#------------------------------------------------------------------------------
#$Date: 2024-03-05 21:43:35 +0100 (Tue, 05 Mar 2024) $
#$Revision: 290334 $
#$URL: svn://www.crystallography.net/cod/cif/2/02/30/2023006.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2023006
loop_
_publ_author_name
'Akkache, Hibet Errahmane Meroua'
'Hamdouni, Noudjoud'
'Boudjada, Ali'
'Medjroubi, Mohamed Larbi'
'Mili, Assia'
'Jeannin, Olivier'
_publ_section_title
;
Crystal structure, Hirshfeld surface analysis and energy frameworks of
1-[(E)-2-(2-fluoro-phen-yl)diazan-1-yl-idene]naphthalen-2(1H)-one.
;
_journal_coeditor_code EE2002
_journal_issue 'Pt 2'
_journal_name_full
'Acta crystallographica. Section E, Crystallographic communications'
_journal_page_first 137
_journal_page_last 142
_journal_paper_doi 10.1107/S2056989024000227
_journal_volume 80
_journal_year 2024
_chemical_absolute_configuration unk
_chemical_compound_source organic
_chemical_formula_iupac 'C16 H11 F N2 O'
_chemical_formula_moiety 'C16 H11 F N2 O'
_chemical_formula_sum 'C16 H11 F N2 O'
_chemical_formula_weight 266.27
_chemical_name_systematic
;
1-[(E)-2-(2-Fluorophenyl)diazan-1-ylidene]naphthalen-2(1H)-one
;
_space_group_IT_number 29
_space_group_name_Hall 'P 2c -2ac'
_space_group_name_H-M_alt 'P c a 21'
_symmetry_cell_setting orthorhombic
_symmetry_space_group_name_Hall 'P 2c -2ac'
_symmetry_space_group_name_H-M 'P c a 21'
_atom_sites_solution_hydrogens geom
_atom_sites_solution_primary dual
_atom_sites_solution_secondary dual
_audit_creation_method SHELXL-2018/3
_cell_angle_alpha 90
_cell_angle_beta 90
_cell_angle_gamma 90
_cell_formula_units_Z 4
_cell_length_a 23.612(3)
_cell_length_b 7.2392(8)
_cell_length_c 7.2122(7)
_cell_measurement_reflns_used 9942
_cell_measurement_temperature 150(2)
_cell_measurement_theta_max 27.48
_cell_measurement_theta_min 2.94
_cell_volume 1232.8(2)
_computing_cell_refinement
;
APEX3 (Bruker, 2015)
;
_computing_data_collection
;
APEX3 (Bruker, 2015)
;
_computing_data_reduction
;
SAINT (Bruker, 2015)
;
_computing_molecular_graphics
;
ORTEP-3 for Windows (Farrugia, 2012),
Mercury (Macrae et al., 2020), OLEX2 (Dolomanov et al.,
2009)
;
_computing_publication_material
;
WinGX publication routines (Farrugia, 2012)
;
_computing_structure_refinement
;
SHELXL2018/3 (Sheldrick, 2015b)
;
_computing_structure_solution
;
SHELXT2018/2 (Sheldrick, 2015a)
;
_diffrn_ambient_temperature 150(2)
_diffrn_detector 'CCD plate'
_diffrn_detector_area_resol_mean 7.39
_diffrn_measured_fraction_theta_full 0.99
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measurement_device 'D8 VENTURE Bruker AXS'
_diffrn_measurement_device_type 'Bruker D8 VENTURE'
_diffrn_measurement_method 'CCD rotation images, thick slices'
_diffrn_radiation_monochromator 'multilayer monochromator'
_diffrn_radiation_probe x-ray
_diffrn_radiation_type MoK\a
_diffrn_radiation_wavelength 0.71073
_diffrn_reflns_av_R_equivalents 0.0209
_diffrn_reflns_av_unetI/netI 0.0496
_diffrn_reflns_limit_h_max 30
_diffrn_reflns_limit_h_min 0
_diffrn_reflns_limit_k_max 9
_diffrn_reflns_limit_k_min -9
_diffrn_reflns_limit_l_max 9
_diffrn_reflns_limit_l_min -9
_diffrn_reflns_number 5289
_diffrn_reflns_reduction_process
;
Scaled and merged with Sortav
R.H. Blessing, (1987) Cryst. Rev. 1, 3-58
R.H. Blessing, (1989) J. Appl. Cryst. 22, 396-397
;
_diffrn_reflns_theta_full 25.242
_diffrn_reflns_theta_max 27.493
_diffrn_reflns_theta_min 2.943
_diffrn_source 'Enraf--Nonius FR590'
_diffrn_standards_decay_% 0
_diffrn_standards_interval_time 0
_diffrn_standards_number 1
_exptl_absorpt_coefficient_mu 0.102
_exptl_absorpt_correction_type none
_exptl_crystal_colour orange-red
_exptl_crystal_density_diffrn 1.435
_exptl_crystal_density_method 'not measured'
_exptl_crystal_description prism
_exptl_crystal_F_000 552
_exptl_crystal_size_max 0.18
_exptl_crystal_size_mid 0.16
_exptl_crystal_size_min 0.06
_refine_diff_density_max 0.322
_refine_diff_density_min -0.23
_refine_ls_abs_structure_details
;
Flack x determined using 1169 quotients
[(I^+^)-(I^-^)]/[(I^+^)+(I^-^)]
(Parsons et al., 2013)
;
_refine_ls_abs_structure_Flack 0.0(3)
_refine_ls_extinction_method none
_refine_ls_goodness_of_fit_ref 1.081
_refine_ls_hydrogen_treatment constr
_refine_ls_matrix_type full
_refine_ls_number_constraints 0
_refine_ls_number_parameters 181
_refine_ls_number_reflns 2803
_refine_ls_number_restraints 1
_refine_ls_restrained_S_all 1.08
_refine_ls_R_factor_all 0.0458
_refine_ls_R_factor_gt 0.0442
_refine_ls_shift/su_max 0
_refine_ls_shift/su_mean 0
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0633P)^2^+0.1870P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.1083
_refine_ls_wR_factor_ref 0.1094
_reflns_number_gt 2700
_reflns_number_total 2803
_reflns_threshold_expression 'I > 2\s(I)'
_cod_data_source_file ee2002sup1.cif
_cod_data_source_block I
_cod_depositor_comments 'Adding full bibliography for 2023006.cif.'
_cod_database_code 2023006
_cod_database_fobs_code 2023006
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_hkl_file
;
1 2 -9 7.44 3.06
2 2 -9 0.49 1.30
3 2 -9 13.35 7.09
4 2 -9 17.84 2.59
5 2 -9 2.90 1.83
1 1 -9 17.34 4.77
2 1 -9 30.38 5.87
3 1 -9 3.43 3.29
4 1 -9 5.14 3.30
5 1 -9 1.17 3.31
6 1 -9 1.56 3.33
1 0 -9 4.04 3.12
2 0 -9 63.40 7.92
3 0 -9 5.21 3.27
4 0 -9 53.30 7.71
5 0 -9 4.69 3.31
6 0 -9 0.48 3.10
7 0 -9 4.39 3.44
8 0 -9 96.95 9.72
0 -1 -9 4.27 3.17
1 -1 -9 17.43 4.29
2 -1 -9 35.42 5.96
3 -1 -9 1.59 3.07
4 -1 -9 3.75 3.12
5 -1 -9 11.08 3.53
6 -1 -9 7.25 3.66
7 -1 -9 13.33 4.14
1 4 -8 17.41 6.55
2 4 -8 11.86 4.30
3 4 -8 21.78 4.78
4 4 -8 10.26 4.25
5 4 -8 4.92 1.47
6 4 -8 7.47 1.79
7 4 -8 4.19 1.41
8 4 -8 8.54 1.86
9 4 -8 13.20 2.24
1 3 -8 231.76 11.89
2 3 -8 71.29 4.80
3 3 -8 41.63 8.62
4 3 -8 35.31 3.16
5 3 -8 46.33 3.10
6 3 -8 49.52 3.88
7 3 -8 9.55 1.48
8 3 -8 4.50 1.36
9 3 -8 16.28 2.41
10 3 -8 2.70 2.28
11 3 -8 2.51 2.58
12 3 -8 32.63 3.73
1 2 -8 83.03 4.19
2 2 -8 42.38 3.75
3 2 -8 75.73 3.94
4 2 -8 4.33 1.08
5 2 -8 19.60 3.65
6 2 -8 53.38 3.05
7 2 -8 5.73 1.37
8 2 -8 13.24 1.64
9 2 -8 4.82 2.36
10 2 -8 64.56 6.66
11 2 -8 3.27 1.62
12 2 -8 18.94 2.51
13 2 -8 21.74 4.68
14 2 -8 56.67 8.16
1 1 -8 18.17 1.71
2 1 -8 12.31 1.59
3 1 -8 22.59 2.01
4 1 -8 32.85 2.27
5 1 -8 2.83 1.12
6 1 -8 10.43 2.02
7 1 -8 17.60 4.45
8 1 -8 22.57 5.34
9 1 -8 23.40 3.76
10 1 -8 31.94 3.28
11 1 -8 45.92 4.08
12 1 -8 53.44 4.37
13 1 -8 28.48 9.83
14 1 -8 27.05 5.56
15 1 -8 60.86 12.42
1 0 -8 0.67 0.99
2 0 -8 41.78 7.12
3 0 -8 4.98 4.22
4 0 -8 73.50 5.02
5 0 -8 0.20 1.35
6 0 -8 51.25 7.13
7 0 -8 3.41 2.73
8 0 -8 88.69 9.29
9 0 -8 4.45 3.23
10 0 -8 10.01 3.59
11 0 -8 4.47 2.91
12 0 -8 61.22 7.69
13 0 -8 8.62 3.52
14 0 -8 51.96 7.31
15 0 -8 -1.07 2.90
0 -1 -8 26.11 2.79
1 -1 -8 17.50 2.22
2 -1 -8 12.86 1.95
3 -1 -8 20.56 2.45
4 -1 -8 30.64 3.02
5 -1 -8 4.71 2.59
6 -1 -8 6.85 1.82
7 -1 -8 16.71 3.82
8 -1 -8 20.34 4.44
9 -1 -8 22.73 4.74
10 -1 -8 22.91 4.89
11 -1 -8 36.04 6.13
12 -1 -8 43.09 6.33
13 -1 -8 19.04 4.95
14 -1 -8 23.68 5.14
15 -1 -8 49.11 7.80
0 -2 -8 205.24 12.28
1 -2 -8 80.35 8.02
2 -2 -8 41.31 3.52
3 -2 -8 77.47 6.87
4 -2 -8 5.56 1.62
5 -2 -8 22.77 4.94
6 -2 -8 54.20 6.05
7 -2 -8 8.72 3.11
8 -2 -8 14.46 3.73
9 -2 -8 8.48 3.08
10 -2 -8 71.93 8.06
11 -2 -8 3.89 3.29
12 -2 -8 24.61 4.99
13 -2 -8 21.10 4.66
14 -2 -8 52.91 7.31
0 -3 -8 291.97 23.42
1 -3 -8 231.29 18.45
2 -3 -8 77.28 7.22
3 -3 -8 51.67 5.09
4 -3 -8 38.22 4.43
5 -3 -8 51.37 5.62
0 -4 -8 133.30 11.34
2 -4 -8 6.77 2.45
3 -4 -8 18.77 3.35
4 -4 -8 10.28 2.42
5 -4 -8 1.79 1.75
1 6 -7 7.76 1.95
2 6 -7 17.38 2.74
3 6 -7 44.44 4.24
4 6 -7 26.30 7.88
5 6 -7 10.30 2.98
1 5 -7 52.54 4.49
2 5 -7 39.27 3.63
3 5 -7 29.33 2.75
4 5 -7 8.19 1.54
5 5 -7 5.38 1.39
6 5 -7 28.99 2.70
7 5 -7 11.87 2.58
8 5 -7 41.55 4.44
9 5 -7 18.88 2.60
10 5 -7 10.56 1.80
11 5 -7 25.20 3.95
12 5 -7 11.30 1.85
1 4 -7 64.23 3.69
2 4 -7 18.21 1.81
3 4 -7 30.72 2.70
4 4 -7 54.67 3.09
5 4 -7 92.12 4.93
6 4 -7 100.83 6.72
7 4 -7 18.05 1.97
8 4 -7 40.67 2.95
9 4 -7 16.01 2.40
10 4 -7 18.19 2.09
11 4 -7 13.04 2.09
12 4 -7 13.62 2.33
13 4 -7 3.04 1.40
14 4 -7 1.16 2.41
15 4 -7 4.94 1.75
1 3 -7 2.64 0.76
2 3 -7 29.65 3.24
3 3 -7 21.51 1.57
4 3 -7 63.53 3.12
5 3 -7 62.40 3.09
6 3 -7 42.82 2.37
7 3 -7 22.84 1.91
8 3 -7 21.89 1.94
9 3 -7 4.72 1.24
10 3 -7 7.35 2.02
11 3 -7 50.78 3.15
12 3 -7 5.24 1.21
13 3 -7 16.73 2.61
14 3 -7 7.74 2.34
15 3 -7 4.36 1.66
16 3 -7 16.44 1.94
17 3 -7 9.76 1.59
1 2 -7 19.70 1.40
2 2 -7 42.58 2.51
3 2 -7 10.94 1.52
4 2 -7 4.20 0.85
5 2 -7 24.75 1.56
6 2 -7 9.58 0.98
7 2 -7 10.03 1.24
8 2 -7 13.32 1.55
9 2 -7 3.94 1.00
10 2 -7 51.52 2.87
11 2 -7 7.26 1.18
12 2 -7 10.18 1.58
13 2 -7 25.53 2.14
14 2 -7 86.46 4.62
15 2 -7 28.32 2.19
16 2 -7 18.76 1.83
17 2 -7 30.45 2.74
18 2 -7 20.79 2.51
19 2 -7 1.36 1.55
1 1 -7 21.38 1.81
2 1 -7 65.23 4.27
3 1 -7 87.12 5.18
4 1 -7 35.69 2.08
5 1 -7 70.93 4.07
6 1 -7 79.43 3.65
7 1 -7 27.18 1.77
8 1 -7 0.89 0.52
9 1 -7 15.33 1.38
10 1 -7 20.72 1.57
11 1 -7 19.60 2.48
12 1 -7 37.08 2.80
13 1 -7 24.99 2.84
14 1 -7 13.11 1.78
15 1 -7 6.77 1.98
16 1 -7 6.24 1.43
17 1 -7 70.23 5.36
18 1 -7 34.86 9.39
20 1 -7 43.38 5.34
1 0 -7 -0.71 1.38
2 0 -7 23.36 2.32
3 0 -7 -0.17 1.28
4 0 -7 64.31 5.21
5 0 -7 4.73 1.65
6 0 -7 75.64 4.62
8 0 -7 171.14 8.47
9 0 -7 3.78 1.49
10 0 -7 47.41 2.89
11 0 -7 3.03 0.73
12 0 -7 74.58 3.60
13 0 -7 5.15 0.91
14 0 -7 90.54 4.38
15 0 -7 7.28 1.40
16 0 -7 124.67 8.06
17 0 -7 2.27 1.46
18 0 -7 69.33 6.48
19 0 -7 4.72 1.90
20 0 -7 91.22 8.79
0 -1 -7 0.78 0.84
1 -1 -7 18.81 1.70
2 -1 -7 62.11 4.07
3 -1 -7 84.52 10.19
4 -1 -7 36.41 2.93
5 -1 -7 71.46 5.56
6 -1 -7 76.24 3.99
7 -1 -7 27.52 2.97
8 -1 -7 1.98 0.90
9 -1 -7 18.57 2.65
10 -1 -7 19.66 1.67
11 -1 -7 16.72 2.19
12 -1 -7 38.18 3.26
13 -1 -7 36.55 5.22
14 -1 -7 13.28 3.65
15 -1 -7 7.86 2.97
16 -1 -7 6.64 1.69
17 -1 -7 67.05 5.77
18 -1 -7 29.62 3.54
19 -1 -7 31.43 3.68
0 -2 -7 2.02 0.97
1 -2 -7 23.68 1.66
2 -2 -7 44.55 3.21
3 -2 -7 9.76 1.49
4 -2 -7 5.54 1.76
5 -2 -7 25.32 3.98
6 -2 -7 10.53 1.67
7 -2 -7 9.69 1.54
8 -2 -7 14.54 1.88
9 -2 -7 3.96 1.21
10 -2 -7 52.56 4.76
11 -2 -7 8.98 2.10
12 -2 -7 10.78 3.08
13 -2 -7 29.15 4.63
14 -2 -7 91.86 9.06
15 -2 -7 32.21 4.96
18 -2 -7 20.52 2.41
19 -2 -7 2.74 1.25
0 -3 -7 -1.08 0.93
1 -3 -7 2.32 0.73
2 -3 -7 28.43 2.57
3 -3 -7 21.72 3.73
4 -3 -7 68.53 9.35
5 -3 -7 67.87 4.44
6 -3 -7 43.62 3.35
7 -3 -7 24.17 6.72
8 -3 -7 20.91 3.38
9 -3 -7 4.30 1.46
10 -3 -7 4.71 1.37
11 -3 -7 50.84 3.96
12 -3 -7 5.18 2.97
13 -3 -7 16.79 3.59
14 -3 -7 6.28 2.62
15 -3 -7 4.35 2.51
16 -3 -7 16.45 3.81
0 -4 -7 5.29 1.79
1 -4 -7 56.02 6.00
2 -4 -7 18.11 2.96
3 -4 -7 31.98 3.93
4 -4 -7 61.82 5.78
5 -4 -7 95.65 8.27
6 -4 -7 108.50 9.21
7 -4 -7 18.88 3.65
9 -4 -7 18.21 3.27
10 -4 -7 20.99 3.17
11 -4 -7 9.90 2.90
0 -5 -7 8.27 2.37
1 -5 -7 54.84 5.60
2 -5 -7 33.68 4.40
3 -5 -7 23.80 3.76
4 -5 -7 6.07 2.22
6 -5 -7 23.47 3.69
7 -5 -7 13.39 2.79
8 -5 -7 45.51 5.30
9 -5 -7 17.73 3.01
10 -5 -7 8.60 2.48
0 -6 -7 1.29 1.81
1 -6 -7 6.74 2.49
2 -6 -7 23.54 3.79
3 -6 -7 34.42 4.63
4 -6 -7 28.71 3.83
5 -6 -7 6.33 2.45
1 7 -6 8.40 2.43
2 7 -6 19.46 5.60
3 7 -6 4.05 2.39
4 7 -6 13.52 3.98
5 7 -6 17.68 3.04
1 6 -6 37.56 3.75
2 6 -6 9.74 1.34
3 6 -6 3.46 1.03
4 6 -6 48.16 2.72
5 6 -6 17.44 2.06
6 6 -6 12.73 1.62
7 6 -6 17.73 1.93
8 6 -6 15.91 2.23
9 6 -6 11.30 2.27
10 6 -6 8.88 3.39
11 6 -6 16.18 3.02
12 6 -6 81.35 5.69
13 6 -6 50.75 5.34
1 5 -6 53.68 3.08
2 5 -6 28.31 2.65
3 5 -6 51.95 2.57
4 5 -6 32.69 1.96
5 5 -6 6.86 1.25
6 5 -6 11.16 1.21
7 5 -6 25.85 1.96
8 5 -6 89.16 6.78
9 5 -6 34.41 2.31
10 5 -6 4.75 1.17
11 5 -6 1.65 1.19
12 5 -6 3.43 1.31
13 5 -6 6.85 1.51
14 5 -6 1.88 1.71
15 5 -6 11.01 2.02
16 5 -6 1.77 1.74
17 5 -6 5.38 3.94
1 4 -6 4.03 0.76
2 4 -6 3.26 0.72
3 4 -6 25.90 1.98
4 4 -6 118.88 5.42
5 4 -6 118.16 4.79
6 4 -6 12.47 1.23
7 4 -6 65.16 3.41
8 4 -6 8.55 1.09
9 4 -6 14.36 1.23
10 4 -6 0.23 0.80
11 4 -6 7.97 1.15
12 4 -6 34.99 3.04
13 4 -6 7.64 1.46
14 4 -6 30.28 2.51
15 4 -6 13.53 1.78
16 4 -6 14.25 1.82
17 4 -6 16.99 5.42
18 4 -6 6.10 1.50
19 4 -6 51.79 3.93
1 3 -6 88.08 3.64
2 3 -6 40.05 1.84
3 3 -6 65.30 3.35
4 3 -6 56.34 2.71
5 3 -6 14.15 1.22
6 3 -6 45.48 2.32
7 3 -6 20.72 1.50
8 3 -6 1.01 0.62
9 3 -6 24.50 1.90
10 3 -6 88.61 4.49
11 3 -6 8.00 1.22
12 3 -6 32.37 2.35
13 3 -6 13.15 1.76
14 3 -6 43.77 2.77
15 3 -6 61.04 4.46
16 3 -6 71.40 4.60
17 3 -6 84.91 5.17
18 3 -6 89.50 7.72
19 3 -6 47.76 5.78
20 3 -6 14.24 1.91
21 3 -6 22.97 2.50
1 2 -6 497.41 21.00
2 2 -6 416.12 20.68
3 2 -6 48.64 6.89
4 2 -6 38.71 2.75
5 2 -6 33.21 2.63
6 2 -6 20.64 1.96
7 2 -6 17.82 1.65
8 2 -6 48.13 2.59
9 2 -6 9.97 1.14
10 2 -6 58.01 3.74
11 2 -6 19.79 1.58
12 2 -6 73.19 3.68
13 2 -6 48.68 3.92
14 2 -6 94.31 5.30
15 2 -6 73.75 4.52
16 2 -6 27.51 2.68
17 2 -6 7.10 2.15
18 2 -6 10.53 1.53
19 2 -6 26.54 2.28
20 2 -6 3.60 1.20
21 2 -6 3.72 5.26
22 2 -6 12.55 2.82
1 1 -6 62.14 2.88
2 1 -6 63.35 2.97
3 1 -6 63.05 2.90
4 1 -6 233.94 9.34
5 1 -6 248.96 10.11
6 1 -6 113.67 5.88
7 1 -6 6.64 0.89
8 1 -6 82.39 3.53
9 1 -6 52.82 3.25
10 1 -6 21.89 2.52
11 1 -6 48.11 2.95
12 1 -6 1.92 0.72
13 1 -6 42.25 3.13
14 1 -6 51.95 2.94
15 1 -6 93.24 7.20
16 1 -6 41.00 3.12
17 1 -6 43.08 3.25
18 1 -6 33.50 3.23
19 1 -6 41.08 3.52
20 1 -6 32.84 3.05
21 1 -6 16.74 2.35
22 1 -6 8.21 1.83
23 1 -6 9.64 1.91
1 0 -6 1.10 1.33
2 0 -6 32.96 2.88
3 0 -6 -0.45 0.96
4 0 -6 35.49 2.01
5 0 -6 0.24 0.44
6 0 -6 149.59 6.03
7 0 -6 3.23 1.80
8 0 -6 89.21 3.84
9 0 -6 0.08 0.57
10 0 -6 43.02 3.69
11 0 -6 2.32 0.82
12 0 -6 125.12 6.44
13 0 -6 3.20 0.67
14 0 -6 64.65 3.96
15 0 -6 0.69 0.60
16 0 -6 70.42 5.01
17 0 -6 7.24 1.14
18 0 -6 291.89 28.93
19 0 -6 4.67 1.28
20 0 -6 140.09 18.59
21 0 -6 2.14 1.29
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5 3 0 59.47 2.16
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9 3 0 586.28 34.41
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5 1 0 75.40 3.09
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14 1 0 34.41 2.51
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6 0 0 4151.37 712.64
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9 0 0 0.71 0.20
10 0 0 2234.41 306.51
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14 0 0 263.16 10.65
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6 8 1 12.30 2.54
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11 8 1 1.10 1.03
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15 8 1 45.17 3.40
1 7 1 20.22 1.48
2 7 1 9.43 1.35
3 7 1 5.85 0.86
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5 7 1 301.47 10.64
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7 7 1 33.45 1.66
8 7 1 65.74 3.19
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11 7 1 7.10 0.93
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13 7 1 8.91 1.36
14 7 1 9.07 1.27
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20 7 1 0.49 2.32
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7 6 1 239.86 8.26
8 6 1 93.85 4.73
9 6 1 98.01 5.18
10 6 1 81.05 3.57
11 6 1 68.47 4.17
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13 6 1 2.27 0.88
14 6 1 26.49 1.76
15 6 1 7.75 1.07
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17 6 1 31.56 2.52
18 6 1 21.25 1.97
19 6 1 13.55 1.68
20 6 1 24.72 2.34
21 6 1 3.51 1.90
22 6 1 6.68 1.84
23 6 1 2.39 1.41
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6 5 1 396.76 14.66
7 5 1 147.23 5.77
8 5 1 85.36 4.46
9 5 1 70.99 4.56
10 5 1 40.28 2.41
11 5 1 188.20 8.12
12 5 1 116.34 6.34
13 5 1 155.03 9.77
14 5 1 689.09 44.94
15 5 1 98.33 6.98
16 5 1 151.68 6.62
17 5 1 65.35 3.63
18 5 1 93.00 3.97
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20 5 1 21.12 1.48
21 5 1 37.15 2.07
22 5 1 52.19 2.94
23 5 1 8.62 1.10
24 5 1 29.91 2.39
25 5 1 28.33 3.29
1 4 1 42.85 1.63
2 4 1 170.04 5.53
3 4 1 213.44 6.92
4 4 1 458.20 14.51
5 4 1 12.69 0.97
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8 4 1 7.27 0.80
9 4 1 11.09 0.85
10 4 1 10.25 1.12
11 4 1 39.42 3.01
12 4 1 106.24 5.42
13 4 1 161.25 9.58
14 4 1 448.92 25.38
15 4 1 309.24 16.99
16 4 1 66.95 4.70
17 4 1 89.80 4.90
18 4 1 16.14 1.26
19 4 1 29.69 1.57
20 4 1 0.72 0.63
21 4 1 3.25 0.79
22 4 1 62.75 2.88
23 4 1 6.30 0.92
24 4 1 0.40 0.66
25 4 1 0.03 0.63
26 4 1 15.73 1.68
27 4 1 38.95 3.27
1 3 1 306.43 9.93
2 3 1 1337.41 43.06
3 3 1 1237.70 42.48
4 3 1 615.52 21.23
5 3 1 30.33 1.30
6 3 1 167.03 8.36
7 3 1 279.15 12.42
8 3 1 607.17 30.84
9 3 1 192.79 10.85
10 3 1 226.21 9.56
11 3 1 59.15 2.46
12 3 1 24.61 2.00
13 3 1 41.07 2.83
14 3 1 51.86 2.80
15 3 1 4.05 0.57
16 3 1 40.96 3.03
17 3 1 4.23 0.64
18 3 1 9.68 0.96
19 3 1 99.79 6.20
20 3 1 136.36 6.63
21 3 1 3.26 0.68
22 3 1 21.61 1.37
23 3 1 16.42 1.22
24 3 1 0.83 0.63
25 3 1 10.35 1.62
26 3 1 1.35 1.23
27 3 1 1.53 0.80
28 3 1 12.01 1.49
1 2 1 182.42 6.59
2 2 1 533.77 17.20
3 2 1 228.36 7.58
4 2 1 39.96 1.76
5 2 1 197.80 10.46
6 2 1 623.11 26.21
7 2 1 105.26 5.92
8 2 1 597.68 36.04
9 2 1 792.55 49.27
10 2 1 724.77 35.35
11 2 1 198.71 10.95
12 2 1 218.34 22.79
13 2 1 116.77 6.78
14 2 1 60.25 2.80
15 2 1 5.43 0.54
16 2 1 64.24 2.73
17 2 1 77.92 3.47
18 2 1 193.85 8.71
19 2 1 17.00 1.15
20 2 1 805.48 36.73
21 2 1 94.77 3.90
22 2 1 162.13 6.86
23 2 1 24.10 1.87
24 2 1 54.69 2.62
25 2 1 1.59 0.78
26 2 1 29.98 2.07
27 2 1 3.03 0.84
28 2 1 6.13 1.03
29 2 1 1.91 1.04
1 1 1 1368.81 92.94
2 1 1 22.05 1.83
3 1 1 233.23 16.21
4 1 1 360.21 17.99
5 1 1 21.17 0.90
6 1 1 309.73 11.35
7 1 1 422.71 22.11
9 1 1 143.68 5.09
10 1 1 541.84 22.43
12 1 1 486.37 19.49
13 1 1 405.37 14.48
14 1 1 328.98 10.66
15 1 1 22.54 1.01
16 1 1 351.55 13.49
17 1 1 29.49 1.38
18 1 1 195.40 7.26
19 1 1 360.24 13.13
20 1 1 338.66 12.72
21 1 1 52.97 2.93
22 1 1 12.22 1.05
23 1 1 111.11 4.63
24 1 1 5.16 0.81
25 1 1 5.30 0.91
26 1 1 5.51 1.22
27 1 1 27.15 1.80
28 1 1 2.86 0.83
29 1 1 0.69 1.39
30 1 1 35.29 2.50
0 0 1 0.07 0.09
1 0 1 0.15 0.06
3 0 1 0.55 0.10
5 0 1 0.87 0.13
6 0 1 470.54 17.03
7 0 1 0.49 0.15
8 0 1 586.54 21.52
9 0 1 0.28 0.20
10 0 1 192.66 6.66
11 0 1 0.11 0.26
12 0 1 717.33 25.76
13 0 1 0.60 0.29
14 0 1 269.12 9.46
15 0 1 0.99 0.31
16 0 1 157.33 5.86
17 0 1 0.15 0.35
18 0 1 30.13 1.45
19 0 1 -0.35 0.95
20 0 1 13.95 1.20
21 0 1 -1.16 1.12
22 0 1 30.66 1.63
23 0 1 -0.50 1.07
24 0 1 45.70 2.26
25 0 1 0.16 0.51
26 0 1 17.74 1.36
27 0 1 0.19 0.56
28 0 1 35.32 2.06
29 0 1 -0.02 1.42
30 0 1 40.43 3.01
0 -1 1 0.08 0.12
1 -1 1 1190.19 95.38
2 -1 1 21.66 0.82
4 -1 1 362.68 11.39
5 -1 1 20.89 0.88
6 -1 1 317.49 11.41
7 -1 1 422.33 18.56
8 -1 1 1110.66 69.50
9 -1 1 138.97 5.95
10 -1 1 507.30 25.57
12 -1 1 450.83 18.77
13 -1 1 375.09 14.51
14 -1 1 293.36 10.77
15 -1 1 19.92 1.04
16 -1 1 336.01 12.37
17 -1 1 24.95 1.31
18 -1 1 188.21 7.18
19 -1 1 332.69 12.77
20 -1 1 324.36 12.56
21 -1 1 51.72 3.01
22 -1 1 11.75 1.56
23 -1 1 108.34 4.59
24 -1 1 4.92 0.73
25 -1 1 5.56 0.90
26 -1 1 5.82 1.21
27 -1 1 28.51 1.77
28 -1 1 3.14 0.75
29 -1 1 0.84 1.03
30 -1 1 32.15 2.33
0 -2 1 -0.08 0.38
1 -2 1 182.45 5.51
2 -2 1 534.10 15.72
3 -2 1 222.97 7.60
4 -2 1 39.43 1.67
5 -2 1 199.78 6.31
6 -2 1 640.79 19.75
7 -2 1 102.52 3.61
8 -2 1 595.03 19.72
9 -2 1 790.21 28.46
10 -2 1 720.14 26.20
11 -2 1 195.81 7.48
12 -2 1 200.83 7.93
13 -2 1 110.07 4.47
14 -2 1 56.44 2.50
15 -2 1 4.57 0.60
16 -2 1 57.41 3.93
17 -2 1 69.31 3.56
18 -2 1 169.59 8.03
19 -2 1 15.33 1.54
20 -2 1 780.17 32.86
21 -2 1 88.10 4.50
22 -2 1 157.18 7.40
23 -2 1 24.76 1.37
24 -2 1 53.09 3.01
25 -2 1 2.10 0.55
26 -2 1 30.33 1.66
27 -2 1 4.04 0.72
28 -2 1 6.81 1.13
29 -2 1 1.61 0.87
0 -3 1 -0.30 0.58
1 -3 1 307.55 9.29
2 -3 1 1321.51 42.94
3 -3 1 1229.50 38.11
4 -3 1 621.33 18.38
5 -3 1 30.06 1.36
6 -3 1 175.67 5.64
7 -3 1 290.69 9.85
8 -3 1 622.00 21.23
9 -3 1 198.58 7.54
10 -3 1 234.41 8.53
11 -3 1 62.28 2.51
12 -3 1 22.94 1.35
13 -3 1 42.29 1.89
14 -3 1 47.01 2.32
15 -3 1 5.64 0.97
16 -3 1 37.12 2.69
17 -3 1 3.94 0.80
18 -3 1 8.66 1.39
19 -3 1 90.42 5.16
20 -3 1 130.77 7.24
21 -3 1 2.38 0.62
22 -3 1 20.09 1.57
23 -3 1 16.58 1.34
24 -3 1 1.73 0.56
25 -3 1 11.77 1.27
26 -3 1 2.71 0.65
27 -3 1 1.93 1.55
28 -3 1 11.85 1.47
0 -4 1 0.13 0.27
1 -4 1 43.63 1.56
2 -4 1 167.88 5.35
3 -4 1 218.11 6.80
4 -4 1 460.45 14.11
5 -4 1 14.27 0.73
6 -4 1 106.20 3.62
7 -4 1 48.66 1.88
8 -4 1 7.07 0.68
9 -4 1 12.04 0.85
10 -4 1 10.17 0.90
11 -4 1 39.95 1.75
12 -4 1 105.19 4.27
13 -4 1 160.90 7.59
14 -4 1 435.45 17.71
15 -4 1 299.29 12.60
16 -4 1 64.27 3.24
17 -4 1 80.14 3.95
18 -4 1 13.22 2.18
19 -4 1 24.32 1.76
20 -4 1 0.76 0.56
21 -4 1 3.30 0.73
22 -4 1 53.38 3.09
23 -4 1 8.22 1.54
24 -4 1 0.86 0.73
25 -4 1 0.99 0.77
26 -4 1 13.03 1.55
27 -4 1 37.80 2.29
0 -5 1 0.09 0.32
1 -5 1 10.07 0.73
2 -5 1 30.87 1.27
3 -5 1 24.49 1.17
4 -5 1 41.37 1.62
5 -5 1 118.33 4.45
6 -5 1 402.62 13.31
7 -5 1 150.11 5.16
8 -5 1 88.30 3.19
9 -5 1 69.38 3.48
10 -5 1 44.43 1.84
11 -5 1 196.86 8.75
12 -5 1 115.95 5.22
13 -5 1 154.64 6.25
14 -5 1 628.80 27.52
15 -5 1 94.55 5.39
16 -5 1 137.60 8.81
17 -5 1 60.25 3.72
18 -5 1 84.57 4.29
19 -5 1 3.38 0.92
20 -5 1 21.93 2.19
21 -5 1 31.22 2.29
22 -5 1 46.68 3.47
23 -5 1 9.37 2.54
24 -5 1 20.12 2.75
25 -5 1 27.60 4.14
0 -6 1 -1.88 1.11
1 -6 1 1.48 0.60
2 -6 1 16.25 1.36
3 -6 1 2.25 0.61
4 -6 1 246.18 8.44
5 -6 1 252.65 9.79
6 -6 1 677.20 23.34
7 -6 1 236.66 8.28
8 -6 1 93.51 5.45
9 -6 1 103.91 3.88
10 -6 1 81.16 3.71
11 -6 1 71.10 3.48
12 -6 1 24.55 1.49
13 -6 1 1.82 0.52
14 -6 1 28.42 1.80
15 -6 1 8.30 1.00
16 -6 1 19.80 1.96
17 -6 1 28.74 2.15
18 -6 1 20.91 2.11
19 -6 1 14.02 1.66
20 -6 1 22.14 3.65
21 -6 1 5.71 1.55
22 -6 1 7.27 2.34
23 -6 1 2.14 1.04
0 -7 1 -0.67 1.28
1 -7 1 17.49 1.26
2 -7 1 9.05 1.02
3 -7 1 5.48 0.75
4 -7 1 40.46 1.88
5 -7 1 302.22 10.74
6 -7 1 190.37 7.30
7 -7 1 33.09 1.90
8 -7 1 66.43 2.98
9 -7 1 37.47 2.33
10 -7 1 0.78 0.54
11 -7 1 7.13 0.93
12 -7 1 89.95 4.63
13 -7 1 11.33 1.40
14 -7 1 9.52 1.38
15 -7 1 19.53 2.97
16 -7 1 22.83 2.35
17 -7 1 11.32 2.40
18 -7 1 20.08 3.74
19 -7 1 -0.52 1.60
20 -7 1 1.20 1.12
0 -8 1 0.75 0.60
1 -8 1 4.67 0.82
2 -8 1 5.83 0.85
3 -8 1 5.96 1.05
4 -8 1 3.82 0.86
5 -8 1 25.49 3.09
6 -8 1 11.15 1.08
7 -8 1 24.61 2.00
8 -8 1 6.40 0.92
9 -8 1 23.98 1.66
10 -8 1 6.85 1.44
11 -8 1 1.24 0.98
12 -8 1 10.62 2.13
13 -8 1 49.64 7.09
14 -8 1 16.48 2.59
15 -8 1 38.96 6.25
0 -9 1 0.46 1.24
1 -9 1 7.28 1.62
2 -9 1 25.22 6.02
3 -9 1 47.37 8.99
4 -9 1 30.51 6.25
5 -9 1 7.36 1.89
6 -9 1 26.47 2.53
7 -9 1 1.90 1.09
8 -9 1 10.44 1.94
1 9 2 -0.34 1.70
2 9 2 21.33 2.67
3 9 2 13.26 4.85
4 9 2 11.39 1.84
5 9 2 2.10 3.08
6 9 2 20.71 2.95
1 8 2 15.70 1.97
2 8 2 8.17 1.16
3 8 2 12.23 1.34
4 8 2 6.45 1.08
5 8 2 32.99 3.25
6 8 2 6.14 2.33
7 8 2 6.66 1.49
8 8 2 2.24 1.32
9 8 2 3.53 1.14
10 8 2 10.97 1.68
11 8 2 4.08 1.61
12 8 2 35.34 5.09
13 8 2 18.32 2.22
14 8 2 21.20 3.88
1 7 2 6.84 0.82
2 7 2 26.76 1.61
3 7 2 1.64 0.60
4 7 2 23.87 1.49
5 7 2 52.58 2.44
6 7 2 114.20 4.90
7 7 2 37.65 2.35
8 7 2 1.00 0.70
9 7 2 18.42 1.68
10 7 2 30.07 1.96
11 7 2 2.74 1.11
12 7 2 1.88 1.43
13 7 2 29.25 2.89
14 7 2 11.76 1.81
15 7 2 6.06 1.34
16 7 2 47.59 5.40
17 7 2 20.72 2.73
18 7 2 5.62 1.96
19 7 2 2.15 1.67
1 6 2 50.72 2.17
2 6 2 33.14 1.58
3 6 2 88.83 3.43
4 6 2 211.36 8.33
5 6 2 52.26 2.30
6 6 2 217.43 9.34
7 6 2 155.18 8.15
8 6 2 84.73 3.56
9 6 2 28.95 1.56
10 6 2 23.46 1.45
11 6 2 9.42 0.97
12 6 2 18.63 1.34
13 6 2 23.80 1.48
14 6 2 66.53 4.20
15 6 2 16.22 1.41
16 6 2 12.82 1.15
17 6 2 25.52 2.12
18 6 2 5.14 0.98
19 6 2 7.23 1.29
20 6 2 4.60 1.04
21 6 2 4.53 1.28
22 6 2 47.45 3.86
1 5 2 52.96 2.09
2 5 2 259.39 9.01
3 5 2 28.75 1.33
4 5 2 205.46 7.16
5 5 2 252.28 12.92
6 5 2 171.82 8.19
7 5 2 125.41 5.52
8 5 2 22.12 1.44
9 5 2 67.99 4.09
10 5 2 83.84 4.37
11 5 2 29.80 2.07
12 5 2 77.57 4.10
13 5 2 149.12 10.11
14 5 2 172.77 9.10
15 5 2 186.23 11.40
16 5 2 17.43 1.23
17 5 2 16.27 1.33
18 5 2 15.52 1.24
19 5 2 48.53 2.70
20 5 2 47.91 2.58
21 5 2 10.90 1.37
22 5 2 2.05 1.38
23 5 2 0.48 0.84
24 5 2 7.16 1.46
25 5 2 21.81 3.06
1 4 2 128.55 4.63
2 4 2 632.12 25.15
3 4 2 266.85 8.91
4 4 2 227.91 9.72
5 4 2 22.76 1.03
6 4 2 48.61 2.32
7 4 2 19.13 1.43
8 4 2 35.72 1.81
9 4 2 113.19 6.77
10 4 2 144.67 7.59
11 4 2 224.39 9.15
12 4 2 77.18 3.94
13 4 2 93.89 4.75
14 4 2 218.77 12.12
15 4 2 401.36 16.82
16 4 2 92.48 4.97
17 4 2 16.06 1.06
18 4 2 85.08 4.06
19 4 2 16.62 1.37
20 4 2 6.48 0.78
21 4 2 13.23 1.17
22 4 2 6.18 1.00
23 4 2 2.58 0.76
24 4 2 3.05 0.90
25 4 2 4.20 1.34
26 4 2 33.01 2.36
1 3 2 564.71 18.90
2 3 2 17.56 0.94
3 3 2 67.42 2.69
4 3 2 358.43 13.10
5 3 2 102.84 5.19
6 3 2 435.52 16.43
7 3 2 219.85 9.62
8 3 2 26.65 1.44
9 3 2 196.39 8.23
10 3 2 37.14 1.92
11 3 2 99.54 6.38
12 3 2 19.82 0.95
13 3 2 202.11 11.89
14 3 2 471.86 25.26
15 3 2 120.79 4.59
16 3 2 27.95 1.89
17 3 2 29.69 1.97
18 3 2 26.88 1.51
19 3 2 52.29 2.71
20 3 2 106.66 4.53
21 3 2 31.24 1.92
22 3 2 55.78 2.88
23 3 2 56.32 2.54
24 3 2 41.32 2.16
25 3 2 -0.43 1.57
26 3 2 3.47 1.21
27 3 2 4.98 1.29
28 3 2 19.57 3.77
1 2 2 396.53 15.23
2 2 2 66.64 2.52
3 2 2 103.05 3.84
4 2 2 264.22 9.45
5 2 2 58.34 2.74
6 2 2 81.66 5.34
7 2 2 993.02 68.50
8 2 2 380.33 19.97
9 2 2 26.36 1.87
10 2 2 47.60 3.04
11 2 2 381.83 15.18
12 2 2 176.64 7.35
13 2 2 34.92 1.62
14 2 2 35.75 2.08
15 2 2 161.07 6.96
16 2 2 69.00 3.46
17 2 2 140.11 8.37
18 2 2 29.52 1.55
19 2 2 267.45 10.33
20 2 2 378.99 15.53
21 2 2 99.75 4.21
22 2 2 7.36 1.08
23 2 2 41.17 2.26
24 2 2 29.96 2.44
25 2 2 12.22 1.21
26 2 2 38.69 2.33
27 2 2 1.18 1.10
28 2 2 34.39 2.43
29 2 2 2.30 1.10
2 1 2 397.05 14.96
3 1 2 247.72 9.06
4 1 2 684.02 39.05
5 1 2 150.84 8.39
6 1 2 440.23 16.46
7 1 2 72.75 3.49
8 1 2 754.67 28.95
9 1 2 14.32 1.02
10 1 2 407.75 13.80
11 1 2 50.74 1.83
12 1 2 244.78 8.69
13 1 2 42.15 2.05
14 1 2 65.52 2.54
15 1 2 131.33 5.14
16 1 2 247.60 9.15
17 1 2 46.97 2.07
18 1 2 113.19 4.41
19 1 2 534.67 20.21
20 1 2 232.20 8.99
21 1 2 7.68 1.37
22 1 2 99.80 4.20
23 1 2 99.70 5.09
24 1 2 15.34 1.24
25 1 2 35.05 1.98
26 1 2 3.18 0.78
27 1 2 7.61 1.13
28 1 2 1.83 0.82
29 1 2 24.26 3.64
1 0 2 6.39 0.56
3 0 2 11.81 1.05
4 0 2 4302.24 294.46
5 0 2 2.01 0.25
6 0 2 35.90 2.14
7 0 2 0.44 0.23
8 0 2 209.88 7.60
9 0 2 0.99 0.23
10 0 2 509.23 17.22
11 0 2 1.82 0.33
12 0 2 985.54 33.78
13 0 2 1.04 0.34
14 0 2 8.08 0.68
15 0 2 0.19 0.31
16 0 2 177.60 6.70
17 0 2 0.36 0.40
18 0 2 136.80 5.80
19 0 2 -0.27 1.12
20 0 2 389.38 15.17
21 0 2 -0.14 1.18
22 0 2 18.08 1.24
23 0 2 -0.40 1.11
24 0 2 13.37 1.32
25 0 2 0.11 0.53
26 0 2 36.71 2.39
27 0 2 0.65 0.61
28 0 2 24.89 1.73
29 0 2 0.86 1.10
1 -1 2 9589.24 889.19
2 -1 2 384.86 12.21
3 -1 2 235.25 7.69
4 -1 2 660.50 35.23
5 -1 2 143.72 5.03
6 -1 2 416.37 17.99
7 -1 2 69.63 2.63
8 -1 2 733.91 31.02
9 -1 2 14.68 0.82
10 -1 2 380.81 14.52
11 -1 2 45.28 2.58
12 -1 2 224.34 8.85
13 -1 2 38.84 1.87
14 -1 2 61.05 2.51
15 -1 2 121.58 4.72
16 -1 2 241.60 9.10
17 -1 2 46.76 2.10
18 -1 2 106.24 4.35
19 -1 2 513.10 19.95
20 -1 2 223.85 9.61
21 -1 2 10.21 1.05
22 -1 2 97.02 4.17
23 -1 2 99.71 5.74
24 -1 2 15.50 1.31
25 -1 2 35.41 2.14
26 -1 2 2.92 0.79
27 -1 2 7.19 0.94
28 -1 2 2.01 0.77
29 -1 2 20.73 1.78
0 -2 2 391.40 13.12
1 -2 2 388.30 11.96
2 -2 2 62.91 2.41
3 -2 2 101.40 3.50
4 -2 2 257.72 8.45
5 -2 2 52.19 1.86
6 -2 2 78.47 3.44
7 -2 2 1004.72 31.66
8 -2 2 412.32 13.97
9 -2 2 24.98 1.31
10 -2 2 47.76 2.05
11 -2 2 373.21 16.90
12 -2 2 159.56 11.25
13 -2 2 33.20 2.79
14 -2 2 34.88 3.00
15 -2 2 143.10 7.04
16 -2 2 65.08 3.09
17 -2 2 131.25 6.33
18 -2 2 31.17 2.61
19 -2 2 251.61 10.02
20 -2 2 355.13 14.13
21 -2 2 97.53 4.38
22 -2 2 5.88 0.72
23 -2 2 40.66 2.79
24 -2 2 30.68 1.64
25 -2 2 12.31 1.74
26 -2 2 37.47 2.28
27 -2 2 1.11 0.61
28 -2 2 34.01 3.39
29 -2 2 2.97 1.19
0 -3 2 12.17 0.65
1 -3 2 558.30 17.32
2 -3 2 17.08 0.99
3 -3 2 64.55 2.28
4 -3 2 349.34 11.09
5 -3 2 101.86 3.44
6 -3 2 454.31 14.53
7 -3 2 230.63 7.38
8 -3 2 25.41 1.11
9 -3 2 193.11 6.65
10 -3 2 36.98 1.57
11 -3 2 100.22 4.56
12 -3 2 18.82 1.11
13 -3 2 193.48 8.94
14 -3 2 428.54 17.50
15 -3 2 105.98 4.80
16 -3 2 30.10 3.11
17 -3 2 28.03 2.62
18 -3 2 27.84 4.34
19 -3 2 47.29 3.35
20 -3 2 100.86 7.45
21 -3 2 27.20 1.75
22 -3 2 49.16 2.81
23 -3 2 54.22 3.47
24 -3 2 43.09 2.44
25 -3 2 1.15 0.68
26 -3 2 4.32 0.78
27 -3 2 6.29 1.04
28 -3 2 22.55 1.95
0 -4 2 24.61 1.19
1 -4 2 126.60 4.09
2 -4 2 613.92 19.75
3 -4 2 261.41 8.55
4 -4 2 229.93 7.55
5 -4 2 22.88 1.21
6 -4 2 46.06 2.02
7 -4 2 19.72 1.04
8 -4 2 38.28 1.57
9 -4 2 118.48 4.31
10 -4 2 149.08 5.37
11 -4 2 236.70 8.69
12 -4 2 74.10 2.98
13 -4 2 93.39 5.51
14 -4 2 202.80 8.74
15 -4 2 371.87 17.40
16 -4 2 80.03 4.12
17 -4 2 17.90 1.57
18 -4 2 71.89 3.78
19 -4 2 11.68 1.32
20 -4 2 5.77 0.88
21 -4 2 11.21 1.35
22 -4 2 8.88 1.31
23 -4 2 3.53 0.97
24 -4 2 3.63 0.84
25 -4 2 4.53 0.86
26 -4 2 33.19 2.27
0 -5 2 135.72 4.68
1 -5 2 51.90 1.95
2 -5 2 262.42 8.43
3 -5 2 28.21 1.24
4 -5 2 203.26 6.91
5 -5 2 251.36 8.48
6 -5 2 174.05 5.97
7 -5 2 128.36 4.81
8 -5 2 23.85 1.26
9 -5 2 66.22 3.15
10 -5 2 83.23 3.47
11 -5 2 28.06 1.67
12 -5 2 75.32 5.70
13 -5 2 132.24 6.42
14 -5 2 180.01 10.50
15 -5 2 190.70 10.71
16 -5 2 19.72 2.19
17 -5 2 15.32 1.43
18 -5 2 18.32 2.27
19 -5 2 42.51 2.71
20 -5 2 42.94 3.31
21 -5 2 10.98 1.87
22 -5 2 1.83 1.06
23 -5 2 1.84 0.86
24 -5 2 9.30 2.87
25 -5 2 19.17 3.20
0 -6 2 21.77 1.51
1 -6 2 49.99 2.12
2 -6 2 30.96 1.53
3 -6 2 87.14 3.17
4 -6 2 217.88 7.71
5 -6 2 54.86 2.25
6 -6 2 222.29 10.20
7 -6 2 143.56 6.11
8 -6 2 83.96 3.39
9 -6 2 31.05 1.99
10 -6 2 21.88 2.17
11 -6 2 9.00 0.97
12 -6 2 17.43 1.97
13 -6 2 27.50 2.64
14 -6 2 61.27 3.86
15 -6 2 18.08 2.11
16 -6 2 12.91 1.36
17 -6 2 27.86 1.93
18 -6 2 5.85 0.95
19 -6 2 7.85 1.73
20 -6 2 4.74 1.22
21 -6 2 4.26 1.31
22 -6 2 40.33 4.25
0 -7 2 143.32 5.36
1 -7 2 5.71 0.80
2 -7 2 28.17 1.63
3 -7 2 0.84 0.59
4 -7 2 24.98 1.56
5 -7 2 56.56 2.32
6 -7 2 115.90 4.44
7 -7 2 40.50 2.14
8 -7 2 0.99 0.54
9 -7 2 16.54 1.67
10 -7 2 30.35 1.80
11 -7 2 2.58 0.76
12 -7 2 1.93 0.84
13 -7 2 31.92 2.13
14 -7 2 11.33 1.61
15 -7 2 8.57 1.11
16 -7 2 45.20 4.32
17 -7 2 22.89 2.78
18 -7 2 6.94 1.36
19 -7 2 3.73 1.37
0 -8 2 9.98 1.11
1 -8 2 15.51 1.27
2 -8 2 7.31 0.91
3 -8 2 12.54 1.49
4 -8 2 7.56 1.03
5 -8 2 35.06 1.92
6 -8 2 6.56 0.90
7 -8 2 10.24 1.09
8 -8 2 2.01 0.69
9 -8 2 1.91 0.74
10 -8 2 11.17 1.32
11 -8 2 2.86 2.65
12 -8 2 31.41 4.08
13 -8 2 12.46 1.82
14 -8 2 27.45 2.78
0 -9 2 13.69 3.23
1 -9 2 0.14 1.38
2 -9 2 23.65 4.92
3 -9 2 14.81 2.35
4 -9 2 12.86 1.78
5 -9 2 2.93 3.01
6 -9 2 22.77 3.17
1 8 3 4.22 1.12
2 8 3 34.97 3.38
3 8 3 31.81 4.84
4 8 3 3.94 2.49
5 8 3 93.81 8.71
6 8 3 26.95 3.61
7 8 3 34.79 4.17
8 8 3 14.38 2.40
9 8 3 1.78 2.05
10 8 3 1.35 1.94
11 8 3 26.23 4.11
12 8 3 11.72 5.84
1 7 3 17.89 1.44
2 7 3 6.99 0.88
3 7 3 27.89 1.71
4 7 3 71.90 3.68
5 7 3 111.11 4.92
6 7 3 76.98 4.25
7 7 3 140.99 7.31
8 7 3 65.94 3.84
9 7 3 20.67 1.88
10 7 3 12.90 1.56
11 7 3 23.89 2.09
12 7 3 3.19 1.34
13 7 3 31.47 2.78
14 7 3 59.64 4.08
15 7 3 1.52 1.14
16 7 3 4.01 1.92
17 7 3 11.54 3.65
1 6 3 15.30 1.32
2 6 3 40.99 2.53
3 6 3 17.99 1.31
4 6 3 51.85 2.92
5 6 3 56.60 2.55
6 6 3 77.34 3.59
7 6 3 108.71 5.81
8 6 3 184.80 9.41
9 6 3 21.17 1.64
10 6 3 92.98 7.10
11 6 3 44.22 2.66
12 6 3 35.77 1.85
13 6 3 170.75 9.18
14 6 3 59.22 3.30
15 6 3 6.69 1.02
16 6 3 22.61 2.00
17 6 3 73.91 6.52
18 6 3 48.52 2.79
19 6 3 21.07 2.07
20 6 3 25.18 3.87
21 6 3 0.82 1.03
1 5 3 2.31 0.45
2 5 3 69.04 3.11
3 5 3 94.50 3.92
4 5 3 104.76 6.91
5 5 3 496.24 22.04
6 5 3 204.41 9.31
7 5 3 22.33 1.91
8 5 3 96.50 3.94
9 5 3 17.10 1.07
10 5 3 55.56 3.43
11 5 3 36.68 2.00
12 5 3 184.82 7.95
13 5 3 166.04 9.31
14 5 3 78.28 4.51
15 5 3 55.53 3.06
16 5 3 29.53 1.66
17 5 3 3.59 0.65
18 5 3 55.67 7.55
19 5 3 4.98 0.91
20 5 3 11.16 1.16
21 5 3 12.60 1.70
22 5 3 1.93 0.82
23 5 3 21.54 1.94
24 5 3 0.55 1.17
1 4 3 304.51 13.07
2 4 3 155.15 6.04
3 4 3 201.13 9.00
4 4 3 59.75 2.82
5 4 3 91.48 3.84
6 4 3 123.52 6.51
7 4 3 14.83 0.89
8 4 3 97.94 4.50
9 4 3 194.75 9.61
10 4 3 5.11 0.52
11 4 3 33.51 1.78
12 4 3 118.06 5.79
13 4 3 89.75 4.81
14 4 3 25.83 1.25
15 4 3 22.59 1.53
16 4 3 134.08 6.35
17 4 3 203.53 10.88
18 4 3 154.55 7.67
19 4 3 5.72 0.74
20 4 3 7.14 0.84
21 4 3 15.42 2.12
22 4 3 18.00 1.94
23 4 3 12.45 1.59
24 4 3 3.95 0.93
25 4 3 40.89 2.70
1 3 3 233.72 10.56
2 3 3 49.56 2.40
3 3 3 61.83 2.88
4 3 3 220.50 8.51
5 3 3 62.04 2.35
6 3 3 83.49 3.33
7 3 3 50.60 2.33
8 3 3 50.53 2.98
9 3 3 137.76 5.50
10 3 3 149.90 5.98
11 3 3 3.08 0.41
12 3 3 56.96 3.32
13 3 3 278.52 15.69
14 3 3 27.13 1.77
15 3 3 92.92 4.25
16 3 3 120.72 6.05
17 3 3 2.66 0.65
18 3 3 156.52 7.87
19 3 3 131.95 6.04
20 3 3 46.86 2.91
21 3 3 88.79 4.13
22 3 3 89.23 4.12
23 3 3 4.00 0.88
24 3 3 17.27 1.43
25 3 3 1.84 0.79
26 3 3 10.10 1.78
27 3 3 36.62 2.48
1 2 3 155.16 5.79
2 2 3 615.46 20.66
3 2 3 325.29 12.63
4 2 3 280.33 10.65
5 2 3 263.38 10.37
6 2 3 189.80 8.57
7 2 3 438.52 36.64
8 2 3 332.53 22.93
9 2 3 54.95 2.85
10 2 3 274.57 9.31
11 2 3 342.69 12.72
12 2 3 48.63 1.98
13 2 3 33.35 1.88
14 2 3 28.25 1.82
15 2 3 28.51 1.56
16 2 3 8.55 0.75
17 2 3 2.71 0.56
18 2 3 106.11 4.93
19 2 3 0.42 0.51
20 2 3 23.30 1.35
21 2 3 26.40 1.92
22 2 3 123.88 5.24
23 2 3 45.37 2.36
24 2 3 69.92 3.33
25 2 3 8.09 1.37
26 2 3 14.22 2.44
27 2 3 2.29 0.85
28 2 3 5.93 1.15
1 1 3 314.39 14.47
2 1 3 104.91 4.28
3 1 3 217.85 14.29
4 1 3 27.04 3.16
5 1 3 388.11 15.83
6 1 3 61.64 2.74
7 1 3 22.57 1.45
8 1 3 482.59 23.22
9 1 3 469.79 17.20
10 1 3 200.09 7.10
11 1 3 8.61 0.64
12 1 3 78.07 2.97
13 1 3 30.75 1.39
14 1 3 94.41 3.71
15 1 3 16.64 0.93
16 1 3 39.53 1.77
17 1 3 112.78 4.45
18 1 3 347.30 13.03
19 1 3 228.08 8.93
20 1 3 29.62 1.73
21 1 3 52.30 3.14
22 1 3 16.45 1.49
23 1 3 22.80 1.51
24 1 3 4.84 1.00
25 1 3 1.83 0.69
26 1 3 9.73 1.33
27 1 3 2.05 1.56
28 1 3 13.10 3.49
0 0 3 0.16 0.23
1 0 3 -0.05 0.50
2 0 3 275.44 10.03
3 0 3 3.01 0.35
4 0 3 1671.68 67.33
5 0 3 2.76 0.42
6 0 3 222.57 7.71
7 0 3 0.45 0.22
8 0 3 10.86 0.69
9 0 3 0.39 0.24
10 0 3 210.72 7.62
11 0 3 4.21 0.67
12 0 3 1680.68 71.75
13 0 3 3.70 0.64
14 0 3 139.67 5.20
15 0 3 0.67 0.36
16 0 3 73.82 3.00
17 0 3 0.96 0.46
18 0 3 490.48 18.77
19 0 3 2.34 0.60
20 0 3 108.12 4.96
21 0 3 0.44 0.54
22 0 3 82.96 3.81
23 0 3 0.44 0.51
24 0 3 92.79 4.16
25 0 3 0.81 0.68
26 0 3 35.11 2.63
27 0 3 0.60 0.79
28 0 3 0.92 1.18
29 0 3 0.19 1.64
0 -1 3 0.19 0.26
1 -1 3 306.62 9.90
2 -1 3 98.84 3.40
3 -1 3 208.23 6.91
4 -1 3 27.45 1.22
5 -1 3 394.78 12.91
6 -1 3 62.23 3.25
7 -1 3 20.43 1.36
8 -1 3 472.04 15.58
9 -1 3 464.83 15.99
10 -1 3 194.85 8.23
11 -1 3 7.54 0.78
12 -1 3 73.53 3.24
13 -1 3 29.07 1.57
14 -1 3 94.47 4.01
15 -1 3 15.81 1.07
16 -1 3 36.13 1.96
17 -1 3 112.95 4.51
18 -1 3 330.36 12.86
19 -1 3 227.97 9.84
20 -1 3 30.16 1.89
21 -1 3 49.78 2.52
22 -1 3 17.05 1.54
23 -1 3 24.68 1.56
24 -1 3 5.19 0.98
25 -1 3 2.08 0.71
26 -1 3 8.81 1.09
27 -1 3 1.45 0.68
28 -1 3 16.12 2.21
0 -2 3 0.41 0.38
1 -2 3 153.16 5.57
2 -2 3 605.45 19.68
3 -2 3 313.35 10.41
4 -2 3 272.66 9.01
5 -2 3 247.66 8.38
6 -2 3 178.01 6.12
7 -2 3 410.23 14.47
8 -2 3 305.31 10.85
9 -2 3 51.80 2.14
10 -2 3 245.24 9.08
11 -2 3 318.70 14.50
12 -2 3 48.44 2.38
13 -2 3 31.64 1.82
14 -2 3 29.69 1.88
15 -2 3 28.18 2.38
16 -2 3 7.64 0.76
17 -2 3 3.37 0.63
18 -2 3 102.08 4.77
19 -2 3 1.29 0.59
20 -2 3 23.11 1.35
21 -2 3 28.37 1.73
22 -2 3 121.24 5.28
23 -2 3 45.46 2.75
24 -2 3 70.58 4.12
25 -2 3 9.11 1.04
26 -2 3 20.66 1.59
27 -2 3 4.05 0.84
28 -2 3 5.76 1.24
0 -3 3 0.80 0.33
1 -3 3 228.57 7.50
2 -3 3 50.57 1.90
3 -3 3 63.01 2.27
4 -3 3 217.29 7.15
5 -3 3 62.53 2.82
6 -3 3 85.00 3.57
7 -3 3 50.30 1.92
8 -3 3 49.75 2.70
9 -3 3 136.99 5.71
10 -3 3 147.45 6.62
11 -3 3 2.86 0.62
12 -3 3 60.72 2.78
13 -3 3 281.71 18.02
14 -3 3 27.54 2.69
15 -3 3 92.19 4.52
16 -3 3 120.77 13.15
17 -3 3 2.52 0.69
18 -3 3 144.29 6.59
19 -3 3 126.61 7.67
20 -3 3 42.85 2.89
21 -3 3 84.89 5.03
22 -3 3 82.59 4.95
23 -3 3 4.52 0.85
24 -3 3 17.42 1.43
25 -3 3 1.90 0.65
26 -3 3 11.29 1.25
27 -3 3 40.35 2.85
0 -4 3 3.36 0.55
1 -4 3 303.99 10.08
2 -4 3 151.56 5.16
3 -4 3 198.72 6.71
4 -4 3 59.38 2.26
5 -4 3 88.84 3.23
6 -4 3 120.16 4.27
7 -4 3 15.01 1.07
8 -4 3 99.01 3.56
9 -4 3 195.83 6.99
10 -4 3 3.67 0.59
11 -4 3 32.90 1.95
12 -4 3 118.75 4.57
13 -4 3 92.08 5.38
14 -4 3 25.97 1.66
15 -4 3 26.58 1.59
16 -4 3 123.11 5.81
17 -4 3 189.30 12.19
18 -4 3 137.54 6.65
19 -4 3 6.80 0.95
20 -4 3 7.02 1.02
21 -4 3 11.90 1.63
22 -4 3 20.41 2.15
23 -4 3 11.13 2.02
24 -4 3 4.35 1.17
25 -4 3 41.09 2.52
0 -5 3 -0.07 1.08
1 -5 3 2.02 0.53
2 -5 3 68.18 2.67
3 -5 3 88.11 3.35
4 -5 3 98.56 3.67
5 -5 3 500.67 16.94
6 -5 3 199.89 7.05
7 -5 3 23.00 1.30
8 -5 3 97.71 3.73
9 -5 3 17.29 1.22
10 -5 3 54.69 2.72
11 -5 3 34.31 2.31
12 -5 3 180.82 8.31
13 -5 3 163.59 8.68
14 -5 3 77.09 3.41
15 -5 3 52.74 3.60
16 -5 3 28.11 1.92
17 -5 3 3.94 0.87
18 -5 3 55.10 3.28
19 -5 3 8.34 1.15
20 -5 3 14.24 1.42
21 -5 3 12.14 1.88
22 -5 3 1.52 0.89
23 -5 3 19.63 4.74
24 -5 3 0.70 0.92
0 -6 3 -1.23 1.15
1 -6 3 16.14 1.21
2 -6 3 40.85 2.34
3 -6 3 18.32 1.30
4 -6 3 51.46 2.15
5 -6 3 53.31 2.56
6 -6 3 77.38 3.42
7 -6 3 114.49 5.47
8 -6 3 192.89 7.36
9 -6 3 23.73 2.33
10 -6 3 100.86 4.02
11 -6 3 42.26 2.29
12 -6 3 37.25 2.07
13 -6 3 169.82 10.31
14 -6 3 58.31 5.58
15 -6 3 8.41 1.65
16 -6 3 22.14 2.64
17 -6 3 66.79 3.97
18 -6 3 41.19 2.98
19 -6 3 19.42 3.02
20 -6 3 23.39 3.57
21 -6 3 2.05 1.25
0 -7 3 -0.11 1.72
1 -7 3 16.80 1.39
2 -7 3 7.03 0.99
3 -7 3 27.85 1.75
4 -7 3 69.63 3.27
5 -7 3 106.10 4.92
6 -7 3 83.12 5.03
7 -7 3 149.05 6.81
8 -7 3 65.41 3.17
9 -7 3 19.83 2.08
10 -7 3 13.84 3.46
11 -7 3 23.31 2.82
12 -7 3 4.52 1.04
13 -7 3 29.96 1.94
14 -7 3 58.03 4.68
15 -7 3 3.31 1.98
16 -7 3 6.39 1.20
17 -7 3 16.59 2.27
0 -8 3 0.21 0.71
1 -8 3 5.22 0.97
2 -8 3 40.06 2.54
3 -8 3 35.34 3.21
4 -8 3 4.61 0.95
5 -8 3 96.60 5.86
6 -8 3 24.47 2.42
7 -8 3 34.74 2.20
8 -8 3 14.25 1.76
9 -8 3 2.72 1.36
10 -8 3 3.04 0.98
11 -8 3 31.18 3.08
12 -8 3 11.34 1.93
1 8 4 4.55 2.18
2 8 4 3.69 2.38
3 8 4 24.01 3.68
4 8 4 34.82 4.66
5 8 4 5.83 3.52
6 8 4 3.21 1.49
7 8 4 13.92 2.88
8 8 4 11.03 3.96
9 8 4 12.13 2.26
1 7 4 5.45 1.38
2 7 4 11.43 1.81
3 7 4 3.85 1.92
4 7 4 81.56 5.61
5 7 4 12.53 5.35
6 7 4 63.21 4.68
7 7 4 51.40 4.01
8 7 4 29.07 2.97
9 7 4 34.50 4.97
10 7 4 3.03 2.65
11 7 4 15.12 2.79
12 7 4 55.60 4.54
13 7 4 20.95 4.18
14 7 4 3.64 1.65
15 7 4 37.31 10.62
1 6 4 5.46 0.87
2 6 4 6.58 0.93
3 6 4 3.32 0.74
4 6 4 71.57 4.27
5 6 4 35.99 2.85
6 6 4 41.71 2.49
7 6 4 5.93 0.98
8 6 4 10.49 0.99
9 6 4 25.76 2.54
10 6 4 61.85 4.42
11 6 4 26.25 1.72
12 6 4 37.87 2.22
13 6 4 33.33 3.24
14 6 4 57.36 4.42
15 6 4 89.31 6.13
16 6 4 10.48 6.66
17 6 4 23.68 2.83
18 6 4 26.88 4.19
1 5 4 12.89 1.07
2 5 4 258.49 12.03
3 5 4 134.29 6.67
4 5 4 159.46 9.68
5 5 4 123.93 16.78
6 5 4 61.46 3.89
7 5 4 4.42 0.77
8 5 4 25.33 1.36
9 5 4 96.57 4.61
10 5 4 118.32 7.76
11 5 4 16.65 1.78
12 5 4 75.42 4.56
13 5 4 68.52 3.12
14 5 4 28.54 1.66
15 5 4 44.12 2.81
16 5 4 17.48 2.18
17 5 4 6.72 0.91
18 5 4 7.43 1.12
19 5 4 17.38 2.03
20 5 4 2.50 2.17
21 5 4 16.32 3.00
22 5 4 6.90 1.76
1 4 4 48.91 2.47
2 4 4 5.44 0.63
3 4 4 36.18 1.91
4 4 4 43.80 2.34
5 4 4 239.56 12.10
6 4 4 56.94 3.35
7 4 4 126.21 6.88
8 4 4 68.53 3.97
9 4 4 41.99 2.32
10 4 4 28.54 1.91
11 4 4 12.41 0.87
12 4 4 33.52 1.79
13 4 4 47.25 2.53
14 4 4 33.71 2.09
15 4 4 44.77 2.18
16 4 4 50.94 2.32
17 4 4 18.70 1.19
18 4 4 31.18 1.86
19 4 4 10.91 1.17
20 4 4 14.37 1.29
21 4 4 28.25 1.92
22 4 4 26.25 1.98
23 4 4 1.17 0.80
24 4 4 2.05 0.95
1 3 4 46.77 2.20
2 3 4 50.07 2.24
3 3 4 31.82 2.29
4 3 4 102.84 4.14
5 3 4 23.58 1.91
6 3 4 55.58 4.08
7 3 4 2.74 0.43
8 3 4 116.15 5.05
9 3 4 15.60 0.85
10 3 4 31.19 2.15
11 3 4 18.24 1.29
12 3 4 253.32 14.05
13 3 4 41.12 1.92
14 3 4 144.39 5.73
15 3 4 327.51 17.57
16 3 4 63.68 3.40
17 3 4 9.32 0.88
18 3 4 120.89 5.32
19 3 4 143.61 6.58
20 3 4 180.03 9.01
21 3 4 61.94 4.69
22 3 4 3.82 0.78
23 3 4 27.84 1.88
24 3 4 5.81 1.06
25 3 4 5.80 1.47
1 2 4 786.93 29.66
2 2 4 617.17 27.64
3 2 4 13.60 1.24
4 2 4 49.10 2.89
5 2 4 395.01 23.62
6 2 4 66.25 4.24
7 2 4 82.95 4.54
8 2 4 138.18 6.28
9 2 4 93.75 4.33
10 2 4 14.45 0.87
11 2 4 89.17 4.77
12 2 4 37.96 1.95
13 2 4 6.54 0.69
14 2 4 84.01 3.61
15 2 4 126.40 6.10
16 2 4 7.48 0.77
17 2 4 47.47 2.38
18 2 4 95.44 4.69
19 2 4 31.34 1.65
20 2 4 7.49 0.94
21 2 4 14.22 1.31
22 2 4 14.76 1.50
23 2 4 11.98 1.97
24 2 4 84.50 4.27
25 2 4 18.84 1.94
26 2 4 19.97 2.52
1 1 4 2577.87 109.29
2 1 4 1603.78 59.03
3 1 4 491.98 30.15
4 1 4 599.46 28.40
5 1 4 184.72 9.19
6 1 4 498.30 34.36
7 1 4 148.50 8.74
8 1 4 88.83 4.48
9 1 4 27.88 1.58
10 1 4 13.80 1.12
11 1 4 36.74 1.72
12 1 4 144.32 5.61
13 1 4 72.52 2.95
14 1 4 30.94 1.84
15 1 4 177.63 6.80
16 1 4 31.75 1.61
17 1 4 10.79 1.08
18 1 4 175.36 6.98
19 1 4 5.54 0.90
20 1 4 38.17 2.05
21 1 4 49.60 2.64
22 1 4 19.87 1.41
23 1 4 7.51 1.09
24 1 4 13.76 1.94
25 1 4 2.57 1.38
26 1 4 2.31 1.01
27 1 4 16.78 1.91
0 0 4 69.78 3.09
1 0 4 0.15 0.34
2 0 4 177.00 6.88
3 0 4 1.68 0.52
4 0 4 458.88 17.16
5 0 4 4.03 0.58
6 0 4 298.51 10.75
7 0 4 1.05 0.27
8 0 4 93.77 3.53
9 0 4 1.14 0.45
10 0 4 75.44 2.84
11 0 4 1.53 0.37
12 0 4 319.29 11.76
13 0 4 1.74 0.42
14 0 4 61.34 2.83
15 0 4 3.44 0.82
16 0 4 317.55 12.17
17 0 4 4.43 0.69
18 0 4 597.45 25.79
19 0 4 3.00 0.77
20 0 4 311.14 12.36
21 0 4 1.65 0.63
22 0 4 96.21 4.23
23 0 4 1.72 0.64
24 0 4 74.89 4.20
25 0 4 1.22 1.21
26 0 4 15.05 1.74
27 0 4 -0.12 2.48
0 -1 4 512.83 17.74
1 -1 4 2531.77 163.04
2 -1 4 1583.96 58.50
3 -1 4 477.86 18.96
4 -1 4 596.55 22.29
5 -1 4 185.73 6.60
6 -1 4 468.82 15.88
7 -1 4 143.09 5.11
8 -1 4 83.14 3.28
9 -1 4 24.87 1.25
10 -1 4 13.36 0.95
11 -1 4 34.79 1.55
12 -1 4 145.25 6.07
13 -1 4 74.10 3.31
14 -1 4 31.54 1.62
15 -1 4 174.55 6.83
16 -1 4 31.26 1.87
17 -1 4 12.88 2.30
18 -1 4 175.90 7.60
19 -1 4 8.09 1.02
20 -1 4 39.05 2.37
21 -1 4 52.05 2.57
22 -1 4 21.20 2.10
23 -1 4 8.45 1.18
24 -1 4 18.15 1.61
25 -1 4 3.06 1.12
26 -1 4 3.30 3.61
27 -1 4 18.56 2.20
0 -2 4 1184.13 39.78
1 -2 4 797.48 26.57
2 -2 4 597.77 21.92
3 -2 4 14.11 0.90
4 -2 4 46.13 1.89
5 -2 4 377.46 12.83
6 -2 4 59.84 2.85
7 -2 4 84.02 3.54
8 -2 4 139.88 5.32
9 -2 4 88.67 3.66
10 -2 4 14.40 0.93
11 -2 4 83.19 3.24
12 -2 4 37.15 1.74
13 -2 4 6.36 0.70
14 -2 4 81.14 3.83
15 -2 4 120.78 5.48
16 -2 4 7.84 1.17
17 -2 4 44.48 2.64
18 -2 4 96.49 4.58
19 -2 4 31.01 2.35
20 -2 4 9.60 1.29
21 -2 4 16.70 1.44
22 -2 4 15.79 2.14
23 -2 4 13.47 1.22
24 -2 4 85.18 5.15
25 -2 4 17.58 1.84
26 -2 4 21.47 2.56
0 -3 4 0.34 0.47
1 -3 4 45.57 1.79
2 -3 4 48.04 1.88
3 -3 4 31.38 1.78
4 -3 4 103.57 3.84
5 -3 4 25.17 1.23
6 -3 4 54.15 2.11
7 -3 4 2.51 0.48
8 -3 4 121.34 5.15
9 -3 4 16.55 1.02
10 -3 4 34.46 1.52
11 -3 4 16.70 1.08
12 -3 4 249.74 11.42
13 -3 4 40.99 3.79
14 -3 4 148.92 6.79
15 -3 4 312.16 13.57
16 -3 4 63.71 3.53
17 -3 4 10.29 1.20
18 -3 4 110.90 5.43
19 -3 4 146.58 8.98
20 -3 4 172.18 8.16
21 -3 4 59.22 3.73
22 -3 4 3.56 0.71
23 -3 4 29.45 2.48
24 -3 4 5.33 1.26
25 -3 4 7.79 1.18
0 -4 4 250.72 8.81
1 -4 4 48.63 1.99
2 -4 4 5.43 0.65
3 -4 4 34.38 1.56
4 -4 4 42.22 1.83
5 -4 4 232.02 7.95
6 -4 4 56.77 2.69
7 -4 4 128.62 4.93
8 -4 4 69.63 2.89
9 -4 4 40.89 1.86
10 -4 4 25.96 1.42
11 -4 4 11.41 1.17
12 -4 4 32.26 1.68
13 -4 4 47.16 2.82
14 -4 4 36.96 2.44
15 -4 4 44.70 2.57
16 -4 4 55.98 4.07
17 -4 4 19.82 2.61
18 -4 4 31.35 2.03
19 -4 4 12.23 1.50
20 -4 4 15.99 2.11
21 -4 4 27.47 2.08
22 -4 4 29.42 2.08
23 -4 4 2.64 0.90
24 -4 4 2.73 1.14
0 -5 4 186.79 6.95
1 -5 4 11.96 1.04
2 -5 4 265.63 9.29
3 -5 4 141.69 5.14
4 -5 4 164.60 5.89
5 -5 4 132.38 4.87
6 -5 4 57.27 2.81
7 -5 4 3.79 0.74
8 -5 4 26.98 1.90
9 -5 4 86.43 3.50
10 -5 4 121.66 4.91
11 -5 4 14.83 1.48
12 -5 4 78.37 3.41
13 -5 4 70.05 4.03
14 -5 4 29.58 1.77
15 -5 4 46.92 2.67
16 -5 4 18.66 2.05
17 -5 4 7.30 1.09
18 -5 4 11.59 1.69
19 -5 4 15.23 1.42
20 -5 4 1.53 0.93
21 -5 4 17.40 2.13
22 -5 4 10.59 1.23
0 -6 4 44.28 2.60
1 -6 4 3.82 1.05
2 -6 4 6.56 1.11
3 -6 4 3.39 0.90
4 -6 4 70.33 3.60
5 -6 4 34.64 2.32
6 -6 4 41.51 2.68
7 -6 4 5.75 0.85
8 -6 4 9.64 1.17
9 -6 4 26.35 2.56
10 -6 4 61.00 3.34
11 -6 4 27.45 2.38
12 -6 4 38.93 2.68
13 -6 4 36.99 2.37
14 -6 4 63.15 4.27
15 -6 4 82.16 4.87
16 -6 4 7.91 1.19
17 -6 4 21.19 4.70
18 -6 4 24.30 3.35
19 -6 4 29.58 4.67
0 -7 4 36.46 2.15
1 -7 4 2.15 0.81
2 -7 4 13.07 1.46
3 -7 4 4.33 1.26
4 -7 4 85.26 4.20
5 -7 4 14.99 1.79
6 -7 4 66.37 3.54
7 -7 4 51.98 3.09
8 -7 4 33.03 3.23
9 -7 4 37.11 2.48
10 -7 4 3.83 0.84
11 -7 4 13.94 2.18
12 -7 4 54.21 4.31
13 -7 4 20.92 4.52
14 -7 4 6.62 1.78
15 -7 4 34.51 4.53
0 -8 4 37.83 4.09
1 -8 4 6.42 1.48
2 -8 4 4.22 1.19
3 -8 4 24.76 3.53
4 -8 4 33.31 3.59
5 -8 4 8.71 1.86
6 -8 4 4.66 1.42
7 -8 4 17.53 2.38
8 -8 4 10.10 1.45
9 -8 4 14.71 1.68
1 7 5 10.24 1.76
2 7 5 1.25 2.72
3 7 5 23.04 3.05
4 7 5 9.94 1.84
5 7 5 59.05 4.47
6 7 5 23.84 2.67
7 7 5 28.96 7.06
8 7 5 16.46 3.21
9 7 5 11.07 2.07
10 7 5 16.33 3.25
11 7 5 12.57 3.33
12 7 5 100.81 6.95
1 6 5 28.97 1.80
2 6 5 2.27 0.85
3 6 5 2.70 1.37
4 6 5 12.86 1.52
5 6 5 23.20 3.93
6 6 5 2.76 1.57
7 6 5 10.45 2.46
8 6 5 32.81 3.90
9 6 5 19.37 2.26
10 6 5 72.81 4.98
11 6 5 44.05 3.62
12 6 5 73.65 5.18
13 6 5 65.38 5.04
14 6 5 97.84 8.85
15 6 5 8.83 2.13
16 6 5 39.25 4.43
17 6 5 42.94 4.09
1 5 5 29.93 1.88
2 5 5 118.95 5.95
3 5 5 168.78 9.72
4 5 5 26.93 1.66
5 5 5 92.76 4.99
6 5 5 115.65 7.87
7 5 5 92.24 5.77
8 5 5 71.49 5.01
9 5 5 15.17 1.38
10 5 5 54.39 3.45
11 5 5 46.55 5.48
12 5 5 21.42 2.49
13 5 5 11.02 2.08
14 5 5 0.89 1.16
15 5 5 -1.05 1.68
16 5 5 8.79 1.44
17 5 5 0.32 1.19
18 5 5 5.37 1.94
19 5 5 9.48 1.64
20 5 5 2.85 1.49
1 4 5 89.76 5.03
2 4 5 47.32 3.45
3 4 5 133.51 6.36
4 4 5 79.77 3.92
5 4 5 142.95 10.14
6 4 5 137.30 9.82
7 4 5 24.12 2.32
8 4 5 114.84 6.74
9 4 5 73.05 5.51
10 4 5 10.25 1.17
11 4 5 13.81 0.98
12 4 5 5.81 1.04
13 4 5 29.16 1.57
14 4 5 38.63 4.85
15 4 5 20.46 1.30
16 4 5 5.18 0.84
17 4 5 25.45 3.24
18 4 5 152.13 9.67
19 4 5 14.17 1.76
20 4 5 71.93 7.11
21 4 5 48.41 3.93
22 4 5 17.68 6.17
1 3 5 20.98 1.70
2 3 5 28.94 1.47
3 3 5 2.06 0.49
4 3 5 60.65 5.85
5 3 5 3.50 0.43
6 3 5 3.24 0.47
7 3 5 19.41 1.70
8 3 5 33.20 2.05
9 3 5 24.16 1.96
10 3 5 49.14 5.25
11 3 5 124.72 9.36
12 3 5 47.61 3.35
13 3 5 73.12 3.82
14 3 5 39.77 2.13
15 3 5 78.12 3.87
16 3 5 11.58 0.94
17 3 5 31.22 1.79
18 3 5 158.81 10.87
19 3 5 22.10 1.54
20 3 5 35.03 3.45
21 3 5 87.73 15.77
22 3 5 25.34 2.52
23 3 5 9.02 3.17
24 3 5 43.07 5.34
1 2 5 10.38 0.70
2 2 5 159.27 6.58
3 2 5 266.61 12.89
4 2 5 195.48 10.89
5 2 5 44.04 3.77
6 2 5 17.59 1.22
7 2 5 10.24 0.74
8 2 5 7.14 0.82
9 2 5 45.04 4.71
10 2 5 45.19 2.50
11 2 5 22.49 1.75
12 2 5 33.32 1.73
13 2 5 62.26 5.06
14 2 5 40.65 2.14
15 2 5 19.84 1.29
16 2 5 18.75 1.26
17 2 5 3.74 0.67
18 2 5 4.41 1.00
19 2 5 3.07 0.79
20 2 5 0.08 1.48
21 2 5 5.30 0.91
22 2 5 2.13 1.05
23 2 5 19.73 2.16
24 2 5 12.49 2.21
25 2 5 9.57 1.97
1 1 5 6.84 1.04
2 1 5 161.29 6.23
3 1 5 120.81 5.05
4 1 5 8.82 0.69
5 1 5 120.02 5.35
6 1 5 64.95 2.77
7 1 5 385.30 14.77
8 1 5 142.12 7.73
9 1 5 107.23 4.90
10 1 5 99.39 4.74
11 1 5 41.05 2.28
12 1 5 32.17 3.22
13 1 5 15.79 1.36
14 1 5 31.61 1.62
15 1 5 32.91 1.71
16 1 5 36.51 1.88
17 1 5 18.06 1.34
18 1 5 73.24 3.28
19 1 5 16.98 1.36
20 1 5 19.93 1.58
21 1 5 10.21 1.43
22 1 5 23.61 3.22
23 1 5 27.42 2.19
24 1 5 19.95 1.80
25 1 5 5.27 1.15
0 0 5 14.33 1.03
1 0 5 0.07 0.33
2 0 5 93.23 3.93
3 0 5 3.38 0.77
4 0 5 212.99 9.51
5 0 5 17.53 1.92
6 0 5 217.95 8.01
7 0 5 1.04 0.42
8 0 5 5.29 0.55
9 0 5 1.72 0.39
10 0 5 246.58 9.82
11 0 5 1.82 0.46
12 0 5 45.39 2.25
13 0 5 4.24 0.61
14 0 5 372.18 14.32
15 0 5 4.99 0.71
16 0 5 183.87 8.72
17 0 5 4.07 0.73
18 0 5 445.76 18.05
19 0 5 3.61 1.17
20 0 5 203.28 8.37
21 0 5 2.79 1.17
22 0 5 74.44 4.20
23 0 5 0.64 0.85
24 0 5 8.82 1.38
25 0 5 0.88 4.02
0 -1 5 -0.69 0.99
1 -1 5 8.05 0.75
2 -1 5 156.12 6.37
3 -1 5 116.04 4.88
4 -1 5 6.86 0.86
5 -1 5 117.57 5.47
6 -1 5 60.73 2.36
7 -1 5 353.63 12.51
8 -1 5 130.89 5.69
9 -1 5 102.37 4.18
10 -1 5 100.25 4.25
11 -1 5 41.94 1.86
12 -1 5 33.09 1.86
13 -1 5 19.64 1.19
14 -1 5 32.62 1.80
15 -1 5 33.53 1.80
16 -1 5 36.70 1.96
17 -1 5 18.18 1.60
18 -1 5 74.86 3.74
19 -1 5 17.25 1.45
20 -1 5 22.37 2.73
21 -1 5 11.40 1.62
22 -1 5 23.77 2.16
23 -1 5 27.94 2.79
24 -1 5 21.84 1.94
25 -1 5 4.10 1.40
0 -2 5 0.13 0.38
1 -2 5 9.21 0.79
2 -2 5 147.24 5.00
3 -2 5 258.91 8.74
4 -2 5 198.72 8.62
5 -2 5 38.99 2.27
6 -2 5 15.84 0.96
7 -2 5 8.35 0.72
8 -2 5 6.07 0.63
9 -2 5 43.60 1.93
10 -2 5 47.25 2.05
11 -2 5 21.16 1.32
12 -2 5 39.00 2.13
13 -2 5 59.27 2.90
14 -2 5 42.85 3.09
15 -2 5 23.80 1.65
16 -2 5 21.78 1.94
17 -2 5 5.38 0.81
18 -2 5 5.50 0.87
19 -2 5 4.61 0.80
20 -2 5 1.06 0.82
21 -2 5 6.79 1.50
22 -2 5 3.41 0.81
23 -2 5 26.43 2.31
24 -2 5 12.41 1.47
25 -2 5 8.84 1.34
0 -3 5 0.04 0.49
1 -3 5 21.72 1.11
2 -3 5 30.33 1.37
3 -3 5 1.57 0.51
4 -3 5 53.47 2.47
5 -3 5 2.83 0.52
6 -3 5 1.75 0.50
7 -3 5 18.38 1.13
8 -3 5 35.39 2.15
9 -3 5 24.50 1.62
10 -3 5 53.45 2.82
11 -3 5 120.14 5.93
12 -3 5 46.43 3.25
13 -3 5 78.46 4.24
14 -3 5 42.45 2.40
15 -3 5 83.60 4.14
16 -3 5 13.12 1.11
17 -3 5 31.50 2.21
18 -3 5 159.35 7.67
19 -3 5 23.32 3.28
20 -3 5 37.81 2.75
21 -3 5 80.62 5.55
22 -3 5 22.79 2.37
23 -3 5 9.45 1.17
24 -3 5 45.65 4.91
0 -4 5 1.29 0.58
1 -4 5 88.71 3.58
2 -4 5 48.44 2.09
3 -4 5 138.79 5.00
4 -4 5 79.06 3.58
5 -4 5 143.82 5.63
6 -4 5 134.66 5.34
7 -4 5 22.79 1.54
8 -4 5 105.43 5.27
9 -4 5 74.44 3.61
10 -4 5 11.64 1.06
11 -4 5 15.37 1.25
12 -4 5 5.00 0.79
13 -4 5 30.72 1.85
14 -4 5 40.97 2.75
15 -4 5 22.58 1.71
16 -4 5 7.62 0.99
17 -4 5 24.50 2.64
18 -4 5 133.21 7.78
19 -4 5 17.51 1.50
20 -4 5 61.79 5.32
21 -4 5 48.07 4.33
22 -4 5 15.43 1.58
0 -5 5 1.21 0.77
1 -5 5 30.10 1.89
2 -5 5 127.02 5.45
3 -5 5 177.13 6.45
4 -5 5 27.14 1.59
5 -5 5 92.08 3.71
6 -5 5 111.86 4.74
7 -5 5 87.63 3.55
8 -5 5 76.07 3.97
9 -5 5 12.83 1.56
10 -5 5 56.30 3.10
11 -5 5 49.02 2.89
12 -5 5 22.31 2.84
13 -5 5 13.16 1.28
14 -5 5 0.93 0.80
15 -5 5 2.15 0.79
16 -5 5 12.26 1.74
17 -5 5 0.68 0.90
18 -5 5 7.32 1.52
19 -5 5 9.94 1.18
20 -5 5 1.84 0.85
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1 -6 5 30.76 1.98
2 -6 5 2.18 0.77
3 -6 5 3.05 0.82
4 -6 5 12.60 1.19
5 -6 5 23.09 2.00
6 -6 5 2.54 0.72
7 -6 5 9.85 1.27
8 -6 5 32.54 2.15
9 -6 5 18.44 1.54
10 -6 5 73.81 5.76
11 -6 5 38.10 2.95
12 -6 5 69.07 6.79
13 -6 5 63.95 4.64
14 -6 5 88.46 6.27
15 -6 5 8.31 1.52
16 -6 5 38.30 3.40
17 -6 5 36.59 2.80
0 -7 5 1.29 1.02
1 -7 5 11.37 1.55
2 -7 5 1.11 0.91
3 -7 5 25.42 1.99
4 -7 5 11.12 2.20
5 -7 5 59.30 3.47
6 -7 5 22.97 2.11
7 -7 5 23.26 2.00
8 -7 5 14.82 1.69
9 -7 5 7.73 1.41
10 -7 5 9.25 1.46
11 -7 5 13.62 1.68
12 -7 5 89.87 5.73
1 7 6 7.11 2.57
2 7 6 22.29 3.68
3 7 6 5.37 2.11
4 7 6 15.13 3.05
5 7 6 17.73 3.49
1 6 6 32.73 2.56
2 6 6 9.70 1.73
3 6 6 3.99 5.28
4 6 6 49.85 8.18
5 6 6 15.88 2.13
6 6 6 16.03 2.93
7 6 6 19.49 6.12
8 6 6 19.43 5.44
9 6 6 6.97 2.46
10 6 6 8.51 2.93
11 6 6 14.20 3.72
12 6 6 85.60 4.99
13 6 6 52.42 5.22
1 5 6 52.01 2.92
2 5 6 25.89 1.34
3 5 6 52.44 2.58
4 5 6 33.65 2.40
5 5 6 5.99 0.84
6 5 6 12.08 1.03
7 5 6 26.51 2.12
8 5 6 103.42 5.21
9 5 6 37.16 2.54
10 5 6 5.10 1.21
11 5 6 1.00 1.06
12 5 6 0.92 1.14
13 5 6 5.28 1.20
14 5 6 1.31 1.68
15 5 6 8.75 1.48
16 5 6 1.95 1.22
17 5 6 7.83 1.87
1 4 6 2.21 0.92
2 4 6 2.42 0.96
3 4 6 26.40 2.27
4 4 6 118.31 6.80
5 4 6 126.44 7.14
6 4 6 11.43 1.02
7 4 6 72.55 3.69
8 4 6 9.05 0.98
9 4 6 16.07 1.16
10 4 6 -0.27 1.16
11 4 6 8.40 1.05
12 4 6 34.72 2.31
13 4 6 6.36 1.33
14 4 6 31.02 3.26
15 4 6 11.78 1.55
16 4 6 17.75 1.79
17 4 6 11.72 2.70
18 4 6 4.07 1.23
19 4 6 55.87 6.45
1 3 6 92.47 4.35
2 3 6 45.01 2.42
3 3 6 69.17 3.41
4 3 6 62.38 4.17
5 3 6 13.99 0.99
6 3 6 49.81 4.11
7 3 6 22.37 1.43
8 3 6 1.09 0.46
9 3 6 23.18 2.31
10 3 6 96.45 6.18
11 3 6 8.86 1.16
12 3 6 33.62 2.03
13 3 6 14.12 1.29
14 3 6 39.57 7.65
15 3 6 52.99 6.00
16 3 6 68.73 5.73
17 3 6 87.04 14.29
18 3 6 84.38 8.24
19 3 6 47.01 16.87
20 3 6 11.49 2.01
21 3 6 18.65 3.60
1 2 6 546.77 27.30
2 2 6 446.02 22.80
3 2 6 49.26 3.16
4 2 6 34.27 2.62
5 2 6 31.70 1.74
6 2 6 24.80 1.99
7 2 6 18.65 1.62
8 2 6 51.93 3.88
9 2 6 10.67 1.88
10 2 6 60.86 4.77
11 2 6 20.12 1.63
12 2 6 69.59 4.26
13 2 6 45.92 3.57
14 2 6 94.02 6.14
15 2 6 73.00 5.11
16 2 6 22.64 2.96
17 2 6 7.94 1.64
18 2 6 8.84 1.75
19 2 6 23.00 2.92
20 2 6 2.79 1.65
21 2 6 1.86 1.24
22 2 6 10.30 4.76
1 1 6 62.18 4.87
2 1 6 65.56 5.57
3 1 6 64.22 4.06
4 1 6 223.95 10.16
5 1 6 247.35 11.60
6 1 6 117.01 6.23
7 1 6 8.41 0.86
8 1 6 86.91 4.71
9 1 6 60.54 5.60
10 1 6 20.24 1.96
11 1 6 48.69 2.85
12 1 6 2.90 0.70
13 1 6 44.44 2.76
14 1 6 46.65 2.57
15 1 6 94.91 6.14
16 1 6 38.71 2.24
17 1 6 38.49 2.40
18 1 6 29.95 3.08
19 1 6 43.70 3.77
20 1 6 33.11 6.04
21 1 6 10.38 3.02
22 1 6 6.60 1.82
23 1 6 6.99 1.71
0 0 6 260.54 11.45
1 0 6 1.34 0.57
2 0 6 33.79 2.74
3 0 6 0.59 0.55
4 0 6 33.20 1.83
5 0 6 0.61 0.58
6 0 6 144.39 8.12
7 0 6 3.12 1.20
8 0 6 88.71 5.42
9 0 6 1.26 0.67
10 0 6 43.77 2.39
11 0 6 2.49 0.65
12 0 6 111.32 4.71
13 0 6 4.12 1.06
14 0 6 64.06 3.17
15 0 6 1.41 0.56
16 0 6 69.00 3.17
17 0 6 7.01 2.18
18 0 6 276.61 12.69
19 0 6 3.97 0.89
20 0 6 133.35 12.14
21 0 6 2.19 1.68
22 0 6 29.72 10.59
23 0 6 2.82 1.63
0 -1 6 184.07 10.81
1 -1 6 65.13 4.18
2 -1 6 65.22 3.12
3 -1 6 61.83 3.03
4 -1 6 224.12 10.24
5 -1 6 247.65 12.30
6 -1 6 114.60 5.14
7 -1 6 6.97 0.90
8 -1 6 87.54 8.84
9 -1 6 56.27 3.25
10 -1 6 20.15 1.98
11 -1 6 49.10 2.52
12 -1 6 2.61 0.66
13 -1 6 42.79 2.17
14 -1 6 47.17 2.33
15 -1 6 91.71 4.04
16 -1 6 37.91 2.17
17 -1 6 39.76 2.47
18 -1 6 33.07 2.32
19 -1 6 44.97 2.79
20 -1 6 31.01 2.49
21 -1 6 14.18 2.46
22 -1 6 10.76 4.47
23 -1 6 6.76 2.53
0 -2 6 967.69 47.21
1 -2 6 510.69 24.73
2 -2 6 426.15 17.57
3 -2 6 45.43 3.43
4 -2 6 33.97 1.93
5 -2 6 31.40 2.58
6 -2 6 24.52 1.51
7 -2 6 19.06 1.61
8 -2 6 48.59 2.17
9 -2 6 10.81 0.92
10 -2 6 56.49 2.76
11 -2 6 19.58 1.52
12 -2 6 70.43 3.28
13 -2 6 47.09 2.64
14 -2 6 95.07 4.77
15 -2 6 75.05 4.28
16 -2 6 28.29 2.51
17 -2 6 11.06 3.02
18 -2 6 8.64 1.15
19 -2 6 27.88 2.54
20 -2 6 4.46 1.18
21 -2 6 2.81 1.36
22 -2 6 11.68 1.66
0 -3 6 265.22 9.61
1 -3 6 93.72 4.53
2 -3 6 38.44 2.06
3 -3 6 67.34 3.05
4 -3 6 61.26 2.33
5 -3 6 14.64 1.18
6 -3 6 47.78 2.11
7 -3 6 23.00 1.22
8 -3 6 0.62 0.75
9 -3 6 23.47 1.53
10 -3 6 91.02 4.46
11 -3 6 8.58 0.88
12 -3 6 32.98 2.14
13 -3 6 15.30 1.60
14 -3 6 44.84 2.40
15 -3 6 65.55 5.15
16 -3 6 68.53 3.98
17 -3 6 77.47 4.31
18 -3 6 84.09 4.57
19 -3 6 44.15 2.97
20 -3 6 13.25 2.24
21 -3 6 27.72 2.43
0 -4 6 78.01 3.24
1 -4 6 3.72 0.76
2 -4 6 2.32 0.90
3 -4 6 26.30 1.69
4 -4 6 115.01 4.45
5 -4 6 122.50 5.06
6 -4 6 11.55 1.07
7 -4 6 70.20 3.40
8 -4 6 7.82 0.98
9 -4 6 16.36 1.73
10 -4 6 0.38 0.64
11 -4 6 9.37 0.93
12 -4 6 34.47 1.95
13 -4 6 8.37 1.08
14 -4 6 32.43 2.02
15 -4 6 14.24 1.63
16 -4 6 19.66 1.62
17 -4 6 15.72 1.75
18 -4 6 5.04 1.05
19 -4 6 53.61 2.94
0 -5 6 232.35 9.01
1 -5 6 56.09 3.03
2 -5 6 24.55 1.71
3 -5 6 54.25 3.32
4 -5 6 31.42 1.82
5 -5 6 6.20 0.92
6 -5 6 11.28 1.14
7 -5 6 26.46 2.73
8 -5 6 94.77 4.97
9 -5 6 36.36 3.40
10 -5 6 4.18 0.84
11 -5 6 2.97 0.92
12 -5 6 2.10 1.27
13 -5 6 7.25 1.10
14 -5 6 2.82 1.48
15 -5 6 8.66 1.89
16 -5 6 3.09 0.99
17 -5 6 7.29 1.76
0 -6 6 10.89 1.48
1 -6 6 33.15 2.13
2 -6 6 10.75 1.51
3 -6 6 3.32 1.06
4 -6 6 46.23 3.11
5 -6 6 17.77 2.56
6 -6 6 10.24 1.45
7 -6 6 15.18 1.60
8 -6 6 14.68 1.63
9 -6 6 10.90 1.26
10 -6 6 8.22 1.48
11 -6 6 15.53 1.96
12 -6 6 78.95 6.37
13 -6 6 47.19 3.20
0 -7 6 0.65 1.47
1 -7 6 6.32 1.63
2 -7 6 16.45 2.18
3 -7 6 2.76 1.28
4 -7 6 16.08 3.31
5 -7 6 16.39 3.42
1 6 7 8.66 2.63
4 6 7 26.21 4.16
5 6 7 12.58 2.79
1 5 7 57.48 5.77
2 5 7 35.82 4.61
3 5 7 21.86 3.55
4 5 7 8.04 2.45
5 5 7 2.36 1.91
6 5 7 23.12 3.87
7 5 7 9.25 2.72
8 5 7 46.39 4.03
9 5 7 21.42 2.52
10 5 7 18.06 3.82
11 5 7 27.64 4.54
12 5 7 12.52 2.00
1 4 7 63.76 6.12
2 4 7 22.00 3.30
3 4 7 31.18 4.19
4 4 7 61.34 4.27
5 4 7 96.49 6.11
6 4 7 110.38 6.65
7 4 7 18.29 1.35
8 4 7 40.56 3.16
9 4 7 17.76 1.61
10 4 7 22.25 1.89
11 4 7 15.63 3.07
12 4 7 16.73 1.73
13 4 7 2.36 1.55
14 4 7 1.39 1.03
15 4 7 7.64 2.10
1 3 7 1.62 1.03
2 3 7 31.38 2.03
3 3 7 21.56 2.38
4 3 7 70.02 3.64
5 3 7 71.21 3.67
6 3 7 50.52 2.83
7 3 7 23.30 1.85
8 3 7 21.07 1.34
9 3 7 5.13 0.73
10 3 7 4.34 0.79
11 3 7 55.95 4.17
12 3 7 4.59 1.19
13 3 7 18.25 2.42
14 3 7 5.30 1.19
15 3 7 7.10 2.22
16 3 7 18.87 2.57
17 3 7 7.76 2.07
1 2 7 23.66 1.39
2 2 7 42.39 3.93
3 2 7 12.90 1.24
4 2 7 5.04 0.85
5 2 7 29.68 1.98
6 2 7 13.00 1.14
7 2 7 9.25 0.86
8 2 7 14.97 1.60
9 2 7 4.07 0.91
10 2 7 44.88 3.58
11 2 7 7.10 1.17
12 2 7 14.23 5.91
13 2 7 26.32 6.22
14 2 7 84.44 10.61
15 2 7 31.56 8.42
16 2 7 19.69 4.24
17 2 7 40.51 5.86
18 2 7 26.60 3.52
19 2 7 1.32 3.25
1 1 7 21.70 2.19
2 1 7 66.28 4.10
3 1 7 93.51 5.39
4 1 7 38.78 3.07
5 1 7 67.32 5.69
6 1 7 74.19 4.64
7 1 7 28.43 1.79
8 1 7 1.71 0.63
9 1 7 12.97 1.81
10 1 7 16.91 2.04
11 1 7 18.28 2.18
12 1 7 37.31 3.35
13 1 7 29.12 4.74
14 1 7 12.40 1.80
15 1 7 6.67 1.53
16 1 7 6.05 1.43
17 1 7 59.67 5.04
18 1 7 36.53 9.94
19 1 7 32.37 3.43
20 1 7 39.80 4.03
1 0 7 -0.60 1.54
2 0 7 26.59 2.44
3 0 7 0.60 0.59
4 0 7 68.43 3.57
5 0 7 4.69 1.11
6 0 7 86.23 7.17
7 0 7 39.44 3.25
8 0 7 180.07 13.77
9 0 7 3.09 0.87
10 0 7 49.76 3.09
11 0 7 3.31 0.82
12 0 7 74.50 6.97
13 0 7 4.05 1.14
14 0 7 85.42 6.42
15 0 7 6.24 2.03
16 0 7 118.33 8.30
17 0 7 2.11 1.30
18 0 7 68.71 8.34
19 0 7 3.78 1.55
20 0 7 83.12 7.17
0 -1 7 0.64 0.83
1 -1 7 19.03 2.00
2 -1 7 60.75 6.88
3 -1 7 85.38 7.30
4 -1 7 37.06 2.70
5 -1 7 69.66 5.30
6 -1 7 80.11 4.44
7 -1 7 28.44 4.41
8 -1 7 2.50 0.66
9 -1 7 16.86 1.61
10 -1 7 19.87 2.21
11 -1 7 21.54 3.25
12 -1 7 41.30 2.64
13 -1 7 32.60 3.22
14 -1 7 16.05 1.81
15 -1 7 9.55 1.73
16 -1 7 6.58 1.39
17 -1 7 64.11 5.57
18 -1 7 31.78 3.83
19 -1 7 34.88 4.83
20 -1 7 45.69 6.10
0 -2 7 -0.20 1.32
1 -2 7 22.56 1.52
2 -2 7 42.11 4.74
3 -2 7 10.88 1.27
4 -2 7 4.86 0.87
5 -2 7 27.01 2.06
6 -2 7 9.18 1.17
7 -2 7 10.11 1.63
8 -2 7 17.12 1.90
9 -2 7 3.67 1.15
10 -2 7 51.11 5.02
11 -2 7 10.57 1.39
12 -2 7 10.27 1.72
13 -2 7 27.99 4.22
14 -2 7 84.51 6.58
15 -2 7 29.05 2.46
16 -2 7 19.44 3.35
17 -2 7 30.83 6.00
18 -2 7 24.12 3.41
19 -2 7 1.79 1.69
0 -3 7 0.92 0.71
1 -3 7 2.75 0.80
2 -3 7 30.95 2.14
3 -3 7 22.47 1.59
4 -3 7 68.68 3.35
5 -3 7 66.36 4.77
6 -3 7 44.89 3.36
7 -3 7 26.67 1.76
8 -3 7 21.76 1.90
9 -3 7 6.08 1.34
10 -3 7 4.44 1.24
11 -3 7 54.39 3.76
12 -3 7 5.31 1.12
13 -3 7 18.49 2.37
14 -3 7 6.35 1.14
15 -3 7 4.57 1.46
16 -3 7 19.58 3.28
17 -3 7 7.84 1.40
0 -4 7 5.43 1.12
1 -4 7 65.67 3.58
2 -4 7 21.96 2.86
3 -4 7 34.15 3.28
4 -4 7 61.67 3.91
5 -4 7 97.62 5.58
6 -4 7 105.48 5.32
7 -4 7 19.68 1.62
8 -4 7 42.22 2.39
9 -4 7 18.19 1.56
10 -4 7 19.69 2.05
11 -4 7 10.22 1.42
12 -4 7 15.48 3.30
13 -4 7 2.26 2.23
14 -4 7 0.72 1.26
15 -4 7 7.36 1.36
0 -5 7 8.31 1.43
1 -5 7 59.22 3.97
2 -5 7 38.98 3.11
3 -5 7 25.92 2.72
4 -5 7 9.12 1.83
5 -5 7 5.23 1.22
6 -5 7 22.73 2.34
7 -5 7 11.10 1.98
8 -5 7 53.00 5.65
9 -5 7 20.26 2.52
10 -5 7 13.45 1.68
11 -5 7 29.47 2.84
12 -5 7 11.61 2.11
0 -6 7 2.14 2.98
1 -6 7 9.79 2.21
2 -6 7 15.23 3.19
3 -6 7 34.53 3.33
4 -6 7 19.52 2.75
5 -6 7 8.77 2.13
1 4 8 7.97 2.31
2 4 8 3.96 2.18
3 4 8 25.26 3.92
4 4 8 9.02 2.59
5 4 8 1.86 1.97
6 4 8 6.53 2.59
7 4 8 2.83 2.35
9 4 8 16.68 3.43
1 3 8 219.32 18.31
2 3 8 81.47 7.43
3 3 8 44.20 5.16
4 3 8 33.72 4.58
5 3 8 54.84 5.70
6 3 8 53.63 5.69
7 3 8 14.19 2.89
8 3 8 6.82 2.33
9 3 8 13.28 3.17
10 3 8 -1.70 1.76
11 3 8 5.30 1.53
12 3 8 34.21 3.22
1 2 8 84.08 5.72
2 2 8 41.37 3.55
3 2 8 79.53 5.39
4 2 8 3.04 1.52
5 2 8 20.70 2.70
6 2 8 50.14 5.67
7 2 8 3.69 2.84
8 2 8 12.63 2.21
9 2 8 5.35 1.05
10 2 8 63.79 7.75
11 2 8 3.94 1.34
12 2 8 21.63 3.62
13 2 8 22.38 5.59
14 2 8 57.08 5.86
1 1 8 14.13 2.25
2 1 8 11.28 1.96
3 1 8 19.79 2.47
4 1 8 35.50 4.76
5 1 8 3.21 2.17
6 1 8 9.16 1.91
7 1 8 17.50 2.98
8 1 8 24.01 3.05
9 1 8 26.07 2.75
10 1 8 31.45 4.96
11 1 8 40.84 6.04
12 1 8 48.68 6.98
13 1 8 29.12 2.37
14 1 8 23.89 3.15
15 1 8 59.68 9.31
0 0 8 10.59 1.90
1 0 8 0.06 1.22
2 0 8 41.20 3.45
3 0 8 5.90 1.59
4 0 8 69.24 5.91
5 0 8 1.57 0.91
6 0 8 59.11 4.31
7 0 8 1.79 1.11
8 0 8 89.07 8.18
9 0 8 3.80 1.91
10 0 8 13.62 2.60
11 0 8 2.93 1.11
12 0 8 66.55 14.63
13 0 8 4.84 1.70
14 0 8 49.67 7.38
15 0 8 1.78 1.17
0 -1 8 26.58 2.26
1 -1 8 16.35 2.21
2 -1 8 10.57 1.17
3 -1 8 20.59 2.49
4 -1 8 30.61 2.02
5 -1 8 4.07 1.17
6 -1 8 6.39 2.11
7 -1 8 17.88 2.12
8 -1 8 23.86 2.64
9 -1 8 22.69 2.71
10 -1 8 29.49 3.91
11 -1 8 46.18 3.85
12 -1 8 46.43 5.38
13 -1 8 28.91 3.57
14 -1 8 22.05 2.56
15 -1 8 54.57 6.64
0 -2 8 204.03 14.14
1 -2 8 86.80 4.83
2 -2 8 47.54 4.36
3 -2 8 76.25 5.96
4 -2 8 6.62 1.42
5 -2 8 17.09 3.62
6 -2 8 52.69 4.48
7 -2 8 5.68 1.41
8 -2 8 14.36 1.63
9 -2 8 6.54 1.27
10 -2 8 67.39 7.13
11 -2 8 6.09 1.64
12 -2 8 26.11 3.08
13 -2 8 23.16 4.25
14 -2 8 56.30 7.06
0 -3 8 283.67 23.06
1 -3 8 217.10 15.65
2 -3 8 80.13 5.87
3 -3 8 42.86 3.24
4 -3 8 38.36 2.33
5 -3 8 55.92 4.96
6 -3 8 55.09 3.98
7 -3 8 9.41 1.21
8 -3 8 5.93 1.66
9 -3 8 19.27 2.74
10 -3 8 1.08 1.11
11 -3 8 3.57 1.15
12 -3 8 35.40 2.90
0 -4 8 118.95 11.82
1 -4 8 10.03 5.68
2 -4 8 11.65 2.66
3 -4 8 19.60 2.76
4 -4 8 10.95 1.96
5 -4 8 3.27 1.59
6 -4 8 5.78 1.19
7 -4 8 2.47 1.28
8 -4 8 6.21 1.39
9 -4 8 16.00 1.89
1 2 9 10.90 2.53
2 2 9 1.15 1.77
3 2 9 13.20 2.84
4 2 9 19.45 3.63
5 2 9 2.66 2.28
1 1 9 18.43 2.82
2 1 9 26.87 6.32
3 1 9 1.27 1.71
4 1 9 0.23 1.70
5 1 9 12.62 2.46
6 1 9 10.88 2.59
7 1 9 16.24 3.90
0 0 9 -0.68 2.90
1 0 9 0.83 3.11
2 0 9 67.83 7.86
3 0 9 5.16 2.99
4 0 9 52.30 7.35
5 0 9 5.56 3.06
6 0 9 6.15 3.32
7 0 9 6.83 5.97
8 0 9 72.67 6.92
0 -1 9 6.38 3.67
1 -1 9 15.80 4.71
2 -1 9 26.87 5.64
3 -1 9 3.95 3.25
4 -1 9 1.86 1.53
5 -1 9 8.39 2.06
6 -1 9 7.60 2.01
7 -1 9 14.40 3.23
0 -2 9 2.01 1.45
1 -2 9 10.59 2.94
2 -2 9 -0.14 2.96
3 -2 9 8.54 1.93
4 -2 9 26.54 3.32
5 -2 9 0.14 1.32
0 0 0 0.00 0.00
_computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)'
;
_shelx_hkl_checksum 41922
_shelx_res_file
;
TITL shelxt_a.res in Pca2(1)
shelx.res
created by SHELXL-2018/3 at 18:35:56 on 19-Jul-2023
CELL 0.71073 23.6120 7.2392 7.2122 90.000 90.000 90.000
ZERR 4.00 0.0030 0.0008 0.0007 0.000 0.000 0.000
LATT -1
SYMM - X, - Y, 1/2 + Z
SYMM 1/2 + X, - Y, Z
SYMM 1/2 - X, Y, 1/2 + Z
SFAC C H F N O
UNIT 64 44 4 8 4
MERG 2
OMIT 3 1 1
OMIT 6 3 0
OMIT 3 3 6
OMIT 3 3 -6
OMIT 6 0 -6
OMIT 6 0 6
OMIT 2 3 0
OMIT 14 0 0
OMIT 10 0 1
OMIT 9 2 2
OMIT 10 0 -1
HTAB N19 O17
EQIV $1 x, y-1, z
HTAB C2 O17_$1
EQIV $2 -x+1, -y+1, z-1/2
HTAB C5 O17_$2
HTAB N19 O17
HTAB C2 O17_$1
HTAB C5 O17_$2
HTAB N19 O17
HTAB C2 O17_$1
HTAB C5 O17_$2
FMAP 2
PLAN 20
ACTA NOHKL
BOND
BOND $H
CONF
LIST 4
L.S. 10
TEMP -123.00
WGHT 0.063300 0.187000
FVAR 0.80123
F18 3 0.484736 0.500400 0.440125 11.00000 0.02925 0.03326 =
0.07870 -0.00009 0.00165 -0.00851
O17 5 0.353477 0.710257 0.636110 11.00000 0.03681 0.02950 =
0.04120 0.00057 -0.00095 -0.00810
N20 4 0.325501 0.344894 0.516352 11.00000 0.02269 0.02464 =
0.02125 0.00433 -0.00052 -0.00107
N19 4 0.379240 0.389806 0.519723 11.00000 0.02192 0.02500 =
0.02933 0.00227 -0.00114 -0.00301
AFIX 43
H21 2 0.390131 0.499630 0.557997 11.00000 -1.20000
AFIX 0
C1 1 0.418852 0.258647 0.460903 11.00000 0.02349 0.02781 =
0.02363 0.00465 -0.00166 0.00073
C2 1 0.406336 0.073111 0.437431 11.00000 0.02699 0.02852 =
0.02942 0.00306 -0.00279 -0.00156
AFIX 43
H22 2 0.369604 0.028034 0.466435 11.00000 -1.20000
AFIX 0
C7 1 0.287961 0.471194 0.565450 11.00000 0.02783 0.02278 =
0.01731 0.00458 -0.00007 0.00071
C4 1 0.500927 0.017675 0.326659 11.00000 0.03231 0.04343 =
0.02770 0.00018 0.00111 0.00916
AFIX 43
H24 2 0.528484 -0.065430 0.279197 11.00000 -1.20000
AFIX 0
C9 1 0.256666 0.780613 0.672910 11.00000 0.04518 0.02505 =
0.02388 0.00072 0.00275 0.00243
AFIX 43
H27 2 0.265059 0.901517 0.716130 11.00000 -1.20000
AFIX 0
C14 1 0.155841 0.195502 0.471823 11.00000 0.03136 0.03582 =
0.03315 0.00526 -0.00016 -0.00456
AFIX 43
H26 2 0.145461 0.075616 0.430408 11.00000 -1.20000
AFIX 0
C13 1 0.212421 0.241459 0.489693 11.00000 0.02489 0.02838 =
0.02757 0.00331 0.00109 0.00236
AFIX 43
H28 2 0.240645 0.152688 0.460149 11.00000 -1.20000
AFIX 0
C10 1 0.202136 0.727606 0.656503 11.00000 0.04120 0.03329 =
0.02329 0.00224 0.00478 0.01143
AFIX 43
H29 2 0.173167 0.813258 0.687556 11.00000 -1.20000
AFIX 0
C3 1 0.447339 -0.046169 0.371815 11.00000 0.03597 0.02921 =
0.03337 -0.00033 -0.00151 0.00092
AFIX 43
H23 2 0.438708 -0.173543 0.357452 11.00000 -1.20000
AFIX 0
C8 1 0.302541 0.657263 0.626094 11.00000 0.03454 0.02708 =
0.02038 0.00422 -0.00025 -0.00101
C11 1 0.186268 0.547392 0.594149 11.00000 0.02975 0.03225 =
0.01999 0.00661 0.00303 0.00768
C6 1 0.473453 0.318709 0.418645 11.00000 0.02528 0.03071 =
0.03519 0.00420 -0.00272 -0.00337
C12 1 0.228540 0.416579 0.550572 11.00000 0.02620 0.02892 =
0.01615 0.00595 0.00134 0.00225
C15 1 0.114004 0.324449 0.514361 11.00000 0.02416 0.05283 =
0.03222 0.00703 -0.00033 0.00085
AFIX 43
H30 2 0.075180 0.292542 0.501361 11.00000 -1.20000
AFIX 0
C16 1 0.128779 0.496936 0.574821 11.00000 0.02659 0.04637 =
0.02961 0.00661 0.00397 0.01148
AFIX 43
H31 2 0.100014 0.583900 0.604186 11.00000 -1.20000
AFIX 0
C5 1 0.514402 0.202383 0.350570 11.00000 0.02401 0.04623 =
0.03582 0.00644 0.00166 0.00077
AFIX 43
H25 2 0.551065 0.247445 0.320609 11.00000 -1.20000
AFIX 0
HKLF 4
REM shelxt_a.res in Pca2(1)
REM wR2 = 0.1094, GooF = S = 1.081, Restrained GooF = 1.080 for all data
REM R1 = 0.0442 for 2700 Fo > 4sig(Fo) and 0.0458 for all 2803 data
REM 181 parameters refined using 1 restraints
END
WGHT 0.0633 0.1847
REM Highest difference peak 0.322, deepest hole -0.230, 1-sigma level 0.058
Q1 1 0.4076 0.1783 0.4125 11.00000 0.05 0.32
Q2 1 0.2942 0.5566 0.6365 11.00000 0.05 0.29
Q3 1 0.1987 0.6455 0.5934 11.00000 0.05 0.27
Q4 1 0.4986 0.1167 0.3108 11.00000 0.05 0.25
Q5 1 0.2138 0.3261 0.5621 11.00000 0.05 0.25
Q6 1 0.3246 0.2465 0.4517 11.00000 0.05 0.24
Q7 1 0.2962 0.5732 0.5403 11.00000 0.05 0.24
Q8 1 0.4806 0.4055 0.5107 11.00000 0.05 0.23
Q9 1 0.4911 0.2720 0.3128 11.00000 0.05 0.22
Q10 1 0.4975 0.2533 0.4289 11.00000 0.05 0.22
Q11 1 0.4773 0.4434 0.3139 11.00000 0.05 0.21
Q12 1 0.2190 0.3447 0.4730 11.00000 0.05 0.21
Q13 1 0.2070 0.4875 0.5723 11.00000 0.05 0.21
Q14 1 0.2782 0.7213 0.6691 11.00000 0.05 0.19
Q15 1 0.1205 0.3821 0.6010 11.00000 0.05 0.19
Q16 1 0.3581 0.7997 0.7184 11.00000 0.05 0.19
Q17 1 0.1297 0.4156 0.4900 11.00000 0.05 0.19
Q18 1 0.3980 0.3194 0.4860 11.00000 0.05 0.18
Q19 1 0.4952 0.6372 0.4645 11.00000 0.05 0.18
Q20 1 0.4303 -0.0090 0.4649 11.00000 0.05 0.18
;
_shelx_res_checksum 7430
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'x+1/2, -y, z'
'-x+1/2, y, z+1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
F F18 0.48474(6) 0.5004(2) 0.4401(3) 0.0471(5) Uani d 1 . .
O O17 0.35348(8) 0.7103(2) 0.6361(3) 0.0358(4) Uani d 1 . .
N N20 0.32550(7) 0.3449(2) 0.5164(3) 0.0229(4) Uani d 1 . .
N N19 0.37924(7) 0.3898(3) 0.5197(3) 0.0254(4) Uani d 1 . .
H H21 0.390131 0.49963 0.557997 0.03 Uiso calc 1 . .
C C1 0.41885(9) 0.2586(3) 0.4609(3) 0.0250(5) Uani d 1 . .
C C2 0.40634(9) 0.0731(3) 0.4374(3) 0.0283(5) Uani d 1 . .
H H22 0.369604 0.028034 0.466435 0.034 Uiso calc 1 . .
C C7 0.28796(9) 0.4712(3) 0.5655(3) 0.0226(4) Uani d 1 . .
C C4 0.50093(12) 0.0177(4) 0.3267(4) 0.0345(5) Uani d 1 . .
H H24 0.528484 -0.06543 0.279197 0.041 Uiso calc 1 . .
C C9 0.25667(12) 0.7806(3) 0.6729(3) 0.0314(5) Uani d 1 . .
H H27 0.265059 0.901517 0.71613 0.038 Uiso calc 1 . .
C C14 0.15584(10) 0.1955(3) 0.4718(4) 0.0334(5) Uani d 1 . .
H H26 0.145461 0.075616 0.430408 0.04 Uiso calc 1 . .
C C13 0.21242(9) 0.2415(3) 0.4897(3) 0.0269(5) Uani d 1 . .
H H28 0.240645 0.152688 0.460149 0.032 Uiso calc 1 . .
C C10 0.20214(11) 0.7276(3) 0.6565(4) 0.0326(5) Uani d 1 . .
H H29 0.173167 0.813258 0.687556 0.039 Uiso calc 1 . .
C C3 0.44734(11) -0.0462(3) 0.3718(4) 0.0328(5) Uani d 1 . .
H H23 0.438708 -0.173543 0.357452 0.039 Uiso calc 1 . .
C C8 0.30254(10) 0.6573(3) 0.6261(3) 0.0273(5) Uani d 1 . .
C C11 0.18627(10) 0.5474(3) 0.5941(3) 0.0273(5) Uani d 1 . .
C C6 0.47345(10) 0.3187(3) 0.4186(4) 0.0304(5) Uani d 1 . .
C C12 0.22854(9) 0.4166(3) 0.5506(3) 0.0238(5) Uani d 1 . .
C C15 0.11400(10) 0.3244(4) 0.5144(4) 0.0364(6) Uani d 1 . .
H H30 0.07518 0.292542 0.501361 0.044 Uiso calc 1 . .
C C16 0.12878(10) 0.4969(4) 0.5748(4) 0.0342(6) Uani d 1 . .
H H31 0.100014 0.5839 0.604186 0.041 Uiso calc 1 . .
C C5 0.51440(10) 0.2024(4) 0.3506(4) 0.0354(6) Uani d 1 . .
H H25 0.551065 0.247445 0.320609 0.042 Uiso calc 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
F18 0.0293(7) 0.0333(7) 0.0787(14) -0.0085(6) 0.0016(8) -0.0001(8)
O17 0.0368(9) 0.0295(8) 0.0412(10) -0.0081(7) -0.0010(8) 0.0006(8)
N20 0.0227(8) 0.0246(8) 0.0213(9) -0.0011(7) -0.0005(7) 0.0043(7)
N19 0.0219(8) 0.0250(8) 0.0293(10) -0.0030(7) -0.0011(7) 0.0023(8)
C1 0.0235(9) 0.0278(10) 0.0236(10) 0.0007(8) -0.0017(8) 0.0047(8)
C2 0.0270(10) 0.0285(10) 0.0294(12) -0.0016(8) -0.0028(9) 0.0031(10)
C7 0.0278(10) 0.0228(10) 0.0173(9) 0.0007(8) -0.0001(8) 0.0046(8)
C4 0.0323(11) 0.0434(14) 0.0277(12) 0.0092(10) 0.0011(10) 0.0002(10)
C9 0.0452(14) 0.0251(9) 0.0239(12) 0.0024(10) 0.0028(10) 0.0007(9)
C14 0.0314(11) 0.0358(12) 0.0332(14) -0.0046(9) -0.0002(10) 0.0053(10)
C13 0.0249(9) 0.0284(11) 0.0276(13) 0.0024(8) 0.0011(9) 0.0033(9)
C10 0.0412(13) 0.0333(12) 0.0233(12) 0.0114(10) 0.0048(10) 0.0022(10)
C3 0.0360(12) 0.0292(11) 0.0334(13) 0.0009(9) -0.0015(11) -0.0003(10)
C8 0.0345(11) 0.0271(10) 0.0204(11) -0.0010(9) -0.0003(9) 0.0042(9)
C11 0.0297(11) 0.0323(11) 0.0200(11) 0.0077(9) 0.0030(8) 0.0066(9)
C6 0.0253(10) 0.0307(11) 0.0352(13) -0.0034(9) -0.0027(10) 0.0042(10)
C12 0.0262(10) 0.0289(11) 0.0161(10) 0.0023(8) 0.0013(8) 0.0059(8)
C15 0.0242(10) 0.0528(14) 0.0322(14) 0.0008(10) -0.0003(10) 0.0070(12)
C16 0.0266(11) 0.0464(14) 0.0296(13) 0.0115(10) 0.0040(10) 0.0066(11)
C5 0.0240(10) 0.0462(14) 0.0358(14) 0.0008(10) 0.0017(10) 0.0064(12)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.006 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_diffrn_standard_refln_index_h
_diffrn_standard_refln_index_k
_diffrn_standard_refln_index_l
0 0 0
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
N19 N20 C7 . . 118.22(18) ?
N20 N19 C1 . . 118.27(18) ?
N20 N19 H21 . . 120.9 ?
C1 N19 H21 . . 120.9 ?
C2 C1 C6 . . 118.2(2) ?
C2 C1 N19 . . 123.5(2) ?
C6 C1 N19 . . 118.2(2) ?
C3 C2 C1 . . 119.9(2) ?
C3 C2 H22 . . 120.1 ?
C1 C2 H22 . . 120.1 ?
N20 C7 C8 . . 124.1(2) ?
N20 C7 C12 . . 115.91(19) ?
C8 C7 C12 . . 119.92(19) ?
C5 C4 C3 . . 120.2(2) ?
C5 C4 H24 . . 119.9 ?
C3 C4 H24 . . 119.9 ?
C10 C9 C8 . . 121.3(2) ?
C10 C9 H27 . . 119.3 ?
C8 C9 H27 . . 119.3 ?
C13 C14 C15 . . 120.2(2) ?
C13 C14 H26 . . 119.9 ?
C15 C14 H26 . . 119.9 ?
C14 C13 C12 . . 120.8(2) ?
C14 C13 H28 . . 119.6 ?
C12 C13 H28 . . 119.6 ?
C9 C10 C11 . . 122.5(2) ?
C9 C10 H29 . . 118.7 ?
C11 C10 H29 . . 118.7 ?
C2 C3 C4 . . 120.8(2) ?
C2 C3 H23 . . 119.6 ?
C4 C3 H23 . . 119.6 ?
O17 C8 C9 . . 120.8(2) ?
O17 C8 C7 . . 121.5(2) ?
C9 C8 C7 . . 117.7(2) ?
C12 C11 C16 . . 119.0(2) ?
C12 C11 C10 . . 119.8(2) ?
C16 C11 C10 . . 121.2(2) ?
F18 C6 C5 . . 120.0(2) ?
F18 C6 C1 . . 117.4(2) ?
C5 C6 C1 . . 122.6(2) ?
C13 C12 C11 . . 119.1(2) ?
C13 C12 C7 . . 122.07(19) ?
C11 C12 C7 . . 118.8(2) ?
C16 C15 C14 . . 120.1(2) ?
C16 C15 H30 . . 120 ?
C14 C15 H30 . . 120 ?
C15 C16 C11 . . 120.8(2) ?
C15 C16 H31 . . 119.6 ?
C11 C16 H31 . . 119.6 ?
C6 C5 C4 . . 118.3(2) ?
C6 C5 H25 . . 120.8 ?
C4 C5 H25 . . 120.8 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
F18 C6 . 1.351(3) ?
O17 C8 . 1.264(3) ?
N20 N19 . 1.310(2) ?
N20 C7 . 1.322(3) ?
N19 C1 . 1.399(3) ?
N19 H21 . 0.88 ?
C1 C2 . 1.386(3) ?
C1 C6 . 1.394(3) ?
C2 C3 . 1.381(3) ?
C2 H22 . 0.95 ?
C7 C8 . 1.457(3) ?
C7 C12 . 1.462(3) ?
C4 C5 . 1.385(4) ?
C4 C3 . 1.386(4) ?
C4 H24 . 0.95 ?
C9 C10 . 1.349(4) ?
C9 C8 . 1.444(3) ?
C9 H27 . 0.95 ?
C14 C13 . 1.383(3) ?
C14 C15 . 1.393(4) ?
C14 H26 . 0.95 ?
C13 C12 . 1.395(3) ?
C13 H28 . 0.95 ?
C10 C11 . 1.430(4) ?
C10 H29 . 0.95 ?
C3 H23 . 0.95 ?
C11 C12 . 1.411(3) ?
C11 C16 . 1.413(3) ?
C6 C5 . 1.373(4) ?
C15 C16 . 1.368(4) ?
C15 H30 . 0.95 ?
C16 H31 . 0.95 ?
C5 H25 . 0.95 ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
N19 H21 O17 . 0.88 1.84 2.541(3) 135 yes
C2 H22 O17 1_545 0.95 2.63 3.242(3) 122.3 yes
C5 H25 O17 2_664 0.95 2.64 3.539(3) 159.1 yes
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
C7 N20 N19 C1 . . . . -177.5(2) ?
N20 N19 C1 C2 . . . . -14.4(3) ?
N20 N19 C1 C6 . . . . 163.7(2) ?
C6 C1 C2 C3 . . . . -0.7(4) ?
N19 C1 C2 C3 . . . . 177.4(2) ?
N19 N20 C7 C8 . . . . -1.0(3) ?
N19 N20 C7 C12 . . . . 177.15(19) ?
C15 C14 C13 C12 . . . . 0.1(4) ?
C8 C9 C10 C11 . . . . 0.6(4) ?
C1 C2 C3 C4 . . . . -0.8(4) ?
C5 C4 C3 C2 . . . . 1.3(4) ?
C10 C9 C8 O17 . . . . 177.6(2) ?
C10 C9 C8 C7 . . . . -1.7(3) ?
N20 C7 C8 O17 . . . . -0.2(4) ?
C12 C7 C8 O17 . . . . -178.3(2) ?
N20 C7 C8 C9 . . . . 179.2(2) ?
C12 C7 C8 C9 . . . . 1.1(3) ?
C9 C10 C11 C12 . . . . 1.2(4) ?
C9 C10 C11 C16 . . . . -178.7(2) ?
C2 C1 C6 F18 . . . . 179.2(2) ?
N19 C1 C6 F18 . . . . 1.0(3) ?
C2 C1 C6 C5 . . . . 1.8(4) ?
N19 C1 C6 C5 . . . . -176.5(2) ?
C14 C13 C12 C11 . . . . 0.0(3) ?
C14 C13 C12 C7 . . . . -178.1(2) ?
C16 C11 C12 C13 . . . . 0.0(3) ?
C10 C11 C12 C13 . . . . -179.9(2) ?
C16 C11 C12 C7 . . . . 178.2(2) ?
C10 C11 C12 C7 . . . . -1.7(3) ?
N20 C7 C12 C13 . . . . 0.5(3) ?
C8 C7 C12 C13 . . . . 178.7(2) ?
N20 C7 C12 C11 . . . . -177.6(2) ?
C8 C7 C12 C11 . . . . 0.6(3) ?
C13 C14 C15 C16 . . . . -0.3(4) ?
C14 C15 C16 C11 . . . . 0.3(4) ?
C12 C11 C16 C15 . . . . -0.2(4) ?
C10 C11 C16 C15 . . . . 179.7(2) ?
F18 C6 C5 C4 . . . . -178.6(3) ?
C1 C6 C5 C4 . . . . -1.3(4) ?
C3 C4 C5 C6 . . . . -0.3(4) ?