#------------------------------------------------------------------------------ #$Date: 2023-12-20 04:03:28 +0100 (Wed, 20 Dec 2023) $ #$Revision: 288434 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/29/2022978.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022978 loop_ _publ_author_name 'Upmann, Daniel' 'Jones, Peter G.' 'Bockfeld, Dirk' 'T\^arcoveanu, Eliza' _publ_section_title ; Crystal structures of sixteen phosphane chalcogenide complexes of gold(I) chloride, bromide and iodide ; _journal_coeditor_code YZ2044 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E Crystallographic Communications' _journal_paper_doi 10.1107/S2056989023010459 _journal_volume 80 _journal_year 2023 _chemical_formula_iupac '[Au I (C10 H23 P S)]' _chemical_formula_moiety 'C10 H23 Au I P S' _chemical_formula_sum 'C10 H23 Au I P S' _chemical_formula_weight 530.18 _chemical_name_systematic ; [(tert-Butyl)bis(propan-2-yl)phosphane sulfide-\kS]iodidogold ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2019/3 _cell_angle_alpha 90 _cell_angle_beta 91.202(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 8.6010(2) _cell_length_b 15.0435(3) _cell_length_c 11.7218(2) _cell_measurement_reflns_used 18460 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 30.7945 _cell_measurement_theta_min 2.1985 _cell_volume 1516.34(5) _computing_cell_refinement ; CrysAlisPro, Version 1.171.35.19 (Rigaku OD, 2020) ; _computing_data_collection ; CrysAlisPro, Version 1.171.35.19 (Rigaku OD, 2020) ; _computing_data_reduction ; CrysAlisPro, Version 1.171.35.19 (Rigaku OD, 2020) ; _computing_molecular_graphics ; Bruker XP (Bruker, 1998) ; _computing_publication_material ; SHELXL-2019/3 (Sheldrick, 2015) ; _computing_structure_refinement ; SHELXL-2019/3 (Sheldrick, 2015) ; _computing_structure_solution ; SHELXS-97 (Sheldrick, 2008) ; _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean 16.1419 _diffrn_measured_fraction_theta_full 0.993 _diffrn_measured_fraction_theta_max 0.959 _diffrn_measurement_device_type 'Oxford Diffraction Xcalibur, Eos' _diffrn_measurement_method '\w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0442 _diffrn_reflns_av_unetI/netI 0.0228 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_number 54148 _diffrn_reflns_theta_full 30.000 _diffrn_reflns_theta_max 30.863 _diffrn_reflns_theta_min 2.203 _diffrn_source 'fine-focus sealed tube' _exptl_absorpt_coefficient_mu 11.950 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.43526 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro, Version 1.171.35.19 (Rigaku OD, 2020) ; _exptl_crystal_colour 'pale yellow' _exptl_crystal_density_diffrn 2.322 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 984 _exptl_crystal_size_max 0.25 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.15 _refine_diff_density_max 0.923 _refine_diff_density_min -0.685 _refine_ls_extinction_coef 0.00148(4) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method ; SHELXL-2019/3 (Sheldrick, 2015) ; _refine_ls_goodness_of_fit_ref 1.120 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 135 _refine_ls_number_reflns 4580 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.120 _refine_ls_R_factor_all 0.0221 _refine_ls_R_factor_gt 0.0178 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0088P)^2^+1.0273P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0316 _refine_ls_wR_factor_ref 0.0327 _reflns_number_gt 4213 _reflns_number_total 4580 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file yz2044sup1.cif _cod_data_source_block 2c _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 2022978 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.154 _shelx_estimated_absorpt_t_max 0.267 _shelx_hkl_file ; 0 0 -2 841090. 16759.6 12 0 0 -2 833256. 16557.6 20 0 0 -2 829475. 16574.0 19 0 0 2 773282. 16555.7 9 0 0 -2 731306. 17147.6 14 0 0 2 822194. 16740.6 12 0 0 2 844712. 16563.5 20 0 0 -2 824126. 16957.7 13 0 0 2 848321. 16647.0 8 0 0 2 858834. 16556.7 4 0 0 -2 856024. 16568.8 4 0 0 2 731145. 16663.9 17 0 0 -2 864562. 16658.7 8 0 0 -3 419.093 146.431 8 0 0 3 259.088 147.120 8 0 0 3 97.5223 153.366 12 0 0 -3 296.436 163.017 12 0 0 3 262.976 113.201 4 0 0 -3 24.7858 151.927 9 0 0 -3 398.842 139.009 20 0 0 3-181.494 284.465 14 0 0 -3 553.714 315.168 14 0 0 -3 390.590 143.526 19 0 0 -3 400.439 127.914 4 0 0 -3 655.026 158.466 17 0 0 3 585.345 199.375 17 0 0 3 461.693 138.649 9 0 0 3 277.651 96.3455 20 0 0 -3 521.922 228.402 13 0 0 -4 315663. 7571.53 3 0 0 4 306431. 8355.68 14 0 0 4 321415. 7143.43 9 0 0 -4 305382. 8218.48 14 0 0 4 326343. 7165.29 20 0 0 4 328041. 7159.77 4 0 0 -4 296256. 7440.61 9 0 0 -4 322045. 7182.49 4 0 0 4 306277. 7524.22 17 0 0 -4 328052. 7331.61 8 0 0 -4 339958. 7711.78 2 0 0 4 322633. 7329.53 8 0 0 -4 317026. 7150.26 19 0 0 4 317218. 7513.58 12 0 0 -4 315239. 7888.56 13 0 0 -4 312289. 7163.45 20 0 0 -4 304103. 7227.00 17 0 0 5 570.977 273.739 12 0 0 5 378.886 166.405 20 0 0 -5 405.055 196.275 21 0 0 -5 190.428 166.482 19 0 0 5 376.316 451.191 14 0 0 5 820.048 183.878 9 0 0 -5 328.081 148.592 4 0 0 -5 312.634 214.459 9 0 0 5-159.901 227.640 8 0 0 -5 445.103 183.798 17 0 0 -5 300.300 181.504 20 0 0 -5 1448.88 424.102 13 0 0 5 477.262 202.697 4 0 0 5 733.191 315.444 17 0 0 -6 133659. 3773.10 17 0 0 6 139958. 3666.04 9 0 0 -6 133764. 5289.37 10 0 0 6 140583. 3972.98 8 0 0 6 136126. 4183.45 12 0 0 -6 133607. 4220.23 9 0 0 -6 133539. 3669.91 19 0 0 6 137573. 3732.37 4 0 0 6 133897. 4308.49 17 0 0 -6 134802. 4617.74 13 0 0 6 133211. 5144.62 14 0 0 -6 140898. 3798.36 20 0 0 -7 378.314 333.808 9 0 0 -7 126.540 238.039 20 0 0 7 419.643 342.666 17 0 0 -7 615.685 650.744 10 0 0 7 177.854 133.054 9 0 0 7 266.904 206.743 4 0 0 -7 463.611 496.383 13 0 0 7-76.8569 369.303 12 0 0 -7 243.239 190.661 19 0 0 7-113.062 262.397 8 0 0 7 681.675 710.719 14 0 0 8 760.754 294.917 4 0 0 -8-150.704 507.975 13 0 0 -8 64.7787 246.782 20 0 0 -8 924.868 726.898 10 0 0 8 619.237 424.483 12 0 0 -8 1173.10 433.369 9 0 0 8 1155.44 624.875 14 0 0 -8 472.857 214.893 19 0 0 8 53.6688 337.937 17 0 0 8 338.371 291.875 8 0 0 9-17.5551 474.456 11 0 0 -9 1414.68 852.115 10 0 0 9 913.408 643.521 14 0 0 -9 239.102 282.071 20 0 0 9 299.852 386.775 17 0 0 -9 168.937 347.212 9 0 0 -9 177.272 220.943 19 0 0 9 95.7453 304.883 8 0 0 9 201.850 219.931 4 0 0 -9-613.055 582.570 13 0 0 9 477.015 410.937 12 0 0 10 106264. 5444.68 14 0 0 10 88114.5 4113.12 17 0 0 -10 93971.8 4602.72 13 0 0 -10 98252.0 3506.05 20 0 0 10 92704.5 3963.37 12 0 0 -10 96400.8 5336.91 10 0 0 -10 98013.9 3221.44 19 0 0 10 97972.0 3731.51 8 0 0 10 93281.5 4487.78 11 0 0 10 93270.9 3371.59 4 0 0 -10 90648.4 3935.64 9 0 0 -11 164.865 325.517 20 0 0 11 438.001 619.023 14 0 0 -11 760.153 646.784 13 0 0 11-227.029 358.916 17 0 0 -11-9.20555 200.961 19 0 0 11-336.315 451.010 8 0 0 11-1.62692 528.061 11 0 0 11 339.641 290.315 4 0 0 -11 141.064 590.780 10 0 0 -12 158860. 5157.98 20 0 0 -12 148007. 7465.69 10 0 0 12 160354. 6709.38 11 0 0 12 145915. 5784.17 12 0 0 12 149038. 4973.69 4 0 0 12 150015. 5406.68 8 0 0 12 151890. 7352.70 14 0 0 -12 140205. 6551.83 13 0 0 -13 348.456 681.509 13 0 0 -13 117.695 687.577 10 0 0 13-1485.26 855.771 14 0 0 13-866.123 794.876 11 0 0 13 968.513 708.129 12 0 0 13-264.168 445.043 8 0 0 -14 100947. 5891.33 13 0 0 -14 106446. 6664.63 10 0 0 14 112247. 4759.52 8 0 0 14 106512. 5833.20 11 0 0 14 102215. 6316.65 14 0 0 14 98241.0 4992.00 12 0 0 -15 96.8252 651.546 10 0 0 15 1358.82 967.857 14 0 0 -15 221.516 657.153 15 0 0 15 265.127 762.897 11 0 0 -15-670.384 1119.54 13 0 0 15 653.824 723.596 12 0 0 -16 71536.6 5305.97 15 0 0 -16 77643.0 6017.79 10 0 0 16 60783.9 5096.69 14 0 0 -16 80164.6 5590.54 13 0 -1 -1 23600.7 769.529 12 0 1 1 25542.9 851.440 11 0 1 -1 21683.2 914.019 9 0 1 1 27626.5 998.462 17 0 1 -1 20218.1 735.198 20 0 -1 2 56252.1 2118.00 14 0 1 2 58870.2 1907.96 17 0 1 -2 56147.2 1828.94 13 0 1 -2 57836.4 1568.55 5 0 -1 2 58788.4 1576.25 4 0 1 2 56326.0 1763.11 3 0 1 2 54792.0 1785.30 11 0 1 2 54567.6 1609.56 8 0 1 -2 57864.5 2134.25 14 0 -1 2 56008.4 1418.38 19 0 -1 2 55242.0 1824.72 13 0 -1 2 59897.9 1838.00 9 0 1 -2 57498.6 1888.92 9 0 1 -2 57328.6 1593.31 16 0 -1 2 60118.4 1582.90 20 0 -1 -2 59288.9 1685.77 12 0 -1 -2 54026.9 1917.00 10 0 -1 2 56740.0 1560.14 5 0 -1 -2 56667.5 1779.47 3 0 -1 -2 54508.6 1754.12 14 0 -1 -2 55617.4 1849.53 2 0 -1 -2 58564.8 1626.84 8 0 -1 -2 56386.1 1520.88 4 0 1 2 57698.9 1550.02 4 0 1 -2 55363.7 1410.80 19 0 1 2 55277.7 1823.29 2 0 1 2 53311.2 1782.95 14 0 -1 2 58177.8 1656.25 12 0 1 -2 56627.3 1579.78 4 0 1 2 56698.1 1663.52 12 0 -1 -2 59947.1 1861.47 17 0 1 -2 56273.9 1581.27 20 0 1 -3 256615. 6336.11 13 0 -1 3 259480. 6098.92 9 0 1 3 258863. 6017.00 12 0 1 -3 261831. 5560.27 17 0 -1 -3 254348. 6355.62 14 0 1 -3 257087. 5998.42 12 0 -1 -3 254173. 5729.11 4 0 1 -3 244497. 5806.22 20 0 -1 -3 253482. 6292.39 2 0 -1 -3 261600. 6021.47 12 0 -1 -3 239145. 5547.77 9 0 -1 3 261540. 5662.31 17 0 1 -3 253115. 5813.76 4 0 1 -3 261313. 5869.36 16 0 1 3 252741. 5469.82 9 0 1 3 239714. 6223.91 11 0 1 3 256303. 5749.73 4 0 -1 3 267749. 5811.93 4 0 -1 -3 254544. 6172.09 3 0 -1 3 255846. 5636.96 19 0 1 3 245924. 6413.41 14 0 -1 -3 248308. 5725.79 20 0 -1 3 265839. 5805.92 20 0 1 -3 239200. 6744.35 14 0 1 -3 256106. 5728.33 21 0 1 -3 267706. 5866.46 5 0 -1 -3 243663. 6591.02 10 0 -1 3 256731. 6319.55 13 0 -1 3 247868. 6809.07 14 0 -1 3 258014. 5993.34 12 0 1 -3 257362. 5591.98 19 0 1 3 262246. 5925.97 8 0 -1 3 248960. 5843.67 8 0 1 -3 240476. 6256.96 9 0 -1 -3 251359. 6142.29 17 0 -1 -3 273179. 5928.69 8 0 1 3 249747. 6312.18 17 0 -1 4 196102. 5074.75 12 0 -1 -4 192575. 4688.23 9 0 -1 -4 194854. 5524.27 14 0 1 4 205512. 4487.13 9 0 1 -4 191990. 5366.08 9 0 1 -4 198353. 4593.38 19 0 -1 4 201064. 4796.95 4 0 1 4 196547. 4749.66 4 0 1 4 197318. 5423.85 17 0 1 -4 202432. 4849.72 4 0 -1 -4 203161. 5420.61 2 0 -1 4 194576. 4884.31 8 0 -1 -4 207811. 4767.00 4 0 1 4 200773. 5117.37 12 0 -1 -4 202837. 4944.68 8 0 1 -4 196512. 4824.61 21 0 -1 4 204393. 5071.22 9 0 1 4 199282. 4958.05 8 0 1 -4 207206. 4930.92 16 0 1 -4 205911. 4936.82 5 0 -1 4 190904. 6012.89 14 0 1 -4 193324. 4824.38 20 0 -1 -4 202406. 5150.70 17 0 -1 -4 192429. 5863.71 10 0 -1 -4 201657. 4760.22 20 0 -1 4 197575. 4807.84 17 0 -1 4 204493. 4802.06 20 0 1 4 191666. 5671.03 14 0 1 -4 202210. 4592.20 17 0 1 -4 195087. 5469.71 13 0 1 -5 335300. 7713.17 4 0 1 5 334873. 7620.48 4 0 -1 -5 327040. 9139.07 10 0 -1 5 317568. 9242.82 14 0 -1 5 333896. 8046.95 12 0 -1 5 329955. 7811.89 17 0 1 5 314551. 8419.31 11 0 -1 -5 329063. 7599.18 20 0 -1 -5 346688. 7622.09 4 0 -1 5 328075. 7634.05 4 0 -1 5 325454. 7776.67 8 0 -1 -5 324340. 7677.43 9 0 1 -5 317071. 7688.12 20 0 1 5 323008. 8897.50 14 0 1 -5 330267. 8602.87 13 0 1 5 337284. 7881.30 8 0 1 5 334410. 7291.07 9 0 1 -5 311118. 8350.88 9 0 -1 5 330334. 7645.18 20 0 1 -5 319166. 7740.12 21 0 1 5 330629. 8057.61 12 0 1 -5 337407. 7433.62 17 0 -1 -5 327521. 7972.40 17 0 -1 5 344193. 7901.09 9 0 1 -5 323003. 7401.78 19 0 -1 -6 238749. 7500.31 10 0 -1 -6 233753. 5775.54 20 0 1 -6 231659. 5877.33 20 0 1 6 232556. 7261.76 14 0 1 6 233999. 6708.15 17 0 1 -6 227650. 5944.23 21 0 -1 6 231100. 5783.15 4 0 1 6 238568. 5432.75 9 0 -1 -6 233762. 5941.05 19 0 -1 -6 249152. 6859.05 13 0 -1 6 246720. 7743.28 14 0 -1 -6 226629. 5989.11 9 0 1 -6 226297. 6636.44 9 0 1 -6 230701. 5561.02 19 0 -1 6 232619. 5994.69 8 0 1 6 232977. 5777.29 4 0 1 6 233017. 6300.11 12 0 1 6 229706. 6031.98 8 0 1 -6 238829. 5607.11 17 0 -1 6 236537. 6132.49 17 0 1 -6 238069. 6889.78 13 0 -1 6 230555. 6269.53 12 0 1 6 234787. 6764.89 11 0 -1 -7 327391. 8545.81 9 0 1 7 348564. 7831.89 9 0 1 -7 336889. 8361.22 20 0 1 -7 342105. 9581.78 13 0 1 7 345779. 8271.12 4 0 -1 7 343785. 8867.84 12 0 1 7 351094. 10154.1 14 0 -1 -7 344186. 8262.23 20 0 1 7 328426. 9333.53 17 0 -1 7 348199. 8277.99 4 0 -1 -7 349448. 8396.05 19 0 1 7 357051. 8937.81 12 0 1 -7 325479. 9230.64 9 0 1 -7 340371. 10632.1 10 0 1 -7 345440. 8001.96 19 0 -1 7 335310. 8496.69 8 0 1 7 352522. 8620.51 8 0 1 -7 345786. 8035.99 17 0 1 7 355183. 9524.01 11 0 -1 -7 346889. 9519.81 13 0 -1 7 343363. 10524.9 14 0 -1 -7 349904. 10376.1 10 0 1 -8 154176. 6514.49 10 0 -1 -8 144019. 4706.30 9 0 1 -8 141872. 5518.78 13 0 1 8 153393. 4424.33 4 0 1 8 151844. 3950.29 9 0 1 -8 151832. 4533.13 20 0 1 8 157563. 4766.56 8 0 -1 -8 146408. 6158.56 10 0 -1 8 152194. 4982.80 12 0 1 8 158023. 6165.16 14 0 1 8 159446. 5058.83 12 0 -1 -8 152599. 5572.19 13 0 -1 -8 157492. 4492.52 19 0 -1 8 161201. 6518.90 14 0 -1 8 154726. 4679.73 8 0 1 8 158956. 5584.61 11 0 -1 8 152020. 4399.40 4 0 -1 -8 154512. 4430.95 20 0 1 -8 155210. 4165.14 19 0 1 -8 148512. 5331.18 9 0 -1 8 155929. 5009.79 17 0 1 8 153603. 5472.15 17 0 -1 -9 209595. 7226.25 13 0 -1 9 218128. 8250.66 14 0 -1 9 213410. 6535.42 12 0 -1 9 210088. 5805.81 4 0 1 9 208641. 5832.43 4 0 1 -9 211728. 7327.84 13 0 1 9 228547. 8063.74 14 0 1 9 218026. 6614.78 12 0 -1 -9 211476. 5835.52 20 0 -1 -9 210581. 5814.86 19 0 -1 -9 204913. 6179.39 9 0 1 9 211818. 7170.56 11 0 1 -9 226426. 8498.16 10 0 -1 9 208631. 6518.93 17 0 1 -9 205424. 5956.89 20 0 1 9 215818. 6241.34 8 0 1 -9 194012. 6770.66 9 0 -1 9 212926. 6154.64 8 0 1 9 212898. 7133.24 17 0 -1 -9 223027. 8184.14 10 0 1 -9 216153. 5520.84 19 0 1 10 79660.5 4108.33 11 0 1 -10 79885.0 3178.44 20 0 -1 10 77679.5 4738.06 14 0 1 -10 80280.9 2766.93 19 0 -1 10 77578.9 3570.41 12 0 -1 -10 82639.3 4797.82 10 0 1 10 84158.1 4688.30 14 0 -1 -10 81543.5 3082.41 20 0 1 10 81502.1 3380.73 8 0 1 -10 80760.9 4928.62 10 0 1 -10 71793.8 3695.96 9 0 -1 10 82411.5 4128.53 11 0 -1 10 81994.9 3072.06 4 0 -1 10 79066.6 3590.66 17 0 -1 -10 82380.6 3321.34 9 0 1 10 77637.4 3030.13 4 0 1 10 81716.7 3639.23 12 0 -1 -10 77165.5 2958.92 19 0 -1 -10 85370.8 4300.54 13 0 1 10 80974.0 4048.66 17 0 -1 10 79602.4 3297.46 8 0 1 -10 79684.7 4233.65 13 0 1 -11 63121.5 3924.93 13 0 -1 11 64134.5 3359.83 12 0 1 -11 68898.2 3000.24 20 0 -1 -11 67042.0 2707.06 19 0 1 -11 66169.8 2486.96 19 0 -1 -11 64329.5 3913.62 13 0 1 11 61485.7 2755.15 4 0 -1 11 66169.8 4516.76 14 0 1 11 62237.7 3315.95 12 0 1 11 67612.3 3170.97 8 0 -1 -11 68508.3 2868.13 20 0 -1 11 62920.3 3033.85 8 0 1 11 70481.8 3997.51 11 0 -1 -11 65250.7 4391.77 10 0 1 -11 70130.4 4737.78 10 0 -1 11 69995.5 3942.18 11 0 1 11 60686.1 3599.62 17 0 1 11 72248.2 4502.39 14 0 1 -11 66781.4 3501.95 9 0 -1 11 61472.8 2728.20 4 0 -1 12 29238.6 1856.84 4 0 -1 -12 34884.6 2974.55 13 0 1 -12 32988.3 3400.87 10 0 1 12 33682.2 2250.87 8 0 1 12 24980.6 2151.79 12 0 -1 12 29170.9 2336.48 12 0 -1 -12 34011.2 1997.26 20 0 -1 12 31397.0 2146.52 8 0 1 -12 32158.5 2057.38 20 0 1 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27101.9 2810.05 17 0 5 -13 12626.9 2404.61 10 0 -5 13 8466.32 1533.85 11 0 -5 13 10305.5 1304.71 8 0 5 -13 9427.65 1834.80 13 0 5 13 8294.01 1259.52 8 0 5 13 8870.09 1650.13 11 0 5 13 11960.0 1636.10 12 0 -5 13 7300.27 1919.85 14 0 -5 -13 7691.82 1558.42 10 0 -5 13 9921.39 1499.81 12 0 -5 -13 10566.8 1757.80 13 0 5 13 11046.8 1873.40 17 0 -5 -13 9511.30 1597.90 15 0 5 14 8473.61 1454.06 12 0 -5 14 9537.36 1516.87 12 0 -5 -14 10474.3 1876.48 10 0 5 14 7292.02 1271.34 8 0 5 14 9465.67 1777.55 11 0 -5 14 11379.6 2352.29 14 0 5 -14 10893.9 1979.58 13 0 5 -14 10053.0 2210.13 10 0 -5 -14 8128.88 1510.92 15 0 -5 14 8506.98 1255.38 8 0 -5 -14 7501.25 1622.57 13 0 -5 14 6406.00 1400.41 11 0 5 -15-260.793 859.122 13 0 5 15 1387.51 930.339 11 0 5 -15-368.013 1150.92 10 0 -5 -15-850.037 959.520 10 0 -5 -15-315.312 754.500 13 0 -5 15-596.448 714.084 12 0 5 15-343.378 697.324 12 0 -5 15 140.915 690.319 11 0 -5 -15 510.596 651.256 15 0 -5 15 135.510 858.805 14 0 -5 -16 5109.80 1507.95 13 0 -5 -16 1799.58 858.307 15 0 -5 -16 4174.85 1341.93 10 0 -6 0 99756.1 3180.07 14 0 -6 0 100120. 3864.56 5 0 6 0 100640. 3636.86 18 0 6 0 95335.4 3779.16 9 0 6 0 97628.5 3712.05 17 0 6 0 102671. 2841.79 7 0 6 0 100128. 3293.78 14 0 6 0 100274. 3525.16 3 0 6 0 94961.2 3643.87 2 0 -6 0 100916. 3935.29 16 0 6 0 98441.2 3526.85 15 0 6 0 106586. 3922.90 13 0 -6 -1 5035.24 812.540 5 0 -6 1 4694.71 779.262 16 0 6 1 5727.29 755.899 18 0 6 -1 4559.11 648.884 15 0 6 -1 4733.29 662.658 3 0 6 -1 4502.16 686.899 18 0 6 -1 4341.05 670.056 14 0 -6 -1 4816.79 619.815 11 0 6 -1 5580.38 862.452 13 0 6 -1 4886.34 791.104 20 0 6 1 5052.04 432.502 10 0 6 -1 6391.71 799.657 2 0 -6 1 5352.62 837.910 5 0 6 1 4709.05 738.434 2 0 -6 1 4919.06 669.478 14 0 6 -1 3654.23 710.422 9 0 -6 -1 4541.57 797.919 16 0 -6 -1 4016.34 559.087 15 0 6 1 4405.26 591.662 15 0 -6 -1 6493.51 898.733 6 0 6 1 5114.32 839.624 17 0 6 -1 4487.26 659.320 17 0 6 1 5279.50 723.877 3 0 -6 1 5174.41 708.089 3 0 6 1 4469.48 483.058 14 0 6 2 49514.5 1623.87 10 0 -6 -2 47748.3 2472.37 16 0 -6 2 53706.6 2486.21 5 0 6 2 52406.4 2119.57 15 0 6 2 56808.1 2805.56 2 0 -6 -2 54214.9 2111.10 15 0 -6 2 54718.3 2614.18 14 0 6 2 52067.5 2286.81 11 0 6 2 50949.7 2397.12 18 0 6 -2 54459.1 2576.79 13 0 6 -2 53440.3 2876.70 9 0 6 2 52602.1 1613.34 14 0 6 -2 52126.8 2559.25 20 0 6 2 49061.8 2406.97 3 0 -6 -2 54635.4 2514.46 6 0 -6 2 55213.4 2370.60 17 0 -6 2 52331.0 2588.95 16 0 6 2 51674.0 2773.05 17 0 6 -2 53361.3 2213.21 3 0 -6 -2 51511.2 2403.72 9 0 -6 -2 51201.4 1583.47 10 0 6 3 33850.6 1451.02 10 0 -6 3 31959.0 1919.29 16 0 6 3 32890.3 1930.27 18 0 6 -3 29394.3 2198.44 9 0 6 3 36053.6 1717.73 15 0 6 3 32559.2 1813.20 11 0 -6 3 33897.2 1698.45 17 0 6 -3 32395.5 2000.35 13 0 6 3 33043.5 2277.43 17 0 -6 3 33219.7 2193.94 14 0 6 3 34187.1 1100.71 14 0 -6 3 35388.1 1812.10 5 0 6 3 33273.8 1990.67 3 0 -6 -3 33145.5 1991.21 16 0 -6 -3 34471.2 1899.10 6 0 -6 -3 34231.9 1619.53 15 0 6 -3 34604.8 2008.14 20 0 -6 -3 36405.1 1818.46 9 0 -6 -3 33470.8 1314.62 10 0 6 3 36516.3 2295.11 2 0 6 4 7614.53 1138.76 17 0 -6 -4 6776.20 706.445 9 0 6 4 7985.39 1119.84 2 0 -6 4 6999.42 836.124 16 0 6 4 7174.03 526.398 14 0 -6 -4 7949.19 792.565 15 0 6 4 9418.31 990.299 11 0 -6 -4 8712.07 726.332 10 0 -6 4 8881.60 745.084 17 0 -6 4 8511.15 822.799 5 0 6 4 9317.04 1036.21 18 0 -6 4 8906.51 1215.01 14 0 6 -4 8863.97 1268.96 9 0 6 4 9133.12 1079.25 3 0 -6 -4 8384.24 935.668 6 0 6 -4 9227.46 1011.66 20 0 6 -4 8973.83 1090.69 13 0 -6 5 22905.4 2118.54 14 0 -6 5 23318.2 1525.34 4 0 -6 -5 23844.5 1220.94 9 0 -6 -5 20615.3 1502.87 6 0 -6 -5 24680.5 1521.58 15 0 -6 5 22787.0 1153.70 17 0 6 -5 20385.7 1708.17 13 0 6 -5 22534.6 1644.50 20 0 6 5 22235.4 2010.29 17 0 6 5 25157.9 1827.47 3 0 6 -5 23437.9 2105.60 9 0 -6 -5 24810.5 1469.82 10 0 6 5 23722.5 1224.24 14 0 -6 5 23646.4 897.563 21 0 -6 5 23239.3 1377.38 5 0 6 5 24394.2 1728.36 11 0 6 5 20805.0 1824.95 2 0 6 5 23393.8 1590.22 12 0 -6 5 22477.2 1515.93 16 0 -6 6 502.651 300.308 5 0 6 6 727.906 440.847 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0 6 -10 15653.2 2086.89 9 0 6 10 21769.7 2397.58 17 0 6 -10 18305.1 2499.88 10 0 -6 -10 16239.5 1311.02 20 0 6 10 19221.9 1743.29 8 0 -6 10 14040.1 2225.05 14 0 -6 10 14792.6 1561.35 12 0 6 11 379.570 712.182 11 0 6 11 796.780 485.394 12 0 -6 -11 544.645 580.532 10 0 6 11 995.638 661.865 17 0 -6 -11 872.505 372.887 20 0 -6 11 1812.56 749.738 12 0 -6 11 636.150 482.298 8 0 6 -11 568.507 448.030 20 0 6 -11 314.873 651.627 9 0 -6 11 657.582 376.190 4 0 -6 11 624.120 945.914 14 0 6 -11 717.097 606.567 13 0 -6 -11 1310.30 695.243 15 0 6 -11 1221.84 1065.94 10 0 6 11 1288.35 539.141 8 0 -6 -11 843.894 495.713 13 0 6 12 19952.4 1951.50 8 0 -6 -12 17446.8 2103.42 13 0 6 -12 18692.9 1902.84 20 0 -6 12 17668.9 2608.66 14 0 -6 12 18991.1 1731.97 8 0 -6 -12 19603.0 2260.46 10 0 -6 12 17111.5 1550.64 4 0 6 12 22552.4 2409.43 11 0 -6 12 19125.2 1955.39 12 0 6 12 24299.4 2757.82 17 0 6 -12 18017.4 2329.27 13 0 -6 -12 16422.4 1957.09 15 0 6 -12 18922.4 2813.53 10 0 6 12 19311.7 1966.55 12 0 -6 -12 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413.104 9 0 7 0 89.2114 353.489 2 0 7 0-52.5483 375.091 13 0 7 0 527.355 296.644 14 0 -7 0 344.208 431.224 5 0 7 0 714.094 423.571 17 0 7 0 420.670 337.235 18 0 7 1 1443.79 464.611 18 0 -7 1 2125.53 632.522 5 0 7 1 1456.88 439.613 15 0 7 -1 3024.65 677.092 2 0 7 -1 1476.61 508.748 17 0 7 1 1539.72 329.308 14 0 -7 -1 1342.12 382.099 15 0 7 -1 1351.09 555.156 20 0 7 -1 1714.04 557.003 13 0 7 1 2528.59 667.886 2 0 7 1 2072.80 649.371 17 0 -7 1 1917.53 652.627 16 0 -7 -1 2735.70 678.915 5 0 7 1 1679.76 270.377 10 0 7 -1 1772.47 509.282 3 0 7 -1 1346.55 544.210 9 0 -7 -1 2255.24 675.701 16 0 -7 1 1825.49 474.652 14 0 7 -1 1983.28 539.165 18 0 7 1 1148.50 439.309 3 0 -7 -1 2364.43 673.018 6 0 7 2 451.189 361.815 18 0 7 -2 1005.78 556.115 9 0 -7 -2 1033.86 507.665 16 0 7 -2 501.677 412.069 20 0 -7 2 1808.98 567.026 14 0 7 2 765.554 201.453 14 0 -7 -2 1598.00 374.155 15 0 -7 -2 1161.08 459.209 6 0 -7 2 1206.36 498.410 16 0 7 -2 1925.97 562.269 18 0 -7 2 671.879 330.522 5 0 7 2 192.067 503.545 2 0 7 2 1061.69 303.809 15 0 7 -2 653.134 333.111 3 0 7 2 623.723 535.530 17 0 7 2 641.604 165.934 10 0 7 2 197.678 393.242 3 0 7 -2 146.247 349.629 13 0 7 -3 7213.87 783.622 3 0 -7 -3 6339.58 495.287 10 0 7 -3 3963.89 756.447 20 0 7 -3 6978.80 1125.14 9 0 7 -3 6391.89 956.799 13 0 7 3 5877.68 1022.98 17 0 -7 3 5747.65 802.346 5 0 7 3 6525.73 564.896 10 0 7 3 6934.31 1066.46 2 0 -7 -3 6601.52 935.025 6 0 -7 3 5786.55 894.860 16 0 -7 3 6454.42 1011.29 14 0 7 3 5772.47 811.447 11 0 7 3 5979.05 402.535 14 0 -7 3 5812.03 750.724 17 0 7 3 6811.12 923.316 18 0 -7 -3 6125.75 920.213 16 0 -7 -3 5934.62 704.625 15 0 7 3 5645.97 878.499 3 0 7 4 12527.0 1213.64 11 0 -7 -4 13677.5 896.607 10 0 7 4 13263.3 1609.72 17 0 7 4 10862.3 1242.41 3 0 -7 -4 13750.5 1069.88 15 0 -7 4 12145.9 1100.85 5 0 -7 4 12525.2 1257.78 16 0 -7 -4 12605.8 1335.12 16 0 -7 4 12720.1 1527.08 14 0 7 4 12609.5 636.582 14 0 7 -4 12593.6 1353.85 13 0 7 -4 14987.0 1425.50 20 0 -7 -4 12159.4 1200.78 6 0 -7 4 12220.9 1007.90 17 0 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5585.33 416.541 21 0 -7 7 6597.48 890.520 4 0 7 7 7747.30 1126.21 11 0 7 7 7240.02 1032.57 12 0 -7 7 7090.30 412.129 17 0 7 7 5986.89 1255.35 17 0 -7 -7 7880.21 1007.44 10 0 7 -7 7491.74 1367.21 9 0 -7 -7 7248.92 1020.44 6 0 -7 7 7257.97 539.429 17 0 7 7 7657.52 1293.07 2 0 -7 7 7850.65 970.570 16 0 -7 -7 8871.70 1038.82 15 0 -7 7 5200.20 1193.07 14 0 7 -7 6903.01 1166.54 13 0 7 -7 7622.35 1075.74 20 0 7 7 6323.43 1096.47 3 0 -7 7 7824.02 879.207 5 0 7 7 7309.79 790.518 14 0 -7 7 7441.27 987.612 12 0 7 8 6831.41 1223.68 2 0 -7 8 6455.82 1397.38 14 0 -7 -8 8868.62 1137.42 6 0 7 8 5173.02 929.667 8 0 7 8 5703.42 1217.25 17 0 7 8 7372.05 1179.81 11 0 7 -8 7087.02 1253.44 13 0 7 8 8369.90 912.750 14 0 -7 -8 6382.52 980.134 15 0 -7 8 7397.62 991.738 4 0 7 8 6465.16 1009.65 12 0 -7 8 6710.16 1006.85 12 0 -7 -8 6846.25 1016.75 10 0 7 -8 5830.02 1019.57 20 0 7 -8 7704.37 1419.50 9 0 7 9 4141.55 1005.97 11 0 -7 9 2651.03 693.115 12 0 -7 -9 3986.02 873.895 10 0 7 -9 2991.44 876.183 9 0 7 -9 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215.260 586.297 9 0 -8 6 503.831 250.806 17 0 -8 6-535.495 879.901 14 0 8 6 151.121 468.538 3 0 8 6 441.035 415.568 11 0 -8 -6 42.7647 253.253 10 0 8 6 39.7289 479.976 2 0 -8 6 941.430 421.305 16 0 -8 -6 714.402 449.514 6 0 8 -6-136.567 508.804 13 0 8 -7 4482.87 1137.00 9 0 -8 7 5243.42 1244.09 14 0 -8 -7 4868.77 745.820 10 0 8 7 4200.53 498.827 14 0 8 7 4978.22 1021.24 11 0 -8 -7 3876.68 787.355 6 0 8 7 5435.50 1058.45 3 0 -8 7 3793.25 321.283 17 0 -8 7 4171.79 763.575 4 0 8 7 4740.35 1110.14 2 0 -8 7 4247.10 336.532 21 0 8 -7 4450.15 940.600 20 0 -8 -7 5152.29 831.605 15 0 -8 7 4602.61 718.150 5 0 8 -7 5107.51 1080.13 13 0 -8 7 3638.60 750.505 16 0 -8 -7 4688.39 353.539 9 0 8 7 5048.70 1331.38 17 0 8 -8 3093.68 945.745 9 0 -8 -8 2753.64 651.841 10 0 8 8 2984.34 841.530 11 0 -8 8 2195.80 494.024 5 0 8 8 3413.37 843.692 12 0 8 8 2493.25 887.774 3 0 -8 -8 2448.11 715.505 6 0 -8 8 3314.38 729.278 4 0 8 8 2173.13 819.162 2 0 -8 -8 2589.05 615.834 15 0 8 8 2545.69 860.850 17 0 -8 8 3622.14 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14 0 -9 -6 36779.3 2124.33 15 0 9 -6 33990.3 2613.67 13 0 -9 -6 35255.5 1796.95 10 0 -9 7 3663.75 1111.44 14 0 -9 -7 5521.00 749.655 10 0 -9 -7 3674.41 823.776 6 0 9 7 2262.35 759.230 3 0 9 7 3968.67 928.649 11 0 9 -7 3499.10 1193.75 9 0 9 7 3175.41 1066.42 17 0 -9 7 3650.23 788.676 16 0 -9 7 3082.27 604.124 5 0 -9 -7 3516.34 887.977 16 0 9 -7 2718.50 792.494 20 0 9 7 3041.86 995.638 2 0 -9 -7 3041.90 671.221 15 0 9 -7 4819.47 1110.07 13 0 -9 7 2007.18 622.669 4 0 -9 -8 54446.7 2932.31 15 0 -9 8 54441.3 2747.25 5 0 -9 -8 51777.2 2677.42 10 0 -9 8 57435.1 4214.77 14 0 -9 -8 55323.3 3453.06 16 0 9 -8 59068.7 4190.26 9 0 9 8 62314.4 4201.05 17 0 9 8 51643.5 3421.04 3 0 9 -8 50109.5 3272.65 20 0 9 -8 50532.7 3517.57 13 0 9 8 53906.6 3742.13 2 0 -9 -8 57180.2 3273.43 6 0 9 8 53672.5 3353.94 11 0 -9 8 51851.5 2948.68 16 0 -9 8 50804.9 2988.94 12 0 -9 8 50558.0 2921.87 4 0 9 9 947.092 692.077 11 0 9 9 824.502 816.970 2 0 -9 9 1304.64 526.575 4 0 9 9 2227.16 1108.63 17 0 -9 -9 981.520 458.923 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747.425 1 -4 -7 -5 813.758 422.851 16 4 -7 5 724.114 222.067 16 -4 7 -5 390.562 477.762 9 -4 -7 -5 700.142 158.641 15 4 7 5 545.120 597.545 3 4 -7 5 383.103 351.961 21 -4 -7 -6 2304.52 358.006 15 -4 7 -6 1974.39 828.415 13 -4 -7 -6 2820.99 405.812 13 4 -7 6 2899.38 716.894 4 4 -7 6 2836.23 591.184 21 4 -7 6 2368.81 553.806 12 -4 7 -6 2040.61 709.581 20 4 -7 6 1948.42 450.922 11 -4 -7 -6 557.332 557.327 19 4 7 6 1952.96 905.439 18 -4 -7 -6 1885.70 756.157 5 -4 -7 -6 1706.44 559.042 16 4 -7 6 2143.91 434.798 16 4 7 6 2093.48 704.059 3 -4 7 -6 2029.74 723.680 9 -4 7 -6 2612.63 846.024 1 -4 -7 -6 1849.56 713.368 1 -4 7 -7 2475.84 1006.04 13 -4 7 -7 1963.08 1005.43 1 -4 -7 -7 1972.85 801.003 1 4 -7 7 3549.19 807.932 4 4 -7 7 2062.21 591.852 21 -4 -7 -7 2707.83 872.099 5 -4 -7 -7 2567.97 580.600 6 4 -7 7 3202.91 690.621 12 -4 7 -7 2406.42 751.645 20 -4 -7 -7 2064.32 695.937 19 4 7 7 3202.52 1016.40 18 -4 -7 -7 3103.32 628.170 9 -4 -7 -7 2339.53 686.385 16 4 7 7 3638.60 995.337 3 -4 7 -7 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12 -4 8 9 32104.3 2959.49 2 -4 8 9 33524.8 2528.27 11 -4 -8 9 33609.6 2153.89 17 4 -8 -9 30514.0 2798.71 10 4 8 -9 32388.3 3313.08 10 -4 8 9 30255.5 2833.84 17 4 -8 -9 30922.6 2844.19 15 -4 -8 9 27344.7 2378.66 8 -4 -8 9 33499.1 3379.98 14 -4 8 9 30624.3 2729.87 14 -4 8 9 29387.6 2483.15 8 -4 -8 9 29135.4 1962.67 4 -4 8 8-334.759 682.902 8 4 8 -8 568.609 423.112 13 4 -8 -8 406.954 434.041 6 4 8 -8 628.678 678.276 10 4 -8 -8 126.465 582.171 10 -4 8 8 1243.62 705.001 17 -4 -8 8 497.634 537.942 5 -4 8 8 293.808 423.159 11 4 -8 -8 701.831 649.519 15 -4 8 8 440.108 723.158 2 -4 -8 8-223.648 654.552 14 -4 8 8 44.6297 461.161 14 4 8 -7 49930.4 3027.71 13 4 -8 -7 50601.6 3312.42 10 4 -8 -7 49495.1 3166.38 6 -4 8 7 55728.8 2944.70 11 -4 8 7 54369.8 3805.16 2 4 8 -7 51615.4 3799.58 10 -4 -8 7 50237.3 3123.35 5 -4 8 7 47587.1 3285.84 17 4 -8 -7 47877.0 3385.68 15 -4 -8 7 54896.7 3958.69 14 -4 8 7 53673.2 3402.31 14 -4 8 7 51293.0 3166.49 8 -4 8 6 446.427 566.958 2 -4 8 6-382.420 641.923 8 4 8 -6 127.168 385.881 13 -4 8 6-91.5135 314.856 11 4 8 -6 943.694 761.496 10 4 -8 -6-142.931 509.108 10 -4 8 6-140.273 741.995 17 -4 -8 6 94.4155 430.499 5 4 -8 -6 761.135 543.010 6 -4 8 6 539.162 200.090 9 4 -8 -6 575.267 627.928 15 -4 -8 6 35.5400 425.787 16 -4 -8 6-341.579 782.549 14 -4 8 6 701.104 556.784 14 4 8 -5 24553.4 1808.35 13 -4 8 5 20038.9 1952.34 17 -4 8 5 20489.4 2201.34 2 4 -8 -5 21954.2 1961.34 6 -4 8 5 24121.5 1647.74 11 -4 -8 5 20168.6 1882.07 5 4 -8 -5 20681.1 1936.05 10 -4 8 5 20508.9 1352.80 9 -4 -8 5 21951.9 1980.15 16 4 8 -5 19854.8 1882.24 15 4 -8 -5 23208.3 2185.98 15 -4 -8 5 23957.6 2302.06 14 -4 8 5 24145.4 1995.06 8 4 8 -5 22432.1 2135.77 10 -4 8 4 4337.19 848.721 8 4 8 -4 4088.12 707.697 13 -4 8 4 2835.71 902.581 2 4 -8 -4 3351.30 844.602 6 -4 8 4 4930.08 688.327 11 4 -8 -4 3465.71 810.752 10 4 8 -4 4353.59 904.151 10 -4 8 4 3471.51 775.510 17 -4 -8 4 3278.39 796.214 5 -4 -8 4 5326.71 1003.62 16 4 -8 -4 3639.46 586.538 4 -4 8 4 5598.51 749.424 9 4 8 -4 3082.41 702.863 15 4 -8 -4 4096.62 1000.68 15 -4 -8 4 3747.32 927.898 14 4 8 -3 4514.76 686.322 13 4 8 -3 3783.77 947.337 3 4 8 -3 3284.67 634.397 15 -4 8 3 4880.15 1083.16 2 -4 8 3 4907.61 600.618 11 -4 8 3 2756.73 639.949 20 -4 8 3 3653.65 806.508 17 4 8 -3 6424.73 1092.32 10 4 -8 -3 3963.82 634.301 4 4 -8 -3 3872.81 834.879 10 -4 -8 3 4184.99 941.245 5 4 -8 -3 2681.15 676.646 6 -4 -8 3 4263.71 873.392 16 -4 8 3 5189.75 738.807 9 4 -8 -3 4510.02 965.942 15 -4 -8 3 3848.55 889.607 14 4 -8 -2 8072.84 916.164 4 4 8 -2 7228.02 1126.95 3 4 8 -2 6237.31 727.148 13 4 -8 -2 4574.63 847.959 7 -4 8 2 5675.96 563.234 11 -4 8 2 5908.20 885.441 20 4 8 -2 6095.30 1216.24 18 4 8 -2 7096.96 988.010 10 -4 -8 2 6598.19 1120.60 5 4 -8 -2 5808.07 993.158 6 -4 -8 2 7254.39 1116.89 16 -4 8 2 8317.46 987.132 9 4 8 -2 8692.89 860.583 15 4 -8 -2 5353.60 1099.46 15 -4 8 2 6225.17 985.222 17 -4 -8 2 6947.11 1022.61 14 4 8 -1 1613.14 680.241 3 4 8 -1 2506.50 451.905 13 4 -8 -1 2339.90 643.503 7 -4 8 1 1846.65 249.556 11 4 -8 -1 1238.97 444.894 4 -4 8 1 1401.06 531.096 20 4 8 -1 2154.67 883.150 18 4 -8 -1 2001.19 342.377 18 4 8 -1 1711.90 487.715 10 4 -8 -1 1310.86 596.179 6 -4 8 1 1959.28 635.080 17 -4 -8 1 1615.51 766.897 5 -4 8 1 1792.18 490.968 9 -4 -8 1 2226.24 633.744 16 4 8 -1 1661.39 318.374 15 4 -8 -1 1946.35 872.931 15 -4 -8 1 1590.04 513.290 14 4 8 0 10851.5 1476.30 3 4 8 0 11033.3 833.791 13 4 -8 0 9808.58 1242.75 7 4 -8 0 10189.9 1087.11 4 4 -8 0 10455.2 1408.24 6 -4 8 0 9119.14 1107.24 20 4 8 0 11542.9 1674.33 18 4 -8 0 11633.4 735.786 18 4 8 0 11147.9 1065.79 10 -4 8 0 11515.6 1190.74 17 -4 -8 0 11344.0 1446.29 5 4 -8 0 12497.0 1345.42 16 -4 -8 0 10259.1 1291.92 16 -4 8 0 10531.0 1200.06 9 4 -8 0 11428.7 1612.37 15 -4 -8 0 10410.7 1092.12 14 4 8 1 3171.92 628.171 7 4 -8 1 3292.61 800.464 7 4 -8 1 1561.31 617.693 6 -4 8 -1 3741.05 761.704 20 4 8 1 4166.98 1158.68 18 -4 -8 -1 3098.20 436.303 10 4 -8 1 2582.14 565.906 4 -4 -8 -1 4831.27 992.942 5 -4 8 -1 3112.35 622.031 17 4 -8 1 3219.83 742.053 16 -4 -8 -1 3252.88 786.541 16 -4 8 -1 2493.65 630.791 9 4 -8 1 3463.91 413.639 3 4 -8 1 3473.26 1073.23 15 4 8 1 3249.23 815.958 3 -4 -8 -1 2897.14 554.706 14 4 8 2 14188.9 1242.70 7 4 -8 2 16260.3 1306.75 5 -4 8 -2 15397.2 1264.78 17 -4 8 -2 13992.8 1385.39 20 -4 -8 -2 16053.9 955.819 10 4 8 2 14434.2 1948.82 18 -4 -8 -2 16212.3 1824.18 5 4 -8 2 15013.4 1500.80 16 -4 -8 -2 16193.5 1629.87 16 -4 8 -2 13834.8 1496.07 9 -4 -8 -2 14490.7 1063.98 14 4 8 2 12083.4 1692.89 3 4 -8 2 14516.7 1373.61 4 -4 8 -3 20210.1 2276.35 13 4 -8 3 21079.7 1375.72 12 -4 8 -3 21322.6 1435.97 17 -4 8 -3 21460.0 1733.05 20 4 -8 3 18935.0 1322.67 5 -4 -8 -3 17496.8 1027.12 10 4 8 3 18696.6 2165.71 18 4 -8 3 20661.6 1817.98 16 -4 -8 -3 16746.4 1704.15 16 -4 -8 -3 21635.8 2155.74 5 -4 8 -3 17960.5 1748.89 9 4 8 3 21736.9 2266.75 3 -4 -8 -3 19772.9 1141.66 14 4 -8 3 19069.7 1624.95 4 -4 8 -4 13055.0 1875.24 13 4 -8 4 11401.5 1055.76 12 4 -8 4 11196.0 1303.83 4 -4 -8 -4 13192.5 1546.32 1 -4 8 -4 9060.15 1228.50 20 4 -8 4 10188.1 715.635 5 4 8 4 15011.9 1921.28 18 -4 8 -4 12189.3 991.200 17 -4 -8 -4 8632.33 1386.57 5 4 -8 4 12396.7 1370.72 16 -4 -8 -4 8368.03 1249.29 16 -4 8 -4 11334.2 1469.83 9 4 8 4 11907.6 1716.60 3 -4 -8 -4 11384.5 760.326 14 -4 8 -4 7767.53 1275.01 1 -4 8 -5 20696.2 2367.66 13 4 -8 5 22461.6 1601.15 12 -4 8 -5 23160.7 1953.52 20 4 8 5 22571.1 2411.18 18 -4 -8 -5 23387.4 2068.76 16 -4 8 -5 23227.4 1299.95 17 -4 -8 -5 23025.3 2376.17 5 -4 8 -5 22186.3 2185.80 1 4 -8 5 22660.7 1694.37 21 -4 -8 -5 25262.8 2231.88 1 4 -8 5 23407.2 1756.96 16 -4 8 -5 25240.9 2207.12 9 4 8 5 26989.6 2574.23 3 4 -8 5 22275.9 1847.29 4 -4 -8 -5 24367.1 1077.10 14 -4 8 -6 912.703 640.098 13 4 -8 6 1108.72 532.550 4 4 -8 6 1783.01 552.882 21 -4 8 -6 525.411 508.992 20 -4 -8 -6 1033.75 568.644 16 4 8 6 1178.89 943.098 18 -4 -8 -6 702.004 557.644 5 4 -8 6 1178.93 381.587 16 4 -8 6 1034.96 492.590 12 4 8 6 318.426 583.684 3 -4 8 -6 859.508 628.924 1 -4 8 -6 692.002 574.734 9 -4 -8 -6 755.389 500.237 1 -4 8 -7 7790.64 1602.70 13 4 -8 7 4299.37 834.701 21 4 -8 7 6047.45 1025.05 4 -4 -8 -7 8720.22 1078.58 6 -4 8 -7 6167.44 1126.58 20 -4 -8 -7 7740.46 1284.05 19 4 8 7 7113.62 1434.11 18 -4 -8 -7 7947.42 1280.81 16 4 8 7 4675.02 1155.03 3 -4 8 -7 4535.52 1037.23 9 -4 -8 -7 6678.11 1355.49 5 4 -8 7 5801.83 906.680 12 -4 8 -7 7396.25 1427.07 1 -4 -8 -7 5838.32 1233.25 1 -4 8 -8-174.345 856.692 13 -4 8 -8 1044.20 660.813 1 -4 -8 -8 324.440 572.926 1 4 -8 8-428.521 556.280 4 4 -8 8-74.5834 349.938 21 4 -8 8-233.413 380.608 12 -4 -8 -8-56.7415 624.797 19 4 8 8 276.883 555.207 18 -4 -8 -8 211.025 533.275 5 -4 8 -8 391.919 597.910 20 -4 -8 -8 797.123 592.807 16 -4 -8 -8 802.030 444.758 9 4 8 8 252.440 678.272 3 -4 8 -8-284.147 684.419 9 -4 8 -9 2800.78 1030.08 13 -4 -8 -9 4205.17 1198.18 5 4 -8 9 2667.42 791.365 4 -4 8 -9 1949.41 928.325 1 4 -8 9 1775.61 651.632 12 -4 -8 -9 2400.69 816.810 1 -4 8 -9 3203.20 892.082 20 4 -8 9 2634.01 711.665 21 4 8 9 4515.63 1337.28 3 -4 8 -9 2685.02 981.875 9 -4 -8 -9 3845.04 1042.65 19 4 -8 10-507.752 612.862 12 -4 8 -10-552.557 940.399 13 4 -8 10 394.126 479.226 4 -4 -8 -10 72.8142 427.836 20 -4 8 -10 764.227 705.766 20 -4 8 -10 189.751 702.970 1 -4 -8 -10 139.420 635.305 19 -4 -8 -10-822.361 699.211 1 4 8 10-134.179 655.040 3 -4 -8 -10 368.548 538.681 5 -4 8 -10-559.489 677.880 9 -4 8 -11-763.223 1153.85 13 4 -8 11 354.053 527.697 4 4 -8 11 416.185 554.849 12 -4 -8 -11 991.704 681.558 20 -4 8 -11 88.1042 635.505 20 -4 -8 -11-355.699 746.737 19 -4 8 -11 310.013 757.349 1 -4 -8 -11-465.764 754.107 5 -4 -8 -11-335.134 842.155 1 4 8 11-803.098 829.903 3 -4 8 -11 757.852 779.390 9 -4 8 -12 799.844 1154.32 13 4 -8 12-1843.72 732.056 4 4 8 12 350.351 680.956 12 4 -8 12 878.177 637.361 12 -4 8 -12 861.389 613.064 20 -4 -8 -12 422.681 548.865 19 -4 -8 -12 481.124 508.284 5 -4 8 -12 344.246 755.061 1 -4 -8 -12-514.460 781.723 1 4 8 12 562.754 623.675 3 -4 8 -12-242.482 682.584 9 -4 -8 -12 490.279 648.288 20 -4 8 -13 3406.24 1210.92 13 4 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626.261 8 -7 -6 10-15.5539 722.669 14 -7 6 10 2244.25 1201.01 14 -7 6 9 4609.62 1124.10 8 7 6 -9 4556.91 1024.64 13 7 6 -9 5809.17 1645.08 10 7 -6 -9 4783.08 1380.07 10 -7 -6 9 6795.83 1244.06 17 -7 6 9 7775.01 1499.57 17 7 6 -9 7897.43 1585.68 15 7 -6 -9 7023.45 1693.38 15 -7 -6 9 4558.56 1097.17 8 -7 -6 9 7067.33 1710.91 14 -7 6 9 6053.72 1575.63 14 -7 6 8 615.349 638.375 8 7 6 -8-355.895 528.520 13 -7 -6 8 8.98852 362.022 12 7 6 -8-568.651 1008.55 10 7 -6 -8-24.2583 737.346 10 -7 -6 8 608.393 554.067 17 -7 6 8-209.059 656.731 17 7 6 -8-172.622 680.717 15 7 -6 -8 439.231 613.663 15 -7 -6 8 305.462 558.632 8 -7 -6 8 249.752 743.059 14 -7 6 8-533.159 868.631 14 -7 6 7 13395.4 1669.47 8 -7 6 7 12069.7 1802.77 2 7 6 -7 14689.2 1633.29 13 7 -6 -7 15269.7 1850.80 6 -7 -6 7 11817.8 1254.25 12 7 6 -7 10218.4 1875.70 10 7 -6 -7 13189.7 2031.88 10 -7 6 7 12092.4 1690.99 17 7 6 -7 11415.5 1749.09 15 7 -6 -7 10196.1 1872.34 15 -7 -6 7 13522.7 1681.29 8 -7 -6 7 12316.4 1898.85 14 -7 6 7 11247.7 2018.63 14 -7 6 6 3227.71 834.910 8 7 6 -6 3958.91 831.687 13 -7 6 6 4495.81 1170.14 2 7 -6 -6 4463.02 1019.44 6 7 6 -6 2481.35 1073.26 10 7 -6 -6 3984.40 1258.04 10 -7 6 6 5541.97 1130.30 17 -7 -6 6 3903.17 978.808 5 -7 6 6 5344.55 790.580 9 7 6 -6 3201.42 924.945 15 7 -6 -6 3684.03 1221.37 15 -7 -6 6 4387.58 904.173 8 -7 -6 6 3143.61 1016.56 14 -7 6 6 5434.45 1271.72 14 -7 6 5 16787.2 1747.43 8 7 6 -5 18034.8 1571.32 13 7 -6 -5 16758.6 1814.96 6 7 6 -5 17628.8 1435.50 21 -7 6 5 17947.6 2115.15 2 7 6 -5 14972.8 2099.72 10 7 -6 -5 15212.6 2138.57 10 -7 6 5 17477.3 1866.33 17 -7 6 5 17641.8 1467.25 9 -7 -6 5 14146.2 1678.18 5 7 6 -5 17891.3 1933.50 15 7 -6 -5 14610.3 2106.13 15 -7 -6 5 14374.2 1595.66 8 -7 -6 5 16359.8 2021.07 14 -7 6 4 14088.0 1548.10 8 7 6 -4 11673.7 1181.07 13 7 -6 -4 14553.3 1656.03 6 7 6 -4 14736.1 1360.75 21 -7 6 4 14365.2 1853.62 2 -7 -6 4 13100.7 1139.37 19 7 6 -4 14344.8 1976.12 10 7 -6 -4 12554.5 1951.37 10 -7 6 4 14130.2 1628.46 17 -7 6 4 14477.3 1365.65 9 -7 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107.493 402.074 20 -7 -6 -1 52.2612 427.956 19 7 6 1 987.720 584.698 18 -7 6 -1 651.951 396.199 17 -7 -6 -1 1159.84 538.880 5 -7 6 -1 716.375 564.836 9 7 -6 1-298.178 866.731 15 -7 -6 -1 832.793 393.710 14 7 6 2 34466.8 2956.01 7 7 -6 2 29294.9 2878.88 7 7 6 2 28651.7 2323.68 21 7 -6 2 28907.8 2251.45 21 -7 6 -2 27938.2 2041.32 20 -7 -6 -2 27040.9 2212.17 19 -7 -6 -2 31935.2 2306.47 5 7 6 2 34517.7 3243.79 18 -7 6 -2 30039.5 2007.76 17 7 6 2 28727.6 2782.50 3 -7 6 -2 27137.6 2213.80 9 -7 -6 -2 29948.8 2000.71 16 7 -6 2 30119.6 2110.09 4 7 6 3 12620.9 1777.42 7 7 -6 3 9781.81 1265.22 4 7 -6 3 10709.6 1809.10 7 7 6 3 9899.57 1425.26 21 7 -6 3 11742.7 1471.17 21 -7 6 -3 12783.4 1407.00 20 -7 -6 -3 12701.0 1573.64 19 7 6 3 10784.9 1843.70 18 -7 6 -3 13810.2 1301.48 17 -7 -6 -3 13265.2 1496.46 5 -7 -6 -3 13689.0 1275.47 16 -7 6 -3 12457.8 1552.87 9 7 6 3 12095.6 1876.35 3 7 -6 4 6004.85 1038.19 4 7 6 4 6670.89 1289.87 7 7 6 4 6628.08 1245.43 21 7 -6 4 7450.28 1192.30 21 -7 6 -4 6871.55 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3152.60 20 -7 -6 -7 48187.6 3448.90 19 7 6 7 47632.9 3870.54 3 7 6 7 55265.5 4016.22 18 -7 6 -7 49725.6 4431.68 1 -7 -6 -7 41428.9 3999.04 1 -7 -6 -7 45697.9 3099.35 9 -7 6 -7 46073.4 3377.82 9 7 6 7 47354.6 3385.09 4 7 -6 7 43947.4 3057.83 4 -7 6 -8 2073.38 1002.70 13 7 -6 8 4919.24 1077.92 4 7 -6 8 5215.29 977.377 12 7 -6 8 3365.08 879.100 21 -7 6 -8 5574.23 1718.67 1 -7 -6 -8 3427.10 1389.31 1 -7 -6 -8 3369.53 983.134 20 -7 6 -8 3271.84 930.489 20 -7 -6 -8 2825.02 844.054 19 7 6 8 6527.45 1488.47 18 -7 -6 -8 3755.47 933.576 9 7 6 8 3471.08 1099.05 3 -7 6 -8 4486.02 1139.76 9 7 6 8 4232.04 1079.13 4 -7 6 -9 45813.7 4226.00 13 7 -6 9 45061.4 2913.44 12 7 -6 9 43304.4 3344.42 21 -7 -6 -9 43501.4 3313.29 20 -7 6 -9 42655.8 3238.61 20 7 6 9 49844.4 3891.53 3 -7 -6 -9 46456.7 3554.89 19 7 6 9 50263.6 3891.97 18 -7 6 -9 47620.5 4658.79 1 -7 -6 -9 49194.6 4628.27 1 -7 -6 -9 46074.9 3188.72 9 -7 6 -9 48250.5 3687.84 9 7 6 9 41006.3 3321.38 4 7 -6 9 41477.8 3153.00 4 -7 6 -10 12986.5 2356.01 13 7 -6 10 10803.0 1710.13 4 7 -6 10 8881.83 1355.93 12 -7 -6 -10 12614.4 1815.05 20 -7 6 -10 13721.7 1913.73 20 -7 -6 -10 13293.5 1943.60 19 -7 6 -10 17434.8 2971.73 1 -7 -6 -10 13421.5 2547.18 1 7 -6 10 10956.8 1741.32 21 7 6 10 13365.6 2014.93 3 -7 -6 -10 10890.2 1522.57 9 -7 6 -10 10797.4 1790.45 9 7 6 10 13109.8 1936.90 4 -7 6 -11 38767.0 4197.64 13 7 -6 11 34412.1 2778.32 12 7 -6 11 33479.4 3185.16 21 -7 -6 -11 30218.5 2920.90 20 -7 6 -11 39890.8 3329.16 20 7 6 11 42231.0 3538.54 3 -7 -6 -11 35361.7 3244.18 19 -7 -6 -11 39046.2 4379.96 1 -7 6 -11 50436.8 5129.90 1 -7 6 -11 31364.4 3230.27 9 7 6 11 37614.6 3312.65 4 7 -6 11 36475.0 3114.41 4 7 -6 12 9302.66 1494.40 12 -7 6 -12 7629.05 1632.23 9 7 7 -12 636.332 623.552 13 -7 7 12 437.083 583.691 11 7 7 -12 1282.98 998.448 15 -7 7 12-171.815 784.905 14 -7 7 11 6615.18 1451.78 8 7 7 -11 4323.69 1184.90 13 7 -7 -11 6754.80 1472.17 6 -7 7 11 5471.69 1213.15 11 7 7 -11 5283.64 1748.59 10 7 -7 -11 5907.12 1638.79 10 -7 7 11 8063.16 1712.28 17 7 7 -11 2890.80 1263.34 15 7 -7 -11 7404.84 1954.97 15 -7 -7 11 5651.70 1303.01 8 -7 -7 11 4243.34 1390.95 14 -7 7 11 8233.30 1937.39 14 -7 7 10 347.455 573.890 8 7 7 -10 1207.88 679.673 13 7 -7 -10 1654.88 931.739 6 7 7 -10 1166.03 1078.38 10 7 -7 -10-1940.50 1009.99 10 -7 -7 10 1096.73 742.247 17 -7 7 10 1943.21 946.867 17 7 7 -10 1166.78 862.676 15 7 -7 -10 314.547 677.105 15 -7 -7 10 218.234 605.498 8 -7 -7 10 22.1686 645.881 14 -7 7 10 2317.03 1252.81 14 -7 7 9 9307.05 1559.75 8 7 7 -9 10773.6 1574.62 13 7 -7 -9 13911.9 1960.52 6 -7 -7 9 10663.4 1351.34 12 7 7 -9 7858.68 1869.81 10 7 -7 -9 9502.04 1942.54 10 -7 -7 9 6977.42 1250.03 17 -7 7 9 10524.2 1788.41 17 7 7 -9 7908.72 1713.17 15 7 -7 -9 11872.9 2138.79 15 -7 -7 9 6281.66 1272.80 8 -7 -7 9 8828.40 1899.49 14 -7 7 9 10453.3 2025.57 14 -7 7 8 39.0781 618.322 8 7 7 -8 1704.80 701.668 13 7 -7 -8 585.287 531.298 6 -7 -7 8 1019.34 520.837 12 7 7 -8-625.920 1080.64 10 7 -7 -8 945.139 651.598 10 -7 7 8 1655.28 958.857 17 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1580.96 724.114 5 -7 7 5 1516.72 513.588 9 7 7 -5 1691.17 668.707 15 7 -7 -5 2259.32 898.276 15 -7 -7 5 678.063 613.786 8 -7 -7 5 1535.77 760.505 14 -7 7 4 8885.16 1305.30 8 7 7 -4 11538.6 1151.89 13 7 -7 -4 10846.3 1504.38 6 7 7 -4 9036.54 1091.80 21 -7 7 4 9847.88 1563.23 2 -7 -7 4 9694.33 994.069 19 7 7 -4 9749.15 1676.46 10 7 -7 -4 10588.7 1781.03 10 -7 7 4 10706.1 1433.40 17 -7 -7 4 8286.55 1310.46 5 -7 7 4 11265.1 1230.73 9 7 7 -4 12875.2 1515.36 15 -7 -7 4 11401.4 1422.16 8 7 -7 -4 9445.99 1796.21 15 -7 -7 4 9286.86 1483.31 14 -7 7 3-71.3030 490.771 8 7 -7 -3 375.742 620.862 7 7 7 -3 353.402 602.060 3 7 -7 -3 203.742 245.449 4 7 -7 -3 49.9596 509.976 6 7 7 -3 821.045 398.414 21 -7 7 3 660.067 357.246 20 -7 -7 3 302.351 330.302 19 7 7 -3 176.204 547.694 10 -7 7 3 1204.41 556.485 17 -7 -7 3-94.0210 444.158 5 -7 7 3 769.235 438.528 9 7 7 -3 384.200 357.226 15 7 -7 -3-170.794 740.168 15 -7 -7 3-107.693 454.877 14 -7 7 2 12430.3 1413.74 8 7 7 -2 14207.7 1819.43 3 7 -7 -2 12240.9 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3159.43 10 8 -6 -10 16516.1 2758.21 10 -8 -6 10 14630.7 1934.91 17 -8 6 10 16619.5 2284.44 17 8 6 -10 14055.4 2418.78 15 8 -6 -10 14218.9 2542.73 15 -8 -6 10 17588.0 2222.16 8 -8 -6 10 16659.0 2668.71 14 -8 6 10 16559.8 2771.18 14 -8 6 9 6782.29 1402.68 8 8 6 -9 7845.31 1362.70 13 8 6 -9 5066.94 1550.13 10 8 -6 -9 6465.08 1677.81 10 -8 -6 9 5752.89 1270.18 17 -8 6 9 7287.42 1536.73 17 8 6 -9 6324.08 1562.37 15 8 -6 -9 8140.60 1958.20 15 -8 -6 9 5479.84 1277.81 8 -8 -6 9 7293.62 1785.48 14 -8 6 9 6319.93 1763.62 14 8 6 -8 39861.7 2914.06 13 8 -6 -8 41032.5 3355.14 6 8 6 -8 37438.4 3936.30 10 8 -6 -8 37608.5 3869.58 10 -8 -6 8 44001.4 3267.59 17 -8 6 8 39844.7 3325.36 17 8 6 -8 38710.3 3581.14 15 8 -6 -8 41441.5 4070.67 15 -8 -6 8 37575.1 3069.09 8 -8 -6 8 39789.6 3786.43 14 -8 6 8 38838.6 3910.81 14 -8 6 8 36816.2 3048.97 8 -8 6 7 6623.14 1275.09 8 8 6 -7 7457.82 1191.39 13 8 -6 -7 6633.28 1319.92 6 8 6 -7 5673.31 1508.87 10 8 -6 -7 8128.67 1867.55 10 -8 6 7 5946.88 1294.27 17 8 6 -7 7443.71 1517.08 15 8 -6 -7 9591.65 2098.47 15 -8 -6 7 5402.85 1133.73 8 -8 -6 7 5451.87 1435.64 14 -8 6 7 6401.34 1637.66 14 8 6 -6 55132.6 3114.76 13 8 -6 -6 48640.1 3456.85 6 8 6 -6 54452.0 4415.74 10 8 -6 -6 50537.2 4315.75 10 -8 6 6 58068.0 4179.77 2 -8 6 6 55188.5 3645.37 17 8 6 -6 53843.7 3827.01 15 8 -6 -6 55765.1 4523.78 15 -8 -6 6 52614.6 3443.24 8 -8 -6 6 57645.2 4206.13 14 -8 6 6 49788.5 3344.24 8 -8 6 6 54202.4 4363.73 14 -8 6 5 1323.77 534.567 8 8 -6 -5 3724.61 1011.80 6 -8 6 5 1918.55 858.273 2 8 6 -5 2834.87 1103.37 10 8 -6 -5 3918.80 1206.52 10 -8 6 5 3395.01 1015.49 17 -8 -6 5 3537.41 940.071 5 -8 6 5 2825.63 689.590 9 8 6 -5 4613.43 1131.25 15 8 -6 -5 2849.75 1013.48 15 -8 -6 5 2317.15 715.108 8 -8 -6 5 2399.53 829.220 14 8 -6 -4 43812.2 3083.34 6 8 6 -4 40343.3 2514.74 21 8 6 -4 42205.9 3621.52 10 8 -6 -4 38374.5 3592.01 10 -8 -6 4 37926.1 2863.89 5 -8 6 4 42174.9 2982.33 17 -8 6 4 45539.8 3501.44 2 -8 6 4 41065.9 2566.04 9 8 6 -4 44094.2 3144.24 15 8 -6 -4 36862.8 3662.54 15 -8 -6 4 40585.2 2794.05 8 -8 -6 4 44607.8 3399.13 14 -8 6 4 40011.0 2801.35 8 -8 6 3 500.985 491.938 8 8 -6 -3 397.511 607.696 7 8 -6 -3 282.908 479.224 6 8 6 -3 640.271 462.685 21 -8 -6 3 443.724 415.279 19 8 6 -3-142.924 622.833 10 -8 6 3 1369.20 564.155 17 -8 -6 3 860.767 641.990 5 -8 6 3 550.143 458.501 9 8 6 -3 1552.77 691.939 15 8 -6 -3 62.3046 816.163 15 -8 -6 3 567.844 532.214 8 -8 -6 3 82.2450 500.909 14 8 -6 -2 23165.3 2685.58 7 8 -6 -2 22552.2 2126.63 6 8 6 -2 21763.1 1900.15 21 -8 6 2 21773.4 1667.26 20 -8 -6 2 22144.7 1812.31 19 8 6 -2 27114.6 2790.21 10 -8 -6 2 22552.3 2069.62 5 8 6 -2 25520.8 2830.56 18 -8 6 2 25175.0 2150.05 17 8 6 -2 27863.2 2660.11 3 -8 6 2 23137.2 1942.58 9 8 -6 -2 22340.1 1652.24 4 -8 -6 2 22811.8 1915.95 8 8 -6 -2 21170.7 2716.11 15 -8 6 2 25450.4 2031.11 8 -8 -6 2 21059.4 2175.10 14 -8 6 1 278.016 391.617 8 8 6 -1-283.049 696.178 3 8 -6 -1-149.370 377.400 4 8 -6 -1-87.2974 724.979 7 8 6 -1 455.138 484.904 21 8 -6 -1 538.760 504.875 6 -8 6 1-158.046 396.538 20 -8 -6 1 489.123 360.381 19 8 6 -1-620.948 897.018 18 -8 6 1 442.571 397.646 17 8 6 -1 667.430 561.080 10 -8 -6 1 347.425 495.553 5 -8 6 1 1160.69 533.007 9 8 -6 -1 324.140 902.853 15 -8 -6 1 209.621 342.780 8 -8 -6 1 931.931 601.505 14 8 6 0 4205.72 1194.88 3 8 6 0 2733.28 991.853 7 8 -6 0 3717.12 779.045 4 8 -6 0 2810.78 893.828 7 8 -6 0 3940.71 927.036 6 -8 6 0 3028.00 695.069 20 -8 -6 0 2134.04 673.387 19 8 6 0 3745.33 1332.06 18 -8 6 0 3509.72 808.250 17 -8 -6 0 2695.82 793.161 5 8 6 0 3025.96 800.670 21 -8 6 0 4218.15 917.921 9 8 -6 0 4114.69 1310.03 15 -8 -6 0 3651.01 706.712 8 -8 -6 0 4864.83 1009.38 14 8 6 1 369.805 618.034 3 8 6 1 1122.25 775.793 7 8 -6 1 463.061 494.192 4 8 -6 1 51.2112 791.890 7 8 6 1 379.862 539.257 21 8 -6 1 527.039 491.980 21 8 -6 1 1176.63 607.149 6 -8 6 -1 373.948 467.972 20 -8 -6 -1 230.910 441.798 19 8 6 1 2456.04 990.106 18 -8 6 -1 733.722 453.560 17 -8 -6 -1 868.348 381.917 5 -8 6 -1 551.044 598.412 9 8 -6 1 160.892 1075.37 15 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20130.4 1932.04 4 8 6 4 21239.6 2633.71 3 8 -6 5 10146.1 1465.04 4 8 6 5 8830.85 1511.29 21 8 -6 5 8265.95 1384.15 21 -8 -6 -5 8936.58 1426.08 20 -8 6 -5 9619.76 1435.37 20 -8 -6 -5 10301.2 1576.33 19 8 6 5 8099.60 1693.41 18 -8 -6 -5 9223.16 1455.06 9 8 6 5 9601.17 1487.86 4 -8 6 -5 9719.64 1561.80 9 8 6 5 11018.6 1962.69 3 8 -6 6 29589.1 2627.36 21 -8 -6 -6 28421.8 2606.94 20 -8 6 -6 27965.4 2467.98 20 -8 -6 -6 28399.2 2682.03 19 8 6 6 37982.4 3557.75 3 8 6 6 30953.0 3173.39 18 -8 -6 -6 32723.6 2728.98 9 -8 6 -6 32610.1 2870.24 9 8 6 6 29583.1 2709.45 4 8 -6 6 27889.5 2460.03 4 8 -6 7 5227.41 1195.53 4 8 -6 7 7779.29 1419.60 21 -8 -6 -7 6091.97 1257.41 20 -8 6 -7 8425.71 1418.70 20 -8 -6 -7 4595.90 1183.73 19 8 6 7 7221.97 1603.05 18 -8 -6 -7 6096.90 1231.46 9 -8 6 -7 8957.43 1555.02 9 8 6 7 4429.29 1277.80 3 8 6 7 5574.26 1238.63 4 8 -6 8 25927.6 2646.92 21 -8 -6 -8 26385.3 2637.75 20 -8 6 -8 25728.3 2527.50 20 -8 -6 -8 22780.0 2528.90 19 8 6 8 30933.4 3137.95 18 -8 -6 -8 24902.7 2457.14 9 -8 6 -8 28819.4 2872.74 9 8 6 8 27926.6 3014.41 3 8 -6 8 30578.0 2725.56 4 8 6 8 26944.2 2743.49 4 -8 6 -9 10236.9 2047.71 13 8 -6 9 8017.94 1522.12 4 8 -6 9 7682.58 1529.60 21 -8 -6 -9 8004.02 1496.43 20 -8 6 -9 9512.99 1609.28 20 -8 -6 -9 8187.65 1639.70 19 -8 6 -9 8184.76 2069.30 1 -8 -6 -9 11095.0 2341.86 1 8 6 9 10378.2 1828.49 18 -8 -6 -9 9150.39 1573.62 9 8 6 9 8328.40 1713.03 3 -8 6 -9 10898.3 1866.73 9 8 6 9 11247.5 1853.33 4 -8 6 -10 20062.4 3275.11 1 -8 -6 -10 16580.1 2946.77 1 8 -6 10 17023.1 2292.29 21 -8 -6 -10 13771.5 2003.49 20 -8 -6 -10 17104.9 2286.36 19 -8 -6 -10 14880.1 1946.90 9 -8 6 -10 14240.5 2139.07 9 8 6 10 9912.24 1743.17 4 8 -6 11 1704.89 884.152 21 8 7 -11 6280.80 1405.14 13 8 7 -11 3075.48 1242.77 15 -8 7 11 4184.89 1645.98 14 -8 7 10 14995.4 2107.31 8 8 7 -10 13624.1 1869.06 13 8 -7 -10 13175.9 2015.08 6 8 7 -10 16826.7 2910.93 10 8 -7 -10 15437.9 2606.44 10 -8 -7 10 12471.2 1897.89 17 -8 7 10 14537.4 2194.01 17 8 7 -10 12619.9 2292.68 15 8 -7 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7 6 1916.27 1016.08 14 -8 7 6 364.085 559.097 8 -8 7 6 1738.13 918.462 2 8 -7 -6 2185.81 924.084 6 8 7 -6 1672.31 944.407 10 8 -7 -6 1462.02 993.211 10 -8 7 6-430.198 684.222 17 -8 -7 6 1812.96 857.601 5 8 7 -6 388.714 485.893 15 8 -7 -6 1484.67 745.314 15 -8 -7 6 1034.07 673.608 8 -8 -7 6 1349.55 756.634 14 -8 7 5 8072.97 1326.00 8 8 -7 -5 5539.25 1192.77 6 -8 7 5 10145.4 1712.27 2 8 7 -5 7295.71 1551.70 10 8 -7 -5 5786.08 1473.33 10 -8 7 5 8188.11 1437.48 17 -8 -7 5 5445.47 1153.89 5 -8 7 5 8089.56 1090.43 9 8 -7 -5 6400.59 1511.31 15 -8 -7 5 4858.78 1042.87 8 -8 -7 5 9437.89 1641.10 14 -8 7 4 3697.46 889.590 8 8 -7 -4 4683.28 1331.72 7 8 -7 -4 3501.58 975.228 6 8 7 -4 3869.47 797.387 21 -8 7 4 3057.33 1034.03 2 8 7 -4 5021.86 1355.88 10 -8 7 4 5284.19 1103.36 17 8 -7 -4 2329.85 1161.94 10 -8 -7 4 3914.35 994.960 5 -8 7 4 5520.51 944.809 9 8 -7 -4 6237.90 1560.19 15 -8 -7 4 5551.02 1092.48 8 -8 -7 4 4016.36 1115.64 14 -8 7 3 16837.9 1755.89 8 8 -7 -3 19751.1 2448.52 7 8 7 -3 13871.4 1955.43 3 8 7 -3 16989.4 1681.29 21 8 -7 -3 15829.6 1827.92 6 -8 -7 3 13494.1 1353.33 19 8 7 -3 16285.0 2262.60 18 8 7 -3 13206.2 1967.16 10 -8 7 3 13885.9 1679.23 17 -8 -7 3 12003.0 1615.00 5 -8 7 3 14078.9 1544.02 9 8 -7 -3 12273.9 2092.94 15 -8 -7 3 14477.5 1639.68 8 -8 -7 3 13692.8 1814.54 14 -8 7 2 6518.51 1114.06 8 8 7 -2 8736.02 1587.99 3 8 -7 -2 6514.88 1471.43 7 8 -7 -2 7633.49 980.656 4 8 7 -2 8023.08 1174.43 21 8 -7 -2 9827.33 1437.35 6 -8 7 2 8139.07 1071.34 20 -8 -7 2 7142.52 1048.08 19 8 7 -2 7848.74 1605.02 18 8 7 -2 8550.01 1558.87 10 -8 7 2 6002.65 1112.37 17 -8 -7 2 11103.6 1511.34 5 -8 7 2 8174.67 1190.51 9 8 -7 -2 8780.79 1865.02 15 -8 -7 2 6814.14 1110.70 8 -8 -7 2 7824.10 1366.62 14 8 7 -1 13203.9 1902.75 3 8 -7 -1 16929.4 2333.28 7 8 -7 -1 19908.8 2094.65 6 8 7 -1 18398.3 1866.66 21 -8 7 1 17766.4 1601.00 20 -8 -7 1 15799.1 1620.65 19 8 7 -1 19357.3 2491.11 18 -8 7 1 15957.9 1730.27 17 8 7 -1 22629.6 2448.00 10 -8 7 1 18887.8 1871.64 9 -8 -7 1 16500.6 1831.28 5 8 -7 -1 17131.7 1535.45 4 -8 -7 1 16857.1 1649.60 8 8 -7 -1 12925.2 2350.90 15 -8 -7 1 15940.8 1829.61 14 8 7 0 23246.5 2546.15 3 8 7 0 21031.1 2496.74 7 8 -7 0 18024.6 2386.54 7 8 7 0 15145.3 1750.51 21 8 -7 0 17335.3 2004.08 6 -8 7 0 21361.4 1833.08 20 -8 -7 0 20491.9 1924.94 19 8 7 0 24965.1 2876.80 18 -8 7 0 19988.3 1868.33 17 -8 7 0 19966.6 1955.15 9 -8 -7 0 17844.1 1905.51 5 -8 -7 0 20255.3 1732.79 8 8 -7 0 19629.8 1710.81 4 8 -7 0 16826.5 2541.32 15 -8 -7 0 23369.5 2151.10 14 8 7 1 25547.8 2685.89 7 8 -7 1 25094.7 2841.27 7 8 -7 1 25233.4 2447.48 6 8 -7 1 21923.7 2146.37 21 8 7 1 19831.0 2041.47 21 -8 7 -1 21339.5 1890.10 20 -8 -7 -1 20700.8 2010.12 19 -8 -7 -1 22256.2 2092.79 5 8 7 1 20039.3 2618.01 18 -8 7 -1 21038.0 1887.09 17 8 7 1 26001.9 2775.02 3 -8 7 -1 22917.1 2141.73 9 8 -7 1 19654.5 1789.47 4 8 -7 1 24194.2 3083.66 15 -8 -7 -1 23652.8 2112.23 14 8 7 2 32158.7 3015.99 7 8 -7 2 30904.0 3183.46 7 8 7 2 31323.6 2625.29 21 8 -7 2 32474.7 2634.13 21 -8 7 -2 31688.8 2357.58 20 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4036.04 1136.57 9 9 3 -11 4700.29 1260.88 13 -9 3 10 1235.96 720.544 8 9 3 -10 1013.62 715.891 13 -9 -3 10 279.425 567.867 17 9 3 -10 540.432 885.412 15 -9 3 10 1519.86 1198.92 14 -9 -3 10-219.122 579.908 8 -9 3 9 16339.8 2110.64 8 9 3 -9 19821.4 2246.75 13 9 3 -9 19253.6 3093.89 10 9 -3 -9 23560.3 3384.95 10 -9 -3 9 12992.2 1893.89 17 -9 3 9 19000.3 2341.61 17 9 3 -9 17274.9 2619.92 15 9 -3 -9 21678.8 3167.56 15 -9 -3 9 24345.9 3124.37 14 -9 -3 9 16888.0 2139.48 8 -9 3 9 22084.8 3145.30 14 -9 3 8 4015.61 1116.63 8 9 3 -8 2255.40 797.937 13 9 3 -8 2403.95 1496.28 10 9 -3 -8 1954.16 923.946 10 -9 -3 8 4139.03 1106.11 17 -9 3 8 3270.71 1037.41 17 9 3 -8 3817.35 1350.63 15 9 -3 -8 4053.08 1534.04 15 -9 -3 8 2738.45 903.094 8 -9 -3 8 2103.57 1217.23 14 -9 3 8 3473.48 1381.10 14 9 3 -7 34255.6 2724.10 13 9 -3 -7 36819.8 4068.76 10 -9 -3 7 34045.8 2914.73 17 -9 3 7 34231.8 2980.99 17 9 3 -7 38906.6 4073.17 10 9 3 -7 33380.6 3433.28 15 9 -3 -7 36052.1 3796.20 15 -9 -3 7 33577.3 2824.36 8 -9 3 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8426.14 1203.33 8 9 -3 -3 6582.79 1634.77 7 9 -3 -3 9398.34 1313.17 6 9 3 -3 7610.94 1194.78 21 9 -3 -3 8291.61 1334.31 21 -9 3 3 8588.56 1348.75 17 9 3 -3 9207.02 1825.70 10 9 -3 -3 8997.66 1935.09 10 -9 3 3 8455.14 1260.21 9 9 3 -3 6620.40 1401.20 15 9 -3 -3 10089.9 1933.71 15 -9 -3 3 7464.83 1153.76 8 -9 -3 3 7033.27 1408.06 14 -9 3 2 11494.4 1344.73 8 9 -3 -2 12122.4 2102.72 7 9 -3 -2 11369.1 1384.37 6 9 3 -2 12950.2 1535.22 21 9 -3 -2 11795.7 1560.26 21 -9 -3 2 12542.1 1343.87 20 9 3 -2 9859.04 1784.43 18 -9 3 2 11189.9 1503.23 17 9 3 -2 10861.9 2036.75 10 -9 3 2 14209.1 1626.84 9 9 3 -2 10659.9 1698.85 15 9 -3 -2 10386.1 1995.11 15 -9 -3 2 11146.1 1310.71 8 -9 -3 2 12001.4 1752.04 14 -9 3 1 1303.62 512.690 8 9 -3 -1 1512.58 491.366 4 9 3 -1 1808.11 999.856 7 9 3 -1 2017.11 930.232 3 9 -3 -1 233.041 808.584 7 9 3 -1 1960.91 720.093 21 9 -3 -1 1942.65 828.230 21 -9 -3 1 1149.02 482.358 20 -9 3 1 1453.70 499.916 20 -9 -3 1 1505.55 637.770 19 9 3 -1 2673.32 1081.75 18 -9 3 1 1758.75 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-2 109.342 529.169 21 11 -5 -2-519.524 671.374 21 11 5 -2 472.375 859.348 18 -11 5 2 320.656 559.725 17 -11 -5 2 864.604 877.041 9 -11 5 2 404.762 562.205 9 11 -5 -2 482.059 800.542 15 -11 -5 2 405.235 678.723 14 11 5 -1 7666.78 1738.43 3 11 5 -1 6377.54 1818.92 7 11 -5 -1 7801.44 1971.72 7 11 5 -1 5583.33 1253.42 21 11 -5 -1 8413.24 1559.64 21 11 5 -1 7986.27 1860.06 18 -11 5 1 5563.67 1275.38 17 -11 -5 1 6339.63 1458.34 9 -11 5 1 7367.08 1415.24 9 11 -5 -1 12088.1 2537.90 15 -11 -5 1 7768.63 1608.24 14 11 5 0 124.655 940.334 7 11 -5 0 1244.85 1246.03 7 11 5 0 684.153 594.985 21 11 -5 0 238.238 705.488 21 -11 -5 0 1596.95 689.492 20 -11 -5 0 504.969 584.841 19 11 5 0 1557.14 1088.84 18 -11 5 0 800.672 632.921 17 -11 -5 0 166.840 659.692 9 -11 5 0 1005.69 784.115 9 11 -5 0-1083.92 1239.16 15 -11 -5 0-30.9363 605.587 14 11 5 1 1230.88 1244.86 7 11 5 1 361.388 598.182 21 11 -5 1-356.784 547.462 21 -11 -5 -1 670.797 608.060 20 -11 -5 -1 2359.27 942.093 19 11 5 1 2230.10 1140.73 18 -11 5 -1 745.764 544.400 17 -11 -5 -1 2307.43 996.241 9 -11 5 -1-171.062 710.951 9 11 5 1 896.258 646.201 3 -11 -5 -1 641.238 529.580 14 11 -5 2 3861.11 1020.24 4 11 5 2 2012.03 1193.37 7 11 5 2 3082.53 1004.72 21 -11 -5 -2 4411.64 1161.92 20 -11 5 -2 3074.45 955.287 20 -11 -5 -2 5064.67 1305.02 19 11 5 2 2801.98 1129.83 18 -11 5 -2 3826.60 1060.52 17 -11 5 -2 2958.07 959.105 9 11 5 2 3822.64 1419.25 3 11 -5 3-224.410 565.138 4 11 5 3-843.714 801.619 7 11 5 3 633.559 811.468 21 -11 -5 -3 1091.80 740.065 20 -11 5 -3 494.269 614.924 20 -11 -5 -3 157.018 477.932 19 11 5 3 2449.69 1392.34 3 11 -5 4 18248.0 2183.72 4 -11 -5 -4 18778.7 2342.33 20 -11 5 -4 19527.7 2227.15 20 -11 6 6 1218.85 722.161 8 -11 -6 6-1283.53 1003.76 8 11 6 -5-641.666 975.338 10 11 6 -4 1110.85 949.707 10 -11 -6 4 100.906 696.135 14 11 6 -3 3019.57 1377.28 3 11 6 -3 7480.83 1899.12 7 11 6 -3 4968.03 1682.03 18 -11 6 3 3640.02 1074.33 17 -11 6 3 3385.99 978.742 9 11 -6 -3 6164.66 1817.00 15 -11 -6 3 4515.05 1367.90 14 11 6 -2 679.921 624.605 3 11 6 -2 3050.64 1358.79 7 11 6 -2 2160.36 889.371 21 11 -6 -2 4014.32 1195.30 21 11 6 -2 2113.36 1226.16 18 -11 6 2 2040.45 819.684 17 -11 6 2 2004.68 769.789 9 11 -6 -2 2892.07 1579.92 15 -11 -6 2 2163.61 1018.21 14 11 6 -1 5763.53 1571.36 3 11 6 -1 7414.45 1897.99 7 11 6 -1 7300.23 1439.12 21 11 -6 -1 6555.13 1447.69 21 11 6 -1 10614.8 2203.30 18 -11 6 1 4411.48 1142.30 17 -11 6 1 5329.05 1214.40 9 11 -6 -1 4771.42 1628.10 15 -11 -6 1 6223.88 1455.35 14 11 6 0 8178.48 1900.01 7 11 6 0 9205.10 1643.44 21 -11 -6 0 7126.02 1349.51 20 -11 -6 0 6462.34 1312.72 19 11 6 0 8184.88 2000.42 18 -11 6 0 5181.87 1128.83 17 -11 6 0 5219.05 1230.66 9 -11 -6 0 8119.23 1618.96 14 11 6 0 8492.93 1825.56 3 11 6 1 1622.95 839.211 7 11 6 1 1823.07 885.507 21 -11 -6 -1 3665.68 1065.94 20 -11 -6 -1 3349.94 1094.10 19 11 6 1 1315.20 799.258 18 -11 6 -1 1360.87 566.198 17 -11 6 -1 2827.04 937.915 9 11 6 1 1218.94 908.979 3 -11 -6 -1 3257.10 1072.92 14 11 -6 2 10415.0 1584.86 4 11 6 2 13679.3 2430.81 7 11 6 2 11064.3 1892.40 21 -11 -6 -2 10601.4 1731.79 20 -11 6 -2 12950.6 1756.59 20 -11 -6 -2 12274.4 1850.59 19 11 6 2 14223.8 2401.46 18 -11 6 -2 11471.6 1636.17 17 11 6 2 8466.70 1879.48 3 11 -6 3 1609.73 835.601 4 11 6 3 2068.65 1093.10 7 -11 -6 -3 295.125 555.699 20 -11 6 -3 1440.37 771.517 20 -11 -6 -3 663.389 731.919 19 11 6 3 640.225 823.844 18 11 6 3 721.531 710.140 3 11 -6 4 5095.82 1204.03 4 -11 6 -4 6776.47 1448.51 20 11 7 -5 1203.17 751.890 10 11 7 -4-746.184 1050.27 10 11 7 -3 11382.5 2305.78 7 11 7 -3 7928.90 1969.24 18 -11 7 3 9513.89 1593.07 9 -11 -7 3 8190.03 1673.23 14 11 7 -2-923.118 1027.50 3 11 7 -2-224.489 638.523 7 -11 7 2 465.194 546.945 17 -11 -7 2 905.997 673.552 5 -11 7 2 594.363 691.269 9 -11 -7 2 1014.95 773.616 14 11 7 -1 7648.57 1781.95 3 11 7 -1 6902.05 1830.60 7 11 7 -1 7076.17 1384.83 21 11 7 -1 8908.79 2036.71 18 -11 7 1 6065.83 1292.43 17 -11 -7 1 6890.48 1335.74 5 -11 7 1 7671.49 1443.24 9 11 -7 -1 6093.94 1899.71 15 -11 -7 1 8511.65 1689.65 14 11 7 0 503.082 587.409 7 11 7 0 1394.87 828.456 21 -11 -7 0 1912.10 766.269 20 -11 -7 0 1483.92 831.979 19 11 7 0 2453.61 1340.28 18 -11 7 0 2862.01 957.128 17 -11 7 0 1090.48 774.046 9 11 7 0 2808.70 1222.68 3 -11 -7 0 2060.93 909.170 14 11 7 1-409.812 718.427 7 11 7 1-63.0917 543.965 21 -11 -7 -1 1966.45 792.374 20 -11 -7 -1 659.941 586.579 19 11 7 1 339.719 731.358 18 -11 7 -1-529.042 633.956 17 -11 7 -1 326.572 572.862 9 11 7 1 361.170 749.465 3 11 -7 2 3301.00 981.518 4 11 7 2 2164.38 984.288 21 -11 -7 -2 2464.45 943.659 20 -11 7 -2 1995.33 780.811 20 -11 -7 -2 2861.98 975.688 19 11 7 2 1896.36 1013.99 18 11 7 2 2356.79 1054.27 3 11 -7 3 3359.97 1018.33 4 -11 -7 -3 1591.59 849.076 20 -11 7 -3 3273.54 989.820 20 -11 -7 -3 1444.82 749.211 19 11 7 3 2962.92 1184.67 18 11 7 3 1553.10 912.071 3 11 -7 4 1065.69 634.512 4 11 7 4 2863.19 1264.90 3 11 8 -3 1044.91 986.849 7 -11 -8 3-172.230 493.467 5 -11 -8 3 1013.16 818.050 14 11 8 -2 7014.47 1700.45 7 11 8 -2 7072.40 1909.49 18 -11 8 2 4125.67 1172.77 17 -11 -8 2 7814.51 1497.93 5 -11 8 2 4248.72 1106.43 9 -11 -8 2 7903.63 1583.27 14 11 8 -1 219.989 601.258 7 11 8 -1 345.134 908.143 18 -11 8 1-464.710 553.464 17 -11 -8 1-505.382 560.699 5 -11 8 1 504.320 557.929 9 -11 -8 1-58.7901 567.627 14 11 8 0 8626.21 1622.75 21 -11 -8 0 11824.9 1791.03 20 11 8 0 12881.7 2460.34 18 -11 8 0 8577.92 1517.00 17 -11 8 0 10499.4 1741.41 9 11 8 1-710.797 767.952 21 -11 -8 -1 228.338 745.160 20 -11 -8 -1 193.393 487.789 19 11 8 1 78.2935 822.409 18 -11 8 -1 10.0444 474.249 17 11 8 1 589.080 678.442 3 -11 -8 -2 18049.5 2308.06 20 -11 -8 -2 14496.5 2049.37 19 11 8 2 18541.9 2929.54 18 11 8 2 14837.7 2488.36 3 11 -8 3 73.3660 518.384 4 -11 8 -3-60.6367 480.193 20 11 8 3-74.0122 704.209 18 11 8 4 7945.51 1926.53 18 -11 -9 3 14525.6 2250.27 14 -11 -9 2 1088.43 794.624 5 -11 9 2-348.014 540.011 9 -11 9 1 7611.84 1512.74 17 -11 -9 1 5192.38 1260.53 5 -11 9 1 8034.20 1498.51 9 -11 -9 0 653.042 680.824 20 -11 9 0-383.219 562.755 17 -11 -9 -1 1300.63 855.743 20 -11 -9 -1 2967.23 1024.64 19 -11 -10 0 11137.5 1833.95 5 -12 0 -3 447.033 614.734 20 -12 0 -3-139.300 652.673 17 12 0 3-417.777 609.917 4 -12 0 -4 52416.5 3832.75 17 12 1 -4 13116.6 1891.34 21 12 -1 -4 14203.1 2675.74 15 12 1 -3 19539.2 2321.82 21 -12 1 -2 13890.3 1972.30 17 12 -1 3 26002.5 2690.98 4 -12 1 -3 21078.3 2357.34 20 -12 1 -3 25449.5 2652.56 17 12 1 3 22593.7 2605.38 4 12 2 -3 11751.6 2178.84 3 12 2 -3 12309.3 1874.79 21 12 -2 -3 13830.5 2673.27 15 12 2 -2 5678.22 1316.74 21 12 -2 -2 6794.11 1934.70 15 12 -2 -1-989.333 1150.70 15 -12 -2 -2 633.423 651.764 20 -12 2 -2 401.163 685.229 17 12 2 2 436.725 537.115 4 -12 2 -3 18354.4 2166.60 20 -12 2 -3 14529.1 1984.58 17 12 3 -3 9537.60 1639.16 21 12 3 -2 11812.2 2194.88 3 12 3 -2 13449.9 1971.50 21 12 -3 -2 14845.5 2695.94 15 12 -3 -1 5233.22 1697.43 15 -12 3 -1 2079.27 970.847 17 -12 -3 -2 23070.2 2468.56 20 -12 3 -2 24451.3 2580.47 17 12 -3 3 1189.97 666.081 4 12 4 -2-196.899 667.971 21 12 4 -1 18564.2 2739.44 3 -12 -4 -2 1646.88 829.129 20 -12 4 -2 2751.90 917.666 17 12 5 0 130.617 894.253 3 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 8174 _shelx_res_file ; TITL Simon in P2(1)/n shelx.res created by SHELXL-2019/3 at 11:35:02 on 19-Oct-2023 CELL 0.71073 8.600988 15.043479 11.721846 90.0000 91.2016 90.0000 ZERR 4.00 0.0002 0.0003 0.0002 0.0000 0.002 0.0000 LATT 1 SYMM 1/2 - X, 1/2 + Y, 1/2 - Z SFAC C H P S I AU UNIT 40 92 4 4 4 4 MERG 2 FMAP 2 PLAN 10 L.S. 6 SIZE 0.25 0.2 0.15 TEMP -173 ACTA 60 CONF 2.3 BOND $H HTAB C13 AU1 HTAB C32 AU1 EQIV $1 1-x,1-y,1-z HTAB C32 AU1_$1 HTAB C3 I1_$1 EQIV $2 0.5-x, 0.5+y, 0.5-z HTAB C2 I1_$2 WGHT 0.008800 1.027300 EXTI 0.001484 FVAR 2.16618 AU1 6 0.474936 0.403782 0.284312 11.00000 0.01542 0.00842 = 0.01597 0.00117 0.00001 0.00169 I1 5 0.744077 0.334058 0.278309 11.00000 0.01663 0.01449 = 0.01896 0.00049 0.00109 0.00388 S1 4 0.225951 0.455512 0.304802 11.00000 0.01473 0.00909 = 0.02425 0.00316 0.00139 0.00003 P1 3 0.233746 0.587881 0.270793 11.00000 0.00963 0.00774 = 0.01145 -0.00006 -0.00040 0.00039 C1 1 0.301076 0.612765 0.123324 11.00000 0.01461 0.01113 = 0.01090 -0.00082 -0.00014 0.00078 C2 1 0.032100 0.627361 0.284785 11.00000 0.01049 0.01338 = 0.01667 -0.00079 -0.00113 0.00289 AFIX 13 H2 2 0.031468 0.692691 0.269023 11.00000 -1.20000 AFIX 0 C3 1 0.345353 0.646624 0.384227 11.00000 0.01511 0.01280 = 0.01052 -0.00137 -0.00145 0.00065 AFIX 13 H3 2 0.294656 0.629094 0.456854 11.00000 -1.20000 AFIX 0 C11 1 0.236030 0.703213 0.083514 11.00000 0.02538 0.01391 = 0.01541 0.00371 0.00050 0.00123 AFIX 137 H11A 2 0.274795 0.750085 0.134732 11.00000 -1.50000 H11B 2 0.122165 0.701820 0.084786 11.00000 -1.50000 H11C 2 0.269733 0.715298 0.005688 11.00000 -1.50000 AFIX 0 C12 1 0.244292 0.538692 0.041285 11.00000 0.02645 0.01799 = 0.01353 -0.00417 -0.00010 -0.00002 AFIX 137 H12A 2 0.276013 0.552714 -0.036485 11.00000 -1.50000 H12B 2 0.130673 0.534550 0.043301 11.00000 -1.50000 H12C 2 0.290158 0.481811 0.064982 11.00000 -1.50000 AFIX 0 C13 1 0.478799 0.615944 0.120735 11.00000 0.01631 0.01882 = 0.01672 -0.00008 0.00432 -0.00094 AFIX 137 H13A 2 0.512145 0.620595 0.041526 11.00000 -1.50000 H13B 2 0.521687 0.561583 0.155051 11.00000 -1.50000 H13C 2 0.516379 0.667689 0.163971 11.00000 -1.50000 AFIX 0 C21 1 -0.082093 0.583484 0.199642 11.00000 0.01160 0.02022 = 0.02642 -0.00188 -0.00286 -0.00022 AFIX 137 H21A 2 -0.075648 0.518716 0.207366 11.00000 -1.50000 H21B 2 -0.055407 0.600599 0.121796 11.00000 -1.50000 H21C 2 -0.188143 0.603120 0.215394 11.00000 -1.50000 AFIX 0 C22 1 -0.025961 0.613826 0.406313 11.00000 0.01539 0.03591 = 0.01997 0.00152 0.00481 0.00638 AFIX 137 H22A 2 -0.130189 0.639457 0.412544 11.00000 -1.50000 H22B 2 0.045174 0.643261 0.460694 11.00000 -1.50000 H22C 2 -0.029986 0.550107 0.423391 11.00000 -1.50000 AFIX 0 C31 1 0.329625 0.748271 0.378950 11.00000 0.02124 0.01543 = 0.02383 -0.00388 -0.00698 0.00104 AFIX 137 H31A 2 0.368103 0.774178 0.450869 11.00000 -1.50000 H31B 2 0.220047 0.764234 0.366862 11.00000 -1.50000 H31C 2 0.390690 0.771245 0.315753 11.00000 -1.50000 AFIX 0 C32 1 0.515815 0.619826 0.400684 11.00000 0.01569 0.01744 = 0.01983 -0.00357 -0.00559 -0.00117 AFIX 137 H32A 2 0.578901 0.650631 0.344340 11.00000 -1.50000 H32B 2 0.526015 0.555442 0.390538 11.00000 -1.50000 H32C 2 0.551796 0.636229 0.477722 11.00000 -1.50000 AFIX 0 HKLF 4 REM Simon in P2(1)/n REM wR2 = 0.0327, GooF = S = 1.120, Restrained GooF = 1.120 for all data REM R1 = 0.0178 for 4213 Fo > 4sig(Fo) and 0.0221 for all 4580 data REM 135 parameters refined using 0 restraints END WGHT 0.0088 1.0269 REM Highest difference peak 0.923, deepest hole -0.685, 1-sigma level 0.133 Q1 1 0.5427 0.4015 0.2181 11.00000 0.05 0.92 Q2 1 0.4076 0.4021 0.3383 11.00000 0.05 0.89 Q3 1 0.8402 0.3315 0.2728 11.00000 0.05 0.76 Q4 1 0.8185 0.3321 0.2284 11.00000 0.05 0.70 Q5 1 0.7121 0.3319 0.3609 11.00000 0.05 0.67 Q6 1 0.8082 0.3316 0.3558 11.00000 0.05 0.56 Q7 1 0.2580 0.5987 0.1812 11.00000 0.05 0.56 Q8 1 0.5063 0.4563 0.2136 11.00000 0.05 0.54 Q9 1 0.5718 0.4141 0.2773 11.00000 0.05 0.54 Q10 1 0.5091 0.4357 0.3553 11.00000 0.05 0.54 ; _shelx_res_checksum 41209 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Au Au1 0.47494(2) 0.40378(2) 0.28431(2) 0.01328(3) Uani d 1 . . I I1 0.74408(2) 0.33406(2) 0.27831(2) 0.01669(4) Uani d 1 . . S S1 0.22595(7) 0.45551(4) 0.30480(5) 0.01601(12) Uani d 1 . . P P1 0.23375(7) 0.58788(4) 0.27079(5) 0.00961(11) Uani d 1 . . C C1 0.3011(3) 0.61276(16) 0.12332(19) 0.0122(4) Uani d 1 . . C C2 0.0321(3) 0.62736(17) 0.2848(2) 0.0135(5) Uani d 1 . . H H2 0.031468 0.692691 0.269023 0.016 Uiso calc 1 . . C C3 0.3454(3) 0.64662(16) 0.38423(19) 0.0128(4) Uani d 1 . . H H3 0.294656 0.629094 0.456854 0.015 Uiso calc 1 . . C C11 0.2360(3) 0.70321(17) 0.0835(2) 0.0182(5) Uani d 1 . . H H11A 0.274795 0.750085 0.134732 0.027 Uiso calc 1 . . H H11B 0.122165 0.701820 0.084786 0.027 Uiso calc 1 . . H H11C 0.269733 0.715298 0.005688 0.027 Uiso calc 1 . . C C12 0.2443(3) 0.53869(17) 0.0413(2) 0.0193(5) Uani d 1 . . H H12A 0.276013 0.552714 -0.036485 0.029 Uiso calc 1 . . H H12B 0.130673 0.534550 0.043301 0.029 Uiso calc 1 . . H H12C 0.290158 0.481811 0.064982 0.029 Uiso calc 1 . . C C13 0.4788(3) 0.61594(17) 0.1207(2) 0.0172(5) Uani d 1 . . H H13A 0.512145 0.620595 0.041526 0.026 Uiso calc 1 . . H H13B 0.521687 0.561583 0.155051 0.026 Uiso calc 1 . . H H13C 0.516379 0.667689 0.163971 0.026 Uiso calc 1 . . C C21 -0.0821(3) 0.58348(18) 0.1996(2) 0.0195(5) Uani d 1 . . H H21A -0.075648 0.518716 0.207366 0.029 Uiso calc 1 . . H H21B -0.055407 0.600599 0.121796 0.029 Uiso calc 1 . . H H21C -0.188143 0.603120 0.215394 0.029 Uiso calc 1 . . C C22 -0.0260(3) 0.6138(2) 0.4063(2) 0.0237(6) Uani d 1 . . H H22A -0.130189 0.639457 0.412544 0.036 Uiso calc 1 . . H H22B 0.045174 0.643261 0.460694 0.036 Uiso calc 1 . . H H22C -0.029986 0.550107 0.423391 0.036 Uiso calc 1 . . C C31 0.3296(3) 0.74827(17) 0.3790(2) 0.0203(5) Uani d 1 . . H H31A 0.368103 0.774178 0.450869 0.030 Uiso calc 1 . . H H31B 0.220047 0.764234 0.366862 0.030 Uiso calc 1 . . H H31C 0.390690 0.771245 0.315753 0.030 Uiso calc 1 . . C C32 0.5158(3) 0.61983(17) 0.4007(2) 0.0177(5) Uani d 1 . . H H32A 0.578901 0.650631 0.344340 0.027 Uiso calc 1 . . H H32B 0.526015 0.555442 0.390538 0.027 Uiso calc 1 . . H H32C 0.551796 0.636229 0.477722 0.027 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Au1 0.01542(5) 0.00842(5) 0.01597(5) 0.00169(3) 0.00001(3) 0.00117(3) I1 0.01663(8) 0.01449(8) 0.01896(8) 0.00388(6) 0.00109(6) 0.00049(6) S1 0.0147(3) 0.0091(3) 0.0242(3) 0.0000(2) 0.0014(2) 0.0032(2) P1 0.0096(3) 0.0077(3) 0.0114(3) 0.0004(2) -0.0004(2) -0.0001(2) C1 0.0146(11) 0.0111(11) 0.0109(10) 0.0008(9) -0.0001(8) -0.0008(8) C2 0.0105(10) 0.0134(12) 0.0167(11) 0.0029(9) -0.0011(8) -0.0008(9) C3 0.0151(11) 0.0128(12) 0.0105(10) 0.0007(9) -0.0015(8) -0.0014(9) C11 0.0254(13) 0.0139(12) 0.0154(11) 0.0012(10) 0.0005(10) 0.0037(9) C12 0.0265(13) 0.0180(13) 0.0135(11) 0.0000(11) -0.0001(10) -0.0042(10) C13 0.0163(11) 0.0188(13) 0.0167(11) -0.0009(10) 0.0043(9) -0.0001(10) C21 0.0116(11) 0.0202(14) 0.0264(13) -0.0002(10) -0.0029(10) -0.0019(11) C22 0.0154(12) 0.0359(17) 0.0200(13) 0.0064(11) 0.0048(10) 0.0015(11) C31 0.0212(12) 0.0154(13) 0.0238(13) 0.0010(10) -0.0070(10) -0.0039(10) C32 0.0157(11) 0.0174(13) 0.0198(12) -0.0012(10) -0.0056(9) -0.0036(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag S1 Au1 I1 . . 173.747(16) y P1 S1 Au1 . . 106.08(3) y C2 P1 C3 . . 104.91(11) y C2 P1 C1 . . 109.11(10) y C3 P1 C1 . . 113.74(11) y C2 P1 S1 . . 105.26(8) y C3 P1 S1 . . 110.25(8) y C1 P1 S1 . . 112.90(8) y C13 C1 C11 . . 108.9(2) ? C13 C1 C12 . . 108.25(19) ? C11 C1 C12 . . 109.92(19) ? C13 C1 P1 . . 110.67(15) ? C11 C1 P1 . . 109.82(16) ? C12 C1 P1 . . 109.31(16) ? C22 C2 C21 . . 109.3(2) ? C22 C2 P1 . . 111.42(16) ? C21 C2 P1 . . 113.20(17) ? C22 C2 H2 . . 107.6 ? C21 C2 H2 . . 107.6 ? P1 C2 H2 . . 107.6 ? C32 C3 C31 . . 110.5(2) ? C32 C3 P1 . . 116.54(16) ? C31 C3 P1 . . 113.76(16) ? C32 C3 H3 . . 104.9 ? C31 C3 H3 . . 104.9 ? P1 C3 H3 . . 104.9 ? C1 C11 H11A . . 109.5 ? C1 C11 H11B . . 109.5 ? H11A C11 H11B . . 109.5 ? C1 C11 H11C . . 109.5 ? H11A C11 H11C . . 109.5 ? H11B C11 H11C . . 109.5 ? C1 C12 H12A . . 109.5 ? C1 C12 H12B . . 109.5 ? H12A C12 H12B . . 109.5 ? C1 C12 H12C . . 109.5 ? H12A C12 H12C . . 109.5 ? H12B C12 H12C . . 109.5 ? C1 C13 H13A . . 109.5 ? C1 C13 H13B . . 109.5 ? H13A C13 H13B . . 109.5 ? C1 C13 H13C . . 109.5 ? H13A C13 H13C . . 109.5 ? H13B C13 H13C . . 109.5 ? C2 C21 H21A . . 109.5 ? C2 C21 H21B . . 109.5 ? H21A C21 H21B . . 109.5 ? C2 C21 H21C . . 109.5 ? H21A C21 H21C . . 109.5 ? H21B C21 H21C . . 109.5 ? C2 C22 H22A . . 109.5 ? C2 C22 H22B . . 109.5 ? H22A C22 H22B . . 109.5 ? C2 C22 H22C . . 109.5 ? H22A C22 H22C . . 109.5 ? H22B C22 H22C . . 109.5 ? C3 C31 H31A . . 109.5 ? C3 C31 H31B . . 109.5 ? H31A C31 H31B . . 109.5 ? C3 C31 H31C . . 109.5 ? H31A C31 H31C . . 109.5 ? H31B C31 H31C . . 109.5 ? C3 C32 H32A . . 109.5 ? C3 C32 H32B . . 109.5 ? H32A C32 H32B . . 109.5 ? C3 C32 H32C . . 109.5 ? H32A C32 H32C . . 109.5 ? H32B C32 H32C . . 109.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Au1 S1 . 2.2959(6) y Au1 I1 . 2.54374(18) y S1 P1 . 2.0322(8) y P1 C2 . 1.844(2) ? P1 C3 . 1.848(2) ? P1 C1 . 1.872(2) ? C1 C13 . 1.530(3) ? C1 C11 . 1.540(3) ? C1 C12 . 1.544(3) ? C2 C22 . 1.533(3) ? C2 C21 . 1.535(3) ? C2 H2 . 1.0000 ? C3 C32 . 1.529(3) ? C3 C31 . 1.536(3) ? C3 H3 . 1.0000 ? C11 H11A . 0.9800 ? C11 H11B . 0.9800 ? C11 H11C . 0.9800 ? C12 H12A . 0.9800 ? C12 H12B . 0.9800 ? C12 H12C . 0.9800 ? C13 H13A . 0.9800 ? C13 H13B . 0.9800 ? C13 H13C . 0.9800 ? C21 H21A . 0.9800 ? C21 H21B . 0.9800 ? C21 H21C . 0.9800 ? C22 H22A . 0.9800 ? C22 H22B . 0.9800 ? C22 H22C . 0.9800 ? C31 H31A . 0.9800 ? C31 H31B . 0.9800 ? C31 H31C . 0.9800 ? C32 H32A . 0.9800 ? C32 H32B . 0.9800 ? C32 H32C . 0.9800 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C13 H13B Au1 . 0.98 2.85 3.724(3) 149.0 yes C32 H32B Au1 . 0.98 2.63 3.539(3) 154.1 yes C32 H32C Au1 3_666 0.98 2.87 3.709(3) 144.4 yes C3 H3 I1 3_666 1.00 3.18 4.056(2) 147.4 yes C2 H2 I1 2 1.00 3.22 3.973(2) 132.9 yes C2 H2 Au1 2 1.00 3.24 4.237(3) 179.2 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag Au1 S1 P1 C2 . . . . 178.84(8) y Au1 S1 P1 C3 . . . . -68.53(8) y Au1 S1 P1 C1 . . . . 59.91(8) y C2 P1 C1 C13 . . . . 157.71(17) ? C3 P1 C1 C13 . . . . 41.0(2) ? S1 P1 C1 C13 . . . . -85.62(17) ? C2 P1 C1 C11 . . . . 37.51(19) ? C3 P1 C1 C11 . . . . -79.22(18) ? S1 P1 C1 C11 . . . . 154.18(14) ? C2 P1 C1 C12 . . . . -83.15(18) ? C3 P1 C1 C12 . . . . 160.11(16) ? S1 P1 C1 C12 . . . . 33.51(18) ? C3 P1 C2 C22 . . . . -54.3(2) ? C1 P1 C2 C22 . . . . -176.55(18) ? S1 P1 C2 C22 . . . . 62.02(19) ? C3 P1 C2 C21 . . . . -178.02(18) ? C1 P1 C2 C21 . . . . 59.8(2) ? S1 P1 C2 C21 . . . . -61.66(18) ? C2 P1 C3 C32 . . . . 174.22(18) ? C1 P1 C3 C32 . . . . -66.6(2) ? S1 P1 C3 C32 . . . . 61.36(19) ? C2 P1 C3 C31 . . . . -55.3(2) ? C1 P1 C3 C31 . . . . 63.8(2) ? S1 P1 C3 C31 . . . . -168.21(15) ? _cod_database_fobs_code 2022978