#------------------------------------------------------------------------------ #$Date: 2024-04-06 01:41:39 +0200 (Sat, 06 Apr 2024) $ #$Revision: 291112 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/30/2023036.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023036 loop_ _publ_author_name 'Dhote, Pawan' 'Tothadi, Srinu' 'Ramana, Chepuri V.' _publ_section_title ; Synthesis, characterization, and crystal structure of 2-(2-azido-phen-yl)-3-oxo-3H-indole 1-oxide. ; _journal_coeditor_code DX2056 _journal_issue 'Pt 3' _journal_name_full 'Acta crystallographica. Section E, Crystallographic communications' _journal_page_first 310 _journal_page_last 313 _journal_paper_doi 10.1107/S2056989024001440 _journal_volume 80 _journal_year 2024 _chemical_formula_iupac 'C14 H8 N4 O2' _chemical_formula_moiety 'C14 H8 N4 O2' _chemical_formula_sum 'C14 H8 N4 O2' _chemical_formula_weight 264.24 _chemical_name_systematic ; 2-(2-Azidophenyl)-3-oxo-3H-indole 1-oxide ; _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _cell_angle_alpha 95.473(16) _cell_angle_beta 105.226(12) _cell_angle_gamma 113.116(13) _cell_formula_units_Z 2 _cell_length_a 7.166(2) _cell_length_b 7.686(3) _cell_length_c 12.172(4) _cell_measurement_reflns_used 9975 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 34.56 _cell_measurement_theta_min 3.10 _cell_volume 579.9(3) _computing_cell_refinement ; SAINT v8.37A (Bruker, 2015) ; _computing_data_collection ; APEX2 (Bruker, 2015) ; _computing_data_reduction ; SAINT v8.37A (Bruker, 2015) ; _computing_molecular_graphics ; Olex2 (Dolomanov et al., 2009) ; _computing_publication_material ; Olex2 (Dolomanov et al., 2009) ; _computing_structure_refinement ; SHELXL (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2014/5 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 100.0 _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.927 _diffrn_measurement_device_type 'Bruker D8 VENTURE Kappa Duo PHOTON II CPAD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0485 _diffrn_reflns_av_unetI/netI 0.0321 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 45548 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 35.205 _diffrn_reflns_theta_min 2.956 _exptl_absorpt_coefficient_mu 0.107 _exptl_absorpt_correction_T_max 0.7453 _exptl_absorpt_correction_T_min 0.6261 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.513 _exptl_crystal_description block _exptl_crystal_F_000 272 _exptl_crystal_size_max 0.12 _exptl_crystal_size_mid 0.06 _exptl_crystal_size_min 0.05 _refine_diff_density_max 0.464 _refine_diff_density_min -0.287 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.053 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 181 _refine_ls_number_reflns 4818 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.053 _refine_ls_R_factor_all 0.0568 _refine_ls_R_factor_gt 0.0422 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0660P)^2^+0.1514P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1131 _refine_ls_wR_factor_ref 0.1220 _reflns_number_gt 3946 _reflns_number_total 4818 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file dx2056sup1.cif _cod_data_source_block I _cod_depositor_comments 'Adding full bibliography for 2023036.cif.' _cod_database_code 2023036 _cod_database_fobs_code 2023036 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.987 _shelx_estimated_absorpt_t_max 0.995 _shelx_hkl_file ; 1 0 0 3794.52 186.98 -2 0 0 1467.85 68.19 -2 0 0 1304.47 69.09 -2 0 0 1314.57 69.49 -2 0 0 1372.86 68.89 -2 0 0 1476.05 67.99 -2 0 0 1281.27 69.79 -2 0 0 1505.95 68.59 -2 0 0 1472.35 68.09 2 0 0 1403.56 68.69 2 0 0 1309.97 68.09 2 0 0 1313.97 68.39 2 0 0 1510.45 69.59 2 0 0 1350.46 68.19 2 0 0 1398.96 67.89 2 0 0 1527.45 70.19 2 0 0 1266.27 67.79 2 0 0 1402.76 68.09 2 0 0 1363.56 68.59 2 0 0 1277.97 68.39 2 0 0 1310.27 67.89 2 0 0 1363.86 69.29 -3 0 0 268.57 14.80 -3 0 0 259.77 15.20 -3 0 0 268.77 16.50 -3 0 0 248.28 15.80 -3 0 0 271.07 13.70 -3 0 0 270.57 13.40 -3 0 0 270.17 14.30 -3 0 0 265.47 13.60 -3 0 0 263.77 13.60 3 0 0 264.87 14.60 3 0 0 274.47 13.60 3 0 0 259.07 13.80 3 0 0 237.18 14.30 3 0 0 225.18 14.00 3 0 0 233.68 14.50 3 0 0 268.77 15.50 3 0 0 268.27 16.40 3 0 0 259.67 13.70 3 0 0 279.57 13.30 3 0 0 248.78 14.10 3 0 0 239.48 15.20 -4 0 0 917.51 44.60 -4 0 0 949.40 47.40 -4 0 0 910.51 48.40 -4 0 0 815.12 46.30 -4 0 0 877.61 44.80 -4 0 0 899.11 46.40 -4 0 0 895.81 44.60 -4 0 0 887.31 44.70 -4 0 0 931.61 48.90 4 0 0 879.11 46.00 4 0 0 893.71 46.40 4 0 0 776.52 45.40 4 0 0 914.01 45.20 4 0 0 920.21 44.50 4 0 0 867.71 48.60 4 0 0 882.51 44.60 4 0 0 924.71 44.80 4 0 0 903.01 45.00 4 0 0 914.71 46.20 4 0 0 912.71 47.60 4 0 0 814.82 47.30 4 0 0 877.71 46.20 4 0 0 959.70 45.70 -5 0 0 325.77 18.10 -5 0 0 338.87 21.30 -5 0 0 377.86 23.10 -5 0 0 353.46 20.60 -5 0 0 330.87 18.90 -5 0 0 301.47 22.60 -5 0 0 368.16 18.40 -5 0 0 323.17 18.30 5 0 0 380.86 20.50 5 0 0 368.96 20.70 5 0 0 357.06 19.20 5 0 0 373.76 20.40 5 0 0 352.06 18.20 5 0 0 347.67 18.50 5 0 0 372.36 18.50 5 0 0 374.66 17.80 5 0 0 350.46 22.10 5 0 0 319.97 19.20 5 0 0 374.66 20.60 5 0 0 314.37 19.40 -6 0 0 10.10 6.00 -6 0 0 19.00 5.40 -6 0 0 29.50 3.60 -6 0 0 24.60 5.30 6 0 0 25.10 4.90 6 0 0 20.80 3.70 6 0 0 28.70 6.50 6 0 0 27.50 3.20 6 0 0 26.50 4.00 6 0 0 22.90 3.40 6 0 0 25.80 3.00 -7 0 0 5.00 2.40 -7 0 0 -2.40 6.10 -7 0 0 3.30 4.90 -7 0 0 6.40 5.10 7 0 0 2.50 5.90 7 0 0 5.10 2.20 7 0 0 3.60 2.90 7 0 0 0.20 3.90 7 0 0 5.10 3.00 -8 0 0 532.15 32.40 -8 0 0 492.35 31.00 -8 0 0 477.85 35.40 8 0 0 526.85 34.40 8 0 0 501.85 25.90 8 0 0 474.95 27.40 8 0 0 481.45 28.20 8 0 0 501.15 31.00 8 0 0 523.15 26.50 8 0 0 503.75 26.30 -9 0 0 22.80 10.10 -9 0 0 19.30 12.80 -9 0 0 21.90 9.50 9 0 0 13.50 3.60 9 0 0 27.50 9.30 9 0 0 -4.90 10.80 9 0 0 18.60 4.80 9 -1 0 107.59 7.40 9 -1 0 79.29 15.00 9 -1 0 105.09 10.50 9 -1 0 115.19 13.00 -9 1 0 102.99 12.50 -9 1 0 92.09 17.10 -9 1 0 101.69 14.70 8 -1 0 166.28 14.20 8 -1 0 185.08 12.20 8 -1 0 167.78 11.70 8 -1 0 175.08 10.80 8 -1 0 188.88 10.50 8 -1 0 177.38 17.20 8 -1 0 194.38 10.20 -8 1 0 185.78 18.90 -8 1 0 170.38 14.60 -8 1 0 183.48 15.70 7 -1 0 19.20 3.50 7 -1 0 13.20 2.80 7 -1 0 17.00 2.10 7 -1 0 21.10 2.80 7 -1 0 17.90 2.80 7 -1 0 15.70 3.40 7 -1 0 24.10 5.10 7 -1 0 17.30 2.90 7 -1 0 21.00 4.70 7 -1 0 9.00 5.30 -7 1 0 15.80 5.00 -7 1 0 23.90 8.50 -7 1 0 17.10 5.40 6 -1 0 19.90 2.40 6 -1 0 15.60 2.30 6 -1 0 15.10 3.00 6 -1 0 14.70 2.30 6 -1 0 15.50 3.80 6 -1 0 20.60 3.20 6 -1 0 13.30 4.50 6 -1 0 17.60 2.40 6 -1 0 12.60 2.30 6 -1 0 10.30 4.40 6 -1 0 14.90 3.30 6 -1 0 15.20 4.60 -6 1 0 16.30 2.20 -6 1 0 16.50 5.60 -6 1 0 15.00 5.70 -6 1 0 17.00 4.60 -6 1 0 18.90 2.80 5 -1 0 343.57 17.70 5 -1 0 317.47 18.30 5 -1 0 344.97 17.40 5 -1 0 362.36 17.40 5 -1 0 304.27 18.10 5 -1 0 356.86 19.70 5 -1 0 353.36 17.60 5 -1 0 348.67 19.10 5 -1 0 327.57 19.00 5 -1 0 337.57 19.20 5 -1 0 345.57 18.10 5 -1 0 365.96 17.60 5 -1 0 329.67 20.60 -5 1 0 330.27 17.10 -5 1 0 300.37 21.40 -5 1 0 320.17 17.40 -5 1 0 315.77 17.80 -5 1 0 302.27 19.70 -5 1 0 346.87 19.50 -5 1 0 355.06 21.60 -5 1 0 319.47 17.10 4 -1 0 304.17 16.80 4 -1 0 293.17 15.70 4 -1 0 309.97 18.70 4 -1 0 289.27 16.20 4 -1 0 301.67 15.20 4 -1 0 291.17 15.20 4 -1 0 306.67 17.70 4 -1 0 268.67 15.30 4 -1 0 293.97 15.10 4 -1 0 306.77 15.00 4 -1 0 268.77 15.60 4 -1 0 266.37 16.20 4 -1 0 294.97 15.40 4 -1 0 312.47 16.40 -4 1 0 274.87 15.40 -4 1 0 299.47 18.60 -4 1 0 294.07 17.90 -4 1 0 305.17 16.60 -4 1 0 299.17 15.20 -4 1 0 281.17 15.00 -4 1 0 291.67 17.10 -4 1 0 287.77 15.00 3 -1 0 158.78 9.60 3 -1 0 159.38 9.70 3 -1 0 150.28 8.80 3 -1 0 155.48 8.80 3 -1 0 164.08 10.80 3 -1 0 158.88 10.10 3 -1 0 150.58 9.10 3 -1 0 159.68 8.40 3 -1 0 151.68 9.30 3 -1 0 165.48 8.60 3 -1 0 153.28 8.80 3 -1 0 161.18 8.60 3 -1 0 166.78 8.70 3 -1 0 167.18 8.60 -3 1 0 169.48 8.50 -3 1 0 168.88 8.50 -3 1 0 166.48 8.60 -3 1 0 161.98 9.80 -3 1 0 148.69 10.20 -3 1 0 157.48 9.30 -3 1 0 167.58 11.00 1 -1 0 3105.49 150.08 -1 1 0 2919.11 149.88 0 -1 0 1.40 0.50 0 -1 0 2.30 0.70 0 -1 0 2.20 0.70 0 -1 0 1.40 0.50 0 -1 0 1.90 0.60 0 -1 0 1.20 0.60 0 -1 0 1.60 0.40 0 -1 0 1.90 0.60 0 -1 0 1.50 0.60 0 -1 0 2.20 0.70 0 1 0 1.30 0.50 0 1 0 1.10 0.60 0 1 0 0.90 0.50 0 1 0 2.50 0.70 0 1 0 1.20 0.50 0 1 0 1.50 0.70 0 1 0 1.40 0.50 0 1 0 1.80 0.40 0 1 0 2.00 0.70 0 1 0 1.40 0.60 -1 -1 0 787.02 42.00 -1 -1 0 880.51 40.80 -1 -1 0 872.21 41.10 -1 -1 0 937.11 42.60 -1 -1 0 842.82 40.60 -1 -1 0 869.61 41.30 -1 -1 0 793.72 41.40 -1 -1 0 837.32 41.00 -1 -1 0 875.81 41.40 -1 -1 0 873.11 40.30 1 1 0 734.13 41.20 1 1 0 773.62 40.40 1 1 0 755.12 41.20 1 1 0 769.12 41.00 1 1 0 917.61 43.10 1 1 0 791.92 40.90 1 1 0 743.33 40.60 1 1 0 823.82 41.80 1 1 0 786.82 41.30 1 1 0 767.42 41.10 -2 -1 0 278.57 15.60 -2 -1 0 307.07 16.50 -2 -1 0 297.47 15.30 -2 -1 0 296.17 15.60 -2 -1 0 253.17 16.10 -2 -1 0 268.97 17.00 -2 -1 0 309.57 15.30 -2 -1 0 299.07 15.70 -2 -1 0 294.77 14.70 -2 -1 0 286.97 16.10 -2 -1 0 310.87 14.60 -2 -1 0 311.67 15.50 2 1 0 283.37 15.30 2 1 0 322.77 17.60 2 1 0 309.67 16.90 2 1 0 290.97 15.70 2 1 0 292.77 16.60 2 1 0 277.67 15.10 2 1 0 274.87 16.00 2 1 0 259.97 15.60 2 1 0 288.37 15.30 2 1 0 268.57 15.60 2 1 0 287.27 14.30 2 1 0 272.07 15.20 2 1 0 256.97 15.60 -3 -1 0 534.35 27.00 -3 -1 0 548.95 26.40 -3 -1 0 547.15 28.40 -3 -1 0 519.95 27.20 -3 -1 0 532.65 27.40 -3 -1 0 490.15 29.70 -3 -1 0 527.75 27.30 -3 -1 0 517.15 28.70 -3 -1 0 518.15 27.40 3 1 0 519.65 27.40 3 1 0 494.25 29.00 3 1 0 531.35 30.10 3 1 0 436.36 27.40 3 1 0 540.65 26.90 3 1 0 529.75 29.30 3 1 0 514.95 27.30 3 1 0 555.54 27.20 3 1 0 531.85 27.80 3 1 0 521.25 28.30 3 1 0 548.95 27.10 3 1 0 499.35 27.60 -4 -1 0 491.25 28.00 -4 -1 0 580.34 27.30 -4 -1 0 559.84 30.40 -4 -1 0 504.75 29.50 -4 -1 0 541.95 32.10 -4 -1 0 477.25 28.20 -4 -1 0 525.55 28.90 -4 -1 0 521.05 28.50 4 1 0 534.15 28.30 4 1 0 557.74 28.00 4 1 0 532.25 28.60 4 1 0 479.75 28.70 4 1 0 579.64 29.40 4 1 0 551.34 29.80 4 1 0 565.34 28.40 4 1 0 553.54 28.90 4 1 0 526.65 29.60 4 1 0 626.14 29.50 4 1 0 483.85 30.50 -5 -1 0 184.48 12.50 -5 -1 0 165.78 9.90 -5 -1 0 189.88 15.30 -5 -1 0 171.68 9.50 -5 -1 0 180.08 13.30 5 1 0 190.18 10.40 5 1 0 148.59 10.80 5 1 0 164.88 11.30 5 1 0 153.58 11.10 5 1 0 151.48 13.20 5 1 0 166.48 11.80 5 1 0 173.08 10.60 5 1 0 166.48 10.40 -6 -1 0 44.80 3.90 -6 -1 0 46.80 7.70 -6 -1 0 44.80 5.20 -6 -1 0 49.10 9.80 -6 -1 0 48.60 7.80 -6 -1 0 43.10 4.30 6 1 0 43.90 5.40 6 1 0 44.20 5.40 6 1 0 47.80 7.20 6 1 0 34.80 5.20 6 1 0 49.60 4.60 6 1 0 37.80 8.00 6 1 0 41.00 5.00 -7 -1 0 6.30 6.30 -7 -1 0 -2.70 5.10 -7 -1 0 9.40 8.00 -7 -1 0 -1.20 3.60 7 1 0 6.20 5.50 7 1 0 7.60 3.00 7 1 0 2.30 3.20 7 1 0 9.20 6.90 7 1 0 8.50 3.50 7 1 0 3.00 2.50 7 1 0 8.60 4.20 -8 -1 0 61.99 10.80 -8 -1 0 53.09 14.10 -8 -1 0 75.89 12.10 8 1 0 61.19 9.10 8 1 0 71.79 7.80 8 1 0 74.89 9.10 8 1 0 74.49 11.60 8 1 0 73.59 13.20 8 1 0 82.19 6.90 -9 -1 0 117.79 15.10 9 1 0 97.19 8.70 9 1 0 115.59 16.60 10 -2 0 5.30 8.70 10 -2 0 -11.50 12.30 -10 2 0 17.00 14.00 -10 2 0 2.40 10.50 9 -2 0 181.08 10.80 9 -2 0 167.28 12.40 9 -2 0 186.48 19.20 9 -2 0 179.98 11.20 9 -2 0 191.38 15.90 9 -2 0 211.58 13.60 -9 2 0 184.28 16.80 -9 2 0 213.48 21.80 -9 2 0 165.08 21.80 8 -2 0 1.90 2.10 8 -2 0 1.50 2.40 8 -2 0 2.60 5.20 8 -2 0 8.40 6.40 8 -2 0 4.00 2.30 8 -2 0 4.10 2.20 8 -2 0 0.50 2.70 8 -2 0 2.00 2.70 -8 2 0 -3.50 5.00 -8 2 0 6.50 6.30 -8 2 0 -0.50 7.30 -8 2 0 2.30 7.30 7 -2 0 482.65 24.80 7 -2 0 425.46 25.10 7 -2 0 458.15 24.30 7 -2 0 448.06 25.10 7 -2 0 466.25 24.10 7 -2 0 460.55 25.70 7 -2 0 426.56 23.90 7 -2 0 470.45 26.80 7 -2 0 464.95 28.80 7 -2 0 487.45 24.30 -7 2 0 483.55 23.30 -7 2 0 463.05 26.50 -7 2 0 468.25 27.60 -7 2 0 459.35 30.30 -7 2 0 410.26 29.30 6 -2 0 15.10 3.50 6 -2 0 19.50 3.10 6 -2 0 10.70 3.30 6 -2 0 16.10 2.50 6 -2 0 15.50 3.10 6 -2 0 14.30 2.10 6 -2 0 12.70 2.20 6 -2 0 19.30 4.50 6 -2 0 16.20 2.70 6 -2 0 16.90 2.40 -6 2 0 11.80 2.40 -6 2 0 14.50 3.80 -6 2 0 13.10 4.00 -6 2 0 13.10 2.00 -6 2 0 15.90 2.40 -6 2 0 19.80 5.60 -6 2 0 10.80 5.10 5 -2 0 262.97 13.60 5 -2 0 239.08 14.70 5 -2 0 239.18 13.70 5 -2 0 230.78 15.10 5 -2 0 269.37 14.00 5 -2 0 245.68 14.10 5 -2 0 254.17 14.00 5 -2 0 251.67 13.50 5 -2 0 246.88 13.20 5 -2 0 255.57 13.40 5 -2 0 266.37 17.30 5 -2 0 270.67 13.80 5 -2 0 226.48 13.70 -5 2 0 262.07 13.10 -5 2 0 249.28 14.60 -5 2 0 229.08 13.50 -5 2 0 247.48 13.10 -5 2 0 238.68 15.30 -5 2 0 253.47 14.00 -5 2 0 225.88 16.70 -5 2 0 241.58 13.40 -5 2 0 259.87 16.70 4 -2 0 4202.58 227.78 4 -2 0 4674.23 229.58 4 -2 0 4744.23 227.28 4 -2 0 4486.15 226.98 4 -2 0 4901.51 230.48 4 -2 0 4124.29 226.98 4 -2 0 4686.83 226.78 4 -2 0 4528.15 226.88 4 -2 0 4686.13 226.88 4 -2 0 4780.52 228.48 4 -2 0 4575.64 226.98 4 -2 0 4832.72 227.48 -4 2 0 4600.84 227.38 -4 2 0 4691.43 226.68 -4 2 0 4435.46 226.78 -4 2 0 4542.75 227.58 -4 2 0 4916.21 228.28 -4 2 0 4866.41 229.98 -4 2 0 4582.74 229.28 -4 2 0 4551.44 226.98 3 -2 0 126.39 7.50 3 -2 0 124.79 8.40 3 -2 0 112.79 7.10 3 -2 0 122.09 7.90 3 -2 0 126.89 8.40 3 -2 0 130.99 7.50 3 -2 0 124.49 6.60 3 -2 0 121.19 7.30 3 -2 0 117.49 7.10 3 -2 0 129.99 7.00 3 -2 0 122.49 7.20 -3 2 0 127.69 7.50 -3 2 0 127.99 8.80 -3 2 0 117.29 6.50 -3 2 0 129.49 7.10 -3 2 0 120.69 6.40 -3 2 0 129.69 6.90 -3 2 0 125.39 7.30 -3 2 0 121.09 7.50 -3 2 0 132.99 7.40 -3 2 0 134.59 7.10 -3 2 0 129.49 8.50 1 -2 0 593.24 28.20 1 -2 0 594.34 29.40 1 -2 0 513.75 28.70 1 -2 0 547.15 28.50 1 -2 0 536.65 28.80 1 -2 0 561.44 28.90 1 -2 0 539.35 28.50 1 -2 0 538.15 28.70 1 -2 0 538.05 28.40 -1 2 0 535.95 28.80 -1 2 0 560.14 28.80 -1 2 0 535.15 28.50 -1 2 0 565.54 28.60 -1 2 0 566.34 28.80 -1 2 0 630.04 29.10 -1 2 0 582.44 28.50 -1 2 0 601.54 28.80 0 -2 0 273.97 15.00 0 -2 0 254.67 14.80 0 -2 0 275.07 14.50 0 -2 0 276.47 14.50 0 -2 0 271.87 14.40 0 -2 0 258.37 14.50 0 -2 0 266.57 14.00 0 -2 0 286.87 15.00 0 2 0 265.07 14.00 0 2 0 256.07 14.80 0 2 0 289.87 14.50 0 2 0 260.67 14.70 0 2 0 235.78 14.30 0 2 0 264.47 14.50 0 2 0 293.87 15.10 0 2 0 293.17 14.80 0 2 0 267.77 14.40 0 2 0 259.07 14.90 0 2 0 272.37 14.90 -1 -2 0 42.30 3.60 -1 -2 0 43.70 4.10 -1 -2 0 40.60 3.90 -1 -2 0 55.39 3.10 -1 -2 0 47.50 3.90 -1 -2 0 51.69 3.90 -1 -2 0 40.80 3.30 -1 -2 0 43.70 4.50 -1 -2 0 39.90 3.80 -1 -2 0 42.90 4.00 -1 -2 0 46.40 4.50 -1 -2 0 50.89 3.50 1 2 0 44.10 2.90 1 2 0 41.50 3.90 1 2 0 43.80 3.90 1 2 0 41.30 3.50 1 2 0 47.20 2.60 1 2 0 41.40 4.10 1 2 0 45.60 4.40 1 2 0 36.30 3.80 1 2 0 47.60 4.80 1 2 0 42.80 3.70 1 2 0 37.80 3.50 1 2 0 41.50 3.60 -2 -2 0 161.88 11.20 -2 -2 0 176.48 9.90 -2 -2 0 178.28 9.10 -2 -2 0 176.88 11.10 -2 -2 0 185.38 9.70 -2 -2 0 180.28 9.80 -2 -2 0 181.08 11.20 -2 -2 0 176.58 10.90 -2 -2 0 169.18 12.30 -2 -2 0 178.88 11.40 -2 -2 0 188.78 11.90 -2 -2 0 174.58 10.40 2 2 0 183.68 11.10 2 2 0 182.88 10.60 2 2 0 163.68 10.90 2 2 0 188.08 12.10 2 2 0 180.98 10.60 2 2 0 162.78 9.60 2 2 0 178.08 10.50 2 2 0 168.08 11.80 2 2 0 180.58 12.50 2 2 0 189.58 9.30 2 2 0 188.78 11.00 2 2 0 190.68 11.60 2 2 0 166.88 11.00 -3 -2 0 91.89 6.60 -3 -2 0 89.39 8.30 -3 -2 0 94.49 7.40 -3 -2 0 101.29 5.80 -3 -2 0 80.59 11.10 -3 -2 0 93.69 6.70 -3 -2 0 101.39 7.90 -3 -2 0 84.59 7.20 -3 -2 0 104.79 5.60 -3 -2 0 101.89 5.40 3 2 0 84.59 6.60 3 2 0 99.69 7.40 3 2 0 94.49 7.40 3 2 0 85.89 7.60 3 2 0 106.49 8.20 3 2 0 93.59 8.50 3 2 0 87.69 6.90 3 2 0 100.09 7.40 3 2 0 103.79 9.80 3 2 0 62.09 9.00 3 2 0 102.39 6.90 3 2 0 100.59 6.30 3 2 0 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67.99 7.40 -8 4 0 58.89 7.80 -8 4 0 56.29 10.60 7 -4 0 80.99 7.10 7 -4 0 90.79 7.10 7 -4 0 97.89 6.70 7 -4 0 92.19 7.60 7 -4 0 105.09 8.00 7 -4 0 85.69 8.20 7 -4 0 84.49 7.50 -7 4 0 100.59 8.10 -7 4 0 90.49 7.00 -7 4 0 91.59 8.30 -7 4 0 95.59 12.00 -7 4 0 100.29 6.70 -7 4 0 124.89 12.50 6 -4 0 1316.17 70.29 6 -4 0 1298.57 69.69 6 -4 0 1328.07 69.19 6 -4 0 1371.56 69.69 6 -4 0 1457.55 69.79 6 -4 0 1379.86 69.19 6 -4 0 1464.25 68.99 6 -4 0 1335.07 69.29 -6 4 0 1291.97 72.29 -6 4 0 1468.65 72.89 -6 4 0 1348.97 68.29 -6 4 0 1418.96 69.49 -6 4 0 1318.17 69.59 5 -4 0 138.59 8.90 5 -4 0 139.29 9.40 5 -4 0 141.49 9.30 5 -4 0 137.39 8.70 5 -4 0 143.09 9.70 5 -4 0 125.79 8.70 5 -4 0 140.99 9.40 5 -4 0 147.99 9.10 -5 4 0 143.49 11.10 -5 4 0 145.09 11.10 -5 4 0 135.09 8.70 -5 4 0 125.09 9.40 -5 4 0 146.69 8.80 -5 4 0 143.09 8.80 -5 4 0 138.99 8.40 -5 4 0 145.89 9.60 4 -4 0 1454.75 71.69 4 -4 0 1420.06 71.39 4 -4 0 1483.55 72.69 4 -4 0 1497.05 72.29 4 -4 0 1253.17 71.49 4 -4 0 1359.06 71.79 4 -4 0 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571.34 32.40 1 -4 0 605.44 31.80 1 -4 0 619.34 32.60 1 -4 0 609.34 31.10 1 -4 0 621.84 32.40 1 -4 0 603.64 31.70 1 -4 0 551.24 31.30 1 -4 0 579.34 31.60 1 -4 0 623.84 30.10 -1 4 0 558.54 31.60 -1 4 0 560.54 31.70 -1 4 0 588.34 32.30 -1 4 0 656.13 32.60 -1 4 0 605.44 32.60 -1 4 0 631.74 31.90 -1 4 0 580.14 32.10 -1 4 0 568.24 31.10 -1 4 0 601.84 31.80 0 -4 0 58.89 6.60 0 -4 0 82.39 6.60 0 -4 0 74.89 5.20 0 -4 0 76.69 5.80 0 -4 0 74.99 7.00 0 -4 0 69.59 6.00 0 -4 0 89.99 6.40 0 -4 0 67.29 6.00 0 -4 0 76.99 5.70 0 4 0 66.19 5.90 0 4 0 79.99 6.70 0 4 0 77.69 6.60 0 4 0 74.59 6.30 0 4 0 74.29 5.30 0 4 0 71.89 5.80 0 4 0 75.29 6.90 0 4 0 67.29 6.60 0 4 0 74.79 6.80 0 4 0 67.29 6.60 -1 -4 0 0.20 1.70 -1 -4 0 1.70 1.60 -1 -4 0 2.20 1.20 -1 -4 0 0.00 1.90 -1 -4 0 0.90 2.30 -1 -4 0 -0.40 2.10 -1 -4 0 1.50 1.60 -1 -4 0 3.00 2.90 -1 -4 0 1.00 2.90 -1 -4 0 0.10 3.40 -1 -4 0 3.80 2.50 1 4 0 0.90 1.80 1 4 0 1.40 3.00 1 4 0 1.00 1.60 1 4 0 5.40 2.70 1 4 0 2.20 2.10 1 4 0 3.80 2.40 1 4 0 2.40 2.00 1 4 0 1.20 2.70 1 4 0 3.80 3.60 1 4 0 5.60 2.50 -2 -4 0 8.10 2.80 -2 -4 0 6.30 1.80 -2 -4 0 12.80 3.70 -2 -4 0 5.40 2.10 -2 -4 0 9.70 3.30 -2 -4 0 4.90 1.30 -2 -4 0 7.80 3.50 -2 -4 0 9.50 2.90 -2 -4 0 7.40 3.20 2 4 0 7.00 2.50 2 4 0 6.70 2.90 2 4 0 5.60 2.90 2 4 0 8.10 2.00 2 4 0 4.90 2.50 2 4 0 9.60 3.30 2 4 0 4.40 3.70 2 4 0 5.90 3.80 -3 -4 0 231.98 12.80 -3 -4 0 190.18 15.10 -3 -4 0 219.28 17.40 -3 -4 0 216.38 15.50 -3 -4 0 219.88 13.20 -3 -4 0 250.77 14.50 -3 -4 0 224.38 15.00 -3 -4 0 228.98 12.80 3 4 0 196.98 14.90 3 4 0 240.88 16.90 3 4 0 223.68 14.70 3 4 0 224.18 14.60 3 4 0 244.68 15.60 3 4 0 209.38 15.50 3 4 0 204.18 14.80 -4 -4 0 1085.69 61.09 -4 -4 0 1157.08 58.89 -4 -4 0 1163.08 57.19 -4 -4 0 1059.09 63.49 -4 -4 0 1193.88 60.09 -4 -4 0 1068.29 60.89 -4 -4 0 1170.28 56.29 4 4 0 1104.29 59.69 4 4 0 1145.59 60.39 4 4 0 1154.78 59.39 4 4 0 1100.29 60.19 4 4 0 1135.19 60.69 4 4 0 1021.70 62.29 4 4 0 1225.68 60.89 -5 -4 0 27.70 7.40 -5 -4 0 13.30 8.10 -5 -4 0 2.80 5.10 -5 -4 0 3.80 4.80 -5 -4 0 15.00 6.30 -5 -4 0 9.80 2.80 5 4 0 12.20 5.20 5 4 0 3.50 6.50 5 4 0 11.80 5.50 5 4 0 14.60 5.00 5 4 0 14.00 5.00 5 4 0 14.70 5.00 5 4 0 8.00 7.50 -6 -4 0 481.95 31.20 -6 -4 0 454.75 35.10 6 4 0 439.26 29.70 6 4 0 441.66 28.00 6 4 0 504.15 29.10 6 4 0 478.45 28.80 6 4 0 459.35 33.10 7 4 0 134.39 17.80 7 4 0 127.79 13.90 7 4 0 126.19 15.20 7 4 0 130.49 14.30 7 4 0 133.89 19.20 -11 5 0 11.70 11.90 10 -5 0 -3.00 7.80 10 -5 0 3.40 8.90 10 -5 0 1.80 5.50 -10 5 0 6.30 8.20 -10 5 0 8.00 13.30 -10 5 0 -13.40 11.40 9 -5 0 26.40 5.80 9 -5 0 32.20 5.20 9 -5 0 35.20 4.90 9 -5 0 30.00 5.20 9 -5 0 34.40 7.20 9 -5 0 33.80 5.80 -9 5 0 23.50 10.70 -9 5 0 29.00 6.80 -9 5 0 21.10 9.70 8 -5 0 544.65 31.00 8 -5 0 534.05 29.60 8 -5 0 523.05 29.60 8 -5 0 552.94 28.50 8 -5 0 507.95 29.10 8 -5 0 547.75 29.70 8 -5 0 535.95 28.90 -8 5 0 594.04 30.10 -8 5 0 518.05 33.60 -8 5 0 439.36 28.70 -8 5 0 521.65 34.00 7 -5 0 356.56 21.00 7 -5 0 347.57 20.10 7 -5 0 338.87 20.60 7 -5 0 381.56 21.00 7 -5 0 378.36 19.80 7 -5 0 309.47 19.70 7 -5 0 333.37 21.20 -7 5 0 334.37 23.50 -7 5 0 318.87 23.40 -7 5 0 348.87 19.90 -7 5 0 373.46 19.00 6 -5 0 238.48 14.70 6 -5 0 227.68 14.30 6 -5 0 225.78 13.80 6 -5 0 231.98 15.90 6 -5 0 240.28 14.90 6 -5 0 226.68 13.90 -6 5 0 231.98 13.60 -6 5 0 233.68 13.40 -6 5 0 220.48 13.10 -6 5 0 213.18 16.40 -6 5 0 211.48 16.10 -6 5 0 220.48 13.50 5 -5 0 37.10 5.00 5 -5 0 34.60 4.30 5 -5 0 46.00 4.60 5 -5 0 33.10 5.30 5 -5 0 42.80 5.40 5 -5 0 30.30 4.30 -5 5 0 35.10 4.00 -5 5 0 43.70 4.10 -5 5 0 46.10 4.00 -5 5 0 38.90 6.00 -5 5 0 42.00 6.40 -5 5 0 35.30 4.50 -5 5 0 38.30 4.40 4 -5 0 1306.37 68.09 4 -5 0 1198.78 67.29 4 -5 0 1186.58 68.39 4 -5 0 1197.18 67.39 4 -5 0 1347.47 67.19 4 -5 0 1335.27 68.29 4 -5 0 1397.36 67.69 4 -5 0 1437.16 67.59 -4 5 0 1362.66 67.49 -4 5 0 1399.56 66.89 -4 5 0 1354.76 67.99 -4 5 0 1433.86 69.39 -4 5 0 1316.17 66.99 -4 5 0 1221.28 66.89 3 -5 0 65.79 6.70 3 -5 0 79.19 6.70 3 -5 0 73.19 5.70 3 -5 0 70.79 7.10 3 -5 0 68.39 6.10 3 -5 0 66.09 6.20 3 -5 0 71.79 6.50 3 -5 0 77.09 7.30 3 -5 0 76.29 6.10 3 -5 0 69.99 6.00 -3 5 0 77.49 7.00 -3 5 0 77.79 6.50 -3 5 0 65.89 7.30 -3 5 0 75.59 6.50 -3 5 0 80.49 6.50 -3 5 0 74.09 6.50 -3 5 0 70.29 5.90 -3 5 0 68.89 6.00 -3 5 0 71.29 7.20 -3 5 0 82.69 8.00 2 -5 0 48.80 4.70 2 -5 0 52.69 6.70 2 -5 0 55.29 6.10 2 -5 0 60.49 6.40 2 -5 0 54.49 3.30 2 -5 0 55.49 6.90 2 -5 0 39.50 5.50 2 -5 0 54.89 4.20 2 -5 0 59.59 6.90 2 -5 0 53.99 5.50 2 -5 0 47.40 5.00 -2 5 0 48.00 5.20 -2 5 0 52.59 4.80 -2 5 0 51.59 6.30 -2 5 0 54.39 5.50 -2 5 0 49.99 6.40 -2 5 0 50.69 5.00 -2 5 0 59.09 5.60 -2 5 0 56.49 5.30 -2 5 0 52.69 5.80 1 -5 0 3.80 2.70 1 -5 0 3.50 2.00 1 -5 0 6.90 2.90 1 -5 0 4.20 1.60 1 -5 0 4.80 2.60 1 -5 0 5.80 3.40 1 -5 0 3.10 3.30 1 -5 0 4.00 1.60 1 -5 0 3.80 1.00 1 -5 0 4.50 2.10 1 -5 0 0.70 2.90 -1 5 0 4.60 3.20 -1 5 0 3.40 2.00 -1 5 0 5.20 2.40 -1 5 0 4.00 2.30 -1 5 0 1.60 2.30 -1 5 0 5.40 2.90 -1 5 0 9.10 3.40 -1 5 0 5.20 2.80 -1 5 0 3.30 3.10 -1 5 0 3.50 2.30 -1 5 0 3.00 2.40 0 -5 0 205.98 14.20 0 -5 0 187.18 14.40 0 -5 0 199.48 13.60 0 -5 0 218.68 13.70 0 -5 0 236.88 13.90 0 -5 0 220.68 12.90 0 -5 0 204.88 13.00 0 -5 0 210.48 12.30 0 5 0 223.58 13.50 0 5 0 200.98 14.60 0 5 0 199.08 13.60 0 5 0 202.28 14.60 0 5 0 192.28 13.50 0 5 0 220.78 14.80 0 5 0 234.58 14.30 0 5 0 230.18 14.60 0 5 0 198.48 13.90 0 5 0 207.88 13.20 -1 -5 0 459.35 25.70 -1 -5 0 428.66 27.00 -1 -5 0 481.85 24.70 -1 -5 0 463.35 26.50 -1 -5 0 464.65 27.20 -1 -5 0 447.56 26.30 1 5 0 492.95 27.10 1 5 0 474.85 27.90 1 5 0 457.35 26.90 1 5 0 456.45 25.00 1 5 0 445.06 27.20 1 5 0 507.15 26.80 1 5 0 481.75 28.30 1 5 0 518.85 28.00 -2 -5 0 0.60 1.80 -2 -5 0 -0.70 2.00 -2 -5 0 1.00 2.90 -2 -5 0 2.60 3.10 -2 -5 0 1.40 1.50 -2 -5 0 1.40 2.70 -2 -5 0 0.40 3.20 2 5 0 2.00 3.40 2 5 0 -0.60 3.80 2 5 0 -0.10 3.10 2 5 0 2.50 2.20 2 5 0 1.90 3.00 2 5 0 -1.10 3.40 2 5 0 4.90 5.30 -3 -5 0 4.70 3.40 -3 -5 0 7.30 4.30 -3 -5 0 5.80 4.10 -3 -5 0 5.10 3.60 -3 -5 0 3.90 2.00 -3 -5 0 4.10 2.60 3 5 0 7.90 3.60 3 5 0 5.10 5.30 3 5 0 6.40 2.20 3 5 0 5.40 3.60 3 5 0 6.00 3.90 3 5 0 6.80 6.70 3 5 0 8.80 4.40 -4 -5 0 35.50 4.20 -4 -5 0 31.90 7.00 -4 -5 0 21.10 6.40 4 5 0 22.90 5.70 4 5 0 31.90 7.10 4 5 0 33.90 7.00 4 5 0 37.40 7.00 4 5 0 31.10 6.30 4 5 0 28.00 7.70 4 5 0 35.30 8.90 -5 -5 0 139.29 10.40 -5 -5 0 168.28 15.90 5 5 0 171.88 14.40 5 5 0 186.38 17.90 5 5 0 169.68 15.50 5 5 0 183.28 14.80 -6 -5 0 24.10 9.50 6 5 0 25.00 11.70 6 5 0 10.30 8.30 6 5 0 22.20 7.20 7 5 0 6.20 10.90 7 5 0 -4.00 12.80 -11 6 0 4.00 19.70 10 -6 0 193.98 13.70 10 -6 0 197.48 14.60 10 -6 0 205.18 14.70 10 -6 0 203.08 15.80 10 -6 0 224.98 17.90 -10 6 0 222.68 24.70 9 -6 0 0.60 3.80 9 -6 0 2.50 3.90 9 -6 0 3.70 4.70 9 -6 0 2.60 3.90 9 -6 0 0.20 5.40 9 -6 0 1.00 5.20 -9 6 0 2.60 5.30 -9 6 0 2.10 9.60 -9 6 0 2.60 8.10 -9 6 0 -6.00 5.00 8 -6 0 991.20 53.29 8 -6 0 1027.40 51.69 8 -6 0 992.50 52.19 8 -6 0 908.91 53.99 8 -6 0 1037.70 53.99 -8 6 0 1032.10 51.49 -8 6 0 937.81 56.49 7 -6 0 94.89 10.10 7 -6 0 72.39 6.90 7 -6 0 76.19 8.20 7 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42.10 -3 6 0 778.72 42.30 2 -6 0 3.50 3.80 2 -6 0 1.90 2.70 2 -6 0 -2.30 2.10 2 -6 0 1.20 2.00 2 -6 0 -0.60 1.50 2 -6 0 2.30 2.00 -2 6 0 -2.20 2.40 -2 6 0 3.10 2.70 -2 6 0 -0.20 2.20 -2 6 0 2.00 2.60 -2 6 0 -2.90 3.10 -2 6 0 0.90 2.80 1 -6 0 695.53 35.90 1 -6 0 631.64 34.90 1 -6 0 663.63 37.10 1 -6 0 663.83 37.70 1 -6 0 674.83 36.40 1 -6 0 700.23 34.50 -1 6 0 707.93 37.70 -1 6 0 649.54 37.30 -1 6 0 624.04 36.60 -1 6 0 552.74 36.40 -1 6 0 665.73 37.00 -1 6 0 666.03 36.60 -1 6 0 696.03 36.60 0 -6 0 184.38 11.80 0 -6 0 169.38 11.90 0 -6 0 159.78 13.00 0 -6 0 157.68 10.80 0 -6 0 176.98 12.60 0 6 0 180.08 13.30 0 6 0 183.18 13.30 0 6 0 215.78 13.10 0 6 0 167.98 12.70 0 6 0 166.28 13.20 0 6 0 201.08 14.40 -1 -6 0 500.55 27.10 -1 -6 0 462.55 27.60 -1 -6 0 454.25 25.70 -1 -6 0 491.35 28.20 -1 -6 0 476.25 29.00 1 6 0 474.65 28.00 1 6 0 463.85 28.30 1 6 0 466.85 26.30 1 6 0 534.65 30.60 1 6 0 545.15 29.80 1 6 0 493.85 28.60 1 6 0 485.65 29.10 -2 -6 0 98.69 6.90 -2 -6 0 112.59 11.20 -2 -6 0 101.79 7.70 -2 -6 0 98.99 8.30 -2 -6 0 107.29 9.90 -2 -6 0 109.59 10.10 2 6 0 95.59 10.20 2 6 0 128.29 11.00 2 6 0 121.89 11.60 2 6 0 106.29 9.90 2 6 0 95.39 11.00 2 6 0 122.29 10.90 -3 -6 0 16.20 5.80 -3 -6 0 3.90 5.10 -3 -6 0 11.80 3.50 -3 -6 0 10.50 3.30 3 6 0 19.00 6.20 3 6 0 6.80 4.50 3 6 0 17.50 6.80 3 6 0 13.90 3.30 3 6 0 12.10 5.70 3 6 0 16.80 5.70 3 6 0 16.50 7.30 -4 -6 0 89.29 7.50 -4 -6 0 80.49 11.70 4 6 0 75.49 10.50 4 6 0 80.59 11.10 4 6 0 83.19 10.70 4 6 0 84.09 14.00 4 6 0 78.79 10.70 -5 -6 0 12.50 10.30 -5 -6 0 -2.60 3.70 5 6 0 0.20 9.80 5 6 0 8.30 7.90 5 6 0 5.70 6.70 5 6 0 5.60 7.30 5 6 0 4.70 8.10 6 6 0 -5.00 13.40 6 6 0 11.00 10.70 10 -7 0 189.28 15.80 10 -7 0 206.48 15.20 10 -7 0 217.68 15.40 10 -7 0 224.48 17.00 9 -7 0 37.30 6.00 9 -7 0 25.30 5.50 9 -7 0 21.10 5.70 9 -7 0 25.40 7.50 9 -7 0 25.80 5.70 -9 7 0 23.10 12.70 -9 7 0 30.40 10.60 8 -7 0 105.59 9.70 8 -7 0 107.29 11.20 8 -7 0 88.29 8.40 8 -7 0 103.39 9.50 8 -7 0 94.39 8.90 -8 7 0 94.99 13.20 -8 7 0 94.79 12.70 7 -7 0 6.00 5.40 7 -7 0 14.20 3.90 7 -7 0 8.40 7.20 7 -7 0 13.20 3.70 7 -7 0 11.20 3.70 7 -7 0 10.80 3.50 -7 7 0 14.20 6.10 -7 7 0 2.40 3.50 -7 7 0 5.90 5.90 -7 7 0 4.70 3.90 -7 7 0 2.30 3.70 6 -7 0 4.30 3.10 6 -7 0 8.00 3.30 6 -7 0 7.00 3.50 6 -7 0 11.20 5.70 6 -7 0 8.40 3.40 -6 7 0 11.30 5.10 -6 7 0 11.80 3.40 -6 7 0 6.20 3.40 -6 7 0 9.20 3.80 -6 7 0 14.80 5.10 -6 7 0 10.60 4.70 -6 7 0 11.70 3.20 5 -7 0 9.20 3.30 5 -7 0 13.70 4.00 5 -7 0 6.90 5.50 5 -7 0 12.10 6.70 5 -7 0 15.20 4.20 5 -7 0 2.50 3.10 -5 7 0 21.60 5.90 -5 7 0 10.60 4.30 -5 7 0 9.10 3.80 -5 7 0 18.60 4.10 -5 7 0 14.60 4.10 -5 7 0 10.30 4.80 4 -7 0 276.57 17.30 4 -7 0 228.08 15.80 4 -7 0 275.37 16.40 4 -7 0 221.78 18.00 4 -7 0 245.68 16.40 4 -7 0 240.78 15.40 -4 7 0 265.87 18.40 -4 7 0 273.67 16.60 -4 7 0 257.57 13.80 -4 7 0 230.98 16.50 -4 7 0 231.98 16.90 -4 7 0 257.87 14.20 -4 7 0 282.57 16.20 3 -7 0 13.40 3.50 3 -7 0 13.80 3.70 3 -7 0 14.20 4.40 3 -7 0 20.20 10.10 3 -7 0 28.50 5.20 3 -7 0 22.30 3.50 -3 7 0 16.10 4.00 -3 7 0 17.80 4.10 -3 7 0 15.20 4.40 -3 7 0 20.30 4.70 -3 7 0 14.40 4.30 2 -7 0 124.39 9.30 2 -7 0 94.59 9.20 2 -7 0 118.29 6.60 2 -7 0 108.99 10.20 2 -7 0 97.69 8.40 -2 7 0 100.99 10.80 -2 7 0 110.99 10.60 -2 7 0 98.79 10.10 -2 7 0 97.09 9.80 -2 7 0 94.99 9.30 1 -7 0 78.39 6.70 1 -7 0 75.09 7.30 1 -7 0 58.99 8.90 1 -7 0 83.09 8.80 1 -7 0 79.39 6.40 -1 7 0 82.19 9.90 -1 7 0 72.49 9.00 -1 7 0 68.99 9.50 -1 7 0 78.19 8.90 0 -7 0 532.05 30.80 0 -7 0 544.65 29.80 0 -7 0 534.65 28.50 0 -7 0 552.24 29.50 0 -7 0 542.35 31.80 0 7 0 508.05 30.90 0 7 0 570.84 32.00 0 7 0 497.35 31.50 0 7 0 505.25 31.40 0 7 0 476.55 31.70 0 7 0 514.05 30.20 -1 -7 0 390.26 22.90 -1 -7 0 391.56 23.60 -1 -7 0 352.56 21.70 -1 -7 0 389.56 20.60 -1 -7 0 380.66 24.40 1 7 0 381.46 24.50 1 7 0 362.46 25.30 1 7 0 336.37 25.40 1 7 0 349.47 22.70 1 7 0 357.36 24.00 1 7 0 346.37 24.10 -2 -7 0 -1.90 3.70 -2 -7 0 1.70 5.20 -2 -7 0 -1.00 2.30 -2 -7 0 2.40 3.30 -2 -7 0 -0.80 6.00 -2 -7 0 1.60 5.40 2 7 0 -4.70 4.40 2 7 0 2.70 5.20 2 7 0 1.30 5.00 2 7 0 1.60 6.10 2 7 0 -3.30 4.70 -3 -7 0 129.09 9.90 -3 -7 0 119.79 10.50 -3 -7 0 112.29 13.30 3 7 0 139.59 13.50 3 7 0 128.59 14.20 3 7 0 131.79 14.10 3 7 0 101.89 12.90 3 7 0 143.79 17.70 -4 -7 0 22.80 8.50 -4 -7 0 24.10 5.10 4 7 0 34.30 8.90 4 7 0 36.70 11.80 4 7 0 39.70 8.70 4 7 0 23.80 7.90 4 7 0 25.70 9.30 10 -8 0 98.39 10.90 10 -8 0 136.89 13.30 10 -8 0 127.29 12.40 9 -8 0 55.39 8.20 9 -8 0 79.59 9.10 9 -8 0 64.79 9.20 9 -8 0 68.79 10.70 9 -8 0 73.99 8.60 -9 8 0 69.39 13.80 8 -8 0 172.78 13.60 8 -8 0 167.98 13.70 8 -8 0 173.48 12.70 8 -8 0 178.68 13.60 -8 8 0 166.28 17.30 7 -8 0 118.99 10.40 7 -8 0 95.89 10.10 7 -8 0 75.69 9.80 7 -8 0 112.09 9.50 -7 8 0 128.49 14.30 -7 8 0 124.69 12.70 -7 8 0 120.99 9.60 6 -8 0 9.40 4.10 6 -8 0 14.90 4.80 6 -8 0 10.00 4.20 6 -8 0 23.50 8.30 -6 8 0 9.80 5.00 -6 8 0 13.70 5.20 -6 8 0 7.70 5.30 -6 8 0 11.90 4.30 5 -8 0 36.50 5.50 5 -8 0 24.30 8.10 5 -8 0 33.80 5.70 5 -8 0 43.60 6.90 5 -8 0 32.90 5.70 -5 8 0 25.90 5.40 -5 8 0 36.10 6.70 -5 8 0 27.10 7.20 -5 8 0 23.30 5.70 -5 8 0 36.50 6.40 4 -8 0 712.03 39.40 4 -8 0 659.03 38.40 4 -8 0 672.13 38.60 4 -8 0 630.14 39.50 4 -8 0 733.93 42.10 4 -8 0 694.23 37.20 -4 8 0 639.14 39.80 -4 8 0 699.53 41.40 -4 8 0 750.92 36.40 -4 8 0 734.43 39.50 -4 8 0 703.33 39.70 -4 8 0 733.83 36.90 -4 8 0 717.83 38.90 3 -8 0 0.60 3.10 3 -8 0 1.90 3.00 3 -8 0 -0.70 3.60 3 -8 0 0.70 3.50 3 -8 0 1.40 2.90 -3 8 0 -0.50 3.30 -3 8 0 2.30 4.90 -3 8 0 0.30 3.70 -3 8 0 0.70 4.10 2 -8 0 2.60 4.10 2 -8 0 0.40 1.90 2 -8 0 1.20 3.80 2 -8 0 0.10 2.80 2 -8 0 1.60 3.70 -2 8 0 -0.50 3.10 -2 8 0 0.70 3.80 -2 8 0 -2.40 4.10 -2 8 0 -1.40 3.60 1 -8 0 274.17 16.80 1 -8 0 254.17 19.00 1 -8 0 283.87 19.10 1 -8 0 270.97 19.70 1 -8 0 286.17 16.30 -1 8 0 266.07 18.80 -1 8 0 272.47 19.60 -1 8 0 248.58 19.30 0 -8 0 43.50 5.90 0 -8 0 46.60 6.90 0 -8 0 51.99 8.60 0 -8 0 59.89 9.70 0 -8 0 48.10 6.80 0 8 0 45.80 8.50 0 8 0 49.90 9.10 0 8 0 60.09 10.30 0 8 0 62.99 9.50 -1 -8 0 42.90 5.40 -1 -8 0 28.00 6.40 -1 -8 0 60.19 10.20 -1 -8 0 34.80 6.30 1 8 0 52.69 9.50 1 8 0 39.40 8.10 1 8 0 46.20 8.20 1 8 0 35.40 8.10 1 8 0 41.20 9.70 -2 -8 0 129.09 12.30 -2 -8 0 108.29 10.60 -2 -8 0 116.59 9.40 -2 -8 0 118.59 14.80 2 8 0 94.19 14.90 2 8 0 111.79 13.80 2 8 0 100.29 13.10 2 8 0 103.69 12.40 2 8 0 110.19 13.80 -3 -8 0 -2.00 7.20 -3 -8 0 -0.60 4.70 -3 -8 0 -3.10 10.10 3 8 0 6.10 7.10 3 8 0 5.10 8.00 3 8 0 -3.30 7.30 3 8 0 -1.30 7.30 3 8 0 2.10 10.50 -4 -8 0 1.70 6.40 4 8 0 21.40 11.10 10 -9 0 34.70 8.20 9 -9 0 19.80 6.70 9 -9 0 16.80 8.10 9 -9 0 19.20 6.40 8 -9 0 1.90 5.00 8 -9 0 9.20 5.90 8 -9 0 6.20 5.60 8 -9 0 9.30 6.10 -8 9 0 4.00 6.30 -8 9 0 0.10 9.90 -8 9 0 -4.40 9.10 7 -9 0 4.00 4.80 7 -9 0 -7.80 4.40 7 -9 0 -4.00 4.30 7 -9 0 -5.90 4.30 -7 9 0 3.50 5.00 -7 9 0 -4.00 5.80 -7 9 0 -4.40 5.20 -7 9 0 5.50 7.40 -7 9 0 3.80 7.20 6 -9 0 130.69 11.10 6 -9 0 114.59 10.20 6 -9 0 128.29 11.70 6 -9 0 99.29 11.20 -6 9 0 107.39 10.90 -6 9 0 84.79 13.30 -6 9 0 117.19 12.30 5 -9 0 37.20 7.30 5 -9 0 36.50 6.80 5 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3 -4 86.89 6.90 2 3 -4 95.19 7.40 2 3 -4 88.69 7.60 2 3 -4 87.99 7.80 2 3 -4 83.09 7.60 2 3 -4 64.59 6.80 -2 -3 4 76.69 7.10 -2 -3 4 94.89 5.70 -2 -3 4 77.79 8.50 -2 -3 4 78.89 7.10 -2 -3 4 94.99 7.20 -2 -3 4 87.19 7.00 -2 -3 4 93.99 7.10 -2 -3 4 85.89 8.40 -2 -3 4 104.49 8.20 -2 -3 4 87.69 7.60 -2 -3 4 80.39 7.10 -2 -3 4 95.29 8.10 1 3 -4 23.40 3.60 1 3 -4 27.10 4.10 1 3 -4 23.30 3.80 1 3 -4 19.50 3.20 1 3 -4 21.00 3.60 1 3 -4 23.50 4.30 1 3 -4 25.80 3.70 1 3 -4 25.30 4.30 1 3 -4 28.00 4.00 1 3 -4 24.60 3.90 1 3 -4 23.60 3.50 -1 -3 4 25.40 4.10 -1 -3 4 19.00 3.80 -1 -3 4 20.90 3.40 -1 -3 4 19.70 3.20 -1 -3 4 19.70 3.30 -1 -3 4 23.10 3.60 -1 -3 4 21.50 3.70 -1 -3 4 23.70 2.80 -1 -3 4 23.20 3.70 -1 -3 4 23.10 3.20 -1 -3 4 21.70 4.20 -1 -3 4 19.20 3.80 0 3 -4 281.57 16.00 0 3 -4 285.97 16.30 0 3 -4 288.17 16.00 0 3 -4 275.77 16.60 0 3 -4 299.97 17.00 0 3 -4 271.77 15.80 0 3 -4 304.57 16.00 0 3 -4 278.47 15.90 0 3 -4 284.77 15.70 0 3 -4 268.37 16.70 0 3 -4 291.67 15.20 0 3 -4 316.57 15.30 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147.39 13.70 7 2 -4 149.29 14.20 7 2 -4 147.19 17.60 7 2 -4 148.79 12.70 -7 -2 4 159.58 19.40 -7 -2 4 169.08 15.40 -7 -2 4 131.09 15.00 6 2 -4 148.89 11.60 6 2 -4 143.79 13.00 6 2 -4 158.58 12.70 6 2 -4 174.58 15.50 6 2 -4 163.38 13.70 6 2 -4 176.78 11.50 6 2 -4 144.69 13.30 -6 -2 4 144.29 13.60 -6 -2 4 153.78 9.10 -6 -2 4 159.08 12.00 -6 -2 4 165.18 13.10 -6 -2 4 164.88 9.60 -6 -2 4 140.49 15.60 -6 -2 4 159.58 13.90 5 2 -4 308.67 17.20 5 2 -4 277.57 17.90 5 2 -4 257.27 18.60 5 2 -4 245.48 18.20 5 2 -4 289.87 20.10 5 2 -4 283.07 16.80 5 2 -4 267.47 17.20 5 2 -4 259.07 18.70 -5 -2 4 307.67 16.50 -5 -2 4 293.87 18.80 -5 -2 4 271.67 20.90 -5 -2 4 253.57 18.70 -5 -2 4 284.87 17.40 -5 -2 4 313.77 15.60 4 2 -4 10.40 2.90 4 2 -4 7.50 3.10 4 2 -4 12.20 3.10 4 2 -4 10.00 3.60 4 2 -4 7.50 3.90 4 2 -4 8.40 3.50 4 2 -4 5.40 3.20 -4 -2 4 7.30 2.20 -4 -2 4 4.50 4.10 -4 -2 4 7.10 3.70 -4 -2 4 8.20 2.60 -4 -2 4 2.90 3.20 -4 -2 4 8.50 2.80 3 2 -4 34.30 5.30 3 2 -4 35.20 4.50 3 2 -4 38.00 5.20 3 2 -4 41.30 5.60 3 2 -4 52.09 6.40 3 2 -4 46.00 5.60 3 2 -4 46.40 5.30 3 2 -4 45.70 6.90 3 2 -4 42.40 5.30 3 2 -4 59.89 7.20 3 2 -4 45.30 6.00 3 2 -4 46.60 4.90 -3 -2 4 45.20 5.90 -3 -2 4 44.90 5.70 -3 -2 4 38.70 4.60 -3 -2 4 37.70 2.80 -3 -2 4 54.39 6.20 -3 -2 4 39.00 3.60 -3 -2 4 42.30 5.00 -3 -2 4 38.80 5.50 -3 -2 4 39.20 6.20 -3 -2 4 35.30 5.20 -3 -2 4 40.60 2.60 -3 -2 4 34.20 4.50 2 2 -4 383.46 20.90 2 2 -4 397.06 21.40 2 2 -4 373.56 21.60 2 2 -4 386.26 20.80 2 2 -4 377.76 21.60 2 2 -4 402.36 20.80 2 2 -4 353.26 20.20 2 2 -4 332.17 20.70 2 2 -4 369.06 21.00 2 2 -4 378.16 21.40 2 2 -4 328.37 20.20 2 2 -4 390.66 21.10 -2 -2 4 377.46 21.60 -2 -2 4 379.46 20.60 -2 -2 4 402.36 20.90 -2 -2 4 369.06 21.30 -2 -2 4 339.17 20.70 -2 -2 4 363.36 20.80 -2 -2 4 412.46 21.80 -2 -2 4 374.96 20.60 -2 -2 4 372.66 21.20 -2 -2 4 327.97 20.80 -2 -2 4 371.66 18.90 -2 -2 4 371.56 19.90 1 2 -4 24.90 3.10 1 2 -4 33.60 3.80 1 2 -4 27.40 3.60 1 2 -4 31.70 3.50 1 2 -4 24.70 3.20 1 2 -4 35.00 3.80 1 2 -4 32.80 4.30 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243.78 14.40 7 -5 7 231.78 16.20 -8 5 -7 0.50 13.10 8 -5 7 6.30 5.80 8 -5 7 -6.70 10.20 8 -5 7 15.20 7.70 9 -5 7 30.30 9.50 7 4 -7 -0.90 10.00 7 4 -7 5.40 10.30 7 4 -7 7.60 9.60 7 4 -7 1.90 6.80 7 4 -7 -7.50 9.80 -7 -4 7 -2.70 11.40 -7 -4 7 7.80 9.50 -7 -4 7 10.70 9.50 -7 -4 7 2.20 5.70 -7 -4 7 -2.10 8.70 6 4 -7 4.40 7.30 6 4 -7 5.10 5.10 6 4 -7 4.80 6.80 6 4 -7 8.20 6.90 6 4 -7 6.20 7.40 -6 -4 7 5.30 6.80 -6 -4 7 2.40 8.10 -6 -4 7 6.90 7.10 -6 -4 7 3.10 5.20 -6 -4 7 6.00 7.60 5 4 -7 3.80 5.40 5 4 -7 -0.60 5.10 5 4 -7 3.70 5.30 5 4 -7 0.40 5.70 5 4 -7 -0.60 4.20 -5 -4 7 3.40 5.70 -5 -4 7 1.10 4.60 -5 -4 7 3.60 5.70 -5 -4 7 5.40 6.60 -5 -4 7 -1.70 4.30 4 4 -7 175.98 15.40 4 4 -7 185.78 15.70 4 4 -7 200.48 16.00 4 4 -7 176.18 14.80 4 4 -7 160.08 13.50 4 4 -7 174.48 13.90 -4 -4 7 182.48 15.90 -4 -4 7 190.98 10.30 -4 -4 7 172.58 13.40 -4 -4 7 192.18 10.10 -4 -4 7 186.98 15.20 -4 -4 7 179.78 13.90 -4 -4 7 186.98 10.80 -4 -4 7 202.28 15.90 3 4 -7 313.57 19.80 3 4 -7 268.17 20.30 3 4 -7 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2471.85 128.19 -4 -3 7 2595.14 129.39 -4 -3 7 2685.83 123.79 -4 -3 7 2462.55 127.79 3 3 -7 68.99 7.70 3 3 -7 68.99 9.20 3 3 -7 82.69 9.60 3 3 -7 75.19 7.90 3 3 -7 76.19 7.30 3 3 -7 73.29 9.50 3 3 -7 77.49 7.00 3 3 -7 61.89 8.10 -3 -3 7 79.39 4.80 -3 -3 7 75.19 7.50 -3 -3 7 79.99 5.80 -3 -3 7 72.59 8.20 -3 -3 7 79.99 8.40 -3 -3 7 53.59 7.80 -3 -3 7 79.09 7.90 -3 -3 7 87.29 8.80 2 3 -7 432.36 28.20 2 3 -7 482.35 27.20 2 3 -7 510.65 27.50 2 3 -7 492.85 26.90 2 3 -7 474.45 28.60 2 3 -7 540.95 27.50 2 3 -7 430.26 27.20 -2 -3 7 438.96 27.90 -2 -3 7 431.26 27.90 -2 -3 7 556.14 28.00 -2 -3 7 499.15 29.50 -2 -3 7 513.15 27.80 -2 -3 7 498.15 27.30 -2 -3 7 455.35 27.50 -2 -3 7 507.55 24.90 -2 -3 7 458.35 27.30 1 3 -7 630.04 35.50 1 3 -7 632.94 33.60 1 3 -7 629.74 35.50 1 3 -7 685.63 36.00 1 3 -7 618.64 34.50 1 3 -7 646.54 33.60 1 3 -7 586.54 34.20 1 3 -7 656.03 33.90 1 3 -7 586.74 34.90 1 3 -7 640.64 34.00 -1 -3 7 638.64 34.40 -1 -3 7 580.34 34.30 -1 -3 7 630.14 32.40 -1 -3 7 704.93 35.80 -1 -3 7 590.24 34.10 -1 -3 7 680.53 35.30 -1 -3 7 690.23 34.50 -1 -3 7 547.75 35.20 -1 -3 7 651.73 34.10 -1 -3 7 656.13 35.40 0 3 -7 412.26 21.80 0 3 -7 413.56 22.00 0 3 -7 402.86 20.90 0 3 -7 412.46 22.00 0 3 -7 402.06 22.60 0 3 -7 354.76 22.10 0 3 -7 371.46 23.10 0 3 -7 408.36 21.50 0 3 -7 398.86 21.80 0 3 -7 371.16 21.80 0 3 -7 379.36 23.30 0 -3 7 381.06 23.30 0 -3 7 441.86 23.30 0 -3 7 391.66 23.20 0 -3 7 357.86 21.70 0 -3 7 415.76 22.10 0 -3 7 388.86 22.30 0 -3 7 392.26 22.60 0 -3 7 399.86 22.50 0 -3 7 430.06 21.50 0 -3 7 419.06 21.20 -1 3 -7 5.70 2.30 -1 3 -7 4.80 2.60 -1 3 -7 4.80 1.90 -1 3 -7 4.30 2.20 -1 3 -7 3.00 1.90 -1 3 -7 3.10 2.40 -1 3 -7 5.30 2.00 1 -3 7 2.50 1.40 1 -3 7 5.30 1.10 1 -3 7 5.40 2.00 1 -3 7 4.70 2.70 1 -3 7 3.10 2.60 1 -3 7 3.10 2.20 1 -3 7 4.10 1.90 1 -3 7 3.30 2.70 1 -3 7 6.20 2.30 1 -3 7 4.30 2.60 -2 3 -7 6.20 2.50 -2 3 -7 3.20 1.60 -2 3 -7 5.90 2.20 -2 3 -7 5.20 2.10 -2 3 -7 6.40 2.50 -2 3 -7 4.10 2.10 -2 3 -7 4.90 2.60 2 -3 7 3.60 2.00 2 -3 7 6.10 1.20 2 -3 7 7.10 2.60 2 -3 7 3.40 2.20 2 -3 7 6.00 2.40 2 -3 7 3.30 2.70 2 -3 7 5.20 1.40 2 -3 7 5.40 2.00 2 -3 7 4.00 1.70 2 -3 7 4.90 2.40 -3 3 -7 4.70 2.20 -3 3 -7 10.20 3.00 -3 3 -7 8.80 1.90 -3 3 -7 6.60 2.80 -3 3 -7 6.20 3.20 -3 3 -7 8.50 2.80 3 -3 7 10.20 3.60 3 -3 7 6.90 2.60 3 -3 7 10.60 2.50 3 -3 7 13.60 4.00 3 -3 7 11.80 2.20 3 -3 7 8.40 2.20 3 -3 7 5.00 1.80 3 -3 7 9.30 2.60 3 -3 7 9.50 3.20 3 -3 7 7.40 2.40 3 -3 7 6.40 2.60 3 -3 7 9.20 2.60 -4 3 -7 106.79 8.20 -4 3 -7 110.29 9.40 -4 3 -7 113.29 10.10 4 -3 7 105.39 6.20 4 -3 7 99.39 9.00 4 -3 7 121.69 10.60 4 -3 7 122.79 7.40 4 -3 7 107.49 7.30 4 -3 7 110.09 8.10 4 -3 7 105.69 6.50 4 -3 7 92.99 7.40 4 -3 7 107.69 8.80 4 -3 7 104.79 6.60 4 -3 7 103.99 6.00 -5 3 -7 45.30 8.10 -5 3 -7 41.00 7.10 5 -3 7 41.50 6.10 5 -3 7 54.79 5.90 5 -3 7 41.70 4.00 5 -3 7 37.40 4.80 5 -3 7 38.10 5.90 5 -3 7 36.60 4.00 -6 3 -7 23.10 6.40 -6 3 -7 31.30 8.80 6 -3 7 33.50 5.10 6 -3 7 24.00 4.70 6 -3 7 27.30 3.20 6 -3 7 29.90 6.60 6 -3 7 29.10 6.30 -7 3 -7 170.58 19.60 -7 3 -7 188.98 16.70 7 -3 7 196.98 13.50 7 -3 7 195.78 16.30 7 -3 7 185.18 14.10 8 -3 7 8.50 10.50 8 -3 7 8.90 7.40 8 -3 7 19.70 7.20 9 2 -7 214.18 19.90 8 2 -7 15.40 7.90 8 2 -7 18.10 8.70 8 2 -7 22.50 10.30 8 2 -7 14.60 7.30 8 2 -7 19.80 8.30 -8 -2 7 21.90 9.30 -8 -2 7 27.90 10.30 -8 -2 7 24.20 11.70 -8 -2 7 0.70 9.80 7 2 -7 139.09 14.90 7 2 -7 134.89 12.30 7 2 -7 136.49 15.50 7 2 -7 134.29 16.20 7 2 -7 139.99 14.20 -7 -2 7 125.89 14.90 -7 -2 7 138.19 11.00 -7 -2 7 142.69 15.20 -7 -2 7 143.29 18.60 6 2 -7 241.28 22.70 6 2 -7 321.27 19.40 6 2 -7 350.96 22.40 6 2 -7 270.87 21.70 6 2 -7 318.57 22.90 6 2 -7 295.77 19.90 -6 -2 7 311.77 20.40 -6 -2 7 344.57 22.10 -6 -2 7 330.67 24.50 -6 -2 7 326.97 19.60 5 2 -7 1823.52 93.49 5 2 -7 1756.02 91.09 5 2 -7 1665.73 92.89 5 2 -7 1806.92 92.59 5 2 -7 1637.04 92.89 5 2 -7 1855.61 90.49 -5 -2 7 1856.51 91.39 -5 -2 7 1761.12 92.79 -5 -2 7 1791.12 94.79 -5 -2 7 1823.62 88.09 -5 -2 7 1636.14 91.89 -5 -2 7 1798.52 87.79 -5 -2 7 1838.52 91.09 -5 -2 7 1755.72 92.79 4 2 -7 2003.00 100.69 4 2 -7 2055.09 101.39 4 2 -7 2147.19 102.09 4 2 -7 1799.62 99.89 4 2 -7 1936.11 100.19 4 2 -7 2062.09 102.39 4 2 -7 2067.69 102.49 4 2 -7 1999.90 99.59 -4 -2 7 1946.81 97.49 -4 -2 7 2005.60 102.89 -4 -2 7 1920.01 103.69 -4 -2 7 1945.01 100.39 -4 -2 7 1926.41 96.59 -4 -2 7 1959.80 101.39 -4 -2 7 1800.82 100.69 -4 -2 7 1980.20 100.29 3 2 -7 191.78 14.60 3 2 -7 200.98 14.00 3 2 -7 223.08 14.20 3 2 -7 223.98 13.20 3 2 -7 211.58 13.40 3 2 -7 178.08 14.40 3 2 -7 197.98 13.10 3 2 -7 212.38 14.00 -3 -2 7 196.58 14.10 -3 -2 7 223.68 11.10 -3 -2 7 198.88 14.30 -3 -2 7 197.98 14.60 -3 -2 7 209.78 11.70 -3 -2 7 209.48 13.90 -3 -2 7 224.58 14.20 -3 -2 7 214.88 13.60 -3 -2 7 237.68 15.50 2 2 -7 48.60 6.60 2 2 -7 30.30 5.40 2 2 -7 46.30 4.60 2 2 -7 46.90 5.30 2 2 -7 36.80 5.00 2 2 -7 44.10 5.40 2 2 -7 44.20 4.30 2 2 -7 37.80 4.90 2 2 -7 33.30 4.50 2 2 -7 32.90 4.90 -2 -2 7 31.60 4.70 -2 -2 7 38.00 5.60 -2 -2 7 36.30 5.50 -2 -2 7 22.90 5.00 -2 -2 7 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357.16 21.20 2 -3 9 414.46 21.90 2 -3 9 368.36 21.40 2 -3 9 377.56 19.50 2 -3 9 386.56 21.30 2 -3 9 380.16 20.70 2 -3 9 335.77 20.60 2 -3 9 371.46 21.30 -3 3 -9 104.29 7.60 -3 3 -9 97.39 7.20 -3 3 -9 87.09 7.90 -3 3 -9 91.09 8.80 -3 3 -9 103.89 9.20 3 -3 9 103.99 7.50 3 -3 9 108.99 9.10 3 -3 9 97.39 7.70 3 -3 9 82.99 8.50 3 -3 9 103.79 8.30 3 -3 9 109.29 8.00 3 -3 9 89.09 7.10 3 -3 9 94.49 7.70 3 -3 9 98.59 9.80 3 -3 9 106.19 7.20 -4 3 -9 1121.29 65.89 -4 3 -9 1164.78 66.29 -4 3 -9 1269.57 66.29 4 -3 9 1261.97 62.19 4 -3 9 1225.68 66.39 4 -3 9 1248.98 63.79 4 -3 9 1309.87 65.89 4 -3 9 1244.28 61.99 4 -3 9 1321.57 64.79 4 -3 9 1282.07 61.99 4 -3 9 1277.77 63.69 4 -3 9 1237.18 62.69 -5 3 -9 100.69 12.20 -5 3 -9 101.29 11.70 5 -3 9 101.59 8.90 5 -3 9 104.49 8.30 5 -3 9 85.99 8.40 5 -3 9 112.29 8.00 5 -3 9 100.59 11.80 -6 3 -9 388.26 27.30 6 -3 9 440.36 26.30 6 -3 9 419.56 24.10 6 -3 9 425.56 24.80 7 -3 9 18.80 7.90 7 -3 9 34.80 10.60 7 -3 9 23.70 6.70 8 2 -9 50.29 14.00 8 2 -9 59.49 10.30 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3 -8 10 154.28 13.90 -4 8 -10 -2.80 7.20 -4 8 -10 4.40 6.60 4 -8 10 0.40 5.90 4 -8 10 1.10 6.30 4 -8 10 5.80 5.00 4 -8 10 3.40 6.10 4 -8 10 0.50 5.60 -5 8 -10 94.19 13.30 5 -8 10 114.19 13.10 5 -8 10 107.09 13.10 5 -8 10 118.89 11.90 5 -8 10 117.99 11.10 -6 8 -10 100.59 15.70 6 -8 10 104.79 12.30 6 -8 10 87.89 9.80 6 -8 10 99.19 10.40 5 7 -10 3.70 13.00 5 7 -10 -8.00 12.20 -5 -7 10 -11.00 12.80 -5 -7 10 -0.80 8.40 4 7 -10 46.40 11.60 4 7 -10 32.20 9.80 4 7 -10 51.49 13.70 4 7 -10 47.80 13.20 4 7 -10 33.70 12.50 -4 -7 10 59.39 12.30 -4 -7 10 -2.10 9.60 -4 -7 10 43.50 12.50 -4 -7 10 47.80 12.20 3 7 -10 154.98 15.00 3 7 -10 118.09 16.40 3 7 -10 158.78 16.30 3 7 -10 182.28 18.50 3 7 -10 117.79 16.50 -3 -7 10 159.78 16.40 -3 -7 10 155.88 18.70 -3 -7 10 135.19 14.20 -3 -7 10 156.58 16.10 -3 -7 10 138.19 16.00 2 7 -10 361.16 26.00 2 7 -10 383.76 29.20 2 7 -10 412.46 28.90 2 7 -10 373.66 26.50 2 7 -10 425.36 21.90 2 7 -10 406.86 26.60 -2 -7 10 403.56 26.30 -2 -7 10 358.76 25.70 -2 -7 10 328.47 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214.68 20.40 -6 6 -10 203.98 18.70 6 -6 10 230.98 18.20 6 -6 10 218.08 12.70 6 -6 10 217.78 13.10 6 -6 10 230.38 16.70 -7 6 -10 13.70 14.10 7 -6 10 1.70 8.40 7 -6 10 -2.30 7.00 -8 6 -10 272.97 30.50 -7 -5 10 70.79 11.90 -7 -5 10 8.70 15.40 6 5 -10 11.90 10.50 6 5 -10 16.60 10.90 6 5 -10 13.40 8.00 6 5 -10 19.90 10.80 6 5 -10 31.60 10.30 -6 -5 10 13.60 10.00 -6 -5 10 16.70 11.00 -6 -5 10 18.90 8.50 -6 -5 10 24.20 11.20 5 5 -10 -2.60 8.10 5 5 -10 -2.00 7.00 5 5 -10 -0.10 7.30 5 5 -10 -4.60 7.60 5 5 -10 0.60 6.00 -5 -5 10 4.60 7.00 -5 -5 10 2.00 3.70 -5 -5 10 4.90 6.90 -5 -5 10 2.20 7.50 -5 -5 10 -7.40 7.80 -5 -5 10 3.00 8.10 4 5 -10 5.20 5.20 4 5 -10 -4.30 5.80 4 5 -10 8.90 6.90 4 5 -10 0.60 7.30 4 5 -10 4.30 6.60 -4 -5 10 4.40 6.00 -4 -5 10 -2.20 5.90 -4 -5 10 4.30 5.90 -4 -5 10 2.30 6.60 -4 -5 10 2.00 3.40 -4 -5 10 2.80 7.10 -4 -5 10 5.10 6.10 3 5 -10 43.10 7.80 3 5 -10 47.80 8.50 3 5 -10 35.90 7.90 3 5 -10 39.70 9.20 -3 -5 10 59.19 8.90 -3 -5 10 59.59 9.60 -3 -5 10 43.00 8.30 -3 -5 10 50.79 8.70 -3 -5 10 60.49 6.80 -3 -5 10 47.50 10.60 2 5 -10 116.89 12.10 2 5 -10 123.39 12.90 2 5 -10 118.99 13.00 2 5 -10 126.89 11.60 2 5 -10 127.09 11.10 2 5 -10 112.49 10.90 -2 -5 10 117.19 9.50 -2 -5 10 118.29 12.10 -2 -5 10 127.89 11.70 -2 -5 10 114.49 11.20 -2 -5 10 107.99 11.00 -2 -5 10 107.39 13.30 1 5 -10 21.60 6.80 1 5 -10 14.30 5.20 1 5 -10 12.40 4.10 1 5 -10 21.00 6.40 1 5 -10 17.40 3.80 1 5 -10 7.80 4.30 -1 -5 10 19.10 5.40 -1 -5 10 14.20 5.60 -1 -5 10 15.50 5.40 -1 -5 10 14.40 4.80 -1 -5 10 19.10 4.50 -1 -5 10 11.80 4.30 -1 -5 10 17.30 4.60 -1 -5 10 6.20 7.30 0 5 -10 181.18 13.20 0 5 -10 181.68 14.90 0 5 -10 176.18 11.50 0 5 -10 177.68 14.90 0 5 -10 194.68 11.20 0 5 -10 167.28 12.00 0 5 -10 156.68 12.30 0 -5 10 180.18 14.50 0 -5 10 170.98 13.90 0 -5 10 162.48 13.30 0 -5 10 171.38 13.30 0 -5 10 181.88 15.30 0 -5 10 172.28 12.70 0 -5 10 155.68 12.30 -1 5 -10 261.47 15.20 -1 5 -10 232.58 17.40 -1 5 -10 239.88 17.30 -1 5 -10 247.08 15.20 -1 5 -10 237.48 14.30 -1 5 -10 247.28 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22.10 6 -5 10 330.07 21.70 6 -5 10 386.36 25.10 -7 5 -10 228.18 24.40 7 -5 10 199.38 17.50 7 -5 10 212.88 16.10 7 4 -10 7.20 9.20 7 4 -10 18.90 9.70 7 4 -10 6.90 10.80 7 4 -10 -0.60 10.30 7 4 -10 -1.40 9.20 -7 -4 10 -9.40 10.80 -7 -4 10 11.40 9.60 -7 -4 10 10.10 7.90 6 4 -10 48.70 11.80 6 4 -10 39.00 10.30 6 4 -10 45.00 10.20 6 4 -10 20.00 8.00 6 4 -10 59.99 11.90 -6 -4 10 66.29 12.50 -6 -4 10 36.30 10.30 -6 -4 10 50.39 11.70 -6 -4 10 40.60 8.50 5 4 -10 -0.40 7.20 5 4 -10 8.70 8.00 5 4 -10 21.80 6.30 5 4 -10 23.00 7.70 5 4 -10 11.40 7.00 -5 -4 10 14.70 8.00 -5 -4 10 2.60 6.20 -5 -4 10 22.00 7.40 -5 -4 10 19.80 7.20 -5 -4 10 22.70 7.60 4 4 -10 0.80 5.10 4 4 -10 4.50 4.40 4 4 -10 20.20 7.70 4 4 -10 1.60 4.90 4 4 -10 0.30 5.90 -4 -4 10 -1.30 5.20 -4 -4 10 7.10 2.30 -4 -4 10 5.20 3.30 -4 -4 10 6.20 4.90 -4 -4 10 3.90 4.90 -4 -4 10 7.70 6.10 -4 -4 10 1.10 4.60 -4 -4 10 3.80 6.40 3 4 -10 212.68 16.80 3 4 -10 245.48 16.60 3 4 -10 209.88 16.20 3 4 -10 214.78 16.40 3 4 -10 252.47 19.00 3 4 -10 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3 -11 -2.40 3.30 -2 -3 11 1.90 5.40 -2 -3 11 4.20 3.40 -2 -3 11 0.40 4.10 -2 -3 11 5.50 4.90 -2 -3 11 1.20 3.30 -2 -3 11 0.50 3.50 -2 -3 11 0.10 3.50 1 3 -11 0.50 5.00 1 3 -11 3.90 4.70 1 3 -11 0.00 3.10 1 3 -11 3.40 3.00 -1 -3 11 2.40 3.00 -1 -3 11 6.40 3.90 -1 -3 11 -0.30 3.50 -1 -3 11 1.50 3.80 -1 -3 11 1.30 3.50 -1 -3 11 2.00 4.70 -1 -3 11 3.70 3.50 0 3 -11 166.78 11.30 0 3 -11 165.88 11.00 0 3 -11 161.88 13.20 0 3 -11 154.68 11.40 0 3 -11 180.28 14.40 0 3 -11 155.58 11.90 0 3 -11 164.78 13.20 0 -3 11 145.49 11.70 0 -3 11 165.68 12.50 0 -3 11 168.98 11.90 0 -3 11 194.48 13.50 0 -3 11 164.68 13.40 0 -3 11 164.28 11.70 0 -3 11 174.88 12.80 0 -3 11 157.18 12.30 -1 3 -11 123.19 9.90 -1 3 -11 125.29 11.60 -1 3 -11 129.99 11.00 -1 3 -11 153.78 8.50 -1 3 -11 129.19 11.90 -1 3 -11 122.19 9.60 1 -3 11 133.79 11.20 1 -3 11 148.49 11.30 1 -3 11 138.49 11.30 1 -3 11 151.58 11.40 1 -3 11 144.79 11.00 1 -3 11 159.28 11.40 1 -3 11 146.69 10.00 1 -3 11 156.78 10.80 1 -3 11 143.99 11.40 -2 3 -11 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150.08 18.70 6 4 -14 128.49 18.70 6 4 -14 166.38 19.00 -6 -4 14 141.09 19.90 -6 -4 14 163.68 18.40 -6 -4 14 131.79 18.40 5 4 -14 24.20 9.30 5 4 -14 1.00 9.40 5 4 -14 10.20 11.60 5 4 -14 3.90 10.10 5 4 -14 16.60 8.80 -5 -4 14 8.40 9.90 -5 -4 14 -3.10 8.60 -5 -4 14 1.80 7.90 -5 -4 14 5.10 9.20 -5 -4 14 9.30 6.30 -5 -4 14 9.60 11.30 4 4 -14 134.89 15.00 4 4 -14 118.49 17.50 4 4 -14 142.69 13.90 4 4 -14 70.99 12.00 4 4 -14 142.59 17.60 -4 -4 14 124.89 12.50 -4 -4 14 132.79 15.10 -4 -4 14 112.69 14.60 -4 -4 14 101.39 13.80 -4 -4 14 137.49 16.00 -4 -4 14 118.79 15.90 -4 -4 14 109.19 15.50 3 4 -14 141.99 13.90 3 4 -14 116.99 17.20 3 4 -14 127.99 14.50 3 4 -14 153.18 18.30 -3 -4 14 119.09 16.20 -3 -4 14 127.69 14.00 -3 -4 14 135.99 14.50 -3 -4 14 151.88 16.50 -3 -4 14 143.59 12.30 -3 -4 14 163.58 14.70 -3 -4 14 148.49 15.00 2 4 -14 246.98 17.10 2 4 -14 223.88 20.50 2 4 -14 243.88 17.60 2 4 -14 255.67 19.80 -2 -4 14 243.98 18.80 -2 -4 14 233.18 20.60 -2 -4 14 250.37 19.20 -2 -4 14 234.48 18.10 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18.50 12.30 -6 -3 14 -0.10 8.70 -6 -3 14 15.40 11.20 -6 -3 14 0.40 6.10 -6 -3 14 10.60 9.50 5 3 -14 55.79 14.50 5 3 -14 67.69 11.10 5 3 -14 62.19 13.20 5 3 -14 71.99 11.40 5 3 -14 51.89 9.50 -5 -3 14 68.49 12.90 -5 -3 14 90.99 13.40 -5 -3 14 60.19 12.70 -5 -3 14 66.19 11.30 -5 -3 14 52.49 12.70 -5 -3 14 76.89 17.30 4 3 -14 193.38 17.40 4 3 -14 219.08 21.30 4 3 -14 242.58 17.00 4 3 -14 193.48 19.90 4 3 -14 204.88 17.60 -4 -3 14 219.58 18.30 -4 -3 14 218.38 19.80 -4 -3 14 239.58 18.30 -4 -3 14 201.68 18.00 -4 -3 14 217.48 20.00 -4 -3 14 212.88 18.30 3 3 -14 47.00 8.60 3 3 -14 59.19 9.40 3 3 -14 78.09 12.70 3 3 -14 66.99 12.20 -3 -3 14 92.29 11.70 -3 -3 14 76.79 11.10 -3 -3 14 63.29 11.10 -3 -3 14 49.99 10.00 -3 -3 14 71.99 10.50 -3 -3 14 63.69 10.00 2 3 -14 142.29 12.40 2 3 -14 117.79 14.70 2 3 -14 127.69 12.20 -2 -3 14 156.18 13.40 -2 -3 14 124.19 12.20 -2 -3 14 134.89 13.60 -2 -3 14 122.19 13.80 -2 -3 14 114.69 13.40 -2 -3 14 141.79 13.40 1 3 -14 120.99 10.90 1 3 -14 106.79 10.40 1 3 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1.90 11.20 3 0 -17 8.20 10.50 3 0 -17 -7.30 7.00 3 0 -17 3.90 4.90 -3 0 17 10.40 7.80 -3 0 17 9.10 8.60 -3 0 17 12.70 8.80 -3 0 17 3.90 9.50 -3 0 17 2.90 11.20 2 0 -17 2.20 4.50 2 0 -17 -1.50 11.50 2 0 -17 3.40 7.20 2 0 -17 -1.40 10.60 -2 0 17 0.40 8.00 -2 0 17 9.50 6.20 -2 0 17 -13.00 7.50 -2 0 17 5.20 7.10 1 0 -17 52.99 7.80 -1 0 17 48.10 9.90 -1 0 17 58.29 11.30 -1 0 17 65.39 9.40 -1 0 17 53.29 11.90 -1 0 17 50.89 10.70 0 0 17 68.89 11.90 1 0 17 62.79 12.30 8 -1 -17 347.07 31.00 7 -1 -17 48.60 14.00 7 -1 -17 49.10 18.90 7 -1 -17 7.00 12.20 -7 1 17 56.69 13.50 6 -1 -17 5.10 10.10 6 -1 -17 33.10 10.10 6 -1 -17 -26.30 13.80 6 -1 -17 35.70 13.00 -6 1 17 36.50 10.80 -6 1 17 32.20 15.40 -6 1 17 38.20 9.90 -6 1 17 24.40 13.00 5 -1 -17 -12.30 15.90 5 -1 -17 16.80 5.50 5 -1 -17 0.70 8.70 5 -1 -17 6.70 11.60 -5 1 17 10.80 8.30 -5 1 17 12.40 9.40 -5 1 17 15.50 9.70 -5 1 17 15.10 8.50 -5 1 17 29.40 13.80 -5 1 17 12.40 9.10 4 -1 -17 17.20 5.70 4 -1 -17 11.90 11.80 4 -1 -17 0.60 7.50 -4 1 17 18.20 8.00 -4 1 17 25.80 10.70 -4 1 17 13.20 8.60 -4 1 17 23.10 13.50 3 -1 -17 142.29 11.60 -3 1 17 173.68 18.30 -3 1 17 155.68 15.60 -3 1 17 150.88 15.80 -3 1 17 126.49 13.60 -3 1 17 134.49 15.60 2 -1 -17 14.10 6.10 2 -1 -17 5.30 12.40 -2 1 17 23.10 9.00 -2 1 17 17.80 9.00 -2 1 17 10.20 6.70 -2 1 17 12.10 7.80 -2 1 17 8.00 8.00 1 -1 -17 108.69 11.30 -1 1 17 77.99 12.60 -1 1 17 100.39 13.40 -1 1 17 92.09 13.60 0 1 17 10.00 9.80 0 1 17 28.80 10.40 1 1 17 -11.00 11.20 8 -2 -17 126.89 23.20 8 -2 -17 119.29 20.40 7 -2 -17 2.40 12.30 7 -2 -17 -1.60 16.00 7 -2 -17 15.90 13.00 -7 2 17 18.90 11.00 6 -2 -17 -6.60 11.30 6 -2 -17 3.40 5.10 6 -2 -17 -13.70 8.40 6 -2 -17 2.50 14.90 -6 2 17 -3.60 8.90 -6 2 17 6.30 10.50 5 -2 -17 36.80 13.00 5 -2 -17 13.80 5.90 5 -2 -17 22.50 8.40 -5 2 17 22.10 8.70 -5 2 17 23.80 12.60 -5 2 17 9.30 9.00 -5 2 17 21.40 9.70 -5 2 17 20.00 11.30 4 -2 -17 12.00 5.50 4 -2 -17 11.80 8.00 4 -2 -17 12.10 11.80 -4 2 17 12.50 8.30 -4 2 17 11.60 8.80 -4 2 17 16.90 7.70 -4 2 17 5.70 8.60 -4 2 17 5.30 9.30 3 -2 -17 29.70 6.00 3 -2 -17 -6.20 11.50 3 -2 -17 22.10 8.60 -3 2 17 33.80 9.60 -3 2 17 26.60 10.80 -3 2 17 21.60 9.20 -3 2 17 2.50 8.20 -3 2 17 19.10 6.80 2 -2 -17 51.19 7.60 -2 2 17 23.40 10.60 -2 2 17 51.29 10.70 -1 2 17 32.50 11.00 -1 2 17 17.80 10.70 0 2 17 8.80 10.70 8 -3 -17 -8.00 20.30 7 -3 -17 -1.70 16.60 -7 3 17 38.40 11.90 6 -3 -17 3.80 13.20 6 -3 -17 3.80 5.20 -6 3 17 8.50 8.80 5 -3 -17 4.80 10.80 5 -3 -17 -10.00 8.20 -5 3 17 6.50 8.00 4 -3 -17 -7.60 8.10 4 -3 -17 -4.10 5.50 4 -3 -17 -9.40 10.40 -4 3 17 -3.00 9.20 -4 3 17 -9.50 6.80 3 -3 -17 -7.60 15.00 3 -3 -17 -4.80 8.50 3 -3 -17 6.10 6.60 -3 3 17 11.30 9.50 -2 3 17 -4.00 10.20 -7 4 17 3.20 10.80 6 -4 -17 10.80 15.70 6 -4 -17 4.60 6.20 -6 4 17 17.70 9.90 5 -4 -17 103.99 18.00 5 -4 -17 142.29 11.70 4 -4 -17 -10.40 13.90 5 -5 -17 17.10 15.30 3 5 -18 12.10 17.50 -3 -5 18 18.70 15.80 2 5 -18 1.50 12.50 2 5 -18 14.40 12.20 4 4 -18 17.30 18.10 4 4 -18 26.50 13.80 3 4 -18 97.69 14.70 3 4 -18 107.59 16.10 3 4 -18 88.99 22.20 -3 -4 18 93.99 16.60 5 3 -18 110.69 16.90 -5 -3 18 76.89 20.80 4 3 -18 128.89 16.70 4 3 -18 89.19 29.50 -4 -3 18 118.99 18.10 -4 -3 18 113.49 16.60 3 3 -18 60.49 17.20 3 3 -18 103.39 13.80 3 3 -18 9.50 9.90 -3 -3 18 62.09 22.40 2 3 -18 11.30 15.70 -1 -3 18 50.69 14.60 -1 -3 18 33.80 11.50 0 -3 18 55.69 13.70 1 -3 18 -0.30 17.30 -6 -2 18 157.28 20.80 5 2 -18 164.18 24.70 5 2 -18 176.48 21.00 -5 -2 18 183.58 23.50 -5 -2 18 204.48 20.40 4 2 -18 140.49 20.00 4 2 -18 104.49 14.80 -4 -2 18 108.39 18.50 -4 -2 18 89.69 15.00 3 2 -18 2.80 9.60 3 2 -18 -7.50 13.00 -3 -2 18 -3.90 8.10 -3 -2 18 1.70 11.50 -3 -2 18 -18.00 12.70 2 2 -18 47.90 8.80 -2 -2 18 67.89 12.40 -2 -2 18 44.30 14.10 -2 -2 18 46.90 12.10 1 2 -18 31.70 7.60 -1 -2 18 16.70 13.20 -1 -2 18 22.00 10.40 -1 -2 18 6.60 10.40 0 -2 18 13.80 11.00 1 -2 18 1.20 11.90 6 1 -18 2.50 12.90 -6 -1 18 3.40 12.10 5 1 -18 109.29 15.40 5 1 -18 74.69 17.60 -5 -1 18 47.70 15.90 -5 -1 18 68.29 12.90 4 1 -18 51.89 8.30 4 1 -18 55.39 16.70 -4 -1 18 34.60 14.80 -4 -1 18 60.49 12.40 -4 -1 18 42.40 11.30 3 1 -18 51.99 11.10 3 1 -18 50.89 7.50 3 1 -18 5.30 14.90 -3 -1 18 46.60 10.20 -3 -1 18 57.99 19.10 -3 -1 18 67.29 14.90 2 1 -18 8.40 6.00 -2 -1 18 6.50 10.30 -2 -1 18 14.30 12.60 -2 -1 18 11.80 10.60 -1 -1 18 19.40 11.40 -1 -1 18 23.50 11.10 0 -1 18 -0.90 9.60 7 0 -18 113.99 21.80 -7 0 18 144.09 19.60 -6 0 18 169.48 18.90 5 0 -18 40.20 7.30 5 0 -18 33.30 10.30 -5 0 18 25.00 16.40 -5 0 18 43.50 11.50 4 0 -18 17.70 14.00 4 0 -18 16.90 9.60 4 0 -18 14.80 5.80 -4 0 18 26.10 16.10 -4 0 18 21.40 11.70 -4 0 18 15.40 8.40 3 0 -18 5.80 6.90 3 0 -18 0.60 12.70 3 0 -18 7.80 9.30 -3 0 18 20.70 20.50 -3 0 18 16.80 10.50 -3 0 18 12.20 8.50 2 0 -18 4.30 5.70 -2 0 18 -1.60 10.80 -2 0 18 23.10 11.90 -1 0 18 214.68 19.50 -1 0 18 160.58 20.30 -7 1 18 52.19 14.90 6 -1 -18 7.40 15.50 -6 1 18 5.20 9.90 5 -1 -18 11.20 6.10 5 -1 -18 16.70 9.90 -5 1 18 9.30 9.00 -5 1 18 55.49 17.40 4 -1 -18 -6.70 8.90 4 -1 -18 15.90 12.90 -4 1 18 5.60 9.60 -4 1 18 5.90 14.00 -4 1 18 25.50 11.70 3 -1 -18 -4.20 9.60 3 -1 -18 4.90 6.30 3 -1 -18 -4.00 16.60 -3 1 18 -10.00 9.10 -1 1 18 93.49 14.60 -7 2 18 -1.50 21.50 -6 2 18 -6.70 16.00 5 -2 -18 3.90 6.30 5 -2 -18 5.50 13.60 5 -2 -18 10.20 9.50 4 -2 -18 106.09 15.30 4 -2 -18 11.40 15.80 6 -3 -18 16.10 7.30 5 -3 -18 -7.30 14.30 5 -3 -18 2.50 11.90 3 4 -19 -7.30 16.00 4 3 -19 -3.60 18.60 3 3 -19 -11.40 12.60 -3 -3 19 -19.00 13.40 -2 -3 19 54.19 19.40 4 2 -19 -1.00 19.40 4 2 -19 8.70 12.80 -4 -2 19 -9.30 17.30 3 2 -19 -5.70 12.30 -3 -2 19 17.40 13.00 -2 -2 19 -7.90 12.50 4 1 -19 -3.40 7.40 4 1 -19 -0.60 12.10 -4 -1 19 -30.80 15.70 3 1 -19 7.70 6.50 -3 -1 19 2.80 15.30 -3 -1 19 -4.00 12.20 -2 -1 19 8.30 17.30 -2 -1 19 2.50 11.70 5 0 -19 -12.00 18.90 4 0 -19 114.99 16.20 4 0 -19 96.09 11.10 -3 0 19 75.49 18.80 -2 0 19 17.70 12.40 5 -1 -19 47.20 9.10 5 -1 -19 54.09 19.50 4 -1 -19 35.50 13.00 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 54431 _shelx_res_file ; TITL mo_PSD_863_0m_a.res in P-1 mo_psd_863_0m-auto.res created by SHELXL-2018/3 at 17:18:43 on 01-Dec-2023 CELL 0.71073 7.1661 7.6864 12.1723 95.473 105.226 113.116 ZERR 2 0.0021 0.0029 0.0038 0.016 0.012 0.013 LATT 1 SFAC C H N O UNIT 28 16 8 4 EADP N1A C1B EADP C17 N17A EXYZ C17 N17A EXYZ N1A C1B L.S. 40 PLAN -3 0 0 SIZE 0.05 0.06 0.12 TEMP -173.15 HTAB BOND $H CONF fmap 2 acta OMIT -10 9 3 OMIT -5 10 8 OMIT -2 -1 2 OMIT 1 0 4 REM REM REM WGHT 0.066000 0.151400 FVAR 1.78607 O1 4 0.678284 -0.039782 0.355374 11.00000 0.01953 0.01487 = 0.01970 0.00356 0.00424 0.00786 O2 4 0.336152 0.297638 0.154228 11.00000 0.02342 0.01382 = 0.02203 0.00386 0.00547 0.00954 N4 3 1.051309 0.879348 0.275159 11.00000 0.03279 0.01783 = 0.03425 0.00740 0.02049 0.00586 N2 3 0.810712 0.569522 0.285042 11.00000 0.01662 0.01211 = 0.01420 0.00307 0.00586 0.00397 N3 3 0.938519 0.735750 0.286886 11.00000 0.01844 0.01527 = 0.01780 0.00371 0.00835 0.00721 C10 1 0.776357 0.533962 0.392459 11.00000 0.01135 0.01198 = 0.01220 0.00227 0.00359 0.00569 C9 1 0.647471 0.340854 0.392176 11.00000 0.01117 0.01158 = 0.01285 0.00225 0.00327 0.00526 C8 1 0.549887 0.186211 0.286502 11.00000 0.01240 0.00992 = 0.01445 0.00236 0.00479 0.00426 PART 1 N1A 3 0.406872 0.176809 0.179879 10.50000 0.01961 0.01028 = 0.02306 0.00145 0.01209 0.00375 PART 0 C14 1 0.340331 -0.009260 0.099613 11.00000 0.01622 0.01097 = 0.01828 0.00310 0.00881 0.00531 C2 1 0.203649 -0.086218 -0.013791 11.00000 0.01704 0.02614 = 0.01939 0.01159 0.00783 0.01181 AFIX 43 H2 2 0.134768 -0.017372 -0.055149 11.00000 -1.20000 AFIX 0 C3 1 0.171215 -0.271576 -0.065219 11.00000 0.01719 0.02695 = 0.01291 0.00121 0.00333 0.00517 AFIX 43 H3 2 0.077902 -0.330058 -0.143374 11.00000 -1.20000 AFIX 0 C11 1 0.867717 0.678704 0.494277 11.00000 0.01337 0.01203 = 0.01452 0.00044 0.00284 0.00533 AFIX 43 H11 2 0.955317 0.808707 0.493893 11.00000 -1.20000 AFIX 0 C12 1 0.830188 0.632130 0.596242 11.00000 0.01647 0.01782 = 0.01305 0.00077 0.00280 0.00959 AFIX 43 H12 2 0.891796 0.730900 0.665580 11.00000 -1.20000 AFIX 0 C13 1 0.702705 0.441415 0.597739 11.00000 0.01745 0.02016 = 0.01302 0.00438 0.00564 0.01041 AFIX 43 H13 2 0.677285 0.410403 0.667753 11.00000 -1.20000 AFIX 0 C15 1 0.612994 0.296879 0.496196 11.00000 0.01478 0.01523 = 0.01530 0.00497 0.00574 0.00741 AFIX 43 H15 2 0.527337 0.166823 0.497471 11.00000 -1.20000 AFIX 0 PART 1 C17 1 0.570401 0.011705 0.278110 10.50000 0.01354 0.01385 = 0.01553 -0.00054 0.00584 0.00152 PART 0 C6 1 0.440153 -0.110006 0.160228 11.00000 0.01339 0.01166 = 0.01281 0.00098 0.00456 0.00289 C5 1 0.410712 -0.291587 0.111542 11.00000 0.01875 0.01316 = 0.01909 0.00564 0.00773 0.00779 AFIX 43 H5 2 0.479954 -0.359268 0.153933 11.00000 -1.20000 AFIX 0 C4 1 0.272628 -0.371395 -0.004301 11.00000 0.02230 0.01326 = 0.01978 -0.00144 0.00874 0.00409 AFIX 43 H4 2 0.247984 -0.496292 -0.041850 11.00000 -1.20000 AFIX 0 PART 2 C1B 1 0.406872 0.176809 0.179879 10.50000 0.01961 0.01028 = 0.02306 0.00145 0.01209 0.00375 N17A 3 0.570401 0.011705 0.278110 10.50000 0.01354 0.01385 = 0.01553 -0.00054 0.00584 0.00152 HKLF 4 REM mo_PSD_863_0m_a.res in P-1 REM wR2 = 0.1220, GooF = S = 1.053, Restrained GooF = 1.053 for all data REM R1 = 0.0422 for 3946 Fo > 4sig(Fo) and 0.0568 for all 4818 data REM 181 parameters refined using 0 restraints END WGHT 0.0660 0.1514 REM Instructions for potential hydrogen bonds EQIV $1 -x+2, -y+1, -z+1 HTAB C11 O1_$1 EQIV $2 x, y-1, z HTAB C5 O2_$2 REM Highest difference peak 0.464, deepest hole -0.287, 1-sigma level 0.066 Q1 1 0.3632 0.0750 0.1377 11.00000 0.05 0.46 Q2 1 0.3852 -0.0663 0.1271 11.00000 0.05 0.46 Q3 1 0.8257 0.6159 0.4397 11.00000 0.05 0.45 ; _shelx_res_checksum 81828 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O O1 0.67828(11) -0.03978(9) 0.35537(6) 0.01840(14) Uani d 1 . . O O2 0.33615(11) 0.29764(9) 0.15423(6) 0.01970(14) Uani d 1 . . N N4 1.05131(16) 0.87935(13) 0.27516(9) 0.02787(19) Uani d 1 . . N N2 0.81071(12) 0.56952(10) 0.28504(6) 0.01489(14) Uani d 1 . . N N3 0.93852(12) 0.73575(11) 0.28689(7) 0.01669(14) Uani d 1 . . C C10 0.77636(12) 0.53396(11) 0.39246(7) 0.01172(14) Uani d 1 . . C C9 0.64747(12) 0.34085(11) 0.39218(7) 0.01194(14) Uani d 1 . . C C8 0.54989(12) 0.18621(11) 0.28650(7) 0.01240(14) Uani d 1 . . N N1A 0.40687(13) 0.17681(11) 0.17988(8) 0.01765(16) Uani d 0.5 A 1 C C14 0.34033(13) -0.00926(12) 0.09961(7) 0.01469(15) Uani d 1 . . C C2 0.20365(14) -0.08622(14) -0.01379(8) 0.01915(17) Uani d 1 . . H H2 0.134768 -0.017372 -0.055149 0.023 Uiso calc 1 . . C C3 0.17122(15) -0.27158(15) -0.06522(8) 0.02109(18) Uani d 1 . . H H3 0.077902 -0.330058 -0.143374 0.025 Uiso calc 1 . . C C11 0.86772(13) 0.67870(12) 0.49428(7) 0.01393(15) Uani d 1 . . H H11 0.955317 0.808707 0.493893 0.017 Uiso calc 1 . . C C12 0.83019(14) 0.63213(13) 0.59624(7) 0.01570(15) Uani d 1 . . H H12 0.891796 0.730900 0.665580 0.019 Uiso calc 1 . . C C13 0.70271(14) 0.44142(13) 0.59774(7) 0.01594(15) Uani d 1 . . H H13 0.677285 0.410403 0.667753 0.019 Uiso calc 1 . . C C15 0.61299(13) 0.29688(12) 0.49620(7) 0.01451(15) Uani d 1 . . H H15 0.527337 0.166823 0.497471 0.017 Uiso calc 1 . . C C17 0.57040(12) 0.01171(11) 0.27811(7) 0.01585(15) Uani d 0.5 A 1 C C6 0.44015(13) -0.11001(12) 0.16023(7) 0.01356(14) Uani d 1 . . C C5 0.41071(14) -0.29159(12) 0.11154(8) 0.01623(15) Uani d 1 . . H H5 0.479954 -0.359268 0.153933 0.019 Uiso calc 1 . . C C4 0.27263(15) -0.37139(13) -0.00430(8) 0.01966(17) Uani d 1 . . H H4 0.247984 -0.496292 -0.041850 0.024 Uiso calc 1 . . C C1B 0.40687(13) 0.17681(11) 0.17988(8) 0.01765(16) Uani d 0.5 A 2 N N17A 0.57040(12) 0.01171(11) 0.27811(7) 0.01585(15) Uani d 0.5 A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.0195(3) 0.0149(3) 0.0197(3) 0.0079(2) 0.0042(2) 0.0036(2) O2 0.0234(3) 0.0138(3) 0.0220(3) 0.0095(2) 0.0055(2) 0.0039(2) N4 0.0328(5) 0.0178(4) 0.0343(5) 0.0059(3) 0.0205(4) 0.0074(3) N2 0.0166(3) 0.0121(3) 0.0142(3) 0.0040(2) 0.0059(2) 0.0031(2) N3 0.0184(3) 0.0153(3) 0.0178(3) 0.0072(3) 0.0084(3) 0.0037(2) C10 0.0113(3) 0.0120(3) 0.0122(3) 0.0057(2) 0.0036(2) 0.0023(2) C9 0.0112(3) 0.0116(3) 0.0128(3) 0.0053(3) 0.0033(2) 0.0023(2) C8 0.0124(3) 0.0099(3) 0.0145(3) 0.0043(2) 0.0048(3) 0.0024(2) N1A 0.0196(4) 0.0103(3) 0.0231(4) 0.0038(3) 0.0121(3) 0.0015(3) C14 0.0162(3) 0.0110(3) 0.0183(4) 0.0053(3) 0.0088(3) 0.0031(3) C2 0.0170(4) 0.0261(4) 0.0194(4) 0.0118(3) 0.0078(3) 0.0116(3) C3 0.0172(4) 0.0269(4) 0.0129(3) 0.0052(3) 0.0033(3) 0.0012(3) C11 0.0134(3) 0.0120(3) 0.0145(3) 0.0053(3) 0.0028(3) 0.0004(3) C12 0.0165(3) 0.0178(4) 0.0130(3) 0.0096(3) 0.0028(3) 0.0008(3) C13 0.0175(4) 0.0202(4) 0.0130(3) 0.0104(3) 0.0056(3) 0.0044(3) C15 0.0148(3) 0.0152(3) 0.0153(3) 0.0074(3) 0.0057(3) 0.0050(3) C17 0.0135(3) 0.0138(3) 0.0155(3) 0.0015(3) 0.0058(3) -0.0005(2) C6 0.0134(3) 0.0117(3) 0.0128(3) 0.0029(3) 0.0046(3) 0.0010(2) C5 0.0187(4) 0.0132(3) 0.0191(4) 0.0078(3) 0.0077(3) 0.0056(3) C4 0.0223(4) 0.0133(3) 0.0198(4) 0.0041(3) 0.0087(3) -0.0014(3) C1B 0.0196(4) 0.0103(3) 0.0231(4) 0.0038(3) 0.0121(3) 0.0015(3) N17A 0.0135(3) 0.0138(3) 0.0155(3) 0.0015(3) 0.0058(3) -0.0005(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag N3 N2 C10 . . 116.77(7) ? N4 N3 N2 . . 171.89(9) ? C9 C10 N2 . . 116.31(7) ? C11 C10 N2 . . 123.03(8) ? C11 C10 C9 . . 120.64(8) ? C10 C9 C8 . . 121.71(7) ? C15 C9 C10 . . 118.70(7) ? C15 C9 C8 . . 119.59(7) ? N1A C8 C9 . . 126.97(7) ? N1A C8 C17 . . 107.79(7) ? C17 C8 C9 . . 125.04(7) ? C1B C8 C9 . . 126.97(7) ? C1B C8 N17A . . 107.79(7) ? N17A C8 C9 . . 125.04(7) ? O2 N1A C8 . . 127.81(8) ? O2 N1A C14 . . 123.50(8) ? C8 N1A C14 . . 108.64(7) ? C2 C14 N1A . . 131.01(8) ? C2 C14 C6 . . 121.74(8) ? C2 C14 C1B . . 131.01(8) ? C6 C14 N1A . . 107.23(8) ? C6 C14 C1B . . 107.23(8) ? C14 C2 H2 . . 121.7 ? C14 C2 C3 . . 116.59(8) ? C3 C2 H2 . . 121.7 ? C2 C3 H3 . . 119.3 ? C4 C3 C2 . . 121.42(8) ? C4 C3 H3 . . 119.3 ? C10 C11 H11 . . 120.1 ? C12 C11 C10 . . 119.71(8) ? C12 C11 H11 . . 120.1 ? C11 C12 H12 . . 119.7 ? C11 C12 C13 . . 120.52(8) ? C13 C12 H12 . . 119.7 ? C12 C13 H13 . . 120.2 ? C15 C13 C12 . . 119.67(8) ? C15 C13 H13 . . 120.2 ? C9 C15 H15 . . 119.6 ? C13 C15 C9 . . 120.76(8) ? C13 C15 H15 . . 119.6 ? O1 C17 C8 . . 127.91(8) ? O1 C17 C6 . . 123.29(8) ? C8 C17 C6 . . 108.80(7) ? C14 C6 C17 . . 107.50(7) ? C14 C6 N17A . . 107.50(7) ? C5 C6 C14 . . 122.61(8) ? C5 C6 C17 . . 129.89(8) ? C5 C6 N17A . . 129.89(8) ? C6 C5 H5 . . 121.9 ? C6 C5 C4 . . 116.25(8) ? C4 C5 H5 . . 121.9 ? C3 C4 C5 . . 121.38(8) ? C3 C4 H4 . . 119.3 ? C5 C4 H4 . . 119.3 ? O2 C1B C8 . . 127.81(8) ? O2 C1B C14 . . 123.50(8) ? C8 C1B C14 . . 108.64(7) ? O1 N17A C8 . . 127.91(8) ? O1 N17A C6 . . 123.29(8) ? C8 N17A C6 . . 108.80(7) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag O1 C17 . 1.2523(11) ? O1 N17A . 1.2523(11) ? O2 N1A . 1.2485(11) ? O2 C1B . 1.2485(11) ? N4 N3 . 1.1323(12) ? N2 N3 . 1.2396(11) ? N2 C10 . 1.4245(11) ? C10 C9 . 1.4061(12) ? C10 C11 . 1.3933(12) ? C9 C8 . 1.4628(12) ? C9 C15 . 1.3996(12) ? C8 N1A . 1.4019(13) ? C8 C17 . 1.4028(12) ? C8 C1B . 1.4019(13) ? C8 N17A . 1.4028(12) ? N1A C14 . 1.4767(12) ? C14 C2 . 1.3762(13) ? C14 C6 . 1.3865(12) ? C14 C1B . 1.4767(12) ? C2 H2 . 0.9500 ? C2 C3 . 1.4033(15) ? C3 H3 . 0.9500 ? C3 C4 . 1.3892(14) ? C11 H11 . 0.9500 ? C11 C12 . 1.3876(12) ? C12 H12 . 0.9500 ? C12 C13 . 1.3950(13) ? C13 H13 . 0.9500 ? C13 C15 . 1.3911(12) ? C15 H15 . 0.9500 ? C17 C6 . 1.4697(12) ? C6 C5 . 1.3744(12) ? C6 N17A . 1.4697(12) ? C5 H5 . 0.9500 ? C5 C4 . 1.4033(13) ? C4 H4 . 0.9500 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA C5 H5 O2 1_545 0.95 2.43 3.1077(16) 128 C11 H11 O1 2_766 0.95 2.57 3.2327(17) 127 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag O1 C17 C6 C14 . . . . 178.78(8) ? O1 C17 C6 C5 . . . . -0.58(14) ? O2 N1A C14 C2 . . . . 2.51(14) ? O2 N1A C14 C6 . . . . -176.07(8) ? N2 C10 C9 C8 . . . . -1.48(11) ? N2 C10 C9 C15 . . . . 178.39(7) ? N2 C10 C11 C12 . . . . -178.73(7) ? N3 N2 C10 C9 . . . . -174.08(7) ? N3 N2 C10 C11 . . . . 4.34(12) ? C10 C9 C8 N1A . . . . -59.12(12) ? C10 C9 C8 C17 . . . . 126.65(9) ? C10 C9 C8 C1B . . . . -59.12(12) ? C10 C9 C8 N17A . . . . 126.65(9) ? C10 C9 C15 C13 . . . . 0.57(12) ? C10 C11 C12 C13 . . . . 0.35(12) ? C9 C10 C11 C12 . . . . -0.38(12) ? C9 C8 N1A O2 . . . . 0.35(14) ? C9 C8 N1A C14 . . . . -177.02(7) ? C9 C8 C17 O1 . . . . -2.70(13) ? C9 C8 C17 C6 . . . . 176.94(7) ? C9 C8 C1B O2 . . . . 0.35(14) ? C9 C8 C1B C14 . . . . -177.02(7) ? C9 C8 N17A O1 . . . . -2.70(13) ? C9 C8 N17A C6 . . . . 176.94(7) ? C8 C9 C15 C13 . . . . -179.56(7) ? C8 N1A C14 C2 . . . . -179.99(9) ? C8 N1A C14 C6 . . . . 1.43(9) ? C8 C17 C6 C14 . . . . -0.88(9) ? C8 C17 C6 C5 . . . . 179.76(8) ? N1A C8 C17 O1 . . . . -177.87(8) ? N1A C8 C17 C6 . . . . 1.78(9) ? N1A C14 C2 C3 . . . . -178.72(8) ? N1A C14 C6 C17 . . . . -0.32(9) ? N1A C14 C6 C5 . . . . 179.09(7) ? C14 C2 C3 C4 . . . . -0.07(13) ? C14 C6 C5 C4 . . . . 0.01(12) ? C14 C6 N17A O1 . . . . 178.78(8) ? C14 C6 N17A C8 . . . . -0.88(9) ? C2 C14 C6 C17 . . . . -179.07(7) ? C2 C14 C6 C5 . . . . 0.35(13) ? C2 C14 C6 N17A . . . . -179.07(7) ? C2 C14 C1B O2 . . . . 2.51(14) ? C2 C14 C1B C8 . . . . -179.99(9) ? C2 C3 C4 C5 . . . . 0.43(14) ? C11 C10 C9 C8 . . . . -179.94(7) ? C11 C10 C9 C15 . . . . -0.08(11) ? C11 C12 C13 C15 . . . . 0.14(13) ? C12 C13 C15 C9 . . . . -0.61(12) ? C15 C9 C8 N1A . . . . 121.02(9) ? C15 C9 C8 C17 . . . . -53.22(11) ? C15 C9 C8 C1B . . . . 121.02(9) ? C15 C9 C8 N17A . . . . -53.22(11) ? C17 C8 N1A O2 . . . . 175.39(8) ? C17 C8 N1A C14 . . . . -1.97(9) ? C17 C6 C5 C4 . . . . 179.29(8) ? C6 C14 C2 C3 . . . . -0.31(13) ? C6 C14 C1B O2 . . . . -176.07(8) ? C6 C14 C1B C8 . . . . 1.43(9) ? C6 C5 C4 C3 . . . . -0.39(13) ? C5 C6 N17A O1 . . . . -0.58(14) ? C5 C6 N17A C8 . . . . 179.76(8) ? C1B C8 N17A O1 . . . . -177.87(8) ? C1B C8 N17A C6 . . . . 1.78(9) ? C1B C14 C2 C3 . . . . -178.72(8) ? C1B C14 C6 C5 . . . . 179.09(7) ? C1B C14 C6 N17A . . . . -0.32(9) ? N17A C8 C1B O2 . . . . 175.39(8) ? N17A C8 C1B C14 . . . . -1.97(9) ? N17A C6 C5 C4 . . . . 179.29(8) ?