#------------------------------------------------------------------------------
#$Date: 2024-02-05 13:07:49 +0100 (Mon, 05 Feb 2024) $
#$Revision: 289690 $
#$URL: svn://www.crystallography.net/cod/cif/2/02/29/2022980.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2022980
loop_
_publ_author_name
'Upmann, Daniel'
'Jones, Peter G.'
'Bockfeld, Dirk'
'Târcoveanu, Eliza'
_publ_section_title
;
Crystal structures of sixteen phosphane chalcogenide complexes of gold(I)
chloride, bromide and iodide.
;
_journal_coeditor_code YZ2044
_journal_issue 'Pt 1'
_journal_name_full
'Acta crystallographica. Section E, Crystallographic communications'
_journal_page_first 34
_journal_page_last 49
_journal_paper_doi 10.1107/S2056989023010459
_journal_volume 80
_journal_year 2024
_chemical_formula_iupac '[Au I (C11 H25 P Se)]'
_chemical_formula_moiety 'C11 H25 Au I P Se'
_chemical_formula_sum 'C11 H25 Au I P Se'
_chemical_formula_weight 591.10
_chemical_name_systematic
;
[Bis(tert-butyl)(propan-2-yl)phosphane selenide-\kSe]iodidogold
;
_space_group_crystal_system tetragonal
_space_group_IT_number 96
_space_group_name_Hall 'P 4nw 2abw'
_space_group_name_H-M_alt 'P 43 21 2'
_atom_sites_solution_hydrogens geom
_atom_sites_solution_primary direct
_atom_sites_solution_secondary difmap
_audit_creation_method SHELXL-2019/3
_cell_angle_alpha 90
_cell_angle_beta 90
_cell_angle_gamma 90
_cell_formula_units_Z 8
_cell_length_a 10.7755(2)
_cell_length_b 10.7755(2)
_cell_length_c 28.3769(5)
_cell_measurement_reflns_used 52249
_cell_measurement_temperature 100(2)
_cell_measurement_theta_max 30.7912
_cell_measurement_theta_min 2.1487
_cell_volume 3294.88(10)
_computing_cell_refinement
;
CrysAlisPro, Version 1.171.35.11 (Rigaku OD, 2020)
;
_computing_data_collection
;
CrysAlisPro, Version 1.171.35.11 (Rigaku OD, 2020)
;
_computing_data_reduction
;
CrysAlisPro, Version 1.171.35.11 (Rigaku OD, 2020)
;
_computing_molecular_graphics
;
Bruker XP (Bruker, 1998)
;
_computing_publication_material
;
SHELXL-2019/3 (Sheldrick, 2015)
;
_computing_structure_refinement
;
SHELXL-2019/3 (Sheldrick, 2015)
;
_computing_structure_solution
;
SHELXS-97 (Sheldrick, 2008)
;
_diffrn_ambient_temperature 100(2)
_diffrn_detector_area_resol_mean 16.1419
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type 'Oxford Diffraction Xcalibur, Eos'
_diffrn_measurement_method '\w scans'
_diffrn_radiation_type MoK\a
_diffrn_radiation_wavelength 0.71073
_diffrn_reflns_av_R_equivalents 0.0441
_diffrn_reflns_av_unetI/netI 0.0134
_diffrn_reflns_limit_h_max 15
_diffrn_reflns_limit_h_min -15
_diffrn_reflns_limit_k_max 15
_diffrn_reflns_limit_k_min -15
_diffrn_reflns_limit_l_max 39
_diffrn_reflns_limit_l_min -39
_diffrn_reflns_number 140787
_diffrn_reflns_theta_full 30.000
_diffrn_reflns_theta_max 30.032
_diffrn_reflns_theta_min 2.373
_diffrn_source 'fine-focus sealed tube'
_exptl_absorpt_coefficient_mu 13.085
_exptl_absorpt_correction_T_max 0.2443
_exptl_absorpt_correction_T_min 0.0916
_exptl_absorpt_correction_type multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro, Version 1.171.35.11 (Rigaku OD, 2020)
;
_exptl_crystal_colour colourless
_exptl_crystal_density_diffrn 2.383
_exptl_crystal_density_method 'not measured'
_exptl_crystal_description plate
_exptl_crystal_F_000 2176
_exptl_crystal_size_max 0.35
_exptl_crystal_size_mid 0.2
_exptl_crystal_size_min 0.15
_refine_diff_density_max 1.402
_refine_diff_density_min -1.513
_refine_ls_abs_structure_details
;
Refined as an inversion twin
;
_refine_ls_abs_structure_Flack 0.086(12)
_refine_ls_extinction_method none
_refine_ls_goodness_of_fit_ref 1.421
_refine_ls_hydrogen_treatment constr
_refine_ls_matrix_type full
_refine_ls_number_parameters 145
_refine_ls_number_reflns 4829
_refine_ls_number_restraints 66
_refine_ls_restrained_S_all 1.413
_refine_ls_R_factor_all 0.0327
_refine_ls_R_factor_gt 0.0320
_refine_ls_shift/su_max 0.001
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+46.6959P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.0782
_refine_ls_wR_factor_ref 0.0784
_reflns_number_gt 4768
_reflns_number_total 4829
_reflns_threshold_expression 'I > 2\s(I)'
_cod_data_source_file yz2044sup1.cif
_cod_data_source_block 7c
_cod_depositor_comments
'Adding full bibliography for 2022965--2022980.cif.'
_cod_original_cell_volume 3294.86(14)
_cod_database_code 2022980
_cod_database_fobs_code 2022980
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min 0.092
_shelx_estimated_absorpt_t_max 0.244
_shelx_hkl_file
;
0 0 3 138.899 64.3056 21
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0 0 -4 127646. 2593.57 16
0 0 -4 130823. 2717.70 14
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0 0 -4 126747. 2783.56 17
0 0 4 137243. 2667.16 25
0 0 -4 134194. 2771.79 24
0 0 -4 124783. 2644.66 7
0 0 4 131019. 2708.03 14
0 0 -4 130084. 2663.22 11
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0 0 -4 132298. 2722.54 21
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0 0 4 125896. 2659.28 11
0 0 4 131871. 2649.52 7
0 0 -5 85.4205 116.952 11
0 0 -5 193.193 111.518 14
0 0 5 215.118 120.495 24
0 0 5 482.606 146.007 21
0 0 5 99.2842 97.4982 25
0 0 -5 160.061 110.090 7
0 0 5 664.515 182.568 17
0 0 5 121.467 84.3253 16
0 0 -5 288.155 111.570 25
0 0 5 366.737 129.807 13
0 0 5 345.704 109.408 11
0 0 -5 192.978 85.9877 16
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0 0 -5 248.868 124.267 17
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0 0 -6 670.030 156.479 24
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0 0 -7 319.680 143.683 14
0 0 -7 223.197 134.699 21
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10 -2 -23 3720.50 1154.09 23
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3 10 -9 7480.86 1048.98 7
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10 -3 -9 8710.66 1203.09 15
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10 3 10 29442.8 1726.74 20
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3 10 -10 33932.5 1820.43 20
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-3 10 10 32068.2 1969.27 19
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3 -10 10 32589.5 1704.58 18
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-10 3 -10 33069.6 2108.92 11
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10 -3 -11 23739.6 1724.85 8
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10 -3 -12 30672.0 1969.07 8
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10 3 12 35076.8 1886.89 4
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3 -10 12 30463.3 1749.31 18
3 10 -12 30092.6 1932.21 7
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10 -3 -19 3136.22 803.702 8
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10 -3 -21 18852.1 1513.57 8
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10 -3 -21 21992.2 1888.60 15
10 -3 -21 20244.3 1585.80 26
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10 -3 -22 23276.9 1951.51 2
10 -3 -22 24429.3 2194.45 23
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10 3 22 21965.9 1755.85 20
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10 -3 -22 23079.3 1969.97 15
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3 -10 23 1068.96 726.983 24
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10 -3 -23 1860.44 907.186 23
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3 -10 23 382.254 737.239 13
3 -10 23 3269.07 1100.81 21
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10 -3 -23 426.455 642.251 2
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10 -3 -23 2987.79 945.550 15
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3 -10 24 31631.5 2525.73 24
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10 -3 -24 26772.3 2401.95 23
10 -3 -24 31701.3 2345.48 2
3 10 -24 27948.0 2489.76 22
3 -10 24 25648.3 2213.73 13
3 -10 24 28259.8 2388.68 21
10 3 24 26504.2 1965.89 20
-3 -10 -24 25442.0 1988.22 12
10 3 24 27306.7 1987.20 4
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3 10 -24 28463.8 2023.08 7
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3 -10 25 3972.48 1090.88 24
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10 -3 -25 3436.23 1119.17 23
3 10 -25 3184.52 1019.61 22
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3 -10 25 3013.52 1025.54 13
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3 -10 25 2164.55 935.034 21
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10 -3 -25 4410.41 1040.21 2
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3 -10 26 21987.4 2137.51 24
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10 -3 -26 21272.0 2318.16 23
3 10 -26 16834.2 1965.09 22
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3 -10 26 21449.3 2058.41 13
3 -10 26 21095.1 2117.25 21
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10 -3 -26 19552.6 1980.06 2
3 10 -26 19810.4 1729.60 7
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10 -3 -26 18808.9 1818.50 15
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3 -10 27 18748.1 2034.94 24
10 -3 -27 22168.0 2381.56 23
10 -3 -27 23634.7 2140.30 2
3 10 -27 18606.0 2093.66 22
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3 -10 27 19966.4 2010.18 13
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10 -3 -27 24416.9 2010.51 15
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3 -10 28 14805.7 1826.28 24
10 -3 -28 18304.5 2203.56 23
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3 10 -28 16500.5 1622.75 7
10 -3 -28 18356.8 1797.13 15
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3 -10 29 2124.24 956.815 24
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4 -10 -29 14340.4 1831.46 2
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4 -10 -28 1915.69 766.249 3
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4 -10 -28 3037.01 995.654 2
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4 -10 -27 3253.81 1111.71 2
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10 -4 26 19938.5 1619.50 1
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10 4 -26 17534.6 1892.51 22
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4 -10 -26 23092.0 2133.23 2
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4 -10 -26 18078.5 1693.27 3
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10 -4 25 21596.9 1687.48 1
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4 -10 -25 24448.0 2186.00 2
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1 -15 -1 14662.0 1755.11 13
-1 15 -1 18020.8 2051.57 22
1 15 1 17214.9 1959.52 22
1 -15 -1 17379.4 2055.57 21
15 1 -1 18638.8 1674.94 20
1 15 1 16981.3 1521.26 19
1 -15 -1 21565.5 2265.64 15
-1 15 0 6554.10 1345.58 22
1 -15 0 6450.98 1431.32 13
1 15 0 5429.52 1235.14 22
1 -15 0 4028.19 1280.03 21
15 1 0 5564.20 1101.31 20
1 15 0 4736.80 909.990 19
-1 15 1 17738.9 1993.70 22
1 -15 1 15255.4 1811.74 13
1 15 -1 21037.7 2153.81 22
1 -15 1 15130.5 1975.01 21
15 1 1 16191.8 1555.13 20
1 15 -1 14147.8 1404.43 19
1 15 -2 822.494 736.796 22
1 -15 2 1415.45 934.195 13
1 -15 2 468.498 843.549 21
15 1 2-318.704 596.830 20
1 15 -2 457.780 547.063 19
1 15 -3 132.210 722.194 22
1 -15 3 2791.94 1045.52 13
1 15 -3 1801.28 725.062 19
1 -15 4 7018.02 1347.41 13
1 15 -4 7135.50 1082.93 19
1 15 -5 344.290 533.893 19
-15 -1 5 370.690 650.847 16
1 15 -6 21428.4 1744.29 19
-15 -1 6 20835.5 1853.53 16
1 15 -7 3766.48 1071.50 19
-15 -1 7 3527.11 954.927 16
-15 1 -7 1314.66 756.892 25
1 15 -8 18156.6 1612.89 19
-15 -1 8 17281.1 1659.95 16
-15 1 -8 18911.7 1834.16 25
-15 -1 9 6739.72 1171.51 16
-15 1 -9 6999.64 1254.26 25
-15 2 5 4229.62 952.160 16
-15 2 4 8824.59 1267.45 16
2 -15 -4 10483.3 1746.77 15
2 -15 -3 2224.22 926.511 21
-15 2 3 2663.76 827.336 16
2 -15 -3 3779.54 1222.29 15
-2 15 -2 1752.77 928.044 22
2 -15 -2 2732.33 927.956 13
2 -15 -2 284.427 821.168 21
15 2 -2 2038.64 755.376 20
-15 2 2 1191.68 741.333 16
2 -15 -2 3817.30 1227.39 15
-2 15 -1 5350.26 1250.36 22
2 -15 -1 6049.88 1216.04 13
2 -15 -1 3095.75 967.380 21
15 2 -1 4247.30 918.601 20
2 -15 -1 5043.25 1183.46 15
-2 15 0 936.434 757.149 22
2 -15 0 405.777 666.900 13
2 15 0 1209.48 867.829 22
2 -15 0-1384.75 1062.05 21
15 2 0 312.089 560.151 20
-2 15 1 2934.40 1037.45 22
2 -15 1 3900.20 1051.92 13
2 15 -1 4840.43 1153.53 22
2 -15 1 4718.93 1271.12 21
15 2 1 3183.31 813.543 20
2 15 -2 2874.55 972.721 22
2 -15 2 1078.15 748.212 13
2 -15 2 2429.85 1066.32 21
15 2 2 27.3558 550.918 20
2 15 -3 2085.19 835.475 22
2 -15 3 3132.80 1049.55 13
2 -15 3 2693.60 1119.53 21
15 2 3 3616.27 809.007 20
2 -15 4 4276.30 1137.29 13
15 2 4 6243.60 1048.03 20
2 -15 5 4105.87 1163.64 13
15 2 5 4909.14 1032.68 20
2 -15 6 17086.8 1987.45 13
15 2 6 17464.3 1662.36 20
-15 2 -6 19468.6 1821.48 25
15 2 7 9140.55 1240.14 20
-2 -15 -7 10489.6 1361.34 12
-15 2 -7 9296.96 1379.57 25
-2 -15 -8 18946.5 1709.21 12
-15 2 -8 18638.3 1813.52 25
-2 -15 -9 3198.39 989.621 12
-15 3 4 8887.18 1294.14 16
-15 3 3 2641.74 780.804 16
3 -15 -3 4461.10 1343.47 15
-15 3 2 2933.72 758.978 16
3 -15 -2 3185.30 1127.93 15
-3 -15 1 413.987 551.345 12
-3 15 0-837.818 888.380 22
3 15 0-692.720 807.155 22
-3 -15 0-365.275 590.829 12
-3 15 1 748.226 836.492 22
3 15 -1 1067.27 850.435 22
-3 -15 -1-85.3903 575.702 12
3 -15 2 1528.22 878.906 21
-3 -15 -2 2910.17 795.567 12
3 -15 3 1263.63 924.138 21
-3 -15 -3 1232.31 714.507 12
3 -15 4 10899.1 1787.18 21
-3 -15 -4 9667.60 1277.40 12
-3 -15 -5 10420.6 1441.95 12
-15 3 -6 28337.7 2248.39 25
;
_shelx_hkl_checksum 32851
_shelx_res_file
;
TITL Roman in P4(3)2(1)2
shelx.res
created by SHELXL-2019/3 at 12:15:39 on 19-Oct-2023
CELL 0.71073 10.775461 10.775461 28.376934 90.0000 90.0000 90.0000
ZERR 8.00 0.0002 0.0002 0.0005 0.0000 0.0000 0.0000
LATT -1
SYMM -x,-y, z+1/2
SYMM -y+1/2, x+1/2, z+3/4
SYMM y+1/2,-x+1/2, z+1/4
SYMM -x+1/2, y+1/2,-z+3/4
SYMM x+1/2,-y+1/2,-z+1/4
SYMM y, x,-z
SYMM -y,-x,-z+1/2
SFAC C H P Se I Au
UNIT 88.00 200.00 8.00 8.00 8.00 8.00
L.S. 6
FMAP 2
PLAN 10
TWIN
ISOR $C 0.01
OMIT 0 11 4
OMIT 1 12 16
OMIT -1 12 16
OMIT 6 12 0
OMIT 0 12 18
OMIT 4 12 0
OMIT 0 12 2
OMIT 5 11 0
TEMP -173
SIZE 0.35 0.2 0.15
SHEL 999 0.71
ACTA 60
CONF 2.3
BOND $H
HTAB C23 AU1
HTAB C32 SE1
EQIV $1 0.5-x, -0.5+y, 0.75-z
EQIV $2 0.5-x, 0.5+y, 0.75-z
EQIV $3 1-y,-x,0.5-z
HTAB C11 I1_$1
HTAB C21 I1_$2
HTAB C22 I1_$2
HTAB C31 I1_$3
HTAB C31 AU1_$3
EQIV $4 -y, -x, 0.5-z
RTAB CONT AU1 I1_$4
RTAB CONT AU1 SE1_$4
WGHT 0.000000 46.695900
BASF 0.08568
FVAR 1.15385
AU1 6 0.104748 0.018957 0.293171 11.00000 0.01105 0.01416 =
0.01408 -0.00219 -0.00131 0.00213
I1 5 -0.066255 0.015981 0.355325 11.00000 0.01695 0.01615 =
0.01721 -0.00046 0.00297 0.00338
P1 3 0.438360 0.027977 0.277106 11.00000 0.01051 0.01213 =
0.00974 -0.00046 0.00084 0.00068
SE1 4 0.266713 0.034954 0.235362 11.00000 0.01311 0.02347 =
0.00961 -0.00172 -0.00205 -0.00144
C1 1 0.469565 -0.136765 0.295210 11.00000 0.01855 0.01696 =
0.02777 0.00196 -0.00045 0.00259
C2 1 0.436964 0.138643 0.328122 11.00000 0.01890 0.02205 =
0.01125 -0.00204 -0.00305 -0.00356
C3 1 0.555166 0.071115 0.231923 11.00000 0.01448 0.02300 =
0.01480 0.00091 0.00251 -0.00937
AFIX 13
H3 2 0.535450 0.016609 0.204401 11.00000 -1.20000
AFIX 0
C11 1 0.583863 -0.147124 0.328792 11.00000 0.00961 0.02564 =
0.04307 0.00919 -0.00580 0.00434
AFIX 137
H11A 2 0.563922 -0.108623 0.359150 11.00000 -1.50000
H11B 2 0.655008 -0.104467 0.314634 11.00000 -1.50000
H11C 2 0.604403 -0.234785 0.333673 11.00000 -1.50000
AFIX 0
C12 1 0.495935 -0.210553 0.249718 11.00000 0.02214 0.01885 =
0.05469 -0.01154 0.00985 -0.00661
AFIX 137
H12A 2 0.502361 -0.299102 0.257209 11.00000 -1.50000
H12B 2 0.574083 -0.181913 0.235796 11.00000 -1.50000
H12C 2 0.428115 -0.197522 0.227246 11.00000 -1.50000
AFIX 0
C13 1 0.353951 -0.196436 0.317852 11.00000 0.02339 0.02015 =
0.04463 0.01395 0.00874 -0.00334
AFIX 137
H13A 2 0.285826 -0.197354 0.294975 11.00000 -1.50000
H13B 2 0.329194 -0.148209 0.345581 11.00000 -1.50000
H13C 2 0.373363 -0.281666 0.327387 11.00000 -1.50000
AFIX 0
C21 1 0.572041 0.171227 0.341695 11.00000 0.01998 0.02365 =
0.02375 -0.01289 -0.00699 -0.00029
AFIX 137
H21A 2 0.612486 0.213461 0.315245 11.00000 -1.50000
H21B 2 0.617442 0.094919 0.349167 11.00000 -1.50000
H21C 2 0.571818 0.225956 0.369277 11.00000 -1.50000
AFIX 0
C22 1 0.369631 0.257452 0.313928 11.00000 0.01885 0.02494 =
0.03642 -0.01345 -0.00630 0.00671
AFIX 137
H22A 2 0.280471 0.240883 0.311313 11.00000 -1.50000
H22B 2 0.401378 0.286347 0.283482 11.00000 -1.50000
H22C 2 0.383792 0.321443 0.337872 11.00000 -1.50000
AFIX 0
C23 1 0.369339 0.084359 0.370367 11.00000 0.01776 0.03886 =
0.01665 -0.00384 0.00019 0.00629
AFIX 137
H23A 2 0.383259 0.137216 0.397969 11.00000 -1.50000
H23B 2 0.400907 0.000742 0.376757 11.00000 -1.50000
H23C 2 0.280248 0.080119 0.363613 11.00000 -1.50000
AFIX 0
C31 1 0.693717 0.048096 0.241412 11.00000 0.01026 0.03751 =
0.02843 0.00283 0.00556 -0.00177
AFIX 137
H31A 2 0.741704 0.068017 0.213067 11.00000 -1.50000
H31B 2 0.706479 -0.039266 0.249700 11.00000 -1.50000
H31C 2 0.721297 0.100862 0.267518 11.00000 -1.50000
AFIX 0
C32 1 0.535341 0.205022 0.213136 11.00000 0.03448 0.03542 =
0.02286 0.01225 -0.00030 -0.01358
AFIX 137
H32A 2 0.572170 0.264555 0.235183 11.00000 -1.50000
H32B 2 0.446257 0.221538 0.210131 11.00000 -1.50000
H32C 2 0.575086 0.213473 0.182239 11.00000 -1.50000
AFIX 0
HKLF 4
REM Roman in P4(3)2(1)2
REM wR2 = 0.0784, GooF = S = 1.421, Restrained GooF = 1.413 for all data
REM R1 = 0.0320 for 4768 Fo > 4sig(Fo) and 0.0327 for all 4829 data
REM 145 parameters refined using 66 restraints
END
WGHT 0.0000 46.7015
REM Highest difference peak 1.402, deepest hole -1.513, 1-sigma level 0.228
Q1 1 0.1681 0.0246 0.2918 11.00000 0.05 1.40
Q2 1 0.1031 0.0589 0.2642 11.00000 0.05 1.27
Q3 1 0.1015 0.1004 0.2926 11.00000 0.05 1.25
Q4 1 0.3950 0.3413 0.3972 11.00000 0.05 1.10
Q5 1 -0.0634 0.0226 0.3892 11.00000 0.05 1.00
Q6 1 0.6151 0.2593 0.1286 11.00000 0.05 0.99
Q7 1 -0.1028 -0.0578 0.3455 11.00000 0.05 0.98
Q8 1 -0.1231 0.0441 0.2941 11.00000 0.05 0.97
Q9 1 0.1063 0.0123 0.3226 11.00000 0.05 0.95
Q10 1 -0.1550 0.0914 0.3526 11.00000 0.05 0.92
;
_shelx_res_checksum 29007
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, z+1/2'
'-y+1/2, x+1/2, z+3/4'
'y+1/2, -x+1/2, z+1/4'
'-x+1/2, y+1/2, -z+3/4'
'x+1/2, -y+1/2, -z+1/4'
'y, x, -z'
'-y, -x, -z+1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au Au1 0.10475(3) 0.01896(4) 0.29317(2) 0.01310(8) Uani d 1 . .
I I1 -0.06625(6) 0.01598(7) 0.35532(2) 0.01677(13) Uani d 1 . .
P P1 0.4384(2) 0.0280(3) 0.27711(9) 0.0108(4) Uani d 1 . .
Se Se1 0.26671(10) 0.03495(11) 0.23536(4) 0.0154(2) Uani d 1 . .
C C1 0.4696(11) -0.1368(10) 0.2952(4) 0.021(2) Uani d 1 . .
C C2 0.4370(11) 0.1386(11) 0.3281(4) 0.017(2) Uani d 1 . .
C C3 0.5552(10) 0.0711(11) 0.2319(4) 0.017(2) Uani d 1 . .
H H3 0.535450 0.016609 0.204401 0.021 Uiso calc 1 . .
C C11 0.5839(11) -0.1471(13) 0.3288(5) 0.026(3) Uani d 1 . .
H H11A 0.563922 -0.108623 0.359150 0.039 Uiso calc 1 . .
H H11B 0.655008 -0.104467 0.314634 0.039 Uiso calc 1 . .
H H11C 0.604403 -0.234785 0.333673 0.039 Uiso calc 1 . .
C C12 0.4959(12) -0.2106(12) 0.2497(5) 0.032(3) Uani d 1 . .
H H12A 0.502361 -0.299102 0.257209 0.048 Uiso calc 1 . .
H H12B 0.574083 -0.181913 0.235796 0.048 Uiso calc 1 . .
H H12C 0.428115 -0.197522 0.227246 0.048 Uiso calc 1 . .
C C13 0.3540(13) -0.1964(12) 0.3179(5) 0.029(3) Uani d 1 . .
H H13A 0.285826 -0.197354 0.294975 0.044 Uiso calc 1 . .
H H13B 0.329194 -0.148209 0.345581 0.044 Uiso calc 1 . .
H H13C 0.373363 -0.281666 0.327387 0.044 Uiso calc 1 . .
C C21 0.5720(11) 0.1712(12) 0.3417(4) 0.022(2) Uani d 1 . .
H H21A 0.612486 0.213461 0.315245 0.034 Uiso calc 1 . .
H H21B 0.617442 0.094919 0.349167 0.034 Uiso calc 1 . .
H H21C 0.571818 0.225956 0.369277 0.034 Uiso calc 1 . .
C C22 0.3696(11) 0.2575(12) 0.3139(5) 0.027(3) Uani d 1 . .
H H22A 0.280471 0.240883 0.311313 0.040 Uiso calc 1 . .
H H22B 0.401378 0.286347 0.283482 0.040 Uiso calc 1 . .
H H22C 0.383792 0.321443 0.337872 0.040 Uiso calc 1 . .
C C23 0.3693(11) 0.0844(13) 0.3704(4) 0.024(3) Uani d 1 . .
H H23A 0.383259 0.137216 0.397969 0.037 Uiso calc 1 . .
H H23B 0.400907 0.000742 0.376757 0.037 Uiso calc 1 . .
H H23C 0.280248 0.080119 0.363613 0.037 Uiso calc 1 . .
C C31 0.6937(10) 0.0481(13) 0.2414(5) 0.025(3) Uani d 1 . .
H H31A 0.741704 0.068017 0.213067 0.038 Uiso calc 1 . .
H H31B 0.706479 -0.039266 0.249700 0.038 Uiso calc 1 . .
H H31C 0.721297 0.100862 0.267518 0.038 Uiso calc 1 . .
C C32 0.5353(14) 0.2050(13) 0.2131(4) 0.031(3) Uani d 1 . .
H H32A 0.572170 0.264555 0.235183 0.046 Uiso calc 1 . .
H H32B 0.446257 0.221538 0.210131 0.046 Uiso calc 1 . .
H H32C 0.575086 0.213473 0.182239 0.046 Uiso calc 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Au1 0.01105(16) 0.01416(16) 0.01408(15) 0.00213(13) -0.00131(13) -0.00219(13)
I1 0.0170(3) 0.0162(3) 0.0172(3) 0.0034(2) 0.0030(2) -0.0005(2)
P1 0.0105(10) 0.0121(11) 0.0097(10) 0.0007(9) 0.0008(8) -0.0005(9)
Se1 0.0131(4) 0.0235(5) 0.0096(4) -0.0014(4) -0.0020(3) -0.0017(4)
C1 0.019(5) 0.017(5) 0.028(5) 0.003(4) 0.000(5) 0.002(4)
C2 0.019(5) 0.022(5) 0.011(4) -0.004(4) -0.003(4) -0.002(4)
C3 0.014(4) 0.023(5) 0.015(4) -0.009(4) 0.003(4) 0.001(4)
C11 0.010(5) 0.026(6) 0.043(7) 0.004(4) -0.006(5) 0.009(5)
C12 0.022(6) 0.019(5) 0.055(8) -0.007(5) 0.010(6) -0.012(5)
C13 0.023(6) 0.020(6) 0.045(7) -0.003(5) 0.009(5) 0.014(5)
C21 0.020(6) 0.024(6) 0.024(6) 0.000(4) -0.007(4) -0.013(4)
C22 0.019(6) 0.025(6) 0.036(6) 0.007(4) -0.006(5) -0.013(5)
C23 0.018(5) 0.039(7) 0.017(5) 0.006(5) 0.000(4) -0.004(5)
C31 0.010(5) 0.038(7) 0.028(6) -0.002(5) 0.006(4) 0.003(5)
C32 0.034(7) 0.035(7) 0.023(6) -0.014(6) 0.000(5) 0.012(5)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
Se1 Au1 I1 . . 176.56(4) y
Se1 Au1 Au1 . 8 78.63(3) y
I1 Au1 Au1 . 8 103.36(2) y
C3 P1 C2 . . 112.3(5) y
C3 P1 C1 . . 107.7(5) y
C2 P1 C1 . . 113.0(5) y
C3 P1 Se1 . . 100.9(4) y
C2 P1 Se1 . . 112.8(4) y
C1 P1 Se1 . . 109.3(4) y
P1 Se1 Au1 . . 103.94(8) y
C13 C1 C12 . . 106.4(10) ?
C13 C1 C11 . . 110.7(10) ?
C12 C1 C11 . . 109.2(10) ?
C13 C1 P1 . . 111.3(8) ?
C12 C1 P1 . . 106.9(9) ?
C11 C1 P1 . . 112.1(8) ?
C23 C2 C22 . . 107.6(10) ?
C23 C2 C21 . . 110.0(9) ?
C22 C2 C21 . . 108.8(10) ?
C23 C2 P1 . . 111.6(8) ?
C22 C2 P1 . . 109.5(8) ?
C21 C2 P1 . . 109.2(8) ?
C31 C3 C32 . . 110.1(10) ?
C31 C3 P1 . . 119.8(8) ?
C32 C3 P1 . . 112.1(9) ?
C31 C3 H3 . . 104.4 ?
C32 C3 H3 . . 104.4 ?
P1 C3 H3 . . 104.4 ?
C1 C11 H11A . . 109.5 ?
C1 C11 H11B . . 109.5 ?
H11A C11 H11B . . 109.5 ?
C1 C11 H11C . . 109.5 ?
H11A C11 H11C . . 109.5 ?
H11B C11 H11C . . 109.5 ?
C1 C12 H12A . . 109.5 ?
C1 C12 H12B . . 109.5 ?
H12A C12 H12B . . 109.5 ?
C1 C12 H12C . . 109.5 ?
H12A C12 H12C . . 109.5 ?
H12B C12 H12C . . 109.5 ?
C1 C13 H13A . . 109.5 ?
C1 C13 H13B . . 109.5 ?
H13A C13 H13B . . 109.5 ?
C1 C13 H13C . . 109.5 ?
H13A C13 H13C . . 109.5 ?
H13B C13 H13C . . 109.5 ?
C2 C21 H21A . . 109.5 ?
C2 C21 H21B . . 109.5 ?
H21A C21 H21B . . 109.5 ?
C2 C21 H21C . . 109.5 ?
H21A C21 H21C . . 109.5 ?
H21B C21 H21C . . 109.5 ?
C2 C22 H22A . . 109.5 ?
C2 C22 H22B . . 109.5 ?
H22A C22 H22B . . 109.5 ?
C2 C22 H22C . . 109.5 ?
H22A C22 H22C . . 109.5 ?
H22B C22 H22C . . 109.5 ?
C2 C23 H23A . . 109.5 ?
C2 C23 H23B . . 109.5 ?
H23A C23 H23B . . 109.5 ?
C2 C23 H23C . . 109.5 ?
H23A C23 H23C . . 109.5 ?
H23B C23 H23C . . 109.5 ?
C3 C31 H31A . . 109.5 ?
C3 C31 H31B . . 109.5 ?
H31A C31 H31B . . 109.5 ?
C3 C31 H31C . . 109.5 ?
H31A C31 H31C . . 109.5 ?
H31B C31 H31C . . 109.5 ?
C3 C32 H32A . . 109.5 ?
C3 C32 H32B . . 109.5 ?
H32A C32 H32B . . 109.5 ?
C3 C32 H32C . . 109.5 ?
H32A C32 H32C . . 109.5 ?
H32B C32 H32C . . 109.5 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Au1 Se1 . 2.4014(11) y
Au1 I1 . 2.5509(8) y
Au1 Au1 8 3.0914(8) y
P1 C3 . 1.856(11) ?
P1 C2 . 1.876(11) ?
P1 C1 . 1.878(11) ?
P1 Se1 . 2.198(3) y
C1 C13 . 1.542(17) ?
C1 C12 . 1.543(18) ?
C1 C11 . 1.561(17) ?
C2 C23 . 1.520(16) ?
C2 C22 . 1.526(17) ?
C2 C21 . 1.546(16) ?
C3 C31 . 1.537(16) ?
C3 C32 . 1.553(17) ?
C3 H3 . 1.0000 ?
C11 H11A . 0.9800 ?
C11 H11B . 0.9800 ?
C11 H11C . 0.9800 ?
C12 H12A . 0.9800 ?
C12 H12B . 0.9800 ?
C12 H12C . 0.9800 ?
C13 H13A . 0.9800 ?
C13 H13B . 0.9800 ?
C13 H13C . 0.9800 ?
C21 H21A . 0.9800 ?
C21 H21B . 0.9800 ?
C21 H21C . 0.9800 ?
C22 H22A . 0.9800 ?
C22 H22B . 0.9800 ?
C22 H22C . 0.9800 ?
C23 H23A . 0.9800 ?
C23 H23B . 0.9800 ?
C23 H23C . 0.9800 ?
C31 H31A . 0.9800 ?
C31 H31B . 0.9800 ?
C31 H31C . 0.9800 ?
C32 H32A . 0.9800 ?
C32 H32B . 0.9800 ?
C32 H32C . 0.9800 ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
C23 H23C Au1 . 0.98 2.83 3.664(12) 143.5 yes
C32 H32B Se1 . 0.98 2.88 3.483(13) 120.6 yes
C11 H11C I1 5_545 0.98 3.22 4.088(13) 148.3 yes
C21 H21C I1 5 0.98 3.21 4.008(12) 140.0 yes
C22 H22C I1 5 0.98 3.30 4.183(12) 151.6 yes
C31 H31A I1 8_655 0.98 3.25 4.166(11) 155.8 yes
C31 H31A Au1 8_655 0.98 3.19 3.642(12) 110.2 yes
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
C3 P1 Se1 Au1 . . . . -169.6(4) y
C2 P1 Se1 Au1 . . . . -49.5(4) y
C1 P1 Se1 Au1 . . . . 77.1(4) y
C3 P1 C1 C13 . . . . -159.2(9) ?
I1 Au1 Au1 I1 . . 8 8 117.89(4) y
Se1 Au1 Au1 Se1 . . 8 8 123.62(6) y
I1 Au1 Au1 Se1 . . 8 8 -59.25(3) y
C2 P1 C1 C13 . . . . 76.2(10) ?
Se1 P1 C1 C13 . . . . -50.3(10) ?
C3 P1 C1 C12 . . . . -43.4(9) ?
C2 P1 C1 C12 . . . . -168.0(8) ?
Se1 P1 C1 C12 . . . . 65.5(9) ?
C3 P1 C1 C11 . . . . 76.3(10) ?
C2 P1 C1 C11 . . . . -48.4(10) ?
Se1 P1 C1 C11 . . . . -174.9(8) ?
C3 P1 C2 C23 . . . . -164.0(8) ?
C1 P1 C2 C23 . . . . -41.8(10) ?
Se1 P1 C2 C23 . . . . 82.8(8) ?
C3 P1 C2 C22 . . . . 77.0(9) ?
C1 P1 C2 C22 . . . . -160.9(8) ?
Se1 P1 C2 C22 . . . . -36.3(9) ?
C3 P1 C2 C21 . . . . -42.1(10) ?
C1 P1 C2 C21 . . . . 80.0(9) ?
Se1 P1 C2 C21 . . . . -155.4(7) ?
C2 P1 C3 C31 . . . . 74.6(11) ?
C1 P1 C3 C31 . . . . -50.5(11) ?
Se1 P1 C3 C31 . . . . -165.0(9) ?
C2 P1 C3 C32 . . . . -56.8(10) ?
C1 P1 C3 C32 . . . . 178.1(8) ?
Se1 P1 C3 C32 . . . . 63.6(8) ?