#------------------------------------------------------------------------------
#$Date: 2024-02-05 13:08:23 +0100 (Mon, 05 Feb 2024) $
#$Revision: 289692 $
#$URL: svn://www.crystallography.net/cod/cif/2/02/29/2022981.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2022981
loop_
_publ_author_name
'Mammadova, Gunay Z.'
'Atioğlu, Zeliha'
'Akkurt, Mehmet'
'Grigoriev, Mikhail S.'
'Volchkov, Nikita S.'
'Azizova, Asmet N.'
'Bhattarai, Ajaya'
'Antonova, Alexandra S.'
_publ_section_title
;
Crystal structure of
[1,3-bis-(2,4,6-tri-methyl-phen-yl)imidazolidin-2-yl-idene]di-chlorido-(2-{[(2-methoxyeth-yl)(meth-yl)amino]-meth-yl}benzyl-idene)ruth-en-ium.
;
_journal_issue 'Pt 1'
_journal_name_full
'Acta crystallographica. Section E, Crystallographic communications'
_journal_page_first 50
_journal_page_last 53
_journal_paper_doi 10.1107/S2056989023010381
_journal_volume 80
_journal_year 2024
_chemical_formula_iupac '[Ru Cl2 (C21 H26 N2) (C12 H17 N O)]'
_chemical_formula_moiety 'C33 H43 Cl2 N3 O Ru'
_chemical_formula_sum 'C33 H43 Cl2 N3 O Ru'
_chemical_formula_weight 669.67
_chemical_name_systematic
'[1,3-Bis(2,4,6-trimethylphenyl)imidazolidin-2-ylidene]dichlorido(2-{[(2-methoxyethyl)(methyl)amino]methyl}benzylidene)ruthenium'
_space_group_crystal_system monoclinic
_space_group_IT_number 14
_space_group_name_Hall '-P 2yn'
_space_group_name_H-M_alt 'P 1 21/n 1'
_atom_sites_solution_hydrogens geom
_audit_creation_method SHELXL-2018/3
_cell_angle_alpha 90
_cell_angle_beta 102.553(4)
_cell_angle_gamma 90
_cell_formula_units_Z 4
_cell_length_a 13.6801(13)
_cell_length_b 10.7078(11)
_cell_length_c 22.035(2)
_cell_measurement_reflns_used 9880
_cell_measurement_temperature 100(2)
_cell_measurement_theta_max 29.84
_cell_measurement_theta_min 2.43
_cell_volume 3150.6(5)
_computing_cell_refinement
;
SAINT (Bruker, 2018)
;
_computing_data_collection
;
APEX3 (Bruker, 2018)
;
_computing_data_reduction
;
SAINT (Bruker, 2018)
;
_computing_molecular_graphics
;
ORTEP-3 for Windows (Farrugia, 2012)
;
_computing_publication_material
;
PLATON (Spek, 2020)
;
_computing_structure_refinement
;
SHELXL2016/6 (Sheldrick, 2015b)
;
_computing_structure_solution
;
SHELXT2016/6 (Sheldrick, 2015a)
;
_diffrn_ambient_temperature 100(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device_type
'Bruker Kappa APEXII area-detector diffractometer'
_diffrn_measurement_method '\f and \w scans'
_diffrn_radiation_type MoK\a
_diffrn_radiation_wavelength 0.71073
_diffrn_reflns_av_R_equivalents 0.0490
_diffrn_reflns_av_unetI/netI 0.0392
_diffrn_reflns_limit_h_max 18
_diffrn_reflns_limit_h_min -19
_diffrn_reflns_limit_k_max 15
_diffrn_reflns_limit_k_min -15
_diffrn_reflns_limit_l_max 31
_diffrn_reflns_limit_l_min -31
_diffrn_reflns_number 54060
_diffrn_reflns_theta_full 25.242
_diffrn_reflns_theta_max 30.173
_diffrn_reflns_theta_min 2.684
_exptl_absorpt_coefficient_mu 0.697
_exptl_absorpt_correction_T_max 0.746
_exptl_absorpt_correction_T_min 0.679
_exptl_absorpt_correction_type multi-scan
_exptl_absorpt_process_details
;
(SADABS; Krause et al., 2015)
;
_exptl_crystal_colour 'dark green'
_exptl_crystal_density_diffrn 1.412
_exptl_crystal_description bulk
_exptl_crystal_F_000 1392
_exptl_crystal_size_max 0.400
_exptl_crystal_size_mid 0.360
_exptl_crystal_size_min 0.240
_refine_diff_density_max 0.433
_refine_diff_density_min -0.576
_refine_ls_extinction_method none
_refine_ls_goodness_of_fit_ref 1.023
_refine_ls_hydrogen_treatment constr
_refine_ls_matrix_type full
_refine_ls_number_parameters 493
_refine_ls_number_reflns 9279
_refine_ls_number_restraints 460
_refine_ls_restrained_S_all 1.010
_refine_ls_R_factor_all 0.0514
_refine_ls_R_factor_gt 0.0320
_refine_ls_shift/su_max 0.001
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0230P)^2^+2.0327P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.0634
_refine_ls_wR_factor_ref 0.0702
_reflns_number_gt 7087
_reflns_number_total 9279
_reflns_threshold_expression 'I > 2\s(I)'
_cod_data_source_file tx2079sup1.cif
_cod_data_source_block I
_cod_depositor_comments 'Adding full bibliography for 2022981.cif.'
_cod_original_sg_symbol_H-M 'P 21/n'
_cod_database_code 2022981
_cod_database_fobs_code 2022981
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min 0.768
_shelx_estimated_absorpt_t_max 0.850
_shelx_hkl_file
;
-1 0 0 0.10 0.10
1 0 0 0.20 0.30
-1 0 0 0.00 0.10
-3 0 0 8.40 2.30
3 0 0 4.80 1.80
3 0 0 2.00 1.00
-3 0 0 -0.20 1.80
-3 0 0 -1.00 1.10
-3 0 0 -0.20 1.30
-4 0 0 51.09 5.80
4 0 0 49.10 3.50
-4 0 0 60.19 4.80
4 0 0 62.69 5.00
-4 0 0 50.29 4.80
5 0 0 3.00 1.60
-5 0 0 1.00 2.20
-5 0 0 0.70 2.70
-5 0 0 6.50 2.40
-6 0 0 201.28 11.20
-6 0 0 199.98 10.70
-6 0 0 204.58 12.90
6 0 0 220.08 9.10
7 0 0 3.00 2.20
-7 0 0 1.20 3.30
-7 0 0 2.30 3.20
-7 0 0 6.40 3.50
-8 0 0 4119.79 122.79
-8 0 0 4013.60 127.79
-8 0 0 4044.90 123.79
8 0 0 4129.69 119.09
9 0 0 -0.50 2.60
-9 0 0 5.40 4.30
-9 0 0 0.00 2.90
-10 0 0 471.75 21.90
10 0 0 469.65 18.20
-10 0 0 449.95 22.70
11 0 0 0.90 2.70
-11 0 0 6.00 4.70
-11 0 0 1.00 4.50
-12 0 0 174.08 16.90
-13 0 0 -1.30 5.60
-14 0 0 334.07 22.60
-15 0 0 11.60 7.90
-16 0 0 512.35 31.20
-17 0 0 -9.10 7.50
-18 0 0 129.99 19.70
0 -1 0 0.00 0.30
0 -1 0 0.40 0.60
0 -1 0 0.00 0.30
0 -1 0 0.00 0.30
0 -1 0 0.00 0.20
0 -1 0 -0.30 0.10
2 -1 0 2330.27 69.29
-2 -1 0 2353.56 70.09
2 -1 0 2439.06 69.79
2 -1 0 2424.86 69.99
-2 -1 0 2424.66 71.29
2 1 0 2411.86 69.89
3 -1 0 91.49 3.40
3 -1 0 78.49 5.10
-3 -1 0 88.09 5.70
3 -1 0 94.69 5.20
-3 -1 0 93.59 5.00
-3 -1 0 97.69 6.60
3 -1 0 90.49 4.60
-3 1 0 84.29 6.60
3 1 0 88.79 5.60
3 1 0 92.89 4.90
-3 1 0 90.69 5.60
4 -1 0 7.90 2.50
-4 -1 0 8.30 3.20
-4 -1 0 5.20 2.50
4 -1 0 3.70 1.70
4 -1 0 6.80 2.30
-4 -1 0 3.70 1.90
-4 1 0 2.10 2.20
-4 1 0 4.10 2.80
4 1 0 1.70 2.00
4 1 0 8.00 1.90
5 -1 0 551.54 19.90
-5 -1 0 507.65 19.40
-5 -1 0 529.95 22.30
5 -1 0 534.85 20.20
-5 -1 0 561.74 20.90
-5 1 0 512.85 20.00
-5 1 0 533.85 20.40
5 1 0 511.25 18.10
-5 1 0 500.95 21.90
-6 -1 0 61.99 8.10
-6 -1 0 58.69 6.90
-6 -1 0 58.69 6.40
6 -1 0 52.69 6.40
6 1 0 54.89 4.60
-6 1 0 40.90 6.80
-6 1 0 45.90 5.90
-6 1 0 56.59 6.60
-7 -1 0 2429.76 75.09
-7 -1 0 2439.76 79.49
-7 -1 0 2396.26 76.39
-7 1 0 2214.18 78.19
7 1 0 2451.55 72.19
-7 1 0 2447.85 76.19
-7 1 0 2454.35 75.69
8 -1 0 34.10 4.80
-8 -1 0 39.70 7.90
-8 -1 0 59.99 7.50
-8 -1 0 48.80 7.60
8 1 0 35.00 4.70
-8 1 0 38.70 7.80
-8 1 0 47.20 7.40
-8 1 0 47.60 7.30
-9 -1 0 2072.19 67.09
9 -1 0 1957.80 60.19
-9 -1 0 2005.50 65.19
9 1 0 1944.81 60.59
-9 1 0 1907.91 65.59
-9 1 0 1897.21 64.69
10 -1 0 45.00 5.40
-10 -1 0 43.60 8.00
-10 -1 0 33.10 7.50
10 1 0 37.30 5.40
-10 1 0 57.39 8.60
-10 1 0 35.80 8.00
-11 -1 0 297.77 19.70
-11 -1 0 260.27 16.90
11 -1 0 273.37 12.80
-11 1 0 292.67 18.40
-11 1 0 274.97 17.20
11 1 0 278.87 13.20
-12 -1 0 28.00 9.00
-12 -1 0 14.10 6.70
-12 1 0 22.80 7.40
12 1 0 14.80 3.90
-12 1 0 20.20 6.70
-13 -1 0 405.56 23.70
-13 1 0 395.96 24.30
-13 1 0 397.06 22.90
-14 -1 0 30.60 9.30
-14 1 0 82.99 13.30
-15 -1 0 321.37 22.80
-15 1 0 386.46 25.70
-16 -1 0 -1.60 8.10
-16 1 0 0.80 8.40
-17 -1 0 249.18 24.30
-17 1 0 220.98 23.60
-18 -1 0 4.60 10.10
-18 1 0 5.80 8.70
0 -2 0 85.89 5.00
0 -2 0 85.79 3.50
0 -2 0 88.69 4.40
0 -2 0 88.49 4.00
1 -2 0 194.68 10.10
1 -2 0 214.78 9.30
1 -2 0 219.08 8.70
1 -2 0 203.48 7.30
1 -2 0 207.88 7.20
1 -2 0 205.08 7.80
-1 -2 0 220.08 8.20
-1 -2 0 204.88 6.70
2 -2 0 1040.10 32.70
2 -2 0 997.70 31.20
2 -2 0 987.30 31.00
2 -2 0 987.00 31.90
2 -2 0 1034.00 30.00
-2 -2 0 1018.50 32.10
2 -2 0 999.60 31.80
-2 -2 0 989.90 33.70
-2 -2 0 1012.40 34.80
2 -2 0 1078.19 30.80
2 -2 0 1047.40 31.40
-2 -2 0 1045.10 31.40
2 -2 0 1030.30 30.80
-2 -2 0 1039.90 34.00
2 2 0 1018.20 34.00
2 2 0 1013.40 32.50
3 -2 0 163.68 10.40
3 -2 0 169.48 5.80
-3 -2 0 175.48 8.70
-3 -2 0 172.28 7.10
3 -2 0 155.78 7.90
-3 -2 0 185.88 10.20
3 -2 0 169.18 6.90
3 -2 0 164.58 8.40
3 -2 0 163.68 7.70
-3 -2 0 173.18 8.30
3 -2 0 173.28 7.50
3 -2 0 171.08 7.90
-3 2 0 160.58 9.70
3 2 0 178.88 10.10
-3 2 0 168.38 9.70
3 2 0 173.78 8.40
4 -2 0 1964.80 58.99
4 -2 0 1953.70 58.59
4 -2 0 1929.71 63.89
-4 -2 0 1914.61 62.19
-4 -2 0 2009.80 58.19
4 -2 0 1947.21 56.49
-4 -2 0 1949.41 59.69
4 -2 0 1965.70 58.39
4 2 0 1943.81 58.99
-4 2 0 1931.51 60.49
-4 2 0 1858.91 61.99
-5 -2 0 17.00 3.70
-5 -2 0 24.00 3.70
5 -2 0 16.30 5.50
5 -2 0 17.30 3.00
5 -2 0 19.50 1.90
-5 -2 0 22.10 4.90
5 -2 0 19.40 3.40
5 -2 0 20.80 4.00
5 2 0 17.80 3.50
-5 2 0 26.40 5.10
-5 2 0 19.20 4.20
6 -2 0 1108.49 36.10
6 -2 0 1180.68 38.50
-6 -2 0 1115.29 37.30
6 -2 0 1163.68 44.40
-6 -2 0 1134.39 39.20
6 -2 0 1119.19 37.80
-6 -2 0 1109.49 41.70
-6 2 0 1125.19 41.60
6 2 0 1112.89 36.90
-6 2 0 1163.58 39.70
-7 -2 0 31.00 6.80
-7 -2 0 42.50 6.50
7 -2 0 25.20 5.40
7 -2 0 31.70 4.30
-7 -2 0 38.90 5.50
7 -2 0 39.10 8.40
-7 2 0 35.00 6.80
7 2 0 40.80 5.10
-7 2 0 45.80 6.90
-8 -2 0 1548.84 53.79
8 -2 0 1566.54 52.99
-8 -2 0 1505.05 56.69
-8 -2 0 1582.04 51.89
8 2 0 1517.75 49.70
-8 2 0 1534.75 56.69
-8 2 0 1602.54 53.89
-8 2 0 1599.14 54.79
-9 -2 0 89.29 9.60
-9 -2 0 96.99 10.90
9 -2 0 99.09 10.80
9 2 0 81.29 7.30
-9 2 0 101.09 11.30
-9 2 0 117.49 12.30
10 -2 0 734.03 31.50
-10 -2 0 753.12 30.20
-10 -2 0 725.33 32.10
-10 2 0 714.73 31.20
-10 2 0 709.33 31.50
10 2 0 712.43 26.80
11 -2 0 49.10 11.90
-11 -2 0 49.80 9.60
-11 -2 0 73.89 10.30
11 -2 0 65.49 6.90
11 -2 0 68.79 10.90
11 2 0 50.29 6.80
-11 2 0 61.99 10.30
-11 2 0 59.39 10.10
12 -2 0 224.28 25.40
-12 -2 0 230.58 16.30
-12 -2 0 241.98 19.00
12 -2 0 247.28 18.40
12 2 0 227.38 13.00
-12 2 0 232.58 18.00
-12 2 0 248.68 17.90
13 -2 0 54.09 14.30
-13 -2 0 45.90 10.30
13 -2 0 58.89 14.10
-13 -2 0 51.49 10.10
-13 2 0 63.29 11.50
-13 2 0 42.80 10.20
14 -2 0 255.57 29.70
-14 -2 0 233.28 18.70
-14 2 0 213.38 18.50
-14 2 0 224.48 19.30
-15 -2 0 13.80 7.50
15 -2 0 16.20 11.50
-15 2 0 14.80 8.80
-15 2 0 12.30 8.00
-16 -2 0 184.48 20.00
16 -2 0 185.78 28.50
-16 2 0 153.98 19.50
-17 -2 0 5.00 9.40
17 -2 0 6.60 13.60
-17 2 0 8.20 9.20
-18 -2 0 173.08 21.20
18 -2 0 168.78 31.70
-18 2 0 176.98 23.10
0 -3 0 1.30 1.40
0 -3 0 -0.60 1.30
0 -3 0 -0.20 1.80
0 -3 0 4.00 1.30
0 -3 0 -1.00 2.10
0 -3 0 1.70 1.60
0 -3 0 -0.90 0.90
0 -3 0 -1.90 1.80
0 -3 0 2.20 2.50
1 -3 0 1991.00 56.39
-1 -3 0 1973.50 55.49
1 -3 0 1717.93 58.49
1 -3 0 1921.11 55.99
-1 -3 0 1892.51 56.89
1 -3 0 1923.81 56.19
-1 -3 0 1932.31 58.89
1 -3 0 1970.50 55.69
1 -3 0 1978.60 57.99
-1 -3 0 1887.71 55.49
-1 -3 0 1940.31 54.29
1 -3 0 1954.30 58.79
1 -3 0 1689.13 60.49
1 -3 0 1948.51 58.19
1 3 0 1876.81 59.09
1 3 0 1921.61 60.99
2 -3 0 1126.09 35.60
-2 -3 0 1160.38 36.90
2 -3 0 1155.08 35.40
-2 -3 0 1196.28 35.70
2 -3 0 1161.28 35.10
2 -3 0 1213.48 36.60
2 -3 0 1155.58 37.70
2 -3 0 1165.18 37.00
-2 -3 0 1220.98 37.10
2 3 0 1168.98 38.30
2 3 0 1133.39 39.90
-3 -3 0 2511.85 77.09
3 -3 0 2586.64 73.79
3 -3 0 2537.85 76.89
-3 -3 0 2566.44 77.09
-3 -3 0 2679.43 80.09
3 -3 0 2541.65 75.09
3 -3 0 2568.14 75.69
-3 -3 0 2641.84 75.99
3 -3 0 2616.44 75.59
3 -3 0 2494.05 75.69
3 3 0 2498.95 80.09
3 3 0 2501.45 77.59
-3 3 0 2503.25 89.69
-4 -3 0 222.88 10.50
4 -3 0 212.58 9.90
-4 -3 0 247.38 13.50
-4 -3 0 207.08 8.50
4 -3 0 197.88 8.80
4 -3 0 200.28 9.30
4 -3 0 201.28 10.10
4 -3 0 212.68 12.20
4 -3 0 199.98 7.40
4 3 0 211.18 13.10
-4 3 0 187.98 12.20
4 3 0 209.38 11.00
5 -3 0 1586.54 49.90
5 -3 0 1604.44 48.00
-5 -3 0 1643.84 55.09
5 -3 0 1555.54 50.29
5 -3 0 1592.04 50.29
-5 -3 0 1619.74 49.00
-5 -3 0 1661.33 51.49
5 -3 0 1583.34 53.89
-5 3 0 1611.24 52.89
-5 3 0 1576.74 55.29
5 3 0 1585.44 55.29
5 3 0 1564.84 51.19
-6 -3 0 251.77 11.80
6 -3 0 279.57 13.50
-6 -3 0 274.67 16.30
6 -3 0 302.07 16.20
-6 -3 0 258.47 13.80
6 -3 0 243.58 12.30
6 -3 0 262.77 9.80
6 -3 0 261.97 12.30
6 3 0 223.58 16.00
6 3 0 273.27 13.30
-6 3 0 261.57 14.50
-6 3 0 262.97 16.10
7 -3 0 737.73 23.30
-7 -3 0 769.22 33.20
-7 -3 0 767.02 27.70
7 -3 0 762.72 33.20
7 -3 0 767.62 29.10
7 -3 0 771.52 27.30
-7 -3 0 788.72 30.10
-7 3 0 788.72 33.20
-7 3 0 752.72 30.70
7 3 0 787.82 28.50
-8 -3 0 19.20 4.80
-8 -3 0 15.60 5.60
-8 -3 0 17.40 6.40
8 -3 0 11.80 4.50
8 -3 0 17.80 4.00
8 -3 0 6.70 5.90
8 3 0 20.80 4.80
-8 3 0 16.60 5.50
-9 -3 0 550.64 25.90
9 -3 0 595.54 25.50
-9 -3 0 552.44 23.40
9 -3 0 558.74 21.70
9 -3 0 535.85 28.30
-9 3 0 541.55 26.20
9 3 0 547.35 22.80
-10 -3 0 109.39 10.90
10 -3 0 80.19 12.10
-10 -3 0 110.29 12.40
10 -3 0 90.39 11.00
-10 3 0 122.89 13.80
10 3 0 108.59 9.30
-11 -3 0 306.47 17.70
-11 -3 0 291.97 19.90
11 -3 0 297.97 19.10
11 -3 0 314.87 21.80
11 3 0 277.87 15.40
-11 3 0 275.57 19.00
-11 3 0 302.67 23.20
12 -3 0 -6.70 5.40
12 -3 0 -2.10 5.30
-12 -3 0 0.30 4.60
-12 -3 0 -4.70 5.30
-12 3 0 3.60 6.30
-12 3 0 -5.70 4.90
12 3 0 1.40 3.90
-13 -3 0 298.47 22.00
13 -3 0 246.98 20.00
13 -3 0 299.67 24.60
-13 -3 0 293.37 19.60
-13 3 0 285.47 21.00
-13 3 0 290.27 21.80
14 -3 0 112.89 18.30
-14 -3 0 141.09 15.20
14 -3 0 99.99 14.80
-14 3 0 115.29 16.00
-14 3 0 109.39 15.90
15 -3 0 182.58 20.30
-15 -3 0 219.18 18.40
15 -3 0 201.18 24.10
-15 3 0 206.38 21.30
-15 3 0 158.08 19.60
16 -3 0 0.00 8.30
-16 -3 0 -5.90 7.10
16 -3 0 5.60 8.90
-16 3 0 -0.10 7.60
-16 3 0 6.10 8.90
-17 -3 0 164.68 19.30
17 -3 0 216.78 26.80
17 -3 0 208.68 23.20
-17 3 0 162.88 21.40
18 -3 0 33.90 12.60
18 -3 0 23.80 12.40
-18 -3 0 36.20 13.00
-18 3 0 33.10 12.60
0 -4 0 2153.58 62.99
0 -4 0 2078.49 67.09
0 -4 0 2167.08 64.59
0 -4 0 2245.48 68.29
0 -4 0 2134.39 62.89
0 -4 0 2270.77 64.89
0 -4 0 2141.19 64.39
1 -4 0 780.02 28.50
1 -4 0 811.32 29.20
-1 -4 0 831.52 25.50
-1 -4 0 817.32 27.00
-1 -4 0 794.12 25.00
1 -4 0 801.22 25.90
-1 -4 0 783.22 23.80
-1 -4 0 831.42 29.60
1 -4 0 813.52 25.90
1 -4 0 834.32 25.40
1 -4 0 822.22 26.20
-1 -4 0 836.12 26.90
1 4 0 780.32 31.70
1 4 0 810.02 29.80
2 -4 0 3309.87 96.19
-2 -4 0 3294.07 94.09
-2 -4 0 3160.68 97.29
2 -4 0 3438.56 96.89
2 -4 0 3273.17 95.19
-2 -4 0 3211.08 95.49
2 -4 0 3324.07 99.39
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1 -1 9 4.50 1.70
1 -1 9 4.10 2.50
-1 -1 -9 3.90 3.10
1 -1 9 9.10 2.60
1 -1 9 1.90 3.10
1 -1 9 1.60 2.20
1 1 9 5.00 2.80
-1 1 -9 5.20 3.20
2 -1 9 102.09 7.00
-2 -1 -9 84.39 7.90
2 -1 9 95.59 6.20
2 -1 9 92.19 6.10
2 -1 9 94.69 6.90
2 -1 9 91.59 5.40
2 -1 9 102.19 7.70
-2 1 -9 98.99 7.70
2 1 9 84.79 7.50
2 1 9 89.29 6.60
2 1 9 96.69 4.90
2 1 9 96.29 6.50
3 -1 9 82.59 8.50
3 -1 9 87.49 6.50
3 -1 9 87.29 6.70
3 -1 9 93.39 5.50
3 -1 9 72.09 6.80
3 -1 9 75.49 7.10
-3 -1 -9 82.19 9.00
-3 -1 -9 86.19 7.30
3 1 9 84.29 6.90
3 1 9 78.49 5.90
3 1 9 77.69 5.30
-3 1 -9 90.09 8.50
3 1 9 88.89 10.60
3 1 9 67.89 8.00
-4 -1 -9 531.05 24.40
4 -1 9 541.75 22.20
-4 -1 -9 571.94 22.70
4 -1 9 558.64 18.70
4 -1 9 556.94 22.20
4 -1 9 570.14 22.70
4 -1 9 594.94 24.90
4 1 9 594.74 21.20
4 1 9 568.74 19.90
4 1 9 594.74 23.20
4 1 9 550.94 25.00
4 1 9 550.84 25.90
5 -1 9 137.99 10.70
-5 -1 -9 160.88 10.70
5 -1 9 151.48 12.30
-5 -1 -9 149.99 11.90
-5 1 -9 140.99 11.10
5 1 9 161.68 13.20
5 1 9 144.59 7.40
5 1 9 170.58 11.50
6 -1 9 690.43 28.00
6 -1 9 644.94 30.00
-6 -1 -9 687.23 30.00
-6 -1 -9 639.24 26.90
6 -1 9 651.23 26.80
6 1 9 615.54 29.80
-6 1 -9 652.33 28.00
6 1 9 633.14 27.40
-7 -1 -9 158.18 15.60
7 -1 9 139.79 8.30
-7 -1 -9 167.08 12.80
7 -1 9 146.09 12.00
7 -1 9 166.28 13.00
7 -1 9 148.19 15.40
7 1 9 172.08 15.50
-7 1 -9 146.39 12.70
7 1 9 146.29 12.60
-8 -1 -9 765.72 41.30
8 -1 9 833.82 33.80
8 -1 9 821.42 34.70
-8 -1 -9 794.32 33.20
8 -1 9 827.02 37.60
8 1 9 787.12 34.60
-8 1 -9 777.82 34.10
8 1 9 868.11 38.90
9 -1 9 29.50 9.10
9 -1 9 8.00 5.50
-9 -1 -9 0.70 5.10
9 -1 9 9.60 5.90
9 1 9 5.00 7.10
9 1 9 5.80 5.50
-9 1 -9 -0.70 5.20
-10 -1 -9 142.09 14.70
10 -1 9 133.09 15.10
10 -1 9 110.69 14.20
10 -1 9 167.98 19.70
-10 1 -9 133.39 14.90
10 1 9 139.69 17.60
10 1 9 175.98 18.50
11 -1 9 15.80 8.20
-11 -1 -9 5.40 7.10
11 -1 9 10.00 7.30
11 -1 9 14.10 7.10
11 1 9 24.70 9.20
11 1 9 4.20 7.40
-11 1 -9 4.50 6.40
12 -1 9 221.38 24.80
-12 -1 -9 191.78 18.90
12 -1 9 185.98 20.40
12 -1 9 181.48 19.10
12 1 9 163.28 21.70
-12 1 -9 187.28 19.30
12 1 9 208.28 22.10
13 -1 9 5.10 8.10
-13 -1 -9 8.30 8.80
13 -1 9 -2.60 7.00
13 -1 9 -6.10 9.00
13 1 9 9.20 9.20
13 1 9 9.40 9.00
-13 1 -9 14.50 9.10
14 -1 9 322.57 25.20
-14 -1 -9 312.97 23.20
14 -1 9 331.47 27.40
-14 1 -9 319.57 24.10
14 1 9 287.37 29.10
15 -1 9 5.60 9.00
15 -1 9 -5.80 8.90
-15 -1 -9 -5.90 8.30
-15 1 -9 -2.80 8.30
15 1 9 -0.80 9.90
-16 -1 -9 315.77 25.90
16 -1 9 282.77 30.50
16 -1 9 262.57 26.90
16 1 9 288.47 30.90
-16 1 -9 269.17 27.40
-19 -2 9 -3.40 9.80
-19 -2 9 5.40 11.10
-19 2 9 -0.40 9.20
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-18 -2 9 20.60 11.40
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-17 -2 9 -1.50 7.40
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16 -2 -9 3.90 6.40
-16 -2 9 11.90 8.10
-16 -2 9 2.30 8.10
16 2 -9 5.60 6.20
-16 2 9 14.80 9.40
-16 2 9 12.00 8.40
-15 -2 9 -6.90 7.50
15 -2 -9 -5.00 5.70
-15 -2 9 1.10 6.60
-15 2 9 1.40 7.40
15 2 -9 11.70 7.20
-15 2 9 17.50 7.80
-14 -2 9 5.10 8.00
14 -2 -9 6.40 6.30
-14 2 9 6.90 7.30
14 2 -9 8.10 6.30
-14 2 9 3.50 6.30
13 -2 -9 22.60 7.80
-13 -2 9 38.00 10.30
13 2 -9 26.30 8.30
-13 2 9 23.90 7.90
-13 2 9 7.90 7.60
-12 -2 9 56.69 10.70
-12 -2 9 53.99 6.80
12 -2 -9 46.20 9.30
-12 2 9 46.50 9.40
12 2 -9 38.30 9.20
-11 -2 9 48.70 10.40
-11 -2 9 51.09 6.20
11 2 -9 35.00 8.20
-11 2 9 27.30 7.60
-10 -2 9 4.70 3.00
-10 -2 9 7.60 5.90
-10 -2 9 12.70 5.20
-10 2 9 6.10 4.40
-10 2 9 1.50 4.20
10 2 -9 16.20 6.00
-9 -2 9 345.67 14.00
-9 -2 9 330.87 19.90
-9 -2 9 333.57 18.80
9 -2 -9 348.67 14.10
9 2 -9 316.97 19.20
-9 2 9 347.47 18.50
-9 2 9 338.57 19.80
-8 -2 9 15.80 3.30
-8 -2 9 30.80 6.70
-8 -2 9 16.10 4.70
-8 -2 9 26.00 5.80
8 -2 -9 23.50 4.00
-8 2 9 16.50 5.60
8 2 -9 18.30 5.80
-8 2 9 12.70 4.60
-8 2 9 16.30 5.20
-7 -2 9 12.10 4.70
-7 -2 9 18.20 4.40
7 -2 -9 18.30 3.70
-7 -2 9 18.00 3.20
7 -2 -9 18.70 5.60
-7 -2 9 16.20 4.50
7 2 -9 9.40 4.30
7 2 -9 14.40 4.40
-7 2 9 15.80 5.10
-7 2 9 22.00 6.00
-6 -2 9 32.10 6.00
-6 -2 9 45.20 5.80
-6 -2 9 47.70 6.30
6 -2 -9 45.20 5.40
6 -2 -9 32.90 6.50
-6 -2 9 51.99 4.70
-6 -2 9 32.50 5.40
6 -2 -9 37.20 6.10
-6 2 9 49.10 6.60
-6 2 9 33.00 6.60
6 2 -9 45.20 7.60
-6 2 9 40.40 6.70
6 2 -9 48.60 6.70
5 -2 -9 133.69 9.80
5 -2 -9 118.99 10.10
-5 -2 9 144.09 9.30
-5 -2 9 124.69 9.80
-5 -2 9 140.29 9.40
5 -2 -9 130.09 8.50
-5 -2 9 134.29 8.10
5 2 -9 150.38 10.90
-5 2 9 123.19 8.80
5 2 -9 123.59 9.30
-5 2 9 128.59 10.80
-4 -2 9 472.15 19.00
-4 -2 9 503.35 19.40
-4 -2 9 484.95 17.10
-4 -2 9 467.05 17.80
-4 -2 9 439.36 20.10
-4 -2 9 471.15 19.70
4 -2 -9 438.56 20.20
4 -2 -9 468.65 19.00
4 2 -9 471.95 19.80
-4 2 9 481.95 18.90
-4 2 9 453.95 23.90
-3 -2 9 757.02 24.50
3 -2 -9 794.32 28.00
3 -2 -9 788.32 29.30
-3 -2 9 746.23 25.20
-3 -2 9 779.42 26.90
-3 -2 9 820.72 29.50
-3 -2 9 733.33 26.80
-3 -2 9 758.82 28.20
3 2 -9 725.23 28.20
-3 2 9 771.52 29.50
-3 2 9 797.22 26.90
-2 -2 9 40.40 2.90
2 -2 -9 58.49 7.10
2 -2 -9 50.09 5.00
-2 -2 9 45.20 5.10
2 -2 -9 44.30 5.80
-2 -2 9 42.00 5.70
-2 -2 9 42.40 3.80
-2 -2 9 27.90 5.00
-2 -2 9 36.10 4.40
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1 -2 -9 626.04 22.30
-1 -2 9 598.34 20.00
-1 -2 9 606.04 21.20
-1 -2 9 606.44 21.30
-1 -2 9 631.54 24.30
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0 -2 9 49.60 3.90
0 -2 9 52.09 6.70
0 -2 9 52.59 4.80
0 -2 -9 44.20 5.40
0 -2 9 50.79 4.50
0 -2 9 53.09 4.50
0 -2 9 53.19 5.70
0 -2 9 54.69 4.50
0 2 9 50.59 6.10
1 -2 9 589.24 20.90
1 -2 9 580.04 20.40
1 -2 9 594.44 21.90
1 -2 9 587.84 20.60
1 -2 9 578.44 24.40
-1 -2 -9 591.54 23.00
1 -2 9 593.04 20.70
1 2 9 592.34 22.70
1 2 9 620.24 21.20
2 -2 9 6.10 2.30
2 -2 9 6.00 2.80
-2 -2 -9 2.50 3.10
2 -2 9 1.00 3.50
2 -2 9 10.20 2.90
2 -2 9 6.10 2.30
2 -2 9 4.10 2.90
2 2 9 5.20 2.60
2 2 9 6.40 3.10
3 -2 9 30.60 4.30
-3 -2 -9 26.30 4.60
3 -2 9 30.30 5.00
-3 -2 -9 22.00 5.10
3 -2 9 27.10 4.50
3 -2 9 25.40 4.00
3 -2 9 29.70 5.60
3 2 9 19.60 4.00
3 2 9 23.60 4.70
3 2 9 24.00 5.60
3 2 9 28.70 4.40
4 -2 9 8.90 3.30
-4 -2 -9 12.50 4.20
4 -2 9 1.40 3.50
4 -2 9 5.60 3.30
-4 -2 -9 11.30 4.90
-4 2 -9 4.20 4.20
4 2 9 6.40 3.30
4 2 9 8.60 4.60
4 2 9 10.80 3.30
4 2 9 2.20 3.30
5 -2 9 770.02 28.00
-5 -2 -9 763.22 31.60
5 -2 9 748.53 29.50
5 -2 9 751.22 23.60
5 -2 9 751.72 23.50
5 -2 9 713.33 27.80
5 -2 9 734.03 31.80
-5 -2 -9 755.52 28.20
5 2 9 767.82 30.50
5 2 9 729.73 28.50
5 2 9 786.12 26.30
-5 2 -9 750.32 30.60
5 2 9 747.33 32.50
6 -2 9 251.27 17.20
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6 -2 9 248.48 15.30
6 -2 9 237.78 13.60
-6 -2 -9 236.38 13.80
6 -2 9 224.78 12.90
6 -2 9 225.88 10.90
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6 2 9 236.58 15.30
6 2 9 219.58 13.90
6 2 9 251.17 17.80
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7 -2 9 510.85 24.40
7 -2 9 464.45 25.90
-7 -2 -9 547.35 23.10
7 -2 9 479.75 17.80
7 -2 9 457.55 21.80
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-7 2 -9 466.75 24.10
7 2 9 491.35 24.60
7 2 9 464.45 26.30
8 -2 9 22.80 6.20
-8 -2 -9 28.20 8.40
-8 -2 -9 28.20 6.90
8 -2 9 20.20 6.80
8 -2 9 33.50 9.30
8 2 9 12.30 6.20
8 2 9 18.20 7.10
8 2 9 14.40 7.30
-8 2 -9 34.60 8.20
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9 -2 9 561.14 31.00
-9 -2 -9 487.45 24.60
9 -2 9 534.25 27.90
9 -2 9 519.65 25.40
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9 2 9 494.35 30.00
9 2 9 535.35 28.30
10 -2 9 312.87 24.10
-10 -2 -9 320.57 23.40
10 -2 9 295.47 21.40
10 -2 9 296.57 19.30
-10 -2 -9 317.97 19.80
10 2 9 297.67 21.90
10 2 9 336.17 24.90
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11 -2 9 179.88 19.00
11 -2 9 159.58 19.50
11 -2 9 185.28 18.20
-11 -2 -9 189.48 17.90
-11 -2 -9 181.38 21.70
11 2 9 179.08 21.90
11 2 9 240.68 23.00
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12 -2 9 9.60 8.90
12 -2 9 7.00 8.40
-12 -2 -9 21.50 8.70
12 -2 9 16.20 7.40
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12 2 9 3.30 7.40
13 -2 9 280.17 21.90
-13 -2 -9 255.07 20.80
13 -2 9 273.17 26.90
13 -2 9 280.77 32.00
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14 -2 9 31.30 12.10
14 -2 9 42.40 12.20
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15 -2 9 225.98 26.90
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15 -2 9 187.88 22.00
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16 -3 -9 4.80 7.20
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15 -3 -9 75.39 12.70
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14 -3 -9 46.00 9.90
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8 -3 -9 263.77 16.70
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8 -3 -9 290.57 15.80
8 -3 -9 264.27 12.20
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7 -3 -9 -0.50 4.50
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6 -3 -9 6.80 3.10
6 -3 -9 6.10 4.50
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5 -3 -9 349.67 17.40
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5 -3 -9 354.26 18.50
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5 -3 -9 350.56 15.30
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5 3 -9 392.66 17.70
4 -3 -9 182.38 10.60
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4 -3 -9 167.18 14.20
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4 3 -9 197.58 11.90
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3 -3 -9 30.90 6.10
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3 3 -9 28.80 5.50
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2 -3 -9 743.13 25.20
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-2 -3 9 764.12 26.10
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2 -3 -9 760.82 29.80
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1 -3 -9 90.49 6.50
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0 -3 9 450.35 15.40
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0 -3 9 438.46 15.40
0 -3 9 452.15 19.70
0 -3 9 369.96 17.70
0 -3 9 440.46 17.40
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1 -3 9 7.00 2.10
1 -3 9 4.80 2.90
1 -3 9 10.00 4.10
-1 -3 -9 2.20 3.10
1 -3 9 14.00 3.20
1 -3 9 6.00 2.90
1 -3 9 11.10 2.30
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2 -3 9 456.45 19.80
2 -3 9 447.16 16.40
2 -3 9 450.45 18.50
2 -3 9 466.45 16.50
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2 3 9 455.25 19.40
3 -3 9 60.79 5.10
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3 -3 9 63.19 8.00
3 -3 9 72.09 7.40
3 -3 9 60.79 5.20
3 3 9 62.69 7.00
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4 -3 9 613.04 27.40
4 -3 9 643.24 25.80
4 -3 9 633.04 22.90
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4 3 9 644.14 25.70
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5 -3 9 85.39 10.70
5 -3 9 87.49 7.50
5 -3 9 84.59 6.00
5 -3 9 85.99 9.70
5 -3 9 87.89 7.30
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5 3 9 81.29 9.30
5 3 9 86.09 8.30
5 3 9 86.59 10.20
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6 -3 9 181.88 11.40
6 -3 9 184.28 13.70
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6 -3 9 172.98 7.70
6 -3 9 174.18 14.80
6 -3 9 151.38 10.50
6 3 9 177.18 12.80
6 3 9 168.18 15.30
6 3 9 170.08 13.50
7 -3 9 23.70 3.90
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7 -3 9 14.00 4.80
7 -3 9 16.00 7.20
7 -3 9 26.50 7.10
7 -3 9 26.00 5.50
7 3 9 23.10 6.60
7 3 9 19.40 7.60
7 3 9 19.10 6.30
8 -3 9 615.54 33.00
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8 -3 9 647.64 27.70
8 -3 9 690.23 31.40
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8 3 9 664.93 34.70
8 3 9 657.73 30.70
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9 -3 9 198.48 16.80
9 -3 9 197.18 14.70
9 -3 9 203.08 20.90
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9 3 9 184.38 18.70
9 3 9 203.68 16.20
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10 -3 9 310.37 22.20
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10 -3 9 327.57 25.00
10 -3 9 302.77 19.30
-10 -3 -9 324.17 23.50
10 3 9 294.67 21.70
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10 3 9 326.37 21.90
10 3 9 304.47 24.50
-11 -3 -9 13.70 7.30
-11 -3 -9 10.60 8.70
11 -3 9 1.10 6.40
11 -3 9 9.70 7.30
11 -3 9 0.80 7.10
-11 3 -9 20.70 8.60
11 3 9 2.00 6.40
11 3 9 10.90 9.10
11 3 9 2.50 7.30
12 -3 9 103.19 15.90
12 -3 9 82.19 15.60
12 -3 9 95.29 14.30
-12 -3 -9 120.79 14.30
-12 -3 -9 92.19 15.50
12 3 9 109.89 16.70
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3 -4 9 1024.20 39.10
3 -4 9 1041.60 32.60
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4 -1 -31 59.59 16.70
-4 -1 31 98.79 20.70
4 1 -31 116.69 21.20
-4 1 31 81.79 20.40
-4 1 31 80.09 17.30
-3 -1 31 42.30 13.20
-3 1 31 2.00 9.90
0 0 0 0.00 0.00
;
_shelx_hkl_checksum 27286
_shelx_res_file
;
TITL ES-tx2079
shelx.res
created by SHELXL-2018/3 at 16:20:49 on 11-Dec-2023
CELL 0.71073 13.6801 10.7078 22.0350 90.000 102.553 90.000
ZERR 4.00 0.0013 0.0011 0.0020 0.000 0.004 0.000
LATT 1
SYMM 1/2 - X, 1/2 + Y, 1/2 - Z
SFAC C H N O CL RU
UNIT 132 172 12 4 8 4
MERG 2
OMIT 0 0 2
OMIT 1 0 1
OMIT 0 1 1
OMIT -1 0 1
OMIT -1 1 2
BOND $H $H
SADI 0.01 RU1 Cl2 RU1 CL2'
EADP CL2 CL2'
EADP C31 C31'
SADI 0.020 Ru1 N2 Ru1 N2'
SIMU 0.01 N2 > C35'
EQIV $1 -x+3/2, y-1/2, -z+1/2
HTAB C4 Cl1_$1
HTAB C5 Cl1_$1
HTAB C24 Cl2
EQIV $2 -x+5/2, y+1/2, -z+1/2
HTAB C24 Cl2_$2
HTAB C33 Cl2
HTAB C34 Cl1
HTAB C24' Cl1
HTAB C32' Cl2'
HTAB C32' Cl2'_$2
HTAB C4 Cl1_$1
HTAB C5 Cl1_$1
HTAB C24 Cl2
HTAB C24 Cl2_$2
HTAB C33 Cl2
HTAB C34 Cl1
HTAB C24' Cl1
HTAB C32' Cl2'
HTAB C32' Cl2'_$2
FMAP 2
PLAN 15
SIZE 0.240 0.360 0.400
ACTA
BOND $H
CONF
LIST 4
L.S. 13
TEMP -173.00
WGHT 0.023000 2.032700
FVAR 0.32945 0.88918
RU1 6 0.994370 0.501476 0.240319 11.00000 0.01335 0.01573 =
0.01514 -0.00009 0.00443 0.00000
CL1 5 0.887777 0.569607 0.304188 11.00000 0.02655 0.02724 =
0.02462 -0.00192 0.01267 0.00392
PART 1
CL2 5 1.133277 0.404243 0.213568 21.00000 0.01834 0.02864 =
0.03183 -0.00125 0.00978 0.00495
PART 2
CL2' 5 1.118086 0.378682 0.207283 -21.00000 0.01834 0.02864 =
0.03183 -0.00125 0.00978 0.00495
PART 0
N1 3 0.873516 0.296801 0.155679 11.00000 0.02590 0.01557 =
0.01623 -0.00083 0.00653 -0.00413
N3 3 0.921086 0.242513 0.252093 11.00000 0.02585 0.01664 =
0.01674 0.00224 0.00625 -0.00341
C2 1 0.917335 0.339974 0.212763 11.00000 0.01559 0.01929 =
0.01689 0.00101 0.00793 0.00082
C4 1 0.881536 0.124484 0.221837 11.00000 0.04078 0.01881 =
0.02590 0.00180 0.00569 -0.00612
AFIX 23
H4A 2 0.826509 0.091262 0.239829 11.00000 -1.20000
H4B 2 0.934834 0.060604 0.225599 11.00000 -1.20000
AFIX 0
C5 1 0.843712 0.163978 0.154663 11.00000 0.03722 0.01723 =
0.02258 -0.00212 0.00951 -0.00847
AFIX 23
H5A 2 0.875913 0.114799 0.126348 11.00000 -1.20000
H5B 2 0.770126 0.154553 0.141719 11.00000 -1.20000
AFIX 0
C6 1 0.839790 0.367100 0.099619 11.00000 0.02799 0.01703 =
0.01359 -0.00109 0.00514 -0.00434
C7 1 0.896787 0.365454 0.053915 11.00000 0.03290 0.02166 =
0.01906 -0.00267 0.00897 -0.00288
C8 1 0.861670 0.434850 -0.000264 11.00000 0.03750 0.03034 =
0.01863 -0.00096 0.01190 -0.00582
AFIX 43
H8 2 0.899326 0.435288 -0.031761 11.00000 -1.20000
AFIX 0
C9 1 0.773632 0.502870 -0.009268 11.00000 0.03737 0.02699 =
0.01632 -0.00103 0.00290 -0.00789
C10 1 0.717236 0.498028 0.036276 11.00000 0.02831 0.02658 =
0.01821 -0.00074 -0.00036 -0.00104
AFIX 43
H10 2 0.655536 0.542040 0.029767 11.00000 -1.20000
AFIX 0
C11 1 0.748668 0.430642 0.090962 11.00000 0.02547 0.02266 =
0.01526 -0.00415 0.00408 -0.00629
C12 1 0.992714 0.292772 0.062607 11.00000 0.04096 0.03851 =
0.02893 0.00426 0.02063 0.00873
AFIX 137
H12A 2 0.977475 0.203641 0.056460 11.00000 -1.50000
H12B 2 1.032465 0.306377 0.104767 11.00000 -1.50000
H12C 2 1.030801 0.320867 0.032265 11.00000 -1.50000
AFIX 0
C13 1 0.739225 0.582618 -0.066345 11.00000 0.05201 0.04157 =
0.02201 0.00798 0.00317 -0.00204
AFIX 137
H13A 2 0.752868 0.670631 -0.055536 11.00000 -1.50000
H13B 2 0.667152 0.570936 -0.082252 11.00000 -1.50000
H13C 2 0.775299 0.558099 -0.098330 11.00000 -1.50000
AFIX 0
C14 1 0.688617 0.432102 0.140679 11.00000 0.02452 0.03742 =
0.01935 -0.00137 0.00619 0.00065
AFIX 137
H14A 2 0.627324 0.480823 0.126258 11.00000 -1.50000
H14B 2 0.728444 0.470074 0.178534 11.00000 -1.50000
H14C 2 0.670993 0.346359 0.149608 11.00000 -1.50000
AFIX 0
C15 1 0.943591 0.247179 0.319068 11.00000 0.02563 0.02041 =
0.01674 0.00365 0.00611 -0.00358
C16 1 0.866443 0.279815 0.348720 11.00000 0.02583 0.02490 =
0.02118 0.00373 0.00784 -0.00531
C17 1 0.888248 0.281197 0.413384 11.00000 0.03491 0.03786 =
0.02263 0.00313 0.01260 -0.00175
AFIX 43
H17 2 0.837725 0.306289 0.434364 11.00000 -1.20000
AFIX 0
C18 1 0.981792 0.246950 0.448272 11.00000 0.04189 0.04256 =
0.01978 0.00361 0.00704 -0.00125
C19 1 1.053763 0.207981 0.417293 11.00000 0.03409 0.03884 =
0.02308 0.01003 -0.00138 0.00406
AFIX 43
H19 2 1.116853 0.180996 0.440809 11.00000 -1.20000
AFIX 0
C20 1 1.036920 0.206899 0.352517 11.00000 0.03022 0.02585 =
0.02380 0.00642 0.00698 0.00204
C21 1 0.762525 0.308697 0.312857 11.00000 0.02456 0.03671 =
0.02771 0.00278 0.00873 -0.00539
AFIX 137
H21A 2 0.728626 0.230919 0.296992 11.00000 -1.50000
H21B 2 0.766193 0.363879 0.277941 11.00000 -1.50000
H21C 2 0.724905 0.350150 0.340223 11.00000 -1.50000
AFIX 0
C22 1 1.003211 0.250330 0.518578 11.00000 0.05850 0.08411 =
0.02079 0.00792 0.00640 0.00852
AFIX 137
H22A 2 1.033192 0.170881 0.535167 11.00000 -1.50000
H22B 2 0.940564 0.263588 0.532379 11.00000 -1.50000
H22C 2 1.049749 0.318708 0.533720 11.00000 -1.50000
AFIX 0
C23 1 1.117781 0.161522 0.320812 11.00000 0.03531 0.04255 =
0.03578 0.01237 0.01143 0.01412
AFIX 137
H23A 2 1.106250 0.073384 0.309524 11.00000 -1.50000
H23B 2 1.183329 0.170749 0.349152 11.00000 -1.50000
H23C 2 1.116202 0.211009 0.283198 11.00000 -1.50000
PART 1
AFIX 0
SAME 0.020 N2' > C35'
N2 3 1.096710 0.664729 0.276149 21.00000 0.02058 0.02302 =
0.02809 -0.00482 0.00179 -0.00291
C24 1 1.145563 0.707295 0.225538 21.00000 0.02524 0.02837 =
0.04158 -0.00111 0.01133 -0.01138
AFIX 23
H24A 2 1.180705 0.635577 0.211559 21.00000 -1.20000
H24B 2 1.196507 0.771195 0.242478 21.00000 -1.20000
AFIX 0
C25 1 1.074004 0.760998 0.170564 21.00000 0.03274 0.02276 =
0.03626 0.00063 0.01779 -0.00561
C26 1 1.101458 0.867951 0.142384 21.00000 0.04944 0.02887 =
0.05764 0.00586 0.02556 -0.01065
AFIX 43
H26 2 1.163691 0.906832 0.159698 21.00000 -1.20000
AFIX 0
C27 1 1.040609 0.919107 0.089889 21.00000 0.07017 0.02884 =
0.05773 0.01566 0.03651 -0.00147
AFIX 43
H27 2 1.061284 0.991924 0.071474 21.00000 -1.20000
AFIX 0
C28 1 0.949608 0.863983 0.064283 21.00000 0.06321 0.03002 =
0.03558 0.01183 0.02788 0.01111
AFIX 43
H28 2 0.907683 0.898325 0.028052 21.00000 -1.20000
AFIX 0
C29 1 0.919914 0.758154 0.091856 21.00000 0.03981 0.02348 =
0.02496 0.00431 0.01907 0.00698
AFIX 43
H29 2 0.857368 0.720626 0.073949 21.00000 -1.20000
AFIX 0
C30 1 0.979669 0.705168 0.145378 21.00000 0.02769 0.01650 =
0.02727 0.00030 0.01378 0.00057
C31 1 0.940910 0.594777 0.171361 21.00000 0.01657 0.01794 =
0.02018 -0.00136 0.00657 -0.00009
AFIX 43
H31 2 0.877511 0.566781 0.148749 21.00000 -1.20000
AFIX 0
C32 1 1.047295 0.774799 0.297879 21.00000 0.03315 0.01936 =
0.03491 -0.00902 0.00270 -0.00316
AFIX 137
H32A 2 1.095373 0.843683 0.307309 21.00000 -1.50000
H32B 2 1.023770 0.752437 0.335407 21.00000 -1.50000
H32C 2 0.990211 0.800737 0.265227 21.00000 -1.50000
AFIX 0
C33 1 1.181216 0.623437 0.327765 21.00000 0.02145 0.03380 =
0.03623 -0.00614 -0.00455 -0.00441
AFIX 23
H33A 2 1.218149 0.698051 0.346998 21.00000 -1.20000
H33B 2 1.228189 0.571875 0.310011 21.00000 -1.20000
AFIX 0
C34 1 1.146961 0.549089 0.377626 21.00000 0.02980 0.03792 =
0.03251 -0.00446 -0.00709 -0.00164
AFIX 23
H34A 2 1.086385 0.587242 0.387542 21.00000 -1.20000
H34B 2 1.131107 0.462151 0.363592 21.00000 -1.20000
AFIX 0
O1 4 1.227539 0.551204 0.430550 21.00000 0.04654 0.05158 =
0.04397 0.00678 -0.02161 -0.00891
C35 1 1.213117 0.466381 0.476649 21.00000 0.06667 0.06937 =
0.04840 0.01530 -0.02262 -0.01591
AFIX 137
H35A 2 1.147148 0.480349 0.486017 21.00000 -1.50000
H35B 2 1.265216 0.478992 0.514398 21.00000 -1.50000
H35C 2 1.216949 0.380769 0.461615 21.00000 -1.50000
PART 2
AFIX 0
N2' 3 1.112436 0.640536 0.283642 -21.00000 0.02511 0.02683 =
0.03064 -0.00551 0.00771 -0.00664
C24' 1 1.064825 0.762962 0.270315 -21.00000 0.02837 0.02504 =
0.03171 -0.00644 0.00853 -0.00898
AFIX 23
H24C 2 1.108807 0.827310 0.294428 -21.00000 -1.20000
H24D 2 1.000941 0.763177 0.284495 -21.00000 -1.20000
AFIX 0
C25' 1 1.043900 0.797731 0.202087 -21.00000 0.03384 0.02077 =
0.03698 0.00486 0.01506 -0.00871
C26' 1 1.077028 0.911726 0.183660 -21.00000 0.04491 0.02490 =
0.04420 0.00492 0.01743 -0.00827
AFIX 43
H26' 2 1.114195 0.966922 0.213816 -21.00000 -1.20000
AFIX 0
C27' 1 1.055879 0.944494 0.121631 -21.00000 0.05275 0.02640 =
0.04496 0.00869 0.02536 0.00015
AFIX 43
H27' 2 1.092008 1.010871 0.108094 -21.00000 -1.20000
AFIX 0
C28' 1 0.983333 0.882816 0.078877 -21.00000 0.05121 0.02644 =
0.04045 0.01173 0.02458 -0.00301
AFIX 43
H28' 2 0.952886 0.921149 0.040544 -21.00000 -1.20000
AFIX 0
C29' 1 0.955485 0.761804 0.093370 -21.00000 0.04053 0.02515 =
0.03366 0.00028 0.01658 -0.00011
AFIX 43
H29' 2 0.913261 0.711548 0.063023 -21.00000 -1.20000
AFIX 0
C30' 1 0.992142 0.717376 0.154302 -21.00000 0.03048 0.01801 =
0.02783 0.00399 0.01039 0.00238
C31' 1 0.958462 0.594075 0.170034 -21.00000 0.01657 0.01794 =
0.02018 -0.00136 0.00657 -0.00009
AFIX 43
H31' 2 0.909606 0.556218 0.138068 -21.00000 -1.20000
AFIX 0
C32' 1 1.202634 0.632736 0.257577 -21.00000 0.02782 0.01969 =
0.05398 -0.00214 0.00544 -0.00825
AFIX 33
H32D 2 1.233756 0.550496 0.266794 -21.00000 -1.50000
H32E 2 1.184002 0.644708 0.212440 -21.00000 -1.50000
H32F 2 1.250184 0.697811 0.276145 -21.00000 -1.50000
AFIX 0
C33' 1 1.142718 0.623533 0.352093 -21.00000 0.02707 0.03130 =
0.02960 -0.00643 -0.00613 -0.00989
AFIX 23
H33C 2 1.204865 0.672026 0.367182 -21.00000 -1.20000
H33D 2 1.090134 0.661197 0.370847 -21.00000 -1.20000
AFIX 0
C34' 1 1.160459 0.494699 0.376320 -21.00000 0.03458 0.03736 =
0.03538 0.00118 -0.00798 -0.00730
AFIX 23
H34C 2 1.098900 0.459873 0.386468 -21.00000 -1.20000
H34D 2 1.181367 0.439951 0.345226 -21.00000 -1.20000
AFIX 0
O1' 4 1.237955 0.504232 0.430736 -21.00000 0.03431 0.04126 =
0.03609 0.00836 -0.01353 -0.00787
C35' 1 1.252738 0.391429 0.464195 -21.00000 0.04839 0.05337 =
0.04516 0.02308 -0.01769 -0.01668
AFIX 33
H35D 2 1.306612 0.402033 0.501224 -21.00000 -1.50000
H35E 2 1.190802 0.368067 0.476824 -21.00000 -1.50000
H35F 2 1.271099 0.325597 0.437849 -21.00000 -1.50000
AFIX 0
HKLF 4
REM ES-tx2079
REM wR2 = 0.0702, GooF = S = 1.023, Restrained GooF = 1.010 for all data
REM R1 = 0.0320 for 7087 Fo > 4sig(Fo) and 0.0514 for all 9279 data
REM 493 parameters refined using 460 restraints
END
WGHT 0.0230 2.0327
REM Highest difference peak 0.433, deepest hole -0.576, 1-sigma level 0.072
Q1 1 1.0047 0.4363 0.2279 11.00000 0.05 0.43
Q2 1 1.0624 0.5078 0.2564 11.00000 0.05 0.42
Q3 1 0.9224 0.4195 0.2240 11.00000 0.05 0.40
Q4 1 0.9531 0.4530 0.2624 11.00000 0.05 0.39
Q5 1 0.9444 0.5017 0.1965 11.00000 0.05 0.38
Q6 1 0.9205 0.4980 0.2217 11.00000 0.05 0.38
Q7 1 0.8460 0.6041 0.2440 11.00000 0.05 0.35
Q8 1 1.0692 0.2563 0.5349 11.00000 0.05 0.34
Q9 1 0.8215 0.4805 0.0003 11.00000 0.05 0.34
Q10 1 0.8190 0.3066 0.3336 11.00000 0.05 0.34
Q11 1 0.7988 0.4461 -0.0112 11.00000 0.05 0.34
Q12 1 0.9217 0.8270 0.0763 11.00000 0.05 0.33
Q13 1 1.0459 0.2218 0.3862 11.00000 0.05 0.33
Q14 1 0.7803 0.3789 0.0918 11.00000 0.05 0.33
Q15 1 0.9588 0.5933 0.2140 11.00000 0.05 0.32
;
_shelx_res_checksum 41826
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ru Ru1 0.99437(2) 0.50148(2) 0.24032(2) 0.01454(4) Uani d 1 . .
Cl Cl1 0.88778(4) 0.56961(5) 0.30419(2) 0.02505(10) Uani d 1 . .
Cl Cl2 1.13328(6) 0.40424(9) 0.21357(6) 0.02561(19) Uani d 0.889(2) A 1
Cl Cl2' 1.1181(6) 0.3787(9) 0.2073(5) 0.02561(19) Uani d 0.111(2) A 2
N N1 0.87352(12) 0.29680(14) 0.15568(7) 0.0189(3) Uani d 1 . .
N N3 0.92109(12) 0.24251(14) 0.25209(7) 0.0195(3) Uani d 1 . .
C C2 0.91734(13) 0.33997(17) 0.21276(8) 0.0166(3) Uani d 1 . .
C C4 0.88154(17) 0.12448(18) 0.22184(9) 0.0287(5) Uani d 1 . .
H H4A 0.826509 0.091262 0.239829 0.034 Uiso calc 1 . .
H H4B 0.934834 0.060604 0.225599 0.034 Uiso calc 1 . .
C C5 0.84371(16) 0.16398(18) 0.15466(9) 0.0252(4) Uani d 1 . .
H H5A 0.875913 0.114799 0.126348 0.030 Uiso calc 1 . .
H H5B 0.770126 0.154553 0.141719 0.030 Uiso calc 1 . .
C C6 0.83979(14) 0.36710(17) 0.09962(8) 0.0194(4) Uani d 1 . .
C C7 0.89679(16) 0.36545(18) 0.05392(9) 0.0240(4) Uani d 1 . .
C C8 0.86167(16) 0.4348(2) -0.00026(9) 0.0279(4) Uani d 1 . .
H H8 0.899326 0.435288 -0.031761 0.034 Uiso calc 1 . .
C C9 0.77363(16) 0.5029(2) -0.00927(9) 0.0273(4) Uani d 1 . .
C C10 0.71724(15) 0.49803(19) 0.03628(9) 0.0252(4) Uani d 1 . .
H H10 0.655536 0.542040 0.029767 0.030 Uiso calc 1 . .
C C11 0.74867(14) 0.43064(18) 0.09096(8) 0.0212(4) Uani d 1 . .
C C12 0.99271(17) 0.2928(2) 0.06261(10) 0.0341(5) Uani d 1 . .
H H12A 0.977475 0.203641 0.056460 0.051 Uiso calc 1 . .
H H12B 1.032465 0.306377 0.104767 0.051 Uiso calc 1 . .
H H12C 1.030801 0.320867 0.032265 0.051 Uiso calc 1 . .
C C13 0.73922(19) 0.5826(2) -0.06635(10) 0.0393(6) Uani d 1 . .
H H13A 0.752868 0.670631 -0.055536 0.059 Uiso calc 1 . .
H H13B 0.667152 0.570936 -0.082252 0.059 Uiso calc 1 . .
H H13C 0.775299 0.558099 -0.098330 0.059 Uiso calc 1 . .
C C14 0.68862(15) 0.4321(2) 0.14068(9) 0.0269(4) Uani d 1 . .
H H14A 0.627324 0.480823 0.126258 0.040 Uiso calc 1 . .
H H14B 0.728444 0.470074 0.178534 0.040 Uiso calc 1 . .
H H14C 0.670993 0.346359 0.149608 0.040 Uiso calc 1 . .
C C15 0.94359(15) 0.24718(17) 0.31907(8) 0.0207(4) Uani d 1 . .
C C16 0.86644(15) 0.27982(18) 0.34872(9) 0.0236(4) Uani d 1 . .
C C17 0.88825(17) 0.2812(2) 0.41338(9) 0.0308(5) Uani d 1 . .
H H17 0.837725 0.306289 0.434364 0.037 Uiso calc 1 . .
C C18 0.98179(18) 0.2470(2) 0.44827(10) 0.0347(5) Uani d 1 . .
C C19 1.05376(17) 0.2080(2) 0.41729(10) 0.0332(5) Uani d 1 . .
H H19 1.116853 0.180996 0.440809 0.040 Uiso calc 1 . .
C C20 1.03692(16) 0.20690(19) 0.35252(9) 0.0265(4) Uani d 1 . .
C C21 0.76253(15) 0.3087(2) 0.31286(10) 0.0292(5) Uani d 1 . .
H H21A 0.728626 0.230919 0.296992 0.044 Uiso calc 1 . .
H H21B 0.766193 0.363879 0.277941 0.044 Uiso calc 1 . .
H H21C 0.724905 0.350150 0.340223 0.044 Uiso calc 1 . .
C C22 1.0032(2) 0.2503(3) 0.51858(11) 0.0548(8) Uani d 1 . .
H H22A 1.033192 0.170881 0.535167 0.082 Uiso calc 1 . .
H H22B 0.940564 0.263588 0.532379 0.082 Uiso calc 1 . .
H H22C 1.049749 0.318708 0.533720 0.082 Uiso calc 1 . .
C C23 1.11778(17) 0.1615(2) 0.32081(11) 0.0373(5) Uani d 1 . .
H H23A 1.106250 0.073384 0.309524 0.056 Uiso calc 1 . .
H H23B 1.183329 0.170749 0.349152 0.056 Uiso calc 1 . .
H H23C 1.116202 0.211009 0.283198 0.056 Uiso calc 1 . .
N N2 1.09671(18) 0.6647(2) 0.27615(12) 0.0244(5) Uani d 0.889(2) A 1
C C24 1.14556(18) 0.7073(2) 0.22554(12) 0.0311(6) Uani d 0.889(2) A 1
H H24A 1.180705 0.635577 0.211559 0.037 Uiso calc 0.889(2) A 1
H H24B 1.196507 0.771195 0.242478 0.037 Uiso calc 0.889(2) A 1
C C25 1.07400(18) 0.7610(2) 0.17056(12) 0.0290(5) Uani d 0.889(2) A 1
C C26 1.1015(2) 0.8680(2) 0.14238(14) 0.0432(7) Uani d 0.889(2) A 1
H H26 1.163691 0.906832 0.159698 0.052 Uiso calc 0.889(2) A 1
C C27 1.0406(3) 0.9191(3) 0.08989(17) 0.0488(8) Uani d 0.889(2) A 1
H H27 1.061284 0.991924 0.071474 0.059 Uiso calc 0.889(2) A 1
C C28 0.9496(3) 0.8640(3) 0.06428(15) 0.0403(8) Uani d 0.889(2) A 1
H H28 0.907683 0.898325 0.028052 0.048 Uiso calc 0.889(2) A 1
C C29 0.9199(2) 0.7582(3) 0.09186(13) 0.0276(6) Uani d 0.889(2) A 1
H H29 0.857368 0.720626 0.073949 0.033 Uiso calc 0.889(2) A 1
C C30 0.9797(4) 0.7052(3) 0.14538(14) 0.0226(6) Uani d 0.889(2) A 1
C C31 0.9409(2) 0.5948(3) 0.17136(18) 0.0178(7) Uani d 0.889(2) A 1
H H31 0.877511 0.566781 0.148749 0.021 Uiso calc 0.889(2) A 1
C C32 1.04729(19) 0.7748(2) 0.29788(13) 0.0299(6) Uani d 0.889(2) A 1
H H32A 1.095373 0.843683 0.307309 0.045 Uiso calc 0.889(2) A 1
H H32B 1.023770 0.752437 0.335407 0.045 Uiso calc 0.889(2) A 1
H H32C 0.990211 0.800737 0.265227 0.045 Uiso calc 0.889(2) A 1
C C33 1.18122(18) 0.6234(2) 0.32777(13) 0.0321(6) Uani d 0.889(2) A 1
H H33A 1.218149 0.698051 0.346998 0.039 Uiso calc 0.889(2) A 1
H H33B 1.228189 0.571875 0.310011 0.039 Uiso calc 0.889(2) A 1
C C34 1.1470(2) 0.5491(3) 0.37763(13) 0.0355(6) Uani d 0.889(2) A 1
H H34A 1.086385 0.587242 0.387542 0.043 Uiso calc 0.889(2) A 1
H H34B 1.131107 0.462151 0.363592 0.043 Uiso calc 0.889(2) A 1
O O1 1.2275(2) 0.5512(2) 0.43055(14) 0.0521(7) Uani d 0.889(2) A 1
C C35 1.2131(3) 0.4664(4) 0.47665(16) 0.0668(11) Uani d 0.889(2) A 1
H H35A 1.147148 0.480349 0.486017 0.100 Uiso calc 0.889(2) A 1
H H35B 1.265216 0.478992 0.514398 0.100 Uiso calc 0.889(2) A 1
H H35C 1.216949 0.380769 0.461615 0.100 Uiso calc 0.889(2) A 1
N N2' 1.1124(14) 0.6405(16) 0.2836(8) 0.027(3) Uani d 0.111(2) A 2
C C24' 1.0648(15) 0.7630(16) 0.2703(7) 0.028(3) Uani d 0.111(2) A 2
H H24C 1.108807 0.827310 0.294428 0.034 Uiso calc 0.111(2) A 2
H H24D 1.000941 0.763177 0.284495 0.034 Uiso calc 0.111(2) A 2
C C25' 1.0439(14) 0.7977(14) 0.2021(7) 0.029(2) Uani d 0.111(2) A 2
C C26' 1.0770(16) 0.9117(16) 0.1837(8) 0.037(3) Uani d 0.111(2) A 2
H H26' 1.114195 0.966922 0.213816 0.044 Uiso calc 0.111(2) A 2
C C27' 1.0559(18) 0.944(2) 0.1216(9) 0.039(3) Uani d 0.111(2) A 2
H H27' 1.092008 1.010871 0.108094 0.047 Uiso calc 0.111(2) A 2
C C28' 0.983(2) 0.883(2) 0.0789(11) 0.037(2) Uani d 0.111(2) A 2
H H28' 0.952886 0.921149 0.040544 0.045 Uiso calc 0.111(2) A 2
C C29' 0.9555(19) 0.762(2) 0.0934(10) 0.032(3) Uani d 0.111(2) A 2
H H29' 0.913261 0.711548 0.063023 0.038 Uiso calc 0.111(2) A 2
C C30' 0.992(4) 0.717(3) 0.1543(11) 0.025(2) Uani d 0.111(2) A 2
C C31' 0.958(3) 0.594(3) 0.1700(16) 0.0178(7) Uani d 0.111(2) A 2
H H31' 0.909606 0.556218 0.138068 0.021 Uiso calc 0.111(2) A 2
C C32' 1.2026(13) 0.6327(17) 0.2576(10) 0.034(4) Uani d 0.111(2) A 2
H H32D 1.233756 0.550496 0.266794 0.052 Uiso calc 0.111(2) A 2
H H32E 1.184002 0.644708 0.212440 0.052 Uiso calc 0.111(2) A 2
H H32F 1.250184 0.697811 0.276145 0.052 Uiso calc 0.111(2) A 2
C C33' 1.1427(16) 0.6235(17) 0.3521(8) 0.031(2) Uani d 0.111(2) A 2
H H33C 1.204865 0.672026 0.367182 0.037 Uiso calc 0.111(2) A 2
H H33D 1.090134 0.661197 0.370847 0.037 Uiso calc 0.111(2) A 2
C C34' 1.160(2) 0.4947(19) 0.3763(11) 0.038(3) Uani d 0.111(2) A 2
H H34C 1.098900 0.459873 0.386468 0.046 Uiso calc 0.111(2) A 2
H H34D 1.181367 0.439951 0.345226 0.046 Uiso calc 0.111(2) A 2
O O1' 1.2380(19) 0.5042(18) 0.4307(11) 0.040(3) Uani d 0.111(2) A 2
C C35' 1.253(2) 0.391(2) 0.4642(12) 0.053(5) Uani d 0.111(2) A 2
H H35D 1.306612 0.402033 0.501224 0.080 Uiso calc 0.111(2) A 2
H H35E 1.190802 0.368067 0.476824 0.080 Uiso calc 0.111(2) A 2
H H35F 1.271099 0.325597 0.437849 0.080 Uiso calc 0.111(2) A 2
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Ru1 0.01335(7) 0.01573(7) 0.01514(7) 0.00000(6) 0.00443(5) -0.00009(6)
Cl1 0.0265(2) 0.0272(2) 0.0246(2) 0.00392(19) 0.01267(19) -0.00192(19)
Cl2 0.0183(4) 0.0286(5) 0.0318(4) 0.0050(3) 0.0098(3) -0.0013(3)
Cl2' 0.0183(4) 0.0286(5) 0.0318(4) 0.0050(3) 0.0098(3) -0.0013(3)
N1 0.0259(8) 0.0156(7) 0.0162(8) -0.0041(6) 0.0065(6) -0.0008(6)
N3 0.0259(9) 0.0166(8) 0.0167(8) -0.0034(6) 0.0062(6) 0.0022(6)
C2 0.0156(8) 0.0193(9) 0.0169(9) 0.0008(7) 0.0079(7) 0.0010(7)
C4 0.0408(13) 0.0188(10) 0.0259(11) -0.0061(9) 0.0057(9) 0.0018(8)
C5 0.0372(12) 0.0172(9) 0.0226(10) -0.0085(8) 0.0095(8) -0.0021(7)
C6 0.0280(10) 0.0170(9) 0.0136(8) -0.0043(7) 0.0051(7) -0.0011(7)
C7 0.0329(11) 0.0217(10) 0.0191(10) -0.0029(8) 0.0090(8) -0.0027(7)
C8 0.0375(12) 0.0303(11) 0.0186(10) -0.0058(9) 0.0119(8) -0.0010(8)
C9 0.0374(11) 0.0270(10) 0.0163(9) -0.0079(10) 0.0029(8) -0.0010(8)
C10 0.0283(10) 0.0266(10) 0.0182(9) -0.0010(9) -0.0004(7) -0.0007(8)
C11 0.0255(10) 0.0227(10) 0.0153(9) -0.0063(8) 0.0041(7) -0.0042(7)
C12 0.0410(13) 0.0385(13) 0.0289(11) 0.0087(10) 0.0206(10) 0.0043(9)
C13 0.0520(15) 0.0416(14) 0.0220(11) -0.0020(11) 0.0032(10) 0.0080(10)
C14 0.0245(10) 0.0374(12) 0.0193(10) 0.0006(9) 0.0062(8) -0.0014(8)
C15 0.0256(10) 0.0204(9) 0.0167(9) -0.0036(8) 0.0061(7) 0.0036(7)
C16 0.0258(10) 0.0249(10) 0.0212(10) -0.0053(8) 0.0078(8) 0.0037(8)
C17 0.0349(12) 0.0379(12) 0.0226(10) -0.0018(10) 0.0126(9) 0.0031(9)
C18 0.0419(13) 0.0426(13) 0.0198(10) -0.0013(11) 0.0070(9) 0.0036(9)
C19 0.0341(12) 0.0388(13) 0.0231(11) 0.0041(10) -0.0014(9) 0.0100(9)
C20 0.0302(11) 0.0259(10) 0.0238(10) 0.0020(8) 0.0070(8) 0.0064(8)
C21 0.0246(11) 0.0367(12) 0.0277(11) -0.0054(9) 0.0087(8) 0.0028(9)
C22 0.0585(18) 0.084(2) 0.0208(12) 0.0085(15) 0.0064(12) 0.0079(13)
C23 0.0353(13) 0.0426(13) 0.0358(13) 0.0141(11) 0.0114(10) 0.0124(10)
N2 0.0206(11) 0.0230(12) 0.0281(11) -0.0029(9) 0.0018(8) -0.0048(9)
C24 0.0252(12) 0.0284(12) 0.0416(14) -0.0114(10) 0.0113(10) -0.0011(10)
C25 0.0327(13) 0.0228(11) 0.0363(13) -0.0056(10) 0.0178(10) 0.0006(10)
C26 0.0494(16) 0.0289(13) 0.0576(18) -0.0106(12) 0.0256(14) 0.0059(12)
C27 0.070(2) 0.0288(15) 0.058(2) -0.0015(15) 0.0365(18) 0.0157(14)
C28 0.063(2) 0.0300(15) 0.0356(17) 0.0111(14) 0.0279(14) 0.0118(13)
C29 0.0398(16) 0.0235(11) 0.0250(12) 0.0070(12) 0.0191(12) 0.0043(9)
C30 0.0277(19) 0.0165(12) 0.0273(14) 0.0006(10) 0.0138(12) 0.0003(11)
C31 0.0166(17) 0.0179(9) 0.0202(9) -0.0001(10) 0.0066(11) -0.0014(7)
C32 0.0332(14) 0.0194(11) 0.0349(14) -0.0032(10) 0.0027(11) -0.0090(10)
C33 0.0214(12) 0.0338(13) 0.0362(14) -0.0044(10) -0.0046(10) -0.0061(11)
C34 0.0298(14) 0.0379(16) 0.0325(14) -0.0016(13) -0.0071(11) -0.0045(13)
O1 0.0465(14) 0.0516(17) 0.0440(12) -0.0089(14) -0.0216(10) 0.0068(14)
C35 0.067(2) 0.069(3) 0.048(2) -0.016(2) -0.0226(18) 0.0153(18)
N2' 0.025(4) 0.027(4) 0.031(4) -0.007(4) 0.008(4) -0.006(4)
C24' 0.028(5) 0.025(5) 0.032(5) -0.009(4) 0.009(4) -0.006(5)
C25' 0.034(4) 0.021(4) 0.037(4) -0.009(4) 0.015(4) 0.005(4)
C26' 0.045(5) 0.025(5) 0.044(5) -0.008(5) 0.017(5) 0.005(5)
C27' 0.053(5) 0.026(4) 0.045(5) 0.000(4) 0.025(5) 0.009(4)
C28' 0.051(4) 0.026(4) 0.040(4) -0.003(4) 0.025(4) 0.012(4)
C29' 0.041(5) 0.025(4) 0.034(4) 0.000(5) 0.017(5) 0.000(4)
C30' 0.030(4) 0.018(4) 0.028(4) 0.002(4) 0.010(4) 0.004(4)
C31' 0.0166(17) 0.0179(9) 0.0202(9) -0.0001(10) 0.0066(11) -0.0014(7)
C32' 0.028(7) 0.020(7) 0.054(8) -0.008(6) 0.005(7) -0.002(7)
C33' 0.027(4) 0.031(4) 0.030(4) -0.010(4) -0.006(4) -0.006(4)
C34' 0.035(5) 0.037(5) 0.035(4) -0.007(5) -0.008(4) 0.001(5)
O1' 0.034(5) 0.041(6) 0.036(5) -0.008(5) -0.014(4) 0.008(5)
C35' 0.048(10) 0.053(10) 0.045(9) -0.017(9) -0.018(8) 0.023(9)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
C31' Ru1 C2 . . 100.5(8) yes
C31 Ru1 C2 . . 97.33(11) yes
C31' Ru1 N2' . . 92.1(8) yes
C2 Ru1 N2' . . 163.8(5) yes
C31 Ru1 N2 . . 88.48(11) yes
C2 Ru1 N2 . . 172.68(8) yes
C31 Ru1 Cl2 . . 103.42(13) yes
C2 Ru1 Cl2 . . 86.77(5) yes
N2 Ru1 Cl2 . . 87.55(7) yes
C31' Ru1 Cl1 . . 104.7(14) yes
C31 Ru1 Cl1 . . 98.02(13) yes
C2 Ru1 Cl1 . . 95.36(5) yes
N2' Ru1 Cl1 . . 91.3(6) yes
N2 Ru1 Cl1 . . 88.21(7) yes
Cl2 Ru1 Cl1 . . 158.02(3) yes
C31' Ru1 Cl2' . . 96.9(15) yes
C2 Ru1 Cl2' . . 78.3(2) yes
N2' Ru1 Cl2' . . 90.2(6) yes
Cl1 Ru1 Cl2' . . 158.4(3) yes
C2 N1 C6 . . 128.05(15) ?
C2 N1 C5 . . 114.09(15) ?
C6 N1 C5 . . 117.11(15) ?
C2 N3 C15 . . 126.88(16) ?
C2 N3 C4 . . 114.39(15) ?
C15 N3 C4 . . 117.90(15) ?
N3 C2 N1 . . 106.27(15) ?
N3 C2 Ru1 . . 121.14(13) yes
N1 C2 Ru1 . . 131.33(13) yes
N3 C4 C5 . . 102.46(15) ?
N3 C4 H4A . . 111.3 ?
C5 C4 H4A . . 111.3 ?
N3 C4 H4B . . 111.3 ?
C5 C4 H4B . . 111.3 ?
H4A C4 H4B . . 109.2 ?
N1 C5 C4 . . 102.64(15) ?
N1 C5 H5A . . 111.2 ?
C4 C5 H5A . . 111.2 ?
N1 C5 H5B . . 111.2 ?
C4 C5 H5B . . 111.2 ?
H5A C5 H5B . . 109.2 ?
C11 C6 C7 . . 121.84(17) ?
C11 C6 N1 . . 118.94(16) ?
C7 C6 N1 . . 119.16(17) ?
C8 C7 C6 . . 117.70(19) ?
C8 C7 C12 . . 120.82(18) ?
C6 C7 C12 . . 121.48(18) ?
C9 C8 C7 . . 121.88(19) ?
C9 C8 H8 . . 119.1 ?
C7 C8 H8 . . 119.1 ?
C8 C9 C10 . . 118.54(18) ?
C8 C9 C13 . . 121.43(19) ?
C10 C9 C13 . . 120.0(2) ?
C11 C10 C9 . . 121.89(19) ?
C11 C10 H10 . . 119.1 ?
C9 C10 H10 . . 119.1 ?
C10 C11 C6 . . 118.04(18) ?
C10 C11 C14 . . 120.70(18) ?
C6 C11 C14 . . 121.18(17) ?
C7 C12 H12A . . 109.5 ?
C7 C12 H12B . . 109.5 ?
H12A C12 H12B . . 109.5 ?
C7 C12 H12C . . 109.5 ?
H12A C12 H12C . . 109.5 ?
H12B C12 H12C . . 109.5 ?
C9 C13 H13A . . 109.5 ?
C9 C13 H13B . . 109.5 ?
H13A C13 H13B . . 109.5 ?
C9 C13 H13C . . 109.5 ?
H13A C13 H13C . . 109.5 ?
H13B C13 H13C . . 109.5 ?
C11 C14 H14A . . 109.5 ?
C11 C14 H14B . . 109.5 ?
H14A C14 H14B . . 109.5 ?
C11 C14 H14C . . 109.5 ?
H14A C14 H14C . . 109.5 ?
H14B C14 H14C . . 109.5 ?
C20 C15 C16 . . 121.73(17) ?
C20 C15 N3 . . 119.80(17) ?
C16 C15 N3 . . 118.11(17) ?
C17 C16 C15 . . 117.70(19) ?
C17 C16 C21 . . 120.32(18) ?
C15 C16 C21 . . 121.95(17) ?
C16 C17 C18 . . 122.0(2) ?
C16 C17 H17 . . 119.0 ?
C18 C17 H17 . . 119.0 ?
C19 C18 C17 . . 118.4(2) ?
C19 C18 C22 . . 120.9(2) ?
C17 C18 C22 . . 120.6(2) ?
C18 C19 C20 . . 122.1(2) ?
C18 C19 H19 . . 118.9 ?
C20 C19 H19 . . 118.9 ?
C19 C20 C15 . . 117.78(19) ?
C19 C20 C23 . . 120.05(19) ?
C15 C20 C23 . . 122.17(18) ?
C16 C21 H21A . . 109.5 ?
C16 C21 H21B . . 109.5 ?
H21A C21 H21B . . 109.5 ?
C16 C21 H21C . . 109.5 ?
H21A C21 H21C . . 109.5 ?
H21B C21 H21C . . 109.5 ?
C18 C22 H22A . . 109.5 ?
C18 C22 H22B . . 109.5 ?
H22A C22 H22B . . 109.5 ?
C18 C22 H22C . . 109.5 ?
H22A C22 H22C . . 109.5 ?
H22B C22 H22C . . 109.5 ?
C20 C23 H23A . . 109.5 ?
C20 C23 H23B . . 109.5 ?
H23A C23 H23B . . 109.5 ?
C20 C23 H23C . . 109.5 ?
H23A C23 H23C . . 109.5 ?
H23B C23 H23C . . 109.5 ?
C32 N2 C24 . . 107.9(2) ?
C32 N2 C33 . . 108.6(2) ?
C24 N2 C33 . . 105.1(2) ?
C32 N2 Ru1 . . 115.62(17) yes
C24 N2 Ru1 . . 108.54(16) yes
C33 N2 Ru1 . . 110.59(15) yes
N2 C24 C25 . . 113.7(2) ?
N2 C24 H24A . . 108.8 ?
C25 C24 H24A . . 108.8 ?
N2 C24 H24B . . 108.8 ?
C25 C24 H24B . . 108.8 ?
H24A C24 H24B . . 107.7 ?
C26 C25 C30 . . 118.8(3) ?
C26 C25 C24 . . 119.0(2) ?
C30 C25 C24 . . 122.2(2) ?
C27 C26 C25 . . 121.8(3) ?
C27 C26 H26 . . 119.1 ?
C25 C26 H26 . . 119.1 ?
C28 C27 C26 . . 119.8(3) ?
C28 C27 H27 . . 120.1 ?
C26 C27 H27 . . 120.1 ?
C27 C28 C29 . . 119.6(3) ?
C27 C28 H28 . . 120.2 ?
C29 C28 H28 . . 120.2 ?
C28 C29 C30 . . 121.8(3) ?
C28 C29 H29 . . 119.1 ?
C30 C29 H29 . . 119.1 ?
C29 C30 C25 . . 118.2(3) ?
C29 C30 C31 . . 117.5(3) ?
C25 C30 C31 . . 124.3(3) ?
C30 C31 Ru1 . . 130.7(2) yes
C30 C31 H31 . . 114.7 ?
Ru1 C31 H31 . . 114.7 ?
N2 C32 H32A . . 109.5 ?
N2 C32 H32B . . 109.5 ?
H32A C32 H32B . . 109.5 ?
N2 C32 H32C . . 109.5 ?
H32A C32 H32C . . 109.5 ?
H32B C32 H32C . . 109.5 ?
N2 C33 C34 . . 113.4(2) ?
N2 C33 H33A . . 108.9 ?
C34 C33 H33A . . 108.9 ?
N2 C33 H33B . . 108.9 ?
C34 C33 H33B . . 108.9 ?
H33A C33 H33B . . 107.7 ?
O1 C34 C33 . . 106.3(2) ?
O1 C34 H34A . . 110.5 ?
C33 C34 H34A . . 110.5 ?
O1 C34 H34B . . 110.5 ?
C33 C34 H34B . . 110.5 ?
H34A C34 H34B . . 108.7 ?
C35 O1 C34 . . 112.1(3) ?
O1 C35 H35A . . 109.5 ?
O1 C35 H35B . . 109.5 ?
H35A C35 H35B . . 109.5 ?
O1 C35 H35C . . 109.5 ?
H35A C35 H35C . . 109.5 ?
H35B C35 H35C . . 109.5 ?
C24' N2' C32' . . 110.3(15) ?
C24' N2' C33' . . 109.1(15) ?
C32' N2' C33' . . 108.5(15) ?
C24' N2' Ru1 . . 105.1(11) yes
C32' N2' Ru1 . . 112.5(13) yes
C33' N2' Ru1 . . 111.4(12) yes
N2' C24' C25' . . 113.5(15) ?
N2' C24' H24C . . 108.9 ?
C25' C24' H24C . . 108.9 ?
N2' C24' H24D . . 108.9 ?
C25' C24' H24D . . 108.9 ?
H24C C24' H24D . . 107.7 ?
C26' C25' C30' . . 117.1(15) ?
C26' C25' C24' . . 120.1(14) ?
C30' C25' C24' . . 122.8(14) ?
C27' C26' C25' . . 120.0(16) ?
C27' C26' H26' . . 120.0 ?
C25' C26' H26' . . 120.0 ?
C28' C27' C26' . . 121.3(17) ?
C28' C27' H27' . . 119.3 ?
C26' C27' H27' . . 119.3 ?
C27' C28' C29' . . 118.4(18) ?
C27' C28' H28' . . 120.8 ?
C29' C28' H28' . . 120.8 ?
C28' C29' C30' . . 118.0(18) ?
C28' C29' H29' . . 121.0 ?
C30' C29' H29' . . 121.0 ?
C29' C30' C25' . . 121.1(17) ?
C29' C30' C31' . . 117.7(18) ?
C25' C30' C31' . . 120.1(19) ?
C30' C31' Ru1 . . 130.8(19) yes
C30' C31' H31' . . 114.6 ?
Ru1 C31' H31' . . 114.6 ?
N2' C32' H32D . . 109.5 ?
N2' C32' H32E . . 109.5 ?
H32D C32' H32E . . 109.5 ?
N2' C32' H32F . . 109.5 ?
H32D C32' H32F . . 109.5 ?
H32E C32' H32F . . 109.5 ?
C34' C33' N2' . . 117.9(16) ?
C34' C33' H33C . . 107.8 ?
N2' C33' H33C . . 107.8 ?
C34' C33' H33D . . 107.8 ?
N2' C33' H33D . . 107.8 ?
H33C C33' H33D . . 107.2 ?
O1' C34' C33' . . 105.7(15) ?
O1' C34' H34C . . 110.6 ?
C33' C34' H34C . . 110.6 ?
O1' C34' H34D . . 110.6 ?
C33' C34' H34D . . 110.6 ?
H34C C34' H34D . . 108.7 ?
C35' O1' C34' . . 112.1(17) ?
O1' C35' H35D . . 109.5 ?
O1' C35' H35E . . 109.5 ?
H35D C35' H35E . . 109.5 ?
O1' C35' H35F . . 109.5 ?
H35D C35' H35F . . 109.5 ?
H35E C35' H35F . . 109.5 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Ru1 C31' . 1.81(3) yes
Ru1 C31 . 1.833(4) yes
Ru1 C2 . 2.0474(18) yes
Ru1 N2' . 2.251(15) yes
Ru1 N2 . 2.271(2) yes
Ru1 Cl2 . 2.3515(8) yes
Ru1 Cl1 . 2.3519(5) yes
Ru1 Cl2' . 2.379(7) yes
N1 C2 . 1.352(2) ?
N1 C6 . 1.434(2) ?
N1 C5 . 1.478(2) ?
N3 C2 . 1.350(2) ?
N3 C15 . 1.441(2) ?
N3 C4 . 1.476(2) ?
C4 C5 . 1.518(3) ?
C4 H4A . 0.9900 ?
C4 H4B . 0.9900 ?
C5 H5A . 0.9900 ?
C5 H5B . 0.9900 ?
C6 C11 . 1.396(3) ?
C6 C7 . 1.401(3) ?
C7 C8 . 1.400(3) ?
C7 C12 . 1.502(3) ?
C8 C9 . 1.384(3) ?
C8 H8 . 0.9500 ?
C9 C10 . 1.393(3) ?
C9 C13 . 1.508(3) ?
C10 C11 . 1.390(3) ?
C10 H10 . 0.9500 ?
C11 C14 . 1.505(3) ?
C12 H12A . 0.9800 ?
C12 H12B . 0.9800 ?
C12 H12C . 0.9800 ?
C13 H13A . 0.9800 ?
C13 H13B . 0.9800 ?
C13 H13C . 0.9800 ?
C14 H14A . 0.9800 ?
C14 H14B . 0.9800 ?
C14 H14C . 0.9800 ?
C15 C20 . 1.397(3) ?
C15 C16 . 1.401(3) ?
C16 C17 . 1.391(3) ?
C16 C21 . 1.501(3) ?
C17 C18 . 1.391(3) ?
C17 H17 . 0.9500 ?
C18 C19 . 1.379(3) ?
C18 C22 . 1.513(3) ?
C19 C20 . 1.396(3) ?
C19 H19 . 0.9500 ?
C20 C23 . 1.511(3) ?
C21 H21A . 0.9800 ?
C21 H21B . 0.9800 ?
C21 H21C . 0.9800 ?
C22 H22A . 0.9800 ?
C22 H22B . 0.9800 ?
C22 H22C . 0.9800 ?
C23 H23A . 0.9800 ?
C23 H23B . 0.9800 ?
C23 H23C . 0.9800 ?
N2 C32 . 1.489(3) ?
N2 C24 . 1.491(4) ?
N2 C33 . 1.501(3) ?
C24 C25 . 1.497(3) ?
C24 H24A . 0.9900 ?
C24 H24B . 0.9900 ?
C25 C26 . 1.393(3) ?
C25 C30 . 1.421(5) ?
C26 C27 . 1.383(5) ?
C26 H26 . 0.9500 ?
C27 C28 . 1.382(5) ?
C27 H27 . 0.9500 ?
C28 C29 . 1.388(4) ?
C28 H28 . 0.9500 ?
C29 C30 . 1.401(4) ?
C29 H29 . 0.9500 ?
C30 C31 . 1.462(3) ?
C31 H31 . 0.9500 ?
C32 H32A . 0.9800 ?
C32 H32B . 0.9800 ?
C32 H32C . 0.9800 ?
C33 C34 . 1.511(4) ?
C33 H33A . 0.9900 ?
C33 H33B . 0.9900 ?
C34 O1 . 1.420(3) ?
C34 H34A . 0.9900 ?
C34 H34B . 0.9900 ?
O1 C35 . 1.408(4) ?
C35 H35A . 0.9800 ?
C35 H35B . 0.9800 ?
C35 H35C . 0.9800 ?
N2' C24' . 1.465(17) ?
N2' C32' . 1.472(18) ?
N2' C33' . 1.486(16) ?
C24' C25' . 1.514(15) ?
C24' H24C . 0.9900 ?
C24' H24D . 0.9900 ?
C25' C26' . 1.393(15) ?
C25' C30' . 1.423(17) ?
C26' C27' . 1.380(17) ?
C26' H26' . 0.9500 ?
C27' C28' . 1.379(18) ?
C27' H27' . 0.9500 ?
C28' C29' . 1.407(17) ?
C28' H28' . 0.9500 ?
C29' C30' . 1.410(16) ?
C29' H29' . 0.9500 ?
C30' C31' . 1.465(17) ?
C31' H31' . 0.9500 ?
C32' H32D . 0.9800 ?
C32' H32E . 0.9800 ?
C32' H32F . 0.9800 ?
C33' C34' . 1.480(16) ?
C33' H33C . 0.9900 ?
C33' H33D . 0.9900 ?
C34' O1' . 1.421(17) ?
C34' H34C . 0.9900 ?
C34' H34D . 0.9900 ?
O1' C35' . 1.407(17) ?
C35' H35D . 0.9800 ?
C35' H35E . 0.9800 ?
C35' H35F . 0.9800 ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
C4 H4A Cl1 2_645 0.99 2.89 3.651(2) 134.3 yes
C5 H5B Cl1 2_645 0.99 2.83 3.622(2) 137.0 yes
C24 H24A Cl2 . 0.99 2.56 3.257(3) 127.0 yes
C24 H24B Cl2 2_755 0.99 2.72 3.693(3) 166.8 yes
C33 H33B Cl2 . 0.99 2.87 3.399(3) 114.4 yes
C34 H34A Cl1 . 0.99 2.94 3.570(3) 122.7 yes
C24' H24D Cl1 . 0.99 2.68 3.391(19) 129.1 yes
C32' H32D Cl2' . 0.98 2.59 3.07(2) 110.1 yes
C32' H32F Cl2' 2_755 0.98 2.62 3.57(2) 163.6 yes
C4 H4A Cl1 2_645 0.99 2.89 3.651(2) 134.3 yes
C5 H5B Cl1 2_645 0.99 2.83 3.622(2) 137.0 yes
C24 H24A Cl2 . 0.99 2.56 3.257(3) 127.0 yes
C24 H24B Cl2 2_755 0.99 2.72 3.693(3) 166.8 yes
C33 H33B Cl2 . 0.99 2.87 3.399(3) 114.4 yes
C34 H34A Cl1 . 0.99 2.94 3.570(3) 122.7 yes
C24' H24D Cl1 . 0.99 2.68 3.391(19) 129.1 yes
C32' H32D Cl2' . 0.98 2.59 3.07(2) 110.1 yes
C32' H32F Cl2' 2_755 0.98 2.62 3.57(2) 163.6 yes
C34' H34C Cg3 . 0.99 2.96 3.83(2) 149 yes
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
C15 N3 C2 N1 . . . . -167.34(17) ?
C4 N3 C2 N1 . . . . 1.9(2) ?
C15 N3 C2 Ru1 . . . . 24.1(2) ?
C4 N3 C2 Ru1 . . . . -166.63(14) ?
C6 N1 C2 N3 . . . . 170.61(17) ?
C5 N1 C2 N3 . . . . 0.9(2) ?
C6 N1 C2 Ru1 . . . . -22.5(3) ?
C5 N1 C2 Ru1 . . . . 167.80(14) ?
C2 N3 C4 C5 . . . . -3.7(2) ?
C15 N3 C4 C5 . . . . 166.58(17) ?
C2 N1 C5 C4 . . . . -3.1(2) ?
C6 N1 C5 C4 . . . . -174.01(16) ?
N3 C4 C5 N1 . . . . 3.7(2) ?
C2 N1 C6 C11 . . . . -78.7(2) ?
C5 N1 C6 C11 . . . . 90.8(2) ?
C2 N1 C6 C7 . . . . 104.2(2) ?
C5 N1 C6 C7 . . . . -86.3(2) ?
C11 C6 C7 C8 . . . . 2.9(3) ?
N1 C6 C7 C8 . . . . 179.88(17) ?
C11 C6 C7 C12 . . . . -177.59(19) ?
N1 C6 C7 C12 . . . . -0.6(3) ?
C6 C7 C8 C9 . . . . -0.3(3) ?
C12 C7 C8 C9 . . . . -179.8(2) ?
C7 C8 C9 C10 . . . . -2.2(3) ?
C7 C8 C9 C13 . . . . 176.8(2) ?
C8 C9 C10 C11 . . . . 2.2(3) ?
C13 C9 C10 C11 . . . . -176.80(19) ?
C9 C10 C11 C6 . . . . 0.3(3) ?
C9 C10 C11 C14 . . . . 177.06(18) ?
C7 C6 C11 C10 . . . . -2.9(3) ?
N1 C6 C11 C10 . . . . -179.88(16) ?
C7 C6 C11 C14 . . . . -179.65(18) ?
N1 C6 C11 C14 . . . . 3.3(3) ?
C2 N3 C15 C20 . . . . -105.2(2) ?
C4 N3 C15 C20 . . . . 85.9(2) ?
C2 N3 C15 C16 . . . . 81.5(2) ?
C4 N3 C15 C16 . . . . -87.4(2) ?
C20 C15 C16 C17 . . . . 5.4(3) ?
N3 C15 C16 C17 . . . . 178.51(18) ?
C20 C15 C16 C21 . . . . -172.71(19) ?
N3 C15 C16 C21 . . . . 0.4(3) ?
C15 C16 C17 C18 . . . . -2.5(3) ?
C21 C16 C17 C18 . . . . 175.7(2) ?
C16 C17 C18 C19 . . . . -1.5(3) ?
C16 C17 C18 C22 . . . . 179.6(2) ?
C17 C18 C19 C20 . . . . 2.7(4) ?
C22 C18 C19 C20 . . . . -178.4(2) ?
C18 C19 C20 C15 . . . . 0.1(3) ?
C18 C19 C20 C23 . . . . -179.1(2) ?
C16 C15 C20 C19 . . . . -4.2(3) ?
N3 C15 C20 C19 . . . . -177.24(18) ?
C16 C15 C20 C23 . . . . 174.9(2) ?
N3 C15 C20 C23 . . . . 1.9(3) ?
C32 N2 C24 C25 . . . . -60.4(3) ?
C33 N2 C24 C25 . . . . -176.1(2) ?
Ru1 N2 C24 C25 . . . . 65.6(2) ?
N2 C24 C25 C26 . . . . 138.3(2) ?
N2 C24 C25 C30 . . . . -42.9(4) ?
C30 C25 C26 C27 . . . . -1.6(5) ?
C24 C25 C26 C27 . . . . 177.2(3) ?
C25 C26 C27 C28 . . . . 0.3(5) ?
C26 C27 C28 C29 . . . . 0.5(5) ?
C27 C28 C29 C30 . . . . 0.2(5) ?
C28 C29 C30 C25 . . . . -1.5(6) ?
C28 C29 C30 C31 . . . . 179.1(4) ?
C26 C25 C30 C29 . . . . 2.2(6) ?
C24 C25 C30 C29 . . . . -176.6(3) ?
C26 C25 C30 C31 . . . . -178.5(4) ?
C24 C25 C30 C31 . . . . 2.8(7) ?
C29 C30 C31 Ru1 . . . . -178.9(3) ?
C25 C30 C31 Ru1 . . . . 1.7(8) ?
C2 Ru1 C31 C30 . . . . -156.7(4) ?
N2 Ru1 C31 C30 . . . . 18.9(5) ?
Cl2 Ru1 C31 C30 . . . . -68.3(5) ?
Cl1 Ru1 C31 C30 . . . . 106.8(4) ?
C32 N2 C33 C34 . . . . 78.3(3) ?
C24 N2 C33 C34 . . . . -166.5(2) ?
Ru1 N2 C33 C34 . . . . -49.6(3) ?
N2 C33 C34 O1 . . . . -162.1(2) ?
C33 C34 O1 C35 . . . . -169.0(3) ?
C32' N2' C24' C25' . . . . 53(2) ?
C33' N2' C24' C25' . . . . 172.0(16) ?
Ru1 N2' C24' C25' . . . . -68.4(17) ?
N2' C24' C25' C26' . . . . -128(2) ?
N2' C24' C25' C30' . . . . 51(4) ?
C30' C25' C26' C27' . . . . 2(4) ?
C24' C25' C26' C27' . . . . -178(2) ?
C25' C26' C27' C28' . . . . 16(4) ?
C26' C27' C28' C29' . . . . -22(5) ?
C27' C28' C29' C30' . . . . 9(5) ?
C28' C29' C30' C25' . . . . 9(7) ?
C28' C29' C30' C31' . . . . 177(4) ?
C26' C25' C30' C29' . . . . -15(6) ?
C24' C25' C30' C29' . . . . 166(3) ?
C26' C25' C30' C31' . . . . 178(4) ?
C24' C25' C30' C31' . . . . -1(7) ?
C29' C30' C31' Ru1 . . . . 175(3) ?
C25' C30' C31' Ru1 . . . . -16(8) ?
C2 Ru1 C31' C30' . . . . -174(5) ?
N2' Ru1 C31' C30' . . . . -5(5) ?
Cl1 Ru1 C31' C30' . . . . 87(5) ?
Cl2' Ru1 C31' C30' . . . . -95(5) ?
C24' N2' C33' C34' . . . . 160(2) ?
C32' N2' C33' C34' . . . . -80(2) ?
Ru1 N2' C33' C34' . . . . 44(2) ?
N2' C33' C34' O1' . . . . 147(2) ?
C33' C34' O1' C35' . . . . 171(3) ?