#------------------------------------------------------------------------------ #$Date: 2024-04-06 01:43:54 +0200 (Sat, 06 Apr 2024) $ #$Revision: 291124 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/30/2023042.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023042 loop_ _publ_author_name 'Alaboosh, Jamal M. H.' 'Hill, Steven P.' 'Kariuki, Benson M.' 'Redman, James E.' _publ_section_title ; Crystal structures of sulfonamide protected bicyclic guanidines: (S)-8-{[(tert-butyl-dimethyl-sil-yl)-oxy]meth-yl}-1-[(2,2,4,6,7-penta-methyl-2,3-di-hydro-benzo-furan-5-yl)sulfon-yl]-1,3,4,6,7,8-hexa-hydro-2H-pyrimido[1,2-a]pyrimidin-1-ium tri-fluoro-methane-sulfonate and (S)-8-(iodo-meth-yl)-1-tosyl-1,3,4,6,7,8-hexa-hydro-2H-pyrimido[1,2-a]pyrimidin-1-ium iodide. ; _journal_coeditor_code DJ2073 _journal_issue 'Pt 3' _journal_name_full 'Acta crystallographica. Section E, Crystallographic communications' _journal_page_first 305 _journal_page_last 309 _journal_paper_doi 10.1107/S2056989024001129 _journal_volume 80 _journal_year 2024 _chemical_absolute_configuration ad _chemical_formula_iupac 'C15 H21 I N3 O2 S +, I -' _chemical_formula_moiety '(C15 H21 I N3 O2 S +), I -' _chemical_formula_sum 'C15 H21 I2 N3 O2 S' _chemical_formula_weight 561.21 _chemical_name_common '(S)-8-(Iodomethyl)-1-tosyl-1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidin-1-ium iodide' _chemical_name_systematic '(S)-8-(Iodomethyl)-1-4-(methylbenzenesulfonyl)-1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidin-1-ium iodide' _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2018/1 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 6.6117(2) _cell_length_b 10.1482(2) _cell_length_c 28.1444(9) _cell_measurement_reflns_used 3858 _cell_measurement_temperature 150(2) _cell_measurement_theta_max 27.44 _cell_measurement_theta_min 2.96 _cell_volume 1888.40(9) _computing_cell_refinement DENZO/SCALEPACK _computing_data_collection 'COLLECT,Nonius BV, 1997-2001' _computing_data_reduction DENZO/SCALEPACK _computing_structure_refinement 'SHELXL-2018/1 (Sheldrick, 2018)' _computing_structure_solution SHELXS _diffrn_ambient_temperature 150(2) _diffrn_measured_fraction_theta_full 0.979 _diffrn_measured_fraction_theta_max 0.982 _diffrn_measurement_device_type 'Nonius KappaCCD' _diffrn_measurement_method 'CCD scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0299 _diffrn_reflns_av_unetI/netI 0.0395 _diffrn_reflns_limit_h_max 8 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 36 _diffrn_reflns_limit_l_min -36 _diffrn_reflns_number 4087 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.440 _diffrn_reflns_theta_min 2.133 _exptl_absorpt_coefficient_mu 3.453 _exptl_absorpt_correction_T_max 0.5451 _exptl_absorpt_correction_T_min 0.3388 _exptl_absorpt_correction_type empirical _exptl_absorpt_process_details Denzo/Scalepack _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.974 _exptl_crystal_description needle _exptl_crystal_F_000 1080 _exptl_crystal_size_max 0.410 _exptl_crystal_size_mid 0.202 _exptl_crystal_size_min 0.201 _refine_diff_density_max 0.772 _refine_diff_density_min -0.787 _refine_ls_abs_structure_details ; Flack x determined using 1475 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.002(19) _refine_ls_extinction_coef 0.0068(4) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2018/1 (Sheldrick 2018)' _refine_ls_goodness_of_fit_ref 1.042 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 207 _refine_ls_number_reflns 4087 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.042 _refine_ls_R_factor_all 0.0359 _refine_ls_R_factor_gt 0.0308 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0251P)^2^+5.6778P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0693 _refine_ls_wR_factor_ref 0.0715 _reflns_number_gt 3858 _reflns_number_total 4087 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file dj2073sup1.cif _cod_data_source_block 2 _cod_depositor_comments 'Adding full bibliography for 2023041--2023042.cif.' _cod_database_code 2023042 _cod_database_fobs_code 2023042 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.332 _shelx_estimated_absorpt_t_max 0.544 _shelx_hkl_file ; 0 0 4 6547.60 4561.30 1 0 0 10 1597.50 52.00 1 0 0 13 7.40 4.10 1 0 0 14 2047.50 66.50 1 0 0 15 8.60 1.90 1 0 0 16 52.90 4.10 1 0 0 25 39.30 5.80 1 0 0 26 1346.20 48.90 1 0 0 28 -1.30 2.30 1 0 0 29 0.50 3.50 1 0 0 30 234.30 13.00 1 0 0 31 11.50 4.80 1 0 0 32 408.40 20.20 1 0 0 33 9.10 3.80 1 0 0 35 -3.30 4.80 1 0 0 36 108.30 10.50 1 0 1 0 0.20 0.10 1 0 1 1 657.10 654.10 1 0 1 3 228.80 5.70 1 0 1 4 419.60 7.30 1 0 1 5 200.30 3.90 1 0 1 6 401.30 7.20 1 0 1 7 29.00 1.10 1 0 1 8 261.40 5.90 1 0 1 9 1375.40 26.30 1 0 1 10 195.90 5.50 1 0 1 11 282.50 7.90 1 0 1 12 1363.10 32.30 1 0 1 13 3.80 1.10 1 0 1 14 129.60 4.40 1 0 1 15 169.70 5.40 1 0 1 16 40.90 3.20 1 0 1 17 43.80 3.60 1 0 1 23 199.00 9.40 1 0 1 24 501.20 20.30 1 0 1 26 641.50 26.10 1 0 1 27 25.50 2.70 1 0 1 28 59.70 4.00 1 0 1 29 127.40 6.10 1 0 1 30 286.30 10.50 1 0 1 31 12.70 2.80 1 0 1 32 278.60 10.60 1 0 1 33 43.60 4.80 1 0 1 34 18.70 3.80 1 0 1 35 13.40 3.40 1 0 1 36 121.80 7.60 1 0 2 0 988.00 16.00 1 0 2 1 2.30 0.20 1 0 2 2 1393.50 20.20 1 0 2 3 15.20 0.50 1 0 2 4 70.20 1.60 1 0 2 5 869.40 14.40 1 0 2 6 2829.00 53.70 1 0 2 7 14.00 0.70 1 0 2 8 1609.80 26.70 1 0 2 9 4.70 0.60 1 0 2 10 199.70 4.10 1 0 2 11 28.90 1.50 1 0 2 12 637.00 15.80 1 0 2 13 523.50 19.10 1 0 2 14 1177.30 39.40 1 0 2 15 459.30 12.30 1 0 2 16 1.50 1.20 1 0 2 17 320.60 9.30 1 0 2 18 495.30 19.10 1 0 2 19 -2.50 1.60 1 0 2 20 796.70 30.70 1 0 2 21 3.50 2.00 1 0 2 22 0.60 2.20 1 0 2 23 1169.10 42.60 1 0 2 24 437.80 18.40 1 0 2 25 19.40 3.60 1 0 2 28 102.60 5.70 1 0 2 29 195.30 7.50 1 0 2 30 112.50 5.70 1 0 2 31 165.50 7.30 1 0 2 32 95.90 5.90 1 0 2 33 145.00 7.70 1 0 2 34 78.40 5.70 1 0 2 35 258.50 12.70 1 0 2 36 8.70 2.80 1 0 3 0 8.70 0.90 1 0 3 1 1478.30 19.50 1 0 3 2 673.80 8.60 1 0 3 3 5683.50 181.30 1 0 3 4 511.10 7.90 1 0 3 5 2457.10 45.90 1 0 3 6 164.00 3.20 1 0 3 7 1366.60 22.40 1 0 3 8 446.50 7.90 1 0 3 9 2157.20 35.00 1 0 3 10 634.60 12.90 1 0 3 11 2767.30 63.70 1 0 3 12 4.50 0.70 1 0 3 13 91.90 2.70 1 0 3 14 51.10 2.40 1 0 3 15 3112.50 73.20 1 0 3 16 236.60 7.30 1 0 3 17 888.20 23.30 1 0 3 18 261.00 8.30 1 0 3 20 12.90 2.30 1 0 3 21 1123.00 40.20 1 0 3 24 270.40 12.00 1 0 3 25 10.90 3.30 1 0 3 26 0.90 2.90 1 0 3 27 211.60 7.80 1 0 3 28 13.90 2.70 1 0 3 29 490.40 15.50 1 0 3 30 71.60 4.60 1 0 3 31 1.70 2.50 1 0 3 32 23.60 3.20 1 0 3 33 169.60 9.20 1 0 3 34 10.40 3.10 1 0 3 35 111.00 7.20 1 0 4 0 277.40 5.20 1 0 4 1 21.20 0.70 1 0 4 2 18.80 0.50 1 0 4 3 31.80 0.70 1 0 4 4 39.50 1.00 1 0 4 5 6.70 0.50 1 0 4 6 6.40 0.50 1 0 4 7 1.20 0.40 1 0 4 8 90.60 2.00 1 0 4 9 453.20 8.20 1 0 4 10 504.50 9.30 1 0 4 11 48.50 1.50 1 0 4 12 24.00 1.10 1 0 4 13 59.20 2.40 1 0 4 14 94.40 3.60 1 0 4 15 509.50 13.00 1 0 4 16 48.30 2.00 1 0 4 17 290.20 7.20 1 0 4 18 115.00 4.50 1 0 4 19 10.50 1.70 1 0 4 20 60.10 3.90 1 0 4 21 507.70 19.80 1 0 4 22 282.30 12.60 1 0 4 23 145.70 8.10 1 0 4 24 99.20 6.40 1 0 4 25 26.50 3.40 1 0 4 26 1.70 2.60 1 0 4 27 242.90 12.20 1 0 4 28 218.00 8.70 1 0 4 29 352.10 12.40 1 0 4 30 30.20 3.50 1 0 4 31 13.20 3.10 1 0 4 32 4.40 2.70 1 0 4 33 130.00 7.60 1 0 4 34 40.50 4.80 1 0 5 0 4.90 0.60 1 0 5 1 977.40 13.70 1 0 5 2 1146.10 15.80 1 0 5 3 2204.00 32.20 1 0 5 4 809.60 10.50 1 0 5 5 784.00 11.20 1 0 5 6 7.70 0.50 1 0 5 7 45.90 1.20 1 0 5 8 463.30 7.70 1 0 5 9 2823.10 54.50 1 0 5 10 855.90 13.60 1 0 5 11 655.00 13.30 1 0 5 12 19.10 1.40 1 0 5 13 11.20 1.00 1 0 5 14 403.30 9.00 1 0 5 15 634.10 16.40 1 0 5 16 526.70 13.60 1 0 5 17 1117.90 28.30 1 0 5 18 1.20 1.30 1 0 5 19 10.40 1.70 1 0 5 20 458.70 17.40 1 0 5 21 349.10 10.30 1 0 5 22 349.00 10.40 1 0 5 23 578.60 23.70 1 0 5 24 51.60 4.30 1 0 5 25 46.80 4.80 1 0 5 26 254.60 9.50 1 0 5 27 241.00 8.80 1 0 5 28 238.50 8.90 1 0 5 29 94.40 5.20 1 0 5 30 2.30 2.90 1 0 5 31 119.30 6.60 1 0 5 32 60.10 4.60 1 0 5 33 2.60 3.40 1 0 6 0 1693.60 32.30 1 0 6 1 476.40 6.50 1 0 6 2 939.60 12.00 1 0 6 3 102.90 2.00 1 0 6 4 196.80 3.00 1 0 6 5 798.50 11.20 1 0 6 6 1164.20 18.00 1 0 6 7 520.50 10.40 1 0 6 8 335.80 7.30 1 0 6 9 93.20 4.10 1 0 6 10 19.10 1.00 1 0 6 11 4.10 0.70 1 0 6 12 1185.20 23.00 1 0 6 13 1306.90 31.10 1 0 6 14 242.90 6.80 1 0 6 15 25.10 1.60 1 0 6 16 110.60 3.90 1 0 6 17 6.40 1.30 1 0 6 18 390.70 10.70 1 0 6 19 195.30 9.00 1 0 6 21 623.50 23.80 1 0 6 22 55.20 4.20 1 0 6 23 5.20 2.20 1 0 6 24 305.60 14.40 1 0 6 25 39.40 3.90 1 0 6 26 107.30 5.30 1 0 6 27 161.00 7.50 1 0 6 28 3.30 2.70 1 0 6 29 100.20 5.90 1 0 6 30 277.70 18.20 1 0 6 31 107.30 10.10 1 0 6 32 84.10 9.90 1 0 7 0 -0.20 0.70 1 0 7 1 6.10 0.60 1 0 7 2 76.10 1.60 1 0 7 3 171.00 3.00 1 0 7 4 164.10 3.20 1 0 7 5 203.70 6.00 1 0 7 6 56.40 1.80 1 0 7 7 79.30 1.80 1 0 7 8 3.30 0.60 1 0 7 9 39.20 1.30 1 0 7 10 6.40 0.80 1 0 7 11 121.80 3.20 1 0 7 12 15.80 1.00 1 0 7 13 84.50 3.00 1 0 7 14 447.90 11.40 1 0 7 15 4.70 1.60 1 0 7 16 25.40 2.30 1 0 7 17 277.10 11.30 1 0 7 18 27.90 2.70 1 0 7 19 81.80 4.90 1 0 7 20 149.90 7.50 1 0 7 21 14.80 2.40 1 0 7 22 29.20 3.10 1 0 7 23 79.80 4.20 1 0 7 24 66.20 6.60 1 0 7 25 329.50 16.60 1 0 7 26 134.30 10.40 1 0 7 27 -3.70 3.80 1 0 7 28 32.20 6.70 1 0 7 29 68.40 8.60 1 0 7 30 -0.20 5.80 1 0 8 0 252.20 5.80 1 0 8 1 750.70 10.80 1 0 8 2 656.80 10.60 1 0 8 3 19.10 0.90 1 0 8 4 158.40 3.20 1 0 8 5 586.00 10.40 1 0 8 6 1117.10 19.80 1 0 8 7 1407.70 33.40 1 0 8 8 60.70 1.70 1 0 8 9 19.00 2.90 1 0 8 10 27.50 2.80 1 0 8 11 715.80 28.30 1 0 8 12 521.90 18.60 1 0 8 13 465.80 17.10 1 0 8 15 234.40 9.90 1 0 8 22 -2.80 2.70 1 0 8 23 91.10 7.60 1 0 8 24 131.90 9.90 1 0 8 25 250.40 15.40 1 0 8 26 102.90 10.60 1 0 8 27 20.60 6.00 1 0 8 28 68.60 7.90 1 0 9 0 -1.40 1.20 1 0 9 1 57.70 2.10 1 0 9 2 824.90 15.00 1 0 9 3 99.90 2.70 1 0 9 4 57.30 2.10 1 0 9 5 12.00 1.80 1 0 9 6 132.30 5.50 1 0 9 7 24.80 2.30 1 0 9 8 159.40 6.10 1 0 9 9 293.50 13.50 1 0 9 10 324.50 16.10 1 0 9 11 2.80 2.20 1 0 9 12 22.10 2.50 1 0 9 13 39.50 3.10 1 0 9 14 71.30 4.10 1 0 9 17 15.70 3.50 1 0 9 21 37.70 5.80 1 0 9 22 46.00 6.60 1 0 9 23 14.40 4.10 1 0 9 24 80.70 7.50 1 0 9 25 26.80 5.00 1 0 9 26 0.80 5.70 1 0 10 0 73.90 6.20 1 0 10 1 326.60 10.90 1 0 10 2 32.50 3.00 1 0 10 3 2.50 2.50 1 0 10 4 7.20 3.70 1 0 10 5 232.00 8.10 1 0 10 6 12.80 1.90 1 0 10 7 187.80 6.90 1 0 10 8 240.00 9.20 1 0 10 9 1.80 2.00 1 0 10 10 15.50 2.50 1 0 10 11 166.10 7.10 1 0 10 12 7.00 2.30 1 0 10 13 189.40 7.40 1 0 10 14 107.40 5.40 1 0 10 15 2.10 4.00 1 0 10 16 89.00 8.10 1 0 10 17 205.00 9.60 1 0 10 18 22.00 3.00 1 0 10 19 130.70 7.60 1 0 10 20 39.10 6.10 1 0 10 21 5.80 4.90 1 0 10 22 189.50 13.90 1 0 10 23 8.70 5.80 1 0 11 0 3.80 3.10 1 0 11 1 13.80 2.60 1 0 11 2 246.00 10.00 1 0 11 3 112.90 8.80 1 0 11 4 771.60 34.10 1 0 11 5 63.90 6.60 1 0 11 6 12.30 3.50 1 0 11 7 36.80 4.70 1 0 11 8 301.80 17.70 1 0 11 9 34.60 5.60 1 0 11 10 316.80 16.50 1 0 11 11 10.90 3.50 1 0 11 12 72.60 7.20 1 0 11 13 15.00 4.10 1 0 11 14 178.10 12.40 1 0 11 15 20.60 5.40 1 0 11 16 248.10 16.50 1 0 11 17 45.20 6.20 1 0 11 18 57.10 7.60 1 0 11 19 12.00 5.40 1 0 11 20 13.80 5.70 1 0 12 0 11.00 5.30 1 0 12 1 55.50 5.20 1 0 12 2 9.10 5.50 1 0 12 3 14.80 4.20 1 0 12 4 3.30 3.40 1 0 12 5 10.70 3.80 1 0 12 6 3.60 4.40 1 0 12 7 78.90 8.10 1 0 12 8 -0.70 3.40 1 0 12 9 -8.70 4.50 1 0 12 10 9.90 5.90 1 0 12 11 -6.40 5.00 1 0 12 12 14.60 4.40 1 0 12 13 30.50 6.20 1 0 12 14 1.30 3.40 1 0 13 0 -7.30 4.20 1 0 13 1 -5.10 6.00 1 0 13 2 179.00 14.70 1 0 13 3 15.10 5.40 1 0 13 4 140.50 11.70 1 0 13 5 15.70 6.40 1 1 0 0 1.70 0.20 1 1 0 1 288.50 5.90 1 1 0 2 125.50 2.90 1 1 0 3 552.20 9.40 1 1 0 4 27.80 0.80 1 1 0 5 1788.10 40.40 1 1 0 6 560.70 11.20 1 1 0 7 1332.20 22.30 1 1 0 8 472.80 8.40 1 1 0 9 109.80 2.50 1 1 0 10 70.10 1.90 1 1 0 11 179.80 3.90 1 1 0 12 26.70 1.30 1 1 0 13 244.00 5.20 1 1 0 14 321.30 7.40 1 1 0 15 109.90 4.20 1 1 0 16 27.80 2.20 1 1 0 17 112.30 5.80 1 1 0 18 557.20 21.80 1 1 0 19 497.30 19.00 1 1 0 20 309.50 9.40 1 1 0 22 195.70 9.20 1 1 0 23 209.00 9.50 1 1 0 26 257.00 12.20 1 1 0 27 163.80 6.70 1 1 0 28 29.90 3.00 1 1 0 29 11.30 2.30 1 1 0 30 243.60 8.70 1 1 0 31 92.40 5.40 1 1 0 32 651.40 19.90 1 1 0 33 5.50 2.80 1 1 0 34 37.60 4.50 1 1 0 35 5.20 3.10 1 1 0 36 56.30 5.10 1 1 1 0 1651.10 23.90 1 1 1 1 480.60 6.80 1 -1 -1 -1 473.10 7.20 1 1 1 2 1946.20 35.80 1 -1 -1 -2 1851.00 34.30 1 1 1 3 350.30 5.50 1 -1 -1 -3 332.70 5.90 1 1 1 4 1359.10 25.60 1 -1 -1 -4 1368.40 19.80 1 1 1 5 240.10 4.60 1 -1 -1 -5 259.30 5.00 1 1 1 7 491.60 8.90 1 -1 -1 -7 467.90 8.30 1 1 1 8 1203.10 20.20 1 -1 -1 -8 1144.30 19.30 1 1 1 9 356.40 6.60 1 -1 -1 -9 348.50 6.60 1 1 1 10 115.80 2.70 1 -1 -1 -10 115.50 2.70 1 1 1 11 366.40 7.00 1 -1 -1 -11 333.10 7.40 1 1 1 12 2465.10 46.20 1 -1 -1 -12 2577.10 59.80 1 1 1 13 154.90 4.30 1 -1 -1 -13 172.90 5.50 1 1 1 14 2567.10 60.90 1 -1 -1 -14 2620.20 86.40 1 1 1 15 29.90 2.10 1 -1 -1 -15 39.80 1.80 1 1 1 16 426.90 17.20 1 -1 -1 -16 435.40 18.20 1 1 1 17 352.40 10.30 1 -1 -1 -17 377.70 15.70 1 1 1 18 711.30 27.70 1 1 1 19 190.20 9.10 1 1 1 20 1609.40 58.00 1 -1 -1 -20 1636.50 56.20 1 1 1 21 333.30 10.80 1 -1 -1 -21 350.90 14.40 1 1 1 22 24.90 2.20 1 -1 -1 -23 47.70 4.70 1 1 1 24 651.80 25.30 1 1 1 25 250.70 8.20 1 -1 -1 -26 380.80 18.70 1 -1 -1 -27 91.70 7.10 1 1 1 28 93.00 6.90 1 -1 -1 -28 133.50 5.70 1 1 1 29 185.60 11.40 1 -1 -1 -29 176.90 7.10 1 1 1 30 276.00 10.30 1 -1 -1 -30 269.60 10.00 1 1 1 31 80.50 5.00 1 -1 -1 -31 89.90 5.30 1 1 1 32 141.00 7.50 1 -1 -1 -32 145.20 7.50 1 1 1 33 31.00 3.90 1 -1 -1 -33 37.40 4.00 1 1 1 34 18.00 3.40 1 -1 -1 -34 24.70 3.60 1 1 1 35 33.60 4.60 1 -1 -1 -35 43.60 4.30 1 1 1 36 39.70 4.80 1 -1 -1 -36 44.70 4.40 1 1 2 0 52.50 50.90 1 1 2 2 291.10 4.60 1 -1 -2 -2 273.10 3.90 1 1 2 3 3284.00 75.70 1 -1 -2 -3 3379.60 76.40 1 1 2 4 361.00 6.50 1 -1 -2 -4 335.00 6.10 1 1 2 5 1880.90 27.20 1 -1 -2 -5 1829.90 41.40 1 1 2 6 326.00 6.00 1 -1 -2 -6 318.80 6.90 1 1 2 7 859.70 13.30 1 -1 -2 -7 886.10 21.30 1 1 2 8 257.10 5.70 1 -1 -2 -8 247.80 5.60 1 1 2 9 3376.90 75.60 1 -1 -2 -9 3087.20 99.90 1 1 2 10 433.10 7.80 1 -1 -2 -10 426.90 9.30 1 1 2 11 651.50 11.70 1 -1 -2 -11 653.90 13.50 1 1 2 12 104.60 2.70 1 -1 -2 -12 98.50 4.70 1 1 2 13 686.60 12.30 1 -1 -2 -13 706.80 18.90 1 1 2 14 235.10 5.90 1 -1 -2 -14 238.80 7.50 1 1 2 15 1480.40 28.60 1 -1 -2 -15 1594.30 54.00 1 1 2 16 273.90 11.80 1 -1 -2 -16 252.10 7.70 1 1 2 17 995.10 24.50 1 1 2 19 532.50 21.20 1 1 2 20 96.50 4.50 1 1 2 21 580.30 16.70 1 1 2 22 50.50 4.80 1 1 2 23 292.10 14.00 1 1 2 24 193.90 7.20 1 1 2 25 127.00 5.60 1 1 2 26 124.50 7.80 1 -1 -2 -26 141.50 9.50 1 1 2 27 584.10 25.00 1 -1 -2 -27 546.80 17.20 1 1 2 28 84.20 4.70 1 -1 -2 -28 72.70 5.00 1 1 2 29 113.10 5.40 1 -1 -2 -29 94.10 5.20 1 1 2 30 154.60 7.30 1 -1 -2 -30 147.60 6.60 1 1 2 31 74.50 5.00 1 -1 -2 -31 51.80 4.40 1 1 2 32 217.70 10.40 1 -1 -2 -32 237.50 10.90 1 1 2 33 85.70 6.50 1 -1 -2 -33 92.70 5.50 1 1 2 34 18.70 3.30 1 -1 -2 -34 16.30 3.50 1 1 2 35 100.20 6.90 1 -1 -2 -35 95.50 6.30 1 1 3 0 2918.30 41.70 1 1 3 1 278.70 4.20 1 -1 -3 -1 282.10 4.20 1 1 3 2 352.30 5.90 1 -1 -3 -2 311.70 4.70 1 1 3 3 151.70 3.10 1 -1 -3 -3 153.00 2.80 1 1 3 4 762.00 13.20 1 -1 -3 -4 684.90 11.70 1 1 3 5 67.20 1.60 1 -1 -3 -5 69.50 1.80 1 1 3 6 460.90 7.50 1 -1 -3 -6 453.10 9.10 1 1 3 7 107.90 2.20 1 -1 -3 -7 94.90 4.70 1 1 3 8 913.30 14.10 1 1 3 9 507.10 8.10 1 -1 -3 -9 505.00 18.20 1 1 3 10 640.00 11.50 1 -1 -3 -10 582.10 15.30 1 1 3 11 601.10 10.60 1 -1 -3 -11 619.80 16.00 1 1 3 12 354.20 6.90 1 -1 -3 -12 363.50 10.40 1 1 3 13 13.90 1.00 1 -1 -3 -13 13.60 2.00 1 1 3 14 332.60 9.00 1 -1 -3 -14 357.00 14.10 1 1 3 15 192.90 5.90 1 -1 -3 -15 213.20 10.30 1 1 3 16 441.20 12.20 1 -1 -3 -16 444.00 18.40 1 1 3 17 682.30 14.70 1 1 3 18 306.90 7.40 1 1 3 19 36.20 2.20 1 1 3 20 118.20 4.80 1 1 3 21 330.70 10.10 1 1 3 22 247.00 9.10 1 1 3 23 682.90 26.50 1 1 3 24 24.60 4.00 1 -1 -3 -24 22.00 2.70 1 1 3 25 31.00 3.00 1 -1 -3 -25 33.00 4.40 1 1 3 26 220.70 8.00 1 1 3 27 187.70 10.00 1 -1 -3 -27 180.20 7.20 1 1 3 28 90.30 7.10 1 -1 -3 -28 96.80 5.20 1 1 3 29 525.00 22.60 1 -1 -3 -29 506.20 17.10 1 1 3 30 30.50 3.20 1 -1 -3 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1 2 0 26 392.60 12.80 1 2 0 27 158.10 10.40 1 2 0 28 23.50 5.00 1 2 0 29 124.00 6.00 1 2 0 30 61.00 6.20 1 2 0 31 190.60 11.60 1 2 0 32 79.70 5.40 1 2 0 33 203.60 10.20 1 2 0 34 8.40 3.60 1 2 0 35 3.00 3.00 1 2 1 0 11.80 0.60 1 2 1 1 2428.20 39.10 1 -2 -1 -1 2412.50 35.10 1 2 1 2 55.20 1.20 1 -2 -1 -2 55.80 1.20 1 2 1 3 525.60 8.40 1 -2 -1 -3 519.90 9.20 1 2 1 4 218.80 3.90 1 -2 -1 -4 207.00 4.10 1 2 1 5 2160.50 31.10 1 -2 -1 -5 2124.20 34.90 1 2 1 6 61.50 1.60 1 -2 -1 -6 58.30 1.60 1 2 1 7 2094.50 39.40 1 -2 -1 -7 1986.80 32.90 1 2 1 8 290.40 5.80 1 -2 -1 -8 290.80 5.70 1 2 1 9 473.50 8.90 1 -2 -1 -9 498.70 9.30 1 2 1 10 74.90 2.10 1 -2 -1 -10 76.10 2.00 1 2 1 11 1723.70 33.60 1 -2 -1 -11 1781.00 30.10 1 2 1 12 219.40 4.80 1 -2 -1 -12 233.50 5.60 1 2 1 13 2221.20 38.30 1 -2 -1 -13 2088.10 40.10 1 2 1 14 196.30 6.20 1 -2 -1 -14 171.50 5.70 1 2 1 15 756.50 19.70 1 -2 -1 -15 760.00 19.80 1 2 1 16 68.10 3.00 1 -2 -1 -16 77.60 4.50 1 2 1 17 442.00 18.00 1 -2 -1 -17 445.40 17.50 1 2 1 18 286.30 12.10 1 -2 -1 -18 281.20 9.00 1 2 1 19 1275.60 45.40 1 -2 -1 -19 1250.60 46.10 1 2 1 20 163.70 6.10 1 -2 -1 -20 189.90 9.00 1 2 1 21 394.50 16.90 1 -2 -1 -21 446.30 13.20 1 2 1 22 242.10 11.90 1 -2 -1 -22 259.30 8.60 1 2 1 23 135.40 5.50 1 -2 -1 -23 113.30 6.90 1 2 1 24 236.00 7.90 1 -2 -1 -24 244.20 12.20 1 2 1 25 564.10 16.40 1 -2 -1 -25 544.00 22.40 1 2 1 26 357.70 11.70 1 -2 -1 -26 337.20 16.10 1 2 1 27 78.90 4.50 1 -2 -1 -27 93.50 4.80 1 2 1 28 29.80 3.20 1 -2 -1 -28 25.60 4.30 1 2 1 29 68.80 4.40 1 -2 -1 -29 45.60 5.50 1 2 1 30 140.30 10.30 1 -2 -1 -30 158.90 7.10 1 2 1 31 166.50 10.30 1 -2 -1 -31 165.90 7.80 1 2 1 32 104.20 5.90 1 -2 -1 -32 104.00 6.30 1 2 1 33 148.30 8.20 1 -2 -1 -33 139.50 7.70 1 2 1 34 93.90 6.30 1 -2 -1 -34 83.30 5.60 1 2 1 35 30.40 4.70 1 -2 -1 -35 27.70 3.70 1 2 2 0 866.20 12.00 1 2 2 1 306.50 4.80 1 -2 -2 -1 283.70 4.80 1 2 2 2 1889.80 27.50 1 -2 -2 -2 1956.40 32.00 1 2 2 3 186.80 3.10 1 -2 -2 -3 195.20 3.40 1 2 2 4 1778.10 26.10 1 -2 -2 -4 1684.60 27.50 1 2 2 5 740.80 11.70 1 -2 -2 -5 720.20 12.40 1 2 2 6 824.10 12.50 1 -2 -2 -6 825.50 16.70 1 2 2 7 8.30 0.70 1 -2 -2 -7 12.10 0.60 1 2 2 8 1247.60 21.40 1 -2 -2 -8 1260.60 21.50 1 2 2 9 56.70 1.80 1 -2 -2 -9 44.20 1.50 1 2 2 10 1706.90 28.90 1 -2 -2 -10 1675.20 32.90 1 2 2 11 306.10 6.30 1 -2 -2 -11 331.10 6.80 1 2 2 12 982.00 17.60 1 -2 -2 -12 956.80 19.40 1 2 2 13 249.50 7.40 1 -2 -2 -13 248.30 6.00 1 2 2 14 938.40 23.60 1 -2 -2 -14 953.20 24.10 1 2 2 15 111.00 4.30 1 -2 -2 -15 107.20 3.90 1 2 2 16 503.00 13.40 1 -2 -2 -16 449.50 16.90 1 2 2 17 138.10 5.70 1 -2 -2 -17 139.10 6.40 1 2 2 18 224.50 7.40 1 -2 -2 -18 243.40 7.70 1 2 2 19 220.90 7.80 1 -2 -2 -19 231.00 7.50 1 2 2 20 768.70 20.50 1 -2 -2 -20 895.30 34.30 1 2 2 21 7.40 1.90 1 -2 -2 -21 2.00 1.50 1 2 2 22 815.90 22.20 1 -2 -2 -22 840.20 30.50 1 2 2 23 553.50 15.70 1 -2 -2 -23 484.90 13.70 1 2 2 24 153.60 6.50 1 -2 -2 -24 132.60 8.30 1 2 2 25 207.20 8.10 1 -2 -2 -25 242.80 8.30 1 2 2 26 82.10 4.60 1 -2 -2 -26 90.70 7.40 1 2 2 27 61.90 4.30 1 -2 -2 -27 46.90 5.70 1 2 2 28 225.80 8.60 1 -2 -2 -28 199.50 12.00 1 2 2 29 193.10 11.80 1 -2 -2 -29 177.40 7.60 1 2 2 30 121.20 9.00 1 -2 -2 -30 81.20 5.10 1 2 2 31 252.10 11.50 1 -2 -2 -31 212.50 10.20 1 2 2 32 105.20 6.60 1 -2 -2 -32 110.20 6.70 1 2 2 33 146.40 8.00 1 -2 -2 -33 113.20 7.10 1 2 2 34 43.70 4.70 1 -2 -2 -34 47.10 4.50 1 2 2 35 48.30 4.50 1 -2 -2 -35 35.70 4.00 1 2 3 0 430.70 6.50 1 2 3 1 785.00 11.00 1 -2 -3 -1 811.90 11.40 1 2 3 2 394.20 6.00 1 -2 -3 -2 408.70 5.50 1 2 3 3 1113.50 15.30 1 -2 -3 -3 1061.40 14.40 1 2 3 4 131.40 2.40 1 -2 -3 -4 147.10 2.50 1 2 3 5 384.60 6.30 1 -2 -3 -5 415.80 7.40 1 2 3 6 256.80 5.00 1 -2 -3 -6 238.50 4.20 1 2 3 7 599.30 10.60 1 -2 -3 -7 597.90 9.60 1 2 3 8 206.80 4.60 1 -2 -3 -8 201.80 4.10 1 2 3 9 1194.50 18.40 1 -2 -3 -9 1143.40 23.10 1 2 3 10 266.40 4.90 1 -2 -3 -10 254.70 5.10 1 2 3 11 998.20 25.40 1 -2 -3 -11 1028.80 17.80 1 2 3 12 120.50 3.60 1 -2 -3 -12 123.70 3.00 1 2 3 13 211.80 6.80 1 -2 -3 -13 229.70 4.90 1 2 3 14 211.90 6.70 1 -2 -3 -14 208.00 5.20 1 2 3 15 944.70 23.80 1 -2 -3 -15 871.40 22.10 1 2 3 16 420.10 12.60 1 -2 -3 -16 407.90 11.40 1 2 3 17 182.80 6.30 1 -2 -3 -17 188.00 6.30 1 2 3 18 109.80 4.50 1 -2 -3 -18 126.40 7.70 1 2 3 19 168.40 6.30 1 -2 -3 -19 150.80 8.20 1 2 3 20 46.00 3.20 1 2 3 21 619.30 17.70 1 2 3 22 304.20 9.90 1 2 3 23 183.60 7.20 1 -2 -3 -23 193.50 7.10 1 2 3 24 224.20 8.00 1 -2 -3 -24 204.50 11.30 1 2 3 25 49.90 3.90 1 2 3 26 25.60 2.90 1 2 3 27 152.00 6.60 1 -2 -3 -27 152.10 9.50 1 2 3 28 198.00 8.40 1 -2 -3 -28 193.10 8.00 1 2 3 29 137.90 6.70 1 -2 -3 -29 180.70 7.90 1 2 3 30 140.80 10.00 1 -2 -3 -30 140.10 7.00 1 2 3 31 0.20 2.50 1 -2 -3 -31 3.40 2.60 1 2 3 32 64.70 5.60 1 -2 -3 -32 55.90 5.10 1 2 3 33 93.90 6.70 1 -2 -3 -33 86.90 6.10 1 2 3 34 161.60 9.60 1 -2 -3 -34 157.20 9.40 1 2 4 0 722.70 9.70 1 2 4 1 120.30 2.20 1 -2 -4 -1 107.50 1.90 1 2 4 2 2593.40 42.10 1 -2 -4 -2 2575.70 37.10 1 2 4 3 439.50 7.30 1 -2 -4 -3 402.40 5.90 1 2 4 4 1338.80 18.30 1 -2 -4 -4 1292.40 17.60 1 2 4 5 185.60 3.60 1 -2 -4 -5 188.10 3.10 1 2 4 6 104.70 2.60 1 -2 -4 -6 109.80 2.00 1 2 4 7 35.30 1.30 1 -2 -4 -7 37.50 1.30 1 2 4 8 1409.00 24.40 1 -2 -4 -8 1358.90 22.60 1 2 4 9 730.10 18.30 1 -2 -4 -9 698.00 12.20 1 2 4 10 2042.70 40.10 1 -2 -4 -10 2053.20 39.40 1 2 4 11 243.70 6.30 1 -2 -4 -11 222.50 5.40 1 2 4 12 141.80 4.70 1 -2 -4 -12 127.90 3.00 1 2 4 13 6.20 1.30 1 -2 -4 -13 5.40 1.40 1 2 4 14 511.60 13.70 1 -2 -4 -14 498.10 18.10 1 2 4 15 416.60 12.00 1 -2 -4 -15 418.30 11.90 1 2 4 16 1073.10 27.90 1 2 4 17 237.20 7.90 1 -2 -4 -17 260.40 11.50 1 2 4 18 353.60 10.90 1 -2 -4 -18 386.10 16.10 1 2 4 19 0.70 1.50 1 -2 -4 -19 2.50 2.10 1 2 4 20 282.70 9.00 1 -2 -4 -20 258.30 12.50 1 2 4 21 213.40 7.50 1 -2 -4 -21 193.40 10.20 1 2 4 22 453.20 20.50 1 -2 -4 -22 384.10 17.30 1 2 4 23 166.00 6.50 1 -2 -4 -23 202.00 7.40 1 2 4 24 310.60 11.10 1 -2 -4 -24 295.60 10.00 1 2 4 25 30.30 3.30 1 -2 -4 -25 28.20 2.80 1 2 4 26 22.60 2.90 1 -2 -4 -26 18.90 2.50 1 2 4 27 162.10 7.10 1 -2 -4 -27 168.10 10.10 1 2 4 28 271.90 10.10 1 -2 -4 -28 304.80 11.00 1 2 4 29 187.50 8.20 1 -2 -4 -29 157.40 7.10 1 2 4 30 108.50 6.50 1 -2 -4 -30 92.40 5.60 1 2 4 31 7.80 2.90 1 -2 -4 -31 13.80 2.80 1 2 4 32 8.30 5.20 1 -2 -4 -32 -0.40 2.70 1 2 4 33 49.60 4.70 1 -2 -4 -33 41.90 4.10 1 2 5 0 716.90 10.20 1 2 5 1 415.00 6.20 1 -2 -5 -1 384.30 5.80 1 2 5 2 662.40 11.50 1 -2 -5 -2 680.10 9.10 1 2 5 3 985.30 20.10 1 -2 -5 -3 1011.80 14.10 1 2 5 4 294.70 6.80 1 -2 -5 -4 297.80 4.70 1 2 5 5 559.00 10.60 1 -2 -5 -5 587.80 9.40 1 2 5 6 140.70 3.10 1 -2 -5 -6 155.10 3.80 1 2 5 7 272.60 5.60 1 -2 -5 -7 255.20 6.00 1 2 5 8 484.80 12.70 1 -2 -5 -8 485.40 7.60 1 2 5 9 1157.80 23.80 1 -2 -5 -9 1082.60 16.30 1 2 5 10 243.30 6.30 1 -2 -5 -10 251.50 5.00 1 2 5 11 411.40 9.40 1 -2 -5 -11 392.20 7.40 1 2 5 12 152.90 5.60 1 -2 -5 -12 159.90 3.60 1 2 5 13 206.00 6.60 1 -2 -5 -13 237.40 6.70 1 2 5 14 371.60 10.20 1 -2 -5 -14 368.20 14.70 1 2 5 15 451.90 12.20 1 -2 -5 -15 481.90 10.90 1 2 5 16 367.20 10.60 1 -2 -5 -16 366.60 8.50 1 2 5 17 893.10 23.30 1 -2 -5 -17 884.00 18.80 1 2 5 18 14.70 2.20 1 -2 -5 -18 17.30 2.00 1 2 5 19 97.60 4.40 1 -2 -5 -19 68.90 3.50 1 2 5 20 309.10 10.30 1 -2 -5 -20 286.10 9.40 1 2 5 21 70.90 3.70 1 -2 -5 -21 75.70 4.80 1 2 5 22 249.20 8.50 1 2 5 23 311.90 10.40 1 -2 -5 -23 315.30 10.60 1 2 5 24 13.10 3.80 1 -2 -5 -24 12.20 2.00 1 2 5 25 101.60 5.20 1 -2 -5 -25 114.10 5.30 1 2 5 26 169.80 6.60 1 -2 -5 -26 163.00 6.60 1 2 5 27 101.30 6.00 1 -2 -5 -27 91.60 5.10 1 2 5 28 193.40 8.80 1 -2 -5 -28 197.90 8.80 1 2 5 29 99.10 7.90 1 -2 -5 -29 88.90 8.20 1 2 5 30 13.80 4.00 1 -2 -5 -30 4.80 5.50 1 2 5 31 40.30 4.20 1 -2 -5 -31 50.10 7.10 1 2 5 32 39.30 4.60 1 -2 -5 -32 44.30 8.30 1 2 6 0 302.70 4.70 1 2 6 1 113.30 2.00 1 -2 -6 -1 116.40 2.50 1 2 6 2 228.50 4.80 1 -2 -6 -2 205.60 3.90 1 2 6 3 337.90 6.80 1 -2 -6 -3 344.40 5.60 1 2 6 4 457.10 8.50 1 -2 -6 -4 439.10 6.70 1 2 6 5 155.60 3.70 1 -2 -6 -5 153.30 3.20 1 2 6 6 549.70 10.30 1 -2 -6 -6 526.50 9.60 1 2 6 7 360.00 7.30 1 -2 -6 -7 365.50 8.40 1 2 6 8 192.30 4.40 1 -2 -6 -8 205.10 5.10 1 2 6 9 140.90 5.10 1 -2 -6 -9 124.70 3.80 1 2 6 10 421.50 16.70 1 -2 -6 -10 387.80 9.20 1 2 6 11 99.30 5.90 1 -2 -6 -11 73.00 2.80 1 2 6 12 491.10 13.10 1 -2 -6 -12 461.70 9.10 1 2 6 13 410.10 11.70 1 -2 -6 -13 405.00 8.60 1 2 6 14 114.00 4.50 1 -2 -6 -14 108.70 3.00 1 2 6 15 545.80 14.80 1 -2 -6 -15 605.10 13.10 1 2 6 16 551.60 15.10 1 -2 -6 -16 562.10 15.10 1 2 6 17 43.80 3.00 1 -2 -6 -17 28.40 2.00 1 2 6 18 287.70 9.30 1 -2 -6 -18 256.30 8.20 1 2 6 19 55.10 3.40 1 -2 -6 -19 55.10 3.60 1 2 6 20 91.90 4.40 1 -2 -6 -20 70.50 3.40 1 2 6 21 276.20 9.30 1 -2 -6 -21 265.30 9.30 1 2 6 22 111.20 7.40 1 -2 -6 -22 92.40 7.30 1 2 6 23 15.30 2.60 1 -2 -6 -23 19.60 4.90 1 2 6 24 365.80 12.50 1 -2 -6 -24 366.80 18.10 1 2 6 25 128.60 5.90 1 -2 -6 -25 143.10 10.40 1 2 6 26 26.80 4.60 1 -2 -6 -26 45.10 6.80 1 2 6 27 128.30 9.90 1 -2 -6 -27 118.00 10.60 1 2 6 28 57.80 4.20 1 -2 -6 -28 54.60 7.80 1 2 6 29 47.50 6.40 1 -2 -6 -29 64.00 8.00 1 2 6 30 115.70 9.70 1 -2 -6 -30 111.10 10.40 1 2 6 31 125.60 7.60 1 -2 -6 -31 103.10 9.90 1 2 7 0 729.80 10.40 1 2 7 1 534.10 11.90 1 -2 -7 -1 564.40 8.40 1 2 7 2 215.10 6.30 1 -2 -7 -2 235.00 4.40 1 2 7 3 8.70 1.20 1 -2 -7 -3 7.10 0.80 1 2 7 4 175.50 4.10 1 -2 -7 -4 172.90 3.60 1 2 7 5 672.40 12.30 1 -2 -7 -5 651.50 10.70 1 2 7 6 853.10 15.70 1 -2 -7 -6 817.60 14.70 1 2 7 7 463.40 10.50 1 -2 -7 -7 461.00 8.90 1 2 7 8 479.40 10.60 1 -2 -7 -8 479.20 9.20 1 2 7 9 8.00 1.10 1 -2 -7 -9 2.60 1.00 1 2 7 10 21.60 2.00 1 -2 -7 -10 17.00 1.90 1 2 7 11 242.90 6.50 1 -2 -7 -11 219.80 10.90 1 2 7 12 401.50 11.70 1 -2 -7 -12 407.40 16.60 1 2 7 13 800.90 21.30 1 -2 -7 -13 702.70 26.00 1 2 7 14 218.80 7.30 1 -2 -7 -14 180.10 8.90 1 2 7 15 9.30 2.00 1 -2 -7 -15 8.30 2.50 1 2 7 16 1.50 1.80 1 -2 -7 -16 1.10 2.20 1 2 7 17 125.30 5.30 1 -2 -7 -17 103.70 7.00 1 2 7 18 150.70 6.00 1 -2 -7 -18 128.10 8.00 1 2 7 19 276.40 9.40 1 -2 -7 -19 266.00 12.90 1 2 7 20 350.50 11.40 1 -2 -7 -20 340.40 16.00 1 2 7 21 88.90 4.70 1 -2 -7 -21 85.10 7.30 1 2 7 22 16.50 2.50 1 -2 -7 -22 7.20 4.40 1 2 7 23 63.50 3.80 1 -2 -7 -23 45.50 6.30 1 2 7 24 109.60 7.90 1 -2 -7 -24 123.30 9.00 1 2 7 25 62.60 6.30 1 -2 -7 -25 64.00 7.90 1 2 7 26 121.70 6.60 1 -2 -7 -26 126.30 11.50 1 2 7 27 18.60 3.70 1 -2 -7 -27 18.80 5.50 1 2 7 28 71.20 7.90 1 -2 -7 -28 70.10 9.00 1 2 7 29 11.40 4.50 1 -2 -7 -29 13.20 5.00 1 2 8 0 249.00 6.50 1 2 8 1 458.90 13.30 1 -2 -8 -1 457.10 7.50 1 2 8 2 176.60 5.00 1 -2 -8 -2 187.80 4.00 1 2 8 3 80.80 3.10 1 -2 -8 -3 74.30 2.70 1 2 8 4 75.20 2.90 1 -2 -8 -4 68.60 2.10 1 2 8 5 110.50 3.10 1 -2 -8 -5 109.90 3.00 1 2 8 6 338.20 8.30 1 -2 -8 -6 333.20 9.70 1 2 8 7 530.20 12.60 1 -2 -8 -7 528.60 14.20 1 2 8 8 67.20 3.30 1 -2 -8 -8 64.30 3.10 1 2 8 9 19.40 1.90 1 -2 -8 -9 22.40 2.10 1 2 8 10 13.80 1.80 1 -2 -8 -10 14.30 2.00 1 2 8 11 346.30 8.70 1 -2 -8 -11 356.30 10.70 1 2 8 12 354.80 9.20 1 -2 -8 -12 347.80 15.10 1 2 8 13 139.40 4.60 1 -2 -8 -13 143.50 8.60 1 2 8 14 116.10 5.10 1 -2 -8 -14 125.10 7.50 1 2 8 15 65.70 3.90 1 -2 -8 -15 69.30 5.40 1 2 8 16 -0.20 1.60 1 -2 -8 -16 7.30 3.30 1 2 8 17 241.40 9.00 1 -2 -8 -17 197.30 11.30 1 2 8 18 139.60 5.90 1 -2 -8 -18 108.40 7.80 1 2 8 19 176.10 7.20 1 -2 -8 -19 190.20 11.80 1 2 8 20 301.80 11.10 1 -2 -8 -20 295.00 15.60 1 2 8 21 8.30 3.60 1 -2 -8 -21 7.00 4.40 1 2 8 22 18.40 3.60 1 -2 -8 -22 16.50 4.10 1 2 8 23 46.50 5.90 1 -2 -8 -23 36.30 6.40 1 -2 -8 -24 63.60 7.60 1 -2 -8 -25 136.40 11.40 1 2 8 26 81.20 9.20 1 -2 -8 -26 72.30 8.50 1 2 8 27 13.40 4.50 1 -2 -8 -27 0.00 6.00 1 2 9 0 482.20 11.70 1 2 9 1 123.20 4.30 1 -2 -9 -1 110.60 5.20 1 2 9 2 138.00 4.70 1 -2 -9 -2 139.10 5.50 1 2 9 3 18.00 1.80 1 -2 -9 -3 9.70 2.30 1 2 9 4 195.30 5.50 1 -2 -9 -4 200.10 7.50 1 2 9 5 89.80 3.40 1 -2 -9 -5 96.50 4.70 1 2 9 6 292.70 7.90 1 -2 -9 -6 291.60 8.80 1 2 9 7 267.90 7.20 1 -2 -9 -7 243.30 7.80 1 2 9 8 297.70 8.00 1 -2 -9 -8 310.40 9.80 1 2 9 9 225.80 6.60 1 -2 -9 -9 239.60 8.40 1 2 9 10 38.90 2.40 1 -2 -9 -10 38.80 2.90 1 2 9 11 27.40 2.20 1 -2 -9 -11 29.90 2.50 1 2 9 12 233.20 6.50 1 -2 -9 -12 218.10 8.10 1 2 9 13 144.90 5.00 1 -2 -9 -13 153.60 6.30 1 2 9 14 152.40 5.20 1 -2 -9 -14 136.80 6.20 1 2 9 15 134.30 4.80 1 -2 -9 -15 124.00 6.20 1 2 9 16 67.20 4.20 1 -2 -9 -16 67.60 5.40 1 2 9 17 14.40 3.30 1 -2 -9 -17 8.90 4.00 1 2 9 18 274.80 15.10 1 -2 -9 -18 272.50 15.40 1 -2 -9 -19 145.30 10.80 1 -2 -9 -20 56.60 6.90 1 2 9 21 106.90 9.10 1 -2 -9 -21 118.50 10.00 1 2 9 22 9.40 4.10 1 -2 -9 -22 3.50 3.80 1 -2 -9 -23 -5.20 4.80 1 -2 -9 -24 107.60 9.90 1 2 9 25 29.60 5.70 1 -2 -9 -25 20.00 6.60 1 2 10 0 14.20 2.60 1 2 10 1 111.90 5.60 1 -2 -10 -1 112.70 5.40 1 2 10 2 41.80 3.50 1 -2 -10 -2 40.40 2.70 1 2 10 3 488.70 16.40 1 -2 -10 -3 437.60 14.60 1 2 10 4 27.40 2.70 1 -2 -10 -4 29.30 3.30 1 2 10 5 257.20 7.30 1 -2 -10 -5 263.10 12.40 1 2 10 6 4.80 1.70 1 -2 -10 -6 1.40 2.10 1 2 10 7 155.50 5.40 1 2 10 8 120.70 9.40 1 -2 -10 -8 108.80 7.30 1 2 10 9 220.80 8.50 1 -2 -10 -9 192.00 11.60 1 2 10 10 26.00 2.80 1 -2 -10 -10 22.30 4.10 1 2 10 11 275.20 9.60 1 -2 -10 -11 269.30 12.90 1 2 10 12 0.60 2.50 1 -2 -10 -12 -1.90 3.10 1 2 10 13 59.30 6.40 1 -2 -10 -13 43.40 5.10 1 2 10 14 40.20 6.40 1 -2 -10 -14 27.20 4.50 1 2 10 15 126.90 7.10 1 -2 -10 -15 101.20 7.70 1 2 10 16 110.00 9.30 1 -2 -10 -16 113.50 8.50 1 2 10 17 167.50 12.20 1 -2 -10 -17 149.00 11.30 1 2 10 18 23.00 3.30 1 -2 -10 -18 16.10 4.60 1 2 10 19 54.20 6.60 1 -2 -10 -19 45.30 6.50 1 2 10 20 26.40 5.40 1 2 10 21 49.40 4.70 1 2 10 22 39.10 4.50 1 2 11 0 5.00 4.80 1 2 11 1 21.50 5.60 1 -2 -11 -1 15.30 2.90 1 2 11 2 77.10 7.70 1 -2 -11 -2 77.10 5.40 1 2 11 3 70.40 7.10 1 -2 -11 -3 62.60 4.30 1 2 11 4 311.50 18.00 1 -2 -11 -4 318.20 16.50 1 2 11 5 30.80 6.30 1 -2 -11 -5 26.60 4.40 1 2 11 6 17.60 3.00 1 -2 -11 -6 28.50 4.10 1 2 11 7 19.80 5.40 1 -2 -11 -7 28.50 4.80 1 2 11 8 34.50 6.30 1 -2 -11 -8 32.60 5.00 1 2 11 9 62.00 4.20 1 -2 -11 -9 60.80 6.30 1 2 11 10 114.80 10.50 1 -2 -11 -10 120.40 8.60 1 2 11 11 75.90 8.10 1 -2 -11 -11 51.60 5.70 1 2 11 12 25.40 3.40 1 -2 -11 -12 39.70 5.40 1 2 11 13 24.80 6.10 1 -2 -11 -13 11.90 5.10 1 2 11 14 124.30 10.60 1 -2 -11 -14 96.70 9.10 1 2 11 15 44.70 4.20 1 -2 -11 -15 67.10 6.80 1 2 11 16 41.50 7.10 1 -2 -11 -16 25.00 4.40 1 2 11 17 37.40 5.60 1 -2 -11 -17 44.10 6.10 1 2 11 18 17.50 5.00 1 -2 -11 -18 22.70 4.50 1 2 12 0 1.10 6.40 1 2 12 1 45.20 6.30 1 -2 -12 -1 43.10 7.30 1 2 12 2 6.80 5.90 1 -2 -12 -2 6.70 4.20 1 2 12 3 269.50 17.70 1 2 12 4 59.40 7.40 1 2 12 5 85.30 9.20 1 2 12 6 9.40 4.80 1 2 12 7 42.70 7.50 1 2 12 8 18.80 4.80 1 2 12 9 215.80 15.70 1 2 12 10 9.40 4.50 1 2 12 11 102.10 9.30 1 2 12 12 9.70 6.50 1 3 0 0 3.10 0.60 1 3 0 1 3583.20 81.80 1 3 0 2 389.50 6.00 1 3 0 3 239.40 3.90 1 3 0 4 26.90 1.00 1 3 0 5 3847.60 87.90 1 3 0 6 1.10 0.60 1 3 0 7 3504.70 81.00 1 3 0 8 38.00 1.50 1 3 0 9 833.10 17.30 1 3 0 10 14.40 1.20 1 3 0 11 1608.30 31.80 1 3 0 12 19.60 2.60 1 3 0 13 2832.40 67.10 1 3 0 14 101.10 4.10 1 3 0 15 241.70 7.80 1 3 0 16 7.40 1.50 1 3 0 17 631.10 16.90 1 3 0 18 1.60 2.30 1 3 0 19 1611.20 58.00 1 3 0 20 65.40 3.40 1 3 0 21 689.10 19.80 1 3 0 22 37.90 2.90 1 3 0 23 422.00 13.10 1 3 0 24 56.60 4.00 1 3 0 25 746.60 21.40 1 3 0 26 3.50 1.90 1 3 0 27 270.90 10.00 1 3 0 28 36.80 3.80 1 3 0 29 25.60 3.30 1 3 0 30 2.90 3.20 1 3 0 31 275.60 11.80 1 3 0 32 68.50 5.60 1 3 0 33 84.30 6.00 1 3 0 34 3.90 2.60 1 3 1 0 386.90 6.50 1 3 1 1 110.60 2.10 1 -3 -1 -1 99.50 1.90 1 3 1 2 921.70 14.30 1 -3 -1 -2 920.60 11.90 1 3 1 3 80.20 1.70 1 -3 -1 -3 69.00 1.60 1 3 1 4 289.10 5.10 1 -3 -1 -4 295.60 5.10 1 3 1 5 34.70 1.20 1 -3 -1 -5 47.70 1.80 1 3 1 6 61.40 1.70 1 -3 -1 -6 55.80 1.70 1 3 1 7 448.00 7.50 1 -3 -1 -7 415.80 8.00 1 3 1 8 652.00 10.60 1 -3 -1 -8 649.40 11.60 1 3 1 9 19.80 1.20 1 -3 -1 -9 17.50 1.30 1 3 1 10 330.80 9.50 1 -3 -1 -10 353.80 8.40 1 3 1 11 192.60 6.20 1 -3 -1 -11 189.20 4.90 1 3 1 12 137.70 5.00 1 -3 -1 -12 153.70 5.40 1 3 1 13 280.50 8.70 1 -3 -1 -13 296.50 7.40 1 3 1 14 244.90 7.90 1 -3 -1 -14 225.20 7.40 1 3 1 15 24.50 2.30 1 -3 -1 -15 25.50 2.30 1 3 1 16 290.00 8.90 1 -3 -1 -16 304.20 9.20 1 3 1 17 287.40 14.10 1 -3 -1 -17 308.80 9.40 1 3 1 18 48.90 4.50 1 -3 -1 -18 51.60 4.00 1 3 1 19 603.50 16.30 1 -3 -1 -19 562.40 22.50 1 3 1 20 222.30 11.50 1 -3 -1 -20 189.50 9.80 1 3 1 21 187.20 9.80 1 -3 -1 -21 193.00 10.20 1 3 1 22 43.00 2.90 1 -3 -1 -22 32.50 2.90 1 3 1 23 132.20 5.60 1 -3 -1 -23 120.30 5.80 1 3 1 24 80.40 4.80 1 -3 -1 -24 75.70 4.20 1 3 1 25 560.40 16.70 1 -3 -1 -25 522.10 15.30 1 3 1 26 64.20 4.00 1 -3 -1 -26 71.60 4.30 1 3 1 27 142.00 9.10 1 -3 -1 -27 155.70 9.50 1 3 1 28 77.50 4.90 1 -3 -1 -28 77.50 4.50 1 3 1 29 37.60 3.30 1 -3 -1 -29 42.50 4.30 1 3 1 30 56.40 4.70 1 -3 -1 -30 52.10 4.40 1 3 1 31 365.90 15.10 1 -3 -1 -31 408.30 22.60 1 3 1 32 24.90 3.90 1 -3 -1 -32 8.40 6.20 1 3 1 33 194.30 9.50 1 -3 -1 -33 152.10 8.10 1 3 1 34 31.20 4.70 1 -3 -1 -34 24.40 4.70 1 3 2 0 124.00 2.60 1 3 2 1 1713.50 23.60 1 -3 -2 -1 1759.40 26.20 1 3 2 2 18.10 0.80 1 -3 -2 -2 15.10 0.80 1 3 2 3 93.60 1.90 1 -3 -2 -3 101.70 1.90 1 3 2 4 9.70 0.70 1 -3 -2 -4 7.90 0.80 1 3 2 5 1355.40 20.50 1 -3 -2 -5 1339.10 22.70 1 3 2 6 46.70 1.40 1 -3 -2 -6 53.10 1.80 1 3 2 7 1598.90 24.40 1 -3 -2 -7 1591.20 27.10 1 3 2 8 57.00 1.80 1 -3 -2 -8 56.50 2.10 1 3 2 9 321.80 7.60 1 -3 -2 -9 328.20 6.50 1 3 2 10 241.70 6.10 1 -3 -2 -10 249.60 5.90 1 3 2 11 409.60 9.30 1 -3 -2 -11 412.00 9.30 1 3 2 12 157.60 5.30 1 -3 -2 -12 135.00 4.90 1 3 2 13 1069.10 26.60 1 -3 -2 -13 974.80 20.40 1 3 2 14 21.70 2.30 1 -3 -2 -14 13.80 1.20 1 3 2 15 306.10 9.10 1 -3 -2 -15 323.40 9.60 1 3 2 16 157.40 5.70 1 -3 -2 -16 147.70 5.10 1 3 2 17 266.70 8.80 1 -3 -2 -17 258.00 7.90 1 3 2 18 121.30 5.20 1 -3 -2 -18 134.30 5.10 1 3 2 19 725.30 19.50 1 -3 -2 -19 752.70 28.60 1 3 2 20 113.40 4.60 1 -3 -2 -20 112.20 5.80 1 3 2 21 47.50 3.20 1 -3 -2 -21 59.90 3.30 1 3 2 22 96.70 4.70 1 -3 -2 -22 101.10 4.80 1 3 2 23 25.90 2.90 1 -3 -2 -23 22.10 2.50 1 3 2 24 94.30 4.90 1 -3 -2 -24 101.00 4.90 1 3 2 25 492.20 15.70 1 -3 -2 -25 447.60 13.80 1 3 2 26 51.70 4.10 1 -3 -2 -26 43.80 3.20 1 3 2 27 177.40 7.50 1 -3 -2 -27 192.20 8.50 1 3 2 28 297.00 11.20 1 -3 -2 -28 329.20 11.40 1 3 2 29 0.80 2.40 1 -3 -2 -29 5.90 3.00 1 3 2 30 83.50 5.50 1 -3 -2 -30 73.90 5.00 1 3 2 31 81.90 6.10 1 -3 -2 -31 75.40 5.80 1 3 2 32 0.90 2.50 1 -3 -2 -32 2.10 2.80 1 3 2 33 78.40 6.40 1 -3 -2 -33 73.40 5.80 1 3 3 0 75.90 2.00 1 3 3 1 162.80 3.20 1 -3 -3 -1 189.00 4.00 1 3 3 2 1854.70 25.30 1 -3 -3 -2 1868.40 27.60 1 3 3 3 936.00 13.50 1 -3 -3 -3 914.60 11.70 1 3 3 4 2620.70 43.20 1 -3 -3 -4 2621.00 49.60 1 3 3 5 376.60 7.30 1 -3 -3 -5 366.00 7.20 1 3 3 6 211.70 4.40 1 -3 -3 -6 209.70 4.30 1 3 3 7 192.80 4.10 1 -3 -3 -7 184.90 4.60 1 3 3 8 1839.90 43.90 1 -3 -3 -8 1950.80 46.70 1 3 3 9 238.00 7.20 1 -3 -3 -9 229.00 4.80 1 3 3 10 2227.80 53.00 1 -3 -3 -10 2212.20 42.80 1 3 3 11 375.60 10.90 1 -3 -3 -11 396.70 9.10 1 3 3 12 72.70 3.50 1 -3 -3 -12 82.60 3.40 1 3 3 13 26.50 2.10 1 -3 -3 -13 28.30 1.60 1 3 3 14 482.20 13.30 1 -3 -3 -14 472.80 10.50 1 3 3 15 371.00 11.10 1 -3 -3 -15 363.10 8.50 1 3 3 16 2359.30 56.90 1 -3 -3 -16 2340.60 55.90 1 3 3 17 341.50 10.20 1 -3 -3 -17 323.30 9.90 1 3 3 18 503.60 14.90 1 -3 -3 -18 481.90 14.00 1 3 3 19 60.50 3.90 1 -3 -3 -19 54.80 3.30 1 3 3 20 311.90 9.90 1 -3 -3 -20 247.80 8.40 1 3 3 21 153.30 6.30 1 -3 -3 -21 169.60 6.20 1 3 3 22 669.00 19.40 1 -3 -3 -22 625.00 18.20 1 3 3 23 114.10 5.20 1 -3 -3 -23 105.50 8.20 1 3 3 24 268.60 10.00 1 -3 -3 -24 247.50 13.20 1 3 3 25 45.10 3.60 1 -3 -3 -25 34.20 3.10 1 3 3 26 124.00 5.80 1 -3 -3 -26 131.30 5.90 1 3 3 27 12.10 3.20 1 -3 -3 -27 11.70 3.30 1 3 3 28 449.00 14.60 1 -3 -3 -28 438.10 15.20 1 3 3 29 142.40 7.70 1 -3 -3 -29 162.20 12.80 1 3 3 30 47.60 4.40 1 -3 -3 -30 56.30 7.20 1 3 3 31 7.20 3.00 1 -3 -3 -31 7.80 3.20 1 3 3 32 4.60 2.80 1 -3 -3 -32 2.30 3.30 1 3 3 33 4.50 3.20 1 -3 -3 -33 -0.70 2.90 1 3 4 0 42.70 1.40 1 3 4 1 12.80 1.00 1 -3 -4 -1 11.60 0.90 1 3 4 2 4.50 0.70 1 -3 -4 -2 5.80 0.50 1 3 4 3 260.00 5.10 1 -3 -4 -3 251.50 4.40 1 3 4 4 51.00 1.60 1 -3 -4 -4 49.70 1.20 1 3 4 5 200.30 4.20 1 -3 -4 -5 206.90 4.20 1 3 4 6 9.20 1.00 1 -3 -4 -6 10.00 0.70 1 3 4 7 15.60 1.30 1 -3 -4 -7 17.80 0.80 1 3 4 8 125.50 4.50 1 -3 -4 -8 126.60 3.60 1 3 4 9 110.90 4.20 1 -3 -4 -9 99.40 2.80 1 3 4 10 259.60 8.10 1 -3 -4 -10 259.50 5.90 1 3 4 11 39.80 2.60 1 -3 -4 -11 55.50 2.00 1 3 4 12 23.50 2.10 1 -3 -4 -12 23.40 1.40 1 3 4 13 30.60 2.40 1 -3 -4 -13 24.70 1.40 1 3 4 14 80.90 3.80 1 -3 -4 -14 67.70 2.50 1 3 4 15 274.10 13.00 1 -3 -4 -15 254.40 8.00 1 3 4 16 278.80 9.00 1 -3 -4 -16 284.50 7.20 1 3 4 17 110.80 4.80 1 -3 -4 -17 103.90 4.50 1 3 4 18 125.80 5.50 1 -3 -4 -18 107.70 7.10 1 3 4 19 5.20 2.20 1 -3 -4 -19 6.40 1.60 1 3 4 20 69.40 4.20 1 -3 -4 -20 72.80 3.80 1 3 4 21 155.60 6.30 1 -3 -4 -21 134.90 6.00 1 3 4 22 476.00 14.90 1 -3 -4 -22 461.30 20.80 1 3 4 23 117.60 5.70 1 -3 -4 -23 142.80 9.90 1 3 4 24 131.90 5.90 1 -3 -4 -24 134.60 9.10 1 3 4 25 10.90 2.70 1 -3 -4 -25 5.10 4.40 1 3 4 26 70.40 4.60 1 -3 -4 -26 73.20 7.30 1 3 4 27 38.40 3.80 1 -3 -4 -27 47.50 6.90 1 3 4 28 349.60 14.30 1 -3 -4 -28 354.80 14.30 1 3 4 29 91.80 5.90 1 -3 -4 -29 85.40 5.50 1 3 4 30 202.40 10.40 1 -3 -4 -30 182.80 9.20 1 3 4 31 5.80 3.00 1 -3 -4 -31 12.70 6.00 1 3 4 32 47.30 5.20 1 -3 -4 -32 50.30 8.70 1 3 5 0 100.70 2.50 1 3 5 1 225.00 4.60 1 -3 -5 -1 215.40 4.60 1 3 5 2 1013.90 17.50 1 -3 -5 -2 1021.10 15.60 1 3 5 3 603.50 10.80 1 -3 -5 -3 656.20 10.50 1 3 5 4 1287.00 25.40 1 -3 -5 -4 1316.40 18.20 1 3 5 5 370.70 10.50 1 -3 -5 -5 359.60 5.40 1 3 5 6 60.20 2.60 1 -3 -5 -6 70.30 1.50 1 3 5 7 329.40 7.80 1 -3 -5 -7 326.00 5.50 1 3 5 8 469.90 10.60 1 -3 -5 -8 477.20 7.80 1 3 5 9 437.00 10.10 1 -3 -5 -9 448.90 8.20 1 3 5 10 1279.00 31.80 1 -3 -5 -10 1228.30 20.90 1 3 5 11 127.50 4.70 1 -3 -5 -11 141.50 3.70 1 3 5 12 403.30 11.90 1 -3 -5 -12 397.70 8.80 1 3 5 13 93.80 4.20 1 -3 -5 -13 93.70 2.90 1 3 5 14 666.00 18.20 1 -3 -5 -14 620.70 16.80 1 3 5 15 330.70 10.50 1 -3 -5 -15 306.00 7.60 1 3 5 16 429.30 12.30 1 -3 -5 -16 437.30 12.80 1 3 5 17 7.60 1.90 1 -3 -5 -17 9.90 2.70 1 3 5 18 240.40 8.00 1 -3 -5 -18 225.30 12.00 1 3 5 19 148.80 6.10 1 -3 -5 -19 108.50 7.60 1 3 5 20 62.90 4.00 1 -3 -5 -20 46.10 4.80 1 3 5 21 222.40 8.70 1 -3 -5 -21 178.90 10.50 1 3 5 22 598.50 18.30 1 -3 -5 -22 620.30 28.00 1 3 5 23 148.00 6.50 1 -3 -5 -23 136.00 9.90 1 3 5 24 111.20 6.40 1 -3 -5 -24 123.30 5.40 1 3 5 25 20.70 2.90 1 -3 -5 -25 16.00 2.60 1 3 5 26 3.90 3.10 1 -3 -5 -26 0.90 4.50 1 3 5 27 134.30 7.10 1 -3 -5 -27 137.50 10.30 1 3 5 28 112.30 6.70 1 -3 -5 -28 89.80 8.90 1 3 5 29 18.40 3.40 1 -3 -5 -29 26.30 7.20 1 3 5 30 205.80 10.10 1 -3 -5 -30 209.80 15.20 1 3 5 31 50.40 4.60 1 -3 -5 -31 42.80 8.30 1 3 6 0 610.60 12.80 1 3 6 1 875.30 17.50 1 -3 -6 -1 880.70 15.40 1 3 6 2 432.40 7.90 1 -3 -6 -2 419.20 7.00 1 3 6 3 28.60 1.50 1 -3 -6 -3 38.40 1.20 1 3 6 4 33.50 1.80 1 -3 -6 -4 30.90 1.00 1 3 6 5 814.10 17.10 1 -3 -6 -5 809.80 10.50 1 3 6 6 371.40 10.80 1 -3 -6 -6 398.40 7.40 1 3 6 7 938.30 23.80 1 -3 -6 -7 949.00 16.50 1 3 6 8 514.30 11.40 1 -3 -6 -8 525.60 11.70 1 3 6 9 12.20 1.80 1 -3 -6 -9 13.10 0.50 1 3 6 10 48.70 2.40 1 -3 -6 -10 39.80 1.10 1 3 6 11 397.90 10.10 1 -3 -6 -11 404.90 7.40 1 3 6 12 172.50 6.10 1 -3 -6 -12 160.50 3.40 1 3 6 13 459.60 13.50 1 -3 -6 -13 395.20 11.70 1 3 6 14 650.90 18.30 1 -3 -6 -14 618.10 16.30 1 3 6 15 8.30 2.00 1 -3 -6 -15 15.20 1.50 1 3 6 16 76.70 4.30 1 -3 -6 -16 69.40 5.50 1 3 6 17 320.60 11.00 1 -3 -6 -17 329.60 10.30 1 3 6 18 283.00 9.70 1 -3 -6 -18 248.00 13.60 1 3 6 19 394.80 12.40 1 -3 -6 -19 365.80 18.80 1 3 6 20 214.50 8.20 1 -3 -6 -20 191.30 12.60 1 3 6 21 42.10 3.30 1 -3 -6 -21 38.00 5.50 1 3 6 22 118.90 5.90 1 -3 -6 -22 98.40 8.50 1 3 6 23 196.20 8.10 1 -3 -6 -23 180.40 12.40 1 3 6 24 15.70 2.80 1 -3 -6 -24 9.30 3.70 1 3 6 25 167.80 8.40 1 -3 -6 -25 112.30 10.90 1 3 6 26 214.70 10.30 1 -3 -6 -26 198.50 13.40 1 3 6 27 17.10 3.70 1 -3 -6 -27 8.50 5.60 1 3 6 28 45.50 4.70 1 -3 -6 -28 38.70 7.50 1 3 6 29 49.70 4.40 1 -3 -6 -29 45.30 6.90 1 3 7 0 289.30 5.50 1 3 7 1 46.20 1.30 1 -3 -7 -1 53.90 1.50 1 3 7 2 105.70 3.30 1 -3 -7 -2 111.50 2.90 1 3 7 3 31.10 1.70 1 -3 -7 -3 26.40 1.30 1 3 7 4 168.00 4.60 1 -3 -7 -4 170.00 4.00 1 3 7 5 27.80 1.80 1 -3 -7 -5 26.50 1.40 1 3 7 6 87.80 3.30 1 -3 -7 -6 88.60 2.90 1 3 7 7 37.90 1.90 1 -3 -7 -7 30.30 1.60 1 3 7 8 107.80 3.60 1 -3 -7 -8 107.40 3.40 1 3 7 9 114.30 4.00 1 -3 -7 -9 122.30 3.60 1 3 7 10 167.90 5.20 1 -3 -7 -10 169.00 6.30 1 3 7 11 15.00 1.60 1 -3 -7 -11 10.30 2.80 1 3 7 12 98.50 3.70 1 -3 -7 -12 88.30 5.70 1 3 7 13 62.90 3.00 1 -3 -7 -13 49.90 4.60 1 3 7 14 21.80 2.40 1 -3 -7 -14 29.10 4.10 1 3 7 15 52.50 3.50 1 -3 -7 -15 45.60 4.40 1 3 7 16 66.10 4.10 1 -3 -7 -16 61.10 5.60 1 3 7 17 12.50 2.20 1 -3 -7 -17 7.70 3.60 1 3 7 18 211.60 8.00 1 -3 -7 -18 209.60 11.60 1 3 7 19 99.10 5.10 1 -3 -7 -19 96.80 7.30 1 3 7 20 12.80 2.50 1 -3 -7 -20 -1.50 3.90 1 3 7 21 104.70 5.40 1 -3 -7 -21 88.60 8.40 1 3 7 22 29.80 3.50 1 -3 -7 -22 34.70 5.50 1 3 7 23 10.90 2.50 1 -3 -7 -23 5.00 5.00 1 3 7 24 129.00 7.30 1 -3 -7 -24 108.50 10.10 1 3 7 25 100.10 6.20 1 -3 -7 -25 91.20 9.40 1 3 7 26 115.60 6.80 1 -3 -7 -26 81.20 9.30 1 3 7 27 77.50 5.40 1 -3 -7 -27 77.10 9.60 1 3 7 28 -3.10 3.50 1 -3 -7 -28 8.40 6.10 1 3 8 0 843.90 31.50 1 3 8 1 346.20 14.80 1 -3 -8 -1 308.70 13.30 1 3 8 2 257.20 12.30 1 -3 -8 -2 253.60 7.90 1 3 8 3 4.90 2.50 1 -3 -8 -3 15.70 1.20 1 3 8 4 132.90 7.20 1 -3 -8 -4 169.50 4.60 1 3 8 5 90.20 3.60 1 -3 -8 -5 89.00 3.20 1 3 8 6 960.00 20.30 1 -3 -8 -6 961.10 25.00 1 3 8 7 460.00 11.50 1 -3 -8 -7 466.30 12.50 1 3 8 8 148.90 6.10 1 -3 -8 -8 146.40 5.20 1 3 8 9 63.50 3.60 1 -3 -8 -9 59.70 3.10 1 3 8 10 42.90 2.70 1 -3 -8 -10 42.60 2.80 1 3 8 11 133.50 5.00 1 -3 -8 -11 118.10 4.80 1 3 8 12 803.50 18.30 1 -3 -8 -12 764.10 21.40 1 3 8 13 239.80 7.10 1 -3 -8 -13 203.80 8.10 1 3 8 14 251.00 7.50 1 -3 -8 -14 268.20 13.90 1 3 8 15 151.70 5.50 1 -3 -8 -15 125.80 9.10 1 3 8 16 27.00 2.40 1 -3 -8 -16 19.00 3.70 1 3 8 17 40.20 3.20 1 -3 -8 -17 34.90 5.00 1 3 8 18 254.80 13.80 1 -3 -8 -18 236.00 14.40 1 3 8 19 145.40 6.50 1 -3 -8 -19 130.40 9.60 1 3 8 20 199.00 9.30 1 -3 -8 -20 203.10 13.60 1 3 8 21 98.80 5.90 1 -3 -8 -21 98.60 8.90 1 3 8 22 6.10 2.20 1 -3 -8 -22 -1.10 3.40 1 3 8 23 7.20 2.70 1 -3 -8 -23 1.80 5.20 1 3 8 24 88.70 6.00 1 -3 -8 -24 95.50 10.10 1 3 8 25 115.10 10.10 1 -3 -8 -25 143.10 11.70 1 3 9 0 0.90 2.00 1 3 9 1 32.40 3.00 1 -3 -9 -1 24.40 2.50 1 3 9 2 104.60 4.90 1 -3 -9 -2 99.70 4.00 1 3 9 3 338.70 9.00 1 -3 -9 -3 359.70 11.40 1 3 9 4 151.40 4.90 1 -3 -9 -4 146.00 5.90 1 3 9 5 185.70 5.90 1 -3 -9 -5 176.20 8.70 1 3 9 6 71.90 3.40 1 -3 -9 -6 66.90 5.20 1 3 9 7 4.90 1.80 1 -3 -9 -7 1.80 2.30 1 3 9 8 144.10 5.00 1 -3 -9 -8 136.70 7.70 1 3 9 9 218.00 6.90 1 -3 -9 -9 197.10 9.90 1 3 9 10 36.60 2.80 1 3 9 11 148.30 5.40 1 -3 -9 -11 162.50 9.20 1 3 9 12 8.50 2.10 1 -3 -9 -12 8.50 3.00 1 3 9 13 69.40 3.50 1 -3 -9 -13 81.50 4.60 1 3 9 14 247.30 8.00 1 -3 -9 -14 237.40 9.10 1 3 9 15 74.10 3.70 1 -3 -9 -15 69.00 4.20 1 3 9 16 25.70 2.80 1 -3 -9 -16 27.10 3.10 1 3 9 17 118.10 6.80 1 -3 -9 -17 98.10 8.50 1 3 9 18 0.80 2.80 1 -3 -9 -18 1.20 4.00 1 3 9 19 31.40 4.30 1 -3 -9 -19 15.80 5.00 1 3 9 20 66.70 6.00 1 -3 -9 -20 57.50 7.20 1 3 9 21 38.40 5.70 1 -3 -9 -21 43.80 5.90 1 3 9 22 40.90 6.50 1 -3 -9 -22 28.80 5.70 1 3 9 23 111.20 9.80 1 -3 -9 -23 112.70 11.10 1 3 10 0 128.70 6.10 1 3 10 1 87.90 4.80 1 -3 -10 -1 99.40 9.10 1 3 10 2 83.50 4.10 1 -3 -10 -2 103.30 8.80 1 3 10 3 63.70 3.60 1 -3 -10 -3 82.90 7.90 1 3 10 4 40.00 2.80 1 -3 -10 -4 62.10 7.70 1 3 10 5 26.40 2.60 1 3 10 6 172.30 6.10 1 3 10 7 66.20 4.30 1 3 10 8 61.90 3.50 1 3 10 9 24.40 2.70 1 3 10 10 55.20 3.30 1 3 10 11 17.60 3.50 1 3 10 12 146.30 8.00 1 3 10 13 113.30 6.70 1 3 10 14 41.10 4.30 1 3 10 15 52.60 4.90 1 3 10 16 41.10 4.20 1 3 10 17 34.60 4.50 1 3 10 18 70.30 5.60 1 3 10 19 33.20 7.70 1 3 11 0 16.30 4.60 1 3 11 1 202.20 13.90 1 -3 -11 -1 209.70 14.50 1 3 11 2 34.10 4.70 1 -3 -11 -2 34.00 6.60 1 3 11 3 451.20 17.00 1 -3 -11 -3 447.60 23.60 1 3 11 4 9.90 2.80 1 3 11 5 141.20 7.80 1 3 11 6 -0.30 3.90 1 3 11 7 23.30 6.50 1 3 11 8 37.30 4.20 1 3 11 9 422.90 26.60 1 3 11 10 92.00 6.30 1 3 11 11 143.10 11.20 1 3 11 12 6.20 6.00 1 3 11 13 3.20 6.10 1 3 11 14 7.10 3.40 1 3 11 15 143.40 8.60 1 3 12 0 9.70 5.00 1 3 12 1 8.50 6.40 1 -3 -12 -1 9.50 5.00 1 3 12 2 48.20 6.90 1 -3 -12 -2 50.00 8.40 1 3 12 3 1.90 6.50 1 3 12 4 4.10 4.40 1 3 12 5 -2.20 6.10 1 3 12 6 38.30 7.10 1 3 12 7 -4.80 6.40 1 4 0 0 227.20 6.60 1 4 0 1 84.70 2.60 1 4 0 2 153.30 3.90 1 4 0 3 84.80 2.20 1 4 0 4 9.90 0.80 1 4 0 5 48.00 1.60 1 4 0 6 167.40 4.30 1 4 0 7 33.20 1.70 1 4 0 8 11.50 1.20 1 4 0 9 36.30 1.90 1 4 0 10 3.80 1.10 1 4 0 11 123.10 4.80 1 4 0 12 137.10 5.20 1 4 0 13 360.00 10.80 1 4 0 14 24.20 2.30 1 4 0 15 2.70 1.90 1 4 0 16 6.70 1.70 1 4 0 17 53.90 3.30 1 4 0 18 2.80 2.00 1 4 0 19 403.70 17.20 1 4 0 20 44.40 3.30 1 4 0 21 52.60 3.80 1 4 0 22 2.70 1.90 1 4 0 23 67.20 4.30 1 4 0 24 17.10 2.70 1 4 0 25 287.10 10.70 1 4 0 26 36.70 3.70 1 4 0 27 274.30 10.60 1 4 0 28 36.10 3.80 1 4 0 29 25.00 3.90 1 4 0 30 36.20 4.40 1 4 0 31 174.60 9.30 1 4 0 32 8.00 4.00 1 4 1 0 8.40 1.00 1 4 1 1 2390.10 45.80 1 -4 -1 -1 2287.40 43.70 1 4 1 2 258.70 4.80 1 -4 -1 -2 293.30 5.90 1 4 1 3 38.40 1.50 1 -4 -1 -3 31.20 1.00 1 4 1 4 173.90 3.90 1 -4 -1 -4 173.70 3.30 1 4 1 5 1419.90 24.30 1 -4 -1 -5 1407.60 21.60 1 4 1 6 152.10 3.60 1 -4 -1 -6 147.60 3.40 1 4 1 7 2147.90 41.80 1 -4 -1 -7 2175.80 52.00 1 4 1 8 93.10 3.00 1 -4 -1 -8 95.60 4.20 1 4 1 9 251.70 6.30 1 -4 -1 -9 225.60 7.80 1 4 1 10 98.30 3.30 1 -4 -1 -10 100.40 4.30 1 4 1 11 1071.80 27.50 1 -4 -1 -11 1119.00 28.50 1 4 1 12 73.20 3.70 1 -4 -1 -12 84.60 3.80 1 4 1 13 1592.90 39.70 1 -4 -1 -13 1606.90 40.10 1 4 1 14 4.10 1.50 1 -4 -1 -14 6.30 1.60 1 4 1 15 268.10 8.90 1 -4 -1 -15 286.20 13.00 1 4 1 16 372.70 11.30 1 -4 -1 -16 352.40 11.60 1 4 1 17 428.20 12.90 1 -4 -1 -17 434.40 13.10 1 4 1 18 96.30 4.70 1 -4 -1 -18 89.10 4.20 1 4 1 19 1186.30 31.40 1 -4 -1 -19 1126.60 30.10 1 4 1 20 7.00 2.10 1 -4 -1 -20 7.90 2.30 1 4 1 21 177.30 7.40 1 -4 -1 -21 167.10 7.00 1 4 1 22 143.00 6.40 1 -4 -1 -22 118.40 5.60 1 4 1 23 118.00 5.90 1 -4 -1 -23 101.70 4.80 1 4 1 24 161.30 7.30 1 -4 -1 -24 161.30 7.00 1 4 1 25 472.80 16.10 1 -4 -1 -25 494.90 16.20 1 4 1 26 15.00 2.80 1 -4 -1 -26 21.20 3.10 1 4 1 27 178.80 7.90 1 -4 -1 -27 158.70 7.60 1 4 1 28 37.80 4.30 1 -4 -1 -28 31.90 3.60 1 4 1 29 23.60 3.30 1 -4 -1 -29 17.70 3.10 1 4 1 30 98.80 6.30 1 -4 -1 -30 76.80 5.70 1 4 1 31 201.10 10.00 1 -4 -1 -31 210.50 10.50 1 4 1 32 10.10 3.00 1 -4 -1 -32 12.20 3.10 1 4 2 0 298.00 6.20 1 4 2 1 40.70 1.70 1 -4 -2 -1 50.60 1.80 1 4 2 2 917.40 14.80 1 -4 -2 -2 914.00 16.20 1 4 2 3 9.40 1.00 1 -4 -2 -3 11.60 1.20 1 4 2 4 2352.80 45.50 1 -4 -2 -4 2330.30 44.50 1 4 2 5 116.30 3.50 1 -4 -2 -5 114.60 2.80 1 4 2 6 84.00 2.40 1 -4 -2 -6 93.20 2.40 1 4 2 7 6.10 1.00 1 -4 -2 -7 8.30 0.90 1 4 2 8 812.40 17.40 1 -4 -2 -8 778.70 16.90 1 4 2 9 28.00 2.10 1 -4 -2 -9 32.30 2.00 1 4 2 10 1056.10 26.30 1 -4 -2 -10 1028.10 26.40 1 4 2 11 158.00 8.50 1 -4 -2 -11 183.50 5.30 1 4 2 12 220.30 7.40 1 -4 -2 -12 234.80 7.60 1 4 2 13 170.50 6.10 1 -4 -2 -13 161.20 5.80 1 4 2 14 982.80 25.40 1 -4 -2 -14 910.10 23.70 1 4 2 15 10.70 1.90 1 -4 -2 -15 7.10 2.20 1 4 2 16 516.00 15.00 1 -4 -2 -16 539.50 15.30 1 4 2 17 132.80 5.40 1 -4 -2 -17 127.50 5.30 1 4 2 18 37.90 2.90 1 -4 -2 -18 47.20 3.10 1 4 2 19 107.60 5.40 1 -4 -2 -19 127.20 5.50 1 4 2 20 245.50 8.80 1 -4 -2 -20 238.00 8.80 1 4 2 21 67.80 6.00 1 -4 -2 -21 74.20 3.90 1 4 2 22 739.50 30.00 1 -4 -2 -22 841.70 23.80 1 4 2 23 87.50 5.00 1 -4 -2 -23 68.70 4.10 1 4 2 24 33.60 3.40 1 -4 -2 -24 41.70 3.40 1 4 2 25 201.00 7.80 1 -4 -2 -25 225.80 8.90 1 4 2 26 78.60 5.20 1 -4 -2 -26 79.10 4.80 1 4 2 27 28.00 3.90 1 -4 -2 -27 31.30 3.60 1 4 2 28 168.60 8.40 1 -4 -2 -28 123.90 7.00 1 4 2 29 18.20 3.10 1 -4 -2 -29 19.50 3.00 1 4 2 30 46.70 5.00 1 -4 -2 -30 49.40 4.40 1 4 2 31 195.70 10.20 1 -4 -2 -31 156.30 8.50 1 4 3 0 62.40 2.10 1 4 3 1 218.30 4.80 1 -4 -3 -1 205.70 4.60 1 4 3 2 43.80 1.50 1 -4 -3 -2 46.40 1.80 1 4 3 3 151.40 3.20 1 -4 -3 -3 158.10 3.70 1 4 3 4 160.10 3.70 1 -4 -3 -4 159.50 4.30 1 4 3 5 250.90 6.40 1 -4 -3 -5 223.90 3.40 1 4 3 6 243.50 6.10 1 -4 -3 -6 227.90 4.70 1 4 3 7 147.70 4.20 1 -4 -3 -7 149.20 4.30 1 4 3 8 28.60 1.70 1 -4 -3 -8 23.70 1.70 1 4 3 9 182.10 5.70 1 -4 -3 -9 177.90 5.00 1 4 3 10 116.20 7.10 1 -4 -3 -10 136.30 4.10 1 4 3 11 111.20 6.90 1 -4 -3 -11 98.00 2.80 1 4 3 12 138.80 5.20 1 -4 -3 -12 156.50 4.50 1 4 3 13 299.00 9.50 1 -4 -3 -13 262.90 8.40 1 4 3 14 122.20 5.10 1 -4 -3 -14 116.20 4.50 1 4 3 15 36.00 2.70 1 -4 -3 -15 36.60 2.50 1 4 3 16 366.60 11.40 1 -4 -3 -16 395.60 12.20 1 4 3 17 10.70 2.20 1 -4 -3 -17 9.80 1.80 1 4 3 18 114.50 5.30 1 -4 -3 -18 113.10 4.90 1 4 3 19 47.40 3.30 1 -4 -3 -19 42.60 3.10 1 4 3 20 47.90 3.60 1 -4 -3 -20 40.70 3.10 1 4 3 21 212.50 7.90 1 -4 -3 -21 199.40 7.60 1 4 3 22 409.00 13.40 1 -4 -3 -22 428.20 13.70 1 4 3 23 28.90 3.70 1 -4 -3 -23 32.00 3.50 1 4 3 24 269.60 10.60 1 -4 -3 -24 271.30 9.60 1 4 3 25 16.40 3.40 1 -4 -3 -25 22.10 2.90 1 4 3 26 3.90 2.40 1 -4 -3 -26 9.00 2.50 1 4 3 27 93.00 6.00 1 -4 -3 -27 69.50 4.90 1 4 3 28 218.90 10.40 1 -4 -3 -28 190.20 9.00 1 4 3 29 1.20 2.40 1 -4 -3 -29 7.60 2.90 1 4 3 30 126.40 7.60 1 -4 -3 -30 165.40 12.60 1 4 3 31 6.70 3.10 1 -4 -3 -31 28.30 6.00 1 4 4 0 56.90 2.00 1 4 4 1 429.70 8.30 1 -4 -4 -1 428.90 8.20 1 4 4 2 1955.40 38.10 1 -4 -4 -2 1975.60 38.30 1 4 4 3 263.20 5.50 1 -4 -4 -3 275.10 5.60 1 4 4 4 1720.40 29.10 1 -4 -4 -4 1713.60 33.60 1 4 4 5 39.80 1.80 1 -4 -4 -5 38.00 1.90 1 4 4 6 105.20 3.40 1 -4 -4 -6 100.60 2.70 1 4 4 7 137.40 3.90 1 -4 -4 -7 156.80 3.50 1 4 4 8 1152.40 23.60 1 -4 -4 -8 1182.60 23.60 1 4 4 9 778.70 21.50 1 -4 -4 -9 767.40 14.20 1 4 4 10 1357.60 47.10 1 -4 -4 -10 1454.20 29.80 1 4 4 11 37.60 2.60 1 -4 -4 -11 36.40 2.30 1 4 4 12 167.00 6.40 1 -4 -4 -12 163.70 4.60 1 4 4 13 61.20 3.80 1 -4 -4 -13 43.00 2.50 1 4 4 14 404.50 12.00 1 -4 -4 -14 422.40 17.60 1 4 4 15 182.20 7.00 1 -4 -4 -15 188.50 6.60 1 4 4 16 962.80 26.30 1 -4 -4 -16 982.50 26.10 1 4 4 17 409.50 12.70 1 -4 -4 -17 390.30 12.20 1 4 4 18 129.10 5.90 1 -4 -4 -18 137.70 5.80 1 4 4 19 64.60 4.20 1 -4 -4 -19 63.60 3.50 1 4 4 20 389.30 12.80 1 -4 -4 -20 403.60 12.20 1 4 4 21 63.90 4.40 1 -4 -4 -21 60.10 3.70 1 4 4 22 485.90 15.40 1 -4 -4 -22 420.30 13.70 1 4 4 23 46.20 4.00 1 -4 -4 -23 46.60 3.40 1 4 4 24 186.90 8.00 1 -4 -4 -24 204.50 8.30 1 4 4 25 22.20 3.10 1 -4 -4 -25 17.90 2.60 1 4 4 26 83.70 5.80 1 -4 -4 -26 80.60 4.80 1 4 4 27 125.90 7.10 1 -4 -4 -27 76.20 9.50 1 4 4 28 226.40 10.70 1 -4 -4 -28 212.90 15.40 1 4 4 29 13.10 3.90 1 -4 -4 -29 1.60 4.50 1 4 4 30 104.70 7.00 1 -4 -4 -30 109.20 10.40 1 4 5 0 64.80 2.10 1 4 5 1 351.20 6.90 1 -4 -5 -1 311.60 6.50 1 4 5 2 49.90 1.80 1 -4 -5 -2 51.60 1.90 1 4 5 3 159.50 3.80 1 -4 -5 -3 163.10 3.80 1 4 5 4 65.00 2.00 1 -4 -5 -4 69.00 2.20 1 4 5 5 235.70 5.00 1 -4 -5 -5 192.70 3.90 1 4 5 6 176.40 4.80 1 -4 -5 -6 180.20 3.30 1 4 5 7 291.60 7.00 1 -4 -5 -7 300.80 5.30 1 4 5 8 81.20 5.90 1 -4 -5 -8 79.10 2.00 1 4 5 9 42.30 3.00 1 -4 -5 -9 30.60 1.40 1 4 5 10 85.30 4.20 1 -4 -5 -10 76.80 2.10 1 4 5 11 563.30 13.70 1 -4 -5 -11 587.00 15.60 1 4 5 12 106.80 4.90 1 -4 -5 -12 104.90 3.30 1 4 5 13 73.20 4.00 1 -4 -5 -13 62.00 3.10 1 4 5 14 191.60 7.00 1 -4 -5 -14 193.20 6.50 1 4 5 15 47.80 3.30 1 -4 -5 -15 50.70 2.80 1 4 5 16 99.50 4.80 1 -4 -5 -16 91.60 4.20 1 4 5 17 210.10 8.00 1 -4 -5 -17 205.50 7.50 1 4 5 18 34.90 2.90 1 -4 -5 -18 34.00 2.50 1 4 5 19 187.80 7.50 1 -4 -5 -19 172.40 10.60 1 4 5 20 171.00 7.50 1 -4 -5 -20 156.70 6.60 1 4 5 21 38.90 4.10 1 -4 -5 -21 23.00 4.90 1 4 5 22 96.50 5.60 1 -4 -5 -22 107.90 8.80 1 4 5 23 82.70 5.40 1 -4 -5 -23 72.60 7.50 1 4 5 24 19.50 3.70 1 -4 -5 -24 15.20 5.50 1 4 5 25 79.20 5.30 1 -4 -5 -25 77.20 8.80 1 4 5 26 27.20 3.60 1 -4 -5 -26 27.50 6.90 1 4 5 27 -2.00 2.80 1 -4 -5 -27 0.90 4.00 1 4 5 28 169.20 9.20 1 -4 -5 -28 134.40 12.80 1 4 5 29 161.90 9.40 1 -4 -5 -29 157.20 14.10 1 4 6 0 38.40 1.70 1 4 6 1 144.50 4.20 1 -4 -6 -1 148.20 4.30 1 4 6 2 238.80 5.10 1 -4 -6 -2 230.30 5.00 1 4 6 3 360.90 8.70 1 -4 -6 -3 359.20 7.20 1 4 6 4 233.20 5.10 1 -4 -6 -4 244.80 5.50 1 4 6 5 75.80 2.70 1 -4 -6 -5 67.20 1.90 1 4 6 6 175.80 9.70 1 -4 -6 -6 194.10 4.20 1 4 6 7 249.50 8.40 1 -4 -6 -7 242.30 5.10 1 4 6 8 53.70 3.20 1 -4 -6 -8 63.00 1.90 1 4 6 9 243.60 8.40 1 -4 -6 -9 253.90 5.50 1 4 6 10 302.40 7.90 1 -4 -6 -10 325.10 9.30 1 4 6 11 100.20 4.00 1 -4 -6 -11 101.50 3.80 1 4 6 12 52.70 2.90 1 -4 -6 -12 38.40 2.30 1 4 6 13 152.30 5.40 1 -4 -6 -13 127.40 7.50 1 4 6 14 2.80 1.60 1 -4 -6 -14 5.90 3.30 1 4 6 15 287.60 9.90 1 -4 -6 -15 285.70 14.80 1 4 6 16 366.10 12.20 1 -4 -6 -16 339.40 16.40 1 4 6 17 22.00 2.70 1 -4 -6 -17 17.30 4.30 1 4 6 18 158.10 7.00 1 -4 -6 -18 159.80 10.00 1 4 6 19 122.90 6.60 1 -4 -6 -19 113.10 8.30 1 4 6 20 14.20 3.30 1 -4 -6 -20 17.30 5.00 1 4 6 21 231.70 9.10 1 -4 -6 -21 211.60 13.00 1 4 6 22 75.90 4.90 1 -4 -6 -22 69.00 7.00 1 4 6 23 18.10 3.70 1 -4 -6 -23 14.70 5.20 1 4 6 24 172.80 9.50 1 -4 -6 -24 173.40 13.20 1 4 6 25 116.90 7.20 1 -4 -6 -25 128.40 10.90 1 4 6 26 34.80 4.70 1 -4 -6 -26 30.60 6.20 1 4 6 27 98.00 6.60 1 -4 -6 -27 100.10 9.70 1 4 7 0 501.70 11.50 1 4 7 1 603.30 13.20 1 -4 -7 -1 607.50 13.60 1 4 7 2 240.10 8.50 1 -4 -7 -2 252.80 6.70 1 4 7 3 11.40 2.20 1 -4 -7 -3 16.30 1.60 1 4 7 4 94.30 4.50 1 -4 -7 -4 93.90 3.50 1 4 7 5 655.60 18.40 1 -4 -7 -5 683.50 14.60 1 4 7 6 670.10 19.60 1 -4 -7 -6 700.80 15.30 1 4 7 7 506.00 15.20 1 -4 -7 -7 494.20 10.90 1 4 7 8 213.80 7.80 1 -4 -7 -8 207.70 6.60 1 4 7 9 13.30 1.90 1 -4 -7 -9 7.00 1.40 1 4 7 10 15.30 2.20 1 -4 -7 -10 19.30 2.00 1 4 7 11 275.00 8.10 1 -4 -7 -11 268.00 8.70 1 4 7 12 441.50 11.00 1 -4 -7 -12 454.80 20.80 1 4 7 13 659.70 16.30 1 -4 -7 -13 590.40 24.20 1 4 7 14 235.80 7.40 1 -4 -7 -14 240.70 13.20 1 4 7 15 10.50 2.00 1 -4 -7 -15 14.60 4.10 1 4 7 16 13.60 2.20 1 -4 -7 -16 0.80 3.60 1 4 7 17 83.40 5.10 1 -4 -7 -17 83.00 7.20 1 4 7 18 141.80 7.00 1 -4 -7 -18 138.50 9.10 1 4 7 19 271.50 10.20 1 -4 -7 -19 261.70 14.50 1 4 7 20 192.80 9.30 1 -4 -7 -20 198.10 14.10 1 4 7 21 16.00 3.90 1 -4 -7 -21 26.80 5.60 1 4 7 22 62.30 5.00 1 -4 -7 -22 54.70 7.50 1 4 7 23 81.40 5.60 1 -4 -7 -23 75.40 8.80 1 4 7 24 64.60 5.30 1 -4 -7 -24 49.90 7.60 1 4 7 25 120.90 7.30 1 -4 -7 -25 93.80 9.90 1 4 8 0 40.50 3.40 1 4 8 1 19.90 2.60 1 -4 -8 -1 23.10 2.70 1 4 8 2 28.60 2.80 1 -4 -8 -2 31.20 3.10 1 4 8 3 15.40 2.50 1 -4 -8 -3 11.50 2.80 1 4 8 4 4.70 2.50 1 -4 -8 -4 9.20 2.30 1 4 8 5 63.90 4.00 1 -4 -8 -5 60.00 5.40 1 4 8 6 45.40 3.40 1 -4 -8 -6 37.50 4.70 1 4 8 7 43.10 3.00 1 4 8 8 82.20 3.80 1 -4 -8 -8 82.50 6.10 1 4 8 9 20.50 2.10 1 -4 -8 -9 27.10 3.50 1 4 8 10 16.60 2.90 1 -4 -8 -10 10.50 3.00 1 4 8 11 36.60 2.80 1 -4 -8 -11 38.80 4.60 1 4 8 12 49.00 3.50 1 -4 -8 -12 49.80 4.70 1 4 8 13 108.70 4.80 1 -4 -8 -13 99.10 7.40 1 4 8 14 25.40 2.60 1 -4 -8 -14 27.50 4.20 1 4 8 15 6.20 2.00 1 -4 -8 -15 5.00 3.40 1 4 8 16 30.10 3.20 1 -4 -8 -16 32.60 5.20 1 4 8 17 72.70 4.40 1 -4 -8 -17 52.60 6.60 1 4 8 18 91.10 4.50 1 -4 -8 -18 58.70 7.20 1 4 8 19 66.60 4.40 1 -4 -8 -19 55.10 6.40 1 4 8 20 98.20 5.30 1 -4 -8 -20 84.00 8.40 1 4 8 21 30.40 3.90 1 -4 -8 -21 24.10 5.10 1 4 8 22 14.40 3.80 1 -4 -8 -22 3.70 6.20 1 4 8 23 24.40 3.80 1 -4 -8 -23 16.40 6.30 1 4 9 0 522.60 16.70 1 4 9 1 203.80 8.00 1 -4 -9 -1 216.10 8.50 1 4 9 2 92.20 5.00 1 -4 -9 -2 87.20 5.30 1 4 9 3 16.00 3.20 1 -4 -9 -3 16.30 2.70 1 4 9 4 100.70 5.30 1 -4 -9 -4 93.60 5.20 1 4 9 5 80.20 4.00 1 4 9 6 281.20 8.70 1 4 9 7 211.80 6.70 1 4 9 8 220.90 7.50 1 4 9 9 64.40 3.50 1 4 9 10 89.00 4.30 1 4 9 11 14.90 2.40 1 4 9 12 174.50 7.10 1 4 9 13 63.30 3.90 1 4 9 14 130.20 5.80 1 4 9 15 98.20 5.10 1 4 9 16 30.60 3.10 1 4 9 17 25.10 2.90 1 4 9 18 252.40 9.80 1 4 9 19 66.90 4.50 1 4 9 20 42.20 4.70 1 4 10 0 12.30 3.10 1 4 10 1 35.00 3.40 1 -4 -10 -1 43.00 4.30 1 4 10 2 101.70 9.00 1 -4 -10 -2 84.20 5.60 1 4 10 3 326.10 10.60 1 -4 -10 -3 355.50 20.90 1 4 10 4 16.80 2.50 1 4 10 5 152.40 6.30 1 4 10 6 25.30 2.80 1 4 10 7 62.80 3.90 1 4 10 8 57.00 4.10 1 4 10 9 162.70 6.80 1 4 10 10 86.00 4.70 1 4 10 11 218.10 10.50 1 4 10 12 -0.60 1.90 1 4 10 13 52.20 6.80 1 4 10 14 27.20 4.70 1 4 10 15 162.40 9.00 1 4 10 16 24.20 4.80 1 4 11 0 20.90 7.10 1 4 11 1 -0.60 2.50 1 -4 -11 -1 5.20 4.80 1 4 11 2 46.20 3.80 1 -4 -11 -2 44.80 7.10 1 4 11 3 1.70 2.70 1 4 11 4 5.90 2.80 1 4 11 5 14.10 4.20 1 4 11 6 34.30 4.00 1 4 11 7 20.20 6.90 1 4 11 8 30.00 8.10 1 4 11 9 31.80 6.50 1 4 11 10 19.80 4.50 1 5 0 0 5.00 1.70 1 5 0 1 864.80 17.60 1 5 0 2 17.70 1.50 1 5 0 3 85.20 3.00 1 5 0 4 132.80 3.90 1 5 0 5 1517.50 26.00 1 5 0 6 3.60 1.00 1 5 0 7 843.00 15.20 1 5 0 8 7.20 1.20 1 5 0 9 18.90 2.10 1 5 0 10 12.40 1.50 1 5 0 11 445.20 10.50 1 5 0 12 271.20 7.20 1 5 0 13 1215.40 31.60 1 5 0 14 8.00 2.00 1 5 0 15 22.40 2.70 1 5 0 16 0.90 1.90 1 5 0 17 304.20 10.30 1 5 0 18 91.30 5.20 1 5 0 19 310.00 10.70 1 5 0 20 131.90 6.10 1 5 0 21 123.70 6.40 1 5 0 22 21.70 3.40 1 5 0 23 141.70 6.50 1 5 0 24 43.50 4.20 1 5 0 25 123.70 7.20 1 5 0 26 74.20 5.50 1 5 0 27 65.70 5.20 1 5 0 28 2.20 2.40 1 5 0 29 29.40 4.10 1 5 1 0 1060.70 21.60 1 5 1 1 6.70 1.30 1 -5 -1 -1 11.10 1.90 1 5 1 2 472.50 10.40 1 -5 -1 -2 481.30 13.60 1 5 1 3 57.60 2.50 1 -5 -1 -3 53.50 2.00 1 5 1 4 205.80 4.70 1 -5 -1 -4 220.80 5.60 1 5 1 5 25.00 1.40 1 -5 -1 -5 26.20 1.20 1 5 1 6 695.20 14.90 1 -5 -1 -6 672.90 12.40 1 5 1 7 193.20 4.50 1 -5 -1 -7 183.40 4.10 1 5 1 8 798.00 16.90 1 -5 -1 -8 779.50 14.50 1 5 1 9 9.80 1.10 1 -5 -1 -9 8.50 1.40 1 5 1 10 337.70 10.60 1 -5 -1 -10 329.40 7.80 1 5 1 11 3.90 2.40 1 -5 -1 -11 3.70 1.40 1 5 1 12 403.30 12.00 1 -5 -1 -12 405.90 9.40 1 5 1 13 152.00 6.20 1 -5 -1 -13 160.20 6.30 1 5 1 14 368.40 16.60 1 -5 -1 -14 343.40 10.70 1 5 1 15 207.80 7.90 1 -5 -1 -15 175.80 6.70 1 5 1 16 217.80 8.10 1 -5 -1 -16 196.30 7.50 1 5 1 17 72.70 4.40 1 -5 -1 -17 85.30 4.70 1 5 1 18 451.20 14.70 1 -5 -1 -18 426.30 13.50 1 5 1 19 107.10 5.20 1 -5 -1 -19 98.30 5.20 1 5 1 20 303.80 10.40 1 -5 -1 -20 302.40 11.00 1 5 1 21 130.60 6.20 1 -5 -1 -21 117.90 5.80 1 5 1 22 42.10 3.80 1 -5 -1 -22 41.00 3.70 1 5 1 23 21.60 3.30 1 -5 -1 -23 22.80 3.20 1 5 1 24 92.00 5.40 1 -5 -1 -24 90.20 5.70 1 5 1 25 270.70 11.90 1 -5 -1 -25 247.00 10.90 1 5 1 26 210.70 10.00 1 -5 -1 -26 212.90 10.00 1 5 1 27 55.00 5.30 1 -5 -1 -27 42.30 4.70 1 5 1 28 26.80 4.00 1 -5 -1 -28 24.20 3.40 1 5 1 29 3.10 3.20 1 -5 -1 -29 8.90 3.20 1 5 2 0 105.80 3.60 1 5 2 1 581.00 12.60 1 -5 -2 -1 650.90 14.20 1 5 2 2 39.50 2.20 1 -5 -2 -2 42.50 2.60 1 5 2 3 764.00 16.20 1 -5 -2 -3 755.30 20.10 1 5 2 4 162.80 4.20 1 -5 -2 -4 176.80 6.30 1 5 2 5 570.70 12.50 1 -5 -2 -5 599.40 12.60 1 5 2 6 85.40 3.20 1 -5 -2 -6 89.10 2.20 1 5 2 7 908.40 19.20 1 -5 -2 -7 882.80 15.50 1 5 2 8 35.10 2.10 1 -5 -2 -8 34.70 1.90 1 5 2 9 215.70 6.00 1 -5 -2 -9 197.00 5.30 1 5 2 10 324.30 8.40 1 -5 -2 -10 314.80 7.90 1 5 2 11 445.90 12.70 1 -5 -2 -11 425.80 10.00 1 5 2 12 74.20 5.80 1 -5 -2 -12 57.50 2.40 1 5 2 13 446.10 12.90 1 -5 -2 -13 460.10 13.70 1 5 2 14 2.70 2.30 1 -5 -2 -14 3.30 1.50 1 5 2 15 358.70 12.00 1 -5 -2 -15 357.40 11.90 1 5 2 16 91.00 4.60 1 -5 -2 -16 103.00 5.20 1 5 2 17 146.40 6.40 1 -5 -2 -17 126.00 6.20 1 5 2 18 315.50 10.60 1 -5 -2 -18 299.90 10.40 1 5 2 19 308.60 10.80 1 -5 -2 -19 297.00 10.60 1 5 2 20 14.10 2.80 1 -5 -2 -20 19.10 2.80 1 5 2 21 130.80 6.50 1 -5 -2 -21 159.30 7.10 1 5 2 22 97.70 5.80 1 -5 -2 -22 84.60 5.10 1 5 2 23 59.80 4.50 1 -5 -2 -23 75.50 4.90 1 5 2 24 93.10 6.00 1 -5 -2 -24 77.10 5.00 1 5 2 25 127.60 7.20 1 -5 -2 -25 105.60 6.30 1 5 2 26 16.70 3.40 1 -5 -2 -26 20.60 3.00 1 5 2 27 60.60 5.00 1 -5 -2 -27 59.60 4.70 1 5 2 28 108.80 7.30 1 -5 -2 -28 89.40 6.40 1 5 2 29 68.80 5.60 1 -5 -2 -29 66.20 5.20 1 5 3 0 160.40 4.60 1 5 3 1 10.30 1.40 1 -5 -3 -1 12.40 1.60 1 5 3 2 993.10 21.00 1 -5 -3 -2 995.90 20.70 1 5 3 3 475.60 10.70 1 -5 -3 -3 444.10 12.70 1 5 3 4 363.10 8.60 1 -5 -3 -4 355.20 11.00 1 5 3 5 32.30 2.10 1 -5 -3 -5 31.70 3.80 1 5 3 6 233.70 6.20 1 -5 -3 -6 249.90 8.20 1 5 3 7 75.00 2.90 1 -5 -3 -7 77.20 2.30 1 5 3 8 493.70 11.40 1 -5 -3 -8 486.40 10.70 1 5 3 9 33.40 2.10 1 -5 -3 -9 47.90 2.20 1 5 3 10 980.20 20.60 1 -5 -3 -10 1024.40 27.30 1 5 3 11 195.30 7.10 1 -5 -3 -11 171.40 6.40 1 5 3 12 54.70 5.20 1 -5 -3 -12 75.30 3.40 1 5 3 13 11.60 2.60 1 -5 -3 -13 9.30 2.20 1 5 3 14 272.30 9.70 1 -5 -3 -14 279.60 9.20 1 5 3 15 153.50 7.60 1 -5 -3 -15 141.50 5.90 1 5 3 16 530.40 15.40 1 -5 -3 -16 562.60 16.30 1 5 3 17 45.00 5.20 1 -5 -3 -17 57.30 3.90 1 5 3 18 58.20 4.20 1 -5 -3 -18 53.40 3.60 1 5 3 19 27.20 3.20 1 -5 -3 -19 32.80 3.70 1 5 3 20 171.80 7.60 1 -5 -3 -20 186.10 7.30 1 5 3 21 69.80 4.90 1 -5 -3 -21 58.30 3.90 1 5 3 22 184.00 8.10 1 -5 -3 -22 169.40 7.80 1 5 3 23 92.90 5.90 1 -5 -3 -23 101.10 6.10 1 5 3 24 62.40 5.00 1 -5 -3 -24 59.40 4.60 1 5 3 25 2.70 2.90 1 -5 -3 -25 1.90 2.80 1 5 3 26 63.50 5.30 1 -5 -3 -26 55.20 4.30 1 5 3 27 54.90 4.70 1 -5 -3 -27 63.40 5.10 1 5 3 28 196.20 10.10 1 -5 -3 -28 160.20 14.80 1 5 4 0 13.70 1.50 1 5 4 1 127.90 4.10 1 -5 -4 -1 129.50 3.90 1 5 4 2 98.80 3.60 1 -5 -4 -2 103.00 3.50 1 5 4 3 733.00 15.70 1 -5 -4 -3 692.90 15.40 1 5 4 4 223.90 5.90 1 -5 -4 -4 222.90 7.70 1 5 4 5 436.70 10.20 1 -5 -4 -5 460.50 13.70 1 5 4 6 10.40 1.50 1 -5 -4 -6 1.90 1.30 1 5 4 7 12.60 1.50 1 -5 -4 -7 6.30 1.80 1 5 4 8 108.90 3.80 1 -5 -4 -8 117.60 4.90 1 5 4 9 322.70 8.40 1 -5 -4 -9 332.90 11.00 1 5 4 10 260.90 8.60 1 -5 -4 -10 261.90 8.80 1 5 4 11 231.90 8.20 1 -5 -4 -11 257.00 7.10 1 5 4 12 72.30 4.20 1 -5 -4 -12 83.80 3.90 1 5 4 13 63.40 3.40 1 -5 -4 -13 55.20 3.30 1 5 4 14 32.20 3.50 1 -5 -4 -14 22.10 2.40 1 5 4 15 341.70 11.80 1 -5 -4 -15 331.00 10.90 1 5 4 16 233.50 9.40 1 -5 -4 -16 219.00 7.60 1 5 4 17 299.90 10.80 1 -5 -4 -17 271.70 9.60 1 5 4 18 44.80 4.20 1 -5 -4 -18 41.70 3.40 1 5 4 19 21.50 5.20 1 -5 -4 -19 29.60 3.00 1 5 4 20 73.10 5.20 1 -5 -4 -20 55.90 4.10 1 5 4 21 121.10 6.10 1 -5 -4 -21 93.20 5.00 1 5 4 22 156.70 8.60 1 -5 -4 -22 148.70 7.40 1 5 4 23 232.70 10.30 1 -5 -4 -23 221.20 15.20 1 5 4 24 81.00 5.90 1 -5 -4 -24 84.90 8.80 1 5 4 25 4.00 3.30 1 -5 -4 -25 1.00 6.00 1 5 4 26 24.00 4.60 1 -5 -4 -26 23.70 5.80 1 5 4 27 65.30 5.10 1 -5 -4 -27 57.10 8.10 1 5 5 0 18.10 1.70 1 5 5 1 73.10 3.10 1 -5 -5 -1 69.70 3.10 1 5 5 2 164.40 4.90 1 -5 -5 -2 167.40 5.00 1 5 5 3 311.10 7.70 1 -5 -5 -3 327.90 7.90 1 5 5 4 1012.90 25.70 1 -5 -5 -4 996.90 25.70 1 5 5 5 249.60 6.60 1 -5 -5 -5 250.40 8.40 1 5 5 6 145.00 4.40 1 -5 -5 -6 119.80 5.00 1 5 5 7 174.60 5.00 1 -5 -5 -7 165.90 6.50 1 5 5 8 328.60 8.30 1 -5 -5 -8 329.70 10.20 1 5 5 9 158.80 6.70 1 -5 -5 -9 157.80 5.10 1 5 5 10 348.20 16.70 1 -5 -5 -10 342.40 8.80 1 5 5 11 97.60 4.90 1 -5 -5 -11 104.90 3.80 1 5 5 12 248.80 8.90 1 -5 -5 -12 250.10 8.60 1 5 5 13 267.30 8.10 1 -5 -5 -13 289.80 13.80 1 5 5 14 232.30 7.20 1 -5 -5 -14 255.80 12.40 1 5 5 15 179.70 6.30 1 -5 -5 -15 188.90 7.20 1 5 5 16 247.70 10.00 1 -5 -5 -16 203.70 12.20 1 5 5 17 23.10 3.60 1 -5 -5 -17 32.70 5.40 1 5 5 18 160.10 7.70 1 -5 -5 -18 192.60 11.60 1 5 5 19 67.20 5.00 1 -5 -5 -19 60.90 6.10 1 5 5 20 10.70 3.10 1 -5 -5 -20 11.10 5.00 1 5 5 21 278.80 11.80 1 -5 -5 -21 238.70 15.60 1 5 5 22 252.70 11.40 1 -5 -5 -22 227.80 15.70 1 5 5 23 37.60 4.80 1 -5 -5 -23 24.80 6.70 1 5 5 24 26.50 3.50 1 -5 -5 -24 22.80 6.10 1 5 5 25 39.00 4.60 1 -5 -5 -25 41.60 6.70 1 5 5 26 11.10 3.70 1 -5 -5 -26 8.20 6.70 1 5 6 0 287.80 7.90 1 5 6 1 474.30 11.80 1 -5 -6 -1 527.50 12.30 1 5 6 2 32.40 2.10 1 -5 -6 -2 29.10 2.10 1 5 6 3 98.90 3.60 1 -5 -6 -3 91.90 3.60 1 5 6 4 56.80 2.60 1 -5 -6 -4 59.20 3.40 1 5 6 5 367.80 9.10 1 -5 -6 -5 381.00 11.80 1 5 6 6 23.80 2.50 1 -5 -6 -6 39.10 3.00 1 5 6 7 167.30 6.90 1 -5 -6 -7 176.40 6.60 1 5 6 8 211.80 7.90 1 -5 -6 -8 187.10 7.20 1 5 6 9 251.80 9.60 1 -5 -6 -9 258.40 9.00 1 5 6 10 30.50 3.20 1 -5 -6 -10 33.30 3.00 1 5 6 11 253.80 8.10 1 -5 -6 -11 243.80 12.20 1 5 6 12 17.30 2.40 1 -5 -6 -12 23.50 4.60 1 5 6 13 231.70 7.40 1 -5 -6 -13 233.20 12.40 1 5 6 14 106.80 4.80 1 -5 -6 -14 119.30 8.80 1 5 6 15 14.80 2.30 1 -5 -6 -15 5.20 3.00 1 5 6 16 32.60 3.00 1 -5 -6 -16 31.90 5.70 1 5 6 17 292.20 9.00 1 -5 -6 -17 247.90 14.40 1 5 6 18 50.50 3.80 1 -5 -6 -18 39.80 6.20 1 5 6 19 98.40 6.50 1 -5 -6 -19 127.00 10.30 1 5 6 20 40.20 4.30 1 -5 -6 -20 34.00 6.10 1 5 6 21 6.60 3.10 1 -5 -6 -21 8.60 5.70 1 5 6 22 42.40 5.00 1 -5 -6 -22 43.80 6.40 1 5 6 23 90.70 6.40 1 -5 -6 -23 92.80 9.60 1 5 6 24 3.80 3.00 1 -5 -6 -24 9.00 4.90 1 5 7 0 48.50 3.80 1 5 7 1 208.30 8.10 1 -5 -7 -1 219.00 8.50 1 5 7 2 106.90 5.40 1 -5 -7 -2 104.00 5.30 1 5 7 3 54.90 3.90 1 -5 -7 -3 57.80 4.00 1 5 7 4 27.60 3.00 1 -5 -7 -4 27.50 3.80 1 5 7 5 211.10 7.90 1 -5 -7 -5 182.90 7.10 1 5 7 6 110.00 5.60 1 -5 -7 -6 114.00 5.00 1 5 7 7 205.40 7.90 1 -5 -7 -7 192.30 7.10 1 5 7 8 48.60 4.60 1 -5 -7 -8 31.80 3.00 1 5 7 9 104.60 5.70 1 -5 -7 -9 93.70 4.60 1 5 7 10 4.00 2.20 1 -5 -7 -10 7.50 3.40 1 5 7 11 81.00 4.10 1 5 7 12 165.80 5.80 1 -5 -7 -12 152.10 9.60 1 5 7 13 243.60 7.80 1 -5 -7 -13 211.00 11.80 1 5 7 14 67.00 3.90 1 -5 -7 -14 37.20 5.60 1 5 7 15 73.30 4.20 1 -5 -7 -15 72.90 7.30 1 5 7 16 12.00 2.70 1 -5 -7 -16 8.60 4.40 1 5 7 17 43.30 3.70 1 -5 -7 -17 44.90 5.80 1 5 7 18 51.40 4.10 1 -5 -7 -18 51.80 6.20 1 5 7 19 231.00 9.30 1 -5 -7 -19 204.50 14.50 1 5 7 20 130.20 6.50 1 -5 -7 -20 132.60 12.00 1 5 7 21 32.70 3.80 1 -5 -7 -21 20.20 6.70 1 5 7 22 8.00 3.50 1 -5 -7 -22 -1.20 6.20 1 5 8 0 259.80 10.00 1 5 8 1 134.60 6.80 1 -5 -8 -1 134.90 6.70 1 5 8 2 141.00 6.50 1 -5 -8 -2 129.10 6.30 1 5 8 3 -0.60 2.80 1 -5 -8 -3 3.70 2.60 1 5 8 4 48.10 4.20 1 -5 -8 -4 40.80 5.50 1 5 8 5 57.70 4.00 1 -5 -8 -5 55.00 5.40 1 5 8 6 333.80 12.00 1 -5 -8 -6 331.20 16.00 1 5 8 7 232.60 8.90 1 -5 -8 -7 265.00 14.50 1 5 8 8 67.70 4.60 1 5 8 9 19.30 2.80 1 5 8 10 29.00 2.90 1 5 8 11 115.20 5.50 1 5 8 12 279.50 10.00 1 5 8 13 93.50 5.10 1 5 8 14 70.50 4.00 1 5 8 15 56.80 4.10 1 5 8 16 35.20 3.90 1 5 8 17 24.50 3.30 1 5 8 18 89.60 6.90 1 5 8 19 147.40 7.10 1 5 9 0 71.00 5.30 1 5 9 1 149.80 7.90 1 -5 -9 -1 149.90 7.80 1 5 9 2 73.90 4.90 1 -5 -9 -2 63.50 4.70 1 5 9 3 63.00 4.90 1 -5 -9 -3 64.20 4.50 1 5 9 4 96.30 5.90 1 -5 -9 -4 82.40 7.40 1 5 9 5 62.80 5.10 1 -5 -9 -5 77.40 7.50 1 5 9 6 60.70 5.00 1 -5 -9 -6 68.00 6.50 1 5 9 7 98.60 6.30 1 5 9 8 46.20 3.70 1 5 9 9 31.50 3.10 1 5 9 10 31.10 3.30 1 5 9 11 48.80 3.90 1 5 9 12 50.80 4.00 1 5 9 13 36.00 3.70 1 5 9 14 178.80 7.90 1 5 9 15 25.80 3.20 1 5 9 16 13.90 3.30 1 5 10 0 37.70 4.70 1 5 10 1 7.80 3.20 1 -5 -10 -1 6.00 3.70 1 5 10 2 91.60 6.60 1 -5 -10 -2 93.80 6.70 1 5 10 3 19.80 3.90 1 -5 -10 -3 14.30 5.10 1 5 10 4 127.70 7.50 1 -5 -10 -4 124.30 9.50 1 5 10 5 16.40 3.90 1 5 10 6 65.50 4.30 1 5 10 7 -4.60 2.90 1 5 10 8 54.90 4.10 1 5 10 9 16.80 3.00 1 5 10 10 141.90 6.90 1 6 0 0 1772.00 61.60 1 6 0 1 51.80 3.60 1 6 0 2 589.20 17.00 1 6 0 3 0.20 1.20 1 6 0 4 268.50 6.90 1 6 0 5 45.30 2.30 1 6 0 6 1663.00 33.80 1 6 0 7 2.50 1.70 1 6 0 8 496.20 11.70 1 6 0 9 173.20 5.50 1 6 0 10 28.70 2.10 1 6 0 11 31.10 2.50 1 6 0 12 1389.50 30.30 1 6 0 13 14.00 2.90 1 6 0 14 491.10 15.40 1 6 0 15 13.40 3.80 1 6 0 16 10.30 2.70 1 6 0 17 40.70 4.00 1 6 0 18 362.30 12.60 1 6 0 19 75.40 7.70 1 6 0 20 445.70 17.40 1 6 0 21 29.20 4.10 1 6 0 22 2.80 3.00 1 6 0 23 12.60 3.30 1 6 0 24 232.70 10.70 1 6 0 25 9.70 3.40 1 6 0 26 194.20 10.10 1 6 1 0 20.30 2.60 1 6 1 1 240.50 8.00 1 -6 -1 -1 216.30 7.80 1 6 1 2 58.70 2.70 1 -6 -1 -2 50.40 3.40 1 6 1 3 103.10 3.70 1 -6 -1 -3 117.30 4.90 1 6 1 4 77.10 4.10 1 -6 -1 -4 79.10 4.00 1 6 1 5 61.30 2.90 1 -6 -1 -5 50.60 3.50 1 6 1 6 106.80 3.70 1 -6 -1 -6 111.50 5.10 1 6 1 7 259.90 6.90 1 -6 -1 -7 267.80 9.20 1 6 1 8 7.80 1.80 1 -6 -1 -8 5.50 2.10 1 6 1 9 238.00 6.40 1 -6 -1 -9 243.20 8.40 1 6 1 10 52.40 2.80 1 -6 -1 -10 68.00 4.20 1 6 1 11 88.10 3.50 1 -6 -1 -11 85.40 4.40 1 6 1 12 128.40 4.50 1 -6 -1 -12 113.80 5.50 1 6 1 13 61.90 3.90 1 -6 -1 -13 64.30 3.90 1 6 1 14 68.40 4.70 1 -6 -1 -14 72.20 4.60 1 6 1 15 63.30 4.60 1 -6 -1 -15 78.70 4.90 1 6 1 16 72.50 4.60 1 -6 -1 -16 89.10 5.40 1 6 1 17 196.20 8.30 1 -6 -1 -17 206.40 7.90 1 6 1 18 114.40 6.20 1 -6 -1 -18 115.60 6.20 1 6 1 19 66.70 5.50 1 -6 -1 -19 71.80 4.90 1 6 1 20 49.20 4.50 1 -6 -1 -20 42.50 4.30 1 6 1 21 57.60 4.90 1 -6 -1 -21 55.30 4.60 1 6 1 22 34.40 4.20 1 -6 -1 -22 25.00 3.40 1 6 1 23 16.00 3.60 1 -6 -1 -23 16.70 3.20 1 6 1 24 151.30 9.00 1 -6 -1 -24 146.50 8.00 1 6 1 25 73.10 5.10 1 -6 -1 -25 68.60 5.50 1 6 2 0 278.00 8.90 1 6 2 1 12.70 1.80 1 -6 -2 -1 19.90 2.70 1 6 2 2 317.30 8.10 1 -6 -2 -2 308.50 10.00 1 6 2 3 70.90 3.00 1 -6 -2 -3 72.90 3.90 1 6 2 4 503.70 11.90 1 -6 -2 -4 493.10 14.40 1 6 2 5 12.50 1.70 1 -6 -2 -5 6.70 2.30 1 6 2 6 470.90 11.10 1 -6 -2 -6 495.50 14.90 1 6 2 7 19.20 2.10 1 -6 -2 -7 9.00 2.20 1 6 2 8 242.10 6.80 1 -6 -2 -8 231.50 8.20 1 6 2 9 8.20 1.50 1 -6 -2 -9 15.00 2.60 1 6 2 10 91.10 3.80 1 -6 -2 -10 94.60 4.60 1 6 2 11 147.30 5.00 1 -6 -2 -11 152.70 6.50 1 6 2 12 329.30 8.50 1 -6 -2 -12 278.00 10.10 1 6 2 13 7.10 3.40 1 -6 -2 -13 2.90 2.10 1 6 2 14 481.50 13.20 1 -6 -2 -14 543.90 16.80 1 6 2 15 56.00 4.60 1 -6 -2 -15 51.90 3.90 1 6 2 16 33.00 3.60 1 -6 -2 -16 35.30 3.30 1 6 2 17 58.20 4.50 1 -6 -2 -17 55.80 4.00 1 6 2 18 114.50 6.10 1 -6 -2 -18 120.40 5.90 1 6 2 19 51.80 4.50 1 -6 -2 -19 50.00 4.10 1 6 2 20 197.90 9.50 1 -6 -2 -20 176.00 8.60 1 6 2 21 52.30 4.40 1 -6 -2 -21 40.50 4.00 1 6 2 22 77.00 5.40 1 -6 -2 -22 81.50 5.60 1 6 2 23 52.40 5.50 1 -6 -2 -23 47.50 4.40 1 6 2 24 52.80 5.40 1 -6 -2 -24 57.80 5.10 1 6 2 25 12.30 4.50 1 -6 -2 -25 10.20 3.40 1 6 3 0 13.50 1.90 1 6 3 1 264.50 7.30 1 -6 -3 -1 263.30 8.90 1 6 3 2 151.30 5.00 1 -6 -3 -2 157.40 6.60 1 6 3 3 923.80 19.70 1 -6 -3 -3 896.40 24.20 1 6 3 4 175.60 5.20 1 -6 -3 -4 188.50 7.10 1 6 3 5 318.90 8.30 1 -6 -3 -5 286.70 9.90 1 6 3 6 129.60 4.60 1 -6 -3 -6 118.20 5.40 1 6 3 7 170.60 5.30 1 -6 -3 -7 168.40 6.60 1 6 3 8 44.00 2.70 1 -6 -3 -8 48.20 3.40 1 6 3 9 1006.30 21.90 1 -6 -3 -9 947.40 25.40 1 6 3 10 119.50 4.40 1 -6 -3 -10 108.10 5.40 1 6 3 11 474.60 11.10 1 -6 -3 -11 478.90 14.70 1 6 3 12 141.00 6.10 1 -6 -3 -12 121.80 5.70 1 6 3 13 59.70 4.00 1 -6 -3 -13 58.90 3.20 1 6 3 14 10.30 2.30 1 -6 -3 -14 19.90 2.70 1 6 3 15 353.80 10.20 1 -6 -3 -15 357.20 12.30 1 6 3 16 91.40 4.60 1 -6 -3 -16 84.80 5.10 1 6 3 17 397.80 14.30 1 -6 -3 -17 429.60 14.30 1 6 3 18 97.40 5.70 1 -6 -3 -18 92.70 5.20 1 6 3 19 0.60 2.30 1 -6 -3 -19 3.20 2.50 1 6 3 20 11.70 3.30 1 -6 -3 -20 15.10 3.00 1 6 3 21 209.30 10.80 1 -6 -3 -21 233.40 10.70 1 6 3 22 54.10 5.00 1 -6 -3 -22 52.70 4.90 1 6 3 23 174.30 9.60 1 -6 -3 -23 189.90 14.50 1 6 3 24 84.90 6.60 1 -6 -3 -24 54.10 8.50 1 6 4 0 8.70 1.90 1 6 4 1 52.80 2.90 1 -6 -4 -1 53.80 3.00 1 6 4 2 204.20 6.20 1 -6 -4 -2 217.80 7.90 1 6 4 3 40.50 2.50 1 -6 -4 -3 31.70 2.80 1 6 4 4 83.60 3.40 1 -6 -4 -4 85.90 4.70 1 6 4 5 4.60 1.70 1 -6 -4 -5 0.10 1.90 1 6 4 6 15.60 1.90 1 -6 -4 -6 13.60 2.80 1 6 4 7 29.70 2.60 1 -6 -4 -7 35.30 3.00 1 6 4 8 111.30 4.20 1 -6 -4 -8 117.70 5.60 1 6 4 9 136.50 5.00 1 -6 -4 -9 125.10 6.00 1 6 4 10 126.40 4.50 1 -6 -4 -10 137.60 6.70 1 6 4 11 8.50 3.00 1 -6 -4 -11 11.90 2.40 1 6 4 12 5.90 2.60 1 -6 -4 -12 6.80 2.40 1 6 4 13 19.10 2.50 1 -6 -4 -13 19.80 4.10 1 6 4 14 37.80 3.10 1 -6 -4 -14 41.90 5.80 1 6 4 15 72.30 4.10 1 -6 -4 -15 68.60 4.60 1 6 4 16 216.70 7.60 1 -6 -4 -16 213.70 8.70 1 6 4 17 51.50 3.70 1 -6 -4 -17 41.60 5.40 1 6 4 18 11.60 3.00 1 -6 -4 -18 19.30 4.50 1 6 4 19 62.30 5.40 1 -6 -4 -19 53.40 6.40 1 6 4 20 79.00 8.60 1 -6 -4 -20 54.30 7.70 1 6 4 21 88.10 5.90 1 -6 -4 -21 94.30 10.20 1 6 4 22 62.90 5.30 1 -6 -4 -22 46.10 6.50 1 6 4 23 38.60 4.80 1 -6 -4 -23 21.20 7.00 1 6 5 0 14.70 2.10 1 6 5 1 104.20 4.10 1 -6 -5 -1 117.70 4.60 1 6 5 2 125.30 4.50 1 -6 -5 -2 111.00 5.40 1 6 5 3 503.20 12.40 1 -6 -5 -3 478.90 14.70 1 6 5 4 224.90 6.40 1 -6 -5 -4 232.40 8.70 1 6 5 5 232.60 6.90 1 -6 -5 -5 249.70 9.10 1 6 5 6 3.30 1.70 1 -6 -5 -6 0.30 1.80 1 6 5 7 82.10 3.80 1 -6 -5 -7 86.40 5.00 1 6 5 8 72.50 3.50 1 -6 -5 -8 90.40 5.00 1 6 5 9 385.80 12.80 1 -6 -5 -9 406.00 12.90 1 6 5 10 154.70 6.80 1 -6 -5 -10 146.60 6.80 1 6 5 11 335.20 12.30 1 -6 -5 -11 318.40 11.70 1 6 5 12 1.50 3.10 1 -6 -5 -12 1.80 3.90 1 6 5 13 8.30 2.20 1 -6 -5 -13 14.20 4.90 1 6 5 14 101.90 4.90 1 -6 -5 -14 106.60 7.90 1 6 5 15 261.70 9.50 1 -6 -5 -15 238.20 15.40 1 6 5 16 107.70 5.60 1 -6 -5 -16 91.20 9.90 1 6 5 17 198.00 8.20 1 -6 -5 -17 203.60 14.50 1 6 5 18 23.20 3.20 1 -6 -5 -18 18.70 6.00 1 6 5 19 32.10 3.30 1 -6 -5 -19 23.20 6.90 1 6 5 20 57.10 4.30 1 -6 -5 -20 52.50 7.00 1 6 5 21 73.70 5.00 1 -6 -5 -21 84.20 8.80 1 6 5 22 43.60 5.10 1 6 6 0 304.70 11.10 1 6 6 1 224.40 8.30 1 -6 -6 -1 244.00 7.50 1 6 6 2 114.80 6.10 1 -6 -6 -2 94.60 4.00 1 6 6 3 118.50 6.20 1 -6 -6 -3 110.40 5.40 1 6 6 4 43.00 3.70 1 -6 -6 -4 34.60 3.10 1 6 6 5 101.70 5.60 1 -6 -6 -5 122.10 5.80 1 6 6 6 199.20 8.40 1 -6 -6 -6 213.10 8.70 1 6 6 7 283.80 10.60 1 -6 -6 -7 270.30 10.60 1 6 6 8 88.10 5.20 1 -6 -6 -8 92.80 5.20 1 6 6 9 58.60 4.50 1 -6 -6 -9 58.20 4.60 1 6 6 10 75.40 4.90 1 -6 -6 -10 60.40 4.60 1 6 6 11 71.80 5.10 1 -6 -6 -11 73.80 4.80 1 6 6 12 150.70 6.50 1 -6 -6 -12 117.70 10.20 1 6 6 13 145.60 6.60 1 -6 -6 -13 139.20 11.00 1 6 6 14 64.30 4.40 1 -6 -6 -14 77.90 8.00 1 6 6 15 86.80 5.10 1 -6 -6 -15 74.80 7.70 1 6 6 16 11.70 2.60 1 -6 -6 -16 0.70 3.60 1 6 6 17 3.60 2.70 1 -6 -6 -17 -4.80 4.90 1 6 6 18 131.50 6.40 1 -6 -6 -18 139.70 11.90 1 6 6 19 131.70 6.80 1 -6 -6 -19 101.60 10.50 1 6 6 20 24.50 3.30 1 -6 -6 -20 23.20 5.40 1 6 7 0 3.30 2.30 1 6 7 1 60.60 4.30 1 -6 -7 -1 65.50 4.60 1 6 7 2 46.90 4.10 1 -6 -7 -2 48.10 4.30 1 6 7 3 50.70 4.60 1 -6 -7 -3 43.10 5.00 1 6 7 4 15.40 3.20 1 -6 -7 -4 14.80 4.50 1 6 7 5 232.20 10.40 1 -6 -7 -5 224.40 13.80 1 6 7 6 33.40 4.00 1 -6 -7 -6 36.00 5.70 1 6 7 7 28.30 3.90 1 -6 -7 -7 28.40 4.50 1 6 7 8 30.60 3.60 1 -6 -7 -8 16.50 5.10 1 6 7 9 7.90 3.90 1 -6 -7 -9 17.80 5.10 1 6 7 10 -1.30 2.60 1 6 7 11 75.20 4.80 1 6 7 12 51.90 4.00 1 6 7 13 190.10 8.10 1 6 7 14 16.50 2.90 1 6 7 15 23.60 3.20 1 -6 -7 -15 30.50 6.30 1 6 7 16 6.40 3.00 1 -6 -7 -16 4.80 5.10 1 6 7 17 44.90 4.30 1 6 8 0 172.60 9.30 1 6 8 1 189.10 9.60 1 -6 -8 -1 202.40 10.10 1 6 8 2 65.50 5.40 1 -6 -8 -2 72.70 8.20 1 6 8 3 12.70 3.40 1 -6 -8 -3 11.80 4.10 1 6 8 4 5.30 4.00 1 -6 -8 -4 8.90 5.10 1 6 8 5 154.30 7.90 1 -6 -8 -5 150.00 10.50 1 6 8 6 149.10 8.50 1 -6 -8 -6 144.70 10.10 1 6 8 7 222.50 11.10 1 -6 -8 -7 239.40 15.30 1 6 8 8 94.60 6.40 1 -6 -8 -8 107.20 9.30 1 6 8 9 16.80 4.00 1 6 8 10 40.50 3.90 1 6 8 11 148.20 7.30 1 6 8 12 67.30 4.70 1 6 8 13 163.60 7.50 1 6 9 0 74.00 6.30 1 6 9 1 14.10 5.20 1 -6 -9 -1 23.30 4.70 1 6 9 2 112.50 7.50 1 -6 -9 -2 117.90 9.40 1 6 9 3 7.70 4.30 1 -6 -9 -3 15.70 4.60 1 6 9 4 110.30 7.30 1 -6 -9 -4 123.90 10.30 1 6 9 5 7.40 4.30 1 -6 -9 -5 20.20 4.60 1 6 9 6 26.60 4.60 1 -6 -9 -6 22.70 5.90 1 6 9 7 14.00 3.60 1 7 0 0 -0.40 2.70 1 7 0 1 4.90 2.10 1 7 0 2 1.60 2.00 1 7 0 3 1.60 1.90 1 7 0 4 11.90 2.70 1 7 0 5 24.00 3.40 1 7 0 6 39.60 3.80 1 7 0 7 8.40 2.30 1 7 0 8 6.30 2.30 1 7 0 9 3.40 3.00 1 7 0 10 5.60 2.70 1 7 0 11 12.50 5.30 1 7 0 12 111.60 6.20 1 7 0 13 18.20 3.40 1 7 0 14 22.90 3.60 1 7 0 15 83.60 6.00 1 7 0 16 8.40 3.80 1 7 0 17 9.10 4.00 1 7 0 18 117.80 7.50 1 7 0 19 6.80 3.50 1 7 0 20 130.10 8.20 1 7 0 21 3.70 3.50 1 7 1 0 701.90 21.00 1 7 1 1 11.70 2.80 1 -7 -1 -1 10.10 2.30 1 7 1 2 281.90 10.30 1 -7 -1 -2 276.30 9.40 1 7 1 3 98.00 5.30 1 -7 -1 -3 102.30 5.60 1 7 1 4 183.00 7.60 1 -7 -1 -4 186.10 7.60 1 7 1 5 27.70 3.50 1 -7 -1 -5 24.80 2.80 1 7 1 6 731.20 21.80 1 -7 -1 -6 681.80 19.20 1 7 1 7 21.30 3.10 1 -7 -1 -7 29.80 3.70 1 7 1 8 352.20 11.90 1 -7 -1 -8 342.90 12.00 1 7 1 9 29.60 3.50 1 -7 -1 -9 25.40 3.70 1 7 1 10 16.90 2.90 1 -7 -1 -10 22.50 3.20 1 7 1 11 59.90 4.60 1 -7 -1 -11 59.10 4.80 1 7 1 12 511.60 16.30 1 -7 -1 -12 507.10 16.60 1 7 1 13 14.70 2.80 1 -7 -1 -13 13.10 2.90 1 7 1 14 297.50 12.90 1 -7 -1 -14 275.90 11.60 1 7 1 15 59.30 5.10 1 -7 -1 -15 44.70 4.70 1 7 1 16 5.50 3.10 1 -7 -1 -16 6.00 3.10 1 7 1 17 17.80 3.60 1 -7 -1 -17 19.40 3.80 1 7 1 18 311.30 13.10 1 -7 -1 -18 325.40 14.20 1 7 1 19 27.50 4.20 1 -7 -1 -19 30.30 4.30 1 7 1 20 214.10 10.60 1 -7 -1 -20 246.20 11.40 1 7 2 0 54.30 3.90 1 7 2 1 133.10 6.20 1 -7 -2 -1 124.60 6.10 1 7 2 2 17.40 3.20 1 -7 -2 -2 24.40 3.10 1 7 2 3 640.30 19.80 1 -7 -2 -3 657.10 19.70 1 7 2 4 11.30 2.80 1 -7 -2 -4 12.60 2.70 1 7 2 5 228.30 8.60 1 -7 -2 -5 217.50 8.30 1 7 2 6 19.10 2.80 1 -7 -2 -6 19.10 3.00 1 7 2 7 83.30 4.90 1 -7 -2 -7 77.30 4.80 1 7 2 8 59.10 4.50 1 -7 -2 -8 64.40 4.20 1 7 2 9 397.90 12.70 1 -7 -2 -9 356.50 12.30 1 7 2 10 42.00 3.70 1 -7 -2 -10 42.90 4.10 1 7 2 11 218.40 8.50 1 -7 -2 -11 222.90 9.20 1 7 2 12 42.80 3.90 1 -7 -2 -12 43.70 4.00 1 7 2 13 45.30 6.20 1 -7 -2 -13 57.60 3.80 1 7 2 14 3.90 2.70 1 -7 -2 -14 14.90 3.60 1 7 2 15 243.00 10.90 1 -7 -2 -15 289.40 12.80 1 7 2 16 35.00 4.30 1 -7 -2 -16 36.50 4.00 1 7 2 17 118.00 7.20 1 -7 -2 -17 97.70 6.80 1 7 2 18 55.30 5.20 1 -7 -2 -18 36.50 4.40 1 7 2 19 12.10 4.40 1 -7 -2 -19 4.20 3.10 1 7 2 20 20.50 4.90 1 -7 -2 -20 25.60 3.80 1 7 3 0 143.30 6.50 1 7 3 1 24.10 3.20 1 -7 -3 -1 18.80 3.00 1 7 3 2 39.60 2.90 1 -7 -3 -2 51.40 4.10 1 7 3 3 3.80 1.90 1 -7 -3 -3 2.80 2.80 1 7 3 4 9.00 2.00 1 -7 -3 -4 12.10 3.00 1 7 3 5 54.70 3.40 1 -7 -3 -5 60.50 4.30 1 7 3 6 91.60 4.30 1 -7 -3 -6 84.30 5.20 1 7 3 7 7.30 2.10 1 -7 -3 -7 4.10 2.60 1 7 3 8 44.60 3.50 1 -7 -3 -8 37.00 3.80 1 7 3 9 41.20 3.50 1 -7 -3 -9 48.50 3.80 1 7 3 10 4.30 2.50 1 -7 -3 -10 1.20 2.50 1 7 3 11 51.10 3.50 1 -7 -3 -11 41.90 4.00 1 7 3 12 60.10 4.90 1 -7 -3 -12 66.90 5.40 1 7 3 13 5.70 4.30 1 -7 -3 -13 8.20 2.10 1 7 3 14 35.20 3.30 1 -7 -3 -14 30.30 3.90 1 7 3 15 77.30 6.10 1 -7 -3 -15 62.30 5.10 1 7 3 16 3.60 3.80 1 -7 -3 -16 8.40 3.50 1 7 3 17 87.90 6.90 1 -7 -3 -17 102.20 6.50 1 7 3 18 25.10 3.80 1 -7 -3 -18 36.00 6.40 1 7 3 19 2.60 3.30 1 -7 -3 -19 2.20 6.20 1 7 4 0 45.50 3.70 1 7 4 1 111.10 4.90 1 -7 -4 -1 106.50 5.60 1 7 4 2 141.70 5.40 1 -7 -4 -2 158.60 7.30 1 7 4 3 716.80 17.30 1 -7 -4 -3 653.60 21.10 1 7 4 4 104.00 4.40 1 -7 -4 -4 79.70 4.90 1 7 4 5 235.00 7.30 1 -7 -4 -5 244.10 9.10 1 7 4 6 61.30 3.40 1 -7 -4 -6 76.80 5.10 1 7 4 7 24.50 2.90 1 -7 -4 -7 28.60 3.90 1 7 4 8 68.30 3.80 1 -7 -4 -8 70.20 5.40 1 7 4 9 468.90 17.90 1 -7 -4 -9 456.50 18.10 1 7 4 10 93.90 6.20 1 -7 -4 -10 98.90 6.00 1 7 4 11 230.50 11.10 1 -7 -4 -11 258.40 11.30 1 7 4 12 13.70 4.20 1 -7 -4 -12 21.90 3.80 1 7 4 13 13.90 3.30 1 -7 -4 -13 14.00 5.60 1 7 4 14 58.50 4.60 1 -7 -4 -14 41.80 7.30 1 7 4 15 249.30 9.50 1 -7 -4 -15 261.60 18.00 1 7 4 16 62.50 5.70 1 -7 -4 -16 37.40 6.00 1 7 4 17 192.80 8.60 1 -7 -4 -17 184.00 13.90 1 7 5 0 135.60 6.50 1 7 5 1 17.20 2.50 1 -7 -5 -1 18.90 3.30 1 7 5 2 24.60 4.20 1 -7 -5 -2 21.60 3.50 1 7 5 3 6.60 3.00 1 -7 -5 -3 2.80 2.60 1 7 5 4 38.50 4.70 1 -7 -5 -4 38.50 3.80 1 7 5 5 28.20 3.90 1 -7 -5 -5 27.60 3.70 1 7 5 6 134.60 7.70 1 -7 -5 -6 138.60 7.40 1 7 5 7 27.10 3.80 1 -7 -5 -7 30.60 3.30 1 7 5 8 27.30 4.30 1 -7 -5 -8 33.20 3.50 1 7 5 9 34.40 4.60 1 -7 -5 -9 28.80 3.80 1 7 5 10 39.80 4.60 1 -7 -5 -10 37.40 4.60 1 7 5 11 -1.50 2.90 1 -7 -5 -11 7.50 3.10 1 7 5 12 114.10 7.00 1 -7 -5 -12 113.10 7.00 1 7 5 13 78.70 4.90 1 -7 -5 -13 60.80 7.90 1 7 5 14 26.50 3.40 1 -7 -5 -14 33.40 7.00 1 7 5 15 47.50 4.00 1 -7 -5 -15 41.80 6.60 1 7 6 0 3.70 4.90 1 7 6 1 59.30 5.30 1 -7 -6 -1 63.80 6.90 1 7 6 2 72.30 5.50 1 -7 -6 -2 71.30 8.20 1 7 6 3 92.70 6.80 1 -7 -6 -3 92.80 9.30 1 7 6 4 40.40 4.60 1 -7 -6 -4 33.30 5.30 1 7 6 5 108.40 7.20 1 -7 -6 -5 104.40 9.60 1 7 6 6 33.20 4.60 1 -7 -6 -6 25.40 5.60 1 7 6 7 8.50 2.90 1 -7 -6 -7 6.40 3.80 1 7 6 8 70.20 6.10 1 -7 -6 -8 79.80 8.60 1 7 6 9 95.30 6.40 1 -7 -6 -9 101.70 9.70 1 7 6 10 21.40 3.60 1 -7 -6 -10 30.20 5.40 1 7 6 11 74.80 6.50 1 -7 -6 -11 71.30 8.70 1 7 6 12 19.80 3.80 1 -7 -6 -12 22.20 5.80 1 7 7 0 197.00 14.40 1 7 7 1 278.60 12.20 1 -7 -7 -1 258.70 16.60 1 7 7 2 42.30 5.10 1 -7 -7 -2 36.60 6.10 1 7 7 3 4.40 3.70 1 -7 -7 -3 11.40 5.50 1 7 7 4 49.70 4.90 1 -7 -7 -4 68.20 8.30 1 7 7 5 185.90 9.70 1 -7 -7 -5 137.40 11.50 1 7 7 6 187.60 10.10 1 -7 -7 -6 162.30 11.80 1 7 7 7 178.20 9.50 1 -7 -7 -7 202.70 14.50 1 7 7 8 101.80 7.40 1 -7 -7 -8 93.90 10.70 1 8 0 0 587.70 28.80 1 8 0 1 16.20 3.90 1 8 0 2 120.00 7.10 1 8 0 3 3.80 3.20 1 8 0 4 53.60 4.80 1 8 0 5 12.00 3.00 1 8 0 6 520.50 19.60 1 8 0 7 9.20 2.90 1 8 0 8 239.80 15.60 1 8 0 9 90.40 6.40 1 8 0 10 64.10 5.90 1 8 0 11 18.90 4.40 1 8 0 12 283.80 13.30 1 8 0 13 19.20 5.60 1 8 1 0 3.20 2.60 1 8 1 1 99.70 6.30 1 -8 -1 -1 118.20 6.90 1 8 1 2 11.50 2.80 1 -8 -1 -2 22.60 3.60 1 8 1 3 101.50 6.10 1 -8 -1 -3 127.30 7.20 1 8 1 4 -3.10 2.70 1 -8 -1 -4 2.40 3.00 1 8 1 5 83.90 5.60 1 -8 -1 -5 79.10 5.80 1 8 1 6 8.20 3.10 1 -8 -1 -6 12.00 3.20 1 8 1 7 74.50 5.40 1 -8 -1 -7 76.90 5.30 1 8 1 8 17.60 3.40 1 -8 -1 -8 22.00 3.80 1 8 1 9 67.50 5.20 1 -8 -1 -9 80.80 5.80 1 8 1 10 2.50 3.20 1 -8 -1 -10 0.00 4.10 1 8 1 11 80.40 6.20 1 -8 -1 -11 70.10 5.80 1 8 1 12 39.80 5.10 1 -8 -1 -12 40.60 4.90 1 8 2 0 191.30 9.60 1 8 2 1 16.80 3.40 1 -8 -2 -1 16.30 3.20 1 8 2 2 121.00 6.90 1 -8 -2 -2 97.70 5.80 1 8 2 3 54.60 4.70 1 -8 -2 -3 59.50 5.30 1 8 2 4 78.70 5.70 1 -8 -2 -4 76.10 5.80 1 8 2 5 66.50 5.30 1 -8 -2 -5 58.60 5.20 1 8 2 6 149.30 7.90 1 -8 -2 -6 159.50 9.00 1 8 2 7 10.40 3.80 1 -8 -2 -7 9.70 4.20 1 8 2 8 110.40 6.80 1 -8 -2 -8 120.70 7.50 1 8 2 9 16.70 3.20 1 -8 -2 -9 24.90 4.80 1 8 2 10 24.50 4.10 1 -8 -2 -10 24.50 3.90 1 8 2 11 52.90 5.40 1 -8 -2 -11 50.10 5.20 1 8 3 0 -7.10 3.70 1 8 3 1 44.90 4.60 1 -8 -3 -1 62.00 5.50 1 8 3 2 17.40 4.10 1 -8 -3 -2 14.20 3.40 1 8 3 3 293.80 12.60 1 -8 -3 -3 325.40 13.40 1 8 3 4 18.80 3.70 1 -8 -3 -4 28.30 4.40 1 8 3 5 136.90 8.10 1 -8 -3 -5 131.70 7.50 1 8 3 6 15.40 3.90 1 -8 -3 -6 9.70 3.10 1 8 3 7 86.50 6.40 1 -8 -3 -7 82.00 6.30 1 8 3 8 15.90 5.20 1 -8 -3 -8 11.50 4.40 1 8 3 9 201.60 10.10 1 -8 -3 -9 177.20 9.40 1 8 3 10 14.60 7.00 1 -8 -3 -10 8.90 3.60 1 8 4 0 24.40 4.10 1 8 4 1 6.40 4.40 1 -8 -4 -1 -4.60 3.70 1 8 4 2 56.70 8.00 1 -8 -4 -2 58.50 5.00 1 8 4 3 36.00 6.10 1 -8 -4 -3 29.70 4.10 1 8 4 4 146.00 12.10 1 -8 -4 -4 137.20 7.50 1 8 4 5 0.40 4.30 1 -8 -4 -5 9.50 3.10 1 8 4 6 19.10 6.80 1 -8 -4 -6 26.00 4.00 1 8 4 7 14.30 6.80 1 -8 -4 -7 15.50 4.40 1 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 49452 _shelx_res_file ; TITL jer1101 in P 21 21 21 shelx.res created by SHELXL-2018/1 at 16:09:55 on 14-Feb-2024 CELL 0.71073 6.6117 10.1482 28.1444 90.000 90.000 90.000 ZERR 4.00 0.0002 0.0002 0.0009 0.000 0.000 0.000 LATT -1 SYMM 1/2 - X, - Y, 1/2 + Z SYMM 1/2 + X, 1/2 - Y, - Z SYMM - X, 1/2 + Y, 1/2 - Z SFAC C H I N O S UNIT 60 84 8 12 8 4 MERG 2 HTAB N1 I1 HTAB N1 O1 htab c7 o2 htab c14 o1 eqiv $1 x-1, y, z htab c6 o1_$1 eqiv $2 x-1/2, -y+1/2, -z+1 htab c7 o2_$2 eqiv $3 x-1/2, -y+1/2, -z+1 htab c10 o2_$3 FMAP 2 PLAN 10 SIZE 0.201 0.202 0.410 ACTA BOND $H L.S. 4 TEMP -123.00 WGHT 0.025100 5.677800 EXTI 0.006839 FVAR 0.26821 C1 1 0.643970 0.297850 0.354473 11.00000 0.02099 0.01469 = 0.01718 -0.00199 -0.00025 0.00344 C2 1 0.841182 0.414462 0.291924 11.00000 0.02300 0.02029 = 0.01661 0.00223 0.00080 -0.00079 AFIX 13 H2 2 0.949093 0.357300 0.277960 11.00000 -1.20000 AFIX 0 C3 1 0.651468 0.400775 0.262004 11.00000 0.02995 0.02361 = 0.01364 0.00158 -0.00348 0.00231 AFIX 23 H3A 2 0.557522 0.474061 0.269212 11.00000 -1.20000 H3B 2 0.687244 0.405578 0.227891 11.00000 -1.20000 AFIX 0 C4 1 0.549220 0.270671 0.272324 11.00000 0.03305 0.03323 = 0.01271 -0.00003 -0.00075 -0.00008 AFIX 23 H4A 2 0.421253 0.264838 0.254181 11.00000 -1.20000 H4B 2 0.637911 0.197383 0.262082 11.00000 -1.20000 AFIX 0 C5 1 0.323752 0.183773 0.336377 11.00000 0.02429 0.02531 = 0.03200 -0.00113 -0.00198 -0.00408 AFIX 23 H5A 2 0.340605 0.090934 0.326324 11.00000 -1.20000 H5B 2 0.206408 0.220687 0.319050 11.00000 -1.20000 AFIX 0 C6 1 0.281942 0.188099 0.388974 11.00000 0.01926 0.02532 = 0.02889 -0.00236 0.00148 -0.00361 AFIX 23 H6A 2 0.178509 0.121590 0.397449 11.00000 -1.20000 H6B 2 0.230543 0.276178 0.398078 11.00000 -1.20000 AFIX 0 C7 1 0.477304 0.159379 0.414751 11.00000 0.02261 0.02134 = 0.02537 0.00029 0.00181 -0.00386 AFIX 23 H7A 2 0.453776 0.158156 0.449487 11.00000 -1.20000 H7B 2 0.530122 0.072116 0.405091 11.00000 -1.20000 AFIX 0 C8 1 0.914883 0.555884 0.291751 11.00000 0.02078 0.02754 = 0.01989 0.00162 -0.00508 0.00179 AFIX 23 H8A 2 0.806441 0.613563 0.304233 11.00000 -1.20000 H8B 2 0.942861 0.582957 0.258602 11.00000 -1.20000 AFIX 0 C9 1 0.568959 0.503553 0.445004 11.00000 0.01656 0.02170 = 0.01780 -0.00319 -0.00164 -0.00268 C10 1 0.377658 0.498902 0.466400 11.00000 0.02112 0.01755 = 0.01985 0.00293 -0.00006 -0.00292 AFIX 43 H10 2 0.329194 0.420139 0.480654 11.00000 -1.20000 AFIX 0 C11 1 0.260969 0.612685 0.466174 11.00000 0.02330 0.02274 = 0.02628 -0.00376 0.00128 -0.00046 AFIX 43 H11 2 0.132677 0.611967 0.481372 11.00000 -1.20000 AFIX 0 C12 1 0.327300 0.727720 0.444239 11.00000 0.02675 0.01893 = 0.02006 -0.00140 -0.00064 0.00181 C13 1 0.519687 0.729735 0.423040 11.00000 0.03139 0.02154 = 0.02480 0.00117 0.00255 -0.00156 AFIX 43 H13 2 0.567125 0.807997 0.408247 11.00000 -1.20000 AFIX 0 C14 1 0.640614 0.618221 0.423586 11.00000 0.02532 0.02208 = 0.01965 -0.00093 -0.00010 -0.00841 AFIX 43 H14 2 0.771147 0.619926 0.409492 11.00000 -1.20000 AFIX 0 C15 1 0.194777 0.848240 0.442045 11.00000 0.04505 0.02875 = 0.03159 -0.00231 0.00069 0.01106 AFIX 137 H15A 2 0.068847 0.831523 0.459393 11.00000 -1.50000 H15B 2 0.163584 0.868658 0.408810 11.00000 -1.50000 H15C 2 0.265650 0.922976 0.456504 11.00000 -1.50000 AFIX 0 I1 3 1.183494 0.583740 0.333641 11.00000 0.02535 0.03161 = 0.02364 0.00262 0.00070 -0.00409 I2 3 0.172763 0.451806 0.175164 11.00000 0.02475 0.03010 = 0.02529 -0.00130 0.00167 -0.00338 N1 4 10.801213 10.370167 10.340930 11.00000 0.01866 0.02500 = 0.01896 0.00064 -0.00066 0.00064 AFIX 43 H1 2 0.888533 0.393510 0.362975 11.00000 -1.20000 AFIX 0 N2 4 0.506289 0.258451 0.323722 11.00000 0.01988 0.02816 = 0.01725 0.00122 -0.00308 -0.00176 N3 4 0.625414 0.263879 0.402477 11.00000 0.02152 0.01781 = 0.01336 0.00307 0.00198 -0.00212 O1 5 0.920310 0.395539 0.433628 11.00000 0.01499 0.03550 = 0.01969 -0.00208 0.00123 -0.00097 O2 5 0.679848 0.289113 0.488856 11.00000 0.02859 0.02680 = 0.01438 0.00459 -0.00095 0.00152 S1 6 0.716906 0.360917 0.446037 11.00000 0.01931 0.02097 = 0.01494 0.00064 -0.00152 0.00101 HKLF 4 REM jer1101 in P 21 21 21 REM R1 = 0.0308 for 3858 Fo > 4sig(Fo) and 0.0359 for all 4087 data REM 207 parameters refined using 0 restraints END WGHT 0.0252 5.6737 REM Highest difference peak 0.772, deepest hole -0.787, 1-sigma level 0.108 Q1 1 0.1737 0.3231 0.3314 11.00000 0.05 0.77 Q2 1 0.1774 0.4579 0.1493 11.00000 0.05 0.73 Q3 1 0.1783 0.4529 0.4891 11.00000 0.05 0.70 Q4 1 0.8165 0.2175 0.3283 11.00000 0.05 0.61 Q5 1 1.1766 0.5900 0.3078 11.00000 0.05 0.59 Q6 1 0.1848 0.7173 0.4913 11.00000 0.05 0.59 Q7 1 0.3290 0.4159 0.5131 11.00000 0.05 0.59 Q8 1 0.5262 -0.0488 0.3288 11.00000 0.05 0.55 Q9 1 1.3309 0.5215 0.3167 11.00000 0.05 0.53 Q10 1 0.4612 0.3557 0.1779 11.00000 0.05 0.51 ; _shelx_res_checksum 28113 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C C1 0.6440(9) 0.2979(6) 0.3545(2) 0.0176(12) Uani d 1 . . C C2 0.8412(10) 0.4145(6) 0.2919(2) 0.0200(12) Uani d 1 . . H H2 0.949093 0.357300 0.277960 0.024 Uiso calc 1 . . C C3 0.6515(10) 0.4008(6) 0.2620(2) 0.0224(13) Uani d 1 . . H H3A 0.557522 0.474061 0.269212 0.027 Uiso calc 1 . . H H3B 0.687244 0.405578 0.227891 0.027 Uiso calc 1 . . C C4 0.5492(11) 0.2707(7) 0.2723(2) 0.0263(15) Uani d 1 . . H H4A 0.421253 0.264838 0.254181 0.032 Uiso calc 1 . . H H4B 0.637911 0.197383 0.262082 0.032 Uiso calc 1 . . C C5 0.3238(11) 0.1838(6) 0.3364(2) 0.0272(13) Uani d 1 . . H H5A 0.340605 0.090934 0.326324 0.033 Uiso calc 1 . . H H5B 0.206408 0.220687 0.319050 0.033 Uiso calc 1 . . C C6 0.2819(9) 0.1881(7) 0.3890(2) 0.0245(14) Uani d 1 . . H H6A 0.178509 0.121590 0.397449 0.029 Uiso calc 1 . . H H6B 0.230543 0.276178 0.398078 0.029 Uiso calc 1 . . C C7 0.4773(10) 0.1594(6) 0.4148(2) 0.0231(14) Uani d 1 . . H H7A 0.453776 0.158156 0.449487 0.028 Uiso calc 1 . . H H7B 0.530122 0.072116 0.405091 0.028 Uiso calc 1 . . C C8 0.9149(9) 0.5559(7) 0.2918(2) 0.0227(13) Uani d 1 . . H H8A 0.806441 0.613563 0.304233 0.027 Uiso calc 1 . . H H8B 0.942861 0.582957 0.258602 0.027 Uiso calc 1 . . C C9 0.5690(9) 0.5036(6) 0.4450(2) 0.0187(13) Uani d 1 . . C C10 0.3777(9) 0.4989(6) 0.4664(2) 0.0195(13) Uani d 1 . . H H10 0.329194 0.420139 0.480654 0.023 Uiso calc 1 . . C C11 0.2610(10) 0.6127(7) 0.4662(2) 0.0241(14) Uani d 1 . . H H11 0.132677 0.611967 0.481372 0.029 Uiso calc 1 . . C C12 0.3273(11) 0.7277(6) 0.4442(2) 0.0219(12) Uani d 1 . . C C13 0.5197(10) 0.7297(7) 0.4230(3) 0.0259(15) Uani d 1 . . H H13 0.567125 0.807997 0.408247 0.031 Uiso calc 1 . . C C14 0.6406(10) 0.6182(6) 0.4236(2) 0.0223(14) Uani d 1 . . H H14 0.771147 0.619926 0.409492 0.027 Uiso calc 1 . . C C15 0.1948(13) 0.8482(7) 0.4420(3) 0.0351(17) Uani d 1 . . H H15A 0.068847 0.831523 0.459393 0.053 Uiso calc 1 . . H H15B 0.163584 0.868658 0.408810 0.053 Uiso calc 1 . . H H15C 0.265650 0.922976 0.456504 0.053 Uiso calc 1 . . I I1 1.18349(7) 0.58374(4) 0.33364(2) 0.02686(13) Uani d 1 . . I I2 0.17276(7) 0.45181(4) 0.17516(2) 0.02671(13) Uani d 1 . . N N1 0.801213 0.370167 0.340930 0.0209(10) Uani d 1 . . H H1 0.888533 0.393510 0.362975 0.025 Uiso calc 1 . . N N2 0.5063(7) 0.2585(5) 0.3237(2) 0.0218(11) Uani d 1 . . N N3 0.6254(8) 0.2639(5) 0.40248(18) 0.0176(11) Uani d 1 . . O O1 0.9203(6) 0.3955(5) 0.43363(16) 0.0234(10) Uani d 1 . . O O2 0.6798(7) 0.2891(4) 0.48886(14) 0.0233(9) Uani d 1 . . S S1 0.7169(2) 0.36092(16) 0.44604(6) 0.0184(3) Uani d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 C1 0.021(3) 0.015(3) 0.017(3) 0.003(2) 0.000(2) -0.002(2) C2 0.023(3) 0.020(3) 0.017(3) -0.001(3) 0.001(2) 0.002(2) C3 0.030(3) 0.024(3) 0.014(3) 0.002(3) -0.003(3) 0.002(2) C4 0.033(4) 0.033(4) 0.013(3) 0.000(3) -0.001(3) 0.000(3) C5 0.024(3) 0.025(3) 0.032(4) -0.004(3) -0.002(3) -0.001(3) C6 0.019(3) 0.025(3) 0.029(4) -0.004(3) 0.001(3) -0.002(3) C7 0.023(3) 0.021(3) 0.025(3) -0.004(3) 0.002(3) 0.000(3) C8 0.021(3) 0.028(4) 0.020(3) 0.002(3) -0.005(2) 0.002(3) C9 0.017(3) 0.022(3) 0.018(3) -0.003(2) -0.002(2) -0.003(2) C10 0.021(3) 0.018(3) 0.020(3) -0.003(2) 0.000(2) 0.003(2) C11 0.023(3) 0.023(3) 0.026(3) 0.000(2) 0.001(2) -0.004(3) C12 0.027(3) 0.019(3) 0.020(3) 0.002(3) -0.001(3) -0.001(2) C13 0.031(4) 0.022(3) 0.025(4) -0.002(3) 0.003(3) 0.001(3) C14 0.025(4) 0.022(3) 0.020(3) -0.008(3) 0.000(2) -0.001(2) C15 0.045(4) 0.029(4) 0.032(4) 0.011(4) 0.001(4) -0.002(3) I1 0.0253(2) 0.0316(2) 0.0236(2) -0.00409(18) 0.00070(18) 0.00262(17) I2 0.0248(2) 0.0301(2) 0.0253(2) -0.00338(18) 0.00167(18) -0.00130(17) N1 0.019(2) 0.025(3) 0.019(2) 0.001(2) -0.001(2) 0.001(2) N2 0.020(3) 0.028(3) 0.017(3) -0.002(2) -0.003(2) 0.001(2) N3 0.022(3) 0.018(3) 0.013(2) -0.002(2) 0.0020(19) 0.003(2) O1 0.015(2) 0.036(3) 0.020(2) -0.0010(19) 0.0012(17) -0.002(2) O2 0.029(2) 0.027(2) 0.0144(19) 0.002(2) -0.001(2) 0.0046(17) S1 0.0193(8) 0.0210(7) 0.0149(7) 0.0010(6) -0.0015(5) 0.0006(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag N2 C1 N1 . . 121.3(5) ? N2 C1 N3 . . 119.9(6) ? N1 C1 N3 . . 118.8(5) ? N1 C2 C8 . . 110.4(5) ? N1 C2 C3 . . 110.1(5) ? C8 C2 C3 . . 110.5(5) ? N1 C2 H2 . . 108.6 ? C8 C2 H2 . . 108.6 ? C3 C2 H2 . . 108.6 ? C4 C3 C2 . . 110.1(5) ? C4 C3 H3A . . 109.6 ? C2 C3 H3A . . 109.6 ? C4 C3 H3B . . 109.6 ? C2 C3 H3B . . 109.6 ? H3A C3 H3B . . 108.2 ? N2 C4 C3 . . 110.3(5) ? N2 C4 H4A . . 109.6 ? C3 C4 H4A . . 109.6 ? N2 C4 H4B . . 109.6 ? C3 C4 H4B . . 109.6 ? H4A C4 H4B . . 108.1 ? N2 C5 C6 . . 112.0(5) ? N2 C5 H5A . . 109.2 ? C6 C5 H5A . . 109.2 ? N2 C5 H5B . . 109.2 ? C6 C5 H5B . . 109.2 ? H5A C5 H5B . . 107.9 ? C5 C6 C7 . . 108.0(5) ? C5 C6 H6A . . 110.1 ? C7 C6 H6A . . 110.1 ? C5 C6 H6B . . 110.1 ? C7 C6 H6B . . 110.1 ? H6A C6 H6B . . 108.4 ? N3 C7 C6 . . 108.3(5) ? N3 C7 H7A . . 110.0 ? C6 C7 H7A . . 110.0 ? N3 C7 H7B . . 110.0 ? C6 C7 H7B . . 110.0 ? H7A C7 H7B . . 108.4 ? C2 C8 I1 . . 112.8(4) ? C2 C8 H8A . . 109.0 ? I1 C8 H8A . . 109.0 ? C2 C8 H8B . . 109.0 ? I1 C8 H8B . . 109.0 ? H8A C8 H8B . . 107.8 ? C14 C9 C10 . . 121.4(6) ? C14 C9 S1 . . 120.6(5) ? C10 C9 S1 . . 118.0(5) ? C11 C10 C9 . . 118.1(6) ? C11 C10 H10 . . 120.9 ? C9 C10 H10 . . 120.9 ? C10 C11 C12 . . 121.6(6) ? C10 C11 H11 . . 119.2 ? C12 C11 H11 . . 119.2 ? C11 C12 C13 . . 119.1(6) ? C11 C12 C15 . . 121.1(7) ? C13 C12 C15 . . 119.8(6) ? C14 C13 C12 . . 120.4(6) ? C14 C13 H13 . . 119.8 ? C12 C13 H13 . . 119.8 ? C13 C14 C9 . . 119.4(6) ? C13 C14 H14 . . 120.3 ? C9 C14 H14 . . 120.3 ? C12 C15 H15A . . 109.5 ? C12 C15 H15B . . 109.5 ? H15A C15 H15B . . 109.5 ? C12 C15 H15C . . 109.5 ? H15A C15 H15C . . 109.5 ? H15B C15 H15C . . 109.5 ? C1 N1 C2 . . 125.2(4) ? C1 N1 H1 . . 117.4 ? C2 N1 H1 . . 117.4 ? C1 N2 C5 . . 124.4(6) ? C1 N2 C4 . . 119.0(5) ? C5 N2 C4 . . 116.0(5) ? C1 N3 C7 . . 117.3(5) ? C1 N3 S1 . . 121.8(4) ? C7 N3 S1 . . 119.0(4) ? O2 S1 O1 . . 119.4(3) ? O2 S1 N3 . . 104.7(3) ? O1 S1 N3 . . 107.6(3) ? O2 S1 C9 . . 109.9(3) ? O1 S1 C9 . . 108.6(3) ? N3 S1 C9 . . 105.7(3) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag C1 N2 . 1.318(8) ? C1 N1 . 1.328(6) ? C1 N3 . 1.400(7) ? C2 N1 . 1.475(6) ? C2 C8 . 1.516(9) ? C2 C3 . 1.517(9) ? C2 H2 . 1.0000 ? C3 C4 . 1.511(10) ? C3 H3A . 0.9900 ? C3 H3B . 0.9900 ? C4 N2 . 1.479(8) ? C4 H4A . 0.9900 ? C4 H4B . 0.9900 ? C5 N2 . 1.469(8) ? C5 C6 . 1.507(9) ? C5 H5A . 0.9900 ? C5 H5B . 0.9900 ? C6 C7 . 1.510(9) ? C6 H6A . 0.9900 ? C6 H6B . 0.9900 ? C7 N3 . 1.484(8) ? C7 H7A . 0.9900 ? C7 H7B . 0.9900 ? C8 I1 . 2.150(6) ? C8 H8A . 0.9900 ? C8 H8B . 0.9900 ? C9 C14 . 1.394(9) ? C9 C10 . 1.402(8) ? C9 S1 . 1.747(6) ? C10 C11 . 1.389(9) ? C10 H10 . 0.9500 ? C11 C12 . 1.391(9) ? C11 H11 . 0.9500 ? C12 C13 . 1.405(10) ? C12 C15 . 1.506(9) ? C13 C14 . 1.386(10) ? C13 H13 . 0.9500 ? C14 H14 . 0.9500 ? C15 H15A . 0.9800 ? C15 H15B . 0.9800 ? C15 H15C . 0.9800 ? N1 H1 . 0.8800 ? N3 S1 . 1.685(5) ? O1 S1 . 1.433(4) ? O2 S1 . 1.429(4) ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag N1 H1 I1 . 0.88 2.87 3.3359(4) 115.1 yes N1 H1 O1 . 0.88 2.00 2.737(5) 140.6 yes C7 H7A O2 . 0.99 2.29 2.807(8) 111.6 yes C14 H14 O1 . 0.95 2.57 2.934(8) 102.8 yes C6 H6B O1 1_455 0.99 2.58 3.425(8) 142.8 yes C7 H7A O2 3_456 0.99 2.56 3.391(8) 140.9 yes C10 H10 O2 3_456 0.95 2.49 3.441(7) 174.4 yes