6 0 -5 2.90 3.40
6 0 -5 1.60 2.10
6 0 -5 0.00 3.30
6 0 -5 1.50 3.70
-5 0 5 891.91 21.00
5 0 -5 830.32 21.40
5 0 -5 864.31 21.00
5 0 -5 844.92 17.40
5 0 -5 837.12 20.40
-4 0 5 -0.10 2.50
4 0 -5 -0.90 1.90
4 0 -5 -0.90 2.60
4 0 -5 -0.90 2.40
4 0 -5 -0.70 2.50
-3 0 5 71.59 2.70
-3 0 5 85.49 5.40
3 0 -5 73.89 5.50
3 0 -5 73.19 2.80
3 0 -5 69.19 4.70
3 0 -5 74.69 5.70
3 0 -5 72.59 3.70
-2 0 5 -0.50 1.50
-2 0 5 -1.20 1.50
-2 0 5 0.60 2.10
-2 0 5 3.10 2.40
2 0 -5 0.20 2.00
2 0 -5 1.00 1.60
2 0 -5 -1.00 1.90
-1 0 5 546.25 12.50
-1 0 5 565.64 12.70
-1 0 5 566.64 12.90
-1 0 5 577.64 12.10
-1 0 5 554.74 12.90
0 0 5 -0.50 1.90
0 0 5 1.00 2.30
0 0 5 0.20 1.70
0 0 5 0.60 2.20
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2 -1 -1 801.72 15.30
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1 -1 -1 1571.04 25.70
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-3 -1 -1 17.00 1.80
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8 1 1 79.19 10.70
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11 -1 -2 -11.10 7.70
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2 -1 -2 1321.37 23.30
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-1 1 2 200.28 5.40
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1 -1 -2 191.98 5.30
1 -1 -2 195.58 4.50
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1 -2 7 7.60 3.40
1 -2 7 5.50 3.20
1 -2 7 8.40 2.50
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6 -3 8 394.26 17.20
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5 -3 8 0.30 5.10
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4 -3 8 183.68 11.00
4 -3 8 201.58 10.60
4 -3 8 170.68 10.90
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3 -3 8 258.67 12.00
3 -3 8 253.17 9.50
3 -3 8 274.07 11.60
3 -3 8 248.68 12.60
3 -3 8 254.57 11.90
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1 -3 8 75.89 6.90
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7 -3 7 40.50 8.20
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3 -3 7 8.20 3.90
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3 -3 7 17.50 4.70
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-3 -3 7 126.59 7.70
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4 -3 6 238.88 10.80
4 -3 6 228.08 7.40
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3 -3 6 449.46 14.10
3 -3 6 418.26 13.70
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2 -3 6 963.90 22.20
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2 -3 6 952.70 22.80
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1 -3 6 46.70 4.10
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4 -3 5 116.69 5.40
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3 -3 5 21.70 4.30
3 -3 5 20.80 4.30
3 -3 5 19.10 2.80
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2 -3 5 16.50 3.60
2 -3 5 16.20 3.50
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1 -3 5 45.40 4.80
1 -3 5 44.70 4.90
1 -3 5 32.20 3.80
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6 -3 4 195.98 11.20
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5 -3 4 7.80 4.00
5 -3 4 6.10 4.00
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4 -3 4 70.99 7.10
4 -3 4 74.89 6.90
4 -3 4 68.19 6.70
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3 -3 4 136.09 7.00
3 -3 4 163.48 8.20
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3 -3 4 160.88 8.10
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4 -3 3 31.60 3.60
4 -3 3 30.00 4.10
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3 -3 3 1185.58 22.90
3 -3 3 1194.78 25.30
3 -3 3 1231.88 25.70
3 -3 3 1206.48 25.50
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0 -18 4 203.28 15.70
1 18 -4 -11.80 6.70
1 18 -4 -7.50 6.00
-1 -18 4 1.20 6.70
-1 -18 4 0.70 5.90
2 18 -4 0.90 7.10
2 18 -4 13.80 8.50
-2 -18 4 -0.40 6.60
3 18 -4 205.18 16.90
3 18 -4 214.78 17.40
-3 -18 4 239.28 17.40
-2 18 -3 3.70 5.80
-2 18 -3 -10.40 7.50
2 -18 3 1.40 6.30
2 -18 3 0.50 6.00
-1 18 -3 47.30 9.00
-1 18 -3 32.60 10.30
1 -18 3 60.19 10.70
1 -18 3 33.70 8.60
0 18 -3 32.80 8.30
0 18 -3 57.89 11.40
0 -18 3 57.29 10.40
0 -18 3 54.19 9.40
1 18 -3 17.60 7.90
1 18 -3 10.50 7.30
-1 -18 3 24.70 7.80
2 18 -3 11.00 8.00
2 18 -3 8.70 7.30
-2 -18 3 1.30 7.00
3 18 -3 -3.00 7.30
3 18 -3 -8.50 6.30
-3 -18 3 -5.30 5.70
-3 18 -2 1.00 8.10
3 -18 2 4.00 6.40
3 -18 2 -2.80 5.80
-2 18 -2 62.79 11.30
2 -18 2 39.20 9.30
2 -18 2 53.09 9.60
-1 18 -2 9.80 8.60
-1 18 -2 2.70 6.20
1 -18 2 6.90 6.10
1 -18 2 -6.10 5.90
0 18 -2 246.88 15.60
0 18 -2 232.58 18.30
0 -18 2 258.57 17.70
0 -18 2 248.58 22.80
1 18 -2 74.19 10.60
1 18 -2 64.19 11.80
-1 -18 2 64.39 10.80
2 18 -2 0.20 6.80
2 18 -2 11.10 8.00
-2 -18 2 12.50 7.50
3 18 -2 110.89 12.90
3 18 -2 112.09 13.60
-3 -18 2 125.99 13.80
-3 18 -1 44.70 10.80
3 -18 1 55.59 10.60
3 -18 1 36.30 8.70
-2 18 -1 34.80 10.40
2 -18 1 52.49 9.40
2 -18 1 41.20 8.90
-1 18 -1 11.80 6.70
-1 18 -1 24.20 8.60
1 -18 1 29.20 8.70
1 -18 1 16.20 7.30
0 18 -1 39.80 9.90
0 18 -1 28.30 7.80
0 -18 1 37.60 9.30
1 18 -1 39.90 9.90
1 18 -1 31.60 8.30
-1 -18 1 31.70 8.70
2 18 -1 17.60 8.00
2 18 -1 2.60 6.90
-2 -18 1 7.60 6.70
3 18 -1 61.79 10.90
3 18 -1 48.00 9.80
-3 -18 1 61.89 10.70
-3 18 0 -1.20 7.40
3 -18 0 -1.00 5.70
3 -18 0 4.60 6.40
-2 18 0 2.20 7.90
2 -18 0 8.80 7.30
2 -18 0 8.40 6.60
-1 18 0 14.90 7.70
1 -18 0 17.10 7.50
0 18 0 134.29 14.50
0 18 0 148.09 13.10
0 -18 0 174.58 15.80
1 18 0 7.80 7.80
1 18 0 -11.10 5.90
-1 -18 0 8.80 6.20
2 18 0 8.80 7.50
2 18 0 0.40 6.70
-2 -18 0 -0.70 6.00
3 18 0 -4.50 6.10
3 18 0 -3.10 6.20
-3 -18 0 11.30 7.20
-3 18 1 45.40 10.60
3 -18 -1 52.99 10.10
3 -18 -1 57.19 10.50
-2 18 1 6.80 7.60
2 -18 -1 15.50 6.90
-1 18 1 31.00 9.40
1 -18 -1 44.70 9.70
0 18 1 51.59 10.60
0 18 1 32.70 8.10
0 -18 -1 52.69 10.30
1 18 1 21.90 8.70
1 18 1 2.70 6.30
-1 -18 -1 19.40 7.70
2 18 1 35.60 8.10
2 18 1 32.20 9.40
-2 -18 -1 44.10 9.20
3 18 1 59.99 9.70
3 18 1 58.19 10.80
-3 -18 -1 64.69 10.50
-3 18 2 140.19 15.20
3 -18 -2 146.69 14.80
-2 18 2 2.90 7.30
2 -18 -2 10.40 6.20
-1 18 2 63.49 11.60
1 -18 -2 73.29 10.80
0 18 2 248.88 17.20
0 -18 -2 262.47 16.90
1 18 2 3.40 5.70
1 18 2 13.00 7.50
-1 -18 -2 4.40 6.20
2 18 2 53.89 9.00
2 18 2 63.29 11.30
-2 -18 -2 62.49 10.20
3 18 2 2.80 6.80
3 18 2 3.60 6.10
-3 -18 -2 1.70 6.20
-3 18 3 -0.10 7.30
3 -18 -3 17.20 7.40
-2 18 3 11.30 7.60
2 -18 -3 14.60 7.30
-1 18 3 20.00 8.30
1 -18 -3 21.10 7.70
0 18 3 67.49 11.40
0 -18 -3 77.99 10.90
1 18 3 38.10 8.10
1 18 3 64.19 11.40
-1 -18 -3 63.49 10.00
2 18 3 2.40 6.70
2 18 3 -1.00 5.60
-2 -18 -3 5.20 6.30
-3 18 4 206.58 17.90
3 -18 -4 257.47 17.20
-2 18 4 6.10 6.80
2 -18 -4 27.10 8.10
-1 18 4 4.70 7.10
1 -18 -4 10.50 6.40
0 18 4 220.28 17.30
0 -18 -4 230.48 16.10
1 18 4 110.39 13.30
-1 -18 -4 106.89 12.50
2 18 4 12.80 7.80
2 18 4 22.10 7.00
-2 -18 -4 11.70 6.70
-3 18 5 7.50 7.00
3 -18 -5 23.40 7.80
-2 18 5 89.49 12.30
2 -18 -5 102.99 12.60
-1 18 5 46.60 9.80
1 -18 -5 61.69 10.10
0 18 5 28.50 8.40
0 -18 -5 16.00 6.90
1 18 5 31.00 9.40
-1 -18 -5 48.20 9.20
-2 18 6 9.60 7.20
2 -18 -6 10.00 6.40
-1 18 6 45.50 10.00
1 -18 -6 61.39 10.40
0 18 6 43.80 10.10
0 -18 -6 70.89 10.60
0 19 -2 60.29 12.00
0 -19 2 65.49 11.30
1 -19 1 26.70 9.00
0 19 -1 -7.00 7.50
0 19 -1 -6.80 6.00
0 -19 1 1.80 7.00
1 19 -1 1.90 7.60
1 19 -1 -0.40 7.10
-1 -19 1 3.20 7.30
-1 19 0 34.50 10.80
1 -19 0 46.60 10.50
0 19 0 0.00 7.50
0 19 0 -11.40 6.10
0 -19 0 14.60 7.80
1 19 0 52.49 10.70
1 19 0 43.00 9.40
-1 -19 0 39.10 9.20
-1 19 1 17.30 9.00
1 -19 -1 12.00 7.80
0 19 1 4.90 7.40
0 -19 -1 3.70 6.10
-1 -19 -1 20.40 8.00
0 -19 -2 75.79 11.60
0 0 0 0.00 0.00
_computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)'
;
_shelx_hkl_checksum 7033
_shelx_res_file
;
TITL djh46bp21n_a.res in P2(1)/n
i.res
created by SHELXL-2019/3 at 11:55:14 on 25-Feb-2024
REM Old TITL DJH46B P21n in P2(1)/n
REM SHELXT solution in P2(1)/n
REM R1 0.089, Rweak 0.005, Alpha 0.027, Orientation as input
REM Formula found by SHELXT: C12 N5 O Cl3 Zn
CELL 0.71073 8.7253 14.3482 14.0718 90 104.76 90
ZERR 4 0.0008 0.0014 0.0013 0 0.002 0
LATT 1
SYMM 0.5-X,0.5+Y,0.5-Z
SFAC C H Cl N O Zn
UNIT 48 100 12 16 8 4
L.S. 5 0 0
PLAN 5
SIZE 0.089 0.116 0.214
TEMP -153.14
CONF
BOND $H
MORE -1
FMAP 2
ACTA
SADI 0.01 O2 H2C O2 H2D O2A H2E O2 H2F
HTAB N3 O1
HTAB N3 O2
HTAB N3 O2A
HTAB O2 Cl2_$4
EQIV $8 -x+3/2, y-1/2, -z+3/2
HTAB O2 N4_$8
HTAB O2 Cl1
HTAB O2A Cl2_$4
HTAB O2A N4_$8
HTAB O2A Cl1
HTAB C1 Cl2
EQIV $1 x-1/2, -y+3/2, z-1/2
HTAB C2 Cl3_$1
EQIV $2 -x+1, -y+2, -z+1
HTAB C3 N2_$2
EQIV $3 x+1/2, -y+3/2, z-1/2
HTAB C4 Cl2_$3
EQIV $4 x+1, y, z
HTAB C5 Cl2_$4
EQIV $5 -x+3/2, y+1/2, -z+3/2
HTAB C5 Cl3_$5
HTAB C6 Cl1_$5
HTAB C6 Cl2_$4
HTAB C7 O1
EQIV $6 -x+1/2, y+1/2, -z+3/2
HTAB C8 Cl2_$6
EQIV $7 x+1/2, -y+3/2, z+1/2
HTAB C8 Cl1_$7
HTAB C10 Cl2
HTAB C10 Cl1_$6
HTAB C12 Cl2_$6
WGHT 0.024400 0.892400
FVAR 0.33907
ZN1 6 0.383521 0.630730 0.741818 11.00000 0.01529 0.00965 =
0.01544 0.00082 0.00307 -0.00118
CL1 3 0.409273 0.542852 0.613360 11.00000 0.03014 0.02090 =
0.01797 -0.00187 0.00584 0.00448
CL2 3 0.117646 0.646101 0.726691 11.00000 0.01487 0.01714 =
0.02979 -0.00108 0.00600 -0.00291
CL3 3 0.505527 0.566141 0.885697 11.00000 0.03416 0.02013 =
0.01772 0.00485 0.00018 0.00302
O1 5 0.483785 0.754154 0.736224 11.00000 0.01342 0.00787 =
0.02095 0.00212 0.00339 0.00191
N1 4 0.402639 0.839223 0.722148 11.00000 0.01456 0.00845 =
0.01554 0.00029 0.00402 0.00172
N2 4 0.491266 0.889771 0.547782 11.00000 0.02169 0.01325 =
0.01317 0.00093 0.00555 0.00283
N3 4 0.732969 0.828439 0.664343 11.00000 0.01485 0.01123 =
0.01934 0.00103 0.00497 -0.00030
AFIX 13
H3 2 0.682588 0.767367 0.672505 11.00000 -1.20000
AFIX 0
N4 4 0.638929 0.925598 0.817841 11.00000 0.01910 0.01556 =
0.01478 -0.00113 0.00258 -0.00364
C1 1 0.284013 0.841232 0.624003 11.00000 0.01455 0.01528 =
0.01799 0.00077 -0.00039 0.00131
AFIX 23
H1A 2 0.200438 0.794152 0.622381 11.00000 -1.20000
H1B 2 0.233240 0.903358 0.612818 11.00000 -1.20000
AFIX 0
C2 1 0.366658 0.820714 0.545166 11.00000 0.02084 0.01691 =
0.01602 -0.00127 0.00057 0.00170
AFIX 23
H2A 2 0.413817 0.757581 0.555104 11.00000 -1.20000
H2B 2 0.289180 0.822203 0.480114 11.00000 -1.20000
AFIX 0
C3 1 0.568783 0.879614 0.467128 11.00000 0.03132 0.01802 =
0.01678 0.00178 0.01127 0.00724
AFIX 23
H3A 2 0.620783 0.939150 0.458245 11.00000 -1.20000
H3B 2 0.487426 0.866169 0.405469 11.00000 -1.20000
AFIX 0
C4 1 0.691917 0.801965 0.486206 11.00000 0.02925 0.01812 =
0.02187 0.00072 0.01171 0.00530
AFIX 23
H4A 2 0.639472 0.741237 0.489173 11.00000 -1.20000
H4B 2 0.745027 0.799462 0.431914 11.00000 -1.20000
AFIX 0
C5 1 0.813132 0.819989 0.582329 11.00000 0.02064 0.01823 =
0.02802 0.00106 0.01332 0.00215
AFIX 23
H5A 2 0.890506 0.768148 0.596338 11.00000 -1.20000
H5B 2 0.871458 0.878211 0.577319 11.00000 -1.20000
AFIX 0
C6 1 0.850223 0.852599 0.758659 11.00000 0.01399 0.01986 =
0.02444 -0.00090 0.00154 -0.00346
AFIX 23
H6A 2 0.900038 0.913375 0.751790 11.00000 -1.20000
H6B 2 0.934682 0.804743 0.773996 11.00000 -1.20000
AFIX 0
C7 1 0.769361 0.857766 0.840951 11.00000 0.01706 0.02062 =
0.02021 0.00094 -0.00104 -0.00392
AFIX 23
H7A 2 0.727310 0.795572 0.851407 11.00000 -1.20000
H7B 2 0.847102 0.876364 0.902397 11.00000 -1.20000
AFIX 0
C8 1 0.562095 0.938726 0.898878 11.00000 0.02974 0.01745 =
0.01492 -0.00187 0.00605 -0.00401
AFIX 23
H8A 2 0.507952 0.999931 0.891293 11.00000 -1.20000
H8B 2 0.644199 0.939192 0.962106 11.00000 -1.20000
AFIX 0
C9 1 0.442028 0.862394 0.901435 11.00000 0.02724 0.01721 =
0.01688 -0.00012 0.00893 -0.00146
AFIX 23
H9A 2 0.496925 0.801698 0.916110 11.00000 -1.20000
H9B 2 0.388001 0.875842 0.953828 11.00000 -1.20000
AFIX 0
C10 1 0.321149 0.857677 0.802776 11.00000 0.01860 0.01411 =
0.02171 -0.00109 0.01102 0.00145
AFIX 23
H10A 2 0.244040 0.807317 0.803837 11.00000 -1.20000
H10B 2 0.262410 0.917304 0.789926 11.00000 -1.20000
AFIX 0
C11 1 0.603674 0.903733 0.639971 11.00000 0.01810 0.00825 =
0.01763 0.00237 0.00522 0.00031
AFIX 13
H11 2 0.659039 0.963672 0.634126 11.00000 -1.20000
AFIX 0
C12 1 0.526420 0.916493 0.724687 11.00000 0.01788 0.00804 =
0.01676 0.00057 0.00482 -0.00214
AFIX 13
H12 2 0.466658 0.976619 0.712488 11.00000 -1.20000
AFIX 0
PART 1 10.5
O2 5 0.748842 0.639637 0.704214 10.50000 0.01969 0.01593 =
0.08359 -0.00028 0.01905 0.00256
H2C 2 0.815956 0.605451 0.683662 10.50000 -1.50000
H2D 2 0.670474 0.603648 0.676525 10.50000 -1.50000
PART 2 10.5
O2A 5 0.728023 0.634483 0.655049 10.50000 0.01801 0.01964 =
0.07889 0.00310 0.00652 0.00141
H2E 2 0.805543 0.618122 0.704289 10.50000 -1.50000
H2F 2 0.630525 0.597787 0.630700 10.50000 -1.50000
PART 0
HKLF 4
REM djh46bp21n_a.res in P2(1)/n
REM wR2 = 0.0556, GooF = S = 1.012, Restrained GooF = 1.012 for all data
REM R1 = 0.0237 for 3572 Fo > 4sig(Fo) and 0.0335 for all 4237 data
REM 220 parameters refined using 3 restraints
END
WGHT 0.0244 0.8924
REM Highest difference peak 0.416, deepest hole -0.328, 1-sigma level 0.063
Q1 1 0.4945 0.5690 0.6210 11.00000 0.05 0.42
Q2 1 0.6661 0.8642 0.6571 11.00000 0.05 0.35
Q3 1 0.5432 0.8896 0.5889 11.00000 0.05 0.35
Q4 1 0.4353 0.8550 0.5487 11.00000 0.05 0.34
Q5 1 0.3942 0.8512 0.8561 11.00000 0.05 0.32
;
_shelx_res_checksum 66697
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Zn Zn1 0.38352(2) 0.63073(2) 0.74182(2) 0.01361(6) Uani d 1 . .
Cl Cl1 0.40927(6) 0.54285(3) 0.61336(3) 0.02305(10) Uani d 1 . .
Cl Cl2 0.11765(5) 0.64610(3) 0.72669(3) 0.02054(9) Uani d 1 . .
Cl Cl3 0.50553(6) 0.56614(3) 0.88570(3) 0.02517(10) Uani d 1 . .
O O1 0.48379(13) 0.75415(7) 0.73622(8) 0.0143(2) Uani d 1 . .
N N1 0.40264(16) 0.83922(9) 0.72215(10) 0.0128(3) Uani d 1 . .
N N2 0.49127(17) 0.88977(9) 0.54778(10) 0.0158(3) Uani d 1 . .
N N3 0.73297(16) 0.82844(9) 0.66434(10) 0.0150(3) Uani d 1 . .
H H3 0.682588 0.767367 0.672505 0.018 Uiso calc 1 . .
N N4 0.63893(17) 0.92560(10) 0.81784(10) 0.0168(3) Uani d 1 . .
C C1 0.2840(2) 0.84123(12) 0.62400(12) 0.0168(3) Uani d 1 . .
H H1A 0.200438 0.794152 0.622381 0.020 Uiso calc 1 . .
H H1B 0.233240 0.903358 0.612818 0.020 Uiso calc 1 . .
C C2 0.3667(2) 0.82071(12) 0.54517(12) 0.0187(4) Uani d 1 . .
H H2A 0.413817 0.757581 0.555104 0.022 Uiso calc 1 . .
H H2B 0.289180 0.822203 0.480114 0.022 Uiso calc 1 . .
C C3 0.5688(2) 0.87961(12) 0.46713(13) 0.0211(4) Uani d 1 . .
H H3A 0.620783 0.939150 0.458245 0.025 Uiso calc 1 . .
H H3B 0.487426 0.866169 0.405469 0.025 Uiso calc 1 . .
C C4 0.6919(2) 0.80197(13) 0.48621(13) 0.0221(4) Uani d 1 . .
H H4A 0.639472 0.741237 0.489173 0.027 Uiso calc 1 . .
H H4B 0.745027 0.799462 0.431914 0.027 Uiso calc 1 . .
C C5 0.8131(2) 0.81999(13) 0.58233(13) 0.0210(4) Uani d 1 . .
H H5A 0.890506 0.768148 0.596338 0.025 Uiso calc 1 . .
H H5B 0.871458 0.878211 0.577319 0.025 Uiso calc 1 . .
C C6 0.8502(2) 0.85260(12) 0.75866(13) 0.0200(4) Uani d 1 . .
H H6A 0.900038 0.913375 0.751790 0.024 Uiso calc 1 . .
H H6B 0.934682 0.804743 0.773996 0.024 Uiso calc 1 . .
C C7 0.7694(2) 0.85777(12) 0.84095(13) 0.0203(4) Uani d 1 . .
H H7A 0.727310 0.795572 0.851407 0.024 Uiso calc 1 . .
H H7B 0.847102 0.876364 0.902397 0.024 Uiso calc 1 . .
C C8 0.5621(2) 0.93873(12) 0.89888(12) 0.0206(4) Uani d 1 . .
H H8A 0.507952 0.999931 0.891293 0.025 Uiso calc 1 . .
H H8B 0.644199 0.939192 0.962106 0.025 Uiso calc 1 . .
C C9 0.4420(2) 0.86239(12) 0.90143(12) 0.0198(4) Uani d 1 . .
H H9A 0.496925 0.801698 0.916110 0.024 Uiso calc 1 . .
H H9B 0.388001 0.875842 0.953828 0.024 Uiso calc 1 . .
C C10 0.3211(2) 0.85768(11) 0.80278(12) 0.0171(3) Uani d 1 . .
H H10A 0.244040 0.807317 0.803837 0.020 Uiso calc 1 . .
H H10B 0.262410 0.917304 0.789926 0.020 Uiso calc 1 . .
C C11 0.6037(2) 0.90373(11) 0.63997(12) 0.0145(3) Uani d 1 . .
H H11 0.659039 0.963672 0.634126 0.017 Uiso calc 1 . .
C C12 0.5264(2) 0.91649(11) 0.72469(12) 0.0142(3) Uani d 1 . .
H H12 0.466658 0.976619 0.712488 0.017 Uiso calc 1 . .
O O2 0.7488(7) 0.6396(4) 0.7042(5) 0.0387(13) Uani d 0.5 A 1
H H2C 0.816(8) 0.605(6) 0.684(5) 0.058 Uiso d 0.5 B 1
H H2D 0.670(6) 0.604(4) 0.677(5) 0.058 Uiso d 0.5 C 1
O O2A 0.7280(7) 0.6345(4) 0.6550(4) 0.0399(14) Uani d 0.5 D 2
H H2E 0.806(8) 0.618(7) 0.704(5) 0.060 Uiso d 0.5 E 2
H H2F 0.631(8) 0.598(4) 0.631(4) 0.060 Uiso d 0.5 F 2
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Zn1 0.01529(10) 0.00965(9) 0.01544(10) -0.00118(7) 0.00307(7) 0.00082(7)
Cl1 0.0301(2) 0.0209(2) 0.0180(2) 0.00448(18) 0.00584(17) -0.00187(16)
Cl2 0.0149(2) 0.01714(19) 0.0298(2) -0.00291(15) 0.00600(17) -0.00108(16)
Cl3 0.0342(3) 0.0201(2) 0.0177(2) 0.00302(18) 0.00018(18) 0.00485(16)
O1 0.0134(6) 0.0079(5) 0.0209(6) 0.0019(4) 0.0034(5) 0.0021(4)
N1 0.0146(7) 0.0085(6) 0.0155(7) 0.0017(5) 0.0040(5) 0.0003(5)
N2 0.0217(8) 0.0133(7) 0.0132(7) 0.0028(5) 0.0055(6) 0.0009(5)
N3 0.0149(7) 0.0112(6) 0.0193(7) -0.0003(5) 0.0050(6) 0.0010(5)
N4 0.0191(7) 0.0156(7) 0.0148(7) -0.0036(6) 0.0026(6) -0.0011(5)
C1 0.0145(8) 0.0153(8) 0.0180(8) 0.0013(6) -0.0004(6) 0.0008(6)
C2 0.0208(9) 0.0169(8) 0.0160(8) 0.0017(7) 0.0006(7) -0.0013(6)
C3 0.0313(10) 0.0180(8) 0.0168(8) 0.0072(7) 0.0113(7) 0.0018(7)
C4 0.0293(10) 0.0181(8) 0.0219(9) 0.0053(7) 0.0117(8) 0.0007(7)
C5 0.0206(9) 0.0182(8) 0.0280(9) 0.0021(7) 0.0133(8) 0.0011(7)
C6 0.0140(8) 0.0199(8) 0.0244(9) -0.0035(7) 0.0015(7) -0.0009(7)
C7 0.0171(9) 0.0206(9) 0.0202(8) -0.0039(7) -0.0010(7) 0.0009(7)
C8 0.0297(10) 0.0175(8) 0.0149(8) -0.0040(7) 0.0060(7) -0.0019(7)
C9 0.0272(10) 0.0172(8) 0.0169(8) -0.0015(7) 0.0089(7) -0.0001(7)
C10 0.0186(9) 0.0141(8) 0.0217(8) 0.0015(7) 0.0110(7) -0.0011(7)
C11 0.0181(8) 0.0083(7) 0.0176(8) 0.0003(6) 0.0052(7) 0.0024(6)
C12 0.0179(8) 0.0080(7) 0.0168(8) -0.0021(6) 0.0048(6) 0.0006(6)
O2 0.020(2) 0.0159(18) 0.084(4) 0.0026(16) 0.019(3) 0.000(3)
O2A 0.018(2) 0.0196(19) 0.079(4) 0.0014(15) 0.007(3) 0.003(3)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
O1 Zn1 Cl3 . . 107.03(4) y
O1 Zn1 Cl1 . . 109.33(4) y
Cl3 Zn1 Cl1 . . 111.812(19) y
O1 Zn1 Cl2 . . 110.93(3) y
Cl3 Zn1 Cl2 . . 111.244(19) y
Cl1 Zn1 Cl2 . . 106.531(18) y
N1 O1 Zn1 . . 124.84(9) y
O1 N1 C1 . . 110.64(12) ?
O1 N1 C10 . . 111.42(12) ?
C1 N1 C10 . . 110.01(13) ?
O1 N1 C12 . . 107.32(11) ?
C1 N1 C12 . . 108.81(12) ?
C10 N1 C12 . . 108.55(12) ?
C11 N2 C2 . . 116.85(13) ?
C11 N2 C3 . . 111.79(14) ?
C2 N2 C3 . . 113.48(14) ?
C6 N3 C5 . . 110.74(13) ?
C6 N3 C11 . . 109.42(13) ?
C5 N3 C11 . . 110.19(12) ?
C6 N3 H3 . . 108.8 ?
C5 N3 H3 . . 108.8 ?
C11 N3 H3 . . 108.8 ?
C12 N4 C7 . . 117.04(13) ?
C12 N4 C8 . . 112.30(14) ?
C7 N4 C8 . . 113.11(14) ?
C2 C1 N1 . . 109.18(13) ?
C2 C1 H1A . . 109.8 ?
N1 C1 H1A . . 109.8 ?
C2 C1 H1B . . 109.8 ?
N1 C1 H1B . . 109.8 ?
H1A C1 H1B . . 108.3 ?
N2 C2 C1 . . 110.04(14) ?
N2 C2 H2A . . 109.7 ?
C1 C2 H2A . . 109.7 ?
N2 C2 H2B . . 109.7 ?
C1 C2 H2B . . 109.7 ?
H2A C2 H2B . . 108.2 ?
N2 C3 C4 . . 112.29(14) ?
N2 C3 H3A . . 109.1 ?
C4 C3 H3A . . 109.1 ?
N2 C3 H3B . . 109.1 ?
C4 C3 H3B . . 109.1 ?
H3A C3 H3B . . 107.9 ?
C5 C4 C3 . . 109.50(15) ?
C5 C4 H4A . . 109.8 ?
C3 C4 H4A . . 109.8 ?
C5 C4 H4B . . 109.8 ?
C3 C4 H4B . . 109.8 ?
H4A C4 H4B . . 108.2 ?
N3 C5 C4 . . 110.20(14) ?
N3 C5 H5A . . 109.6 ?
C4 C5 H5A . . 109.6 ?
N3 C5 H5B . . 109.6 ?
C4 C5 H5B . . 109.6 ?
H5A C5 H5B . . 108.1 ?
N3 C6 C7 . . 110.23(14) ?
N3 C6 H6A . . 109.6 ?
C7 C6 H6A . . 109.6 ?
N3 C6 H6B . . 109.6 ?
C7 C6 H6B . . 109.6 ?
H6A C6 H6B . . 108.1 ?
N4 C7 C6 . . 110.56(14) ?
N4 C7 H7A . . 109.5 ?
C6 C7 H7A . . 109.5 ?
N4 C7 H7B . . 109.5 ?
C6 C7 H7B . . 109.5 ?
H7A C7 H7B . . 108.1 ?
N4 C8 C9 . . 112.18(14) ?
N4 C8 H8A . . 109.2 ?
C9 C8 H8A . . 109.2 ?
N4 C8 H8B . . 109.2 ?
C9 C8 H8B . . 109.2 ?
H8A C8 H8B . . 107.9 ?
C10 C9 C8 . . 109.44(14) ?
C10 C9 H9A . . 109.8 ?
C8 C9 H9A . . 109.8 ?
C10 C9 H9B . . 109.8 ?
C8 C9 H9B . . 109.8 ?
H9A C9 H9B . . 108.2 ?
N1 C10 C9 . . 110.21(14) ?
N1 C10 H10A . . 109.6 ?
C9 C10 H10A . . 109.6 ?
N1 C10 H10B . . 109.6 ?
C9 C10 H10B . . 109.6 ?
H10A C10 H10B . . 108.1 ?
N2 C11 C12 . . 112.94(14) ?
N2 C11 N3 . . 113.56(13) ?
C12 C11 N3 . . 110.86(13) ?
N2 C11 H11 . . 106.3 ?
C12 C11 H11 . . 106.3 ?
N3 C11 H11 . . 106.3 ?
N4 C12 C11 . . 113.04(14) ?
N4 C12 N1 . . 113.60(13) ?
C11 C12 N1 . . 110.04(13) ?
N4 C12 H12 . . 106.5 ?
C11 C12 H12 . . 106.5 ?
N1 C12 H12 . . 106.5 ?
H2C O2 H2D . . 92(7) ?
H2E O2A H2F . . 124(9) ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Zn1 O1 . 1.9856(11) y
Zn1 Cl3 . 2.2345(5) y
Zn1 Cl1 . 2.2616(5) y
Zn1 Cl2 . 2.2856(5) y
O1 N1 . 1.3996(16) ?
N1 C1 . 1.500(2) ?
N1 C10 . 1.508(2) ?
N1 C12 . 1.542(2) ?
N2 C11 . 1.427(2) ?
N2 C2 . 1.465(2) ?
N2 C3 . 1.469(2) ?
N3 C6 . 1.495(2) ?
N3 C5 . 1.499(2) ?
N3 C11 . 1.536(2) ?
N3 H3 . 1.0000 ?
N4 C12 . 1.429(2) ?
N4 C7 . 1.470(2) ?
N4 C8 . 1.475(2) ?
C1 C2 . 1.498(2) ?
C1 H1A . 0.9900 ?
C1 H1B . 0.9900 ?
C2 H2A . 0.9900 ?
C2 H2B . 0.9900 ?
C3 C4 . 1.523(2) ?
C3 H3A . 0.9900 ?
C3 H3B . 0.9900 ?
C4 C5 . 1.512(3) ?
C4 H4A . 0.9900 ?
C4 H4B . 0.9900 ?
C5 H5A . 0.9900 ?
C5 H5B . 0.9900 ?
C6 C7 . 1.504(3) ?
C6 H6A . 0.9900 ?
C6 H6B . 0.9900 ?
C7 H7A . 0.9900 ?
C7 H7B . 0.9900 ?
C8 C9 . 1.522(2) ?
C8 H8A . 0.9900 ?
C8 H8B . 0.9900 ?
C9 C10 . 1.516(2) ?
C9 H9A . 0.9900 ?
C9 H9B . 0.9900 ?
C10 H10A . 0.9900 ?
C10 H10B . 0.9900 ?
C11 C12 . 1.523(2) ?
C11 H11 . 1.0000 ?
C12 H12 . 1.0000 ?
O2 H2C . 0.87(4) ?
O2 H2D . 0.87(4) ?
O2A H2E . 0.87(4) ?
O2A H2F . 0.98(6) ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
N3 H3 O1 . 1.00 2.15 2.8297(18) 123.3 yes
N3 H3 O2 . 1.00 1.94 2.763(6) 137.8 yes
N3 H3 O2A . 1.00 1.98 2.786(7) 136.3 yes
O2 H2C Cl2 1_655 0.87(4) 2.61(8) 3.154(6) 121(7) yes
O2 H2C N4 2_646 0.87(4) 2.61(8) 3.262(6) 133(8) yes
O2 H2D Cl1 . 0.87(4) 2.39(4) 3.227(6) 162(6) yes
O2A H2E Cl2 1_655 0.87(4) 2.69(8) 3.295(6) 128(9) yes
O2A H2E N4 2_646 0.87(4) 2.84(9) 3.202(6) 107(7) yes
O2A H2F Cl1 . 0.98(6) 2.04(7) 2.996(6) 163(5) yes
C1 H1A Cl2 . 0.99 2.78 3.6198(18) 143.0 n
C2 H2B Cl3 4_575 0.99 2.96 3.7412(18) 136.2 n
C3 H3A N2 3_676 0.99 2.64 3.348(2) 129.0 n
C4 H4B Cl2 4_675 0.99 2.92 3.6201(19) 128.1 n
C5 H5A Cl2 1_655 0.99 2.92 3.8290(19) 153.6 n
C5 H5B Cl3 2_656 0.99 2.90 3.8493(19) 161.0 n
C6 H6A Cl1 2_656 0.99 2.87 3.6295(18) 134.6 n
C6 H6B Cl2 1_655 0.99 2.95 3.8679(19) 154.3 n
C7 H7A O1 . 0.99 2.40 2.953(2) 114.9 n
C8 H8A Cl2 2_556 0.99 2.73 3.6088(19) 148.8 n
C8 H8B Cl1 4_676 0.99 2.73 3.7009(19) 167.9 n
C10 H10A Cl2 . 0.99 2.67 3.5420(17) 146.9 n
C10 H10B Cl1 2_556 0.99 2.89 3.7018(17) 139.3 n
C12 H12 Cl2 2_556 1.00 2.74 3.6524(17) 151.9 n
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
Zn1 O1 N1 C1 . . . . -62.44(15) ?
Zn1 O1 N1 C10 . . . . 60.28(15) ?
Zn1 O1 N1 C12 . . . . 178.98(9) ?
O1 N1 C1 C2 . . . . -55.24(16) ?
C10 N1 C1 C2 . . . . -178.78(13) ?
C12 N1 C1 C2 . . . . 62.43(16) ?
C11 N2 C2 C1 . . . . 52.82(19) ?
C3 N2 C2 C1 . . . . -174.84(14) ?
N1 C1 C2 N2 . . . . -59.05(17) ?
C11 N2 C3 C4 . . . . 55.33(19) ?
C2 N2 C3 C4 . . . . -79.42(19) ?
N2 C3 C4 C5 . . . . -56.6(2) ?
C6 N3 C5 C4 . . . . -176.21(14) ?
C11 N3 C5 C4 . . . . -55.01(17) ?
C3 C4 C5 N3 . . . . 56.74(19) ?
C5 N3 C6 C7 . . . . -178.14(14) ?
C11 N3 C6 C7 . . . . 60.20(17) ?
C12 N4 C7 C6 . . . . 51.16(19) ?
C8 N4 C7 C6 . . . . -175.92(14) ?
N3 C6 C7 N4 . . . . -56.85(18) ?
C12 N4 C8 C9 . . . . 54.02(19) ?
C7 N4 C8 C9 . . . . -81.15(18) ?
N4 C8 C9 C10 . . . . -55.69(19) ?
O1 N1 C10 C9 . . . . 60.84(16) ?
C1 N1 C10 C9 . . . . -176.07(13) ?
C12 N1 C10 C9 . . . . -57.12(16) ?
C8 C9 C10 N1 . . . . 58.25(18) ?
C2 N2 C11 C12 . . . . -48.08(19) ?
C3 N2 C11 C12 . . . . 178.82(13) ?
C2 N2 C11 N3 . . . . 79.25(17) ?
C3 N2 C11 N3 . . . . -53.85(17) ?
C6 N3 C11 N2 . . . . 176.31(13) ?
C5 N3 C11 N2 . . . . 54.33(18) ?
C6 N3 C11 C12 . . . . -55.28(17) ?
C5 N3 C11 C12 . . . . -177.27(13) ?
C7 N4 C12 C11 . . . . -47.23(19) ?
C8 N4 C12 C11 . . . . 179.49(13) ?
C7 N4 C12 N1 . . . . 79.08(18) ?
C8 N4 C12 N1 . . . . -54.20(18) ?
N2 C11 C12 N4 . . . . 176.91(13) ?
N3 C11 C12 N4 . . . . 48.17(18) ?
N2 C11 C12 N1 . . . . 48.73(17) ?
N3 C11 C12 N1 . . . . -80.01(16) ?
O1 N1 C12 N4 . . . . -64.71(16) ?
C1 N1 C12 N4 . . . . 175.53(13) ?
C10 N1 C12 N4 . . . . 55.82(17) ?
O1 N1 C12 C11 . . . . 63.16(15) ?
C1 N1 C12 C11 . . . . -56.59(16) ?
C10 N1 C12 C11 . . . . -176.31(13) ?