#------------------------------------------------------------------------------ #$Date: 2024-04-06 01:41:30 +0200 (Sat, 06 Apr 2024) $ #$Revision: 291111 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/30/2023035.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023035 loop_ _publ_author_name 'Rybczyńska, Małgorzata' 'Sikorski, Artur' _publ_section_title ; Crystal structure of the tetra-ethyl-ammonium salt of the non-steroidal anti-inflammatory drug nimesulide (polymorph II). ; _journal_coeditor_code DX2059 _journal_issue 'Pt 3' _journal_name_full 'Acta crystallographica. Section E, Crystallographic communications' _journal_page_first 314 _journal_page_last 317 _journal_paper_doi 10.1107/S2056989024001300 _journal_volume 80 _journal_year 2024 _chemical_formula_iupac 'C8 H20 N +, C13 H11 N2 O5 S -' _chemical_formula_moiety 'C8 H20 N +, C13 H11 N2 O5 S -' _chemical_formula_sum 'C21 H31 N3 O5 S' _chemical_formula_weight 437.55 _chemical_melting_point 388 _chemical_name_systematic ; Tetraethylammonium N-methanesulfonyl-4-nitro-2-phenoxyanilinide ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary difmap _audit_creation_method SHELXL-2017/1 _cell_angle_alpha 90 _cell_angle_beta 91.792(9) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 11.0276(10) _cell_length_b 10.7661(8) _cell_length_c 19.635(2) _cell_measurement_reflns_used 15531 _cell_measurement_temperature 291(2) _cell_measurement_theta_max 25.002 _cell_measurement_theta_min 3.327 _cell_volume 2330.0(4) _computing_cell_refinement ; CrysAlis RED Version 1.171.32.15 (Oxford Diffraction, 2008) ; _computing_data_collection ; CrysAlis CCD Version 1.171.32.15 (Oxford Diffraction, 2008) ; _computing_data_reduction ; CrysAlis RED Version 1.171.32.15 (Oxford Diffraction, 2008) ; _computing_molecular_graphics ; ORTEP-3 for Windows (Farrugia, 2012) ; _computing_publication_material ; publCIF (Westrip, 2010) ; _computing_structure_refinement ; SHELXL2017/1 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 291(2) _diffrn_detector_area_resol_mean 10.4002 _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Oxford Diffraction Ruby CCD' _diffrn_measurement_method \w _diffrn_radiation_monochromator graphite _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0727 _diffrn_reflns_av_unetI/netI 0.0796 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_number 15531 _diffrn_reflns_theta_full 25.002 _diffrn_reflns_theta_max 25.002 _diffrn_reflns_theta_min 3.327 _exptl_absorpt_coefficient_mu 0.174 _exptl_absorpt_correction_T_max 0.998 _exptl_absorpt_correction_T_min 0.966 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (CrysAlis RED; Oxford Diffraction, 2008). ; _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.247 _exptl_crystal_description plate _exptl_crystal_F_000 936 _exptl_crystal_size_max 0.420 _exptl_crystal_size_mid 0.200 _exptl_crystal_size_min 0.090 _refine_diff_density_max 0.161 _refine_diff_density_min -0.229 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.097 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 276 _refine_ls_number_reflns 4094 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.097 _refine_ls_R_factor_all 0.1210 _refine_ls_R_factor_gt 0.0657 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0316P)^2^+0.0136P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1074 _refine_ls_wR_factor_ref 0.1277 _reflns_number_gt 2549 _reflns_number_total 4094 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file dx2059sup1.cif _cod_data_source_block I _cod_depositor_comments 'Adding full bibliography for 2023035.cif.' _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 2023035 _cod_database_fobs_code 2023035 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.930 _shelx_estimated_absorpt_t_max 0.985 _shelx_hkl_file ; 0 0 -4 111617. 716.500 3 0 0 -4 115273. 749.170 2 0 0 -5 15.8034 17.0770 3 0 0 5 15.2339 9.36410 3 0 0 -5 28.7481 19.9436 2 0 0 -6 2643.97 135.641 3 0 0 6 2446.43 132.349 3 0 0 6 2465.73 134.069 2 0 0 -6 2689.59 140.409 2 0 0 7-0.90518 10.0993 3 0 0 -7-3.91476 8.66255 3 0 0 -7 6.58768 9.13770 2 0 0 7-6.28486 19.5212 2 0 0 8 407.383 61.1669 3 0 0 -8 432.309 63.9599 3 0 0 -8 388.684 62.4043 2 0 0 8 412.375 62.5201 2 0 0 -9 36.6157 16.6107 3 0 0 9 4.88782 16.5029 3 0 0 9 10.2826 6.32421 2 0 0 -9-19.3851 24.0531 2 0 0 10 14106.4 410.746 3 0 0 -10 14322.7 404.359 3 0 0 10 14125.8 418.022 2 0 0 -10 14637.2 426.782 2 0 0 -11 18.6605 20.0412 3 0 0 -11-10.5381 21.7039 2 0 0 11 15.7897 4.16973 2 0 0 -12 603.615 95.0945 3 0 0 12 521.189 88.3751 2 0 0 -12 570.955 95.3698 2 0 0 -13 24.7310 25.0214 3 0 0 -13-25.9109 25.8530 2 0 0 -14 151.905 53.9099 3 0 0 -14 132.375 47.9113 2 0 0 -15-13.7749 19.5011 3 0 0 15 11.8018 22.5070 2 0 0 -15 13.1458 8.18035 2 0 0 -16 76.1100 42.1078 3 0 0 16 102.742 68.0975 2 0 0 -16 52.8842 27.5277 2 0 0 -17 7.02611 30.2686 3 0 0 17 77.5203 54.8886 2 0 0 -17-0.86370 24.6340 2 0 0 -18 154.531 65.5193 2 0 0 -18 136.979 61.3610 3 0 0 18 169.860 81.7105 2 0 0 -19 66.7743 47.6167 3 0 0 -19 9.28045 29.4090 2 0 0 -20 16.7291 44.4844 2 0 0 -20 65.1358 57.1571 3 0 0 -21 3.82943 22.2841 2 0 0 -21 59.8249 36.6762 3 0 0 -22 38.3676 43.4690 2 0 0 -22 10.8987 38.6533 3 0 0 -23 21.5280 26.8297 2 0 0 -24-9.02401 13.7358 2 0 0 -25 39.4692 33.6007 2 0 -1 -3 3357.14 139.218 3 0 1 -3 3387.63 92.0286 3 0 -1 -3 3234.89 93.6079 2 0 1 -3 3474.16 137.819 2 0 -1 4 18281.6 246.586 3 0 -1 -4 18955.2 361.014 3 0 1 -4 18383.6 239.553 3 0 1 4 18190.6 270.320 2 0 -1 -4 19494.9 257.281 2 0 1 -4 17838.3 348.140 2 0 -1 5 3659.24 125.639 3 0 -1 -5 3771.23 172.635 3 0 1 -5 3804.11 122.887 3 0 -1 -5 3707.87 131.036 2 0 1 -5 3832.05 176.133 2 0 1 5 3657.55 136.935 2 0 1 -6 1335.23 82.8420 3 0 -1 6 1322.64 86.0513 3 0 -1 -6 1251.51 109.449 3 0 1 6 1360.20 92.3340 2 0 -1 -6 1305.49 88.0527 2 0 1 -6 1333.96 110.532 2 0 -1 -7 5967.24 252.413 3 0 1 -7 6199.45 196.235 3 0 -1 7 6167.63 201.307 3 0 1 -7 6196.29 256.061 2 0 1 7 6066.57 211.685 2 0 -1 -7 6311.73 210.241 2 0 -1 8 22.9214 5.43576 3 0 -1 -8-9.08801 12.9330 3 0 1 8 34.9839 23.2893 2 0 1 -8 31.5338 21.8947 3 0 -1 8 80.6949 35.6940 2 0 1 -8 21.0516 7.87364 2 0 -1 -8 17.3315 17.3837 2 0 -1 9 72.8212 25.3546 3 0 -1 -9 28.4553 15.0173 3 0 1 9 105.623 33.2650 2 0 -1 9 62.2882 23.0053 2 0 1 -9 88.4627 28.0517 3 0 -1 -9 60.7152 27.3514 2 0 1 -9 94.0194 36.2220 2 0 -1 10 261.853 52.4782 3 0 -1 -10 279.593 62.1406 3 0 -1 10 305.948 62.7182 2 0 1 -10 314.839 53.4365 3 0 1 10 331.076 64.2441 2 0 -1 -10 284.658 55.7418 2 0 1 -10 245.901 57.0141 2 0 -1 -11 2734.17 204.447 3 0 1 -11 3038.70 179.485 3 0 -1 11 2980.33 183.307 3 0 -1 11 2977.25 215.242 2 0 1 11 2982.89 196.464 2 0 1 -11 3086.28 218.754 2 0 -1 -11 3017.80 191.703 2 0 -1 12 168.333 42.1950 3 0 -1 -12 206.158 58.1854 3 0 -1 -12 221.896 53.9458 2 0 1 12 235.606 63.4373 2 0 1 -12 239.910 53.9341 3 0 1 -12 219.348 62.1091 2 0 -1 -13 96.2338 41.3592 3 0 -1 13 21.5113 9.08879 3 0 1 -13 52.0485 38.8166 3 0 -1 -13 69.9785 30.8603 2 0 1 -13 79.6096 37.6133 2 0 1 13 59.0750 44.3815 2 0 -1 13 16.4768 33.9637 2 0 -1 -14 59.7134 42.9954 3 0 1 -14 21.7658 21.8020 2 0 -1 14 10.1459 11.2008 2 0 1 -14 50.5665 32.7656 3 0 -1 -14-39.1309 33.4241 2 0 1 -15 485.852 83.0983 3 0 -1 -15 528.290 104.610 3 0 -1 -15 521.677 94.2495 2 0 -1 15 503.875 99.8600 2 0 1 -15 539.917 107.683 2 0 -1 -16 70.4665 52.6457 3 0 1 16 46.1539 33.5215 2 0 1 -16 103.035 49.8736 2 0 -1 -16 37.1435 32.5171 2 0 -1 16 50.8325 55.6705 2 0 1 -16 16.4185 19.3543 3 0 -1 -17 181.884 68.3174 3 0 1 -17 159.700 54.6622 3 0 1 -17 121.310 49.0682 2 0 -1 17 164.216 69.8975 2 0 -1 -17 123.485 48.7629 2 0 1 17 193.284 61.0667 2 0 -1 -18 142.825 62.7709 3 0 1 18 134.607 53.3896 2 0 1 -18 147.851 64.0203 2 0 -1 -18 203.288 62.6800 2 0 1 -18 148.708 51.1718 3 0 -1 -19 54.5882 48.4762 3 0 1 -19 39.9814 39.3523 2 0 -1 -19-0.97829 12.3570 2 0 1 -19 19.5255 30.7983 3 0 1 19 15.4872 19.8081 2 0 -1 -20 59.7943 35.8527 3 0 -1 -20 71.4401 42.0054 2 0 1 -20 70.7576 43.3928 2 0 1 -20 53.1738 43.2063 3 0 -1 -21 93.5281 62.0834 3 0 1 -21 7.87332 23.3753 2 0 -1 -21 56.0329 38.0976 2 0 1 -21 63.5600 35.8813 3 0 -1 -22 89.9437 63.1975 3 0 1 -22 77.2588 43.1538 3 0 1 -22-16.6800 27.5128 2 0 -1 -22 13.6521 15.7535 2 0 -1 -23-15.4118 25.7663 3 0 -1 -23 7.39597 38.2745 2 0 1 -23 45.2207 51.6427 2 0 1 -24 62.0264 56.9177 2 0 -1 -24-20.4027 18.9908 2 0 1 -25 87.7151 79.7624 2 0 1 -26 63.6960 65.4107 2 0 -2 0 31846.8 400.953 4 0 -2 -1 40315.5 420.645 4 0 -2 1 40084.0 492.594 4 0 -2 -1 38379.3 473.523 1 0 2 -1 40633.2 468.667 2 0 2 2 143.642 24.9589 4 0 -2 -2 139.786 24.6556 4 0 2 -2 111.456 26.5024 2 0 -2 -2 188.407 39.7957 1 0 2 3 18260.0 284.747 4 0 -2 -3 18883.7 281.986 4 0 2 -3 18911.6 376.179 2 0 -2 4 502.701 46.9585 3 0 2 4 503.987 51.4363 4 0 -2 -4 570.534 53.1445 4 0 2 -4 564.715 71.0837 2 0 -2 -5 1516.22 132.056 3 0 -2 5 1526.53 83.9853 3 0 2 5 1420.45 92.1815 4 0 2 -5 1500.09 121.050 2 0 -2 -5 1558.55 83.3573 2 0 -2 6 1796.82 94.0168 3 0 2 6 1567.01 107.091 4 0 -2 -6 1772.87 145.982 3 0 -2 -6 1624.47 91.0053 2 0 2 -6 1876.55 143.614 2 0 -2 -7 1558.64 148.269 3 0 2 7 1630.93 120.837 4 0 2 -7 1735.12 97.9758 3 0 -2 7 1649.72 97.9636 3 0 2 -7 1683.30 145.540 2 0 -2 -7 1644.88 99.2593 2 0 -2 -8 331.389 68.2064 3 0 -2 8 361.812 50.6955 3 0 2 -8 345.744 45.1141 3 0 2 8 355.289 62.6417 4 0 -2 -8 315.277 43.8112 2 0 2 -8 391.573 71.5675 2 0 2 8 347.070 53.4741 2 0 -2 9 12.1637 15.3049 3 0 -2 -9 5.69167 15.0161 3 0 -2 -9 52.2051 25.1638 2 0 2 -9 22.6485 24.5316 2 0 2 9 35.6676 29.0816 2 0 2 -9 16.0271 15.3431 3 0 -2 9 7.14023 23.5503 2 0 -2 10 1758.98 122.967 3 0 -2 -10 1777.70 172.845 3 0 2 -10 1779.03 117.756 3 0 -2 -10 1793.70 131.382 2 0 2 -10 1721.17 169.172 2 0 2 10 1822.72 141.975 2 0 -2 11 1052.29 99.7021 3 0 2 -11 1156.27 101.323 3 0 -2 -11 1145.27 138.610 3 0 2 11 1151.44 119.342 2 0 -2 -11 1160.41 111.759 2 0 2 -11 1089.52 138.105 2 0 -2 12 86.0358 32.9010 3 0 -2 -12 156.659 57.2245 3 0 -2 -12 99.0089 38.3618 2 0 2 12 125.723 45.9731 2 0 2 -12 92.2057 46.4324 2 0 2 -12 140.424 34.9634 3 0 -2 12 63.3701 25.9071 2 0 -2 13 201.046 51.2255 3 0 -2 -13 132.083 51.6219 3 0 2 13 205.766 57.5128 2 0 -2 -13 277.555 61.4520 2 0 2 -13 205.654 61.8451 2 0 -2 13 286.210 79.7999 2 0 2 -13 239.995 53.6998 3 0 -2 -14 53.2909 29.9849 3 0 -2 14 29.7577 25.2260 3 0 2 -14 61.6825 32.3284 3 0 2 -14 101.712 46.2952 2 0 2 14 90.7260 42.4691 2 0 -2 14 23.2175 41.8388 2 0 -2 -14 47.8255 20.8970 2 0 -2 15 10.4265 9.66364 3 0 -2 -15 29.1940 35.8564 3 0 2 -15 40.7862 36.2031 2 0 -2 15 16.3055 15.0976 2 0 2 -15 67.3702 32.2055 3 0 -2 -15 30.3587 25.0013 2 0 -2 -16 74.7191 48.9474 3 0 -2 -16 92.6014 42.2888 2 0 2 -16 125.397 53.2903 2 0 2 -16 100.490 40.7447 3 0 -2 -17 71.9593 47.8102 3 0 -2 -17 39.0476 16.5681 2 0 2 -17 101.365 49.2262 2 0 2 -17 97.8148 43.9631 3 0 2 17 110.389 44.6233 2 0 -2 -18 165.780 70.7582 3 0 2 -18 89.6423 46.6773 3 0 2 18 102.870 54.4766 2 0 2 -18 118.832 67.1367 2 0 -2 -18 106.513 53.6605 2 0 -2 -19-13.3248 18.9438 3 0 2 -19 4.01947 20.7470 3 0 2 19 68.9930 64.5248 2 0 2 -19 3.78110 29.6888 2 0 -2 -19 68.1340 47.6045 2 0 -2 -20-7.34290 16.6797 3 0 -2 -20 35.4113 40.9179 2 0 2 -20 40.1660 26.2420 3 0 2 -20-13.8659 15.1894 2 0 -2 -21 48.5091 37.9344 3 0 2 -21 20.6825 31.7591 3 0 -2 -21 63.2397 38.3657 2 0 2 -21 35.5736 41.5539 2 0 -2 -22-9.50230 4.19663 3 0 2 -22 39.2930 29.7633 2 0 -2 -22 75.4879 54.6416 2 0 -2 -23 66.2099 51.7685 3 0 -2 -23 80.2392 51.8693 2 0 2 -23 82.1277 69.4333 2 0 -2 -24 65.5894 55.2210 3 0 2 -24-6.18113 18.6485 2 0 2 -25 12.3674 26.7178 2 0 2 -26-25.7103 17.3061 2 0 -3 0-8.98077 3.52455 4 0 -3 0 11.9735 9.20420 2 0 -3 -1 4532.16 178.752 4 0 3 1 4337.79 175.090 4 0 -3 1 4646.21 199.345 4 0 -3 -1 4584.52 166.506 2 0 -3 -1 4458.68 195.547 1 0 3 -1 4709.02 189.892 2 0 -3 -2 87.2817 26.4689 4 0 -3 2 76.2236 38.9300 4 0 3 2 91.5050 31.1101 4 0 3 -2 127.150 36.7487 2 0 -3 -2 110.266 30.5929 1 0 -3 -3 300.507 42.0687 4 0 3 3 322.308 44.1825 4 0 3 -3 328.922 57.3144 2 0 -3 -4 119.342 34.3302 4 0 3 4 96.7785 31.7765 4 0 3 -4 79.1800 24.3972 2 0 3 5 4794.76 183.285 4 0 -3 -5 5062.53 187.170 4 0 3 -5 5190.72 247.588 2 0 3 6 491.027 59.5980 4 0 -3 6 722.570 73.0864 3 0 -3 -6 424.444 79.5822 3 0 3 -6 470.290 83.1560 2 0 -3 -6 527.166 54.7535 2 0 -3 7 326.070 49.1804 3 0 3 7 247.941 46.0973 4 0 -3 -7 223.712 56.7494 3 0 -3 -7 260.177 41.5670 2 0 3 -7 355.369 78.8539 2 0 3 8 138.946 36.5284 4 0 -3 -8 128.538 42.4086 3 0 3 -8 133.267 49.1248 2 0 -3 8 128.822 29.4395 3 0 -3 -8 141.091 31.1383 2 0 3 9 36.3424 25.1189 4 0 -3 -9 46.2238 24.7892 3 0 -3 9 83.1845 32.6010 3 0 3 -9 41.4187 35.3829 2 0 -3 -9 22.8901 5.60639 2 0 3 10 628.977 85.2830 4 0 -3 -10 584.864 107.057 3 0 -3 10 545.020 68.8005 3 0 3 -10 552.774 100.479 2 0 -3 -10 534.988 64.6694 2 0 -3 -11 673.925 117.164 3 0 -3 11 674.341 78.0404 3 0 3 11 637.230 91.4015 4 0 3 -11 604.414 107.638 2 0 -3 11 734.590 122.135 2 0 -3 -11 671.324 80.3952 2 0 3 12 535.012 92.6762 4 0 -3 -12 311.738 80.1162 3 0 -3 12 383.428 58.5944 3 0 -3 -12 445.068 70.1514 2 0 3 -12 352.984 87.7306 2 0 -3 12 517.251 107.485 2 0 -3 -13 419.905 94.2105 3 0 -3 13 416.456 67.4146 3 0 3 13 478.125 87.5726 4 0 -3 -13 448.257 72.2631 2 0 -3 13 573.490 116.688 2 0 3 -13 504.762 108.422 2 0 3 14 668.276 114.717 4 0 3 -14 547.515 71.8782 3 0 -3 -14 576.518 120.642 3 0 -3 14 624.328 85.0851 3 0 -3 -14 629.044 89.5033 2 0 3 -14 652.216 125.859 2 0 -3 14 623.001 123.666 2 0 -3 -15 826.764 147.042 3 0 -3 15 805.983 99.7536 3 0 3 -15 740.490 89.0382 3 0 3 -15 888.625 149.909 2 0 -3 -15 759.302 104.848 2 0 3 -16 475.737 74.0020 3 0 -3 16 571.268 88.0205 3 0 -3 -16 439.982 108.765 3 0 3 -16 564.599 134.073 2 0 -3 -16 513.186 89.1478 2 0 3 17 569.884 117.233 4 0 3 -17 551.162 79.6237 3 0 -3 -17 586.431 133.054 3 0 3 -17 587.164 133.562 2 0 -3 -17 550.602 96.6286 2 0 3 18 15.3777 15.3773 4 0 -3 -18-18.1093 32.9427 3 0 3 -18 128.551 72.1870 2 0 -3 -18 96.1893 45.2821 2 0 3 -18 63.7908 19.6402 3 0 -3 -19 86.8064 53.2335 3 0 3 19-4.21903 10.6520 4 0 3 -19 47.7799 35.3694 2 0 3 -19-24.2219 19.5501 3 0 -3 -19 23.3357 24.7074 2 0 -3 -20 96.9888 54.4085 3 0 3 -20 185.669 81.1810 2 0 -3 -20 130.712 55.4662 2 0 -3 -21 9.93805 23.8597 3 0 -3 -21 117.916 54.9169 2 0 3 -21 127.506 72.1178 2 0 -3 -22 63.5404 62.2792 3 0 -3 -22 23.4617 34.6359 2 0 3 -22-8.81450 21.3808 2 0 -3 -23-18.7279 34.1209 3 0 3 -23 21.8851 58.0965 2 0 -3 -24-9.70416 24.4093 3 0 3 -24 37.9281 8.63873 2 0 3 -25-16.3161 18.7003 2 0 -4 0 1008.04 100.568 4 0 -4 0 1006.42 95.6300 2 0 4 1 6125.89 243.127 4 0 -4 1 6545.03 270.648 4 0 -4 -1 6402.80 247.362 4 0 -4 1 6353.63 252.467 2 0 -4 -1 6307.04 270.000 1 0 -4 -1 6141.78 225.724 2 0 -4 -2 29.0465 21.8516 4 0 4 2 31.6406 16.6540 4 0 -4 2 8.46967 1.35741 4 0 -4 -2 15.9680 10.8307 2 0 4 -2 22.5614 14.5173 2 0 -4 -2 19.8043 20.0938 1 0 4 3 370.636 55.0115 4 0 -4 3 388.071 70.9393 4 0 -4 -3 336.566 54.1032 4 0 4 -3 371.207 68.1382 2 0 -4 -3 402.631 73.6500 1 0 4 4 183.604 34.8712 4 0 -4 -4 196.276 42.4600 4 0 4 -4 183.316 48.1197 2 0 4 5 2555.96 145.323 4 0 -4 -5 2729.96 150.069 4 0 4 -5 2713.98 196.258 2 0 4 6 3178.10 162.968 4 0 -4 -6 3371.97 173.719 4 0 4 -6 3305.80 225.375 2 0 -4 -7 1.40074 4.62502 4 0 4 7 15.3617 8.92043 4 0 -4 -7-28.3107 41.3195 3 0 -4 7-6.13632 18.5642 3 0 -4 -7 50.2373 25.3087 2 0 4 -7 11.3357 13.5682 2 0 4 8-13.6008 10.7862 4 0 -4 -8-12.2353 6.30528 3 0 -4 8 26.8969 20.4377 3 0 -4 -8-7.85449 6.05127 2 0 4 -8-5.01590 14.7987 2 0 -4 -9 593.759 115.051 3 0 4 9 564.893 76.7367 4 0 -4 9 634.076 71.0849 3 0 4 -9 598.551 106.423 2 0 -4 -9 595.070 67.7948 2 0 -4 10 3108.30 163.628 3 0 4 10 3066.08 185.986 4 0 -4 -10 3033.99 262.695 3 0 -4 -10 3211.94 157.758 2 0 4 -10 3155.83 251.537 2 0 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250.469 77.6361 2 0 -6 6 321.940 76.6310 2 0 6 7 313.804 59.0733 4 0 -6 7 376.275 90.6988 4 0 -6 -7 306.620 62.5621 4 0 -6 7 286.658 79.9016 2 0 6 -7 303.175 83.9591 2 0 6 8 198.480 46.0277 4 0 -6 8 229.581 75.6065 4 0 -6 -8 234.241 56.9449 4 0 -6 -8 295.051 82.7323 3 0 6 8 278.355 80.2096 1 0 6 -8 212.389 69.0274 2 0 -6 8 231.748 69.6445 2 0 6 9 883.676 104.671 4 0 -6 -9 770.519 151.860 3 0 -6 -9 807.358 104.264 4 0 -6 9 717.619 88.6273 3 0 6 -9 703.964 135.009 2 0 -6 -9 868.998 92.6097 2 0 -6 9 872.743 154.772 2 0 6 9 924.285 156.056 1 0 -6 -10 808.191 152.564 3 0 6 10 761.165 98.6498 4 0 -6 10 800.696 97.7439 3 0 -6 -10 827.209 86.9007 2 0 6 -10 734.673 135.270 2 0 6 10 751.419 148.583 1 0 -6 -11 59.7384 44.8665 3 0 6 11 46.4247 29.6611 4 0 -6 -11 35.7985 28.1366 2 0 6 -11 20.9606 37.5190 2 0 6 11 58.0801 68.0930 1 0 -6 11 55.3357 32.2372 3 0 -6 -12 124.160 57.3546 3 0 6 12 138.562 48.3727 4 0 -6 12 287.241 67.8063 3 0 -6 -12 91.6962 27.9916 2 0 6 12 89.2511 63.2133 1 0 6 -12 100.871 39.3846 2 0 -6 13 656.959 88.9516 3 0 -6 -13 662.105 155.265 3 0 6 13 614.853 94.3268 4 0 6 -13 612.231 137.568 2 0 -6 -13 602.257 71.0100 2 0 6 13 637.583 137.348 1 0 -6 14 445.327 72.4074 3 0 6 14 376.192 75.9948 4 0 -6 -14 335.811 113.692 3 0 -6 -14 401.753 62.1237 2 0 6 -14 399.597 115.178 2 0 6 14 511.676 131.040 1 0 -6 15 118.023 36.7799 3 0 -6 -15 75.9206 67.6014 3 0 6 15 105.654 46.1302 4 0 6 15 174.675 100.011 1 0 -6 -15 132.806 40.7976 2 0 6 -15 62.9283 49.5507 2 0 -6 -16-26.5045 54.1821 3 0 -6 -16 17.9618 18.9287 2 0 6 16 63.4945 93.4277 1 0 6 -16 23.1196 14.7518 2 0 -6 -17 102.172 64.7179 3 0 6 17 100.148 74.8163 1 0 6 -17 63.1364 53.0907 2 0 -6 -17 71.0205 29.8914 2 0 -6 -18 52.6539 58.3752 3 0 6 -18 106.837 71.9009 2 0 6 18 160.214 98.9274 1 0 -6 -19 106.930 72.8016 3 0 6 -19 99.6215 69.0881 2 0 6 19 40.8936 89.9757 1 0 -6 -20 43.0352 54.7354 3 0 6 -20 18.9823 42.0531 2 0 6 20 15.7486 81.1472 1 0 -6 -21 70.4137 60.6860 3 0 6 -21 102.052 63.5496 2 0 6 21 139.938 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42.1033 2 0 -7 6 86.1926 36.2370 2 0 7 7 202.583 55.9024 4 0 -7 -7 292.062 72.1612 4 0 -7 7 216.192 79.2350 4 0 -7 7 149.386 64.4535 2 0 -7 -7 203.164 43.6024 2 0 7 7 98.9524 35.3222 1 0 7 -7 136.140 49.8931 2 0 -7 -8 175.016 50.7427 4 0 -7 -8 93.8035 38.2766 3 0 -7 8 130.624 66.8246 4 0 7 8 138.341 46.5611 4 0 7 -8 103.156 44.3225 2 0 7 8 82.5556 27.0714 1 0 -7 9 73.2039 44.7659 4 0 -7 -9 82.0452 52.6331 4 0 7 9 61.0085 31.9070 4 0 -7 -9-34.6583 32.3441 3 0 7 9 41.3799 44.8712 1 0 7 -9-40.3630 47.0042 2 0 7 10 25.4387 18.8434 4 0 -7 -10 37.6600 31.5021 4 0 -7 10 38.5540 38.8655 4 0 -7 -10 44.1191 13.3611 3 0 7 10 36.0922 53.3030 1 0 -7 -10 83.5466 34.2260 2 0 -7 10 24.2711 14.3857 3 0 7 -10 31.2165 18.5191 2 0 -7 11 172.065 69.3852 4 0 7 11 199.171 54.1412 4 0 -7 -11 189.753 77.2769 3 0 7 -11 201.643 83.4619 2 0 -7 11 294.081 62.3724 3 0 -7 -11 231.861 47.6724 2 0 7 11 240.949 88.7943 1 0 -7 -12 11.0987 25.6697 3 0 7 12 45.1237 27.2353 4 0 -7 12 40.5200 33.6808 4 0 -7 -12 84.9937 27.3481 2 0 -7 12 104.406 40.0275 3 0 7 -12-2.44612 44.1389 2 0 7 12 17.6175 43.2836 1 0 -7 13 92.8617 66.6558 4 0 7 13 47.8348 17.5960 4 0 -7 -13 88.6165 73.0531 3 0 -7 13 114.205 41.5319 3 0 -7 -13 79.0589 26.5695 2 0 7 -13 35.8879 9.63500 2 0 7 13 79.8456 64.1064 1 0 7 14 33.7176 25.8652 4 0 -7 -14 33.0748 33.5611 3 0 -7 14-1.91055 16.3499 4 0 7 -14 10.5813 32.3106 2 0 -7 -14 5.37640 16.9062 2 0 -7 14 39.2160 30.5011 3 0 7 14 12.2267 43.5086 1 0 -7 -15 62.1095 53.8263 3 0 -7 15 14.9036 58.1927 4 0 7 -15-4.84799 48.8633 2 0 7 15 28.0294 45.6600 1 0 -7 -15 26.2143 24.9223 2 0 -7 -16 2.55178 9.86264 3 0 -7 16 12.7300 60.6153 4 0 7 -16 56.8662 75.4942 2 0 7 16 36.9163 50.2641 1 0 -7 17 104.229 70.3455 4 0 -7 -17 99.2129 62.9403 3 0 7 17 194.713 98.8025 1 0 7 -17 141.794 85.3328 2 0 -7 18-14.7228 10.1437 4 0 -7 -18 5.06615 33.9849 3 0 7 -18-13.7944 21.5372 2 0 7 18 5.85707 65.0924 1 0 -7 19 8.23089 20.3483 4 0 -7 -19 92.1668 73.1930 3 0 7 19 26.8508 77.0464 1 0 7 -19 11.6015 31.1620 2 0 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73.5429 3 -1 -5 22 115.481 42.9445 4 1 5 -22 106.495 88.4907 2 1 -5 -21 70.0792 63.3829 3 -1 -5 21 91.2390 67.1693 4 1 5 -21-18.2073 16.2940 2 -1 -5 20 60.1442 64.0780 4 1 -5 -20 59.1801 62.4633 3 1 5 -20 59.1797 45.3414 2 -1 -5 19-10.1328 25.1982 4 1 -5 -19-4.21519 18.8300 3 1 5 -19 51.5177 40.4915 2 1 -5 -18 164.182 78.1509 3 1 5 -18 86.5082 71.0995 2 1 -5 -18 96.4798 30.7576 2 -1 5 17 552.995 130.988 4 1 -5 -17 733.974 238.290 3 1 -5 -17 36.0918 24.4456 2 -1 5 17 352.896 129.374 1 -1 -5 16 31.1161 30.6411 3 1 -5 -16 72.8520 48.7124 3 -1 5 16 25.5949 29.2472 4 1 -5 -16 35.7978 21.1159 2 -1 5 16 21.5996 63.2165 1 1 5 -16 34.7022 48.0881 2 -1 5 15 82.5708 35.2880 4 -1 -5 15 153.740 55.5929 3 1 -5 -15 133.588 59.5833 3 1 5 -15 73.7404 51.5426 2 1 -5 -15 133.277 30.3220 2 -1 5 15 238.840 105.633 1 -1 -5 14 158.802 57.2790 3 1 -5 -14 64.5200 54.1208 3 -1 5 14 185.199 47.9265 4 -1 5 14 210.443 90.8465 1 1 -5 -14 148.248 30.2398 2 1 5 -14 145.047 69.2429 2 -1 -5 13 131.070 44.2751 3 1 -5 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8 130.659 39.5693 3 1 -5 -8 157.347 25.9315 2 1 -5 -7 517.336 65.1889 4 -1 5 7 379.034 53.2255 4 1 -5 -7 380.349 96.3568 3 -1 -5 7 398.733 89.9639 4 1 -5 -7 391.089 40.6129 2 -1 -5 6 949.550 139.109 4 1 -5 -6 827.939 134.242 3 -1 5 6 853.004 79.4359 4 1 -5 -6 775.345 72.5231 4 1 -5 -6 849.372 64.0515 2 1 -5 -5 2604.22 226.873 3 -1 -5 5 2721.82 225.694 4 1 -5 -5 2695.57 142.118 4 -1 5 5 2468.20 137.689 4 1 -5 -5 2717.86 123.723 2 1 -5 -4 477.665 65.0502 4 1 -5 -4 435.396 89.7074 3 -1 -5 4 448.840 90.5841 4 1 -5 -4 526.106 97.9669 1 1 -5 -4 460.764 55.7387 2 -1 -5 3 159.090 46.5990 4 1 -5 -3 164.321 40.9828 4 1 -5 -3 204.960 63.3016 1 1 -5 -3 169.495 34.9385 2 -1 -5 2 2471.43 198.666 4 1 -5 -2 2535.18 158.566 4 1 -5 -2 2538.54 146.748 2 -1 -5 2 2310.65 181.249 2 1 -5 -2 2507.38 196.041 1 1 5 -1 815.465 111.868 4 -1 -5 1 876.423 114.060 4 1 -5 -1 896.080 97.8003 4 1 -5 -1 784.134 106.626 1 1 -5 -1 812.481 89.6260 2 -1 -5 1 760.992 97.4623 1 -1 -5 1 828.702 104.599 2 1 5 0 38.7046 32.7310 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40.5604 3 1 5 17 121.284 65.7988 4 -1 -5 -17 146.910 55.5228 2 -1 5 -17 146.206 75.9643 2 -1 -5 -18-16.1749 12.5784 3 -1 -5 -18 58.5095 43.1745 2 -1 5 -18 53.0607 66.7266 2 -1 -5 -19 46.8510 47.8752 3 -1 -5 -19-0.60392 20.3768 2 -1 5 -19-6.03571 32.5445 2 -1 -5 -20 29.9230 38.5621 3 -1 5 -20 68.5344 59.6535 2 -1 -5 -20 98.2167 47.9584 2 -1 -5 -21 2.20849 22.7099 3 -1 5 -21 20.3253 25.5394 2 -1 -5 -22-100.401 63.5835 3 -1 5 -22-17.6969 17.2536 2 -1 -5 -23 87.0601 77.4822 3 -1 5 -23-68.0964 47.4699 2 -1 -5 -24 20.5663 29.3542 3 1 -6 -24 70.0277 85.9776 3 1 -6 -23 127.717 85.3852 3 -1 -6 22 112.919 91.6275 4 1 -6 -22 52.1363 88.7859 3 -1 6 22 62.0721 86.8927 1 1 -6 -21 38.1902 61.5975 3 -1 -6 21-38.5728 71.5989 4 -1 6 21 151.644 118.511 1 1 -6 -20 34.8617 41.1591 3 -1 -6 20-45.0349 68.7047 4 -1 -6 19 40.2682 49.3453 4 1 -6 -19 52.5687 59.5009 3 1 6 -19 87.9728 67.4304 2 -1 6 19 57.2182 72.5598 1 1 -6 -18-13.0326 32.7961 3 -1 -6 18-0.57102 18.6551 4 1 6 -18 31.7090 16.7959 2 1 -6 -17 116.848 81.5457 3 -1 -6 17 2.71059 24.2657 4 -1 6 17 146.279 101.337 1 1 6 -17 116.130 68.9505 2 -1 -6 16 217.128 91.4198 4 -1 -6 16 230.658 64.1569 3 1 -6 -16 79.8712 51.6420 3 -1 6 16 219.240 114.036 1 1 6 -16 213.777 85.4752 2 1 -6 -16 111.446 19.4263 2 -1 6 15 262.281 55.5724 4 1 -6 -15 167.436 78.9156 3 -1 -6 15 175.360 54.3198 3 -1 -6 15 215.535 91.2235 4 1 -6 -15 130.450 18.6280 2 1 6 -15 178.224 77.9260 2 -1 6 15 181.000 102.005 1 1 -6 -14 37.6570 35.5050 3 -1 -6 14 72.6616 65.7711 4 -1 -6 14 157.117 51.3244 3 1 6 -14 72.0240 54.3877 2 -1 -6 13 35.6683 48.6155 4 -1 6 13 121.035 36.9881 4 1 -6 -13 84.5942 61.1775 3 -1 6 13 126.861 80.3294 1 -1 -6 13 111.249 39.1396 3 1 6 -13 67.5532 51.1163 2 -1 -6 12 26.1401 13.5554 4 -1 6 12 54.9579 26.2835 4 1 -6 -12 76.1165 63.3688 3 1 6 -12 56.0658 36.9621 2 -1 6 12 50.5470 62.4460 1 -1 -6 12 98.7230 33.0777 3 -1 6 11 8.24768 2.82280 4 1 -6 -11 30.8639 29.7095 3 -1 -6 11 4.71280 22.0927 4 -1 6 11 47.6586 34.0504 1 1 6 -11-21.0877 18.9699 2 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2062.80 208.087 1 -1 -6 5 2030.99 200.498 2 1 -6 -4 887.251 134.342 3 -1 -6 4 979.327 143.220 4 1 -6 -4 934.906 101.911 4 -1 -6 4 957.861 135.402 2 1 -6 -4 923.477 134.814 1 1 -6 -4 917.190 90.0802 2 1 -6 -3 24.5611 26.5297 4 -1 -6 3 21.2858 33.8263 4 1 -6 -3 28.9283 14.4752 2 -1 -6 3 39.0508 28.5305 2 1 -6 -3-0.49938 40.1078 1 -1 -6 2 71.4807 41.4051 4 1 -6 -2 75.3926 29.4261 4 -1 -6 2 123.837 47.1244 2 1 -6 -2 132.352 49.1205 1 1 -6 -2 87.8594 31.6626 2 1 -6 -1 83.4281 37.8792 4 -1 -6 1 44.3302 22.0039 4 1 -6 -1 40.0295 20.5759 1 -1 -6 1 30.6660 28.4451 1 -1 -6 1 27.9737 17.1583 2 1 -6 -1 30.8892 20.3165 2 -1 -6 0 2407.09 201.191 4 1 -6 0 2462.40 187.441 4 1 6 0 2351.27 204.503 4 -1 -6 0 2371.00 188.373 2 1 -6 0 2406.64 178.456 2 -1 -6 0 2289.97 191.783 1 1 6 1 217.870 58.0126 4 -1 -6 -1 299.110 73.7402 4 1 -6 1 234.453 58.2764 4 1 -6 1 216.140 52.2650 2 -1 -6 -1 249.875 65.9068 1 -1 -6 -1 272.997 62.5463 2 1 -6 2 7.48378 17.6656 4 1 6 2-4.23787 16.1438 4 -1 -6 -2 21.1520 59.9016 1 1 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200.096 3 -2 -2 11 1902.78 172.268 3 2 2 -11 1806.25 181.712 2 -2 2 11 1783.23 117.088 2 2 -2 -11 1850.16 121.430 2 -2 -2 10 3408.19 254.207 4 -2 -2 10 3554.24 225.808 3 -2 2 10 3788.42 266.768 3 2 2 -10 3403.34 212.713 3 2 -2 -10 3328.66 248.572 3 -2 2 10 3265.59 144.631 2 2 2 -10 3354.32 242.430 2 2 2 -9 3864.37 219.519 3 -2 -2 9 4040.90 256.167 4 -2 2 9 3919.15 268.552 3 2 -2 -9 3753.97 253.893 3 -2 -2 9 3963.03 230.896 3 -2 2 9 3754.32 140.281 2 -2 -2 9 3826.48 242.270 2 2 -2 -8 19.9617 17.0754 3 -2 -2 8-2.69841 20.0599 4 2 2 -8 23.7547 23.1911 3 -2 2 8 2.41814 9.67229 2 -2 -2 8 8.79177 14.8434 2 -2 -2 8 11.2272 5.18428 3 -2 -2 7 185.101 48.9120 4 2 -2 -7 179.853 57.0989 3 2 2 -7 211.629 47.4943 3 -2 2 7 195.821 21.7853 2 -2 -2 7 199.092 46.7606 3 -2 -2 7 215.011 51.1021 2 -2 -2 6 1496.73 141.109 4 -2 -2 6 1531.87 129.449 3 2 2 -6 1560.98 125.892 3 2 -2 -6 1470.03 143.321 3 -2 2 6 1761.94 141.798 1 -2 -2 5 8129.24 313.401 4 -2 -2 5 7914.94 280.570 3 2 -2 -5 7939.47 317.311 3 2 2 -5 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37.8273 3 -2 2 -15 139.211 33.1494 3 -2 2 -15 64.9326 18.2421 2 -2 -2 -15 146.214 60.8377 2 -2 2 -16 331.704 50.6918 3 -2 -2 -16 328.799 84.6668 3 2 2 16 347.147 103.161 4 -2 -2 -16 368.033 88.8739 2 -2 2 -16 384.787 103.836 2 -2 -2 -17 65.4116 38.2292 3 -2 2 -17 53.3052 37.2139 2 -2 -2 -17 48.5947 24.4376 2 -2 2 -17 25.7802 17.8646 3 -2 -2 -18 19.7196 17.6563 3 -2 2 -18 42.2483 23.5056 3 -2 2 -18-15.4099 14.1769 2 -2 -2 -18-18.1100 16.6441 2 -2 -2 -19 190.667 74.8442 3 -2 2 -19 101.287 32.5843 3 -2 -2 -19 116.630 56.6272 2 -2 2 -19 119.699 59.2894 2 -2 -2 -20 53.7472 45.4569 3 -2 -2 -20 33.6953 44.1018 2 -2 2 -20 143.782 71.1643 2 -2 -2 -21 157.148 66.3770 3 -2 -2 -21 145.387 63.2192 2 -2 2 -21 155.325 75.7036 2 -2 -2 -22 118.722 61.5161 3 -2 2 -22 65.6847 48.0383 2 -2 -2 -22-11.5756 44.9624 2 -2 2 -23 41.5200 53.0748 2 -2 -2 -23-24.4550 37.1283 2 -2 2 -24-7.50081 14.7416 2 -2 -2 -24 11.1931 8.70418 2 -2 2 -25 148.166 111.717 2 -2 -3 26 58.5408 67.3428 4 -2 -3 25-53.3972 47.9929 4 2 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178.129 3 -2 -3 15 2187.66 248.669 4 -2 3 15 2069.00 178.958 4 -2 -3 15 2193.87 206.089 3 2 -3 -15 1785.84 232.480 3 -2 3 15 2082.50 155.109 2 2 -3 -15 1954.80 140.604 2 2 3 -15 2215.90 236.048 2 2 -3 -14 690.870 137.902 3 -2 3 14 727.872 97.3928 4 -2 -3 14 803.625 123.801 3 -2 -3 14 681.969 137.239 4 2 3 -14 618.752 100.576 3 2 -3 -14 563.792 71.2005 2 2 3 -14 766.869 135.247 2 -2 3 14 689.487 85.8676 2 -2 -3 14 723.835 136.238 2 2 3 -13 550.334 90.2317 3 -2 -3 13 626.223 108.515 3 2 -3 -13 525.464 125.574 3 -2 3 13 545.975 74.9026 4 -2 -3 13 628.944 127.040 4 2 3 -13 556.692 117.746 2 -2 -3 13 660.639 125.280 2 -2 3 13 602.798 74.0203 2 2 -3 -12 55.8817 51.7547 3 -2 -3 12-20.6042 28.6208 4 -2 3 12 32.1936 43.8964 4 -2 -3 12 66.2554 38.6101 3 -2 3 12 32.1839 29.6105 2 2 3 -12 12.0783 14.2357 2 2 3 -12 50.0354 15.3360 3 -2 -3 12 26.5008 15.2762 2 -2 3 11 66.8451 27.8142 4 2 -3 -11 79.3452 44.7513 3 -2 -3 11 49.0015 25.1151 3 -2 -3 11 9.24651 21.5107 4 2 3 -11 63.5415 38.2501 2 -2 -3 11 39.4396 27.0469 2 2 3 -11 34.6694 19.9847 3 2 -3 -10 203.637 69.1021 3 -2 3 10 120.877 54.1850 3 -2 -3 10 179.017 60.7602 4 -2 3 10 208.408 35.3868 4 -2 -3 10 98.1101 42.1635 2 -2 -3 10 152.947 47.5923 3 -2 -3 9 561.510 85.8550 3 2 -3 -9 533.273 105.191 3 -2 3 9 525.928 57.7297 4 -2 -3 9 490.516 100.516 4 -2 -3 8 91.0331 36.0771 4 2 -3 -8 42.2992 9.17495 3 -2 3 8 94.3023 18.3647 4 -2 -3 8 86.2548 27.5606 3 -2 -3 7 1097.64 137.101 4 -2 -3 7 1172.07 119.193 3 2 -3 -7 1082.41 138.959 3 2 -3 -6 825.567 116.200 3 -2 -3 6 829.377 115.445 4 -2 -3 6 814.973 95.2363 3 -2 -3 5 370.400 71.7051 4 2 -3 -5 417.180 78.3201 3 -2 -3 5 321.866 57.6244 3 -2 -3 4 33.7147 25.9376 4 2 -3 -4 62.2879 33.7627 3 2 -3 -4 38.6110 28.9834 1 -2 -3 3 5524.07 267.050 4 2 -3 -3 5569.76 260.504 3 2 -3 -3 5359.04 120.734 4 -2 3 3 5348.22 125.448 2 2 -3 -3 5583.18 252.590 1 2 -3 -3 5284.55 129.972 2 -2 -3 2 959.476 106.003 4 2 -3 -2 969.652 104.787 3 2 -3 -2 988.077 64.8616 2 2 -3 -2 971.417 102.473 1 -2 3 2 1031.80 66.2800 2 2 -3 -1 1832.28 136.820 3 -2 -3 1 1927.45 152.580 4 -2 -3 1 1763.04 103.310 1 -2 3 1 1887.81 100.758 2 2 -3 -1 1785.54 100.473 2 2 -3 0 2301.06 144.478 3 -2 -3 0 2463.93 167.856 4 2 -3 0 2140.45 118.961 2 -2 3 0 2164.76 121.687 2 -2 -3 0 2263.08 122.244 1 2 -3 1 276.979 46.9153 3 -2 -3 -1 211.708 48.4041 4 -2 3 -1 232.409 42.6635 2 2 3 1 250.851 41.6411 1 2 -3 1 208.936 39.1551 2 -2 -3 -2 2014.79 151.171 4 2 -3 2 1987.97 114.601 3 2 3 2 2094.81 132.160 1 -2 3 -2 2118.96 142.724 2 2 -3 2 1922.16 132.852 2 -2 -3 -3 55.7673 40.6752 4 2 -3 3 42.2827 11.8491 3 2 3 3 33.4567 14.0349 4 -2 3 -3 51.6206 24.0822 2 -2 -3 -4 140.532 65.1302 4 2 -3 4 21.1115 8.65779 3 2 3 4 56.5981 51.5840 4 -2 3 -4 60.7238 32.0806 2 -2 -3 -5 59.4030 36.4730 4 2 -3 5 58.4577 12.4758 3 2 3 5 27.5614 29.7937 4 -2 3 -5 55.7145 20.5701 2 -2 -3 -6 689.600 97.1727 4 2 3 6 664.625 93.3020 4 -2 3 -6 662.620 96.9980 2 -2 -3 -7 16.4326 22.3895 4 2 3 7 107.885 41.4176 4 -2 -3 -7 34.9207 25.7384 2 -2 3 -7 68.7252 41.0191 2 2 3 8 58.1971 45.7104 4 -2 -3 -8 14.8044 14.1122 2 -2 3 -8 14.4881 26.7317 2 2 3 9 1033.61 131.039 4 -2 -3 -9 955.932 115.901 2 -2 3 -9 934.928 133.512 2 2 3 10 7.09191 32.9668 4 -2 3 -10-8.55468 29.8772 2 -2 -3 -10 48.6522 41.7307 2 -2 3 -11 33.1328 17.0243 2 -2 -3 -11 24.2745 30.1519 2 -2 -3 -12 143.766 61.2373 3 -2 3 -12 161.730 65.2133 2 -2 -3 -12 99.5935 43.3106 2 2 -3 12 97.8144 49.6521 2 -2 -3 -13 576.836 113.966 3 2 3 13 671.099 122.829 4 2 -3 13 626.327 123.317 2 -2 3 -13 566.072 117.842 2 -2 -3 -13 571.212 97.0996 2 -2 -3 -14 124.461 57.3632 3 2 3 14 63.4116 39.2943 4 -2 3 -14 138.915 55.5541 2 -2 -3 -14 84.7612 29.6827 2 2 3 15 37.8545 11.1918 4 -2 -3 -15 32.7528 32.9556 3 -2 3 -15 40.1994 29.7964 2 -2 -3 -15 46.7627 12.1141 2 -2 -3 -16 249.907 81.5516 3 2 3 16 380.416 103.554 4 -2 3 -16 256.603 81.9296 2 -2 -3 -16 265.614 80.7494 2 2 3 17 18.2400 22.3341 4 -2 -3 -17 84.4451 52.3699 3 -2 -3 -17 70.7096 34.1568 2 -2 3 -17 63.1347 38.6346 2 -2 -3 -18 372.973 104.878 3 -2 -3 -18 443.939 108.387 2 -2 3 -18 356.322 114.204 2 -2 -3 -19 375.287 113.178 3 -2 3 -19 265.936 95.6059 2 -2 -3 -19 289.509 82.6358 2 -2 -3 -20 36.0811 45.2066 3 -2 -3 -20 38.9997 27.8264 2 -2 3 -20-38.0157 39.7071 2 -2 -3 -21 37.8780 36.7115 3 -2 3 -21 4.42614 16.2070 2 -2 -3 -21 43.1063 35.2310 2 -2 -3 -22 111.911 75.5000 3 -2 3 -22 36.7325 39.8104 2 -2 -3 -22 9.16774 17.2353 2 -2 -3 -23 68.0109 59.4386 3 -2 -3 -23-14.9688 8.10164 2 -2 3 -23 41.7488 57.6950 2 -2 3 -24 75.9716 68.6070 2 -2 -4 25 72.0620 18.5022 4 2 -4 -25 120.599 71.9461 3 2 -4 -24 96.1864 78.3086 3 -2 -4 24-13.7525 27.3282 4 -2 -4 23-99.6694 68.2997 4 2 -4 -23 106.676 42.4039 3 -2 -4 22 72.1872 37.6095 4 2 -4 -22 126.031 68.8668 3 2 -4 -21 62.8207 65.6871 3 -2 -4 21 100.119 55.5753 4 2 -4 -20 121.119 74.0598 3 -2 -4 20 15.0012 39.6156 4 -2 -4 19-53.4802 53.9096 4 2 -4 -19 28.3699 11.8093 3 2 -4 -18 261.319 105.258 3 -2 -4 18 360.522 90.5795 3 -2 -4 18 241.102 98.1327 4 -2 4 17 277.361 71.0941 4 -2 -4 17 329.271 114.678 4 2 -4 -17 387.914 116.370 3 -2 -4 17 373.831 97.4084 3 2 -4 -16-1.31541 9.75140 3 -2 -4 16-39.2181 47.5034 4 -2 4 16 57.0526 25.0270 4 -2 -4 16 34.1096 30.2045 3 -2 -4 15 86.6717 45.3935 3 -2 4 15 7.49623 21.2197 4 2 -4 -15 27.2458 25.7992 3 -2 -4 15 29.6338 6.06426 4 2 -4 -14 91.0935 41.1630 3 -2 4 14 137.525 42.3580 4 -2 -4 14 117.227 37.1380 4 -2 -4 14 196.188 61.9638 3 -2 4 14 353.269 100.524 1 -2 4 13 1031.35 91.7868 4 2 -4 -13 1020.72 175.020 3 -2 -4 13 1119.30 177.352 4 -2 -4 13 996.179 132.024 3 -2 4 13 1199.40 179.806 1 2 -4 -12 130.267 57.7380 3 -2 4 12 142.834 33.8373 4 -2 -4 12 150.551 65.0414 4 -2 -4 12 178.149 55.7615 3 -2 -4 12 156.521 64.6489 2 -2 4 12 186.618 77.9188 1 2 -4 -11-9.12005 31.5117 3 -2 4 11 14.3546 12.3180 4 -2 -4 11-24.6267 40.1236 4 -2 -4 11 14.9602 25.7140 3 -2 4 11 92.9013 69.4138 1 -2 -4 11 17.7952 21.3598 2 -2 -4 10 25.1410 26.4154 4 2 -4 -10 38.9920 13.4255 3 -2 4 10 2.30049 7.31436 4 -2 4 10 23.2481 41.1749 1 -2 -4 10 45.0638 33.0302 3 -2 -4 10 18.4823 21.2193 2 -2 -4 9 847.944 114.971 3 -2 -4 9 1107.77 154.450 4 2 -4 -9 790.414 134.784 3 -2 4 9 697.060 120.123 1 2 -4 -8 1941.75 200.447 3 -2 -4 8 1820.92 195.670 4 -2 -4 8 1846.91 158.728 3 -2 -4 7 79.8881 42.4243 4 2 -4 -7 140.609 60.6534 3 -2 -4 7 162.916 43.7329 3 -2 -4 6 1347.81 158.679 4 2 -4 -6 1334.16 162.029 3 -2 -4 6 1252.56 123.759 3 -2 -4 5 2756.92 218.124 4 2 -4 -5 3040.73 226.725 3 2 -4 -5 3067.72 218.152 1 2 -4 -4 2904.61 217.784 3 -2 -4 4 2809.53 213.129 4 2 -4 -4 2766.46 102.183 4 2 -4 -4 2786.96 93.4850 2 2 -4 -4 3002.96 209.340 1 2 -4 -3 1216.96 133.277 3 2 -4 -3 1254.97 81.9927 4 -2 -4 3 1273.29 138.009 4 -2 4 3 1222.62 77.7752 2 2 -4 -3 1230.32 130.480 1 2 -4 -3 1198.89 74.8277 2 -2 -4 2 23.7910 18.8905 4 2 -4 -2 31.9032 22.6468 4 2 -4 -2 95.1601 43.3849 3 -2 4 2 23.3127 19.0865 2 2 -4 -2 62.7776 24.0289 2 2 -4 -1 5.34889 16.4190 3 -2 -4 1-1.90966 17.9808 4 2 -4 -1 9.69021 6.68142 2 -2 4 1 37.3883 20.5940 2 -2 -4 1-6.48426 5.04926 1 2 -4 0 6194.67 268.842 3 -2 -4 0 6053.35 285.192 4 2 -4 0 6166.49 232.441 2 -2 4 0 6060.29 227.538 2 -2 -4 0 5871.50 230.968 1 2 -4 1 1526.65 128.203 3 2 4 1 1596.99 147.718 4 -2 -4 -1 1532.27 146.928 4 2 -4 1 1425.81 121.394 2 2 4 1 1574.10 125.252 1 -2 4 -1 1523.60 120.373 2 2 -4 2 688.414 80.6581 3 -2 -4 -2 736.024 99.0199 4 2 4 2 627.237 89.4709 4 2 -4 2 682.114 89.5887 2 2 4 2 696.747 86.7915 1 -2 4 -2 668.743 86.4635 2 2 -4 3 2339.69 137.856 3 2 4 3 2267.93 173.408 4 -2 -4 -3 2112.45 165.245 4 2 -4 3 2176.47 166.848 2 -2 4 -3 2157.04 163.040 2 2 4 3 2286.33 165.262 1 2 -4 4 1148.88 89.4482 3 -2 -4 -4 1138.15 124.085 4 2 4 4 1127.77 124.976 4 2 -4 4 1174.73 126.887 2 2 4 4 1167.91 122.643 1 -2 4 -4 1110.14 123.034 2 2 -4 5 12.0913 12.3784 3 2 4 5-23.3666 27.9546 4 -2 -4 -5 37.1824 24.9830 4 -2 4 -5-10.1312 19.9633 2 2 4 6 910.360 113.328 4 -2 -4 -6 809.703 112.287 4 2 -4 6 853.532 62.8908 3 -2 4 -6 859.418 119.031 2 -2 -4 -7 166.574 52.4164 4 2 -4 7 183.948 23.0509 3 2 4 7 187.578 47.4403 4 -2 4 -7 170.774 56.2294 2 2 4 8 57.9535 33.6925 4 -2 -4 -8 29.1836 29.0996 4 -2 -4 -8 68.4712 41.7009 2 -2 4 -8 2.62388 27.6634 2 2 4 9 547.358 96.1118 4 -2 -4 -9 522.190 84.3080 2 -2 4 -9 478.610 101.540 2 -2 -4 -10 5.05998 33.4445 2 -2 4 -10-21.2324 34.5269 2 -2 4 -11 901.536 145.432 2 2 -4 11 1049.02 157.179 2 -2 -4 -11 979.041 124.056 2 -2 4 -12 25.6822 23.5337 2 -2 -4 -12 86.0425 39.1036 2 -2 -4 -13 92.0883 57.8522 3 2 4 13 47.8000 34.2478 4 -2 4 -13 7.29483 33.1565 2 -2 -4 -13 32.8827 26.5475 2 2 4 14 177.345 65.9609 4 -2 -4 -14 155.362 75.7790 3 -2 -4 -14 149.203 49.0806 2 -2 4 -14 142.191 64.4290 2 -2 -4 -15 66.4787 46.2358 3 2 4 15 71.3223 50.2378 4 -2 -4 -15 86.8524 47.1666 2 -2 4 -15 173.467 77.0497 2 2 4 16 79.7546 70.4274 4 -2 -4 -16-8.85005 5.93884 3 -2 -4 -16-55.3083 43.1340 2 -2 4 -16-11.6929 16.9489 2 2 4 17 74.4111 43.1432 4 -2 -4 -17 38.7045 40.2852 3 -2 4 -17 29.8883 30.1485 2 -2 -4 -17 197.059 71.5795 2 -2 -4 -18 76.9100 54.2446 3 -2 4 -18 145.375 80.4074 2 -2 -4 -18 58.7059 42.2815 2 -2 -4 -19 287.893 118.735 3 -2 -4 -19 153.464 61.2826 2 -2 4 -19 64.7038 56.1446 2 -2 -4 -20 62.3462 57.2789 3 -2 -4 -20 0.56742 35.6058 2 -2 4 -20 20.8270 34.5996 2 -2 -4 -21 38.3048 35.4544 3 -2 -4 -21 18.8331 35.9850 2 -2 4 -21 60.0220 64.2190 2 -2 -4 -22 40.4650 45.4771 3 -2 4 -22 5.78741 70.0254 2 -2 -4 -22 157.065 71.4310 2 -2 -4 -23 56.2220 61.6626 3 -2 4 -23 20.2138 48.3518 2 -2 4 -24 74.3249 69.3901 2 2 -5 -25 76.8931 64.7822 3 2 -5 -24-57.0209 58.1877 3 -2 -5 24 65.3363 78.6764 4 -2 -5 23-5.51174 13.8646 4 -2 5 23 5.71607 73.9270 1 2 -5 -22-9.69023 7.79996 3 -2 -5 22 26.8923 57.3791 4 2 -5 -21 132.159 95.2632 3 -2 -5 21 2.43054 31.5523 4 -2 5 21 101.341 107.266 1 -2 -5 20 257.083 109.025 4 2 -5 -20 231.119 99.2296 3 -2 5 20 270.758 130.568 1 2 -5 -19 54.3922 79.7973 3 -2 -5 19 26.5375 24.6185 4 -2 5 19 166.674 109.589 1 2 -5 -18 241.723 101.200 3 -2 -5 18 267.413 102.677 4 -2 5 18 197.602 109.014 1 -2 -5 17 32.8028 36.0433 4 -2 -5 17 97.9073 55.1141 3 2 -5 -17 83.4868 68.5564 3 -2 5 17 21.1937 65.8515 1 -2 -5 16 83.7732 56.7544 4 -2 -5 16 89.9485 42.5059 3 -2 5 16 90.6869 33.0878 4 2 -5 -16 127.173 69.0454 3 -2 5 16 165.830 75.8742 1 2 -5 -15 70.6099 53.7218 3 -2 5 15 27.0344 14.2236 4 -2 -5 15 36.5081 16.7306 3 -2 -5 15 11.8929 12.1675 4 -2 5 15 150.160 95.4281 1 -2 -5 14 829.927 126.496 3 2 -5 -14 879.993 166.889 3 -2 5 14 825.365 74.2259 4 -2 -5 14 782.425 156.935 4 -2 5 14 977.315 176.616 1 -2 -5 13 594.568 138.541 4 2 -5 -13 610.689 142.228 3 -2 5 13 474.354 53.9126 4 -2 -5 13 487.461 92.0432 3 -2 5 13 550.056 121.576 1 2 -5 -12-31.4071 21.5892 3 -2 -5 12 64.6963 36.8657 4 -2 5 12 41.3135 18.5064 4 -2 5 12 78.6945 64.6230 1 -2 -5 12-10.7887 9.28274 3 -2 -5 11 1414.90 152.090 3 2 -5 -11 1301.62 190.239 3 -2 -5 11 1287.99 186.451 4 -2 5 11 1088.57 61.5247 4 -2 -5 11 1418.85 192.521 2 -2 5 11 1355.15 192.229 1 -2 -5 10 1574.37 159.397 3 2 -5 -10 1606.91 202.362 3 -2 -5 10 1559.09 203.100 4 -2 -5 10 1527.75 192.453 2 -2 5 10 1798.70 204.850 1 -2 -5 9 293.072 93.7985 4 2 -5 -9 291.828 85.6308 3 -2 -5 9 353.277 73.0994 3 -2 -5 9 362.488 91.5147 2 -2 5 9 285.843 89.7283 1 -2 -5 8 1241.07 170.754 4 -2 -5 8 1097.81 125.014 3 2 -5 -8 1210.37 164.981 3 -2 -5 7 1357.28 138.056 3 -2 -5 7 1402.95 179.276 4 2 -5 -7 1596.26 191.309 3 -2 -5 6 126.267 57.3257 4 2 -5 -6 104.754 52.6432 3 2 -5 -6 75.2246 16.0821 4 2 -5 -5 6.57732 5.28501 4 2 -5 -5-6.09043 14.0071 3 -2 -5 5 43.8630 33.6399 4 2 -5 -5 62.6081 45.4579 1 2 -5 -5-9.81640 8.39772 2 2 -5 -4 1890.61 110.324 4 -2 -5 4 1860.35 188.489 4 2 -5 -4 1942.52 194.230 3 2 -5 -4 2141.72 194.190 1 2 -5 -4 1843.60 100.162 2 2 -5 -3 4036.79 266.535 3 2 -5 -3 4068.84 177.502 4 -2 -5 3 4113.34 272.988 4 2 -5 -3 4071.97 167.393 2 2 -5 -3 3924.69 262.871 1 -2 -5 2 5.31723 23.7216 4 2 -5 -2 42.4314 24.9609 4 2 -5 -2-3.11022 10.3357 3 -2 5 2 26.5433 17.1346 2 2 -5 -2 44.0766 23.9431 2 2 -5 -2-5.02374 23.7234 1 -2 -5 2 8.95479 15.6350 1 2 -5 -1 397.603 65.8901 4 -2 -5 1 474.079 89.6024 4 2 -5 -1 503.899 85.6673 3 -2 5 1 410.196 61.7010 2 -2 -5 1 362.060 60.8714 1 2 -5 -1 359.056 59.2657 2 2 5 0 249.700 68.3417 4 -2 -5 0 303.962 76.2698 4 2 -5 0 222.951 55.2411 3 2 -5 0 208.454 48.6386 2 -2 5 0 224.987 51.7533 2 -2 -5 0 220.667 48.1370 1 2 5 1 311.345 73.3792 4 -2 -5 -1 330.640 79.2076 4 2 -5 1 335.985 69.4784 3 -2 -5 -1 279.643 60.6002 1 -2 5 -1 303.235 62.0166 2 2 -5 1 341.054 67.1920 2 -2 -5 -2 327.846 71.4045 4 2 -5 2 475.835 75.7178 3 2 5 2 404.221 79.0678 4 2 -5 2 395.957 75.4666 2 2 5 2 408.389 74.6513 1 -2 5 -2 412.422 74.8949 2 2 -5 3 1573.38 132.699 3 2 5 3 1408.04 147.784 4 -2 -5 -3 1514.48 153.234 4 2 5 3 1532.03 149.621 1 -2 5 -3 1475.77 143.989 2 2 -5 3 1579.09 154.439 2 2 5 4 102.094 43.2793 4 2 -5 4 90.5009 27.2400 3 -2 -5 -4 135.915 44.9448 4 -2 5 -4 98.2176 40.6068 2 2 -5 4 185.764 61.2203 2 2 5 4 131.775 42.3652 1 2 5 5 96.2282 43.2105 4 2 -5 5 65.9488 22.8738 3 -2 -5 -5 125.805 49.3788 4 2 5 5 60.4185 48.3514 1 2 -5 5 166.005 61.9688 2 -2 5 -5 64.0255 38.6459 2 2 5 6 454.807 86.6882 4 -2 -5 -6 442.662 86.5419 4 2 -5 6 375.319 53.3218 3 2 5 6 432.009 94.4400 1 -2 5 -6 375.208 83.9058 2 2 -5 6 502.812 100.665 2 2 5 7 69.0811 47.2217 4 2 -5 7 65.0406 30.4534 3 -2 -5 -7 57.3231 33.9593 4 -2 5 -7 102.493 53.6621 2 2 5 7 82.5690 51.7443 1 2 -5 8 328.537 40.8020 3 2 5 8 290.943 63.8260 4 -2 -5 -8 320.073 82.4231 4 -2 5 -8 263.865 77.2132 2 -2 -5 -9 759.749 121.055 4 -2 -5 -9 720.389 108.974 2 -2 5 -9 774.831 131.264 2 2 -5 9 667.448 122.748 2 2 -5 10 4.49951 27.1460 2 -2 -5 -10 66.9713 40.2302 2 -2 5 -10 27.0431 47.6620 2 -2 -5 -11 122.417 41.4081 2 -2 5 -11 57.8646 36.3429 2 2 5 12 190.740 65.0543 4 -2 -5 -12 313.183 79.1407 2 -2 5 -12 277.357 88.6876 2 2 5 13 636.154 120.060 4 -2 -5 -13 450.791 117.379 3 -2 -5 -13 711.035 115.813 2 -2 5 -13 484.577 117.851 2 -2 -5 -14 407.875 121.842 3 2 5 14 458.620 108.140 4 -2 -5 -14 511.470 95.2036 2 -2 5 -14 360.892 103.377 2 -2 -5 -15 49.4952 43.6573 3 2 5 15 44.6987 30.1835 4 -2 -5 -15 36.1142 26.1460 2 -2 5 -15 15.0944 33.3618 2 -2 -5 -16 68.4125 47.1025 3 2 5 16 42.7431 41.3084 4 -2 -5 -16-1.63369 24.2461 2 -2 5 -16 6.53102 17.9673 2 -2 -5 -17 0.22509 19.6740 3 2 5 17 53.7310 38.8274 4 -2 -5 -17-40.8196 17.1593 2 -2 5 -17 21.9289 31.8497 2 -2 -5 -18 283.026 93.5677 3 -2 5 -18 397.583 119.272 2 -2 -5 -18 378.044 96.5612 2 -2 -5 -19 1.45118 14.5020 3 -2 5 -19 100.812 67.2366 2 -2 -5 -19 79.0790 46.2057 2 -2 -5 -20-2.12484 23.7979 3 -2 -5 -20-7.47132 21.8253 2 -2 5 -20 38.9253 45.6612 2 -2 -5 -21 26.5387 41.9804 3 -2 5 -21 91.7803 66.1306 2 -2 -5 -22 30.4693 10.8494 3 -2 5 -22 81.2242 64.4000 2 -2 -5 -23 39.9361 33.6774 3 -2 5 -23 7.85230 26.2470 2 -2 -5 -24 86.1929 101.803 3 2 -6 -23 163.922 88.3959 3 -2 -6 22-32.8115 18.2341 4 2 -6 -22 9.22888 28.0063 3 -2 6 22 18.5779 66.5575 1 -2 -6 21 77.8592 88.0794 4 2 -6 -21 233.533 117.191 3 -2 6 21 116.415 103.315 1 2 -6 -20 8.15668 55.1197 3 -2 -6 20-58.5176 46.1449 4 -2 6 20 69.8619 81.2299 1 2 -6 -19 51.1929 45.6758 3 -2 -6 19 26.4567 43.3402 4 -2 6 19-11.4187 33.8744 1 2 -6 -18-14.9481 24.5579 3 -2 -6 18 97.6112 65.5957 4 -2 6 18 22.2824 71.7622 1 -2 -6 17 15.7849 16.6966 4 2 -6 -17 6.35252 19.8182 3 -2 6 17 9.60621 25.3255 1 -2 -6 16 18.0582 23.9108 4 -2 -6 16 5.69263 4.17958 3 2 -6 -16-84.1058 56.0327 3 -2 6 16 99.2652 88.5624 1 -2 -6 15 60.5486 51.7499 4 2 -6 -15 109.526 66.2673 3 -2 -6 15 75.2555 39.4690 3 -2 6 15 45.1157 13.9194 4 -2 6 15 40.5469 64.1257 1 -2 -6 14 15.5019 30.5333 4 -2 6 14 43.1040 13.8063 4 -2 6 14 66.9987 71.9840 1 -2 -6 14 44.9586 26.4186 3 -2 -6 13-16.9202 42.2500 4 2 -6 -13 46.6896 29.8747 3 -2 6 13 32.1729 41.3454 1 -2 -6 13 27.1354 26.8867 3 2 -6 -12 100.234 48.6618 3 -2 -6 12 40.3454 37.1393 4 -2 6 12 174.863 81.2815 1 -2 -6 12 104.628 41.1115 3 2 -6 -11 16.8979 32.4241 3 -2 -6 11 42.1923 44.6256 4 -2 6 11-9.46070 25.5310 1 -2 -6 11 38.0287 34.1286 3 2 -6 -10 85.6664 49.8401 3 -2 -6 10 96.7352 42.1955 4 -2 6 10 122.030 63.8980 1 -2 -6 10 149.274 53.0935 3 2 -6 -9 418.638 109.074 3 -2 -6 9 391.140 105.456 4 -2 6 9 414.195 103.444 1 -2 -6 9 383.174 76.9042 3 -2 -6 8 155.843 64.1239 4 2 -6 -8 90.2966 54.6138 3 -2 -6 8 139.063 42.3933 3 -2 6 8 106.397 50.3041 1 -2 -6 8 152.916 67.9046 2 -2 -6 7 239.046 77.4656 4 2 -6 -7 209.154 33.1208 4 2 -6 -7 184.940 75.8221 3 -2 -6 7 174.852 67.2281 2 2 -6 -6 354.243 92.4252 3 -2 -6 6 343.640 98.4424 4 2 -6 -6 375.341 50.0759 4 2 -6 -6 328.181 38.2847 2 -2 -6 5 207.049 72.5623 4 2 -6 -5 124.618 32.8120 4 2 -6 -5 153.703 64.2229 3 2 -6 -5 123.254 28.7471 2 2 -6 -5 207.679 72.8714 1 -2 -6 4 7.18694 10.7018 4 2 -6 -4 30.7165 26.4064 4 2 -6 -4-8.18337 14.8826 3 -2 -6 4-17.6265 26.5486 2 2 -6 -4 0.13473 28.1052 1 2 -6 -4 29.6928 23.6190 2 -2 -6 3 1612.52 182.693 4 2 -6 -3 1564.28 179.890 3 2 6 -3 535.323 110.285 4 2 -6 -3 1556.40 127.358 4 -2 -6 3 1665.96 174.676 2 2 -6 -3 1579.84 121.907 2 2 -6 -3 1753.43 191.788 1 -2 -6 2 593.743 106.419 4 2 -6 -2 608.307 85.9582 4 2 -6 -2 593.585 103.694 3 2 6 -2-13.5304 25.7454 4 -2 -6 2 601.640 91.3306 1 2 -6 -2 677.789 85.6482 2 -2 -6 2 774.363 117.001 2 2 -6 -2 667.288 111.829 1 -2 -6 1 562.214 98.8203 4 2 -6 -1 586.624 86.0232 4 2 -6 -1 517.279 95.6499 3 -2 -6 1 539.124 96.2053 2 2 -6 -1 574.851 85.9115 2 2 -6 -1 625.912 109.317 1 -2 6 1 498.870 77.7702 2 -2 -6 1 528.608 87.1259 1 2 -6 0 3396.21 240.968 3 -2 -6 0 3462.72 253.716 4 2 -6 0 3301.14 214.983 4 2 -6 0 3247.87 210.620 2 -2 -6 0 3271.54 219.823 1 -2 6 0 3103.07 201.621 2 2 -6 1 2021.28 178.433 4 2 -6 1 2100.98 184.431 3 -2 -6 -1 2000.99 193.595 4 2 -6 1 1964.76 172.469 2 -2 6 -1 1956.00 166.494 2 -2 -6 -1 1934.69 173.196 1 2 -6 2 765.318 109.280 3 -2 -6 -2 745.697 116.318 4 2 -6 2 737.448 109.750 2 -2 6 -2 779.391 109.990 2 2 -6 3 539.386 85.3845 3 -2 -6 -3 547.373 96.4553 4 2 6 3 474.663 90.1774 1 2 -6 3 519.863 102.715 2 -2 6 -3 451.061 88.1118 2 2 -6 4 624.375 91.1211 3 -2 -6 -4 639.393 107.092 4 2 -6 4 720.712 117.746 2 -2 6 -4 651.654 107.032 2 2 6 4 695.784 108.989 1 2 -6 5 486.357 73.4745 3 -2 -6 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675.705 118.736 2 2 -7 4 32.0009 22.3673 3 -2 -7 -4 35.5524 26.8297 4 2 7 4 4.00884 3.83558 4 -2 7 -4 119.746 53.3451 2 2 -7 4 59.9784 41.5634 2 2 -7 5 270.174 63.0005 3 -2 -7 -5 251.552 72.2688 4 2 -7 5 277.461 87.3294 2 2 7 5 175.094 64.9426 1 -2 7 -5 248.166 71.7793 2 2 -7 6 226.690 58.3383 3 -2 -7 -6 258.454 75.1423 4 2 -7 6 261.070 85.0146 2 2 7 6 227.780 74.3267 1 -2 7 -6 178.188 66.6580 2 2 -7 7 768.077 98.1926 3 2 7 7 248.425 69.9347 4 -2 -7 -7 598.870 115.650 4 2 -7 7 724.429 138.253 2 -2 7 -7 683.652 127.312 2 2 7 7 656.261 127.105 1 2 7 8 19.0116 22.2921 4 2 -7 8 23.1319 10.0531 3 -2 -7 -8 72.8846 52.5677 4 -2 7 -8 104.963 58.1325 2 2 7 8 59.0131 23.9500 1 2 7 9 540.029 101.987 4 2 -7 9 495.098 71.1268 3 -2 -7 -9 512.737 106.962 4 2 7 9 505.043 118.195 1 -2 7 -9 474.308 117.480 2 2 7 10 395.339 91.7265 4 2 -7 10 328.571 53.1220 3 -2 -7 -10 361.130 89.2495 4 2 -7 10 366.148 50.7474 3 2 7 10 427.122 111.546 1 -2 7 -10 385.786 107.786 2 2 -7 11 87.2020 27.5794 3 -2 -7 -11 82.4686 45.5234 4 2 7 11 70.6787 42.2286 4 -2 -7 -11 49.0745 37.4277 2 2 7 11 45.1187 60.3484 1 -2 7 -11 19.3899 32.2348 2 2 -7 11 83.5214 24.4356 3 2 7 12 222.074 70.4202 4 -2 -7 -12 166.559 57.3524 2 2 7 12 131.204 91.6091 1 -2 7 -12 191.335 86.1432 2 -2 -7 -13 46.2592 18.3676 3 2 7 13 60.6654 47.1784 4 2 7 13 91.1812 61.6487 1 -2 -7 -13 74.8215 48.1318 2 -2 7 -13 49.2012 47.6558 2 -2 -7 -14-42.1290 41.6779 3 2 7 14 64.5334 46.0293 4 -2 -7 -14 88.3861 49.6398 2 2 7 14 69.2618 88.2153 1 -2 7 -14 35.4676 33.6873 2 -2 -7 -15 89.4302 71.7517 3 2 7 15 210.593 112.969 1 -2 -7 -15 209.972 65.1234 2 -2 7 -15 145.826 84.0439 2 -2 -7 -16-21.4379 31.5703 3 -2 7 -16 150.133 84.3312 2 2 7 16 192.577 108.704 1 -2 -7 -16 48.6491 35.1898 2 -2 -7 -17-19.5554 20.3721 3 -2 7 -17 34.1712 39.4016 2 -2 -7 -17 7.17685 22.8890 2 -2 -7 -18 76.5055 67.9013 3 2 7 18 99.5314 108.508 1 -2 7 -18 35.1771 44.9251 2 -2 -7 -19 122.492 89.0640 3 -2 7 -19 45.7859 58.5768 2 2 7 19 29.8450 80.2976 1 -2 -7 -20-40.7625 10.3901 3 2 7 20 70.9734 98.0963 1 -2 7 -20 139.662 61.2290 2 -2 -7 -21 0.95999 36.0021 3 -2 -7 -22-139.155 83.0063 3 -2 -7 -23-48.0289 59.4727 3 2 -8 -20 70.0101 92.2231 3 -2 -8 19 44.6495 50.7262 4 2 -8 -19 61.1366 48.2544 3 -2 8 19-9.94875 38.7066 1 2 -8 -18-2.91710 11.9010 3 -2 8 18-28.4831 34.2082 1 -2 -8 17-32.7628 48.9230 4 2 -8 -17 56.1838 69.3085 3 -2 8 17 27.1794 74.1824 1 -2 -8 16 13.2339 31.0183 4 2 -8 -16 58.1014 71.0093 3 -2 8 16 33.6840 66.4733 1 2 -8 -15 56.4526 48.5128 3 -2 -8 15 69.8315 84.0089 4 -2 8 15 16.4899 43.2465 1 2 -8 -14-26.1783 44.6373 3 -2 -8 14-19.6337 18.7124 4 -2 8 14-96.7828 60.6859 1 2 -8 -13 95.5987 56.9089 3 -2 -8 13 239.655 112.372 4 -2 8 13 8.75710 21.6744 1 -2 -8 13 153.466 59.4413 3 2 -8 -12 61.3707 39.8991 3 -2 -8 12 49.0615 42.9451 4 -2 -8 12 89.3258 58.2559 3 -2 8 12-58.5778 66.1602 1 2 -8 -11 75.5224 63.5298 3 -2 -8 11 61.7519 49.3154 4 -2 8 11-6.73627 14.7996 1 -2 -8 11 28.5894 17.1145 3 2 -8 -10 50.3778 32.5286 3 -2 -8 10 129.924 74.7677 4 -2 -8 10 115.719 51.4679 3 -2 -8 9 104.184 76.1940 4 2 -8 -9 182.966 70.9744 3 -2 -8 9 86.5324 39.7468 3 -2 -8 8 3.67680 16.0589 4 2 -8 -8-53.7387 41.1535 3 2 -8 -8 3.70050 12.3461 4 2 -8 -8-2.97197 10.2273 2 2 -8 -7-1.63518 17.0860 4 2 -8 -7 39.0254 31.4830 3 -2 -8 7-6.07379 12.2652 4 2 -8 -7 26.9872 17.7197 2 -2 -8 6 1188.01 189.944 4 2 -8 -6 1325.64 125.934 4 2 -8 -6 1256.23 199.715 3 2 -8 -6 1188.57 105.342 2 -2 -8 5 58.7906 28.3836 4 2 -8 -5 109.622 43.2035 4 2 -8 -5 71.8870 24.1268 3 2 -8 -5 108.473 36.2463 2 -2 -8 4 60.2815 20.9808 4 2 -8 -4 177.671 60.6570 4 2 -8 -4 234.334 91.1707 3 2 -8 -4 66.4143 36.7086 2 -2 -8 4 70.6840 36.3505 1 -2 -8 3 462.109 102.868 4 2 -8 -3 502.496 109.751 3 2 -8 -3 485.114 84.9291 4 2 -8 -3 529.527 88.0188 2 -2 -8 3 508.698 101.591 1 -2 -8 3 524.006 109.194 2 2 -8 -2 59.5408 43.7381 4 -2 -8 2 30.2930 29.2133 4 2 -8 -2-3.76061 17.1886 3 -2 -8 2 61.3496 47.9831 1 -2 -8 2 56.7620 45.3827 2 2 -8 -2 52.3181 38.8894 2 2 -8 -1 652.378 107.158 4 -2 -8 1 614.769 128.228 4 2 -8 -1 629.424 122.670 3 2 8 -1 745.685 141.497 4 -2 -8 1 579.018 113.648 2 -2 -8 1 620.197 122.068 1 2 -8 -1 639.670 106.131 2 2 -8 0 175.061 66.4967 4 -2 -8 0 262.882 83.2512 4 2 -8 0 184.765 64.7502 3 2 8 0 251.079 80.3657 4 -2 -8 0 279.945 85.0104 2 -2 -8 0 316.096 95.9870 1 2 -8 0 191.990 64.3684 2 2 -8 1 2608.33 242.414 3 -2 -8 -1 2630.98 252.123 4 2 -8 1 2471.11 228.066 4 2 8 1 2812.96 266.210 4 -2 -8 -1 2800.23 242.862 2 -2 -8 -1 2508.48 238.075 1 2 -8 1 2611.30 229.893 2 -2 -8 -2 491.662 112.785 4 2 -8 2 484.052 102.695 3 2 -8 2 500.043 105.168 4 2 8 2 617.792 123.956 4 -2 -8 -2 505.077 101.828 2 -2 8 -2 467.899 104.188 2 2 -8 2 477.740 104.598 2 -2 -8 -3 514.619 107.746 4 2 -8 3 492.073 96.8378 3 2 -8 3 471.391 103.493 4 2 8 3 592.525 126.681 4 2 -8 3 524.205 119.895 2 -2 8 -3 525.982 108.666 2 2 -8 4 92.6195 45.8018 3 2 -8 4 22.5666 38.4370 4 -2 -8 -4 5.09100 24.4643 4 2 8 4 31.1635 44.5223 4 -2 8 -4 11.1786 13.7120 2 2 -8 4 13.7007 19.7363 2 -2 -8 -5 1655.04 193.829 4 2 -8 5 1729.89 174.532 3 2 -8 5 1584.71 210.419 4 2 8 5 1565.68 189.531 4 2 -8 5 1506.02 200.444 2 -2 8 -5 1558.23 192.895 2 2 -8 6 280.631 68.3678 3 -2 -8 -6 359.931 93.4631 4 2 -8 6 286.542 77.3354 4 2 8 6 349.069 93.7012 4 -2 8 -6 376.184 99.3800 2 2 -8 7 566.028 94.1807 3 -2 -8 -7 486.761 111.113 4 2 8 7 592.692 112.812 4 -2 8 -7 444.738 108.716 2 2 8 7 449.222 105.083 1 2 8 8-2.08110 17.7328 4 2 -8 8 7.04104 16.0999 3 2 8 8-14.3056 13.8348 1 -2 8 -8 6.32566 17.3826 2 2 -8 9-2.55595 10.2264 3 -2 -8 -9 13.0323 40.8487 4 2 8 9-5.18767 34.9428 4 2 8 9 29.6519 25.1062 1 -2 8 -9 4.33010 26.1229 2 -2 -8 -10 5.19521 38.5813 4 2 -8 10 1.69488 2.25831 3 2 8 10 0.98290 19.8471 4 -2 8 -10 56.6944 49.1906 2 2 8 10 44.2387 47.5764 1 -2 -8 -11 237.993 82.7981 4 2 8 11 325.624 85.9302 4 2 -8 11 332.793 56.1620 3 -2 8 -11 341.811 106.405 2 2 8 11 214.997 86.5173 1 2 -8 11 250.101 43.4278 3 2 8 12 177.270 62.5445 4 2 -8 12 169.201 35.6145 3 -2 -8 -12 243.100 74.9811 2 2 8 12 107.987 63.7754 1 2 -8 12 158.165 33.4780 3 -2 8 -12 131.882 60.7965 2 2 8 13 58.4785 47.6690 4 -2 -8 -13 62.6581 62.0353 3 2 8 13 25.1109 45.8857 1 -2 8 -13 112.891 58.2963 2 -2 -8 -13 109.249 54.9749 2 -2 -8 -14-22.2839 36.1868 3 2 8 14 40.2659 71.1796 1 -2 8 -14 59.3051 42.8417 2 -2 -8 -14 67.6549 46.0231 2 -2 -8 -15 52.6921 42.8815 3 -2 8 -15 80.1855 59.3539 2 2 8 15 119.256 98.0862 1 -2 -8 -15 162.178 58.7995 2 -2 -8 -16 148.236 74.5239 3 -2 8 -16 143.340 77.1071 2 2 8 16 218.293 108.092 1 -2 -8 -17 22.9679 50.4256 3 -2 8 -17 19.0936 58.2075 2 2 8 17 49.2270 73.5282 1 -2 -8 -18 105.711 72.2711 3 2 8 18 73.9395 101.069 1 -2 8 -18 87.5835 67.5922 2 -2 -8 -19 151.461 78.9183 3 -2 8 -19 106.585 87.1942 2 2 8 19 60.1864 98.1103 1 -2 -8 -20 35.7644 6.59150 3 -2 -8 -21-9.48452 25.2530 3 -2 -9 18-25.3512 48.8078 4 2 -9 -18 9.17702 18.3281 3 -2 9 18 25.0234 28.1439 1 2 -9 -17 45.8222 57.3856 3 -2 -9 17 5.09403 89.9178 4 -2 9 17-90.9119 65.8521 1 -2 -9 16 126.350 118.849 4 2 -9 -16 10.3687 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212.865 67.5507 2 3 2 12 230.274 73.2416 4 -3 2 -12 169.256 64.0481 2 3 -2 12 234.618 86.0825 2 -3 -2 -12 176.460 58.3626 2 -3 -2 -13 1320.77 158.713 3 3 2 13 1341.40 193.383 4 -3 2 -13 1238.64 179.925 2 3 -2 13 1384.70 194.626 2 -3 -2 -13 1150.92 147.718 2 3 2 14 68.7561 51.7338 4 -3 -2 -14-25.9797 36.8078 3 -3 2 -14 29.3083 42.3167 2 -3 2 -14 17.8121 10.1677 3 -3 -2 -14-54.6895 31.9738 2 3 2 15 37.0966 64.1924 4 -3 -2 -15 67.2238 30.5227 3 -3 -2 -15-32.1116 39.3947 2 -3 2 -15 18.2505 12.8108 3 -3 2 -15-23.5039 21.5749 2 -3 -2 -16 100.810 50.4760 3 -3 2 -16 107.329 54.3560 2 -3 2 -16 87.0567 19.5332 3 -3 -2 -16 93.0402 38.1599 2 -3 -2 -17 400.411 86.7138 3 -3 2 -17 316.443 37.0145 3 -3 2 -17 428.193 108.459 2 -3 -2 -17 421.228 109.024 2 -3 -2 -18-27.0075 33.9063 3 -3 -2 -18 22.5757 35.9807 2 -3 2 -18 23.7985 12.8872 3 -3 2 -18-19.3557 34.6469 2 -3 -2 -19 138.384 60.1774 3 -3 2 -19 19.3452 13.3937 2 -3 -2 -19 81.4660 51.3022 2 -3 -2 -20-9.98181 28.2526 3 -3 -2 -20-20.6607 19.1303 2 -3 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3 -3 6 -15 217.763 89.6582 2 -3 -6 -15 243.338 76.9075 2 -3 -6 -16-15.3065 30.1404 3 -3 -6 -16 12.5061 18.0457 2 -3 6 -16 22.9796 24.2098 2 -3 -6 -17 13.3227 27.7827 3 -3 -6 -17 10.2683 33.7198 2 -3 6 -17 9.01853 19.2701 2 -3 -6 -18 13.5879 27.3055 3 -3 -6 -18 37.0916 16.4750 2 -3 6 -18 79.6641 53.1586 2 -3 -6 -19 66.6197 66.1619 3 -3 6 -19 225.168 99.3429 2 -3 -6 -19 142.530 60.7844 2 -3 -6 -20-26.9394 30.4918 3 -3 6 -20 144.899 88.6007 2 -3 -6 -21-24.1013 40.7547 3 -3 6 -21 122.152 81.5123 2 -3 -6 -22 24.1707 12.6517 3 -3 -6 -23 264.754 114.515 3 -3 -7 21 127.524 78.8285 4 3 -7 -21 111.793 99.8522 3 -3 7 21 23.9583 53.3172 1 -3 -7 20 103.249 91.3562 4 3 -7 -20 156.281 119.091 3 -3 7 20 30.9620 35.0449 1 -3 -7 19 100.356 82.7230 4 3 -7 -19 69.7397 69.8435 3 -3 7 19 60.8890 81.6077 1 -3 -7 18 117.585 82.1694 4 3 -7 -18 93.8700 93.7212 3 -3 7 18 127.295 74.2730 1 -3 -7 17 146.009 99.8520 4 3 -7 -17 150.205 88.8194 3 -3 7 17 68.7846 78.7224 1 3 -7 -16 168.999 97.1922 3 -3 -7 16 144.787 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1141.28 175.400 2 -3 8 -4 1077.80 153.655 2 -3 -8 -5 1153.36 173.786 4 3 -8 5 1191.83 142.522 3 3 8 5 1276.56 182.441 4 -3 8 -5 963.074 156.862 2 3 -8 5 1001.26 162.044 2 -3 -8 -6 1007.99 165.944 4 3 -8 6 1038.22 129.049 3 3 8 6 1028.85 154.665 4 3 8 6 814.439 143.481 1 -3 8 -6 841.235 148.843 2 3 8 7 34.9649 32.3380 4 -3 -8 -7 44.8621 35.4269 4 3 -8 7 40.3437 20.1576 3 3 8 7 3.06941 13.3199 1 -3 8 -7 60.0830 39.1728 2 3 8 8 249.842 80.1360 4 3 -8 8 298.365 61.4437 3 -3 -8 -8 337.731 108.191 4 3 8 8 332.613 90.5431 1 -3 8 -8 182.687 67.8435 2 3 -8 9 583.553 81.5269 3 3 8 9 654.859 129.859 4 -3 -8 -9 598.343 129.527 4 3 8 9 557.211 131.724 1 -3 8 -9 615.960 134.268 2 3 8 10 616.818 128.339 4 3 -8 10 534.819 66.4136 3 -3 -8 -10 466.793 113.010 4 -3 8 -10 519.491 130.812 2 3 8 10 443.382 112.162 1 3 8 11 59.6019 51.4795 4 -3 -8 -11 5.08832 19.0196 4 3 -8 11 39.7002 15.6983 3 3 -8 11 31.0536 13.0561 3 -3 8 -11 90.7708 66.4973 2 3 8 11 22.3530 42.4881 1 -3 -8 -12 23.0051 52.8615 4 -3 -8 -12 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235.675 2 -4 3 -9 2516.99 235.754 2 4 3 10 27.2800 31.9076 4 -4 3 -10 74.1403 48.0947 2 4 -3 10 104.711 69.0473 2 -4 -3 -10 46.8886 32.6196 2 4 3 11 399.158 100.693 4 -4 3 -11 476.306 113.601 2 -4 -3 -11 416.831 93.0637 2 4 -3 11 578.963 131.398 2 4 3 12 141.022 67.0175 4 -4 3 -12 39.8165 45.4392 2 -4 -3 -12 110.378 56.5294 2 4 3 13 503.620 122.002 4 -4 3 -13 313.582 93.6407 2 -4 -3 -13 350.681 96.1239 2 -4 3 -14 111.722 59.2218 2 -4 -3 -14 138.576 61.3210 2 -4 -3 -15 621.739 123.451 3 -4 3 -15 651.615 142.203 2 -4 -3 -15 597.647 121.221 2 -4 -3 -16-30.0576 35.9219 3 -4 3 -16-5.21929 34.2815 2 -4 -3 -16 16.5197 23.7037 2 -4 -3 -17 44.5706 32.2898 3 -4 -3 -17-27.2124 42.7971 2 -4 3 -17 0.76982 24.3027 2 -4 -3 -18 125.892 64.5253 3 -4 3 -18 136.623 74.6372 2 -4 -3 -18 51.5032 26.5315 2 -4 -3 -19 534.464 125.232 3 -4 3 -19 489.948 137.205 2 -4 -3 -19 512.048 123.564 2 -4 -3 -20 37.4449 27.9074 3 -4 -3 -20 37.0256 44.0087 2 -4 3 -20-3.37840 50.2910 2 -4 -3 -21 32.8494 18.6262 3 -4 -3 -21 41.1407 34.2429 2 -4 3 -21-31.7493 40.0586 2 -4 -3 -22 67.3338 59.9513 2 -4 3 -22 42.2375 62.1539 2 -4 -3 -23 143.496 77.0078 2 -4 3 -23 157.885 94.2858 2 -4 -3 -24 81.8939 80.8285 2 -4 -4 25 69.1682 62.3683 4 -4 -4 24 48.3388 69.4300 4 4 -4 -24 17.2245 41.7829 3 -4 4 24 70.2660 73.8725 1 -4 -4 23 89.6059 72.0028 4 4 -4 -23-21.2138 58.0558 3 -4 4 23-59.2698 16.3706 1 -4 -4 22 87.2087 75.0994 4 4 -4 -22-9.25473 54.7224 3 -4 4 22 124.640 75.0582 1 -4 -4 21 68.6584 64.7430 4 -4 4 21 41.4198 54.1245 1 4 -4 -21 47.7026 56.4029 3 4 -4 -20 160.513 95.7713 3 -4 -4 20 47.9116 56.2820 4 -4 4 20 146.303 98.0985 1 -4 -4 19 36.0379 40.0902 4 4 -4 -19 103.738 66.2174 3 -4 4 19 162.108 87.3647 1 -4 -4 18-10.4466 4.59458 4 4 -4 -18 87.9888 62.9331 3 -4 4 18 77.7374 77.2920 1 -4 -4 17 92.8524 60.6109 4 -4 4 17 108.427 29.8263 4 4 -4 -17 90.8116 65.5820 3 -4 -4 16 186.037 86.3065 4 4 -4 -16 256.390 96.2157 3 -4 4 16 206.385 27.5219 4 -4 -4 16 255.153 79.7238 3 -4 4 16 162.264 24.9831 4 -4 4 16 342.712 111.721 1 -4 -4 15 41.3743 31.9265 4 -4 -4 15 30.0940 38.4509 3 4 -4 -15 35.9568 40.7671 3 -4 4 15 61.2850 57.0486 1 -4 -4 14 102.068 56.6056 4 4 -4 -14-41.7728 40.1308 3 -4 -4 14 59.7355 49.2278 3 -4 4 14 37.6197 22.0854 1 -4 -4 13 415.145 116.973 4 4 -4 -13 563.923 130.645 3 -4 -4 13 538.374 111.683 3 -4 4 13 529.025 115.908 1 -4 -4 12 188.363 78.4954 4 4 -4 -12 191.162 77.5498 3 -4 4 12 151.448 70.0353 1 -4 -4 12 162.372 61.6990 3 -4 -4 11 603.307 115.616 3 4 -4 -11 689.185 141.107 3 -4 -4 11 556.737 130.649 4 -4 -4 11 706.431 130.540 2 -4 4 11 643.298 118.215 1 4 -4 -10 90.1564 60.5587 3 -4 4 10 124.790 66.3582 3 -4 -4 10 99.4303 53.8715 4 -4 4 10 104.793 47.6607 1 -4 -4 10 97.2644 44.6483 3 -4 -4 10 112.768 50.2633 2 -4 -4 9 276.561 74.6059 4 4 -4 -9 357.230 96.2536 3 -4 -4 9 265.331 71.0238 2 -4 -4 9 340.112 87.0965 3 -4 4 9 282.864 73.5024 1 -4 -4 8 342.504 86.6004 4 4 -4 -8 440.326 99.6040 3 -4 -4 8 368.962 94.6059 2 -4 4 8 114.379 45.2189 1 -4 -4 8 390.191 90.6604 3 -4 -4 7 292.832 76.9599 4 4 -4 -7 443.457 101.553 3 4 4 -7 358.666 85.3567 4 -4 -4 7 391.423 87.1072 3 -4 -4 6 278.593 78.1317 4 4 -4 -6 245.887 77.6831 3 4 -4 -6 336.702 84.2308 1 -4 4 6 244.282 26.7194 2 -4 -4 6 255.917 65.6876 3 4 -4 -5 621.934 113.155 3 -4 -4 5 553.323 110.166 4 -4 -4 5 551.145 97.4923 3 -4 4 5 609.667 53.6130 2 4 -4 -5 588.054 101.645 1 -4 -4 4 112.136 46.5465 4 4 -4 -4 85.3006 43.8042 3 4 -4 -4 94.0957 20.2753 4 -4 4 4 141.932 30.2464 2 -4 -4 4 66.9076 26.9225 3 4 -4 -4 95.2355 43.6236 1 -4 -4 4 92.0115 19.7648 1 4 -4 -3 4378.68 176.180 4 4 -4 -3 4244.26 269.643 3 -4 -4 3 4371.74 290.376 4 -4 4 3 4477.66 183.320 2 4 -4 -3 4550.56 274.869 1 -4 -4 3 4200.88 153.622 1 -4 4 2 2427.83 204.073 3 4 -4 -2 2506.69 201.312 3 -4 -4 2 2393.60 213.233 4 4 -4 -2 2239.11 154.780 2 -4 4 2 2374.72 145.654 2 -4 4 1 4619.19 267.252 3 4 -4 -1 4611.63 260.936 3 -4 -4 1 4649.81 296.137 4 4 -4 -1 4441.43 222.942 2 -4 4 1 4828.66 220.995 2 -4 4 0 738.952 101.743 3 4 -4 0 713.389 101.176 3 -4 -4 0 669.375 109.656 4 4 -4 0 684.099 94.6129 2 -4 4 0 720.870 91.5465 2 4 4 0 611.934 70.0115 1 -4 4 -1 3615.46 215.492 3 4 -4 1 3755.49 212.200 3 -4 -4 -1 3675.13 266.917 4 4 -4 1 3604.48 222.219 2 -4 4 -1 3816.78 220.571 2 4 4 1 3655.63 183.618 1 -4 4 -2 12197.7 377.649 3 4 -4 2 12168.4 365.146 3 -4 -4 -2 12290.9 479.378 4 4 -4 2 12489.4 431.978 2 4 4 2 12709.3 362.480 1 -4 4 -2 12469.7 419.889 2 -4 -4 -3 1077.47 141.922 4 -4 4 -3 1147.75 108.757 3 4 -4 3 1099.37 104.126 3 4 -4 3 1148.90 140.694 2 -4 4 -3 1079.73 129.392 2 -4 -4 -4 7.06752 38.2088 4 4 -4 4-8.84049 20.1103 3 -4 4 -4 7.88947 27.2184 2 4 -4 4 48.2611 36.4218 2 -4 -4 -5 177.729 62.9757 4 4 -4 5 221.692 37.8438 3 -4 4 -5 185.256 67.4867 2 4 -4 5 215.130 73.6216 2 4 -4 6 2281.66 109.148 3 -4 -4 -6 2044.24 210.735 4 4 -4 6 2240.06 209.307 2 -4 4 -6 2218.03 209.935 2 -4 -4 -7 459.779 103.859 4 4 4 7 400.809 83.8582 4 -4 4 -7 423.924 95.5506 2 4 -4 7 474.977 104.379 2 -4 -4 -8 34.0750 20.6144 4 4 4 8 79.0905 48.7680 4 -4 4 -8 16.8453 18.3612 2 4 -4 8 86.4721 57.4853 2 -4 -4 -9 576.961 120.987 4 4 4 9 710.587 132.333 4 4 -4 9 621.196 130.046 2 -4 -4 -9 666.166 124.194 2 -4 4 -9 559.779 119.154 2 4 4 10 61.1516 46.5759 4 -4 4 -10-25.6029 18.7928 2 4 -4 10 30.5322 50.8822 2 4 4 11 29.6907 52.6359 4 -4 4 -11 53.2807 17.3480 2 -4 -4 -11-8.63408 38.9528 2 4 4 12 1130.79 183.180 4 -4 -4 -12 1067.62 156.646 2 -4 4 -12 1078.24 174.521 2 4 4 13 180.415 76.2265 4 -4 4 -13 40.9487 39.1048 2 -4 -4 -13 149.466 86.4083 2 -4 4 -14-23.4327 25.3750 2 -4 -4 -14 43.1380 47.9000 2 -4 4 -15 116.400 66.2444 2 -4 -4 -15 69.4831 45.2835 2 -4 -4 -16 952.418 172.505 3 -4 -4 -16 943.987 156.000 2 -4 4 -16 1086.43 194.927 2 -4 -4 -17 113.929 56.7062 3 -4 4 -17 189.457 77.9005 2 -4 -4 -17 194.699 72.0092 2 -4 -4 -18 26.2733 26.4662 3 -4 -4 -18-18.8716 24.1899 2 -4 4 -18 24.5030 20.4335 2 -4 -4 -19 15.0776 51.9636 3 -4 4 -19-7.96334 46.4183 2 -4 -4 -19-58.1164 59.6630 2 -4 -4 -20 355.757 113.081 3 -4 -4 -20 399.683 117.010 2 -4 4 -20 423.841 138.860 2 -4 -4 -21 132.739 73.6474 3 -4 -4 -21 143.054 60.9291 2 -4 4 -21 175.751 92.8628 2 -4 -4 -22 71.8186 65.1454 3 -4 -4 -22 12.2438 44.1401 2 -4 4 -22 68.9960 75.9266 2 -4 -4 -23 3.05391 10.1653 2 -4 -5 24 153.214 100.117 4 -4 -5 23 64.5015 47.0072 4 4 -5 -23 40.6892 56.7964 3 -4 5 23 87.8221 104.556 1 -4 -5 22 42.3897 47.4940 4 4 -5 -22 95.8446 91.7112 3 -4 5 22 34.0405 78.9997 1 -4 -5 21 46.2056 59.7843 4 4 -5 -21 28.7447 24.3302 3 -4 5 21 115.362 84.9538 1 -4 -5 20 96.8119 55.8687 4 4 -5 -20 69.0019 73.4786 3 -4 5 20 60.7295 73.8642 1 -4 -5 19 50.8303 53.6954 4 4 -5 -19 0.13640 31.2328 3 -4 5 19 108.548 70.6045 1 -4 -5 18 315.656 116.249 4 4 -5 -18 225.733 92.8093 3 -4 5 18 253.042 121.934 1 -4 -5 17 78.8053 72.0455 4 4 -5 -17 157.377 91.2557 3 -4 5 17-34.0645 32.6924 1 -4 -5 16 45.7606 41.0823 4 -4 5 16-1.56069 20.7819 1 -4 -5 15-11.7000 18.3703 4 -4 -5 15 36.3712 35.0360 3 4 -5 -15 21.7830 35.2371 3 -4 5 15 70.4250 53.8789 1 -4 -5 14 227.692 102.941 4 4 -5 -14 355.810 114.213 3 -4 5 14 349.007 106.248 1 -4 -5 14 254.325 79.8660 3 -4 -5 13 103.634 54.5463 4 4 -5 -13 102.626 71.6154 3 -4 -5 13 82.2035 51.5084 3 -4 5 13 6.17945 16.6850 1 -4 -5 12 308.067 94.3859 4 4 -5 -12 341.596 109.205 3 -4 5 12 397.516 102.099 1 -4 -5 12 224.964 71.3527 3 4 -5 -11 132.431 72.5896 3 -4 -5 11 25.6937 47.1256 4 -4 5 11-14.9543 47.9873 1 -4 -5 11 62.2230 27.4943 3 4 -5 -10 81.6732 58.0143 3 -4 -5 10 120.263 59.5841 4 -4 5 10 91.6780 43.0740 1 -4 -5 10 151.375 59.0401 3 4 -5 -9 839.425 151.464 3 -4 -5 9 912.089 143.584 3 -4 -5 9 810.005 140.098 4 -4 -5 9 930.180 153.212 2 -4 -5 8 778.671 137.121 4 -4 -5 8 843.522 128.620 3 -4 5 8 824.198 149.463 3 4 -5 -8 857.577 151.586 3 -4 -5 8 929.238 149.213 2 -4 -5 7 18.2264 10.8127 4 4 -5 -7 2.67571 22.3410 3 -4 5 7-22.6903 33.5539 3 -4 -5 7 4.07821 6.15515 2 -4 -5 7 11.4224 9.28139 3 4 -5 -6 11.4620 36.6196 3 -4 -5 6 2.16254 9.26176 4 -4 5 6-21.5932 39.7406 3 -4 -5 6 35.9318 20.1931 3 4 -5 -6 9.93589 39.8762 1 -4 5 5 1606.26 191.469 3 4 -5 -5 1378.97 175.001 3 -4 -5 5 1353.04 174.670 4 4 -5 -5 1154.78 59.2827 4 4 -5 -5 1194.36 59.7328 4 -4 -5 5 1240.09 150.100 3 4 -5 -5 1455.44 172.411 1 -4 5 5 1343.23 81.9330 2 4 -5 -4 1187.98 159.004 3 -4 5 4 454.028 96.7717 3 -4 -5 4 1370.16 176.072 4 -4 -5 4 1168.71 97.3540 1 4 -5 -4 1308.03 164.009 1 -4 5 4 1224.32 91.2257 2 4 -5 -3 44.4375 34.1306 3 -4 -5 3 44.5995 45.4759 4 4 -5 -3-9.23365 42.8047 1 4 -5 -3 49.3361 29.9101 2 -4 5 3-6.12948 8.50314 2 -4 -5 3 9.67946 9.60632 1 4 -5 -2 726.757 116.243 3 -4 -5 2 702.655 129.700 4 -4 5 2 622.353 80.1319 2 4 -5 -2 602.672 83.8839 2 4 -5 -1 253.665 70.0769 3 -4 -5 1 221.300 87.0823 4 -4 5 1 230.505 51.3951 2 4 -5 -1 163.563 45.9307 2 4 -5 0 21.9745 27.7747 3 -4 -5 0-22.3819 24.8227 4 -4 5 0 9.53722 12.2759 2 4 -5 0 60.2600 42.1170 2 4 -5 1 230.257 56.9985 3 -4 -5 -1 233.788 71.5005 4 -4 5 -1 261.025 59.9755 2 4 -5 1 314.758 72.9399 2 4 5 1 193.117 45.1954 1 4 5 2 18.5725 26.0011 4 4 -5 2-7.45911 18.5633 3 -4 -5 -2 35.7874 34.3587 4 -4 5 -2 21.5314 30.7613 2 4 5 2 53.6239 25.7805 1 4 -5 2-0.30513 14.3833 2 4 5 3 12.1464 25.2182 4 -4 -5 -3 69.7259 63.5967 4 4 -5 3 66.2787 29.7892 3 -4 5 -3 133.465 50.1611 2 4 -5 3 115.576 50.0789 2 4 5 3 92.2768 49.5748 1 -4 -5 -4 797.117 135.488 4 4 -5 4 750.049 90.9134 3 4 5 4 619.621 117.101 4 4 -5 4 659.950 112.779 2 -4 5 -4 733.741 115.108 2 4 5 4 760.955 108.077 1 -4 -5 -5 989.628 142.094 4 4 -5 5 1107.67 100.090 3 4 5 5 1273.33 173.169 4 -4 5 -5 1079.29 145.617 2 4 5 5 1128.34 140.127 1 4 -5 5 950.207 143.037 2 -4 -5 -6 432.823 108.589 4 4 5 6 506.964 110.288 4 4 -5 6 367.486 51.1028 3 -4 5 -6 401.420 93.4006 2 4 -5 6 445.942 101.720 2 4 5 7 168.973 51.7658 4 -4 -5 -7-12.6778 12.5616 4 -4 5 -7 85.8744 46.5847 2 4 -5 7 107.673 57.6631 2 4 -5 7 97.8348 18.7409 3 -4 -5 -8 641.381 134.552 4 4 5 8 620.606 116.644 4 4 -5 8 652.205 128.795 2 -4 5 -8 612.456 119.557 2 -4 -5 -9 137.309 66.8448 4 4 5 9 222.159 78.8505 4 -4 5 -9 155.075 51.6295 2 -4 -5 -10 653.877 138.041 4 4 5 10 1020.00 160.847 4 -4 -5 -10 887.599 145.224 2 -4 5 -10 931.071 157.547 2 4 5 11 298.798 88.0435 4 -4 -5 -11 210.663 71.4072 2 -4 5 -11 272.649 86.8347 2 4 5 12 18.2085 39.7802 4 -4 5 -12 19.9294 39.4051 2 -4 -5 -12 22.1126 13.9226 2 -4 5 -13 568.095 133.777 2 -4 -5 -13 642.178 124.773 2 -4 -5 -14 1008.04 161.520 2 -4 5 -14 842.297 166.120 2 -4 5 -15 62.4010 56.5737 2 -4 -5 -15 184.185 69.6603 2 -4 -5 -16 404.651 127.904 3 -4 5 -16 449.235 127.273 2 -4 -5 -16 476.823 114.387 2 -4 -5 -17 259.621 107.950 3 -4 5 -17 380.664 119.654 2 -4 -5 -17 342.516 100.010 2 -4 -5 -18 206.187 91.2057 3 -4 -5 -18 173.813 66.3993 2 -4 5 -18 356.450 120.563 2 -4 -5 -19-43.4531 31.8172 2 -4 5 -19 6.65772 31.1111 2 -4 5 -20 118.765 88.0103 2 -4 -5 -20 118.163 65.9696 2 -4 -5 -21-25.5881 24.6504 3 -4 -5 -21 33.7887 48.7689 2 -4 5 -21 25.7740 32.8217 2 -4 -5 -22 53.0859 47.9849 3 -4 -6 22 59.9006 107.166 4 4 -6 -22 140.917 88.6773 3 -4 6 22 40.8868 58.1210 1 4 -6 -21 163.023 106.605 3 -4 -6 21 44.6337 58.7019 4 -4 6 21 6.56309 40.4372 1 -4 -6 20 143.413 97.7071 4 4 -6 -20 51.8755 62.4289 3 -4 6 20 61.2625 70.2814 1 -4 -6 19 48.0887 53.8608 4 4 -6 -19 130.959 86.8048 3 -4 6 19 50.3676 65.3378 1 4 -6 -18 277.121 126.167 3 -4 -6 18 159.400 84.3684 4 -4 6 18 202.779 106.298 1 -4 -6 17 61.9080 69.6069 4 4 -6 -17 79.9108 66.0617 3 -4 6 17 31.0713 28.7190 1 -4 -6 16 543.325 145.420 4 4 -6 -16 543.860 152.555 3 -4 6 16 456.031 134.238 1 -4 -6 15 75.2587 35.2838 4 4 -6 -15 118.476 76.8807 3 -4 6 15 44.8704 62.4683 1 -4 -6 14 81.5618 57.4235 4 -4 -6 14 97.9151 46.2016 3 4 -6 -13 78.0022 49.9797 3 -4 -6 13 114.552 71.0858 4 -4 6 13 11.6361 38.3163 1 -4 -6 13-9.22828 13.6793 3 4 -6 -12 830.179 170.618 3 -4 -6 12 855.521 143.882 3 -4 -6 12 795.764 165.487 4 -4 6 12 842.785 155.513 1 4 -6 -11 58.3360 51.0627 3 -4 -6 11 43.5403 15.1919 4 -4 6 11-42.8602 34.5840 1 -4 -6 11 39.3923 45.3462 3 4 -6 -10 304.709 102.543 3 -4 -6 10 208.882 62.9423 4 -4 -6 10 301.521 84.0891 3 -4 -6 9 361.442 101.653 4 4 -6 -9 434.180 118.037 3 -4 -6 9 281.533 78.0989 3 4 -6 -8 821.570 160.611 3 -4 -6 8 719.299 123.570 3 -4 -6 8 821.499 153.536 4 -4 -6 7 634.062 115.719 3 -4 -6 7 558.538 127.182 4 4 -6 -7 619.400 128.114 3 4 -6 -7 729.525 143.448 1 -4 -6 6 7.48276 26.4734 4 4 -6 -6 10.1390 39.6405 3 4 6 -6 38.7226 51.4355 4 -4 -6 6-11.0553 5.87783 3 -4 -6 6 0.64032 16.2156 2 4 -6 -6 44.9081 47.0353 1 4 -6 -5 162.391 26.6849 4 -4 -6 5 204.594 61.7592 4 4 -6 -5 281.588 84.1878 3 4 6 -5 251.656 71.6200 4 4 -6 -5 246.650 76.0197 1 -4 -6 5 171.897 65.9845 2 -4 -6 5 164.511 39.4828 1 -4 -6 4 146.379 61.9019 4 4 -6 -4 157.401 34.4488 4 4 -6 -4 131.983 56.5582 3 4 6 -4 142.210 56.0704 4 4 -6 -4 111.060 34.7397 2 -4 6 4 134.465 33.5424 2 4 -6 -4 95.1835 49.9006 1 -4 -6 4 104.912 30.9744 1 -4 -6 3 344.136 90.6142 4 4 -6 -3 284.302 73.4292 3 4 6 -3 322.988 89.6150 4 4 -6 -3 286.217 53.3250 4 4 -6 -3 183.076 52.2046 1 -4 6 3 271.465 51.7749 2 -4 -6 3 275.000 56.5751 1 4 -6 -3 246.388 51.6026 2 4 -6 -2 622.144 110.839 3 4 6 -2 821.558 143.992 4 -4 -6 2 735.421 134.008 4 4 -6 -2 632.927 87.4605 2 4 -6 -2 649.684 119.822 1 -4 6 2 682.537 88.1130 2 -4 -6 2 754.088 100.054 1 4 6 -1 153.103 68.7102 4 -4 -6 1 160.595 81.6447 4 4 -6 -1 144.848 51.2891 3 4 -6 -1 152.808 49.9849 2 -4 6 1 121.387 44.2237 2 4 6 0 177.943 65.2550 4 -4 -6 0-12.2398 46.9387 4 4 -6 0 76.8525 38.9517 3 -4 6 0 97.2102 33.5462 2 4 -6 0 153.476 57.6624 2 4 6 1 263.754 77.1617 4 -4 -6 -1 213.133 67.1687 4 4 -6 1 243.221 68.0053 3 -4 6 -1 209.716 51.8469 2 4 -6 1 236.406 65.6137 2 4 -6 2 1267.61 139.271 3 4 6 2 1376.35 179.538 4 -4 -6 -2 1057.65 156.690 4 4 -6 2 1182.76 144.207 2 -4 6 -2 1180.17 140.820 2 4 -6 3 5573.63 281.857 3 4 6 3 6162.21 381.710 4 -4 -6 -3 5537.85 358.617 4 4 -6 3 5276.41 316.472 2 4 6 3 5601.15 302.901 1 -4 6 -3 5508.43 319.628 2 4 6 4 176.752 69.1692 4 4 -6 4 247.475 57.6880 3 -4 -6 -4 173.395 78.3684 4 -4 6 -4 120.547 45.1088 2 4 6 4 232.943 66.7034 1 4 -6 4 233.784 73.2040 2 4 6 5 87.1985 69.7341 4 4 -6 5 71.2288 36.2355 3 -4 -6 -5 125.624 54.3758 4 4 6 5 86.9441 47.8579 1 -4 6 -5 33.2368 13.4928 2 4 -6 5 70.4593 38.2800 2 -4 -6 -6-27.3185 31.9344 4 4 -6 6 42.4720 29.1226 3 4 6 6 81.6306 69.7493 4 -4 6 -6 37.4737 29.9901 2 4 6 6 7.07823 57.3245 1 4 -6 6 32.9256 39.6097 2 4 -6 7 447.777 59.7670 3 4 6 7 545.603 120.576 4 -4 -6 -7 248.622 79.4451 4 -4 6 -7 311.297 81.6864 2 4 6 7 490.314 105.215 1 4 -6 7 499.628 121.547 2 4 6 8 93.5404 65.3801 4 -4 -6 -8 17.8388 35.1301 4 -4 6 -8 3.47646 32.9210 2 4 6 8 53.8217 57.5640 1 4 -6 8 32.0381 10.9446 3 -4 -6 -9 492.662 116.085 4 4 6 9 589.470 121.208 4 -4 6 -9 501.892 108.031 2 4 6 9 530.866 122.583 1 4 6 10 652.155 126.851 4 -4 -6 -10 562.480 138.636 4 -4 6 -10 491.114 111.225 2 -4 -6 -11-6.64001 33.3133 4 4 6 11-31.2351 59.9528 4 -4 -6 -11-2.72374 40.4582 2 -4 6 -11-23.3721 36.0575 2 -4 -6 -12-12.1503 8.64277 2 -4 6 -12-21.9018 26.8298 2 -4 -6 -13 1215.34 179.775 2 -4 6 -13 1135.40 194.231 2 -4 -6 -14 68.9031 49.9344 2 -4 6 -14 100.065 54.4977 2 -4 6 -15 15.0658 45.2011 2 -4 -6 -15 57.4697 54.6454 2 -4 -6 -16 34.6076 36.5140 3 -4 6 -16 62.2592 53.5762 2 -4 -6 -16 66.1851 61.4449 2 -4 -6 -17 63.0955 51.1069 3 -4 6 -17 51.8371 63.8042 2 -4 -6 -17 69.6952 56.5014 2 -4 -6 -18-38.9123 61.2626 3 -4 6 -18 18.6508 16.6159 2 -4 -6 -18 19.0832 8.21211 2 -4 -6 -19 0.13853 28.0656 3 -4 6 -19 71.7271 48.6571 2 -4 -6 -20-75.1980 56.6980 3 -4 -6 -20 55.7220 34.7333 2 -4 6 -20 18.1517 58.6963 2 -4 -6 -21 9.83582 46.8536 3 -4 -6 -22 13.2204 30.4360 3 -4 -6 -23 82.0140 71.9104 3 -4 -7 20 49.5716 75.0578 4 4 -7 -20 26.0379 86.8146 3 -4 7 20 44.8721 55.3592 1 4 -7 -19 93.4799 94.6445 3 -4 -7 19 186.373 102.191 4 -4 7 19 133.029 89.9668 1 -4 -7 18 215.692 105.070 4 4 -7 -18 100.459 112.234 3 -4 7 18-0.29295 35.1299 1 -4 -7 17 207.287 105.102 4 4 -7 -17 78.2062 85.5229 3 -4 7 17 57.9256 57.9440 1 -4 -7 16 81.8532 66.9151 4 4 -7 -16 45.1346 73.0044 3 -4 7 16-12.0638 34.1120 1 -4 -7 15 272.125 109.666 4 4 -7 -15 187.219 99.5645 3 -4 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223.695 62.7983 1 -4 -7 -5 1710.61 212.261 4 4 -7 5 1662.90 153.786 3 4 7 5 1782.22 212.952 4 4 -7 5 1648.72 199.785 2 4 7 5 1700.43 189.622 1 -4 7 -5 1740.34 203.747 2 4 -7 6 53.2499 29.6652 3 4 7 6 120.078 57.2956 4 -4 -7 -6 100.471 58.4577 4 4 7 6 10.6456 30.9716 1 -4 7 -6 62.0810 44.0668 2 4 -7 6 31.0811 31.9931 2 4 7 7 76.9223 43.4020 4 4 -7 7 79.7736 36.4381 3 -4 -7 -7 101.572 58.2996 4 -4 7 -7 106.816 58.3387 2 4 7 7 51.3213 47.8229 1 4 7 8 358.576 105.366 4 4 -7 8 345.111 54.8981 3 -4 -7 -8 299.465 89.7694 4 -4 7 -8 347.905 100.400 2 4 7 8 377.064 103.053 1 -4 -7 -9 449.911 126.611 4 4 -7 9 499.548 46.7337 3 -4 7 -9 572.544 130.672 2 4 7 9 502.313 122.519 1 -4 -7 -10 124.436 73.9928 4 4 7 10 114.989 88.6688 1 -4 7 -10 8.79913 31.9690 2 -4 -7 -11 317.421 103.709 4 -4 -7 -11 307.889 91.7749 2 -4 7 -11 237.451 89.4131 2 4 7 11 372.685 113.424 1 -4 -7 -12 98.9786 61.9823 2 4 7 12 20.9589 62.7283 1 -4 7 -12-28.6482 46.1869 2 4 7 13 183.140 94.6383 1 -4 -7 -13 133.970 67.6741 2 -4 7 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558.134 103.533 1 -4 -8 1 193.293 92.7111 4 4 -8 -1 27.7777 27.5088 3 4 -8 -1 88.1313 33.4463 4 -4 8 1 72.9622 34.3834 2 4 -8 -1 76.1334 36.6308 2 4 -8 0-13.2842 7.37045 3 -4 -8 0-57.2541 23.9631 4 4 -8 0 3.33180 22.1396 4 -4 8 0 66.5760 42.6755 2 4 -8 0 57.0460 34.3091 2 4 -8 1 173.854 64.0306 3 -4 -8 -1 200.425 54.6069 4 -4 8 -1 196.027 59.2902 2 4 -8 1 152.889 53.7707 2 4 -8 2 1571.78 184.247 3 -4 -8 -2 1456.58 203.643 4 4 -8 2 1197.19 168.805 2 -4 8 -2 1487.89 177.858 2 4 -8 3 787.951 125.044 3 -4 -8 -3 911.860 158.691 4 4 -8 3 648.830 126.783 2 -4 8 -3 788.541 132.308 2 4 -8 4 351.061 81.5805 3 -4 -8 -4 318.084 102.577 4 4 -8 4 306.000 90.2640 2 -4 8 -4 321.249 90.0360 2 4 -8 5 34.0545 32.8144 3 -4 -8 -5 40.8853 64.5519 4 -4 8 -5 22.4365 31.2735 2 4 8 5-74.7660 42.2767 1 -4 -8 -6 185.123 86.7803 4 4 -8 6 232.671 60.8936 3 -4 8 -6 162.771 73.8297 2 4 8 6 116.320 63.0801 1 4 -8 7 207.241 52.6336 3 -4 -8 -7 235.078 95.9595 4 4 8 7 88.1223 54.8055 1 -4 8 -7 132.529 59.9098 2 4 -8 8 633.161 85.3027 3 -4 -8 -8 535.351 133.227 4 4 8 8 505.962 120.249 1 -4 8 -8 565.381 130.858 2 4 -8 9 205.787 46.7025 3 -4 -8 -9 209.058 83.8237 4 4 8 9 188.733 83.6962 1 -4 8 -9 174.219 71.2553 2 4 8 10 23.3073 47.7319 1 4 -8 10 11.0701 9.50419 3 -4 8 -10-24.1359 8.05747 2 -4 -8 -11 71.8732 49.3018 4 4 8 11-8.06095 14.6869 1 -4 8 -11 36.3986 40.6023 2 -4 -8 -12 342.916 125.097 4 -4 -8 -12 424.349 117.502 2 4 8 12 380.531 131.197 1 -4 8 -12 434.722 132.251 2 -4 -8 -13 235.181 82.9892 2 -4 8 -13 288.431 105.563 2 4 8 13 195.762 103.573 1 -4 -8 -14 191.930 72.4235 2 4 8 14 101.215 86.4654 1 -4 8 -14 99.3290 60.2993 2 4 8 15 55.6442 73.4662 1 -4 -8 -15 30.2826 54.2373 2 -4 8 -15 30.7969 74.6993 2 -4 -8 -16 23.6978 44.1545 3 4 8 16 46.9113 88.1669 1 -4 -8 -16 169.337 90.8674 2 -4 8 -16 90.2019 67.8346 2 -4 -8 -17 42.6141 38.1048 3 4 8 17 57.8614 78.6289 1 -4 -8 -17 95.5398 67.5641 2 -4 8 -17 3.58455 38.6914 2 -4 -8 -18-15.6133 23.5527 3 4 8 18 56.2185 93.4244 1 -4 8 -18 7.98644 6.06088 2 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48.6375 4 4 -9 -4-66.6247 58.7186 3 -4 -9 4 24.3368 29.4427 1 4 -9 -4 3.99903 17.3733 2 4 -9 -3 10.1426 17.7783 4 -4 -9 3 28.1260 50.6908 4 4 -9 -3-2.68874 20.9509 3 -4 -9 3 20.4803 40.9274 1 4 -9 -3 30.0181 26.0511 2 4 -9 -2 42.0086 33.2191 4 4 -9 -2 13.2865 25.5134 3 -4 -9 2 45.6985 44.4076 4 -4 -9 2 47.1360 45.8258 1 4 -9 -2 44.4593 25.7379 2 4 -9 -1-35.7906 32.4480 3 4 -9 -1 83.5571 54.5605 4 4 -9 -1 42.4021 28.5044 2 4 -9 0 1294.53 186.820 3 4 -9 0 1336.85 170.539 4 -4 -9 0 1266.00 203.575 4 -4 9 0 1326.03 165.554 2 4 -9 0 1217.70 159.232 2 4 -9 1 309.266 87.5423 3 -4 -9 -1 215.554 76.9505 4 4 -9 1 240.070 73.3871 4 -4 9 -1 267.241 75.5127 2 4 -9 1 207.125 81.7268 2 4 -9 2 79.1100 49.9072 3 -4 -9 -2-2.32886 13.7114 4 4 -9 2-2.15361 23.0288 4 -4 9 -2 8.30235 26.3347 2 4 -9 2 13.4137 36.6208 2 4 -9 3 18.2114 10.4685 3 -4 -9 -3 36.7396 56.8202 4 4 -9 3-39.5264 43.2091 4 -4 9 -3 26.3184 21.1921 2 4 -9 4 585.320 115.242 3 -4 -9 -4 696.453 157.517 4 -4 9 -4 579.695 126.652 2 4 -9 5 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50.3437 3 -5 5 22-8.00128 8.14663 1 -5 -5 21 116.119 87.3161 4 5 -5 -21 94.2308 41.7977 3 -5 5 21 20.3778 25.8741 1 -5 -5 20 146.669 73.2198 4 5 -5 -20 150.426 96.9948 3 -5 5 20 198.077 76.3205 1 -5 -5 19 73.2126 70.7385 4 5 -5 -19 114.533 89.3187 3 -5 5 19 26.7325 30.8850 1 -5 -5 18 20.1425 30.7733 4 5 -5 -18 104.123 63.4321 3 -5 5 18-28.2903 60.3512 1 -5 -5 17 124.718 64.9228 4 5 -5 -17 93.4998 74.1761 3 -5 5 17-13.5309 11.8017 1 -5 -5 16 20.2013 43.7804 4 5 -5 -16 53.2034 62.7548 3 -5 5 16-30.0518 20.9940 1 -5 -5 15-33.8025 51.7131 4 5 -5 -15 49.8017 56.2190 3 -5 5 15 3.07308 14.6735 1 -5 -5 14 15.6526 31.2642 4 5 -5 -14 15.8679 19.6427 3 -5 5 14-2.91304 20.2762 1 -5 -5 13 50.8686 27.7353 4 5 -5 -13 98.4710 75.9910 3 -5 5 13 11.9268 35.3825 1 -5 -5 12-44.9633 34.7257 4 -5 5 12 41.8595 12.2751 1 -5 -5 11 96.6791 45.3908 4 5 -5 -11 271.305 103.971 3 -5 -5 11 196.244 71.7533 3 -5 -5 10 235.109 84.0616 4 5 -5 -10 400.465 114.239 3 -5 -5 10 197.280 77.2827 3 5 -5 -9 123.591 68.2060 3 -5 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323.940 101.009 2 5 -5 5 265.591 52.3946 3 5 5 6 103.924 59.3283 4 -5 -5 -6 160.300 67.2790 4 -5 5 -6 143.690 62.5260 2 5 -5 6 172.639 82.0654 2 5 -5 6 114.050 33.1340 3 5 -5 7 397.268 51.6528 3 5 5 7 552.686 112.123 4 -5 -5 -7 369.169 102.673 4 -5 5 -7 397.286 102.533 2 5 -5 7 490.660 123.910 2 -5 -5 -8 1011.41 173.883 4 5 5 8 1069.08 169.791 4 -5 5 -8 1060.39 162.007 2 -5 -5 -9 740.628 154.945 4 5 5 9 753.346 142.073 4 -5 5 -9 719.329 137.236 2 -5 -5 -10-62.3559 59.4912 4 -5 5 -10 30.0667 40.9172 2 -5 -5 -10 1.58833 26.9350 2 -5 5 -11 497.805 120.859 2 -5 -5 -11 419.425 124.954 2 -5 -5 -12 1412.89 203.481 2 -5 5 -12 1176.61 188.482 2 -5 -5 -13 1112.62 179.604 2 -5 5 -13 909.253 170.844 2 -5 5 -14-12.4922 24.5631 2 -5 -5 -14 69.0657 46.0710 2 -5 5 -15 43.1677 18.8731 2 -5 -5 -15 171.761 98.0108 2 -5 5 -16 565.760 146.178 2 -5 -5 -16 634.433 139.146 2 -5 -5 -17-94.0587 58.1074 3 -5 5 -17-31.9156 47.3284 2 -5 -5 -17-7.81526 27.6814 2 -5 -5 -18 96.5661 63.2973 3 -5 5 -18 103.899 78.3772 2 -5 -5 -18-50.2646 46.7469 2 -5 -5 -19 52.6050 43.4295 2 -5 5 -19 81.1377 30.7148 2 -5 -5 -20 47.2175 68.5404 3 -5 5 -20 8.89358 47.8257 2 -5 -5 -20-76.6417 56.4422 2 -5 -5 -21 73.5229 57.8717 3 -5 -5 -21-36.7064 15.8313 2 -5 -5 -22 70.1830 46.4195 2 -5 -6 22-37.1752 43.5805 4 -5 6 22-36.9474 32.7590 1 5 -6 -21 64.1308 66.4072 3 -5 6 21-23.4552 46.6242 1 -5 -6 20 83.7735 78.3293 4 5 -6 -20 116.297 93.2921 3 -5 6 20 150.043 93.8840 1 -5 -6 19 131.344 92.7236 4 5 -6 -19 130.059 92.5557 3 -5 6 19 64.0255 69.1283 1 -5 -6 18-73.0506 47.7695 4 5 -6 -18 33.6193 62.4249 3 -5 6 18-60.5155 26.6904 1 -5 -6 17-24.4225 50.0945 4 5 -6 -17 21.0784 59.9289 3 -5 6 17 89.4656 64.6796 1 -5 -6 16 151.523 87.1664 4 5 -6 -16 162.949 111.485 3 -5 6 16 241.117 94.0275 1 -5 -6 15 134.440 71.5046 4 5 -6 -15 150.102 84.7621 3 -5 6 15 111.385 46.2737 1 -5 -6 14-18.2371 30.0876 4 5 -6 -14 2.39245 7.85828 3 -5 6 14-56.9445 73.6178 1 5 -6 -13 229.427 107.262 3 -5 -6 13 114.462 41.0949 4 -5 -6 12-13.1926 44.1777 4 5 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109.547 4 -5 -6 2 332.624 102.242 4 5 -6 -2 388.523 94.5876 3 5 -6 -2 355.369 76.6419 2 5 -6 -2 313.144 78.7741 1 -5 6 2 339.162 63.8935 2 5 -6 -1 883.536 142.884 3 -5 -6 1 766.491 139.802 4 5 6 -1 1054.19 171.677 4 5 -6 -1 831.084 121.933 2 -5 6 1 903.603 112.939 2 5 -6 0 958.453 141.096 3 -5 -6 0 793.715 143.245 4 5 6 0 883.006 150.625 4 5 -6 0 786.429 120.214 2 -5 6 0 827.360 111.557 2 5 -6 1 1678.28 174.054 3 5 6 1 2065.27 233.723 4 -5 -6 -1 1646.43 207.852 4 5 -6 1 1745.05 182.026 2 -5 6 -1 1697.95 169.283 2 5 -6 2 812.260 115.780 3 5 6 2 952.098 160.818 4 -5 -6 -2 773.365 147.487 4 5 -6 2 859.248 138.957 2 -5 6 -2 784.878 121.261 2 5 6 2 767.654 106.398 1 5 -6 3 38.5311 14.1839 3 5 6 3 132.127 62.8724 4 -5 -6 -3 89.5054 57.6768 4 5 6 3 85.4646 29.7525 1 -5 6 -3 79.0315 38.3049 2 5 -6 3 194.689 75.8319 2 5 6 4 127.441 71.9569 4 -5 -6 -4 137.096 82.7855 4 5 -6 4 103.838 38.4863 3 5 6 4 97.5810 41.1977 1 -5 6 -4 113.493 45.8422 2 5 -6 4 218.505 80.1207 2 -5 -6 -5 1626.35 216.443 4 5 6 5 1952.60 227.912 4 5 -6 5 1594.66 139.358 3 5 -6 5 1790.34 214.284 2 -5 6 -5 1802.59 201.159 2 5 6 5 1774.79 185.842 1 5 6 6 710.678 137.279 4 -5 -6 -6 621.374 136.519 4 5 -6 6 532.458 74.8910 3 5 -6 6 709.981 139.076 2 -5 6 -6 526.954 108.075 2 5 6 6 598.279 115.267 1 5 -6 7 771.937 76.9845 3 -5 -6 -7 823.133 157.626 4 -5 6 -7 856.153 148.356 2 5 6 7 922.922 149.837 1 -5 -6 -8 594.672 141.280 4 5 -6 8 445.124 48.7175 3 -5 6 -8 499.146 117.794 2 5 6 8 541.472 119.820 1 -5 -6 -9 1623.56 226.789 4 -5 6 -9 1755.30 222.948 2 -5 -6 -10 1095.57 192.379 4 -5 6 -10 1187.44 189.668 2 -5 -6 -11 173.855 78.9064 4 -5 -6 -11 307.135 94.9344 2 -5 6 -11 265.738 89.8653 2 -5 -6 -12 356.749 155.444 2 -5 6 -12-15.3400 29.5353 2 -5 -6 -13-56.5849 29.3476 2 -5 6 -13 61.6515 49.9035 2 -5 6 -14 256.595 72.6889 2 -5 -6 -14 181.648 76.0160 2 -5 6 -15 36.7226 23.7901 2 -5 -6 -15 148.690 74.3934 2 -5 6 -16 1.73553 26.7490 2 -5 -6 -16 117.788 73.4866 2 -5 6 -17 46.2692 5.37774 2 -5 -6 -17 106.151 60.3476 2 -5 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2 -5 7 -1 19.2383 16.7216 2 5 -7 2 143.258 56.2588 3 -5 -7 -2 76.1973 63.2715 4 -5 7 -2 103.906 47.3697 2 5 -7 2 158.590 76.5003 2 -5 -7 -3 2039.15 243.137 4 5 -7 3 2131.30 195.557 3 5 -7 3 1936.53 224.548 2 -5 7 -3 1933.96 204.179 2 5 -7 4 182.781 56.7887 3 -5 -7 -4 179.966 82.0418 4 5 7 4 145.602 50.2761 1 -5 7 -4 117.581 36.8526 2 5 -7 4 148.698 74.8166 2 5 -7 5 596.445 94.7455 3 -5 -7 -5 588.025 145.590 4 5 7 5 554.865 106.240 1 -5 7 -5 488.629 114.926 2 5 -7 5 527.192 130.308 2 5 -7 6 152.992 49.9665 3 -5 -7 -6 155.356 77.7480 4 -5 7 -6 68.5790 14.8191 2 5 7 6 66.1505 34.4142 1 -5 -7 -7 1180.19 189.321 4 5 -7 7 1216.56 111.692 3 -5 7 -7 1181.47 180.764 2 5 7 7 1336.63 176.021 1 -5 -7 -8-15.9617 25.1869 4 5 -7 8-2.45645 8.82128 3 -5 7 -8 54.4175 37.1712 2 5 7 8 69.6388 54.9144 1 -5 -7 -9 711.528 158.563 4 5 -7 9 541.862 41.2550 3 -5 7 -9 706.546 146.409 2 5 7 9 987.783 193.156 1 -5 -7 -10 173.034 90.5464 4 -5 7 -10 157.581 76.8231 2 5 7 10 221.113 91.4441 1 -5 -7 -11 71.8279 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867.400 96.1237 2 -7 -6 5 25.3611 41.1942 4 7 -6 -5 85.3209 25.8853 4 -7 6 5 49.1055 28.1407 2 7 -6 -5 117.777 65.6403 3 -7 -6 4 33.9406 29.8311 4 7 -6 -4 127.154 47.8885 4 -7 6 4 140.693 50.5594 2 7 -6 -4 99.8816 51.9569 3 -7 -6 3 289.551 103.955 4 7 -6 -3 392.984 81.8244 4 -7 6 3 275.558 66.9099 2 7 -6 -3 250.053 81.2509 3 -7 -6 2 340.360 107.437 4 -7 6 2 344.457 96.3982 3 7 -6 -2 346.436 77.4149 4 -7 6 2 276.268 69.9990 2 7 -6 -2 289.322 91.8085 3 7 -6 -1 321.690 75.9387 4 -7 -6 1 311.468 103.446 4 -7 6 1 296.832 82.7945 3 -7 6 1 299.156 77.7672 2 7 -6 -1 211.748 69.2354 3 7 -6 0 195.654 64.2980 4 -7 -6 0 302.598 107.147 4 -7 6 0 288.242 87.5563 3 -7 6 0 279.501 76.4773 2 7 -6 0 303.456 79.7136 3 7 -6 1 320.328 80.6448 4 -7 6 -1 254.006 77.5227 3 -7 6 -1 214.775 75.0616 2 7 -6 1 198.688 64.4824 3 -7 6 -2 445.069 97.2970 3 -7 -6 -2 436.470 124.822 4 -7 6 -2 496.070 108.275 2 7 -6 2 427.950 103.628 2 7 -6 2 465.444 100.842 3 7 6 2 432.827 75.7498 1 -7 -6 -3 172.809 84.0361 4 -7 6 -3 185.772 75.3733 2 7 -6 3 154.898 76.0052 2 7 6 3 196.204 56.3017 1 7 -6 3 206.351 61.8549 3 -7 -6 -4 425.133 120.966 4 7 6 4 489.123 95.4279 1 -7 6 -4 455.605 111.856 2 7 -6 4 387.879 87.1179 3 -7 -6 -5 59.1164 51.5048 4 -7 6 -5 82.2240 47.7998 2 7 6 5 119.387 62.3751 1 7 -6 5 89.2460 44.6882 3 7 -6 6 572.419 90.0392 3 -7 -6 -6 520.104 147.943 4 -7 6 -6 480.980 120.482 2 7 6 6 724.767 131.473 1 -7 -6 -7 89.1685 80.4248 4 7 -6 7 99.6704 34.3184 3 -7 6 -7 98.4409 61.2035 2 7 6 7 146.110 72.8097 1 -7 -6 -8 241.427 107.654 4 -7 6 -8 167.932 89.2696 2 -7 -6 -9-55.9019 60.1837 4 -7 6 -9 23.2961 37.6849 2 -7 -6 -10 24.1725 55.6976 4 -7 6 -10-27.3934 24.4941 2 -7 -6 -10 64.8896 56.7389 2 -7 -6 -11 128.983 90.0250 4 -7 6 -11 50.4693 37.7889 2 -7 -6 -11 101.807 69.5465 2 -7 6 -12 67.3629 60.7342 2 -7 -6 -12-13.2189 25.7491 2 -7 6 -13 180.018 84.1142 2 -7 -6 -13 372.300 118.870 2 -7 6 -14 253.802 95.5003 2 -7 -6 -14 293.942 105.357 2 -7 6 -15 21.6345 26.6990 2 -7 -6 -15 35.7842 55.8304 2 -7 6 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884.131 125.354 3 -7 -7 -5 877.053 182.544 4 -7 7 -5 842.189 156.731 2 7 7 5 884.080 137.497 1 -7 -7 -6 132.241 93.9836 4 -7 7 -6 64.0884 46.9537 2 7 7 6 131.530 60.7045 1 7 -7 6 151.253 54.4377 3 -7 -7 -7 122.867 41.0304 4 -7 7 -7 39.1136 27.1950 2 7 7 7 47.5952 47.9799 1 7 -7 7 27.5630 21.8379 3 -7 -7 -8-17.9813 45.4119 4 7 -7 8 16.8050 16.1987 3 -7 7 -8 23.9263 30.4476 2 7 7 8 30.3757 46.9125 1 -7 -7 -9 209.077 98.8983 4 -7 7 -9 138.101 73.3944 2 7 7 9 147.121 82.0644 1 -7 -7 -10 150.626 90.2761 4 7 7 10 69.7145 73.1396 1 -7 7 -10 21.5843 41.0748 2 -7 -7 -11 120.755 75.8407 4 -7 -7 -11 23.2185 59.0450 2 -7 7 -11 37.1112 18.9785 2 7 7 11 97.3078 89.2718 1 -7 -7 -12 17.6530 80.2552 2 -7 7 -12 92.1061 65.9449 2 -7 -7 -13 207.507 95.9603 2 -7 7 -13 176.604 81.7323 2 -7 -7 -14 114.392 71.9753 2 -7 7 -14-6.31660 30.6351 2 -7 7 -15 38.1221 49.1402 2 -7 -7 -15 28.5026 30.8436 2 -7 7 -16 6.60954 11.8731 2 -7 -7 -16 88.8307 59.8022 2 -7 -7 -17 279.004 113.849 2 -7 -7 -18 10.9852 58.1805 2 -7 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2 11.3059 31.3660 2 7 -8 -1 35.2445 31.7872 3 7 -8 -1 10.1631 24.6377 4 -7 -8 1-12.6813 30.6513 4 -7 8 1 15.6596 23.9625 2 -7 -8 0 197.158 99.2574 4 7 -8 0 208.112 75.8117 3 7 -8 0 200.774 86.6749 2 -7 8 0 166.294 57.1582 2 -7 -8 -1 621.594 156.368 4 7 -8 1 590.924 137.199 2 -7 8 -1 498.901 107.151 2 7 -8 1 562.316 123.718 3 -7 -8 -2 286.919 113.074 4 -7 8 -2 420.920 101.163 2 7 -8 2 509.583 111.443 3 -7 8 -3 47.0375 14.7585 2 7 -8 3 32.5792 18.3636 3 -7 -8 -4 149.227 87.5130 4 -7 8 -4 2.90790 27.6969 2 7 -8 4 89.3488 53.1604 3 -7 -8 -5-4.76696 16.0437 4 -7 8 -5 16.5730 36.2352 2 7 -8 5 96.3519 42.6438 3 7 8 5 44.3320 34.3955 1 -7 -8 -6 344.077 130.086 4 7 8 6 306.963 86.9025 1 -7 8 -6 275.794 85.8459 2 7 -8 6 294.200 76.4378 3 7 8 7 76.9503 65.0847 1 -7 8 -7 12.5786 13.2316 2 7 -8 7 60.8885 34.7243 3 -7 -8 -8-18.1467 24.2923 4 -7 8 -8-3.01685 35.9272 2 7 8 8-20.7800 3.96858 1 -7 -8 -9 49.2597 58.8238 4 -7 8 -9 81.0249 58.0246 2 7 8 9 61.9781 54.5551 1 -7 -8 -10 142.162 73.4803 4 7 8 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73.3365 3 -7 -9 6 720.863 183.273 4 7 -9 -6 472.865 154.710 3 -7 -9 5 193.922 79.2891 4 7 -9 -5 224.746 110.860 3 -7 -9 4-18.0878 62.3160 4 7 -9 -4 15.4695 20.4396 3 -7 9 4 15.0199 27.3554 2 -7 -9 3 30.6477 38.9603 4 7 -9 -3-7.22115 19.3333 3 7 -9 -3 23.1891 35.0609 4 -7 9 3 11.3904 10.8251 2 -7 -9 2 53.2231 60.3862 4 7 -9 -2 52.9513 34.8445 4 7 -9 -2 7.85988 21.8927 3 -7 9 2 27.1668 26.5797 2 7 -9 -1 188.912 78.5765 3 -7 -9 1 253.982 121.385 4 -7 9 1 150.888 65.2838 2 7 -9 0 48.5295 42.7457 3 -7 9 0 73.8653 50.0359 2 7 -9 1 2.38661 34.9179 3 -7 -9 -1 41.4477 50.5046 4 -7 9 -1 36.1403 50.0701 2 -7 -9 -2 61.1489 67.0311 4 7 -9 2 27.6250 25.8319 3 -7 9 -2 23.3431 24.4495 2 -7 9 -3 75.2082 45.3708 2 7 -9 3 22.6990 8.41914 3 -7 -9 -4 241.599 137.469 4 -7 9 -4 295.800 100.326 2 7 -9 4 234.940 69.9391 3 -7 -9 -5 166.101 101.343 4 -7 9 -5 159.494 75.3890 2 7 -9 5 70.4494 46.2210 3 -7 -9 -6 27.9308 42.9532 4 -7 9 -6 16.0872 36.0354 2 7 -9 6-34.2874 26.1715 3 -7 -9 -7-9.20650 60.2221 4 -7 9 -7 6.03090 16.0597 2 7 9 7-4.87196 15.3653 1 -7 -9 -8 1.21328 42.0009 4 7 9 8 96.1643 55.5013 1 -7 9 -8 83.8520 55.4939 2 -7 -9 -9 84.1040 73.6367 4 7 9 9 150.034 70.0074 1 -7 9 -9 90.6776 55.9154 2 -7 -9 -10 86.3873 66.1645 4 7 9 10 31.4538 49.0744 1 -7 9 -10-23.5212 23.5902 2 -7 9 -11 5.73611 32.1261 2 7 9 11 34.5956 47.7446 1 -7 -9 -12-3.11492 24.0784 4 -7 -9 -12 89.7902 59.0327 2 -7 9 -12 41.6977 40.5186 2 7 9 12 11.5908 13.2279 1 -7 9 -13 18.1584 42.8326 2 7 9 13 106.445 92.9914 1 7 9 14 125.861 86.5543 1 -7 -9 -14-6.33207 43.6445 2 7 9 15 145.977 112.191 1 -7 -9 -15 55.2106 52.0560 2 7 9 16 13.2750 53.1786 1 -7 -9 -16 41.5525 71.5248 2 7 -10 -11 40.1391 56.6046 3 -7 -10 10 75.0064 79.8377 4 7 -10 -10 5.70255 9.76920 3 7 -10 -9 16.8100 47.1774 3 -7 -10 9 243.183 123.839 4 7 -10 -8 145.790 110.400 3 -7 -10 8 293.222 130.340 4 7 -10 -7-2.62403 65.3620 3 -7 -10 7 92.7233 78.6863 4 7 -10 -6 43.0561 67.6666 3 -7 -10 6 26.5224 53.4076 4 7 -10 -5 44.3409 61.8520 3 -7 -10 5 99.6861 74.1142 4 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3 -3 1981.12 196.365 3 -8 3 -3 2117.95 227.424 2 -8 -3 -4 285.666 99.2302 4 8 -3 4 423.417 116.149 4 -8 3 -4 408.174 107.543 2 -8 -3 -5 574.517 142.565 4 -8 3 -5 596.203 126.574 2 -8 -3 -6 121.137 86.0069 4 -8 3 -6 54.2114 36.5245 3 -8 3 -6 102.635 56.5220 2 -8 -3 -7 1414.34 231.543 4 -8 3 -7 1372.28 142.818 3 -8 -3 -7 1347.90 226.104 2 -8 3 -7 1341.26 197.851 2 -8 3 -8 1242.59 128.401 3 -8 -3 -8 1373.34 227.416 2 -8 3 -8 1091.13 181.137 2 -8 3 -9 184.366 47.0148 3 -8 -3 -9 164.386 82.7798 2 -8 3 -9 108.137 42.7307 2 -8 3 -10 47.3172 26.5472 3 -8 -3 -10 41.0575 49.6176 2 -8 3 -10-3.75373 36.6131 2 -8 3 -11 195.010 41.0098 3 -8 -3 -11 317.344 113.292 2 -8 3 -11 187.368 67.4652 2 -8 -3 -12 499.175 146.770 2 -8 3 -12 522.212 129.650 2 -8 -3 -13 284.157 112.255 2 -8 3 -13 121.223 70.1448 2 -8 3 -14 38.1991 36.0271 2 -8 -3 -14 110.541 54.8546 2 -8 3 -15 57.6534 46.7334 2 -8 -3 -15 106.754 81.5523 2 -8 3 -16 152.561 92.3932 2 -8 -3 -16 230.196 106.231 2 -8 3 -17 181.641 106.088 2 -8 -3 -17 67.6560 46.3096 2 -8 3 -18 78.6132 86.3673 2 -8 -3 -18 10.9496 45.5699 2 -8 -3 -19 43.0631 48.4625 2 -8 -3 -20 39.7086 36.8144 2 -8 -4 21 103.482 58.7681 4 -8 -4 20 66.3980 51.8437 4 -8 -4 19 71.7950 64.1589 4 8 -4 -19-3.21333 58.9272 3 -8 -4 18 65.2563 52.2748 4 8 -4 -18 34.4706 45.5306 3 -8 -4 17 69.1808 49.4345 4 8 -4 -17 250.078 133.185 3 -8 -4 16 40.9835 66.4046 4 8 -4 -16 17.9851 48.2265 3 -8 -4 15 102.953 72.3934 4 8 -4 -15 48.2681 67.6243 3 -8 -4 14 40.4326 51.7277 4 8 -4 -14 74.2634 39.6953 3 -8 -4 13 58.6399 59.3888 4 8 -4 -13 79.8835 63.9781 3 -8 -4 12 119.143 86.4222 4 -8 4 12 100.994 31.1085 2 8 -4 -12 75.8506 68.3665 3 -8 -4 11 221.983 92.0916 4 -8 4 11 93.4979 34.0566 2 -8 4 11 84.4536 39.6771 2 8 -4 -11 63.6398 62.7237 3 -8 -4 10 34.6276 13.5932 4 -8 4 10 92.4591 33.1646 2 8 -4 -10 67.9640 59.3999 3 -8 -4 9 0.74562 43.8237 4 -8 4 9 99.7678 41.6557 2 8 -4 -9 109.661 72.3500 3 -8 -4 8 353.522 105.027 4 8 -4 -8 320.215 57.3943 4 -8 4 8 336.840 69.1181 2 8 -4 -8 259.877 114.349 3 8 -4 -7 7113.37 476.083 3 -8 -4 7 0.10389 51.2402 4 8 -4 -7 5188.08 292.722 4 -8 4 7 265.716 108.014 2 8 -4 -7 370.839 154.019 1 8 -4 -6 170.885 52.0767 4 -8 -4 6 41.3251 45.9537 4 -8 4 6 180.683 61.1727 2 8 -4 -6 164.156 61.2362 1 8 -4 -6 65.7763 41.3102 3 8 -4 -5 34.7689 28.5558 4 -8 -4 5 51.6940 47.9233 4 -8 4 5 76.2592 41.6291 2 8 -4 -5 17.8654 34.7506 1 8 -4 -5 41.6696 34.1423 3 8 -4 -4 254.898 65.8566 4 -8 -4 4 174.625 74.4360 4 8 -4 -4 215.661 71.0539 1 -8 4 4 275.347 74.4853 2 8 -4 -4 118.873 46.4396 3 8 -4 -3 39.8068 32.9980 4 -8 -4 3 45.5730 47.1043 4 -8 4 3 23.1388 22.8979 2 8 -4 -3-17.2701 34.2615 1 8 -4 -3-29.6900 35.3002 3 -8 4 2 8.04047 19.3606 3 -8 -4 2 29.0983 11.2720 4 8 -4 -2 82.3763 50.9256 4 -8 4 2 31.9693 45.2233 2 8 -4 -2 66.8288 43.3359 3 -8 -4 1 1244.35 198.508 4 8 -4 -1 1457.73 173.090 4 -8 4 1 1425.55 189.650 3 8 -4 -1 1409.12 179.641 3 -8 4 1 1212.84 160.757 2 -8 4 0 33.8652 30.1833 3 -8 -4 0 155.857 69.9679 4 8 -4 0 35.8580 15.6867 4 8 4 0 37.1205 14.5450 1 -8 4 0 37.1399 28.7630 2 8 -4 0 50.0077 36.7739 3 -8 4 -1 297.906 84.9971 3 -8 -4 -1 282.580 97.9282 4 8 -4 1 338.950 92.1555 4 8 4 1 324.056 55.5240 1 -8 4 -1 402.055 92.7750 2 8 -4 1 308.044 84.5650 3 8 -4 2 762.302 126.685 3 -8 4 -2 588.850 111.496 3 -8 -4 -2 591.670 150.651 4 8 -4 2 743.802 140.527 4 -8 4 -2 650.109 124.281 2 8 -4 3 80.6059 38.9165 4 -8 4 -3 93.1088 42.1423 3 -8 -4 -3 111.950 75.7521 4 8 -4 3 108.832 54.1989 3 -8 4 -3 48.9992 38.2372 2 8 -4 4-24.6436 31.9890 4 -8 -4 -4 63.1893 72.2812 4 8 -4 4 31.0777 26.2326 3 -8 4 -4 30.2108 9.58180 2 -8 -4 -5 61.6219 38.2027 4 8 -4 5 129.472 43.4807 3 -8 4 -5 138.088 14.7412 2 -8 -4 -6 538.469 144.899 4 -8 4 -6 413.570 81.0514 3 -8 4 -6 407.211 108.291 2 -8 -4 -7 785.923 169.260 4 -8 4 -7 670.375 101.060 3 -8 4 -7 629.070 129.341 2 -8 -4 -8 378.128 132.412 4 -8 4 -8 484.443 78.2358 3 -8 -4 -8 570.379 145.634 2 -8 4 -8 566.944 133.449 2 -8 4 -9 336.833 62.2640 3 -8 -4 -9 487.348 144.100 2 -8 4 -9 167.013 79.0323 2 -8 4 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144.087 4 8 -5 -12 170.641 94.6453 3 -8 -5 11 120.262 77.2148 4 8 -5 -11 32.3025 41.2620 3 -8 -5 10 121.952 84.7052 4 8 -5 -10-2.97011 45.1464 3 -8 5 10 73.2045 17.9531 2 -8 -5 9-0.34669 13.2684 4 -8 5 9 39.1486 17.1482 2 -8 -5 8 65.6443 29.4937 4 8 -5 -8 38.4655 17.1962 4 -8 5 8 113.400 35.7686 2 8 -5 -8 138.210 86.4199 3 8 -5 -7 288.488 52.3998 4 -8 -5 7 270.706 107.962 4 -8 5 7 351.864 65.3141 2 8 -5 -7 319.251 115.180 3 8 -5 -6 40.0788 29.3669 4 -8 -5 6 34.1662 32.5025 4 -8 5 6 26.4103 4.61506 2 8 -5 -6 71.2136 56.8956 3 8 -5 -5 6.77910 21.7026 4 -8 -5 5-6.94520 31.5278 4 -8 5 5 7.10812 10.9749 2 8 -5 -5-2.02134 32.2629 3 8 -5 -4 177.718 71.5854 4 -8 -5 4 79.8971 64.4560 4 -8 5 4 14.4966 40.8868 2 8 -5 -4 145.256 92.1730 3 -8 -5 3 38.1396 56.2317 4 8 -5 -3 89.3026 34.1410 4 -8 5 3 52.6974 36.6277 2 8 -5 -3 22.5977 21.6076 3 -8 -5 2 283.810 101.044 4 8 -5 -2 234.620 67.8396 4 -8 5 2 200.994 58.4335 2 8 -5 -2 220.103 67.6535 3 -8 5 1 22.8563 8.28079 3 -8 -5 1 57.7176 57.3730 4 8 -5 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126.616 57.0108 3 -8 6 0 148.246 67.2132 2 8 -6 0 125.449 58.7841 3 8 -6 1 575.600 121.335 4 8 -6 1 624.859 123.707 3 -8 6 -1 625.484 126.038 3 -8 -6 -1 552.019 145.945 4 -8 6 -1 638.794 128.367 2 8 -6 2 958.505 147.939 3 -8 6 -2 849.882 141.367 3 8 -6 2 1022.94 170.076 4 -8 -6 -2 892.695 189.421 4 -8 6 -2 922.352 154.249 2 8 6 2 948.855 112.520 1 8 -6 3 73.8189 64.5000 4 -8 6 -3-15.6365 36.3702 3 -8 -6 -3-5.44538 36.9166 4 -8 6 -3 59.9639 56.8170 2 8 6 3-0.69925 25.4261 1 8 -6 3 118.311 62.7488 3 -8 6 -4 18.5102 15.0655 3 -8 -6 -4-13.9285 30.0509 4 -8 6 -4 91.1244 54.0851 2 8 6 4 67.2221 39.3319 1 8 -6 4 104.065 49.5751 3 -8 -6 -5 92.8394 73.0614 4 8 -6 5 105.371 45.6939 3 -8 6 -5 145.199 63.1668 2 8 6 5 148.652 58.2074 1 -8 -6 -6-14.2701 44.7020 4 8 -6 6 19.5253 29.3786 3 -8 6 -6 21.4907 36.2573 2 8 6 6 112.573 64.8568 1 -8 -6 -7 139.461 79.8612 4 -8 6 -7 53.6018 32.2883 2 8 6 7 104.674 75.8925 1 -8 -6 -8 148.758 78.7487 4 -8 6 -8 68.9235 50.0468 2 -8 -6 -9 272.414 112.933 4 -8 6 -9 271.722 101.953 2 -8 -6 -10 92.5118 77.7146 4 -8 6 -10 40.2483 46.4653 2 -8 -6 -10 52.5457 38.6956 2 -8 6 -11 94.9239 61.3820 2 -8 -6 -11 239.155 108.701 2 -8 6 -12 65.2721 58.9473 2 -8 -6 -12 362.184 172.482 2 -8 6 -13 42.0199 36.2051 2 -8 -6 -13 78.8775 68.6200 2 -8 6 -14 133.962 79.1508 2 -8 -6 -14 24.6185 35.0329 2 -8 6 -15 3.61608 56.1763 2 -8 -6 -15 61.6721 80.0035 2 -8 6 -16 63.1886 70.5626 2 -8 -6 -16 143.043 90.2803 2 -8 -6 -17 102.908 67.7021 2 -8 -6 -18 86.5982 67.1615 2 -8 -6 -19 16.4651 25.4714 2 -8 -7 17 53.8678 51.3953 4 -8 -7 16 63.3621 60.8473 4 -8 -7 15 180.313 112.946 4 8 -7 -15 51.9514 80.2871 3 -8 -7 14 57.6409 67.7562 4 8 -7 -14 72.0950 74.2957 3 -8 -7 13 63.5430 49.3633 4 8 -7 -13 12.9288 33.1674 3 -8 -7 12 172.273 95.0148 4 8 -7 -12 10.8118 56.6886 3 -8 -7 11 124.819 85.8769 4 8 -7 -11 82.4800 90.6956 3 -8 -7 10 54.6699 87.7450 4 8 -7 -10-5.47784 18.0522 3 -8 -7 9 92.6625 58.6173 4 8 -7 -9 41.1846 59.8249 3 -8 -7 8 107.995 57.6166 4 8 -7 -8 33.2289 47.2086 3 -8 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8 -7 3 262.219 83.6769 3 -8 -7 -4 23.2170 30.7303 4 8 7 4 4.05669 21.3879 1 -8 7 -4 29.4086 16.0080 2 8 -7 4 112.297 55.1655 3 -8 -7 -5 26.0783 45.8773 4 -8 7 -5-2.42829 17.3368 2 8 7 5-17.0102 17.7684 1 8 -7 5 8.43089 40.3627 3 -8 -7 -6-21.5721 35.9354 4 8 -7 6 40.9387 40.2205 3 -8 7 -6-28.5260 35.1981 2 8 7 6 12.3917 20.4296 1 -8 -7 -7 266.524 128.861 4 8 -7 7 199.304 59.8738 3 -8 7 -7 137.729 69.4718 2 8 7 7 241.690 85.7176 1 -8 -7 -8 24.9032 40.8106 4 -8 7 -8 29.9297 27.9671 2 8 7 8 40.2914 41.7154 1 -8 -7 -9 81.5551 50.3590 4 -8 7 -9 150.940 78.2146 2 8 7 9 150.789 84.0893 1 -8 -7 -10 77.4693 60.8632 4 8 7 10 73.5439 73.8983 1 -8 7 -10-76.6095 52.6196 2 -8 -7 -11 130.572 81.8926 4 -8 -7 -11 232.141 94.2876 2 -8 7 -11-19.2157 33.3113 2 8 7 11 129.566 82.3787 1 -8 -7 -12 28.8419 51.7602 2 -8 7 -12 62.3716 60.2443 2 -8 7 -13-21.2376 32.6343 2 -8 -7 -13 136.649 77.8790 2 -8 7 -14 40.8236 29.0139 2 -8 -7 -14 37.7710 67.9739 2 -8 7 -15 75.7672 71.1222 2 -8 -7 -15 19.9839 37.4819 2 -8 -7 -16 173.248 106.140 2 -8 -7 -17 112.267 117.084 2 -8 -7 -18 133.424 80.1626 2 -8 -8 15 153.956 121.209 4 -8 -8 14 135.167 107.702 4 8 -8 -14 61.2800 88.5874 3 -8 -8 13 60.5010 77.8911 4 8 -8 -13 170.297 102.207 3 -8 -8 12 135.881 110.859 4 8 -8 -12 126.829 113.834 3 -8 -8 11 292.275 123.367 4 8 -8 -11 40.1485 69.4193 3 -8 -8 10 19.9547 78.9766 4 8 -8 -10 22.1228 64.5307 3 -8 -8 9 153.348 83.3415 4 8 -8 -9 9.78871 45.2109 3 -8 -8 8-38.1218 45.7871 4 8 -8 -8-7.50024 20.4414 3 -8 -8 7 280.295 112.901 4 8 -8 -7 211.797 123.179 3 -8 -8 6 217.348 111.827 4 8 -8 -6 162.019 87.4310 3 -8 -8 5 4.42880 19.7825 4 -8 8 5 14.7449 29.3304 2 8 -8 -5 18.4348 29.6407 3 -8 -8 4 127.185 69.0926 4 -8 8 4 217.115 64.1949 2 8 -8 -4 108.305 65.3568 3 -8 -8 3-10.1800 49.6434 4 -8 8 3 8.98868 18.3624 2 8 -8 -3-1.10040 33.4809 3 -8 -8 2-36.6875 24.7874 4 -8 8 2-15.4850 15.7028 2 8 -8 -2 13.3332 18.7971 3 -8 8 1 19.5041 25.2562 2 8 -8 -1-0.39961 39.9212 3 -8 -8 0 65.6457 55.9500 4 -8 8 0 73.2777 53.4172 2 8 -8 0 61.0543 41.1925 3 -8 -8 -1 305.591 134.968 4 -8 8 -1 175.926 63.5837 2 8 -8 1 225.726 82.2579 3 -8 8 -2 14.0252 27.7462 2 8 -8 2 74.5676 63.3359 3 -8 -8 -3-40.7253 52.1330 4 -8 8 -3 14.7836 13.8214 2 -8 -8 -4-65.1624 61.4086 4 -8 8 -4-17.8391 47.2840 2 8 -8 4 85.6439 48.1986 3 -8 -8 -5-22.6633 29.8146 4 -8 8 -5 22.7295 27.5089 2 8 8 5 121.327 66.0984 1 8 -8 5 115.141 60.6345 3 -8 -8 -6 133.863 105.571 4 8 8 6 13.4432 30.7264 1 -8 8 -6 52.9718 32.8023 2 8 -8 6 33.7182 37.5567 3 -8 -8 -7 3.38643 60.5803 4 -8 8 -7 31.4563 44.2524 2 8 8 7 51.9470 61.8881 1 -8 -8 -8 133.303 89.6190 4 -8 8 -8 64.7814 62.7108 2 8 8 8 120.827 78.8553 1 -8 -8 -9 373.712 180.188 4 -8 8 -9 55.0068 43.4658 2 8 8 9 215.717 97.8772 1 -8 -8 -10 19.0220 48.6675 4 8 8 10 88.1245 48.3178 1 -8 8 -10 84.4020 75.7286 2 -8 -8 -11 12.3914 77.2844 4 -8 -8 -11 49.0402 67.7226 2 -8 8 -11 43.2158 47.6519 2 8 8 11 87.5760 84.1165 1 -8 -8 -12 46.2544 69.6477 2 -8 8 -12-24.9093 41.3815 2 8 8 12-0.48387 48.8800 1 8 8 13 97.3197 80.7849 1 -8 -8 -13 91.7122 82.3903 2 -8 8 -13 62.9803 55.3467 2 -8 -8 -14 21.9980 42.3066 2 8 8 14 96.5365 79.2423 1 -8 8 -14 34.8821 66.9103 2 -8 -8 -15 34.2481 38.6033 2 8 8 15 137.781 90.2962 1 -8 -8 -16 118.249 82.1127 2 8 8 16 49.7733 77.2386 1 -8 -8 -17 92.7265 75.9722 2 -8 -9 12 401.774 158.368 4 8 -9 -12 10.5580 53.2191 3 -8 -9 11 253.274 125.665 4 8 -9 -11 110.150 100.280 3 -8 -9 10 304.421 134.455 4 8 -9 -10 79.6592 77.8018 3 -8 -9 9 284.302 121.094 4 8 -9 -9 133.398 107.886 3 -8 -9 8 6.55478 42.7800 4 8 -9 -8 76.6288 82.2545 3 -8 -9 7 41.9862 29.7899 4 8 -9 -7 73.4136 78.6545 3 8 -9 -6 119.313 86.7564 3 -8 -9 6 195.734 95.0912 4 -8 -9 5 86.7856 87.2002 4 8 -9 -5 101.084 74.8869 3 8 -9 -4 84.6515 63.6124 3 -8 -9 4 13.2984 49.0711 4 -8 -9 3 34.9825 30.2296 4 8 -9 -3 79.4617 72.9109 3 -8 -9 2 323.467 121.807 4 -8 9 2 293.832 82.0797 2 8 -9 -2 332.676 116.145 3 -8 -9 1 20.4415 33.8707 4 -8 9 1 94.7975 54.2265 2 8 -9 -1 77.3221 63.3549 3 -8 -9 0 58.5944 84.4762 4 -8 9 0 60.8748 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266.717 106.717 2 -9 3 -11 64.2091 43.5498 2 -9 -3 -12 58.5506 30.2461 2 -9 3 -12 126.875 63.7652 2 -9 -3 -13 55.0125 63.2481 2 -9 3 -13-58.1781 74.7401 2 -9 -3 -14 75.3797 67.5128 2 -9 3 -14-12.4299 57.1228 2 -9 3 -15 91.3882 63.0650 2 -9 -3 -15 53.8657 53.0566 2 -9 3 -16 22.2319 55.2701 2 -9 -3 -16 3.11607 43.9243 2 -9 3 -17 103.157 97.3141 2 -9 -3 -17 9.27040 49.2583 2 -9 -3 -18 126.415 107.320 2 -9 -4 20 185.764 99.8636 4 -9 -4 19 131.728 126.319 4 -9 -4 18 137.105 88.1087 4 -9 -4 17 199.517 110.174 4 9 -4 -17-18.4882 38.4241 3 -9 -4 16 209.659 100.093 4 9 -4 -16 96.7442 68.8001 3 -9 -4 15 123.421 69.4185 4 9 -4 -15 55.9085 59.8752 3 -9 -4 14 2.18222 32.6546 4 9 -4 -14 15.9685 59.4841 3 -9 -4 13-9.22571 32.6660 4 9 -4 -13-38.5694 34.8356 3 -9 -4 12 50.5587 33.7776 4 9 -4 -12 4.62410 17.2649 3 -9 -4 11 115.876 72.7229 4 -9 4 11 32.0775 26.0596 2 9 -4 -11 10.0343 29.9029 3 -9 -4 10 173.345 82.6817 4 -9 4 10 185.801 58.7142 2 9 -4 -10 198.152 110.976 3 -9 -4 9 90.0147 59.8910 4 -9 4 9 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7.43972 11.5492 2 -9 4 -12 86.5536 51.6339 2 -9 -4 -12 107.350 83.9987 2 -9 4 -13 117.546 77.4420 2 -9 -4 -13-4.12762 25.4836 2 -9 4 -14 74.2916 91.3544 2 -9 -4 -14 229.069 104.269 2 -9 4 -15 77.6928 65.9579 2 -9 -4 -15 53.1451 75.9413 2 -9 4 -16 13.0175 56.9434 2 -9 -4 -16 130.799 82.0644 2 -9 -4 -17 197.465 107.731 2 -9 -4 -18 66.4950 85.4212 2 -9 -5 20 201.940 107.429 4 -9 -5 19 137.824 108.495 4 -9 -5 18 254.778 121.071 4 -9 -5 17 118.062 94.8101 4 -9 -5 16-46.1901 27.7428 4 9 -5 -16 11.7903 62.6977 3 -9 -5 15 160.856 89.9338 4 9 -5 -15 59.6002 82.8003 3 -9 -5 14 151.099 100.536 4 9 -5 -14 62.5009 71.7544 3 -9 -5 13-71.1734 50.8363 4 9 -5 -13 57.6717 52.1197 3 -9 -5 12 67.1939 66.0193 4 9 -5 -12-10.0180 42.0597 3 -9 -5 11 84.2116 91.7847 4 9 -5 -11-84.0943 58.0837 3 -9 -5 10 128.691 55.4340 4 9 -5 -10 65.9969 65.9813 3 -9 -5 9 14.2097 48.3935 4 -9 5 9 0.16244 19.0439 2 9 -5 -9 21.0397 42.0874 3 -9 -5 8 142.640 65.4244 4 -9 5 8 171.398 52.0049 2 9 -5 -8 149.399 82.3164 3 -9 -5 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-1 51.3320 48.2761 4 -13 3 -1 51.7082 67.7771 2 -13 -3 -2 106.827 79.0359 4 -13 3 -2 48.0123 68.4958 2 -13 -3 -3 221.045 121.731 4 -13 -3 -3 53.6184 71.2314 2 -13 3 -3 96.3859 78.5774 2 -13 -3 -4 96.5717 100.736 2 -13 3 -4 41.9129 56.3373 2 -13 -3 -5 292.596 168.054 2 -13 3 -5 17.9774 51.3396 2 -13 3 -6 11.0610 34.5422 2 -13 3 -7 93.0016 71.8831 2 -13 -4 12 82.8966 106.877 4 -13 -4 11 160.667 113.047 4 -13 -4 10-10.7680 64.7482 4 -13 -4 9-1.02750 37.8435 4 -13 -4 8 215.771 113.786 4 -13 -4 7 18.9777 79.0637 4 13 -4 -7 11.0111 45.1510 3 -13 -4 6-11.9423 54.5852 4 13 -4 -6-66.9907 55.4678 3 -13 -4 5 129.695 96.2823 4 13 -4 -5 50.7001 36.6093 3 -13 -4 4 174.653 115.484 4 13 -4 -4 26.5133 66.5218 3 -13 4 4 93.0408 75.4167 2 -13 -4 3 12.7272 47.8907 4 13 -4 -3-20.9459 27.6062 3 -13 4 3-7.09701 25.5358 2 13 -4 -2-24.1962 56.7875 3 -13 4 2-11.7589 21.3741 2 -13 -4 1 91.0791 70.2210 4 13 -4 -1 34.3158 39.7420 3 -13 4 1 78.9542 48.8193 2 -13 -4 0 190.700 113.997 4 -13 4 0 16.6158 8.33622 2 -13 -4 -1 9.05883 53.9265 4 -13 4 -1 19.0351 51.7904 2 -13 -4 -2 288.310 229.777 4 -13 4 -2 165.512 86.8666 2 -13 -4 -3 62.8020 71.9425 4 -13 4 -3-42.4876 8.08402 2 -13 -4 -4 150.387 82.8089 4 -13 4 -4 22.4245 31.9744 2 -13 4 -5 147.624 88.5638 2 -13 4 -6 246.167 108.412 2 -13 4 -7 20.3462 30.9851 2 -13 -5 7 249.719 134.049 4 -13 -5 6 165.852 116.380 4 13 -5 -6 62.9012 69.7360 3 -13 -5 5 171.624 105.448 4 13 -5 -5 24.7470 55.3101 3 -13 -5 4 53.7036 93.9475 4 13 -5 -4-104.012 67.8045 3 -13 -5 3 167.992 109.319 4 13 -5 -3 58.0545 67.6608 3 -13 -5 2 78.5499 127.504 4 13 -5 -2 39.0868 38.7352 3 -13 5 2 106.904 67.3367 2 13 -5 -1-45.4073 48.5297 3 -13 5 1 9.04134 12.0381 2 13 -5 0-30.9240 20.3654 3 -13 5 0-13.1866 39.6961 2 -13 5 -1 28.8930 21.3395 2 -13 5 -2 2.97185 47.3902 2 -13 5 -3-64.1606 72.8381 2 -13 5 -4-27.2729 15.8949 2 -13 5 -5 33.4434 27.9978 2 -13 5 -6-35.3832 42.6731 2 13 -6 -5 4.05092 31.6801 3 13 -6 -4 3.62442 40.5791 3 13 -6 -3 86.2676 59.5687 3 13 -6 -2-1.41682 30.8255 3 13 -6 -1 13.6075 41.4125 3 13 -6 0-0.26501 41.1562 3 -13 6 0 33.0543 21.4747 2 13 -6 1 10.8955 30.0673 3 -13 6 -1 53.3423 19.8387 2 -13 6 -2-57.0967 42.2725 2 -13 6 -3-8.24206 42.8051 2 -13 6 -4 48.5603 49.7005 2 -13 6 -5 45.8836 14.8217 2 -13 6 -6 202.934 108.616 2 13 -7 -3 124.144 82.3471 3 13 -7 -2 37.0971 66.1241 3 13 -7 -1 48.2492 50.2548 3 -13 7 -3 117.067 79.4586 2 -13 7 -4-4.86316 24.0033 2 -14 0 7 55.4820 49.9924 4 -14 0 7-16.0999 42.5207 2 -14 0 6 145.426 119.208 2 -14 0 5-38.6501 46.6904 2 -14 0 4 55.0916 56.6446 2 -14 0 3 140.137 89.2298 2 -14 0 2 233.359 116.653 2 -14 0 1 142.379 107.617 2 -14 0 0 103.999 79.0132 2 -14 0 -1 12.2603 40.6571 2 -14 0 -2 125.746 94.9967 2 -14 0 -3 25.3038 84.1217 2 -14 -1 8 26.8002 54.7149 4 -14 1 8 63.8640 49.3099 2 -14 -1 7 92.6725 68.5653 4 -14 1 7 34.8002 24.3778 2 -14 -1 6 26.3353 68.6356 4 -14 1 6 73.6679 83.1951 2 -14 -1 5 42.9805 60.2342 4 -14 1 5 18.8570 53.9090 2 -14 -1 4 0.16575 43.9788 4 -14 1 4 74.4617 54.1636 2 -14 -1 3-3.85820 65.5706 4 -14 1 3-60.1980 39.0733 2 -14 -1 2 134.780 135.804 2 -14 1 2-26.8502 43.3091 2 -14 -1 1 191.287 115.148 2 -14 1 1-33.2834 31.5910 2 -14 -1 0 47.8069 86.4252 2 -14 1 0 60.8388 70.5140 2 -14 -1 -1 91.3186 77.1998 2 -14 1 -1 185.461 89.2597 2 -14 -1 -2 109.515 105.326 2 -14 1 -2 71.8350 64.2786 2 -14 1 -3 238.378 112.055 2 -14 -2 9-10.5346 28.8158 4 -14 -2 8 59.8688 67.8387 4 -14 -2 7 167.084 85.5274 4 -14 -2 6 23.8137 65.8467 4 -14 2 6 148.381 102.600 2 -14 -2 5 121.364 81.2580 4 -14 2 5 218.700 120.173 2 -14 -2 4-11.5725 39.6870 4 -14 2 4 35.1220 19.1471 2 -14 -2 3-14.3149 10.1454 4 -14 2 3-2.41933 32.2115 2 -14 -2 2-55.0383 29.8279 4 -14 2 2 35.0682 28.5897 2 -14 -2 1-62.2386 61.2870 4 -14 -2 1 200.966 122.328 2 -14 2 1 214.230 109.454 2 -14 -2 0 100.732 81.0938 4 -14 -2 0 175.845 107.280 2 -14 2 0 134.047 74.5859 2 -14 2 -1 74.2067 79.5296 2 -14 2 -2 84.4535 71.7060 2 -14 2 -3-33.4226 11.5144 2 -14 2 -4 86.5124 59.2210 2 -14 -3 9-36.7862 42.0816 4 -14 -3 8 75.1689 79.8077 4 -14 -3 7 127.538 101.656 4 -14 -3 6 62.6248 65.1132 4 -14 -3 5 1.46449 63.6085 4 -14 -3 4 94.0927 90.9978 4 -14 3 4 179.896 104.739 2 -14 -3 3 197.488 115.175 4 -14 3 3 176.117 84.2085 2 -14 -3 2 76.8606 81.0575 4 -14 3 2 44.4296 67.1737 2 -14 -3 1 74.7147 99.5027 4 -14 3 1 104.218 92.6534 2 -14 3 0 13.6612 70.8938 2 -14 3 -1 66.6533 70.7102 2 -14 3 -2 100.426 67.8695 2 -14 3 -3 76.3599 71.7560 2 -14 3 -4 80.0445 75.7847 2 -14 4 2 157.218 92.7418 2 -14 4 1-1.41824 18.1299 2 -14 4 0 26.3537 17.1534 2 -14 4 -1 128.022 76.4694 2 -14 4 -2 133.997 75.1177 2 -14 4 -3 74.0553 71.5239 2 14 -5 -2-16.4735 43.8510 3 -14 5 0 23.1821 40.9522 2 -14 5 -1 44.5544 57.0477 2 -14 5 -2 159.845 88.0654 2 -14 5 -3-49.5402 63.6395 2 -15 1 4 128.783 72.1120 2 -15 1 3 51.2870 71.8240 2 -15 2 2 51.4016 78.5270 2 0 0 0 0.00 0.00 0 TITL exp_7590 in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 0.71073 11.027632 10.766072 19.635158 90.0000 91.7917 90.0000 ZERR 4.00 0.001004 0.000841 0.002034 0.0000 0.0092 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O S UNIT 84 124 12 20 4 TREF HKLF 4 END ; _shelx_hkl_checksum 97052 _shelx_res_file ; TITL exp_7590 in P2(1)/c 2.res created by SHELXL-2017/1 at 19:53:08 on 07-Jan-2024 CELL 0.71073 11.027632 10.766072 19.635158 90.0000 91.7917 90.0000 ZERR 4.00 0.001004 0.000841 0.002034 0.0000 0.0092 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O S UNIT 84 124 12 20 4 omit -2 50.01 size 0.42 0.20 0.09 acta 50.01 L.S. 10 BOND $H OMIT 6 2 1 OMIT 5 8 9 conf htab temp 18 FMAP 2 PLAN 20 WGHT 0.031600 0.013600 FVAR 1.23749 N22 3 0.864643 0.678588 0.669977 11.00000 0.05225 0.03623 = 0.05102 0.00306 -0.00385 0.01454 C23 1 0.736437 0.658933 0.643222 11.00000 0.05033 0.05414 = 0.09829 -0.00721 -0.01409 0.01527 AFIX 23 H23A 2 0.738581 0.638164 0.595204 11.00000 -1.20000 H23B 2 0.692237 0.736376 0.647115 11.00000 -1.20000 AFIX 0 C24 1 0.666891 0.556577 0.680058 11.00000 0.07313 0.05615 = 0.20495 0.00140 0.01446 -0.00317 AFIX 137 H24A 2 0.590665 0.541912 0.656474 11.00000 -1.50000 H24B 2 0.652626 0.582332 0.725925 11.00000 -1.50000 H24C 2 0.713924 0.481527 0.680791 11.00000 -1.50000 AFIX 0 C25 1 0.867721 0.708243 0.745294 11.00000 0.08719 0.05946 = 0.05632 0.00369 -0.00680 0.01816 AFIX 23 H25A 2 0.951411 0.722287 0.759958 11.00000 -1.20000 H25B 2 0.839097 0.636099 0.769643 11.00000 -1.20000 AFIX 0 C26 1 0.793370 0.819646 0.765883 11.00000 0.11872 0.06124 = 0.06111 -0.00286 0.01520 0.02401 AFIX 137 H26A 2 0.804123 0.833377 0.814002 11.00000 -1.50000 H26B 2 0.709188 0.804419 0.755044 11.00000 -1.50000 H26C 2 0.819681 0.891737 0.741652 11.00000 -1.50000 AFIX 0 C27 1 0.914445 0.787367 0.630145 11.00000 0.07384 0.04468 = 0.06443 -0.00010 0.00699 0.00702 AFIX 23 H27A 2 0.905286 0.768693 0.581930 11.00000 -1.20000 H27B 2 0.865104 0.859849 0.638968 11.00000 -1.20000 AFIX 0 C28 1 1.045335 0.820261 0.645534 11.00000 0.07179 0.06839 = 0.15143 -0.00590 0.02052 -0.00231 AFIX 137 H28A 2 1.064308 0.897193 0.623559 11.00000 -1.50000 H28B 2 1.096702 0.755682 0.628966 11.00000 -1.50000 H28C 2 1.058343 0.828854 0.693876 11.00000 -1.50000 AFIX 0 C29 1 0.941626 0.563524 0.661621 11.00000 0.05757 0.04180 = 0.08011 -0.00012 -0.00030 0.01917 AFIX 23 H29A 2 1.021525 0.579523 0.681782 11.00000 -1.20000 H29B 2 0.905901 0.496372 0.687120 11.00000 -1.20000 AFIX 0 C30 1 0.956349 0.520651 0.589229 11.00000 0.09741 0.05510 = 0.09099 -0.01126 0.00909 0.02373 AFIX 137 H30A 2 1.002975 0.445354 0.589154 11.00000 -1.50000 H30B 2 0.997549 0.583607 0.564185 11.00000 -1.50000 H30C 2 0.877894 0.505702 0.568264 11.00000 -1.50000 AFIX 0 C1 1 0.583688 0.105846 0.629353 11.00000 0.03997 0.03741 = 0.04099 -0.00154 -0.00051 0.00083 C2 1 0.487696 0.017226 0.629203 11.00000 0.04365 0.03395 = 0.05250 0.00315 -0.00517 0.00025 C3 1 0.372959 0.046105 0.606507 11.00000 0.04231 0.04762 = 0.05607 0.00278 -0.00174 -0.00547 AFIX 43 H3A 2 0.312492 -0.014135 0.605923 11.00000 -1.20000 AFIX 0 C4 1 0.346886 0.165898 0.584278 11.00000 0.04040 0.04508 = 0.04714 -0.00400 -0.00357 0.01251 C5 1 0.435180 0.256512 0.586970 11.00000 0.05667 0.03850 = 0.05671 -0.00149 -0.00530 0.00857 AFIX 43 H5A 2 0.416335 0.337348 0.573719 11.00000 -1.20000 AFIX 0 C6 1 0.550686 0.227456 0.609168 11.00000 0.04955 0.03356 = 0.06126 -0.00003 -0.00350 -0.00084 AFIX 43 H6A 2 0.609174 0.289699 0.611006 11.00000 -1.20000 AFIX 0 N7 3 0.696082 0.063911 0.649243 11.00000 0.04203 0.03586 = 0.06043 0.00231 -0.00972 -0.00428 S8 5 0.814728 0.145754 0.643589 11.00000 0.04298 0.03789 = 0.06248 -0.00057 -0.00884 -0.00190 O9 4 0.911052 0.077987 0.677985 11.00000 0.05112 0.05131 = 0.09085 0.00742 -0.03033 -0.00017 O10 4 0.803055 0.273355 0.665596 11.00000 0.06500 0.03538 = 0.09427 -0.01201 -0.00340 -0.00645 C11 1 0.848587 0.150250 0.556870 11.00000 0.05737 0.08273 = 0.07012 0.00536 0.00332 0.00366 AFIX 137 H11A 2 0.923935 0.193215 0.551381 11.00000 -1.50000 H11B 2 0.784964 0.192962 0.531955 11.00000 -1.50000 H11C 2 0.855381 0.067033 0.539846 11.00000 -1.50000 AFIX 0 O12 4 0.518920 -0.097962 0.655606 11.00000 0.05699 0.03974 = 0.09732 0.02161 -0.02457 -0.01011 C13 1 0.444933 -0.200342 0.639593 11.00000 0.04112 0.03080 = 0.06893 0.01211 -0.00284 0.00170 C14 1 0.435316 -0.243611 0.574434 11.00000 0.06885 0.05998 = 0.05942 0.01464 0.00452 -0.00504 AFIX 43 H14A 2 0.471834 -0.201598 0.539124 11.00000 -1.20000 AFIX 0 C15 1 0.369897 -0.351639 0.561920 11.00000 0.07729 0.05812 = 0.06390 -0.00821 -0.00485 -0.00199 AFIX 43 H15A 2 0.362559 -0.382462 0.517737 11.00000 -1.20000 AFIX 0 C16 1 0.316177 -0.413234 0.613667 11.00000 0.05255 0.03837 = 0.09347 0.00390 0.00016 -0.00676 AFIX 43 H16A 2 0.272162 -0.485449 0.604827 11.00000 -1.20000 AFIX 0 C17 1 0.327492 -0.368113 0.678500 11.00000 0.07435 0.05182 = 0.07934 0.00575 0.01977 -0.01429 AFIX 43 H17A 2 0.291625 -0.410340 0.713952 11.00000 -1.20000 AFIX 0 C18 1 0.391658 -0.260430 0.691912 11.00000 0.06944 0.04809 = 0.05784 0.00006 0.00899 -0.00179 AFIX 43 H18A 2 0.398465 -0.229272 0.736042 11.00000 -1.20000 AFIX 0 N19 3 0.226960 0.194548 0.558378 11.00000 0.05289 0.05882 = 0.06377 -0.00793 -0.00411 0.01201 O20 4 0.150730 0.111369 0.553562 11.00000 0.04481 0.07924 = 0.15514 0.01186 -0.01799 -0.00022 O21 4 0.203069 0.302170 0.540801 11.00000 0.07625 0.06190 = 0.09121 -0.00516 -0.02398 0.02747 HKLF 4 REM exp_7590 in P2(1)/c REM R1 = 0.0657 for 2549 Fo > 4sig(Fo) and 0.1210 for all 4094 data REM 276 parameters refined using 0 restraints END WGHT 0.0316 0.0136 REM Instructions for potential hydrogen bonds EQIV $1 x, y+1, z HTAB C23 O12_$1 HTAB C24 O10 EQIV $2 -x+2, y+1/2, -z+3/2 HTAB C25 O9_$2 HTAB C26 O9_$1 HTAB C27 O9_$1 HTAB C6 O10 EQIV $3 x+1, y, z HTAB C11 O20_$3 EQIV $4 -x+1, -y, -z+1 HTAB C11 O20_$4 REM Highest difference peak 0.161, deepest hole -0.229, 1-sigma level 0.039 Q1 1 0.1627 0.1326 0.6056 11.00000 0.05 0.16 Q2 1 0.1565 0.0983 0.6154 11.00000 0.05 0.16 Q3 1 0.9316 0.6376 0.7801 11.00000 0.05 0.16 Q4 1 0.1889 0.1223 0.5324 11.00000 0.05 0.15 Q5 1 0.8424 0.7343 0.5795 11.00000 0.05 0.14 Q6 1 0.9774 0.0423 0.6853 11.00000 0.05 0.14 Q7 1 0.6937 0.1402 0.6757 11.00000 0.05 0.14 Q8 1 0.9679 0.0671 0.6943 11.00000 0.05 0.14 Q9 1 0.5272 -0.1238 0.6013 11.00000 0.05 0.14 Q10 1 0.4775 0.2378 0.6316 11.00000 0.05 0.14 Q11 1 0.7747 0.1363 0.5178 11.00000 0.05 0.14 Q12 1 0.6399 0.0711 0.6483 11.00000 0.05 0.14 Q13 1 1.1762 0.7617 0.5768 11.00000 0.05 0.14 Q14 1 0.8997 0.1216 0.6711 11.00000 0.05 0.13 Q15 1 0.5868 -0.1798 0.7101 11.00000 0.05 0.13 Q16 1 0.7049 0.5527 0.6331 11.00000 0.05 0.13 Q17 1 0.5539 0.0580 0.6120 11.00000 0.05 0.13 Q18 1 0.7033 0.4610 0.7721 11.00000 0.05 0.13 Q19 1 0.0929 0.1969 0.6090 11.00000 0.05 0.13 Q20 1 1.0970 0.6624 0.7165 11.00000 0.05 0.13 ; _shelx_res_checksum 56355 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group N N22 0.8646(2) 0.6786(2) 0.66998(12) 0.0466(7) Uani d 1 . . C C23 0.7364(3) 0.6589(3) 0.6432(2) 0.0679(10) Uani d 1 . . H H23A 0.738581 0.638164 0.595204 0.082 Uiso calc 1 . . H H23B 0.692237 0.736376 0.647115 0.082 Uiso calc 1 . . C C24 0.6669(4) 0.5566(3) 0.6801(3) 0.1112(17) Uani d 1 . . H H24A 0.590665 0.541912 0.656474 0.167 Uiso calc 1 . . H H24B 0.652626 0.582332 0.725925 0.167 Uiso calc 1 . . H H24C 0.713924 0.481527 0.680791 0.167 Uiso calc 1 . . C C25 0.8677(4) 0.7082(3) 0.74529(16) 0.0678(10) Uani d 1 . . H H25A 0.951411 0.722287 0.759958 0.081 Uiso calc 1 . . H H25B 0.839097 0.636099 0.769643 0.081 Uiso calc 1 . . C C26 0.7934(4) 0.8196(3) 0.76588(18) 0.0801(12) Uani d 1 . . H H26A 0.804123 0.833377 0.814002 0.120 Uiso calc 1 . . H H26B 0.709188 0.804419 0.755044 0.120 Uiso calc 1 . . H H26C 0.819681 0.891737 0.741652 0.120 Uiso calc 1 . . C C27 0.9144(3) 0.7874(3) 0.63015(17) 0.0609(10) Uani d 1 . . H H27A 0.905286 0.768693 0.581930 0.073 Uiso calc 1 . . H H27B 0.865104 0.859849 0.638968 0.073 Uiso calc 1 . . C C28 1.0453(4) 0.8203(3) 0.6455(2) 0.0968(15) Uani d 1 . . H H28A 1.064308 0.897193 0.623559 0.145 Uiso calc 1 . . H H28B 1.096702 0.755682 0.628966 0.145 Uiso calc 1 . . H H28C 1.058343 0.828854 0.693876 0.145 Uiso calc 1 . . C C29 0.9416(3) 0.5635(3) 0.66162(18) 0.0599(9) Uani d 1 . . H H29A 1.021525 0.579523 0.681782 0.072 Uiso calc 1 . . H H29B 0.905901 0.496372 0.687120 0.072 Uiso calc 1 . . C C30 0.9563(4) 0.5207(3) 0.58923(19) 0.0810(12) Uani d 1 . . H H30A 1.002975 0.445354 0.589154 0.122 Uiso calc 1 . . H H30B 0.997549 0.583607 0.564185 0.122 Uiso calc 1 . . H H30C 0.877894 0.505702 0.568264 0.122 Uiso calc 1 . . C C1 0.5837(3) 0.1058(3) 0.62935(14) 0.0395(7) Uani d 1 . . C C2 0.4877(3) 0.0172(3) 0.62920(15) 0.0435(8) Uani d 1 . . C C3 0.3730(3) 0.0461(3) 0.60651(15) 0.0487(8) Uani d 1 . . H H3A 0.312492 -0.014135 0.605923 0.058 Uiso calc 1 . . C C4 0.3469(3) 0.1659(3) 0.58428(15) 0.0443(8) Uani d 1 . . C C5 0.4352(3) 0.2565(3) 0.58697(16) 0.0508(9) Uani d 1 . . H H5A 0.416335 0.337348 0.573719 0.061 Uiso calc 1 . . C C6 0.5507(3) 0.2275(3) 0.60917(15) 0.0482(8) Uani d 1 . . H H6A 0.609174 0.289699 0.611006 0.058 Uiso calc 1 . . N N7 0.6961(2) 0.0639(2) 0.64924(12) 0.0463(7) Uani d 1 . . S S8 0.81473(7) 0.14575(7) 0.64359(4) 0.0480(2) Uani d 1 . . O O9 0.9111(2) 0.07799(19) 0.67799(12) 0.0651(7) Uani d 1 . . O O10 0.8031(2) 0.27336(18) 0.66560(12) 0.0650(7) Uani d 1 . . C C11 0.8486(3) 0.1503(3) 0.55687(17) 0.0700(10) Uani d 1 . . H H11A 0.923935 0.193215 0.551381 0.105 Uiso calc 1 . . H H11B 0.784964 0.192962 0.531955 0.105 Uiso calc 1 . . H H11C 0.855381 0.067033 0.539846 0.105 Uiso calc 1 . . O O12 0.5189(2) -0.09796(19) 0.65561(12) 0.0652(7) Uani d 1 . . C C13 0.4449(3) -0.2003(3) 0.63959(18) 0.0470(8) Uani d 1 . . C C14 0.4353(3) -0.2436(3) 0.57443(18) 0.0627(10) Uani d 1 . . H H14A 0.471834 -0.201598 0.539124 0.075 Uiso calc 1 . . C C15 0.3699(3) -0.3516(3) 0.56192(18) 0.0666(10) Uani d 1 . . H H15A 0.362559 -0.382462 0.517737 0.080 Uiso calc 1 . . C C16 0.3162(3) -0.4132(3) 0.6137(2) 0.0615(10) Uani d 1 . . H H16A 0.272162 -0.485449 0.604827 0.074 Uiso calc 1 . . C C17 0.3275(3) -0.3681(3) 0.6785(2) 0.0681(11) Uani d 1 . . H H17A 0.291625 -0.410340 0.713952 0.082 Uiso calc 1 . . C C18 0.3917(3) -0.2604(3) 0.69191(17) 0.0583(9) Uani d 1 . . H H18A 0.398465 -0.229272 0.736042 0.070 Uiso calc 1 . . N N19 0.2270(3) 0.1945(3) 0.55838(14) 0.0586(8) Uani d 1 . . O O20 0.1507(2) 0.1114(3) 0.55356(16) 0.0935(9) Uani d 1 . . O O21 0.2031(2) 0.3022(2) 0.54080(13) 0.0770(8) Uani d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 N22 0.0522(17) 0.0362(15) 0.0510(16) 0.0145(12) -0.0039(14) 0.0031(12) C23 0.050(2) 0.054(2) 0.098(3) 0.0153(18) -0.014(2) -0.007(2) C24 0.073(3) 0.056(3) 0.205(5) -0.003(2) 0.014(3) 0.001(3) C25 0.087(3) 0.059(2) 0.056(2) 0.018(2) -0.007(2) 0.0037(18) C26 0.119(4) 0.061(2) 0.061(2) 0.024(2) 0.015(2) -0.0029(19) C27 0.074(3) 0.045(2) 0.064(2) 0.0070(18) 0.007(2) -0.0001(17) C28 0.072(3) 0.068(3) 0.151(4) -0.002(2) 0.021(3) -0.006(3) C29 0.058(2) 0.0418(19) 0.080(2) 0.0192(17) 0.000(2) -0.0001(17) C30 0.097(3) 0.055(2) 0.091(3) 0.024(2) 0.009(3) -0.011(2) C1 0.040(2) 0.0374(17) 0.0410(17) 0.0008(15) -0.0005(15) -0.0015(14) C2 0.044(2) 0.0340(18) 0.0525(19) 0.0003(15) -0.0052(16) 0.0032(15) C3 0.042(2) 0.0476(19) 0.056(2) -0.0055(16) -0.0017(17) 0.0028(16) C4 0.040(2) 0.045(2) 0.0471(18) 0.0125(16) -0.0036(15) -0.0040(15) C5 0.057(2) 0.0385(19) 0.057(2) 0.0086(17) -0.0053(18) -0.0015(15) C6 0.050(2) 0.0336(18) 0.061(2) -0.0008(15) -0.0035(18) 0.0000(15) N7 0.0420(16) 0.0359(14) 0.0604(16) -0.0043(12) -0.0097(13) 0.0023(12) S8 0.0430(5) 0.0379(5) 0.0625(5) -0.0019(4) -0.0088(4) -0.0006(4) O9 0.0511(15) 0.0513(14) 0.0908(17) -0.0002(11) -0.0303(13) 0.0074(12) O10 0.0650(16) 0.0354(13) 0.0943(18) -0.0065(11) -0.0034(14) -0.0120(12) C11 0.057(2) 0.083(3) 0.070(2) 0.004(2) 0.003(2) 0.005(2) O12 0.0570(15) 0.0397(13) 0.0973(18) -0.0101(11) -0.0246(13) 0.0216(12) C13 0.041(2) 0.0308(17) 0.069(2) 0.0017(15) -0.0028(18) 0.0121(17) C14 0.069(3) 0.060(2) 0.059(2) -0.005(2) 0.005(2) 0.0146(19) C15 0.077(3) 0.058(2) 0.064(2) -0.002(2) -0.005(2) -0.008(2) C16 0.053(2) 0.0384(19) 0.093(3) -0.0068(16) 0.000(2) 0.004(2) C17 0.074(3) 0.052(2) 0.079(3) -0.014(2) 0.020(2) 0.006(2) C18 0.069(2) 0.048(2) 0.058(2) -0.0018(18) 0.009(2) 0.0001(17) N19 0.053(2) 0.059(2) 0.0638(18) 0.0120(17) -0.0041(16) -0.0079(16) O20 0.0448(17) 0.0792(19) 0.155(3) -0.0002(15) -0.0180(17) 0.0119(18) O21 0.0763(19) 0.0619(17) 0.0912(18) 0.0275(14) -0.0240(15) -0.0052(14) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C23 N22 C25 . . 111.3(3) ? C23 N22 C29 . . 111.7(2) ? C25 N22 C29 . . 106.5(2) ? C23 N22 C27 . . 106.2(2) ? C25 N22 C27 . . 110.1(2) ? C29 N22 C27 . . 111.2(2) ? N22 C23 C24 . . 114.4(3) ? N22 C23 H23A . . 108.7 ? C24 C23 H23A . . 108.7 ? N22 C23 H23B . . 108.7 ? C24 C23 H23B . . 108.7 ? H23A C23 H23B . . 107.6 ? C23 C24 H24A . . 109.5 ? C23 C24 H24B . . 109.5 ? H24A C24 H24B . . 109.5 ? C23 C24 H24C . . 109.5 ? H24A C24 H24C . . 109.5 ? H24B C24 H24C . . 109.5 ? N22 C25 C26 . . 115.6(3) ? N22 C25 H25A . . 108.4 ? C26 C25 H25A . . 108.4 ? N22 C25 H25B . . 108.4 ? C26 C25 H25B . . 108.4 ? H25A C25 H25B . . 107.4 ? C25 C26 H26A . . 109.5 ? C25 C26 H26B . . 109.5 ? H26A C26 H26B . . 109.5 ? C25 C26 H26C . . 109.5 ? H26A C26 H26C . . 109.5 ? H26B C26 H26C . . 109.5 ? C28 C27 N22 . . 115.9(3) ? C28 C27 H27A . . 108.3 ? N22 C27 H27A . . 108.3 ? C28 C27 H27B . . 108.3 ? N22 C27 H27B . . 108.3 ? H27A C27 H27B . . 107.4 ? C27 C28 H28A . . 109.5 ? C27 C28 H28B . . 109.5 ? H28A C28 H28B . . 109.5 ? C27 C28 H28C . . 109.5 ? H28A C28 H28C . . 109.5 ? H28B C28 H28C . . 109.5 ? C30 C29 N22 . . 115.5(3) ? C30 C29 H29A . . 108.4 ? N22 C29 H29A . . 108.4 ? C30 C29 H29B . . 108.4 ? N22 C29 H29B . . 108.4 ? H29A C29 H29B . . 107.5 ? C29 C30 H30A . . 109.5 ? C29 C30 H30B . . 109.5 ? H30A C30 H30B . . 109.5 ? C29 C30 H30C . . 109.5 ? H30A C30 H30C . . 109.5 ? H30B C30 H30C . . 109.5 ? N7 C1 C6 . . 127.6(3) ? N7 C1 C2 . . 116.6(3) ? C6 C1 C2 . . 115.8(3) ? C3 C2 O12 . . 123.0(3) ? C3 C2 C1 . . 122.0(3) ? O12 C2 C1 . . 115.0(3) ? C2 C3 C4 . . 119.7(3) ? C2 C3 H3A . . 120.2 ? C4 C3 H3A . . 120.2 ? C5 C4 C3 . . 120.4(3) ? C5 C4 N19 . . 120.2(3) ? C3 C4 N19 . . 119.4(3) ? C6 C5 C4 . . 120.0(3) ? C6 C5 H5A . . 120.0 ? C4 C5 H5A . . 120.0 ? C5 C6 C1 . . 122.0(3) ? C5 C6 H6A . . 119.0 ? C1 C6 H6A . . 119.0 ? C1 N7 S8 . . 122.7(2) ? O9 S8 O10 . . 114.35(14) ? O9 S8 N7 . . 106.51(13) ? O10 S8 N7 . . 115.20(13) ? O9 S8 C11 . . 107.03(16) ? O10 S8 C11 . . 106.68(16) ? N7 S8 C11 . . 106.53(16) ? S8 C11 H11A . . 109.5 ? S8 C11 H11B . . 109.5 ? H11A C11 H11B . . 109.5 ? S8 C11 H11C . . 109.5 ? H11A C11 H11C . . 109.5 ? H11B C11 H11C . . 109.5 ? C2 O12 C13 . . 119.0(2) ? C14 C13 C18 . . 121.5(3) ? C14 C13 O12 . . 120.5(3) ? C18 C13 O12 . . 117.8(3) ? C13 C14 C15 . . 118.6(3) ? C13 C14 H14A . . 120.7 ? C15 C14 H14A . . 120.7 ? C16 C15 C14 . . 120.8(3) ? C16 C15 H15A . . 119.6 ? C14 C15 H15A . . 119.6 ? C15 C16 C17 . . 119.5(3) ? C15 C16 H16A . . 120.2 ? C17 C16 H16A . . 120.2 ? C16 C17 C18 . . 120.6(3) ? C16 C17 H17A . . 119.7 ? C18 C17 H17A . . 119.7 ? C13 C18 C17 . . 119.1(3) ? C13 C18 H18A . . 120.5 ? C17 C18 H18A . . 120.5 ? O20 N19 O21 . . 121.5(3) ? O20 N19 C4 . . 119.4(3) ? O21 N19 C4 . . 119.1(3) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag N22 C23 . 1.508(4) ? N22 C25 . 1.512(4) ? N22 C29 . 1.514(3) ? N22 C27 . 1.520(4) ? C23 C24 . 1.536(5) ? C23 H23A . 0.9700 ? C23 H23B . 0.9700 ? C24 H24A . 0.9600 ? C24 H24B . 0.9600 ? C24 H24C . 0.9600 ? C25 C26 . 1.515(4) ? C25 H25A . 0.9700 ? C25 H25B . 0.9700 ? C26 H26A . 0.9600 ? C26 H26B . 0.9600 ? C26 H26C . 0.9600 ? C27 C28 . 1.508(5) ? C27 H27A . 0.9700 ? C27 H27B . 0.9700 ? C28 H28A . 0.9600 ? C28 H28B . 0.9600 ? C28 H28C . 0.9600 ? C29 C30 . 1.508(4) ? C29 H29A . 0.9700 ? C29 H29B . 0.9700 ? C30 H30A . 0.9600 ? C30 H30B . 0.9600 ? C30 H30C . 0.9600 ? C1 N7 . 1.365(4) ? C1 C6 . 1.412(4) ? C1 C2 . 1.425(4) ? C2 C3 . 1.364(4) ? C2 O12 . 1.383(3) ? C3 C4 . 1.389(4) ? C3 H3A . 0.9300 ? C4 C5 . 1.378(4) ? C4 N19 . 1.436(4) ? C5 C6 . 1.370(4) ? C5 H5A . 0.9300 ? C6 H6A . 0.9300 ? N7 S8 . 1.584(2) ? S8 O9 . 1.439(2) ? S8 O10 . 1.447(2) ? S8 C11 . 1.755(3) ? C11 H11A . 0.9600 ? C11 H11B . 0.9600 ? C11 H11C . 0.9600 ? O12 C13 . 1.401(3) ? C13 C14 . 1.363(4) ? C13 C18 . 1.363(4) ? C14 C15 . 1.387(5) ? C14 H14A . 0.9300 ? C15 C16 . 1.364(5) ? C15 H15A . 0.9300 ? C16 C17 . 1.365(5) ? C16 H16A . 0.9300 ? C17 C18 . 1.379(4) ? C17 H17A . 0.9300 ? C18 H18A . 0.9300 ? N19 O20 . 1.230(3) ? N19 O21 . 1.235(3) ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_D _geom_hbond_site_symmetry_H _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C11 H11A O20 1_555 1_555 1_655 0.96 2.65 3.360(4) 131 yes C11 H11C O20 1_555 1_555 3_656 0.96 2.66 3.555(4) 156 yes C17 H17A N7 1_555 1_555 2_646 0.93 2.70 3.478(4) 142 yes C24 H24C O10 1_555 1_555 1_555 0.96 2.47 3.415(4) 168 yes C25 H25A O9 1_555 1_555 2_756 0.97 2.47 3.155(5) 128 yes C26 H26C O9 1_555 1_555 1_565 0.96 2.58 3.541(4) 175 yes C27 H27B O9 1_555 1_555 1_565 0.97 2.52 3.267(4) 134 yes C14 H14A Cg1 1_555 1_555 3_656 0.93 3.07 3.951(5) 158 yes C24 H24A Cg2 1_555 1_555 1_565 0.96 2.88 3.608(5) 134 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C25 N22 C23 C24 . . . . -57.0(4) ? C29 N22 C23 C24 . . . . 61.9(4) ? C27 N22 C23 C24 . . . . -176.7(3) ? C23 N22 C25 C26 . . . . -56.6(4) ? C29 N22 C25 C26 . . . . -178.6(3) ? C27 N22 C25 C26 . . . . 60.8(4) ? C23 N22 C27 C28 . . . . -176.8(3) ? C25 N22 C27 C28 . . . . 62.7(4) ? C29 N22 C27 C28 . . . . -55.0(4) ? C23 N22 C29 C30 . . . . 61.3(4) ? C25 N22 C29 C30 . . . . -177.1(3) ? C27 N22 C29 C30 . . . . -57.2(4) ? N7 C1 C2 C3 . . . . -176.0(3) ? C6 C1 C2 C3 . . . . 4.3(4) ? N7 C1 C2 O12 . . . . 5.9(4) ? C6 C1 C2 O12 . . . . -173.7(3) ? O12 C2 C3 C4 . . . . 176.3(3) ? C1 C2 C3 C4 . . . . -1.6(5) ? C2 C3 C4 C5 . . . . -2.0(4) ? C2 C3 C4 N19 . . . . 178.0(3) ? C3 C4 C5 C6 . . . . 2.6(5) ? N19 C4 C5 C6 . . . . -177.4(3) ? C4 C5 C6 C1 . . . . 0.4(5) ? N7 C1 C6 C5 . . . . 176.7(3) ? C2 C1 C6 C5 . . . . -3.8(4) ? C6 C1 N7 S8 . . . . -8.2(4) ? C2 C1 N7 S8 . . . . 172.3(2) ? C1 N7 S8 O9 . . . . 172.0(2) ? C1 N7 S8 O10 . . . . 44.0(3) ? C1 N7 S8 C11 . . . . -74.0(3) ? C3 C2 O12 C13 . . . . 20.9(4) ? C1 C2 O12 C13 . . . . -161.0(3) ? C2 O12 C13 C14 . . . . 66.3(4) ? C2 O12 C13 C18 . . . . -118.9(3) ? C18 C13 C14 C15 . . . . -0.2(5) ? O12 C13 C14 C15 . . . . 174.3(3) ? C13 C14 C15 C16 . . . . 0.1(5) ? C14 C15 C16 C17 . . . . -0.3(6) ? C15 C16 C17 C18 . . . . 0.6(6) ? C14 C13 C18 C17 . . . . 0.6(5) ? O12 C13 C18 C17 . . . . -174.1(3) ? C16 C17 C18 C13 . . . . -0.8(5) ? C5 C4 N19 O20 . . . . 176.9(3) ? C3 C4 N19 O20 . . . . -3.1(4) ? C5 C4 N19 O21 . . . . -2.4(4) ? C3 C4 N19 O21 . . . . 177.6(3) ?