#------------------------------------------------------------------------------ #$Date: 2024-01-20 03:42:15 +0100 (Sat, 20 Jan 2024) $ #$Revision: 289169 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/30/2023012.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023012 loop_ _publ_author_name 'D\"oring, Cindy' 'Jones, Peter G.' _publ_section_title ; Crystal structures of five gold(I) complexes with methylpiperidine ligands ; _journal_coeditor_code YZ2046 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E Crystallographic Communications' _journal_paper_doi 10.1107/S2056989023010940 _journal_volume 80 _journal_year 2023 _chemical_formula_iupac '[Au (C6 H13 N)2] Cl' _chemical_formula_moiety 'C12 H26 Au N2 +, Cl -' _chemical_formula_sum 'C12 H26 Au Cl N2' _chemical_formula_weight 430.76 _chemical_name_systematic ; Bis(4-methylpiperidine-\kN)gold(I) chloride ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 103.946(4) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 6.4068(3) _cell_length_b 25.2542(15) _cell_length_c 9.3395(4) _cell_measurement_reflns_used 8714 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 30.9001 _cell_measurement_theta_min 2.2423 _cell_volume 1466.58(13) _computing_cell_refinement ; CrysAlisPro, Version 1.171.35.21. Rigaku OD (2020) ; _computing_data_collection ; CrysAlisPro, Version 1.171.35.21. Rigaku OD (2020) ; _computing_data_reduction ; CrysAlisPro, Version 1.171.35.21. Rigaku OD (2020) ; _computing_molecular_graphics ; Siemens XP (Siemens, 1994) ; _computing_publication_material ; SHELXL-2018/3 (Sheldrick, 2015) ; _computing_structure_refinement ; SHELXL-2018/3 (Sheldrick, 2015) ; _computing_structure_solution ; SHELXS-97 (Sheldrick, 2008) ; _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean 16.1419 _diffrn_measured_fraction_theta_full 0.994 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measurement_device_type 'Oxford Diffraction Xcalibur, Eos' _diffrn_measurement_method '\w scan' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0679 _diffrn_reflns_av_unetI/netI 0.0357 _diffrn_reflns_limit_h_max 8 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 35 _diffrn_reflns_limit_k_min -35 _diffrn_reflns_limit_l_max 12 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_number 49187 _diffrn_reflns_theta_full 30.000 _diffrn_reflns_theta_max 30.030 _diffrn_reflns_theta_min 2.387 _diffrn_source 'Enhance (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 10.193 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.39752 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (CrysAlisPro; Rigaku OD, 2020) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.951 _exptl_crystal_density_method 'not measured' _exptl_crystal_description lath _exptl_crystal_F_000 832 _exptl_crystal_size_max 0.21 _exptl_crystal_size_mid 0.03 _exptl_crystal_size_min 0.01 _refine_diff_density_max 1.128 _refine_diff_density_min -1.569 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.157 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 155 _refine_ls_number_reflns 4248 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.157 _refine_ls_R_factor_all 0.0446 _refine_ls_R_factor_gt 0.0326 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0141P)^2^+1.4591P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0462 _refine_ls_wR_factor_ref 0.0482 _reflns_number_gt 3650 _reflns_number_total 4248 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file yz2046sup1.cif _cod_data_source_block 1 _cod_original_cell_volume 1466.57(12) _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 2023012 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.223 _shelx_estimated_absorpt_t_max 0.905 _shelx_hkl_file ; 0 0 -1 15.9821 74.1285 9 0 0 -1-23.4654 68.2755 11 0 0 2 14649.5 547.766 14 0 0 -2 13777.9 529.490 16 0 0 2 13636.0 507.340 10 0 0 -2 13700.3 438.185 17 0 0 -2 13485.8 525.237 10 0 0 -2 14067.4 552.008 18 0 0 -2 14437.6 582.655 9 0 0 2 12029.0 784.768 19 0 0 -2 14798.0 477.411 8 0 0 -2 15056.7 581.239 12 0 0 2 13805.0 510.138 16 0 0 -2 14718.8 564.203 11 0 0 2 12175.8 900.780 6 0 0 2 14568.3 576.570 9 0 0 -2 15573.2 552.156 14 0 0 2 14785.1 433.310 8 0 0 -2 10974.7 798.120 6 0 0 2 14016.2 558.091 11 0 0 -3 253.928 122.530 13 0 0 3 239.899 240.474 11 0 0 -3-259.555 215.950 3 0 0 3 172.203 179.674 16 0 0 -3-30.9624 145.099 4 0 0 -3 29.3767 97.6392 17 0 0 -3-83.9416 151.387 8 0 0 -3-144.111 221.191 12 0 0 3-91.6385 218.726 14 0 0 3-518.217 547.833 19 0 0 -3 173.858 195.601 10 0 0 3 567.466 632.873 6 0 0 3-122.135 240.099 9 0 0 3 141.691 196.239 10 0 0 3 22.1143 102.591 8 0 0 -3 4.93070 181.113 16 0 0 -4 13507.9 619.814 8 0 0 4 13179.6 709.893 9 0 0 4 13132.8 678.065 14 0 0 4 11233.0 997.103 19 0 0 -4 13067.3 634.011 3 0 0 4 12624.5 608.573 10 0 0 4 12274.4 682.653 11 0 0 4 12364.8 608.244 16 0 0 4 13127.1 1149.97 6 0 0 -4 12852.3 579.217 4 0 0 4 13342.1 488.791 8 0 0 -4 12107.6 513.608 13 0 0 -4 13581.2 616.626 12 0 0 -4 13053.2 488.982 17 0 0 -5 66.0266 214.539 12 0 0 5-29.0356 313.793 14 0 0 5-8.00271 221.958 16 0 0 5 0.26761 221.977 10 0 0 -5 213.706 133.071 17 0 0 -5 88.2896 219.639 4 0 0 -5 24.9433 192.177 8 0 0 5 200.539 307.245 9 0 0 -5-3.32757 116.619 13 0 0 5 30.2332 618.145 19 0 0 -5-149.438 271.871 3 0 0 5 230.079 320.950 11 0 0 5-182.469 142.034 8 0 0 -6 88061.8 2202.12 13 0 0 6 91325.7 2628.94 10 0 0 6 92834.8 2350.75 8 0 0 6 89410.2 2764.92 11 0 0 -6 91269.4 2675.30 3 0 0 6 86735.5 2767.36 9 0 0 -6 94164.0 2657.17 4 0 0 -6 89501.4 2361.86 17 0 0 6 88876.6 3363.93 19 0 0 6 98365.8 3565.31 6 0 0 6 92992.1 2646.32 16 0 0 -6 86503.3 2514.46 12 0 0 6 88015.8 2735.96 14 0 0 7-126.728 393.261 9 0 0 -7 14.9313 310.189 4 0 0 7 171.969 303.086 10 0 0 -7-45.2322 43.0715 13 0 0 7 63.3742 144.045 8 0 0 -7-132.668 337.273 3 0 0 7-176.221 289.594 16 0 0 7-1146.15 449.919 14 0 0 7-395.892 706.227 19 0 0 -7-740.016 398.342 15 0 0 -7-303.035 272.164 12 0 0 8 355.282 425.158 9 0 0 -8 52.0556 344.176 15 0 0 -8-6.91565 234.196 12 0 0 -8-151.135 308.625 4 0 0 8-162.853 282.010 10 0 0 8 10.6746 696.269 19 0 0 -8 457.647 351.543 3 0 0 8 221.644 313.091 16 0 0 -9 381.930 368.172 3 0 0 9-384.591 667.947 19 0 0 9 263.299 313.414 16 0 0 -9 506.398 385.843 15 0 0 9 298.631 324.038 10 0 0 -9-392.435 278.173 12 0 0 9 396.584 425.974 9 0 0 10 10231.7 803.881 16 0 0 -10 9964.24 865.367 3 0 0 10 11202.3 829.939 10 0 0 10 8708.74 1208.33 19 0 0 -10 9659.86 884.365 15 0 0 10 8413.11 896.195 9 0 0 11 835.618 500.386 9 0 0 -11 1164.43 472.416 3 0 0 -11 237.286 479.346 5 0 0 11 504.363 673.755 19 0 0 -11-235.376 425.927 15 0 0 12 15558.1 1333.52 9 0 0 -12 16346.3 1229.99 3 0 0 12 15539.8 1581.09 19 0 1 -1 51613.1 1282.16 9 0 1 -1 52910.4 1283.41 14 0 -1 1 52005.7 1305.98 10 0 1 -1 52030.3 1311.41 11 0 -1 1 51154.0 1275.59 4 0 -1 1 52722.1 1309.61 16 0 -1 -1 52157.2 1312.28 8 0 1 1 52460.3 1276.50 18 0 -1 -1 54636.5 1291.07 14 0 -1 -1 51903.5 1327.10 9 0 1 1 53326.9 1251.03 3 0 -1 1 45371.2 1434.81 19 0 -1 -1 51148.7 1274.52 11 0 1 2 4464.06 237.297 8 0 -1 -2 4400.88 292.491 14 0 -1 2 4462.24 330.579 11 0 1 2 3651.52 286.199 11 0 -1 -2 3898.99 240.698 17 0 1 -2 4033.12 300.952 10 0 1 -2 3951.19 296.358 16 0 -1 -2 4371.26 288.019 8 0 1 -2 4697.29 282.488 14 0 1 2 3906.25 294.486 14 0 1 -2 4420.47 258.869 13 0 1 -2 3823.13 540.883 6 0 -1 -2 4293.57 323.143 9 0 -1 -2 3822.41 237.007 16 0 1 2 4301.79 344.681 9 0 1 2 3268.89 508.037 19 0 1 -2 4058.38 303.176 11 0 -1 -2 3892.50 283.791 11 0 -1 -2 3161.94 547.173 6 0 -1 2 4303.15 307.951 9 0 -1 2 4232.20 303.017 14 0 1 2 3884.61 298.093 18 0 -1 -2 4235.32 239.763 12 0 1 2 3434.31 614.059 6 0 -1 2 2906.42 613.200 6 0 -1 -2 4131.81 278.550 18 0 -1 2 3928.30 284.979 10 0 -1 -2 4105.64 248.737 10 0 1 -2 4014.12 264.622 4 0 -1 2 3533.70 525.487 19 0 1 2 3803.56 234.172 16 0 -1 2 4088.78 204.650 13 0 1 -2 4018.83 378.032 12 0 1 2 4011.04 235.252 10 0 -1 2 3854.93 286.520 16 0 -1 -2 4147.90 256.623 3 0 1 -2 3796.37 291.593 18 0 1 -2 4111.27 300.022 9 0 1 3 1842.20 637.282 6 0 -1 3 1616.53 268.394 16 0 -1 -3 1465.10 252.016 11 0 1 -3 1595.88 220.551 13 0 -1 -3 2071.90 229.124 10 0 -1 -3 1629.24 219.964 16 0 1 -3 1616.42 134.569 17 0 -1 3 1784.89 679.750 6 0 -1 3 1674.91 283.146 9 0 1 -3 1763.23 275.109 10 0 -1 -3 1565.46 225.048 3 0 1 3 1973.93 284.325 14 0 1 -3 1920.89 180.420 8 0 1 3 1540.46 207.310 16 0 -1 3 1703.34 255.411 10 0 1 3 1892.23 295.736 11 0 1 3 1618.14 178.281 8 0 -1 3 1219.91 529.303 19 0 1 -3 1693.92 234.496 4 0 -1 -3 1517.60 245.723 18 0 1 3 1583.07 209.008 10 0 -1 -3 1898.23 220.767 12 0 1 3 1445.95 317.602 9 0 -1 3 1102.63 239.821 14 0 -1 3 1761.73 139.704 8 0 -1 -3 1956.77 191.875 17 0 -1 -3 1890.65 251.592 8 0 -1 3 1832.95 315.165 11 0 1 3 1423.28 561.469 19 0 1 -3 1326.43 254.835 16 0 1 -3 1903.48 336.223 12 0 1 -4 7603.12 418.321 8 0 1 4 7935.06 580.748 9 0 1 4 7923.76 455.572 10 0 1 -4 7307.21 479.047 4 0 -1 4 8173.89 334.785 8 0 -1 -4 7974.61 426.320 12 0 1 4 8682.96 996.113 6 0 -1 4 7282.73 508.457 14 0 -1 4 7579.71 493.633 16 0 -1 4 7383.48 519.747 9 0 -1 4 7334.12 845.331 19 0 1 4 7640.20 454.891 16 0 -1 -4 8399.44 516.404 16 0 1 4 7831.77 383.068 8 0 1 4 7933.43 529.718 11 0 1 4 8269.69 544.646 14 0 -1 -4 7550.20 404.773 4 0 -1 -4 8005.34 388.866 17 0 -1 -4 8163.79 507.254 8 0 -1 4 8197.46 972.483 6 0 -1 -4 8150.21 499.750 10 0 1 4 7900.22 866.690 19 0 -1 4 7547.49 489.278 10 0 1 -4 8779.28 531.427 12 0 -1 4 7126.85 546.235 11 0 -1 -4 8037.23 483.104 3 0 1 -4 8478.81 342.775 17 0 1 -4 7234.38 445.302 13 0 -1 -5 21465.4 640.050 13 0 1 5 22800.6 923.941 16 0 -1 -5 20159.8 947.334 8 0 -1 -5 21571.0 782.495 17 0 -1 5 21737.8 998.636 14 0 1 5 20922.8 1393.22 19 0 1 -5 23663.0 839.542 13 0 1 -5 23384.2 732.346 17 0 1 5 22204.1 782.742 8 0 1 -5 22935.8 978.009 4 0 -1 5 28485.7 1644.73 6 0 1 -5 21709.8 953.408 3 0 -1 -5 24093.6 968.250 3 0 -1 5 22107.7 1014.93 9 0 -1 5 22746.7 1043.88 11 0 -1 -5 22841.3 832.439 12 0 -1 5 23395.8 721.122 8 0 -1 5 21904.5 942.930 10 0 -1 -5 22999.0 878.635 4 0 1 5 21604.0 995.924 14 0 1 5 21724.1 1050.05 9 0 -1 5 21652.0 1449.64 19 0 1 -5 23375.6 950.934 12 0 -1 5 21476.9 945.467 16 0 1 5 27288.5 1633.97 6 0 1 5 22034.5 1001.54 11 0 1 5 23139.0 920.857 10 0 1 -6 56.5100 135.940 13 0 1 6-42.4692 349.389 14 0 1 6 939.745 835.870 6 0 1 6 528.114 361.359 9 0 -1 -6-175.416 318.896 3 0 1 6 51.2819 239.893 16 0 1 -6 49.2979 304.671 3 0 1 6-64.8228 267.623 10 0 1 -6 382.339 135.369 17 0 -1 6-159.021 285.952 16 0 -1 6 373.303 378.827 11 0 -1 -6 334.108 192.929 12 0 -1 6 440.190 141.457 8 0 1 -6 290.327 307.798 4 0 1 6 468.038 183.800 8 0 -1 6 732.639 655.342 19 0 1 6 282.546 716.393 19 0 -1 6 1686.15 877.665 6 0 -1 6 29.6237 256.321 10 0 -1 -6 98.5244 291.620 15 0 1 -6 336.147 284.862 12 0 -1 6 210.177 322.898 9 0 -1 -6 271.645 253.050 4 0 1 7 18416.1 739.081 8 0 1 -7 16908.5 578.690 13 0 -1 -7 19278.6 931.889 4 0 -1 -7 17269.0 787.267 12 0 -1 7 17322.7 1056.06 9 0 -1 -7 18485.9 1015.57 15 0 1 7 16479.2 1008.48 14 0 -1 7 17889.6 953.779 10 0 -1 -7 19569.6 1000.50 3 0 1 -7 17460.2 974.084 3 0 1 7 18385.3 936.664 16 0 1 -7 18504.8 1003.40 4 0 1 -7 17781.0 881.979 12 0 1 7 19489.7 1504.53 19 0 1 7 16606.3 1065.29 9 0 -1 7 18532.8 1082.56 11 0 1 7 19405.2 955.412 10 0 -1 7 17785.0 959.409 16 0 -1 7 15975.7 1400.76 19 0 -1 8 5108.64 949.118 19 0 1 8 4842.75 910.812 19 0 1 8 5721.15 570.240 10 0 -1 8 5730.69 686.208 9 0 1 -8 5473.35 492.532 12 0 1 8 6093.49 408.811 8 0 1 8 5554.23 575.736 16 0 1 -8 6568.60 651.453 3 0 -1 -8 5742.67 470.805 12 0 -1 -8 6312.39 672.876 3 0 1 8 5676.74 714.402 9 0 -1 -8 5775.81 629.195 15 0 -1 8 6105.68 614.185 16 0 1 8 4071.78 591.148 14 0 1 -8 5487.04 559.018 4 0 1 -8 5428.47 643.907 15 0 -1 8 6806.26 638.605 10 0 -1 -8 6429.65 551.485 4 0 -1 9 3331.77 885.099 19 0 1 -9 2030.95 373.396 12 0 1 9 3257.31 470.982 10 0 1 9 2171.91 809.904 19 0 1 -9 1951.91 479.296 15 0 -1 -9 2259.47 504.254 15 0 1 9 2703.71 578.158 9 0 -1 9 1784.90 499.557 9 0 1 -9 2149.88 492.301 3 0 -1 -9 3038.24 526.471 3 0 1 9 3050.69 456.652 16 0 -1 9 2044.82 446.584 16 0 -1 9 2080.74 442.728 10 0 -1 10 2872.80 527.433 10 0 1 10 2290.22 582.507 9 0 -1 10 2591.41 477.513 16 0 1 -10 1849.53 497.229 15 0 -1 -10 3090.25 550.370 3 0 1 10 2008.07 753.105 19 0 -1 10 1736.25 518.345 9 0 -1 10 1905.79 755.801 19 0 1 -10 2352.22 526.663 3 0 -1 -10 2482.89 548.289 15 0 -1 -11 7692.86 819.168 3 0 1 11 9815.71 1226.94 19 0 1 -11 10944.2 999.345 15 0 1 -11 9217.35 894.581 3 0 -1 11 9650.19 985.883 9 0 -1 -11 9979.52 993.129 5 0 -1 11 10924.9 1286.42 19 0 -1 -11 8270.31 877.764 15 0 1 -11 9612.78 933.957 5 0 1 11 9435.97 994.210 9 0 1 12 811.777 757.015 19 0 -1 -12 786.805 513.487 15 0 -1 -12-493.822 513.363 3 0 -1 12 685.649 508.568 9 0 -1 12-268.090 659.627 19 0 1 12-110.017 488.510 9 0 -1 -12 212.676 524.655 5 0 1 -12 265.096 452.525 3 0 -2 1 16794.9 551.136 4 0 -2 -1 17033.4 462.377 3 0 2 1 16088.5 478.771 18 0 -2 1 16320.2 659.844 19 0 -2 1 17010.9 571.750 16 0 2 -1 16597.0 538.432 11 0 -2 1 16590.2 471.500 9 0 -2 -1 16144.2 590.341 8 0 -2 1 16418.2 564.857 10 0 -2 -1 16301.0 512.124 14 0 2 1 16732.9 533.107 15 0 2 1 17179.6 464.519 3 0 2 -1 16649.0 480.845 9 0 2 1 16817.7 567.859 8 0 -2 -1 17137.9 483.646 18 0 2 -1 14133.3 639.957 6 0 -2 1 18373.5 570.354 13 0 2 -1 16142.8 499.646 2 0 -2 -1 15950.8 544.456 9 0 -2 -2 7819.56 373.712 18 0 -2 -2 7429.63 376.158 14 0 2 2 6519.00 604.973 19 0 -2 2 7054.33 419.611 11 0 -2 -2 7534.52 313.639 16 0 2 -2 7807.54 393.337 9 0 -2 2 7460.89 371.581 9 0 -2 -2 7561.28 399.717 17 0 2 -2 7440.14 276.025 7 0 -2 -2 7584.29 404.422 15 0 2 -2 7745.14 439.024 10 0 -2 -2 8129.35 353.836 3 0 2 2 7783.68 458.262 9 0 -2 2 7227.38 414.185 10 0 2 -2 7796.39 380.693 14 0 -2 2 7764.17 663.135 19 0 2 2 7171.09 700.493 6 0 2 2 7723.01 313.519 10 0 2 -2 7856.05 419.484 13 0 -2 2 6384.49 699.972 6 0 2 2 7651.66 332.913 3 0 2 -2 7610.60 425.836 11 0 -2 2 7214.82 330.529 13 0 2 -2 7631.97 578.012 12 0 -2 -2 6443.97 638.109 6 0 2 2 7184.21 374.472 18 0 -2 -2 7398.95 374.670 11 0 -2 -2 7916.84 437.642 8 0 2 -2 7805.42 420.163 4 0 2 -2 6104.38 649.372 6 0 2 2 7678.96 382.258 8 0 -2 -2 7527.75 448.655 9 0 2 -2 7422.33 438.697 16 0 2 2 7879.64 317.644 16 0 2 2 8249.59 403.706 14 0 -2 -2 7421.46 309.910 10 0 -2 2 7500.93 424.545 16 0 -2 -3 88914.6 2161.83 12 0 2 3 92049.3 2908.93 6 0 2 -3 88693.5 2111.10 8 0 2 3 78057.1 2725.27 19 0 2 3 90945.7 2471.15 9 0 2 3 87019.3 2344.05 11 0 2 -3 91747.6 2419.87 9 0 -2 3 86740.9 2373.05 16 0 -2 3 86254.5 2876.53 6 0 -2 -3 90013.6 2360.91 18 0 -2 3 88365.6 2415.77 11 0 -2 -3 88874.9 2265.18 10 0 2 -3 91862.1 2473.00 16 0 2 -3 92089.0 2469.57 10 0 2 3 87608.0 2252.18 8 0 -2 3 91755.0 2202.78 13 0 -2 -3 92498.2 2299.44 17 0 -2 -3 88333.8 2375.72 11 0 2 3 89873.6 2371.57 14 0 2 -3 87935.4 2363.87 13 0 -2 -3 90541.4 2366.60 15 0 2 3 89789.0 2249.22 16 0 2 3 89251.3 2243.31 10 0 -2 -3 92193.1 2435.33 8 0 -2 -3 92597.9 2294.41 3 0 -2 -3 90105.7 2271.31 16 0 -2 3 87234.0 2838.99 19 0 2 -3 89338.1 2532.60 12 0 -2 3 87683.4 2348.16 9 0 2 -3 88002.8 2368.52 4 0 2 -3 87345.3 2085.72 17 0 2 -3 80843.7 2069.70 7 0 -2 3 86143.5 2367.65 10 0 -2 -4 1572.90 249.677 16 0 2 4 2127.98 721.467 6 0 2 -4 1333.31 171.226 8 0 -2 -4 1633.00 211.978 17 0 2 4 1577.40 232.190 16 0 2 -4 1274.37 283.709 13 0 -2 4 2040.95 325.310 10 0 -2 -4 1623.44 269.092 3 0 -2 4 1511.29 680.249 6 0 -2 4 1202.71 582.980 19 0 2 -4 1427.23 332.096 12 0 -2 -4 1635.72 239.083 10 0 2 4 1515.57 541.727 19 0 -2 -4 1394.02 297.395 8 0 -2 4 1453.88 292.783 16 0 2 4 2002.93 388.909 9 0 -2 4 1901.12 314.856 9 0 2 4 1608.78 308.384 14 0 -2 -4 1341.05 301.977 15 0 2 -4 1316.90 125.871 17 0 2 4 1690.59 218.470 8 0 2 -4 1739.54 301.229 4 0 -2 -4 1752.00 200.657 12 0 -2 4 1200.37 332.558 11 0 2 4 1771.37 249.158 10 0 -2 5 1966.00 416.937 11 0 -2 -5 2193.56 236.963 12 0 2 -5 2080.75 353.789 4 0 -2 5 2220.59 803.347 6 0 -2 5 1642.03 341.387 9 0 2 -5 2388.43 320.705 13 0 2 5 2115.55 294.114 16 0 2 -5 1952.22 163.284 17 0 -2 5 2040.72 333.264 10 0 -2 -5 2260.59 352.620 15 0 2 5 1647.99 809.133 6 0 -2 -5 1932.75 246.565 4 0 2 5 2101.72 433.582 9 0 -2 -5 1902.69 310.364 3 0 -2 5 1475.90 316.003 16 0 2 5 2202.71 250.231 8 0 2 5 2309.01 675.925 19 0 2 5 1791.95 367.874 14 0 2 5 2039.93 291.493 10 0 -2 5 1742.13 635.352 19 0 2 -5 2065.12 352.891 12 0 -2 -6 23140.8 868.947 12 0 -2 -6 24491.0 1059.57 3 0 2 -6 24620.1 1148.91 4 0 -2 -6 24375.7 1140.25 15 0 -2 6 24726.1 1200.95 11 0 2 -6 22420.0 1049.95 12 0 2 -6 26253.9 911.845 13 0 2 6 23323.3 1206.98 9 0 2 6 25206.2 1017.63 16 0 2 6 25351.5 1019.96 10 0 2 -6 23921.4 759.840 17 0 2 -6 21676.0 1062.02 3 0 -2 6 30433.3 1816.48 6 0 -2 6 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635.630 9 0 -7 9 2702.55 829.160 19 0 7 9 2403.80 546.718 14 0 -7 9 2414.46 524.674 10 0 -7 9 3240.01 559.063 9 0 7 -9 2065.65 525.655 3 0 7 9 3768.75 765.551 19 0 7 -9 2011.50 356.771 1 0 -7 -9 3138.16 627.967 5 0 -7 9 2917.29 546.354 16 0 -7 9 3658.39 691.257 11 0 7 -9 2422.55 535.268 4 0 7 -9 2835.59 519.861 12 0 -7 -9 4437.61 720.499 15 0 7 9 3014.43 419.954 8 0 -7 -9 2361.03 436.792 3 0 7 10 880.497 491.370 9 0 -7 -10 1590.72 443.106 3 0 -7 -10 790.944 454.869 15 0 7 10 916.872 491.175 14 0 -7 10 1013.09 427.215 10 0 7 -10 980.753 452.266 3 0 7 -10 1396.94 413.390 12 0 -7 10 1171.68 440.096 9 0 -7 -10 834.769 491.655 5 0 7 10 1671.28 664.109 19 0 -7 10 1937.65 497.539 16 0 -7 10 1114.07 744.761 19 0 -7 -11 11391.9 1099.73 5 0 7 11 10271.5 1036.28 14 0 -7 11 12164.8 1051.65 9 0 -7 11 11616.0 1342.82 19 0 7 11 10630.0 1186.87 19 0 -7 -11 10513.1 1063.14 15 0 -7 11 10814.0 1017.24 16 0 7 -11 10226.8 1030.77 3 0 7 11 10405.0 1112.59 9 0 -7 11 11119.3 1020.68 10 0 -7 -12 435.816 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374.582 16 0 8 -1 6475.31 658.014 13 0 8 -1 5992.32 544.135 4 0 8 -1 6502.56 513.760 8 0 -8 1 6385.29 377.491 19 0 8 1 6491.12 628.454 8 0 -8 1 6594.75 421.885 15 0 -8 -1 6424.34 455.275 5 0 8 1 6508.77 474.272 12 0 -8 1 6454.40 475.078 2 0 -8 1 6688.20 349.815 5 0 -8 1 6252.82 414.136 11 0 -8 2 778.354 317.761 6 0 -8 2 663.288 86.7500 1 0 -8 -2 680.811 130.301 10 0 8 2 404.975 154.912 4 0 -8 2 894.130 273.823 2 0 8 -2 1268.92 413.153 4 0 8 -2 634.092 145.011 5 0 -8 2 997.612 324.165 19 0 -8 -2 444.193 126.109 16 0 -8 -2 1075.37 323.745 15 0 8 2 772.818 218.315 13 0 -8 2 807.528 299.479 11 0 -8 2 394.551 346.415 16 0 8 2 928.646 236.924 19 0 8 -2 1237.04 542.242 12 0 -8 -2 860.227 337.283 5 0 8 2 676.687 401.722 8 0 8 2 267.510 141.899 3 0 8 2 1655.60 313.582 14 0 8 -2 821.435 423.436 13 0 -8 -2 402.193 152.976 4 0 -8 -2 767.799 267.450 6 0 8 2 738.597 154.064 12 0 8 -2 422.684 224.394 8 0 8 2 521.047 145.840 18 0 8 2 653.354 295.018 9 0 -8 -2 347.166 278.231 13 0 8 -2 958.432 264.714 6 0 8 -2 669.795 90.9493 1 0 8 -2 687.455 127.247 9 0 -8 -2 267.338 161.481 3 0 -8 2 889.076 357.150 10 0 8 3 79284.0 1976.66 3 0 -8 -3 73069.0 1925.73 4 0 -8 -3 73864.3 2237.95 15 0 -8 -3 72513.5 2252.49 5 0 8 3 72098.0 1984.03 13 0 8 -3 68332.2 2381.78 4 0 -8 3 72295.1 2363.28 16 0 8 -3 74140.9 2639.94 12 0 8 3 73854.7 2017.22 18 0 -8 -3 78946.5 2222.15 13 0 -8 -3 75691.7 1997.12 3 0 8 3 74916.4 2274.16 19 0 -8 3 70656.7 2344.11 10 0 8 3 73484.6 2158.75 14 0 -8 3 83052.5 2466.22 6 0 8 -3 69894.4 2003.18 8 0 8 3 84414.2 2464.39 6 0 8 -3 79919.7 1861.68 1 0 8 3 71615.4 2288.55 9 0 8 -3 72726.3 2508.10 13 0 -8 -3 73045.5 1990.57 18 0 -8 3 73992.7 2266.80 11 0 8 -3 73601.9 2011.55 9 0 -8 3 76442.6 2447.71 19 0 8 3 72547.0 2340.77 8 0 -8 -4 3251.57 220.293 10 0 -8 4 3400.99 317.335 9 0 8 -4 3057.04 231.698 8 0 8 4 3277.92 507.390 9 0 8 4 3504.06 367.623 18 0 8 4 4432.84 636.421 6 0 8 -4 3632.65 244.158 1 0 -8 4 3972.13 539.883 10 0 -8 -4 4080.78 352.525 13 0 8 4 3920.67 258.948 13 0 8 4 4016.56 481.173 8 0 8 -4 4015.48 699.884 12 0 8 -4 3246.56 533.129 4 0 8 4 3472.01 515.459 19 0 -8 4 3579.74 628.834 19 0 -8 -4 3470.65 458.562 15 0 -8 -4 3371.56 205.536 4 0 8 -4 3944.98 571.154 13 0 -8 4 2784.92 493.902 16 0 -8 4 4297.49 684.738 6 0 -8 -4 3273.34 222.651 16 0 -8 -4 2965.02 308.238 3 0 -8 4 3189.52 487.161 11 0 8 4 3341.64 420.097 14 0 -8 -4 3734.15 495.950 5 0 8 5 353.525 357.600 14 0 -8 5 628.069 523.279 19 0 8 -5 736.437 517.652 12 0 8 5 492.414 405.276 9 0 -8 -5 420.072 153.210 16 0 8 -5 461.166 159.885 1 0 -8 5 695.505 261.349 9 0 -8 -5 454.817 153.517 10 0 -8 -5 495.008 129.113 13 0 -8 5 393.583 373.550 10 0 -8 5-20.0668 365.897 16 0 8 5 257.948 307.521 8 0 -8 -5 453.750 82.5162 4 0 -8 -5 335.260 341.243 15 0 8 5 292.135 415.079 19 0 8 -5 1153.38 478.768 13 0 8 -5 536.002 436.280 4 0 -8 5 769.463 600.465 6 0 -8 5 608.605 396.313 11 0 -8 -5 661.232 256.609 3 0 -8 -5 499.227 388.851 5 0 -8 -6 18210.3 775.447 16 0 8 6 20094.9 1273.97 19 0 8 6 17907.7 688.335 7 0 8 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304.091 8 0 10 -8 335.456 447.866 4 0 10 -8 281.786 223.739 1 0 10 8-33.8578 398.639 14 0 -10 -8-489.488 463.628 5 0 10 -8-72.5174 293.595 13 0 -10 8-197.760 629.392 19 0 -10 -8 729.372 355.684 3 0 -10 8 443.013 422.437 16 0 10 8 281.998 447.364 9 0 -10 8-177.626 410.585 10 0 -10 8 298.925 495.076 11 0 10 -8 606.053 491.120 12 0 -10 8 352.570 328.780 9 0 10 -9 21608.0 1423.15 4 0 10 -9 17540.6 1234.91 3 0 10 -9 19713.3 1309.90 12 0 10 9 19279.4 1385.15 19 0 -10 9 16201.7 1431.73 19 0 -10 9 21164.0 1366.27 10 0 10 9 18690.0 1252.23 14 0 10 9 19676.0 1115.45 8 0 -10 9 19896.3 1166.68 9 0 -10 -9 18494.6 1330.88 5 0 -10 -9 19875.5 1365.83 15 0 10 9 18641.7 1393.18 9 0 -10 9 20333.5 1403.47 11 0 -10 9 20494.2 1363.75 16 0 -10 -10 1870.99 623.808 15 0 10 -10 2004.43 545.545 4 0 -10 10 2409.36 604.342 16 0 10 10 1755.27 624.835 9 0 -10 10 1292.05 651.549 19 0 10 10 643.013 539.433 19 0 10 -10 697.227 446.478 3 0 -10 -10 1436.00 533.998 5 0 10 -10 998.994 448.836 12 0 -10 10 2061.57 567.736 10 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596.409 16 0 12 -3 4787.90 307.624 9 0 12 3 4075.45 243.490 12 0 12 3 5098.24 360.685 4 0 12 3 4196.18 334.603 19 0 -12 -3 4316.04 278.564 10 0 12 3 3984.32 625.476 8 0 12 3 4503.02 421.116 13 0 -12 -3 4831.06 452.327 2 0 12 3 4755.12 330.800 3 0 12 3 4642.72 522.114 14 0 12 -3 5104.08 701.567 13 0 -12 -3 4584.26 292.118 16 0 12 3 3739.02 498.673 9 0 -12 3 4282.57 506.145 11 0 12 -4 10969.2 1023.07 12 0 -12 -4 10104.0 546.400 3 0 -12 -4 9646.58 757.943 15 0 12 -4 9124.61 880.638 4 0 -12 4 10897.8 509.603 17 0 -12 -4 9542.86 394.422 10 0 12 4 9291.09 832.873 8 0 12 -4 11372.2 991.240 13 0 -12 4 9708.16 799.867 19 0 12 -4 11553.1 590.958 8 0 12 4 10034.4 552.330 18 0 12 4 10028.9 569.621 13 0 12 -4 9495.74 370.488 1 0 12 4 10772.8 826.762 9 0 -12 -4 9516.11 398.495 16 0 -12 4 9835.63 875.571 16 0 -12 -4 8321.47 729.063 5 0 -12 4 9994.09 793.875 11 0 12 4 9305.83 690.820 14 0 12 4 9578.74 609.693 19 0 -12 -4 10655.0 542.486 4 0 -12 4 9266.25 828.748 10 0 -12 5 296.434 67.4133 17 0 -12 5 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436.112 427.127 3 0 -12 -9 1037.20 538.117 15 0 12 9 2205.54 667.335 9 0 12 9 447.231 403.333 19 0 12 -9 1250.76 546.201 4 0 12 -10 6024.08 808.997 12 0 -12 -10 7460.43 949.586 5 0 12 10 7481.03 881.047 14 0 -12 10 7975.03 972.752 16 0 -12 -10 7883.55 940.574 15 0 -12 10 9922.47 1084.18 11 0 -12 10 8409.83 976.894 10 0 12 10 8586.81 988.719 19 0 12 -10 8138.65 976.861 4 0 12 10 6997.65 969.840 9 0 12 -10 8081.18 935.465 3 0 -12 10 6250.91 1015.42 19 0 12 -11-208.538 490.253 3 0 12 11 491.588 513.306 19 0 12 -11-497.381 491.635 12 0 -12 -11 541.098 546.101 5 0 -12 11 18.5167 460.143 10 0 -12 -11 1011.60 546.051 15 0 12 11 192.694 523.617 9 0 -12 11 1274.80 757.294 19 0 12 11-466.368 470.095 14 0 -12 11-152.974 465.625 16 0 -12 -12 6709.94 985.383 15 0 -12 12 10050.3 1095.78 10 0 -12 12 8375.26 1035.10 16 0 -13 0-2.47658 189.713 11 0 -13 0 521.914 357.261 2 0 -13 0 225.499 309.589 10 0 13 0 135.093 431.943 8 0 13 0-30.0447 421.332 13 0 13 0-20.7816 164.790 9 0 -13 0 535.862 351.219 15 0 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341.216 8 0 -13 -4 1771.92 175.114 16 0 13 4 2297.41 337.039 13 0 -13 -4 1830.47 474.232 5 0 13 -4 2387.84 697.405 12 0 13 4 2019.98 473.324 9 0 -13 -4 1452.38 279.923 3 0 -13 -4 2321.61 514.728 15 0 -13 4 1271.57 423.900 19 0 -13 4 1911.89 573.795 10 0 13 -4 1038.56 502.065 4 0 -13 4 2254.11 272.091 17 0 13 -4 2367.91 651.997 13 0 -13 4 1869.39 537.986 16 0 13 4 1384.50 427.549 14 0 -13 -4 2485.06 321.667 4 0 -13 4 1714.71 454.195 11 0 13 -4 1955.88 153.628 1 0 -13 -4 1867.53 180.747 10 0 13 5 26900.6 1344.56 8 0 -13 5 25966.0 1384.58 19 0 -13 -5 28160.3 1356.90 15 0 -13 5 22625.0 695.913 17 0 13 -5 25682.5 1470.05 4 0 13 5 25460.7 1364.34 9 0 -13 -5 25038.2 1324.27 5 0 -13 -5 23513.1 714.954 10 0 -13 -5 22022.7 711.592 16 0 -13 5 25400.8 1342.85 11 0 13 -5 28464.2 1551.33 13 0 -13 5 26996.4 1443.23 10 0 13 5 26224.5 1055.12 18 0 13 5 23856.7 1193.60 14 0 -13 -5 23399.1 716.821 16 0 -13 -5 21851.0 708.409 10 0 13 -5 25541.1 1593.47 12 0 -13 5 24305.9 1390.13 16 0 -13 5 22288.5 711.837 17 0 13 5 26965.8 973.447 13 0 -13 -5 27442.3 916.484 4 0 -13 -5 26486.9 1009.48 3 0 13 5 26007.8 1144.40 19 0 13 -5 25004.9 825.433 8 0 13 -5 26299.5 760.549 1 0 13 -6 665.713 595.966 12 0 -13 6-481.226 503.356 10 0 -13 6 7.73094 508.643 19 0 13 -6-490.739 528.494 13 0 13 6 351.097 389.525 19 0 -13 6 322.402 518.500 16 0 13 -6 3.38679 129.160 1 0 -13 -6-438.854 476.560 15 0 13 6 471.146 446.309 14 0 13 6 200.502 398.156 8 0 -13 -6 449.461 313.020 3 0 -13 6 349.134 478.586 11 0 13 6 650.897 549.201 9 0 -13 -6 539.849 504.495 5 0 13 -6-60.5852 526.464 4 0 -13 7 12897.7 1061.59 11 0 -13 7 11689.1 1044.82 16 0 -13 7 14594.4 1128.83 10 0 13 -7 13891.0 1178.56 12 0 13 -7 12591.2 1120.80 4 0 -13 -7 12022.9 1001.26 15 0 13 7 12186.4 1068.91 9 0 -13 7 12801.5 1097.96 19 0 13 -7 12049.7 994.878 13 0 13 7 13018.7 948.557 8 0 -13 -7 14958.1 809.571 3 0 13 7 12861.6 975.993 14 0 13 7 14221.4 1008.81 19 0 -13 -7 14539.5 1091.21 5 0 13 -8 2347.99 612.070 4 0 -13 -8 2932.64 644.890 5 0 13 8 2127.31 519.817 19 0 13 -8 3274.87 554.613 13 0 -13 8 2864.13 635.557 11 0 -13 -8 1663.29 544.049 15 0 -13 8 3160.81 657.208 16 0 13 -8 2462.74 638.990 12 0 13 8 2077.37 624.261 9 0 -13 8 1479.14 592.370 19 0 -13 8 2483.70 597.134 10 0 13 8 1783.72 432.597 8 0 13 8 3108.03 567.098 14 0 13 9 1849.50 659.345 9 0 -13 9 1280.35 554.812 11 0 13 -9 917.916 505.281 4 0 13 9 1073.89 491.918 14 0 -13 9 936.457 587.099 19 0 -13 -9 2581.67 662.994 5 0 -13 9 1315.58 510.826 16 0 13 -9 855.782 448.787 3 0 13 -9 812.452 565.061 12 0 -13 -9 526.940 498.985 15 0 13 9 768.786 365.215 8 0 -13 9 1787.36 576.380 10 0 13 9 1270.59 462.060 19 0 13 -10 142.581 450.438 12 0 -13 10 1621.04 611.686 10 0 -13 10 1773.66 693.572 19 0 13 10 509.270 499.609 19 0 13 -10 983.543 513.200 3 0 13 -10 1217.00 535.063 4 0 -13 10 1227.44 563.988 16 0 -13 10 1507.29 653.076 11 0 -13 -10 290.678 474.803 5 0 -13 -10 508.332 505.633 15 0 13 10 1181.06 512.909 14 0 13 10 443.790 534.128 9 0 -13 11 10314.1 1236.93 19 0 -13 -11 10118.5 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394.419 8 0 -16 -2 687.217 360.794 2 0 16 2 1003.79 219.927 18 0 16 2 1020.54 301.596 12 0 -16 3 49621.1 2094.47 16 0 16 -3 47801.5 1377.31 9 0 -16 3 50250.4 1706.21 19 0 -16 3 49720.8 1872.18 11 0 16 3 52776.2 2143.64 8 0 -16 -3 49056.8 1894.96 5 0 16 -3 54160.2 2300.80 13 0 16 3 49525.4 1497.65 12 0 16 3 54237.3 1881.38 14 0 16 -3 49874.8 2099.52 4 0 16 -3 51763.6 2300.47 12 0 -16 -3 50582.4 1806.90 2 0 -16 3 49633.6 2075.91 10 0 16 3 50835.0 1471.97 18 0 -16 -3 51754.5 1568.04 10 0 -16 -3 52960.3 1583.01 16 0 16 -3 57207.1 1907.80 8 0 16 3 52225.4 1887.71 9 0 16 3 49058.1 1811.42 13 0 -16 3 46332.9 1266.26 1 0 16 3 52272.9 1669.82 4 0 -16 3 52588.1 1907.13 2 0 -16 -3 49162.9 1923.02 15 0 -16 -4 2031.27 520.000 5 0 -16 4 1602.29 556.015 10 0 16 -4 1431.27 525.185 4 0 16 4 1695.67 497.961 9 0 -16 -4 1773.58 234.159 10 0 -16 -4 2074.62 574.659 15 0 16 4 1830.77 478.672 14 0 16 -4 1325.79 648.820 12 0 -16 4 1621.02 412.629 19 0 -16 4 2012.14 579.015 16 0 -16 -4 1475.42 404.302 2 0 -16 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386.805 16 1 9 3 197.415 208.837 13 1 9 3-36.4767 354.277 8 -1 9 -3 76.9559 167.274 9 -1 -9 -3 83.4283 163.359 11 1 9 3 292.914 365.557 14 -1 9 -3 81.0653 90.5550 8 -1 9 -3 527.212 454.461 12 -1 -9 -3 117.765 343.523 15 -1 9 -3 127.387 424.761 4 -1 -9 -3 268.537 270.601 3 1 9 3 12.2580 78.7122 4 1 9 3 193.606 338.546 9 1 -9 3 153.320 136.524 9 1 9 3 99.6186 115.704 12 -1 9 -3 125.648 309.653 13 -1 9 -4 3117.77 583.843 12 1 9 4 1601.82 369.715 14 1 9 4 2003.68 157.152 12 -1 9 -4 2656.79 445.593 13 1 -9 4 1988.50 492.733 10 1 -9 4 2841.45 531.539 16 -1 -9 -4 1917.16 453.530 15 1 -9 4 2214.71 482.164 11 1 9 4 1907.61 454.068 8 1 9 4 2143.43 231.820 13 -1 9 -4 1981.94 561.806 4 -1 9 -4 2276.82 174.394 1 1 -9 4 2294.71 276.023 9 -1 -9 -4 1838.75 383.998 3 1 9 4 2187.14 500.691 9 -1 9 -5 23525.8 1300.40 12 1 9 5 24206.3 1218.47 8 1 -9 5 24040.2 1306.23 16 1 -9 5 23487.6 1266.17 11 1 -9 5 23365.9 1281.70 10 -1 9 -5 20213.4 1288.63 4 1 -9 5 24668.4 978.256 9 -1 -9 -5 25526.1 1109.81 3 1 -9 5 22536.7 1432.99 19 -1 9 -5 23498.6 1166.27 3 1 9 5 23499.5 1272.74 9 1 9 5 21477.7 653.192 13 -1 -9 -5 25388.3 1275.11 15 1 9 5 25744.3 1203.94 14 -1 9 -5 23378.0 1119.89 13 1 9 6 160.095 589.874 19 1 9 6 417.309 498.165 9 1 -9 6-8.42066 649.114 19 1 -9 6 710.112 537.774 11 1 -9 6 27.7907 275.484 9 1 9 6 853.924 402.802 8 -1 9 -6-501.542 540.411 12 -1 9 -6 861.352 542.744 4 1 -9 6-67.0613 444.915 10 -1 -9 -6 369.423 402.668 3 1 9 6 64.8965 428.472 14 -1 9 -6-123.174 427.262 3 -1 -9 -6 643.927 486.806 15 1 -9 6 481.636 472.204 16 -1 9 -6 297.777 288.688 13 1 9 7 18495.1 1362.27 19 1 -9 7 17859.4 1436.91 19 1 -9 7 20071.3 1031.75 9 -1 9 -7 18608.3 1194.54 12 1 -9 7 21168.6 1296.06 11 -1 9 -7 17579.3 1147.25 3 -1 9 -7 19907.9 960.673 13 1 -9 7 16828.6 1157.02 10 1 9 7 17949.6 1259.35 9 -1 9 -7 18009.6 1242.66 4 1 -9 7 17922.4 1190.69 16 -1 -9 -7 19617.5 1258.66 15 1 9 7 18442.5 1037.82 8 -1 -9 -7 20442.4 1093.13 3 1 9 7 19145.7 1166.92 14 1 -9 8-88.4908 646.005 19 -1 9 -8-68.9794 376.283 12 1 9 8 60.6671 261.328 8 1 -9 8 640.084 508.395 11 1 9 8 190.183 516.758 19 -1 9 -8-423.556 416.788 3 -1 9 -8 1013.22 475.843 4 1 -9 8 151.266 405.829 10 1 -9 8 159.083 322.537 9 1 9 8 143.979 447.345 9 -1 -9 -8 423.308 464.203 15 1 9 8-34.6675 380.602 14 1 -9 8-107.379 377.338 16 -1 -9 -8 456.719 408.134 3 -1 -9 -9 2335.57 548.742 3 1 -9 9 1417.03 582.737 11 1 9 9 995.994 469.978 14 1 -9 9 2223.57 561.083 10 1 9 9 1905.01 603.429 9 -1 9 -9 1961.00 518.984 4 -1 9 -9 932.444 465.099 3 1 -9 9 740.517 331.855 9 -1 9 -9 537.556 437.426 12 1 -9 9 1739.44 704.588 19 -1 -9 -9 1213.81 561.746 5 1 9 9 902.848 588.818 19 1 -9 9 1725.01 572.046 16 -1 -9 -9 1300.73 543.958 15 1 9 10 620.077 521.676 9 1 -9 10 1423.64 530.242 16 -1 -9 -10 1491.75 572.532 15 1 -9 10 472.009 551.030 11 -1 -9 -10 1247.31 541.702 3 -1 -9 -10-51.1474 494.898 5 1 9 10 1096.87 545.330 14 -1 9 -10 163.007 372.688 12 1 -9 10 94.7597 399.896 10 1 -9 10-961.422 681.915 19 1 -9 10 1212.34 427.346 9 -1 9 -10 777.109 517.521 3 1 9 10 62.4607 545.162 19 1 -9 11 9355.69 990.913 10 -1 9 -11 9189.48 1039.09 3 1 -9 11 10976.8 1153.48 11 1 -9 11 8350.19 1212.30 19 1 -9 11 9863.04 1028.47 16 1 9 11 7806.69 1048.75 9 1 9 11 8822.72 1154.51 19 -1 -9 -11 9912.95 1113.08 15 1 9 11 9010.51 1020.33 14 -1 -9 -11 9240.84 1076.03 5 -1 -10 12 6537.41 908.500 10 -1 10 12 5731.50 918.695 19 1 -10 -12 6066.28 896.108 5 -1 -10 12 5519.45 838.528 16 1 -10 -12 5650.66 857.276 15 1 10 -12 5456.68 854.074 3 1 10 -11 183.629 401.092 12 1 -10 -11 362.673 440.862 15 1 10 -11-389.264 533.739 3 -1 10 11 768.125 576.746 9 -1 -10 11 842.409 497.090 10 1 -10 -11 573.574 507.211 5 -1 -10 11 1728.71 780.643 19 -1 -10 11 310.888 503.940 16 -1 10 11 1818.63 639.497 19 -1 10 11 201.978 478.459 14 -1 10 10 13742.8 1200.01 19 -1 -10 10 16285.5 1248.90 16 1 10 -10 14563.0 1231.18 4 1 -10 -10 15800.8 1228.34 5 -1 -10 10 15798.1 1221.74 10 -1 10 10 15773.9 1171.29 14 -1 -10 10 17002.9 1531.49 19 1 10 -10 14157.7 1185.00 12 1 -10 -10 16021.8 1195.27 15 -1 10 10 15982.1 1027.51 8 -1 10 10 16397.9 1358.24 9 -1 -10 9 3128.45 823.392 6 -1 -10 9 2088.52 770.755 19 -1 -10 9 2146.35 560.629 10 -1 10 9 2575.89 639.973 19 1 10 -9 1751.25 566.857 12 -1 10 9 3148.03 835.325 6 -1 10 9 2393.16 676.951 9 1 10 -9 2497.72 403.107 1 -1 10 9 1545.06 479.024 14 -1 -10 9 1957.18 561.728 16 -1 10 9 2277.23 438.584 8 1 10 -9 1985.47 555.409 4 1 -10 -9 851.334 478.201 5 1 -10 -9 2203.05 539.909 15 1 10 -9 2168.79 492.545 13 -1 10 8 628.721 309.085 8 -1 10 8 1445.29 540.615 19 -1 -10 8 598.043 633.928 6 -1 10 8 396.295 507.975 9 1 -10 -8 1204.18 452.706 15 -1 -10 8 616.999 590.209 19 -1 10 8-24.6482 344.765 14 -1 10 8 401.349 356.684 18 -1 -10 8 218.747 433.417 10 -1 -10 8 620.032 500.028 16 1 -10 -8 893.853 280.319 3 -1 10 8 1417.76 704.159 6 1 -10 -8 1253.83 500.339 5 1 10 -8 573.086 468.891 4 1 10 -8 867.004 527.567 12 1 10 -8 1063.15 299.727 1 1 10 -8 292.904 353.740 13 1 10 -7 2014.63 650.513 12 -1 -10 7 2779.96 796.110 6 1 10 -7 2620.15 358.539 1 1 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1 10 -5 1115.84 236.985 1 -1 -10 5 1590.69 469.498 11 -1 10 5 1109.13 343.695 19 -1 -10 5 1345.64 481.748 10 -1 -10 5 1046.58 176.000 17 -1 -10 5 1101.41 587.859 6 1 -10 -5 1470.16 257.614 2 -1 10 5 1343.76 524.404 9 1 -10 -5 1581.80 424.442 15 -1 10 5 1693.47 423.759 8 -1 -10 5 1240.60 487.055 16 -1 10 5 948.571 552.257 6 -1 10 5 1153.40 364.345 14 1 10 -5 991.516 406.949 13 -1 10 5 1441.01 386.532 18 1 10 -5 490.075 393.848 4 1 -10 -5 883.567 179.323 3 -1 -10 4 36394.0 1478.43 11 1 -10 -4 37347.0 1482.04 5 1 -10 -4 31371.4 943.299 3 -1 10 4 34898.8 1448.30 8 -1 -10 4 35354.6 1540.53 6 1 10 -4 35199.5 1512.51 4 -1 -10 4 38134.9 1501.98 19 -1 -10 4 35137.3 1517.22 10 -1 10 4 36312.9 1302.20 18 -1 10 4 32517.2 1484.58 9 1 -10 -4 36793.4 1208.57 2 -1 10 4 37620.5 1236.86 13 -1 -10 4 37308.7 1558.68 16 1 10 -4 34455.7 1511.77 13 1 10 -4 38812.4 1152.51 1 -1 10 4 34477.7 1549.79 6 1 -10 -4 36937.0 1433.45 15 -1 -10 4 35338.6 1112.39 17 -1 10 4 36938.8 1311.80 14 -1 -10 4 36062.5 1325.81 2 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574.174 10 2 -30 -5 180.441 491.299 15 -2 30 5 1507.55 669.980 8 -2 -30 5 668.097 517.815 2 2 30 -5 563.684 635.734 4 -2 30 5 728.371 494.827 13 2 30 -5 832.161 726.808 13 2 30 -4 11417.8 1318.42 12 -2 -30 4 11415.3 1173.97 10 2 -30 -4 10974.1 1084.00 5 -2 -30 4 11054.1 1180.01 16 2 30 -4 13650.4 1386.50 4 2 -30 -4 10435.1 1106.51 15 -2 30 4 12385.6 1301.25 8 -2 30 4 9435.81 1055.61 13 -2 -30 4 10672.2 1076.39 2 2 30 -4 10578.9 1352.13 13 2 30 -3 2660.80 768.435 12 2 30 -3 2832.59 712.303 8 -2 -30 3 1971.44 599.870 10 -2 30 3 1860.86 621.749 13 -2 -30 3 1575.49 595.414 16 2 -30 -3 1913.83 606.737 5 2 -30 -3 1554.16 614.943 15 -2 30 3 2417.75 731.348 8 2 30 -3 1890.47 697.285 4 -2 -30 3 2620.54 657.819 2 2 30 -3 2755.56 861.067 13 -2 -30 2 652.135 500.234 2 2 -30 -2 996.384 474.177 5 -2 30 2 1202.37 566.718 4 2 30 -2 1582.57 686.924 12 -2 -30 2 1227.09 526.755 10 -2 -30 2 742.162 488.430 16 -2 -30 2 238.831 365.039 15 -2 30 2-55.9618 526.934 8 2 30 -2-10.4718 479.423 8 2 30 -2 662.176 524.771 4 -2 30 2 1042.73 563.342 13 2 30 -2-200.554 585.994 13 -2 -30 1 2333.63 641.675 2 -2 30 1 2183.31 661.341 4 -2 -30 1 1496.21 493.858 15 -2 30 1 3292.51 622.428 12 2 30 -1 2768.72 727.146 12 2 -30 -1 3046.05 630.912 10 2 -30 -1 2363.21 593.995 16 -2 30 1 2454.15 693.156 8 2 30 -1 2793.38 766.384 8 2 30 -1 2824.22 684.343 4 -2 30 1 1780.85 681.790 13 2 30 -1 2576.26 761.927 13 -2 -30 0 10235.6 1047.85 2 -2 30 0 8592.02 966.211 12 2 30 0 8199.11 954.687 12 2 -30 0 9890.67 1062.07 10 -2 30 0 9298.36 1036.33 8 2 -30 0 9300.88 1010.85 16 -2 -30 0 9450.08 962.959 15 -2 30 0 8894.95 1049.19 4 2 30 0 8612.66 1089.92 8 2 30 0 9792.91 988.152 4 -2 30 0 9915.26 1197.47 13 2 30 0 9006.29 1117.44 13 -2 -30 -1-29.5458 461.196 2 -2 30 -1 183.328 472.670 12 -2 -30 -1 462.849 428.858 15 2 -30 1 814.988 558.243 10 2 -30 1 322.582 502.692 16 -2 30 -1 819.531 464.979 8 -2 30 -1 813.487 610.259 4 2 30 1 1548.09 691.868 8 -2 30 -1 760.447 631.097 13 2 30 1 517.292 512.251 13 -2 -30 -2 9141.40 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537.795 545.797 3 2 31 -5 8356.24 1184.65 12 -2 -31 5 8593.07 1087.12 10 -2 -31 5 9970.42 1174.29 16 -2 31 5 7409.56 959.392 13 2 31 -4-258.209 636.398 12 2 -31 -4 684.831 554.793 15 -2 -31 4-11.4838 490.979 10 2 -31 -4 578.039 512.477 5 -2 -31 4 705.959 572.172 16 -2 31 4 312.693 512.165 8 2 31 -4 755.163 620.450 4 -2 31 4 100.184 458.340 13 -2 -31 4 126.314 438.700 2 2 31 -4 935.093 735.209 13 2 -31 -3 2896.71 628.469 5 2 31 -3 1581.78 712.671 12 -2 -31 3 3321.98 684.068 10 -2 -31 3 2308.17 663.706 16 2 -31 -3 3009.54 755.950 15 -2 31 3 2496.55 714.991 8 2 31 -3 2348.49 653.822 8 2 31 -3 3935.17 802.000 4 -2 31 3 2860.80 698.715 13 -2 -31 3 2340.18 667.981 2 2 31 -3 3560.54 808.044 13 -2 -31 2 916.489 542.282 2 2 31 -2 237.902 534.560 12 2 -31 -2-96.4864 418.576 5 -2 -31 2-801.259 421.560 15 -2 31 2 694.464 518.275 4 -2 31 2 1163.55 635.521 8 2 31 -2 454.837 513.499 8 2 31 -2 756.231 523.939 4 -2 31 2 289.254 553.689 13 2 31 -2 308.474 607.012 13 -2 -31 1 6179.16 861.770 2 2 31 -1 4697.39 851.236 12 2 -31 -1 6229.68 848.284 10 2 -31 -1 6260.09 899.284 16 -2 -31 1 5419.10 751.588 15 -2 31 1 6172.65 871.966 4 -2 31 1 6500.32 933.275 8 2 31 -1 6418.20 956.309 8 2 31 -1 5263.97 823.994 4 -2 31 1 6229.47 987.637 13 2 31 -1 5496.79 953.854 13 -2 -31 0 673.342 546.409 2 -2 -31 0 432.968 440.492 15 -2 31 0 117.894 464.760 12 2 -31 0 667.347 483.250 10 2 -31 0 2021.92 599.406 16 -2 31 0 1028.93 580.859 4 -2 31 0 296.488 512.768 8 2 31 0 341.320 510.676 8 2 31 0 887.164 496.650 4 -2 31 0-258.723 595.722 13 2 31 0 89.4719 534.680 13 -2 31 -1 8077.28 933.298 8 2 -31 1 7468.95 964.187 10 -2 -31 -1 7067.60 939.402 2 -2 31 -1 8495.68 1043.72 12 2 -31 1 7885.84 995.022 16 -2 -31 -1 6614.70 859.443 15 -2 31 -1 6733.53 975.161 4 2 31 1 10953.8 1243.96 8 -2 31 -1 7136.93 1048.04 13 2 31 1 6597.97 956.006 13 -2 -31 -2 382.918 477.444 2 -2 31 -2 295.192 541.929 12 -2 -31 -2-64.6595 383.481 5 2 -31 2 1178.18 609.885 16 -2 -31 -2 1193.81 561.501 15 2 -31 2-23.3697 480.038 10 -2 31 -2 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1119.99 505.180 15 -2 32 -1 545.574 585.481 4 2 32 1 2375.13 770.360 8 -2 32 -1 435.754 621.222 13 2 32 1-331.132 475.144 13 -2 -32 -2 5341.97 808.267 2 -2 32 -2 3612.46 831.252 12 2 -32 2 4496.70 813.310 10 2 -32 2 4762.05 858.534 16 -2 -32 -2 4419.26 762.797 15 -2 32 -2 6565.91 1019.21 4 2 32 2 4694.76 789.790 13 -2 -32 -3 5415.35 885.113 2 2 -32 3 3449.99 814.730 10 -2 32 -3 4718.96 910.368 12 2 -32 3 3432.82 797.648 16 -2 -32 -3 4755.65 772.591 5 -2 -32 -3 5062.29 874.979 15 -2 -32 -4 2156.60 582.078 5 -2 -33 4 3017.77 779.508 10 -2 -33 4 2758.99 712.680 16 -2 33 4 1741.28 661.874 13 2 33 -3 1055.75 616.397 12 2 -33 -3 543.961 441.873 5 2 33 -3 460.006 502.415 8 2 33 -3 1406.86 611.473 4 -2 33 3 1567.68 617.111 13 2 33 -2 6366.99 1010.27 12 2 -33 -2 7090.76 898.183 5 -2 33 2 5523.06 925.328 13 -2 33 2 7089.02 951.193 4 -2 33 2 8279.35 1092.94 8 2 33 -2 7029.77 995.423 8 2 33 -2 6104.56 954.367 4 2 33 -1 1373.94 632.210 8 -2 -33 1 2032.69 606.319 15 -2 33 1 2888.96 742.079 4 -2 33 1 1472.85 588.136 8 2 33 -1 2014.57 610.490 4 -2 33 1 2884.82 769.481 13 2 33 -1 138.126 534.560 13 -2 33 0 1265.58 564.733 12 2 -33 0 876.256 549.530 16 2 -33 0 1229.32 534.592 10 -2 33 0 546.350 511.217 8 -2 -33 0 1008.60 499.481 15 -2 33 0 927.695 585.824 4 2 33 0 971.862 591.537 8 2 33 0 1724.10 681.282 13 2 -33 1 881.049 515.826 10 -2 33 -1 1784.32 638.881 12 2 -33 1 1823.85 626.227 16 -2 -33 -1 840.226 516.893 15 -2 33 -1 1770.64 640.487 4 2 33 1-90.2069 497.788 13 2 -33 2 4890.63 867.536 10 -2 33 -2 4562.53 899.696 12 2 -33 2 4090.87 849.239 16 -2 -33 -2 2511.83 657.028 15 2 33 2 3887.42 796.271 13 2 34 -3 6479.36 1029.27 12 2 34 -2-216.809 533.514 12 -2 34 2 739.967 551.880 4 2 34 -2 115.228 460.870 4 -2 -34 1 6388.06 870.737 15 -2 34 1 7620.38 1017.51 4 -2 34 1 9468.61 1102.05 8 2 34 -1 9467.11 1162.59 8 2 34 -1 8533.12 1033.28 4 -2 34 0 1.09420 522.659 8 2 -34 0 213.739 455.787 10 2 -34 0-133.271 518.749 16 -2 -34 0-363.999 471.871 15 2 -34 1-80.1193 474.547 10 -2 34 -1 295.506 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4557.98 794.066 11 3 -11 8 2550.89 801.887 19 -3 -11 -8 4828.27 778.038 3 3 -11 8 3657.76 700.844 10 -3 11 -8 4337.36 763.479 3 3 11 8 5395.10 860.923 9 3 -11 8 4538.28 753.891 16 -3 -11 -8 2986.35 687.435 15 3 11 8 3878.54 692.156 14 -3 11 -9 14.5238 491.571 12 3 -11 9 578.363 549.985 11 3 -11 9 623.548 468.463 10 3 11 9-839.599 741.296 19 -3 -11 -9 633.906 512.094 3 3 -11 9 673.943 699.863 19 -3 11 -9 17.8084 537.409 3 3 11 9 308.697 512.837 9 3 -11 9 275.968 445.494 16 -3 -11 -9 1267.33 648.095 15 3 11 9 147.383 435.146 14 3 -11 10 5775.12 844.067 10 -3 11 -10 4031.33 764.240 12 -3 -11 -10 5548.75 900.302 3 3 11 10 6571.88 1139.17 19 3 -11 10 6111.61 908.154 16 3 12 -12 1014.30 615.286 4 3 12 -12 565.144 573.101 12 -3 12 12 1537.20 907.384 6 -3 -12 12 530.415 822.479 6 3 -12 -12 1324.04 656.505 5 3 12 -11 3790.34 784.942 4 3 12 -11 2032.65 696.196 12 -3 -12 11 4826.71 1102.03 6 -3 12 11 3925.66 735.865 18 3 -12 -11 4316.48 823.365 5 3 -12 -11 2817.46 648.687 1 3 -12 -10 195.719 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334.198 1 5 -18 -6 321.587 432.472 5 -5 18 6 321.458 471.931 18 -5 -18 6 253.208 341.846 17 -5 18 6 280.559 522.686 17 5 -18 -6 770.417 417.998 1 -5 -18 5 4992.67 710.973 7 5 18 -5 4796.41 776.919 13 5 18 -5 4486.74 655.821 1 -5 -18 5 3623.84 640.373 2 -5 18 5 4698.33 702.906 7 -5 18 5 4927.74 813.165 18 -5 -18 5 5179.77 698.300 17 -5 18 5 5844.87 805.694 17 5 -18 -5 4029.46 600.985 1 -5 -18 4 2799.84 592.222 7 5 18 -4 2368.02 620.821 13 5 18 -4 2409.19 534.511 1 -5 18 4 2133.52 538.523 12 -5 18 4 3575.99 637.720 7 -5 -18 4 2560.97 591.556 2 -5 18 4 3306.65 707.340 18 -5 -18 4 2129.82 533.670 17 5 -18 -4 3140.33 506.433 1 -5 18 4 2277.04 618.975 17 5 -18 -4 4103.78 725.495 16 5 18 -3 4715.84 642.621 1 -5 -18 3 4177.59 683.063 7 5 18 -3 3692.52 659.952 13 -5 18 3 3823.52 674.613 12 -5 18 3 4509.55 703.406 7 5 -18 -3 4003.00 524.165 1 5 -18 -3 5690.86 822.098 10 -5 -18 3 4578.73 690.409 17 -5 18 3 3522.67 647.475 17 5 -18 -3 4488.32 744.095 16 5 -18 -2 156.522 269.396 1 -5 -18 2-309.427 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11481.0 1236.99 16 5 18 5 10866.3 1177.34 9 -5 -18 -5 11482.9 1159.40 15 5 18 5 9652.55 1049.98 14 -5 -18 -6 79.9292 612.439 3 5 -18 6 96.3565 593.157 10 -5 18 -6 282.106 649.472 3 5 -18 6-107.026 542.798 16 5 18 6-97.0508 544.344 8 -5 19 10-170.623 452.454 18 5 19 -9 1834.78 712.167 13 5 -19 -9 1572.39 626.090 1 -5 19 9 475.982 479.647 18 5 -19 -9 2369.18 735.371 5 -5 19 9 156.820 552.848 17 5 19 -8 7066.65 997.485 13 5 19 -8 6611.64 978.893 4 -5 19 8 6951.60 817.599 7 5 -19 -8 7003.60 942.656 1 5 19 -8 6669.89 794.839 1 -5 -19 8 6345.31 977.897 6 -5 19 8 7257.03 939.391 18 5 -19 -8 6828.67 934.536 5 -5 19 8 6388.15 1010.86 17 -5 -19 8 5892.55 801.637 7 -5 -19 7-68.4885 398.004 7 5 19 -7 647.124 588.243 13 -5 -19 7 374.617 379.592 2 5 19 -7 526.710 546.218 4 5 -19 -7 785.379 491.815 1 -5 19 7 1030.08 538.766 7 5 19 -7 307.026 362.509 1 -5 -19 7 30.6795 490.410 6 5 -19 -7 272.046 492.878 5 -5 19 7-242.045 556.412 18 -5 -19 7 476.807 369.632 17 -5 19 7 305.033 505.670 17 5 -19 -6 17446.0 1311.23 5 5 19 -6 18722.7 1209.71 1 -5 19 6 18838.5 1406.81 18 -5 -19 6 18379.5 1230.32 17 -5 19 6 16601.9 1392.25 17 5 -19 -6 16353.1 1224.00 1 5 19 -6 16835.2 1366.27 4 -5 -19 6 16696.6 1201.63 2 -5 -19 6 18305.1 1309.73 7 5 19 -6 16491.6 1387.77 13 -5 19 6 14945.8 1162.93 7 -5 -19 5 1153.68 508.554 7 5 19 -5 277.572 478.057 13 5 19 -5 108.413 439.001 4 5 19 -5 1604.33 474.130 1 -5 -19 5 1421.82 489.143 2 -5 19 5 421.881 400.889 7 -5 19 5 53.8223 545.173 18 -5 -19 5 949.560 437.571 17 -5 19 5 841.036 506.864 17 5 -19 -5 1069.55 426.672 1 -5 -19 4 152.671 429.712 7 5 19 -4 945.487 491.820 13 5 19 -4-65.0008 369.086 1 -5 19 4 182.216 417.796 12 -5 19 4 790.099 469.584 7 -5 -19 4 894.033 493.091 2 5 -19 -4 1280.45 563.248 10 -5 19 4 882.374 597.862 18 -5 -19 4 393.945 439.404 17 5 -19 -4-365.091 322.138 1 -5 19 4 360.255 437.947 17 5 -19 -4 1030.88 524.833 16 -5 -19 3 1613.02 536.669 7 5 19 -3 1252.44 564.652 13 -5 19 3 1724.40 558.707 12 -5 19 3 1625.10 542.686 7 5 -19 -3 1200.05 365.445 1 5 -19 -3 1003.62 557.536 10 -5 -19 3 1390.01 510.136 17 -5 19 3 268.352 423.845 17 5 -19 -3 1127.59 580.413 16 5 19 -3 1257.86 442.587 1 -5 19 2 14357.8 1145.03 12 5 19 -2 14179.6 1090.04 1 5 -19 -2 16542.7 1244.00 10 -5 -19 2 15013.7 1162.09 17 -5 19 2 13816.7 1132.51 17 5 -19 -2 13261.0 1154.33 16 -5 -19 2 14029.7 1143.89 7 5 19 -2 12653.9 1128.32 13 -5 19 2 12114.2 1068.54 7 -5 -19 1-46.1040 395.330 7 5 19 -1 231.508 444.213 13 5 19 -1 203.661 354.700 4 -5 19 1 747.393 528.582 12 -5 19 1-249.785 406.204 7 5 -19 -1-498.638 465.289 10 -5 19 1-332.739 409.635 17 5 -19 -1-604.261 560.747 16 -5 -19 1 669.435 366.305 15 5 19 -1-69.2057 371.948 1 -5 19 0 15422.6 1282.67 12 5 -19 0 15735.3 1270.14 10 -5 19 0 16238.9 1157.56 17 5 -19 0 15025.4 1273.57 16 -5 -19 0 16152.8 1077.67 15 5 19 0 16204.9 1070.53 4 -5 -19 0 16274.4 1237.62 7 5 19 0 16493.1 1213.29 13 -5 19 0 14456.9 1151.65 7 -5 -19 -1 1336.50 488.596 7 5 19 1 1443.54 447.669 13 -5 19 -1 1260.46 643.554 12 -5 19 -1 1788.00 518.437 7 5 -19 1 1470.94 572.012 11 5 -19 1 1858.20 615.974 10 -5 19 -1 2003.80 531.334 3 -5 19 -1 774.884 391.054 17 5 -19 1 721.068 568.151 16 5 19 1 1254.93 513.509 9 -5 -19 -1 1881.92 488.064 15 -5 -19 -2 796.951 439.329 7 5 19 2 1364.43 431.557 13 -5 19 -2 1795.41 719.452 12 -5 19 -2 1309.47 477.327 7 5 -19 2 663.543 518.017 11 5 -19 2 1190.53 578.476 10 -5 19 -2 1225.91 552.660 3 5 -19 2 1667.02 644.313 16 5 19 2 1965.93 604.555 9 -5 -19 -2 944.174 482.482 15 5 19 2 3075.60 684.724 14 -5 -19 -3-104.699 413.418 7 -5 19 -3-152.930 603.283 12 -5 19 -3 15.1620 388.319 7 5 -19 3 291.686 498.286 11 5 -19 3 1453.19 647.387 10 -5 19 -3 11.0668 590.317 3 5 -19 3-547.413 552.139 16 5 19 3-501.621 517.156 9 -5 -19 -3 391.919 459.067 15 5 19 3 191.729 459.580 14 -5 19 -4 8556.10 1207.31 12 -5 19 -4 7458.45 811.898 7 5 -19 4 6920.67 962.280 11 5 -19 4 7872.98 1092.65 10 -5 19 -4 7166.72 1034.27 3 5 -19 4 7669.69 1090.12 16 5 19 4 7565.64 977.355 9 -5 -19 -4 7819.13 960.532 15 5 19 4 7648.20 956.338 14 -5 -19 -4 7938.83 928.133 7 -5 19 -5 1183.98 768.063 12 5 -19 5-25.6379 527.909 11 5 -19 5-698.378 583.063 10 -5 19 -5-757.793 632.887 3 5 -19 5-299.406 572.266 16 5 19 5 591.365 618.034 9 -5 -19 -5 457.570 574.096 15 5 19 5-1121.28 597.582 14 -5 -19 -6 1932.57 711.826 3 -5 19 -6 3143.96 836.926 3 5 19 6 1221.93 620.534 8 -5 20 10 4367.95 816.690 18 5 20 -9 1028.69 744.932 13 5 -20 -9 286.061 561.680 1 5 -20 -9 1463.88 667.867 5 -5 20 9-220.065 472.042 18 5 20 -8 2787.10 755.226 13 5 20 -8 1985.87 701.324 4 -5 20 8 1794.40 558.231 7 5 -20 -8 2165.24 692.558 1 5 -20 -8 2603.92 724.853 5 -5 20 8 1796.65 601.524 18 -5 20 8 3158.61 746.653 17 -5 -20 8 1275.34 523.841 7 5 20 -7 9647.83 1172.05 13 -5 -20 7 7865.66 846.610 2 5 20 -7 8110.16 1038.15 4 5 -20 -7 7960.45 956.833 1 5 20 -7 9170.79 885.053 1 -5 20 7 7838.67 873.405 7 5 -20 -7 7082.63 942.934 5 -5 20 7 7857.88 970.347 18 -5 -20 7 9058.05 864.100 17 -5 20 7 7318.75 1058.29 17 -5 -20 7 7914.34 906.166 7 -5 -20 6 393.508 390.548 7 5 20 -6 1062.71 584.439 13 5 20 -6 1634.99 582.583 4 -5 -20 6 1308.00 476.803 2 5 20 -6 1543.34 468.037 1 -5 20 6 1776.46 532.332 7 5 -20 -6 1295.95 570.819 5 -5 20 6 1954.80 638.537 18 -5 -20 6 1317.93 471.098 17 -5 20 6 1280.44 587.460 17 5 -20 -6 1587.40 522.931 1 -5 -20 5 572.168 489.007 7 5 20 -5 1715.33 683.769 13 5 20 -5 1336.78 463.041 1 5 20 -5 1593.26 592.909 4 -5 -20 5 1699.89 532.349 2 -5 20 5 2116.19 553.737 7 -5 20 5 1013.46 610.547 18 -5 -20 5 1862.54 519.255 17 -5 20 5 1420.18 596.400 17 5 -20 -5 2339.29 682.945 16 5 -20 -5 1879.08 503.763 1 -5 -20 4 9660.06 982.150 7 5 20 -4 10826.0 1112.36 13 -5 20 4 9930.90 916.556 12 -5 20 4 9118.41 955.802 7 5 -20 -4 10976.0 1049.04 10 5 20 -4 11131.9 952.012 1 -5 20 4 9359.75 1044.06 18 -5 -20 4 8382.62 880.139 17 -5 20 4 8874.31 1025.90 17 5 -20 -4 9159.46 987.595 16 5 -20 -4 8854.25 779.623 1 5 20 -4 11306.3 1076.38 4 -5 -20 4 11036.8 1024.01 2 -5 -20 3 539.997 472.924 7 5 20 -3 1538.35 599.605 13 5 20 -3 2015.19 567.095 4 -5 20 3 1396.74 516.130 12 -5 20 3 2022.25 594.253 7 -5 -20 3 2070.91 587.683 2 5 -20 -3 1397.43 372.653 1 5 -20 -3 1646.80 586.812 10 -5 -20 3 2607.18 598.778 17 -5 20 3 455.231 441.687 17 5 -20 -3 1310.39 593.769 16 5 20 -3 1772.82 449.476 1 -5 -20 2 1636.94 500.121 7 5 20 -2 2334.78 586.667 13 5 20 -2 2444.73 544.236 4 -5 20 2 2103.12 614.907 12 -5 20 2 1991.02 576.581 7 5 -20 -2 2066.70 609.399 10 -5 20 2 3167.31 653.426 17 5 -20 -2 2717.35 665.414 16 5 20 -2 2982.85 615.278 1 -5 20 1 11149.4 1090.34 12 5 -20 -1 11702.9 1125.14 10 -5 20 1 12476.5 1075.80 17 5 -20 -1 13252.7 1177.99 16 5 20 -1 11719.4 961.679 4 -5 -20 1 11677.2 1066.26 7 5 20 -1 10918.1 1057.55 13 -5 20 1 11533.0 1063.24 7 -5 -20 0 3726.19 681.582 7 5 20 0 2846.82 615.056 13 5 20 0 3834.86 597.759 4 -5 20 0 3740.48 780.853 12 -5 20 0 2867.56 626.685 7 5 -20 0 4145.67 755.253 10 -5 20 0 3696.68 616.701 17 5 -20 0 4620.55 816.669 16 5 20 0 5259.23 769.701 9 -5 -20 0 3810.96 593.955 15 -5 -20 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20 -4 1476.64 709.916 3 5 -20 4 774.700 640.909 16 5 20 4 1014.46 592.886 9 -5 -20 -4 1096.52 597.736 15 5 20 4 699.876 555.544 14 -5 -20 -4-6.80510 457.014 7 5 -20 5 5121.97 977.321 10 -5 20 -5 3683.69 873.910 3 5 -20 5 4569.43 909.266 16 5 20 5 6741.55 983.629 9 -5 -20 -5 6459.81 939.734 15 5 20 5 4471.35 838.984 14 5 20 5 3077.47 780.076 8 5 20 6 1366.26 649.553 8 -5 21 9 10545.6 1147.13 18 5 21 -8 1542.43 695.585 13 5 21 -8-185.803 556.647 4 -5 21 8 353.040 491.714 7 5 -21 -8 804.952 568.044 1 5 -21 -8 471.983 553.749 5 -5 21 8-438.872 521.656 18 -5 21 8-211.119 620.423 17 -5 -21 8-678.156 495.533 7 5 21 -7 346.257 579.471 13 -5 -21 7 865.449 420.938 2 5 21 -7-629.104 574.948 4 5 -21 -7 10.4329 449.696 1 5 21 -7-128.094 366.676 1 -5 21 7-175.582 405.947 7 5 -21 -7 765.289 561.775 5 -5 21 7-434.076 531.372 18 -5 21 7-147.912 569.848 17 -5 -21 7 547.638 495.065 7 5 21 -6 2821.67 740.404 13 5 21 -6 2142.94 687.942 4 5 21 -6 1979.39 510.539 1 -5 -21 6 1374.76 507.653 2 -5 21 6 1037.54 468.720 7 5 -21 -6 1743.49 621.987 5 -5 21 6 1740.76 639.681 18 -5 -21 6 1309.03 507.932 17 -5 21 6 1601.67 700.802 17 5 -21 -6 3628.00 719.442 16 5 -21 -6 2208.52 565.074 1 -5 -21 6 2073.35 590.531 7 -5 -21 5 7998.27 934.029 7 5 21 -5 8320.89 1064.40 13 5 21 -5 8840.72 853.623 1 5 21 -5 8735.81 1040.54 4 -5 21 5 8056.43 988.972 18 -5 -21 5 10134.2 992.249 2 -5 21 5 8028.23 921.729 7 5 -21 -5 8454.40 954.973 10 -5 -21 5 8266.21 869.468 17 -5 21 5 7758.88 998.104 17 5 -21 -5 10234.9 1038.09 16 5 -21 -5 7954.87 815.103 1 -5 -21 4 223.162 450.373 7 5 21 -4-515.282 535.145 13 5 21 -4 397.782 477.430 4 -5 21 4 374.549 403.039 12 -5 -21 4-274.581 459.344 2 -5 21 4 83.5511 476.008 7 5 -21 -4 921.460 530.043 10 -5 21 4 1054.03 586.793 18 -5 -21 4 114.658 428.063 17 5 -21 -4 634.972 351.419 1 -5 21 4 432.825 517.763 17 5 -21 -4 704.959 555.570 16 5 21 -4 374.509 402.182 1 -5 21 3 12569.6 1093.03 12 5 21 -3 13065.4 1054.56 1 5 -21 -3 13429.6 1168.38 10 -5 -21 3 12687.0 1097.35 17 -5 21 3 12038.7 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18 -8 -5 4 813.471 491.510 18 8 -5 -4 1683.27 548.727 1 -8 -5 4 1401.90 551.088 17 -8 5 4 1806.37 611.033 17 8 5 -3 11579.2 1095.98 1 8 -5 -3 10568.2 1011.20 1 -8 5 3 11790.9 1249.82 18 -8 -5 3 9943.57 1011.21 18 -8 5 3 10933.8 1100.81 17 -8 -5 3 10766.1 1086.07 17 -8 -5 3 12128.5 1135.21 7 -8 5 3 12464.0 1135.37 7 -8 -5 2 784.056 469.858 7 8 5 -2 1434.84 525.236 1 -8 5 2 1240.32 545.869 7 8 -5 -2 1031.94 462.118 1 -8 5 2 812.027 623.056 3 -8 5 2 1557.15 703.297 18 -8 -5 2 2026.04 604.904 18 -8 -5 2 588.509 558.010 17 -8 5 2 1313.82 547.253 17 8 5 -1 1787.25 596.698 1 -8 -5 1 1482.40 581.689 7 -8 5 1 2000.34 717.543 7 8 -5 -1 934.024 448.888 1 -8 5 1 1178.59 599.937 3 -8 -5 1 867.530 501.611 18 -8 -5 1 1598.78 600.390 17 -8 5 1 1458.75 562.791 17 8 -5 0 2931.10 586.277 1 -8 -5 0 3865.10 709.332 7 -8 5 0 4098.95 764.963 7 -8 -5 0 2811.11 729.926 3 -8 5 0 3677.88 768.733 3 8 -5 0 5322.59 876.431 10 -8 -5 0 3253.37 681.897 17 -8 5 0 3585.45 667.395 17 8 -5 0 4867.51 853.558 16 8 5 0 5655.48 808.010 1 -8 -5 -1 2525.24 635.142 7 -8 5 -1 2029.45 563.593 7 -8 -5 -1 3181.34 845.562 3 8 -5 1 4891.87 865.901 11 -8 5 -1 3884.23 901.835 3 8 -5 1 2868.60 728.399 10 -8 -5 -1 5459.68 830.119 17 -8 5 -1 2081.85 562.995 17 8 -5 1 2643.90 679.825 16 8 -5 1 2404.83 641.431 9 8 5 1 3830.51 777.303 9 8 5 1 5100.73 790.959 1 -8 -5 -2 210.428 487.130 7 -8 5 -2 172.460 414.908 7 8 -5 2 940.592 602.028 11 -8 5 -2 2226.62 780.988 3 8 -5 2 949.332 592.258 10 -8 -5 -2 321.907 486.754 17 8 -5 2 1208.52 571.146 16 -8 -5 -3 5682.00 799.952 7 -8 5 -3 6115.59 816.629 7 -8 -5 -3 6923.99 930.548 17 -8 -5 -3 4189.03 758.981 15 -8 -6 8 6907.97 908.784 7 -8 6 8 6792.59 876.869 7 -8 -6 7-784.320 530.997 7 -8 6 7 579.295 507.833 7 -8 -6 7 303.815 530.495 18 -8 -6 7-194.277 470.824 17 8 -6 -7 67.3128 448.891 1 -8 -6 6 1084.40 557.483 7 -8 6 6 77.0557 472.163 7 8 6 -6 469.560 470.763 1 -8 6 6 947.630 686.200 18 -8 -6 6 610.153 538.236 18 -8 -6 6 1063.64 582.685 17 -8 6 6 365.006 451.157 17 8 -6 -6 567.685 438.692 1 -8 -6 5 601.003 500.813 7 -8 6 5-0.48311 420.093 7 8 6 -5-247.812 453.337 1 -8 -6 5 342.503 472.430 18 -8 -6 5 38.1263 444.433 17 8 -6 -5 446.836 457.531 1 -8 6 5 889.532 547.363 17 8 6 -4 16649.4 1281.53 1 -8 -6 4 12485.0 1135.49 18 -8 6 4 12074.8 1264.00 18 8 -6 -4 13070.5 1138.49 1 -8 -6 4 16919.6 1313.03 17 -8 6 4 13126.7 1199.21 17 -8 -6 4 12556.1 1173.90 7 -8 6 4 13706.2 1230.22 7 -8 -6 3 403.362 589.953 7 -8 6 3 271.882 454.462 7 8 6 -3 41.5202 429.146 1 8 -6 -3-96.4817 376.974 1 -8 6 3 723.635 696.140 18 -8 -6 3 643.953 468.156 18 -8 -6 3 2018.10 644.911 17 -8 6 3 264.731 455.033 17 -8 -6 2 7583.32 941.682 7 8 6 -2 6575.85 883.929 1 -8 6 2 7043.85 905.530 7 8 -6 -2 6457.42 808.988 1 -8 6 2 6398.77 832.616 3 -8 6 2 8336.19 1104.19 18 -8 -6 2 7383.20 856.229 18 -8 -6 2 6261.02 874.438 17 -8 6 2 6157.67 844.513 17 8 6 -1 390.474 431.304 1 -8 -6 1-494.206 522.703 7 -8 6 1 89.0495 435.881 7 8 -6 -1 32.7554 399.758 1 -8 6 1-322.575 580.524 3 -8 -6 1 1000.21 558.386 17 -8 6 1-463.927 457.883 17 8 -6 0 13.5850 344.923 1 -8 -6 0 387.909 527.052 7 -8 -6 0-33.1315 599.329 3 -8 6 0-172.049 429.076 7 -8 6 0 1067.87 631.700 3 8 -6 0 816.171 605.352 10 -8 -6 0 77.7191 465.922 17 -8 6 0 617.187 450.795 17 8 -6 0 984.744 671.912 16 8 6 0 798.836 451.912 1 -8 -6 -1 42.0415 460.362 7 -8 6 -1-726.135 484.733 7 -8 -6 -1-500.184 685.931 3 8 -6 1 1579.64 677.313 11 -8 6 -1 39.5067 620.678 3 8 -6 1 848.148 601.062 10 -8 -6 -1 1286.97 483.969 17 -8 6 -1 100.347 399.383 17 8 -6 1-43.2739 529.354 16 8 6 1 1204.26 614.015 9 8 6 1-44.4739 442.594 1 -8 -6 -2 11874.5 1120.92 7 -8 6 -2 10212.8 1035.88 7 8 -6 2 11835.2 1184.34 11 -8 6 -2 11775.6 1317.88 3 8 -6 2 9923.90 1118.43 10 -8 -6 -2 10675.0 1116.50 17 8 -6 2 11038.2 1174.79 16 -8 -6 -3-174.491 436.402 7 -8 6 -3 950.918 475.575 7 8 -6 3 251.644 479.400 10 -8 -6 -3-456.203 477.701 17 8 -6 3-175.724 507.952 16 -8 -6 -3-702.548 541.659 15 -8 -7 7 1793.64 585.778 7 -8 7 7 2119.56 620.354 7 -8 -7 7 3090.94 707.274 18 -8 -7 6 2261.40 631.081 7 -8 7 6 1022.93 466.218 7 8 7 -6 2837.82 672.106 1 -8 7 6 956.990 602.774 18 -8 -7 6 1875.79 592.152 18 -8 -7 6 1912.58 629.171 17 -8 7 6 1624.40 591.825 17 8 -7 -6 1747.85 571.411 1 -8 -7 5 1119.43 555.361 7 -8 7 5 1000.62 510.923 7 8 7 -5 1725.94 577.005 1 -8 7 5 1642.56 708.285 18 -8 -7 5 1307.57 567.969 18 -8 -7 5 947.385 509.337 17 -8 7 5 634.447 491.914 17 8 -7 -5 1801.87 569.355 1 -8 -7 4 521.029 476.479 7 -8 7 4 978.439 587.339 7 8 7 -4-81.9222 450.630 1 -8 7 4 184.138 591.279 18 -8 -7 4 561.457 524.644 18 8 -7 -4 562.132 492.718 1 -8 -7 4 1349.17 617.522 17 -8 7 4 1256.76 584.491 17 8 7 -3 14188.2 1222.59 1 -8 -7 3 12397.3 1078.62 18 -8 7 3 11461.8 1254.16 18 8 -7 -3 12302.9 1075.33 1 -8 7 3 13531.1 1200.20 17 -8 -7 3 11862.4 1150.64 17 -8 -7 3 13318.3 1213.14 7 -8 7 3 12433.3 1172.01 7 8 7 -2 574.221 491.592 1 -8 -7 2 199.108 446.057 7 -8 7 2 1459.51 639.503 7 8 -7 -2 559.253 436.301 1 -8 7 2 1544.90 773.638 18 -8 -7 2 130.338 478.526 17 -8 7 2 321.597 452.463 17 -8 -7 1 1806.16 607.733 7 -8 7 1 1845.58 616.571 7 8 -7 -1 729.728 419.500 1 -8 7 1 3016.80 760.477 3 -8 -7 1 1977.56 669.698 17 -8 7 1 1216.73 520.251 17 8 7 -1 2373.01 615.392 1 -8 -7 0 1741.96 616.656 7 -8 7 0 1963.27 579.445 7 -8 7 0 2757.67 780.898 3 8 -7 0 3263.76 727.782 10 -8 -7 0 1311.12 553.113 17 -8 7 0 1822.71 526.895 17 8 -7 0 2694.94 728.270 16 8 7 0 2716.13 649.443 1 -8 -7 -1 2426.51 630.870 7 -8 7 -1 3271.41 642.482 7 8 7 1 2930.53 653.771 1 8 -7 1 3061.49 754.904 11 -8 7 -1 3594.48 821.879 3 8 -7 1 3036.52 771.745 10 -8 -7 -1 2083.88 608.374 17 -8 7 -1 2094.92 534.652 17 8 -7 1 2609.95 733.675 16 8 7 1 4320.26 835.435 9 -8 -7 -2-277.533 467.701 7 -8 7 -2 433.786 444.628 7 -8 7 -2-134.988 623.047 3 8 -7 2-493.463 517.958 10 -8 -7 -2-73.7823 451.528 17 8 -7 2 212.889 506.305 16 -8 -7 -3 6340.93 863.438 7 -8 7 -3 5961.84 811.794 7 -8 -7 -3 7120.66 924.215 17 -8 -7 -3 5801.07 847.638 15 -8 -8 7 5881.04 867.198 7 -8 8 7 6276.87 842.253 7 -8 -8 7 7023.11 915.940 18 -8 -8 6 955.559 636.790 7 -8 8 6 520.572 526.047 7 -8 8 6 700.367 683.131 18 -8 -8 6 871.120 488.096 18 -8 -8 6 709.559 440.985 17 8 -8 -6 879.739 487.341 1 -8 -8 5 3921.10 736.856 7 -8 8 5 3141.66 661.946 7 8 8 -5 4831.51 789.977 1 -8 8 5 4694.25 897.195 18 -8 -8 5 3100.12 635.621 18 -8 -8 5 3946.23 746.139 17 -8 8 5 3528.49 706.203 17 8 -8 -5 3788.38 706.331 1 -8 -8 4 3662.61 717.921 7 -8 8 4 4305.94 804.235 7 8 8 -4 4488.37 773.638 1 -8 8 4 3125.55 800.865 18 -8 -8 4 3007.71 615.866 18 8 -8 -4 4547.24 723.921 1 -8 -8 4 4461.82 756.900 17 -8 8 4 3763.48 730.875 17 -8 -8 3 105.792 463.253 7 8 8 -3 822.805 536.103 1 -8 8 3 840.260 505.816 7 8 -8 -3 7.90533 389.656 1 -8 8 3 1101.97 724.349 18 -8 -8 3 370.249 498.163 17 -8 8 3 600.148 512.826 17 8 8 -2 2065.85 603.938 1 -8 -8 2 1896.05 595.823 7 -8 8 2 1749.27 608.492 7 8 -8 -2 1350.52 493.498 1 -8 8 2 3365.08 841.393 18 -8 -8 2 2088.77 606.760 17 -8 8 2 1878.31 597.412 17 -8 -8 1 11062.2 1114.72 7 -8 8 1 9719.96 1037.69 7 8 -8 -1 9609.75 908.289 1 -8 -8 1 10089.9 1092.89 17 -8 8 1 7355.42 911.081 17 8 -8 -1 9757.28 1133.06 16 8 8 -1 9472.13 1026.80 1 -8 -8 0-220.900 452.899 7 -8 8 0-338.940 438.582 7 -8 8 0 1312.72 713.340 3 8 -8 0 1229.99 651.173 10 -8 -8 0 510.207 502.930 17 -8 8 0 51.9978 441.322 17 8 -8 0 841.430 638.806 16 8 8 0 1031.40 558.173 1 -8 -8 -1 2532.52 642.006 7 -8 8 -1 2788.79 658.969 7 8 8 1 2961.16 686.161 1 8 -8 1 5261.20 889.547 11 -8 8 -1 3595.35 877.388 3 8 -8 1 2946.31 774.782 10 -8 -8 -1 2396.32 632.722 17 -8 8 -1 4108.14 738.694 17 8 -8 1 3130.97 755.861 16 -8 -8 -2 3724.49 722.989 7 -8 8 -2 3870.68 699.521 7 -8 8 -2 4386.93 890.943 3 8 -8 2 4467.88 867.443 10 -8 -8 -2 4230.32 780.161 17 8 -8 2 3801.25 805.903 16 -8 -8 -3 506.792 454.149 7 -8 8 -3 530.113 450.325 7 -8 -9 7-121.428 467.226 18 -8 -9 6 15929.2 1296.65 18 -8 -9 6 15703.1 1332.25 17 8 -9 -6 16317.3 1292.19 1 -8 -9 6 15451.4 1342.53 7 -8 9 6 16997.1 1352.85 7 -8 -9 5 82.6736 455.287 7 -8 9 5 347.811 531.707 7 8 9 -5 286.337 421.109 1 -8 9 5 784.876 631.759 18 -8 -9 5-811.326 530.149 18 -8 -9 5 417.759 544.136 17 -8 9 5 874.677 549.416 17 8 -9 -5 543.486 475.756 1 -8 -9 4 2829.40 666.629 7 -8 9 4 3369.92 722.191 7 8 9 -4 2238.47 631.036 1 -8 9 4 2547.47 802.539 18 8 -9 -4 1545.16 504.115 1 -8 -9 4 3206.54 681.766 17 -8 9 4 1644.64 575.835 17 -8 -9 3 373.070 512.376 7 8 9 -3 290.248 469.938 1 -8 9 3 877.246 472.035 7 8 -9 -3 414.198 466.928 1 -8 9 3 1062.17 657.692 18 -8 -9 3-73.5633 466.624 17 -8 9 3 283.851 496.217 17 8 9 -2 2127.89 641.658 1 -8 -9 2 3424.31 744.926 7 -8 9 2 4000.08 776.038 7 8 -9 -2 3444.65 622.974 1 -8 -9 2 2619.93 665.971 17 -8 9 2 3768.85 723.089 17 -8 -9 1-29.0410 486.683 7 -8 9 1-620.150 450.140 7 8 -9 -1 2193.95 731.920 10 -8 -9 1-338.916 479.200 17 -8 9 1 894.302 525.014 17 8 -9 -1 2079.61 712.299 16 8 9 -1 91.2082 470.463 1 8 9 0 14612.6 1250.29 1 -8 9 0 12679.9 1249.59 3 8 -9 0 15186.7 1391.85 10 -8 -9 0 14356.6 1275.79 17 -8 9 0 13202.2 1160.82 17 8 -9 0 13361.6 1300.25 16 -8 -9 0 13410.0 1240.75 7 -8 9 0 13439.7 1196.49 7 -8 -9 -1 352.937 491.696 7 -8 9 -1 670.081 512.939 7 -8 9 -1 765.433 639.844 3 8 -9 1 56.4710 513.044 10 -8 -9 -1 606.656 539.426 17 -8 9 -1 539.666 460.076 17 8 -9 1 364.603 557.908 16 -8 -9 -2 1116.11 508.288 7 -8 9 -2 116.273 459.605 7 -8 9 -2 235.082 617.411 3 -8 -10 7 10918.4 1123.17 18 -8 -10 6 605.264 489.668 18 8 -10 -6 239.977 456.708 1 -8 -10 5 8567.88 1036.72 7 -8 10 5 8577.15 1006.45 7 8 10 -5 10851.2 1089.84 1 -8 10 5 8002.30 1134.24 18 -8 -10 5 8948.88 1031.62 17 -8 10 5 9152.88 1055.41 17 8 -10 -5 8611.23 952.905 1 -8 -10 4 643.682 554.668 7 -8 10 4 2139.12 692.655 7 8 10 -4 1024.15 545.485 1 -8 10 4 837.635 682.167 18 8 -10 -4 955.159 475.969 1 -8 -10 4 854.882 576.348 17 -8 10 4 1050.33 569.137 17 -8 -10 3 1068.68 602.549 7 8 10 -3 517.215 498.456 1 -8 10 3 539.744 543.520 7 8 -10 -3 55.6648 365.169 1 -8 10 3 417.014 638.213 18 -8 -10 3-135.102 522.076 17 -8 10 3 541.888 479.621 17 8 10 -2-392.310 530.973 1 -8 -10 2 831.592 531.704 7 -8 10 2 764.283 480.498 7 8 -10 -2 1774.59 495.381 1 -8 -10 2 1424.08 566.609 17 -8 10 2 74.0267 447.730 17 -8 10 1 11268.9 1133.63 7 8 -10 -1 13283.6 1296.94 10 8 10 -1 12774.8 1193.93 1 -8 -10 1 12814.0 1212.18 17 -8 10 1 11303.1 1100.76 17 8 -10 -1 12943.8 1261.22 16 -8 -10 1 13110.4 1200.39 7 -8 -10 0 660.120 556.619 7 -8 10 0 595.552 491.691 7 8 -10 0-132.533 559.848 10 -8 -10 0-75.3895 446.654 17 -8 10 0-468.479 424.420 17 -8 -10 -1 4652.54 775.404 7 -8 10 -1 2966.76 709.144 7 -8 10 -1 5234.41 950.733 3 -8 10 -2 1681.47 732.328 3 8 -11 -6 5001.44 773.914 1 8 -11 -5-2.75435 407.721 1 -8 -11 4 2147.35 710.622 7 8 11 -4 2055.93 598.387 1 -8 11 4 1922.13 647.151 7 -8 11 4 1435.61 663.130 18 8 -11 -4 1224.09 524.251 1 -8 -11 4 3136.43 749.711 17 -8 11 4 1090.32 565.284 17 -8 -11 3 8919.50 1044.34 7 8 11 -3 6003.09 846.776 1 -8 11 3 6158.95 885.546 7 8 -11 -3 6630.54 789.025 1 -8 11 3 6360.10 1050.51 18 -8 -11 3 6817.83 907.008 17 -8 11 3 5660.84 851.491 17 8 11 -2 1632.56 584.640 1 -8 -11 2 1627.82 657.182 7 -8 11 2 859.625 545.843 7 -8 11 2 3305.97 966.099 18 -8 -11 2 1423.60 572.664 17 -8 11 2 1444.43 588.223 17 8 -11 -2 1841.59 727.842 16 -8 -11 1 1987.54 627.029 7 -8 11 1 623.865 566.738 7 8 -11 -1 2323.20 743.222 10 -8 -11 1 742.404 536.454 17 -8 11 1 1341.06 589.379 17 8 -11 -1 840.741 656.894 16 -8 -11 0 6282.33 887.553 7 -8 11 0 6102.18 902.773 7 -8 11 0 6689.63 874.693 17 -8 11 -1 2661.80 806.467 3 -8 11 -2-370.416 624.984 3 8 -12 -6 1127.63 535.107 1 8 -12 -5 696.985 475.521 1 8 -12 -4 10487.1 1012.41 1 -8 12 4 11523.2 1174.86 17 8 -12 -3 1214.78 502.162 1 -8 12 3 1838.85 844.510 18 -8 12 3 246.286 450.483 17 8 -12 -2 7256.34 1044.80 10 -8 12 2 8793.11 1228.97 18 -8 12 2 6357.08 887.035 17 8 -12 -2 7190.01 1069.40 16 -8 12 1-37.0479 423.211 17 -8 12 0 19.4033 422.516 17 -8 12 -2 7906.78 1133.20 3 8 -13 -6 4085.94 701.240 1 8 -13 -5 2991.02 655.782 1 8 -13 -4 1660.40 514.061 1 -8 13 3 10484.7 1137.08 17 -8 13 2 605.406 492.929 17 -8 13 1 2221.29 582.725 17 8 13 0 1390.26 549.122 13 -8 13 0 1285.43 536.366 17 8 -14 -6 229.156 441.346 1 8 -14 -5 4522.30 738.600 1 -8 14 3-321.576 522.977 17 8 14 -2 1360.00 557.134 13 -8 14 2 1559.40 585.387 17 8 14 -1 5919.74 864.328 13 -8 14 1 4997.03 815.090 17 8 14 0-331.366 430.180 13 -8 14 0 1002.54 510.040 17 8 -15 -6 8469.42 970.018 1 8 -15 -5 125.097 423.662 1 -8 15 2 2356.13 606.847 17 8 15 -1 272.108 437.082 13 -8 15 1 534.314 483.112 17 8 15 0 10277.3 1084.15 13 -8 16 2 511.642 496.799 17 -8 16 1 10413.3 1116.62 17 -8 17 1-40.6478 474.150 17 -9 0 3 582.181 575.669 18 -9 0 2 347.085 555.808 18 -9 0 1 2340.64 721.076 18 -9 -1 3 3988.36 800.919 18 -9 -1 2 595.545 569.380 18 -9 -1 1 735.887 563.132 18 -9 -2 4 3543.58 761.479 18 -9 -2 3 1033.05 579.781 18 -9 -2 2 5726.94 919.567 18 -9 2 1 1244.16 656.177 3 -9 -3 4 628.500 638.580 18 -9 -3 3 13212.7 1251.17 18 -9 3 1 3396.58 815.580 3 -9 -4 4 1548.35 582.803 18 -9 4 1-71.5180 626.198 3 9 -5 -2 843.729 480.361 1 9 -6 -2 884.659 543.662 1 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 58908 _shelx_res_file ; TITL Gera in P2(1)/n shelx.res created by SHELXL-2018/3 at 11:30:15 on 17-Sep-2021 CELL 0.71073 6.406758 25.254219 9.339531 90.0000 103.9460 90.0000 ZERR 4.00 0.000260 0.001480 0.000404 0.0000 0.0041 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H N Cl Au UNIT 48.00 104.00 8.00 4.00 4.00 L.S. 8 TEMP -173 SIZE 0.21 0.03 0.01 SHEL 999 0.71 EQIV $1 -x, -y+1, -z+1 EQIV $2 -x+1, -y+1, -z+1 EQIV $3 x+1, y, z HTAB N21 Cl1 HTAB N11 Cl1_$1 HTAB C16 Cl1_$2 HTAB C22 Au1_$2 HTAB C23 Au1_$3 ACTA 60 CONF FMAP 2 PLAN 10 SADI N11 H01 N21 H02 WGHT 0.014100 1.459100 FVAR 1.08267 AU1 5 0.278502 0.581046 0.410858 11.00000 0.01176 0.01306 = 0.01248 0.00032 0.00385 -0.00121 CL1 4 0.073335 0.423716 0.253931 11.00000 0.01632 0.01831 = 0.02561 0.00744 0.00599 -0.00304 N11 3 0.221537 0.632225 0.567643 11.00000 0.00925 0.01598 = 0.01395 0.00157 0.00421 -0.00325 H01 2 0.139366 0.612366 0.613255 11.00000 0.01767 C12 1 0.098620 0.680273 0.505206 11.00000 0.00976 0.02176 = 0.01620 -0.00132 0.00219 0.00294 AFIX 23 H12A 2 0.058954 0.700496 0.585531 11.00000 -1.20000 H12B 2 -0.035734 0.669534 0.434086 11.00000 -1.20000 AFIX 0 C13 1 0.229350 0.715214 0.428161 11.00000 0.01433 0.01248 = 0.01459 0.00032 0.00089 0.00333 AFIX 23 H13A 2 0.145689 0.747515 0.391848 11.00000 -1.20000 H13B 2 0.255772 0.696126 0.341629 11.00000 -1.20000 AFIX 0 C14 1 0.446000 0.731335 0.529955 11.00000 0.01397 0.01065 = 0.01497 -0.00126 0.00354 0.00096 AFIX 13 H14 2 0.415702 0.754449 0.609509 11.00000 -1.20000 AFIX 0 C15 1 0.563485 0.681860 0.603290 11.00000 0.01338 0.01450 = 0.01411 -0.00130 0.00334 0.00201 AFIX 23 H15A 2 0.609429 0.660305 0.527799 11.00000 -1.20000 H15B 2 0.694185 0.692767 0.677764 11.00000 -1.20000 AFIX 0 C16 1 0.423258 0.648337 0.677382 11.00000 0.01493 0.01668 = 0.01141 0.00115 0.00097 0.00154 AFIX 23 H16A 2 0.503518 0.616358 0.720715 11.00000 -1.20000 H16B 2 0.385848 0.668775 0.758154 11.00000 -1.20000 AFIX 0 C17 1 0.583463 0.762998 0.447875 11.00000 0.02243 0.01908 = 0.02482 -0.00056 0.00653 -0.00192 AFIX 137 H17A 2 0.719934 0.772491 0.516224 11.00000 -1.50000 H17B 2 0.506738 0.795302 0.407423 11.00000 -1.50000 H17C 2 0.612007 0.741537 0.367261 11.00000 -1.50000 AFIX 0 N21 3 0.333381 0.529311 0.254500 11.00000 0.01442 0.00980 = 0.01616 0.00178 0.00623 -0.00340 H02 2 0.262526 0.498522 0.265880 11.00000 0.01275 C22 1 0.564423 0.514571 0.278196 11.00000 0.01990 0.01627 = 0.01830 0.00302 0.00640 0.00564 AFIX 23 H22A 2 0.580427 0.486931 0.206434 11.00000 -1.20000 H22B 2 0.617710 0.499995 0.378789 11.00000 -1.20000 AFIX 0 C23 1 0.696293 0.563137 0.258971 11.00000 0.01248 0.01647 = 0.01682 0.00208 0.00318 0.00116 AFIX 23 H23A 2 0.848096 0.552454 0.270366 11.00000 -1.20000 H23B 2 0.691474 0.589011 0.337743 11.00000 -1.20000 AFIX 0 C24 1 0.615211 0.589850 0.108666 11.00000 0.01881 0.00710 = 0.01672 -0.00237 0.00770 -0.00193 AFIX 13 H24 2 0.644492 0.565394 0.031584 11.00000 -1.20000 AFIX 0 C25 1 0.373040 0.598722 0.076349 11.00000 0.01538 0.01574 = 0.00889 0.00245 0.00176 -0.00146 AFIX 23 H25A 2 0.342750 0.627499 0.140439 11.00000 -1.20000 H25B 2 0.320515 0.610250 -0.027422 11.00000 -1.20000 AFIX 0 C26 1 0.251462 0.549376 0.101453 11.00000 0.01257 0.01568 = 0.01624 -0.00107 0.00159 -0.00063 AFIX 23 H26A 2 0.096396 0.557673 0.084466 11.00000 -1.20000 H26B 2 0.268389 0.521627 0.030228 11.00000 -1.20000 AFIX 0 C27 1 0.734685 0.641903 0.099597 11.00000 0.02381 0.02022 = 0.02604 0.00104 0.00803 -0.00672 AFIX 137 H27A 2 0.692865 0.655692 -0.001365 11.00000 -1.50000 H27B 2 0.890107 0.635485 0.126803 11.00000 -1.50000 H27C 2 0.697421 0.667793 0.167558 11.00000 -1.50000 AFIX 0 HKLF 4 REM Gera in P2(1)/n REM wR2 = 0.0482, GooF = S = 1.157, Restrained GooF = 1.157 for all data REM R1 = 0.0326 for 3650 Fo > 4sig(Fo) and 0.0446 for all 4248 data REM 155 parameters refined using 1 restraints END WGHT 0.0141 1.4669 REM Highest difference peak 1.128, deepest hole -1.569, 1-sigma level 0.169 Q1 1 0.2179 0.5490 0.4105 11.00000 0.05 1.13 Q2 1 0.3341 0.6159 0.3921 11.00000 0.05 0.99 Q3 1 0.2266 0.6179 0.4112 11.00000 0.05 0.92 Q4 1 0.3149 0.7591 0.7241 11.00000 0.05 0.83 Q5 1 0.3482 0.5496 0.4120 11.00000 0.05 0.76 Q6 1 0.2495 0.6080 0.5019 11.00000 0.05 0.75 Q7 1 0.0827 0.7419 0.6460 11.00000 0.05 0.73 Q8 1 0.0389 0.5824 0.3840 11.00000 0.05 0.73 Q9 1 0.4412 0.5842 0.4255 11.00000 0.05 0.72 Q10 1 0.2179 0.4700 0.2684 11.00000 0.05 0.70 ; _shelx_res_checksum 50568 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Au Au1 0.27850(2) 0.58105(2) 0.41086(2) 0.01228(4) Uani d 1 . . Cl Cl1 0.07333(15) 0.42372(4) 0.25393(10) 0.01992(19) Uani d 1 . . N N11 0.2215(5) 0.63222(12) 0.5676(3) 0.0128(6) Uani d 1 . . H H01 0.139(6) 0.6124(15) 0.613(4) 0.018(11) Uiso d 1 . . C C12 0.0986(6) 0.68027(15) 0.5052(4) 0.0161(8) Uani d 1 . . H H12A 0.058954 0.700496 0.585531 0.019 Uiso calc 1 . . H H12B -0.035734 0.669534 0.434086 0.019 Uiso calc 1 . . C C13 0.2293(6) 0.71521(14) 0.4282(4) 0.0142(7) Uani d 1 . . H H13A 0.145689 0.747515 0.391848 0.017 Uiso calc 1 . . H H13B 0.255772 0.696126 0.341629 0.017 Uiso calc 1 . . C C14 0.4460(6) 0.73133(13) 0.5300(4) 0.0132(7) Uani d 1 . . H H14 0.415702 0.754449 0.609509 0.016 Uiso calc 1 . . C C15 0.5635(6) 0.68186(14) 0.6033(4) 0.0140(7) Uani d 1 . . H H15A 0.609429 0.660305 0.527799 0.017 Uiso calc 1 . . H H15B 0.694185 0.692767 0.677764 0.017 Uiso calc 1 . . C C16 0.4233(6) 0.64834(14) 0.6774(4) 0.0147(7) Uani d 1 . . H H16A 0.503518 0.616358 0.720715 0.018 Uiso calc 1 . . H H16B 0.385848 0.668775 0.758154 0.018 Uiso calc 1 . . C C17 0.5835(7) 0.76300(15) 0.4479(4) 0.0220(8) Uani d 1 . . H H17A 0.719934 0.772491 0.516224 0.033 Uiso calc 1 . . H H17B 0.506738 0.795302 0.407423 0.033 Uiso calc 1 . . H H17C 0.612007 0.741537 0.367261 0.033 Uiso calc 1 . . N N21 0.3334(5) 0.52931(12) 0.2545(3) 0.0130(6) Uani d 1 . . H H02 0.263(6) 0.4985(13) 0.266(4) 0.013(10) Uiso d 1 . . C C22 0.5644(6) 0.51457(15) 0.2782(4) 0.0179(8) Uani d 1 . . H H22A 0.580427 0.486931 0.206434 0.021 Uiso calc 1 . . H H22B 0.617710 0.499995 0.378789 0.021 Uiso calc 1 . . C C23 0.6963(6) 0.56314(14) 0.2590(4) 0.0153(7) Uani d 1 . . H H23A 0.848096 0.552454 0.270366 0.018 Uiso calc 1 . . H H23B 0.691474 0.589011 0.337743 0.018 Uiso calc 1 . . C C24 0.6152(6) 0.58985(13) 0.1087(4) 0.0136(7) Uani d 1 . . H H24 0.644492 0.565394 0.031584 0.016 Uiso calc 1 . . C C25 0.3730(6) 0.59872(14) 0.0763(4) 0.0135(7) Uani d 1 . . H H25A 0.342750 0.627499 0.140439 0.016 Uiso calc 1 . . H H25B 0.320515 0.610250 -0.027422 0.016 Uiso calc 1 . . C C26 0.2515(6) 0.54938(14) 0.1015(4) 0.0152(7) Uani d 1 . . H H26A 0.096396 0.557673 0.084466 0.018 Uiso calc 1 . . H H26B 0.268389 0.521627 0.030228 0.018 Uiso calc 1 . . C C27 0.7347(7) 0.64190(15) 0.0996(5) 0.0230(9) Uani d 1 . . H H27A 0.692865 0.655692 -0.001365 0.035 Uiso calc 1 . . H H27B 0.890107 0.635485 0.126803 0.035 Uiso calc 1 . . H H27C 0.697421 0.667793 0.167558 0.035 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Au1 0.01176(6) 0.01306(6) 0.01248(7) -0.00121(6) 0.00385(4) 0.00032(6) Cl1 0.0163(4) 0.0183(5) 0.0256(5) -0.0030(4) 0.0060(4) 0.0074(4) N11 0.0093(14) 0.0160(15) 0.0139(16) -0.0032(13) 0.0042(12) 0.0016(12) C12 0.0098(17) 0.0218(19) 0.0162(18) 0.0029(15) 0.0022(14) -0.0013(15) C13 0.0143(19) 0.0125(17) 0.0146(18) 0.0033(14) 0.0009(14) 0.0003(14) C14 0.0140(18) 0.0106(16) 0.0150(17) 0.0010(14) 0.0035(14) -0.0013(13) C15 0.0134(18) 0.0145(17) 0.0141(18) 0.0020(14) 0.0033(14) -0.0013(14) C16 0.0149(18) 0.0167(18) 0.0114(17) 0.0015(15) 0.0010(14) 0.0011(14) C17 0.022(2) 0.019(2) 0.025(2) -0.0019(17) 0.0065(17) -0.0006(16) N21 0.0144(15) 0.0098(14) 0.0162(15) -0.0034(12) 0.0062(12) 0.0018(12) C22 0.020(2) 0.0163(19) 0.0183(19) 0.0056(15) 0.0064(16) 0.0030(15) C23 0.0125(18) 0.0165(17) 0.0168(18) 0.0012(14) 0.0032(14) 0.0021(14) C24 0.0188(19) 0.0071(17) 0.0167(17) -0.0019(14) 0.0077(14) -0.0024(13) C25 0.0154(18) 0.0157(17) 0.0089(16) -0.0015(14) 0.0018(14) 0.0024(13) C26 0.0126(19) 0.0157(17) 0.0162(18) -0.0006(14) 0.0016(15) -0.0011(15) C27 0.024(2) 0.0202(19) 0.026(2) -0.0067(18) 0.0080(17) 0.0010(18) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag N11 Au1 N21 . . 179.43(12) y C12 N11 C16 . . 109.5(3) ? C12 N11 Au1 . . 113.8(2) ? C16 N11 Au1 . . 112.8(2) ? N11 C12 C13 . . 111.2(3) ? C12 C13 C14 . . 112.4(3) ? C17 C14 C15 . . 111.8(3) ? C17 C14 C13 . . 111.9(3) ? C15 C14 C13 . . 109.5(3) ? C16 C15 C14 . . 112.2(3) ? N11 C16 C15 . . 110.3(3) ? C26 N21 C22 . . 109.6(3) ? C26 N21 Au1 . . 112.7(2) ? C22 N21 Au1 . . 112.8(2) ? N21 C22 C23 . . 109.9(3) ? C22 C23 C24 . . 112.8(3) ? C25 C24 C23 . . 110.5(3) ? C25 C24 C27 . . 111.2(3) ? C23 C24 C27 . . 111.4(3) ? C26 C25 C24 . . 112.6(3) ? N21 C26 C25 . . 110.7(3) ? C12 N11 H01 . . 109(3) ? C16 N11 H01 . . 109(3) ? Au1 N11 H01 . . 102(3) ? N11 C12 H12A . . 109.4 ? C13 C12 H12A . . 109.4 ? N11 C12 H12B . . 109.4 ? C13 C12 H12B . . 109.4 ? H12A C12 H12B . . 108.0 ? C12 C13 H13A . . 109.1 ? C14 C13 H13A . . 109.1 ? C12 C13 H13B . . 109.1 ? C14 C13 H13B . . 109.1 ? H13A C13 H13B . . 107.9 ? C17 C14 H14 . . 107.8 ? C15 C14 H14 . . 107.8 ? C13 C14 H14 . . 107.8 ? C16 C15 H15A . . 109.2 ? C14 C15 H15A . . 109.2 ? C16 C15 H15B . . 109.2 ? C14 C15 H15B . . 109.2 ? H15A C15 H15B . . 107.9 ? N11 C16 H16A . . 109.6 ? C15 C16 H16A . . 109.6 ? N11 C16 H16B . . 109.6 ? C15 C16 H16B . . 109.6 ? H16A C16 H16B . . 108.1 ? C14 C17 H17A . . 109.5 ? C14 C17 H17B . . 109.5 ? H17A C17 H17B . . 109.5 ? C14 C17 H17C . . 109.5 ? H17A C17 H17C . . 109.5 ? H17B C17 H17C . . 109.5 ? C26 N21 H02 . . 109(2) ? C22 N21 H02 . . 106(3) ? Au1 N21 H02 . . 106(3) ? N21 C22 H22A . . 109.7 ? C23 C22 H22A . . 109.7 ? N21 C22 H22B . . 109.7 ? C23 C22 H22B . . 109.7 ? H22A C22 H22B . . 108.2 ? C22 C23 H23A . . 109.0 ? C24 C23 H23A . . 109.0 ? C22 C23 H23B . . 109.0 ? C24 C23 H23B . . 109.0 ? H23A C23 H23B . . 107.8 ? C25 C24 H24 . . 107.9 ? C23 C24 H24 . . 107.9 ? C27 C24 H24 . . 107.9 ? C26 C25 H25A . . 109.1 ? C24 C25 H25A . . 109.1 ? C26 C25 H25B . . 109.1 ? C24 C25 H25B . . 109.1 ? H25A C25 H25B . . 107.8 ? N21 C26 H26A . . 109.5 ? C25 C26 H26A . . 109.5 ? N21 C26 H26B . . 109.5 ? C25 C26 H26B . . 109.5 ? H26A C26 H26B . . 108.1 ? C24 C27 H27A . . 109.5 ? C24 C27 H27B . . 109.5 ? H27A C27 H27B . . 109.5 ? C24 C27 H27C . . 109.5 ? H27A C27 H27C . . 109.5 ? H27B C27 H27C . . 109.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Au1 N11 . 2.051(3) y Au1 N21 . 2.052(3) y N11 C12 . 1.487(5) ? N11 C16 . 1.499(5) ? C12 C13 . 1.513(5) ? C13 C14 . 1.536(5) ? C14 C17 . 1.526(5) ? C14 C15 . 1.532(5) ? C15 C16 . 1.517(5) ? N21 C26 . 1.488(4) ? N21 C22 . 1.490(5) ? C22 C23 . 1.524(5) ? C23 C24 . 1.531(5) ? C24 C25 . 1.524(5) ? C24 C27 . 1.534(5) ? C25 C26 . 1.517(5) ? N11 H01 . 0.90(3) ? C12 H12A . 0.9900 ? C12 H12B . 0.9900 ? C13 H13A . 0.9900 ? C13 H13B . 0.9900 ? C14 H14 . 1.0000 ? C15 H15A . 0.9900 ? C15 H15B . 0.9900 ? C16 H16A . 0.9900 ? C16 H16B . 0.9900 ? C17 H17A . 0.9800 ? C17 H17B . 0.9800 ? C17 H17C . 0.9800 ? N21 H02 . 0.92(3) ? C22 H22A . 0.9900 ? C22 H22B . 0.9900 ? C23 H23A . 0.9900 ? C23 H23B . 0.9900 ? C24 H24 . 1.0000 ? C25 H25A . 0.9900 ? C25 H25B . 0.9900 ? C26 H26A . 0.9900 ? C26 H26B . 0.9900 ? C27 H27A . 0.9800 ? C27 H27B . 0.9800 ? C27 H27C . 0.9800 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag N21 H02 Cl1 . 0.92(3) 2.23(3) 3.144(3) 171(3) yes N11 H01 Cl1 3_566 0.90(3) 2.25(3) 3.140(3) 170(4) yes C16 H16A Cl1 3_666 0.99 2.85 3.623(4) 135.5 yes C22 H22B Au1 3_666 0.99 2.80 3.724(4) 154.9 yes C23 H23A Au1 1_655 0.99 2.85 3.685(4) 142.9 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C16 N11 C12 C13 . . . . 60.1(4) ? Au1 N11 C12 C13 . . . . -67.1(3) y N11 C12 C13 C14 . . . . -56.3(4) ? C12 C13 C14 C17 . . . . 175.6(3) y C12 C13 C14 C15 . . . . 51.1(4) ? C17 C14 C15 C16 . . . . -176.5(3) y C13 C14 C15 C16 . . . . -52.0(4) ? C12 N11 C16 C15 . . . . -60.6(4) ? Au1 N11 C16 C15 . . . . 67.2(3) y C14 C15 C16 N11 . . . . 57.6(4) ? C26 N21 C22 C23 . . . . 61.4(4) ? Au1 N21 C22 C23 . . . . -65.0(3) y N21 C22 C23 C24 . . . . -56.1(4) ? C22 C23 C24 C25 . . . . 49.5(4) ? C22 C23 C24 C27 . . . . 173.6(3) y C23 C24 C25 C26 . . . . -49.2(4) ? C27 C24 C25 C26 . . . . -173.4(3) y C22 N21 C26 C25 . . . . -61.6(4) ? Au1 N21 C26 C25 . . . . 64.9(3) y C24 C25 C26 N21 . . . . 56.0(4) ? _cod_database_fobs_code 2023012