#------------------------------------------------------------------------------
#$Date: 2023-12-20 04:03:28 +0100 (Wed, 20 Dec 2023) $
#$Revision: 288434 $
#$URL: svn://www.crystallography.net/cod/cif/2/02/29/2022973.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2022973
loop_
_publ_author_name
'Upmann, Daniel'
'Jones, Peter G.'
'Bockfeld, Dirk'
'T\^arcoveanu, Eliza'
_publ_section_title
;
 Crystal structures of sixteen phosphane chalcogenide complexes of gold(I)
 chloride, bromide and iodide
;
_journal_coeditor_code           YZ2044
_journal_issue                   1
_journal_name_full
'Acta Crystallographica Section E Crystallographic Communications'
_journal_paper_doi               10.1107/S2056989023010459
_journal_volume                  80
_journal_year                    2023
_chemical_formula_iupac          '[Au Br (C12 H27 P S)]'
_chemical_formula_moiety         'C12 H27 Au Br P S'
_chemical_formula_sum            'C12 H27 Au Br P S'
_chemical_formula_weight         511.24
_chemical_name_systematic
;
Bromido(tri-<i>tert</i>-butylphosphane sulfide-\k<i>S</i>)gold
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-2019/3
_cell_angle_alpha                90
_cell_angle_beta                 90.424(6)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   8.3107(6)
_cell_length_b                   13.4820(5)
_cell_length_c                   14.7591(9)
_cell_measurement_reflns_used    7046
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      30.8003
_cell_measurement_theta_min      2.4458
_cell_volume                     1653.64(17)
_computing_cell_refinement
;
CrysAlisPro, Version 1.171.35.21 (Rigaku OD, 2020)
;
_computing_data_collection
;
CrysAlisPro, Version 1.171.35.21 (Rigaku OD, 2020)
;
_computing_data_reduction
;
CrysAlisPro, Version 1.171.35.21 (Rigaku OD, 2020)
;
_computing_molecular_graphics
;
Bruker XP (Bruker, 1998)
;
_computing_publication_material
;
SHELXL-2019/3 (Sheldrick, 2015)
;
_computing_structure_refinement
;
SHELXL-2019/3 (Sheldrick, 2015)
;
_computing_structure_solution
;
SHELXS-97 (Sheldrick, 2008)
;
_diffrn_ambient_temperature      100(2)
_diffrn_detector_area_resol_mean 16.1419
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Oxford Diffraction Xcalibur, Eos'
_diffrn_measurement_method       '\w scan'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0785
_diffrn_reflns_av_unetI/netI     0.0430
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            44298
_diffrn_reflns_theta_full        29.000
_diffrn_reflns_theta_max         29.122
_diffrn_reflns_theta_min         2.451
_diffrn_source                   'fine-focus sealed tube'
_exptl_absorpt_coefficient_mu    11.513
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.44468
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro, Version 1.171.35.21 (Rigaku OD, 2020)
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    2.053
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             976
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.04
_exptl_crystal_size_min          0.04
_refine_diff_density_max         2.677
_refine_diff_density_min         -1.318
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.043
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     155
_refine_ls_number_reflns         4445
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.043
_refine_ls_R_factor_all          0.0486
_refine_ls_R_factor_gt           0.0373
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0357P)^2^+8.6603P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0791
_refine_ls_wR_factor_ref         0.0842
_reflns_number_gt                3863
_reflns_number_total             4445
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            yz2044sup1.cif
_cod_data_source_block           4b
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               2022973
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.277
_shelx_estimated_absorpt_t_max   0.656
_shelx_hkl_file
;
   0   0  -2 226.919 42.0275   7
   0   0  -2 290.145 66.3107   4
   0   0   2 183.947 54.7542  12
   0   0  -2 210.874 53.5259   8
   0   0  -2 195.712 47.4105  12
   0   0   2 342.443 60.6997   8
   0   0  -2 318.969 71.4537  13
   0   0   2 249.930 60.4832   4
   0   0   2 233.242 63.5840   1
   0   0  -3-40.3922 69.2134   8
   0   0  -3 33.5427 45.8935   7
   0   0  -3 10.8421 56.7175  12
   0   0   3 19.0205 90.9476  13
   0   0   3-13.7700 77.0176   4
   0   0  -3 9.34798 62.6708   4
   0   0  -3 3.47741 89.1633   1
   0   0   3 18.0286 75.3152   1
   0   0  -3-10.2204 73.0997  13
   0   0   3-62.1089 58.9179   8
   0   0  -4 7854.97 317.702  12
   0   0  -4 8548.92 429.016   1
   0   0   4 8034.62 368.717   4
   0   0  -4 9294.80 371.049   8
   0   0  -4 8553.92 301.651   7
   0   0   4 8745.97 368.310   8
   0   0  -4 8770.12 389.776   4
   0   0   4 8979.02 423.136   1
   0   0   4 8648.98 405.494  13
   0   0  -4 8118.52 379.636  13
   0   0   5 27.6346 111.290   4
   0   0   5-96.5988 130.843  13
   0   0  -5-20.4532 69.5121  12
   0   0  -5 20.1780 97.1776   3
   0   0  -5 63.6358 54.5278   7
   0   0   5 23.0155 88.9516   8
   0   0  -5-7.06278 127.621   1
   0   0  -5 37.1206 98.4608   8
   0   0  -6 2179.48 216.929   3
   0   0  -6 1962.71 158.668   7
   0   0   6 1768.46 232.134  13
   0   0  -6 1955.68 212.962   8
   0   0   6 1813.90 206.989   4
   0   0  -6 1704.92 163.484  12
   0   0  -6 1858.05 251.182   1
   0   0  -7 165.471 176.280   1
   0   0  -7-27.3685 81.4128  12
   0   0  -7 204.729 134.060   3
   0   0   7 110.623 131.236   4
   0   0   7-34.1609 153.700  13
   0   0  -7 96.8220 70.7120   7
   0   0  -8 71365.7 1788.01  12
   0   0   8 73932.2 2096.51  13
   0   0  -8 76455.3 1941.64   3
   0   0   8 75387.0 1994.70   4
   0   0  -8 73376.0 2146.36   1
   0   0  -9 59.2984 100.857  12
   0   0  -9-98.3463 205.073   1
   0   0   9 260.160 183.028   4
   0   0   9 177.356 185.810  13
   0   0  -9 38.7385 125.866   3
   0   0 -10 2100.04 218.921  12
   0   0 -10 2265.39 375.103   1
   0   0  10 2588.41 374.668  13
   0   0  10 2440.74 318.448   4
   0   0 -10 2130.65 286.860   3
   0   0 -11 13.0748 98.1950  12
   0   0 -11-129.365 158.042   3
   0   0 -11 61.1711 224.817   1
   0   0  11 39.7985 184.651   4
   0   0  11-25.0918 200.558  13
   0   0 -12 1336.91 341.361   1
   0   0 -12 1506.89 204.941  12
   0   0  12 905.053 239.279   4
   0   0 -12 1687.28 283.369   3
   0   0  12 1358.30 328.403  13
   0   0 -13-19.5520 174.123   3
   0   0 -13-12.6966 89.1253  12
   0   0  13-9.88517 205.478   4
   0   0 -13-50.6082 233.698   1
   0   0  13 121.210 228.264  13
   0   0 -14 817.549 307.305   1
   0   0 -14 1061.52 183.822  12
   0   0  14 1183.46 374.874  13
   0   0  14 1046.46 269.686   4
   0   0 -14 974.603 261.381   3
   0   0 -15-252.810 230.416   3
   0   0  15-29.8060 222.247   4
   0   0  15 58.0303 255.903  13
   0   0  16 10808.7 960.082  13
   0   0  16 9880.37 802.674   4
   0   0 -16 9500.10 754.819   3
   0   0  17-121.619 343.679  13
   0   0 -17 230.471 219.168   3
   0   0  17-53.2466 233.315   4
   0   0  18 3226.78 521.428   4
   0   0 -18 2346.35 416.394   3
   0   0  18 2410.85 528.508  13
   0   0 -19-334.796 268.219   3
   0   0  19-211.205 266.229   4
   0   0 -20 339.719 273.040   3
   0   0  20-351.053 361.452  13
   0   0  20-612.590 321.989   4
   0   0 -21 350.063 285.252   3
   0   1  -2 28893.1 663.815   7
   0   1   2 29475.3 729.246   1
   0   1  -2 29172.0 704.264  13
   0  -1   2 26269.9 783.980  10
   0  -1   2 30473.0 758.811   9
   0  -1  -2 29262.8 734.268   1
   0   1  -2 28030.3 772.604  10
   0  -1   2 30500.8 665.103   7
   0   1   2 30965.4 787.013  13
   0   1   2 31812.3 770.794   8
   0  -1   2 29919.6 791.035   1
   0   1  -2 29209.9 734.824   3
   0  -1   2 30647.6 741.802   3
   0   1  -2 28711.5 780.014   1
   0  -1   2 29771.0 756.654  14
   0  -1  -2 29581.4 784.546  13
   0  -1  -2 30155.5 761.920   8
   0   1   2 30227.0 777.053   6
   0   1   2 30469.1 711.700   4
   0  -1   2 29643.5 746.202   5
   0  -1   2 29780.0 712.470  13
   0  -1  -2 29773.4 715.084   4
   0  -1  -3 7754.41 299.823   4
   0  -1  -3 7175.82 321.515   8
   0  -1  -3 6486.32 248.187  15
   0  -1  -3 6831.79 318.857   1
   0   1   3 6990.29 312.653   1
   0   1  -3 6685.01 292.073  10
   0  -1  -3 7418.51 343.954  13
   0  -1   3 7342.02 302.207   3
   0   1   3 6993.87 288.667   4
   0   1   3 6736.33 341.330   6
   0  -1  -3 6574.55 326.619  12
   0   1  -3 7157.90 289.479  13
   0  -1   3 6894.40 298.908  13
   0  -1   3 6629.71 252.244  15
   0   1  -3 6264.78 336.470   1
   0  -1   3 6900.66 317.998   4
   0   1  -3 6691.84 295.801   3
   0  -1   3 7134.32 347.504   1
   0  -1   3 7226.69 232.771   7
   0  -1   3 6503.44 316.587  10
   0   1   3 7390.70 350.164  13
   0   1  -3 6849.21 229.084   7
   0   1   3 7395.92 321.388   8
   0  -1   4 588.483 135.132   4
   0   1  -4 761.508 127.027  13
   0   1   4 862.480 169.696  13
   0   1   4 973.939 132.677   4
   0  -1  -4 1110.99 160.392   8
   0  -1  -4 869.262 168.306  13
   0   1  -4 828.162 87.0349   7
   0  -1   4 633.151 86.1335  12
   0  -1   4 961.326 140.022   3
   0  -1   4 944.913 123.590   8
   0   1   4 918.738 139.097   1
   0  -1   4 902.349 148.887  13
   0  -1   4 853.772 92.0979   7
   0   1  -4 860.113 126.260   3
   0   1  -4 822.975 172.017   1
   0  -1  -4 923.735 156.017   1
   0   1   4 833.898 152.567   6
   0   1  -4 858.459 78.9764  12
   0  -1  -4 1052.76 133.402   4
   0  -1   4 922.754 135.811  10
   0  -1   4 866.402 159.935   1
   0   1  -4 974.176 113.338  10
   0  -1  -4 818.400 149.342  12
   0   1   4 912.500 146.713   8
   0  -1   5 3982.70 290.747   4
   0  -1  -5 3282.01 260.985  12
   0   1  -5 3634.02 313.222   1
   0   1  -5 3666.87 266.354   3
   0   1  -5 3863.10 266.120  13
   0   1   5 4035.92 275.051   4
   0   1   5 3631.84 302.741  13
   0   1  -5 3863.72 192.372  10
   0  -1   5 4096.76 205.985   7
   0   1  -5 3554.92 176.666  12
   0  -1   5 3264.83 277.092  13
   0   1  -5 4142.04 196.664   7
   0  -1  -5 4153.64 285.296   8
   0  -1  -5 3955.89 312.973   1
   0  -1   5 4345.13 267.968   8
   0  -1   5 3798.31 229.051  10
   0   1  -6 30184.9 784.416  12
   0  -1  -6 31133.1 1075.72   1
   0  -1  -6 29900.2 954.236  12
   0   1  -6 32306.5 1112.53   1
   0  -1   6 30801.2 814.097  10
   0   1  -6 33078.7 824.322   7
   0  -1  -6 32958.9 1005.39   8
   0   1   6 31190.5 1074.27  13
   0   1  -6 30397.1 763.892  10
   0   1  -6 32137.1 969.112   3
   0  -1   6 31050.5 831.229   7
   0  -1  -6 31663.2 875.052   7
   0  -1   6 31451.1 1005.34   4
   0   1   6 32109.5 981.979   4
   0  -1   6 30714.1 1021.18  13
   0   1   7 188.745 140.373   4
   0   1  -7 255.568 134.018   3
   0   1  -7 218.093 71.0378   7
   0  -1  -7 79.5440 127.154   8
   0   1  -7 322.385 80.0476  12
   0   1  -7 471.152 189.805   1
   0  -1   7 141.394 151.299   4
   0   1   7 252.070 170.045  13
   0  -1   7 331.795 162.750  13
   0  -1  -7 40.9068 101.018  12
   0  -1   7 81.3596 53.0319  10
   0  -1  -7 93.9295 156.198   1
   0  -1   8 5177.09 226.305  10
   0  -1  -8 5910.07 420.708   8
   0  -1  -8 5313.37 482.198   1
   0   1  -8 5994.93 288.590  12
   0   1  -8 6436.05 525.039   1
   0   1   8 5981.89 412.708   4
   0  -1   8 6593.82 455.359   4
   0  -1  -8 6232.34 386.382  12
   0   1   8 6493.27 496.869  13
   0  -1   8 6272.29 465.159  13
   0   1  -8 6138.27 413.778   3
   0   1  -9 4680.10 382.469   3
   0   1  -9 4483.65 260.957  12
   0  -1  -9 5334.95 402.812   3
   0  -1   9 3631.60 170.088  10
   0  -1   9 3958.76 423.825  13
   0  -1   9 4672.89 422.253   4
   0  -1  -9 4842.14 349.569  12
   0   1  -9 4658.32 485.304   1
   0  -1  -9 4773.67 485.907   1
   0   1   9 5021.46 481.062  13
   0   1   9 4858.68 398.315   4
   0  -1  -9 4896.28 409.169   8
   0  -1 -10 7628.86 459.693  12
   0  -1  10 7664.16 591.732  13
   0  -1 -10 8453.23 561.603   8
   0  -1  10 8003.96 562.362   4
   0  -1 -10 8335.57 649.635   1
   0   1 -10 7002.95 628.191   1
   0   1  10 7551.08 609.395  13
   0   1 -10 7578.07 367.234  12
   0   1 -10 7288.47 509.497   3
   0  -1 -10 8025.29 515.913   3
   0   1  10 7350.38 518.403   4
   0   1  11 1208.82 324.425  13
   0  -1  11 1409.24 307.398  13
   0  -1 -11 1843.23 347.258   1
   0   1 -11 1317.27 322.019   1
   0   1  11 1806.50 297.292   4
   0   1 -11 1660.64 269.435   3
   0  -1 -11 1470.55 223.564  12
   0   1 -11 1752.66 181.995  12
   0  -1 -11 1317.78 251.862   3
   0  -1  11 1707.42 293.953   4
   0   1 -12 763.231 133.963  12
   0  -1  12 579.605 276.506  13
   0  -1 -12 319.655 225.484   1
   0  -1 -12 275.114 173.070   3
   0  -1 -12 600.062 171.652  12
   0   1  12 643.461 300.423  13
   0   1 -12 459.980 202.585   3
   0  -1  12 1019.47 271.819   4
   0   1  12 676.467 239.144   4
   0   1 -12 454.029 253.284   1
   0   1  13 1106.57 250.137   4
   0   1 -13 1350.48 281.466   3
   0  -1  13 1300.14 305.511   4
   0  -1 -13 1674.94 290.684   3
   0   1 -13 1440.42 182.623  12
   0  -1 -13 1699.62 381.479   1
   0  -1  13 1132.95 320.432  13
   0   1 -13 1745.55 379.604   1
   0  -1 -13 1153.55 206.120  12
   0   1  13 1752.53 381.230  13
   0  -1 -14 7411.42 750.719   1
   0  -1  14 8366.14 687.238   4
   0  -1  14 8571.72 786.046  13
   0   1  14 7324.23 630.461   4
   0  -1 -14 7270.69 600.912   3
   0   1  14 8250.73 774.526  13
   0   1 -14 8259.05 641.302   3
   0  -1 -14 8132.78 520.021  12
   0  -1  15-91.2464 288.973  13
   0   1 -15 507.381 226.304   3
   0  -1 -15 176.398 204.783   3
   0  -1  15 844.102 285.416   4
   0   1  15 297.755 206.358   4
   0  -1 -15 598.064 278.971   1
   0   1  15 627.500 331.850  13
   0   1 -16 4498.90 529.947   3
   0  -1  16 5157.06 590.524   4
   0  -1 -16 4699.53 531.124   3
   0   1  16 5002.86 690.044  13
   0   1  16 3823.98 499.880   4
   0  -1  16 4802.69 652.649  13
   0   1  17 2562.06 453.940   4
   0  -1  17 2255.35 466.915   4
   0   1  17 2393.08 507.187  13
   0   1 -17 1976.07 392.229   3
   0  -1 -17 2622.53 435.064   3
   0  -1  17 2141.19 478.460  13
   0  -1 -18 711.212 280.546   3
   0  -1  18 392.721 347.135  13
   0   1  18-196.508 321.102  13
   0  -1  18 522.235 292.595   4
   0   1  18 535.763 296.522   4
   0   1 -18 974.018 314.001   3
   0   1  19 48.5004 257.038   4
   0  -1  19 471.943 372.257  13
   0  -1 -19 73.8118 208.339   3
   0  -1  19-187.180 246.964   4
   0   1 -19 359.538 264.285   3
   0   1  19 273.274 364.605  13
   0  -1  20 91.0827 361.899  13
   0   1  20 542.736 325.242   4
   0  -1  20 472.885 297.888   4
   0  -1 -20-98.6590 260.947   3
   0   1 -20 506.425 293.266   3
   0   1  20 955.187 477.274  13
   0  -1 -21 439.922 284.185   3
   0  -2   0 15577.7 385.311  11
   0   2   0 15393.9 432.135   8
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   1   8   8 1421.49 340.887   2
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   1   8   8 1018.37 209.094  10
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   1   8  10 7672.65 721.719   2
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   1  -8  11 503.519 184.194   7
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   1   8  11 427.198 257.670   2
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   1  -8  11 111.409 208.032  11
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   1  -8  11 874.251 224.569  15
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  -1  -8 -11 94.5265 234.570  12
   1   8  11 437.993 168.965   4
   1  -8  12 1982.83 401.089  11
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   1   8  12 1974.05 431.368   2
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   1   8  12 1775.63 289.237   4
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   1  -8  12 1686.31 265.743   7
   1  -8  12 1142.02 347.442   4
   1   8  13 2758.20 362.188   4
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   1  -8  13 2759.35 482.355   4
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   1   8  13 2028.24 449.308   2
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   1  -8  13 2576.16 483.796  11
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   1  -8  14 753.719 338.731  11
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   1  -8  14 804.237 338.050   4
   1   8  14 1210.47 396.391   2
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   1   8  14 892.614 230.806   4
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   1  -8  15 955.885 405.790  11
   1   8  15 974.046 260.650   4
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   1  -8  15 1051.88 425.478   4
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   1   8  15 849.344 398.686   2
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   1   9 -15 7140.07 765.617   3
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   1  -9 -14 890.553 293.246   1
   1  -9 -14 881.374 364.752   8
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   1  -9 -13 489.254 229.538  12
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   1   9 -13 911.236 313.249   3
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   1   9 -12 450.655 267.450   3
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   1   9 -11 5655.88 570.272  10
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   1   9 -10 118.238 184.669  10
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   1  -9  -7 15354.6 737.771   1
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   1   9  -6 2766.90 416.728  10
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   1  -9  -5 1717.17 233.849   1
  -1   9   5 1572.85 275.622   5
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   1   9  -4 1727.71 169.994   2
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   1  -9  -4 1970.95 227.495   1
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   1  -9  -4 1500.96 296.978   8
   1   9  -4 1431.14 212.900   5
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   1   9  -4 1522.54 369.829  10
   1   9  -4 1881.99 338.701   9
   1   9  -4 1663.25 324.475  14
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   1   9  -4 1905.44 319.407   3
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   1  -9  -3 12332.2 730.107   8
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   1   9  -3 11891.8 709.611   3
   1   9  -3 10795.9 854.782  10
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   1   9  -3 11493.9 747.818  14
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   1  -9  -3 11977.3 584.175  11
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  -1   9   2 1893.10 390.817  10
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   1   9  -2 1586.88 214.510   5
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   1  -9  -2 2286.23 316.796   8
   1  -9  -2 1880.39 386.851  15
  -1   9   2 1926.38 291.896  14
   1   9  -2 2533.65 445.037  10
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   1   9  -2 1932.14 195.036   2
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   1   9  -2 1762.15 308.678  14
   1   9  -2 1829.19 306.145   9
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   1   9  -1 11793.7 731.037   9
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   1   9  -1 12496.3 898.109  10
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  -1   9   0 1129.30 322.716  10
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   1   9   0 1376.21 188.585   2
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  -1  -9   0 1268.39 138.032  11
  -1   9   0 1325.80 275.385  14
   1   9   0 1113.61 172.012   5
   1  -9   0 1410.45 213.904  11
   1   9   0 1207.79 369.171  10
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  -1   9   0 1260.80 253.229   9
  -1   9   0 1013.18 203.563   5
   1  -9   0 1261.08 368.873  15
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   1  -9   0 1437.11 242.393   8
   1   9   0 1138.22 251.845   9
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  -1   9  -1 9080.67 563.625   5
   1   9   1 9723.38 773.207  10
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   1   9   1 8594.63 600.323   9
   1  -9   1 8560.87 500.697  11
   1   9   1 9235.56 485.368   5
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   1  -9   1 7944.12 749.718  15
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   1   9   1 9370.99 505.211   2
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   1  -9   1 9054.04 462.755  13
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   1  -9   1 8138.07 296.509   6
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  -1   9  -1 8297.51 606.809  14
  -1   9  -2 2606.57 308.386   5
   1  -9   2 2224.12 204.946  13
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   1  -9   2 2380.27 457.704  15
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   1  -9   2 2121.61 274.205   8
   1  -9   2 2424.84 319.384   7
  -1   9  -2 2320.87 120.817   2
   1  -9   2 1884.78 111.212   6
   1   9   2 2355.87 173.175  11
   1   9   2 2342.01 329.222   9
  -1   9  -2 2492.32 450.903  10
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   1   9   2 2803.80 443.658  10
   1   9   2 2716.72 281.932   2
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   1   9   2 2797.27 268.376   5
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  -1  -9  -2 2344.94 265.552   6
   1  -9   2 2419.77 270.837  11
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   1   9   3 7308.57 661.914  10
  -1  -9  -3 6172.44 645.607  12
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   2 -11   4 476.927 173.376   8
   2 -11   4 307.059 190.111  11
   2 -11   4 414.951 257.346  15
   2  11   4 461.276 214.569   9
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   2  11   5 4305.08 529.551  10
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   2 -11   5 4967.23 492.300  11
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   2  11   5 5234.94 412.339   5
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   2 -11   6 5220.49 520.629  11
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   2 -11   6 5275.70 504.827   7
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   2 -11   6 4460.30 578.199  15
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   2  11   6 4587.84 412.628   5
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   2  11   7 2590.82 336.046   5
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   2 -11   7 3337.43 503.594  15
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   2  11   7 2729.82 414.308   2
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   2 -11   7 3131.11 403.977   7
   2 -11   7 2995.36 426.077  11
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   2 -11   8 599.700 226.548   7
   2  11   8 447.880 234.836   2
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   2 -11   8 43.3564 194.930  15
   2  11   8 476.759 189.784   5
   2 -11   8 268.800 227.758  11
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   2  11   9 4250.72 554.859   2
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   2 -11   9 3881.68 520.874  15
   2 -11   9 3627.71 439.221   7
   2 -11   9 5232.63 582.930  11
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   2 -11  10 1456.93 302.674  15
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   2  11  10 1576.64 388.083   2
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   3   1   8 7661.41 598.561   2
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   3   1  17 888.058 393.925   2
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   3   1  18 1845.40 507.895   2
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   3   1  19 498.286 358.069   2
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   3   1  19 403.107 271.273   4
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   3   2 -12 3448.57 386.671   3
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   3   5   5 772.229 75.2744   4
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   3   5   6 1713.41 194.058  11
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   3  -5   6 1690.60 253.331   7
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   3   5   6 1770.47 319.725   2
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   3  -5   7 4809.11 424.728   7
   3   5   7 6291.23 569.989   2
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   3   5   8 16304.2 548.391   4
   3  -5   8 16621.6 595.563   2
   3  -5   8 14884.6 724.414   7
   3   5   8 16689.1 951.785   2
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   3   5   9 3353.76 270.524   4
   3   5   9 3226.56 478.619   2
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   3  -5   9 3502.60 293.392   2
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   3  -5  10 417.546 280.799  11
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   3   5  10 391.859 283.653   2
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   3  -5  11 4490.80 545.975  11
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   3   5  11 4594.06 362.299   4
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   3  -5  12 1611.95 390.839  11
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   3  -5  12 1484.07 250.968   2
   3  -5  12 1950.55 387.228   4
   3   5  12 1977.89 450.478   2
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   3   5  12 2277.90 273.544   4
   3  -5  12 1708.87 316.686   7
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   3  -5  13 160.349 245.716  11
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   3   5  13 344.985 310.907   2
   3  -5  13-310.671 251.454   4
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   3   5  13 50.1648 122.804   4
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   3  -5  14 1690.70 414.331  11
   3  -5  14 677.570 266.644   7
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   3   5  14 1492.55 458.915   2
   3  -5  14 1608.01 365.097   4
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   3   5  14 1473.77 262.240   4
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   3  -5  15 1502.51 417.093  11
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   3   5  15 1799.01 487.633   2
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   3  -5  16 4105.13 641.824  11
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   3  -5  16 3667.72 472.722   7
   3   5  16 4366.30 726.971   2
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   3  -5  17 91.3627 263.379  11
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   3   6 -19 232.164 245.337   3
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   3   6 -12 2375.46 426.689   1
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   3  -6 -12 2030.61 380.957   1
   3   6 -12 1864.09 357.818   3
   3   6 -11 67.7531 212.025   1
   3  -6 -11 46.4309 178.819   1
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   3  -6 -10 6647.04 598.299   1
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   3   6 -10 5468.02 571.592   1
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   3   6 -10 6669.64 593.027  14
   3   6 -10 6336.95 567.642   3
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   3   6  -9 165.213 202.191   1
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   3   6  -9 409.914 233.231   9
   3  -6  -9-18.0374 227.541   8
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   3   6  -9 190.624 175.968  14
   3   6  -9 643.499 246.364   3
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   3   6  -8 6774.95 557.427   9
   3  -6  -8 5880.05 540.118   8
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   3   6  -8 6213.03 546.686  14
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   3   6  -8 7164.73 569.024   3
   3  -6  -8 7973.86 577.972   1
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   3   6  -7 137.552 169.516   9
   3   6  -7 56.7792 140.799   1
   3  -6  -7-72.1982 148.843   1
   3  -6  -7 171.911 187.925   8
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   3   6  -7-44.4488 184.928  14
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   3   6  -6 22638.1 1030.90  14
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   3   6  -6 22394.6 941.228   1
   3   6  -6 20919.4 970.680   3
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   3   6  -6 21344.5 691.841  12
   3  -6  -6 22398.8 649.318   3
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   3  -6  -5 1877.57 270.320   1
   3   6  -5 1202.54 245.802   9
   3   6  -5 1281.58 222.404   1
   3  -6  -5 1373.29 126.120   3
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   3  -6  -5 967.507 235.541   8
   3  -6  -5 1687.92 273.541  15
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   3   6  -5 1373.08 204.568   2
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   3   6  -5 1403.42 167.275  12
   3   6  -5 1434.47 270.646   3
   3  -6  -4 817.671 100.052   3
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   3   6  -4 1002.36 239.706   9
   3  -6  -4 814.690 203.070  11
   3   6  -4 831.763 164.177   1
   3  -6  -4 767.521 217.700  15
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   3  -6  -4 643.608 183.417   8
   3  -6  -4 874.234 222.964   7
   3   6  -4 857.039 175.768   2
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   3   6  -4 742.591 204.853   3
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  -3   6   4 851.113 184.719  13
  -3   6   3 136.373 158.840   5
   3  -6  -3 20.7884 59.1014   3
   3  -6  -3 193.438 168.055  15
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   3  -6  -3 99.0719 61.7337   9
   3   6  -3 1.74186 150.249   9
   3   6  -3 72.6103 99.4014   1
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   3  -6  -3 52.1754 122.711   8
   3  -6  -3 84.7116 159.878   7
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   3   6  -3-132.993 118.488   2
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   3  -6  -3 38.2647 128.640  11
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   3   6  -2 17692.7 582.078   1
   3   6  -2 15556.4 796.672   9
   3  -6  -2 16490.9 580.925   9
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   3  -6  -2 16998.5 693.626   8
   3   6  -2 17970.4 711.336   2
   3  -6  -2 17254.8 785.095   7
   3  -6  -2 16486.8 799.767  15
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   3  -6  -2 17932.5 545.326   3
   3  -6  -2 16765.4 764.412  11
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   3  -6  -1 230.761 85.7078  13
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   3   6  -1 91.5805 155.003   9
   3  -6  -1 74.8122 65.8942   3
   3  -6  -1 221.083 183.133  15
   3   6  -1 279.990 84.2827   1
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   3  -6  -1 389.076 137.268   8
   3  -6  -1 335.199 170.052   7
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   3   6  -1 177.996 121.798   2
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  -3  -6   1 102.925 47.5925  11
  -3   6   1 262.814 100.379   3
   3  -6  -1 96.0491 136.550  11
  -3   6   0 2696.32 307.614   5
  -3   6   0 3016.72 348.135  10
   3  -6   0 2607.00 342.480  15
   3  -6   0 2439.04 170.454  13
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   3   6   0 2509.62 146.148   1
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   3   7   2 535.223 187.652   2
   3   7   2 130.135 52.0204   5
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   3  -7   2 106.572 143.249  11
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   3  -7   3 1819.27 313.308   7
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   3 -11   1 928.142 289.979   7
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   3 -14  11-399.327 305.748  11
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   4   1   0 1021.07 193.516   2
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   4   1   1 1524.80 198.154  11
   4  -1   1 1283.18 222.477  11
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   4   1   2 11997.0 468.093   4
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   4   1   2 14783.8 669.723   2
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   4   1   2 14888.5 623.765   7
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   4   1   2 11529.1 471.509   5
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   4   1   3 1687.46 234.303   7
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   4  -1   3 1917.37 231.609   2
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   4   1   4 3498.08 351.981   2
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   4   1   4 3335.81 319.971   7
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   4   1   4 2581.39 269.999  11
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   4  -1   6 25313.2 978.072   2
   4   1   6 25120.1 1048.27   2
   4  -1   6 24849.9 966.820   7
   4   1   6 24831.4 975.252   7
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   4  -1   8 943.459 248.058  11
   4   1   8 848.057 232.905  11
   4  -1   8 735.819 206.232   2
   4   1   8 141.961 180.112   2
   4   1   8 725.143 164.800   4
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   4   1   8 512.740 200.776   7
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   4   1   9 2275.70 382.618   2
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   4   1   9 2173.69 280.472   4
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   4   1  10 4961.01 424.897   4
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   4   1  10 5987.75 619.405   2
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   4   1  10 5956.15 580.152  11
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   4   1  11-19.2054 209.055  11
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   4  -1  11-73.0835 184.126   2
   4   1  11 143.188 223.942   2
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   4   1  11 442.319 177.166   4
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   4  -1  12 2489.12 435.101   2
   4   1  12 3720.62 542.093   2
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   4   1  12 2707.11 364.706   4
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   4   1  12 2979.06 478.000  11
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   4   1  13 1211.37 335.055  11
   4  -1  13 1037.91 323.512   2
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   4   1  13 1706.84 432.557   2
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   4   1  13 960.164 230.958   4
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   4  -1  14 5382.84 697.834  11
   4   1  14 6516.94 744.972  11
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   4   1  14 6555.81 755.457   2
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   4   1  14 6005.04 534.739   4
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   4  -1  15 617.239 331.547  11
   4   1  15 130.740 260.175  11
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   4   1  15 287.384 279.043   2
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   4  -1  15 640.227 272.994   4
   4   1  15 137.257 174.729   4
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   4  -1  16 493.442 332.503  11
   4   1  16 743.276 373.824  11
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   4  -1  16 288.255 247.651   2
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   4   1  16 398.517 328.844   2
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   4   1  17 774.257 369.349   2
   4  -1  17 281.640 230.140   4
   4   1  17 1238.34 318.117   4
   4   1  17 1015.38 409.517  11
   4  -1  18 794.024 416.848  11
   4   1  18 833.425 412.245  11
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   4  -1  18 584.220 336.462   2
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   4   1  18 854.880 385.865   2
   4  -1  18 995.219 316.999   4
   4  -1  19-635.181 378.496  11
   4   1  19 474.941 321.259  11
   4   1  19 131.506 283.007   2
   4  -1  19-40.2138 216.054   4
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   4   2 -18 899.722 401.806   1
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   4   2 -17 1027.98 434.019   1
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   4   2 -16 224.965 263.522   1
   4  -2 -16 412.384 281.843   1
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   4   2 -15 2132.79 356.126   3
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   4  -2 -14 559.868 279.057   1
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   4   2 -13 664.495 220.948   3
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   4   2 -13 555.030 277.813   1
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   4   2 -11 7875.22 564.649   3
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   4   2 -11 8057.96 712.468   1
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   4  -2  -8 1645.01 157.834   3
   4   2  -7 8105.29 470.138   9
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   4  -2  -7 7515.53 376.188   7
   4   2  -7 8077.48 473.552  14
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   4  -2  -7 6638.76 278.377   3
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   4  -2  -7 8082.03 580.261   1
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   4   2  -6 1534.48 207.893   9
   4   2  -6 1759.75 269.249   1
   4  -2  -6 1362.03 268.526   1
   4  -2  -6 1721.17 182.633   7
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   4   2  -6 1749.11 229.237   3
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   4   2  -5 6228.95 396.527   9
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   4   2  -5 5336.18 441.016   1
   4   2  -4 11812.3 557.081   9
   4   2  -4 11655.2 636.966   2
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   4  -2  -4 13100.6 676.449   1
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   4   2  -3 17646.8 581.550   7
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   4  -2  -3 18053.1 784.616  11
   4   2  -3 18145.6 741.013   1
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   4  -2  -2 256.919 136.972   2
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   4  -2  -2 460.603 130.615   7
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   4   2  -2 285.972 106.669   7
   4   2  -2 472.396 180.034   2
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   4   2   0 1131.04 120.173   4
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   4   2   0 990.430 151.905  11
   4   2   0 921.045 207.559   2
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   4  -2   1 4630.02 333.550   2
   4   2   1 4377.98 362.918   2
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   4   2   1 4351.13 321.676   7
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   4   2   1 4601.46 290.542  11
   4  -2   1 4415.78 353.730  11
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   4   2   1 4633.23 233.487   5
   4   2   2 785.455 104.220   5
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   4   2   2 989.442 207.866   2
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   4   2   2 865.802 137.591  11
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   4   2   2 694.383 169.184   7
   4  -2   2 898.655 185.816   7
   4   2   2 817.888 94.3085   4
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   4  -2   2 677.176 145.397   2
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   4  -2   2 720.025 180.688  11
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   4   2   3 13828.7 450.355   4
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   4  -2   3 14791.8 637.380   2
   4   2   3 16327.6 744.604   2
   4  -2   3 15792.6 684.501   7
   4   2   3 16149.0 688.498   7
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   4   2   3 15988.3 596.645  11
   4  -2   3 16361.7 721.305  11
   4   2   3 13894.7 526.920   5
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   4  -2   4 13994.1 622.228   2
   4   2   4 14734.5 732.821   2
   4  -2   4 13606.5 668.130   7
   4   2   4 14845.4 679.973   7
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   4   2   4 13775.6 574.808  11
   4  -2   4 14643.6 698.562  11
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   4   2   5 9490.59 486.937  11
   4  -2   5 10076.9 528.432   2
   4   2   5 10114.5 623.539   2
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   4   3   4 2696.68 141.960   4
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   4   3   5 8304.70 439.886  11
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   4   3   6 639.895 103.813   4
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   4  -3   6 489.853 211.001  11
   4  -3   6 679.311 165.010   2
   4   3   6 598.707 157.143  11
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   4   3   7 6399.56 328.125   4
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   4  -3   7 6862.83 448.211   2
   4   3   7 6968.26 586.803   2
   4  -3   7 7173.54 514.905   7
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   4  -3   7 6339.71 547.258  11
   4   3   7 6440.49 438.713  11
   4  -3   8 2575.38 387.589  11
   4   3   8 2284.14 298.125  11
   4  -3   8 2377.04 287.370   2
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   4   3   8 2394.23 381.734   2
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   4   3   8 2480.20 221.150   4
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   4  -3   8 2302.58 310.155   7
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   4   3   9 8814.58 459.714   4
   4  -3   9 8601.75 558.677   2
   4   3   9 9648.38 760.278   2
   4  -3   9 8800.99 609.560   7
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   4  -3   9 8814.16 713.966  11
   4   3   9 8027.80 602.959  11
   4  -3  10 1121.56 314.359  11
   4   3  10 554.321 241.034  11
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   4  -3  10 725.944 206.278   2
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   4   3  10 737.838 314.223   2
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   4   3  10 734.385 170.950   4
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   4   3  11 586.034 232.059  11
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   4  -3  11 713.926 212.614   2
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   4   3  11 804.473 318.449   2
   4  -3  11 1195.30 291.064   4
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   4   3  11 695.219 164.507   4
   4  -3  11 798.058 287.352  11
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   4  -3  11 364.578 196.379   7
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   4  -3  12 739.400 294.176  11
   4   3  12 959.748 302.477  11
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   4  -3  12 608.603 224.516   2
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   4   3  12 949.580 372.278   2
   4  -3  12 926.097 281.286   4
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   4   3  12 1012.10 203.336   4
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   4  -3  13 4727.69 641.198  11
   4   3  13 6341.02 687.029  11
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   4   3  13 6981.48 807.950   2
   4   3  13 5517.33 446.709   4
   4  -3  13 5626.27 600.614   4
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   4  -3  13 4429.70 510.302   7
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   4  -3  14 349.511 277.859  11
   4   3  14 634.833 319.414  11
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   4   3  14 553.406 331.006   2
   4  -3  14 369.072 244.817   4
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   4   3  14 36.4049 160.649   4
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   4  -3  15 1301.90 416.428  11
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   4  -3  15 1504.07 327.520   2
   4   3  15 931.362 345.646   2
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   4  -3  15 762.065 333.419   7
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   4  -3  16 868.213 405.068  11
   4   3  16 896.910 354.384  11
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   4  -3  17 2448.00 560.585  11
   4   3  17 2946.85 571.783  11
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   4   3  17 3602.96 704.906   2
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   4  -3  17 3455.21 537.207   4
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   4  -3  18 207.271 280.034  11
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   4   3  18 69.7956 291.877   2
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   4  -4 -18 930.291 380.630   1
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   4   4 -17 891.531 434.322   1
   4  -4 -17 627.487 358.306   1
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   4   4 -16 418.109 211.108   3
   4   4 -16-116.323 267.066   1
   4  -4 -16 593.395 329.621   1
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   4   4 -15 8287.79 699.727   3
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   4   4 -15 8616.92 864.252   1
   4  -4 -15 8022.47 816.679   1
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   4   4 -14 763.905 336.053   1
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   4  -4 -14 508.219 306.487   1
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   4   4 -14 427.229 221.506   3
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   4  -4 -13 183.659 214.230   1
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   4   4 -12 636.103 282.808   1
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   4   4 -12 581.937 228.557   3
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   4  -4 -11 3884.99 503.066   1
   4   4 -11 3422.32 478.551   1
   4  -4 -11 3408.00 339.311   7
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   4   4 -11 3386.43 412.421   3
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   4   4 -10 2915.90 362.061   9
   4  -4 -10 2577.41 419.124   1
   4   4 -10 3072.76 460.629   1
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   4   4 -10 2710.70 351.634  14
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   4   4 -10 2775.81 362.421   3
   4  -4  -9 1155.30 132.713   3
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   4   4  -9 1826.69 331.620   1
   4   4  -9 1923.73 335.740   3
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   4   4  -8 532.424 215.479  14
   4   4  -8 1356.73 274.049   9
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   4  -4  -8 904.162 203.002   7
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   4   4  -8 870.055 248.107   1
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   4   4  -8 1069.08 254.666   3
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   4   4  -7 25111.3 1019.83   9
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   4  -4  -7 23891.9 917.747   7
   4   4  -7 25231.4 1024.28  14
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   4   4  -7 23857.6 1048.68   1
   4   4  -7 24137.8 1010.34   3
   4  -4  -7 26184.1 1118.88   1
   4  -4  -6 423.547 229.381   1
   4   4  -6 367.755 176.513   9
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   4  -4  -6 448.006 171.738   7
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   4   4  -6 438.547 182.547   3
   4   4  -6 528.051 193.469   1
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   4   4  -5 737.712 205.289   1
   4  -4  -5 852.807 247.917   1
   4   4  -5 802.957 207.488   9
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   4  -4  -5 669.400 173.343   7
   4   4  -5 619.104 184.556   2
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   4  -4  -4 1267.07 92.9103   9
   4   4  -4 2132.59 273.173   9
   4   4  -4 1687.23 234.045   1
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   4   4  -4 1627.06 253.060   2
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   4  -4  -4 1256.06 91.8675  14
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   4  -4  -3 4259.93 404.605  11
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   4   4  -1 11654.8 424.586   4
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   4  -4  -1 11147.9 640.739  11
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   4   4  -1 11332.5 509.873   1
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   4   4   0 2430.18 293.770   2
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   4  -4   0 2352.79 309.252  11
   4   4   0 2668.46 220.989   1
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   4  -4   1 27792.8 1033.74  11
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   4  -4   1 26934.1 888.821   2
   4   4   1 25851.3 1001.92   2
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   4   4   1 27256.1 753.532  11
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   4  -4   2 2315.30 229.172   2
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   4   4   2 1872.26 159.962  11
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   4  -4   2 1888.47 274.441   7
   4  -4   2 1500.28 273.179  11
   4   4   2 2178.80 298.184   2
   4   4   3 4798.57 247.363   5
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   4  -4   3 5366.00 334.195   2
   4   4   3 5455.13 455.938   2
   4  -4   3 4779.85 392.725   7
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   4   4   3 5380.48 278.451  11
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   4  -4   3 5235.93 436.763  11
   4   4   4 1353.63 257.448   2
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   4   4   4 1072.22 140.981   5
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   4  -4   4 1476.42 244.661   7
   4  -4   4 1062.66 164.028   2
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   4   4   4 1089.91 146.041  11
   4  -4   4 631.601 202.609  11
   4   4   5 1879.12 297.412   2
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   4  -4   5 1782.32 271.162   7
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   4  -4   5 1967.25 210.512   2
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   4   4   5 1744.49 176.810  11
   4  -4   5 1879.17 298.895  11
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   4   4   6 1698.89 316.220   2
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   4   4   6 1631.38 120.462   4
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   4  -4   6 1661.99 201.367   2
   4  -4   6 2025.23 289.337   7
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   4   4   6 1854.27 209.607  11
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   4  -4   6 1498.15 286.124  11
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  -4   4  -7 16556.6 750.550  12
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   4   4   7 16223.2 528.039   4
   4  -4   7 16356.1 696.110   2
   4   4   7 17530.2 954.769   2
   4  -4   7 15623.3 800.357   7
  -4   4  -7 15923.8 822.022   3
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   4   4   7 16095.0 706.168  11
   4  -4   7 16122.0 921.348  11
   4   4   8 2556.69 289.604  11
   4  -4   8 2294.94 261.635   2
  -4   4  -8 2370.36 341.834  10
  -4   4  -8 2689.16 354.741   3
   4   4   8 2471.95 405.223   2
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   4   4   8 2385.03 201.979   4
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   4  -4   8 2084.62 318.810   7
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   4  -4   8 2514.83 392.824  11
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   4   4   9 7116.33 381.737   4
   4  -4   9 7298.60 478.311   2
   4   4   9 8062.17 719.823   2
   4  -4   9 6223.50 518.583   7
  -4   4  -9 6962.58 470.968  12
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  -4   4  -9 7384.29 582.898   3
   4  -4   9 7713.98 667.832  11
   4   4   9 6646.00 511.274  11
   4  -4  10 2222.23 407.603  11
   4   4  10 2600.65 364.402  11
   4  -4  10 2562.43 301.605   2
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   4   4  10 2562.61 437.588   2
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   4   4  10 2517.46 245.949   4
   4  -4  10 2512.25 346.307   7
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   4  -4  11 4578.16 564.857  11
   4   4  11 4243.11 497.965  11
  -4   4 -11 4627.86 461.951  10
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  -4   4 -11 3742.64 467.085   3
   4   4  11 5153.97 642.640   2
   4   4  11 3856.80 324.736   4
  -4  -4 -11 4603.39 494.953   8
   4  -4  11 4509.10 411.839   2
  -4   4 -11 3844.84 365.676  12
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   4  -4  11 3313.85 439.440   7
   4  -4  12 507.124 261.547  11
   4   4  12-157.230 211.451  11
  -4   4 -12 388.470 191.606  10
   4  -4  12 251.044 149.506   2
  -4   4 -12 329.878 242.460   3
   4  -4  12 458.290 258.452   4
   4   4  12 365.507 320.225   2
  -4  -4 -12 604.670 239.351   8
   4   4  12 347.570 142.673   4
   4  -4  12 431.734 221.018   7
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   4  -6  -3 388.419 86.1246   9
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   4   6   0 27833.1 1050.68   2
   4  -6   0 28742.0 1084.47   7
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   4  -6   0 27798.0 1087.62  11
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   4  -6   2 885.187 260.500   7
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   4   6   2 661.485 96.4522   1
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   4  -6   2 796.670 222.347  11
   4   6   3 1097.90 100.606   5
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   4   6   4 5440.91 305.260   5
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   4   6   4 7856.82 591.594   2
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   4   6   4 7378.16 328.038   1
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   4  -6   4 6954.36 550.489  11
   4   6   5 507.633 207.788   2
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   4   6   5 522.049 107.754   1
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   4  -6   5 748.260 221.252   7
   4  -6   5 572.602 114.492   2
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   4   6   5 278.140 74.6261  11
   4  -6   5 567.854 222.365  11
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   4   6   6 1523.67 334.709   2
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   4   6   6 1571.22 161.296  11
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   4  -6   7 1170.80 279.518   7
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   4  -6   7 1059.42 287.618  11
   4   6   7 918.761 150.612  11
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   4   6   8 15151.5 975.551   2
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   4  -6   8 14161.5 929.637  11
   4   6   8 13544.0 623.113  11
   4   6   9 769.691 181.944  11
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   4   6   9 488.156 280.441   2
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   4  -6  10 1565.49 381.299  11
   4   6  10 1818.15 283.175  11
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   4   6  10 1877.13 415.762   2
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   4  -6  10 1370.85 302.959   7
   4  -6  11 1074.62 333.801  11
   4   6  11 799.259 219.542  11
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   4   6  11 317.604 264.059   2
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   4  -6  11 1008.08 267.026   7
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   4  -6  12 2145.13 436.131  11
   4   6  12 2230.75 367.460  11
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   4   6  12 2042.60 485.130   2
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   4  -6  12 2270.66 380.274   7
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   4  -6  13 192.801 278.441  11
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   4  -6  14 1423.53 393.986  11
   4  -6  14 590.748 277.172   7
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   4  -6  15 2.29105 307.794  11
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   4   6  15 105.830 309.228   2
   4  -6  15 124.282 267.571   4
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   4  -6  15 385.171 269.447   7
   4  -6  16 3623.02 631.394  11
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   4   6  16 4212.74 716.498   2
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   4  -6  16 3762.16 530.687   7
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   4  -6  17-217.555 302.376  11
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   4   7 -18-123.859 231.366   3
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   4  -7 -17 155.714 309.693   1
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   4   7 -17 456.042 254.875   3
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   4   7 -16 2923.24 550.712   1
   4  -7 -16 3098.86 540.093   1
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   4  -7 -16 2948.86 515.798  12
   4   7 -16 2645.61 482.640   3
   4   7 -15-409.844 297.621   1
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   4  -7 -15-120.480 253.155   1
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   4   7 -15-398.706 246.962   3
   4   7 -14 4290.07 597.109   1
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   4  -7 -14 4642.30 595.203   1
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   4   7 -14 4496.72 560.672   3
   4   7 -13 1218.61 349.720   1
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   4   7 -13 299.996 210.893   3
   4  -7 -13 500.381 263.570   1
   4   7 -12 2180.59 426.676   1
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   4  -7 -12 1296.21 365.127   1
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   4   7 -12 1560.77 360.344   3
   4   7 -11 293.950 230.087  14
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   4   7 -11 554.784 261.571   1
   4   7 -11 233.364 213.163   9
   4  -7 -11 529.212 246.459   1
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   4   7 -11 53.8617 198.970   3
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   4   7 -10 2763.70 426.513   1
   4   7 -10 2673.45 397.532   9
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   4  -7 -10 2993.91 444.009   1
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   4   7 -10 3767.65 463.686  14
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   4   7 -10 2821.62 416.299   3
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   4   7  -9 503.736 253.192   9
   4  -7  -9 304.922 208.083   7
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   4   7  -9 396.039 221.102  14
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   4  -7  -9 394.978 219.304   1
   4   7  -9 474.508 229.361   3
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   4   7  -8 4357.22 475.324   9
   4   7  -8 4344.97 445.996   1
   4  -7  -8 4243.59 469.319   1
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   4   7  -8 4510.27 493.381  14
   4  -7  -8 4294.54 464.527   7
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   4   7  -8 4266.19 480.595   3
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   4   7  -7 77.2253 186.190   9
   4   7  -7 95.3159 146.526   1
   4  -7  -7 170.451 206.726   1
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   4  -7  -7 150.333 180.142   7
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   4   7  -7-18.5259 163.501  14
   4   7  -7 190.333 189.380   3
  -4   7   6 16980.3 901.244  10
   4   7  -6 16715.9 923.467   9
  -4  -7   6 15850.1 825.449   4
   4   7  -6 15854.4 810.124   2
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   4  -8   0 13418.6 768.910  11
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   4  -8   1 2430.73 357.129  11
   4   8   1 2711.88 332.715   2
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   4  -9   8 172.394 198.636   7
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   4  -9   8 732.772 290.951  11
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   4  -9   9 4410.26 492.121   7
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   4  -9   9 4662.41 605.169  11
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   4  -9  10 379.540 251.558  11
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   4   9  11 3705.85 559.427   2
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   4  -9  11 4316.56 601.018  11
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   4  -9  12 179.519 217.535   7
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   4  -9  12 403.975 281.051  11
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   4   9  13 4977.82 715.670   2
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   4  -9  13 4013.16 524.922   7
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   4  -9  13 4478.40 651.516  11
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   4  -9  14 267.126 221.840   7
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   4  -9  14 717.590 377.480  11
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   5   1   4 29905.7 1112.40   7
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   5  -1   7 3090.93 374.500   2
   5   1   7 3256.27 409.608   2
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   5   1   7 3180.94 364.252  11
   5  -1   8 1705.81 284.621   2
   5   1   8 1200.67 259.009   2
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   5   1   8 1415.17 274.411   7
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   5   1   8 1695.35 289.401  11
   5  -1   9 193.690 165.358   2
   5   1   9 112.936 193.603   2
   5   1   9 411.199 151.513   4
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   5  -1   9-46.9402 166.243   7
   5   1   9 67.8794 221.458   7
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   5   1  10 1325.74 321.376  11
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   5   1  10 839.191 201.513   4
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   5  -1  11 2054.77 422.650  11
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   5   1  11 1505.41 362.632   2
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   5  -1  11 1664.35 303.653   4
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   5   1  11 1527.74 259.297   4
   5  -1  11 1963.90 346.596   7
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   5  -1  12 9000.74 676.988   4
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   5   1  12 10205.3 636.144   4
   5  -1  12 10183.3 783.866   2
   5   1  12 10791.0 888.589   2
   5  -1  12 8998.23 726.658   7
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   5  -1  12 9229.22 828.097  11
   5   1  12 8994.59 791.655  11
   5  -1  13-138.811 253.920  11
   5   1  13 506.348 295.342  11
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   5   1  13-229.269 253.311   2
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   5  -1  13 73.2006 187.247   4
   5   1  13 119.611 147.377   4
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   5  -1  14 2377.69 528.987  11
   5   1  14 1332.30 406.156  11
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   5  -1  14 2039.44 396.164   2
   5   1  14 1874.25 448.936   2
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   5  -1  14 2150.90 367.834   4
   5   1  14 1919.70 331.312   4
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   5  -1  15 325.716 268.027  11
   5   1  15 235.531 254.164  11
   5  -1  15 764.229 314.001   2
   5   1  15 599.089 302.726   2
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   5  -1  15 936.776 305.825   4
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   5  -1  16 185.632 313.238  11
   5   1  16 304.212 288.377  11
   5  -1  16 509.731 290.306   2
   5   1  16-427.558 333.001   2
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   5  -1  16 229.110 209.967   4
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   5  -1  17 302.023 362.743  11
   5   1  17 167.482 325.938  11
   5  -1  17-56.5568 230.581   2
   5   1  17 114.016 252.308   2
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   5  -1  18 410.796 349.543  11
   5   1  18 438.958 339.431  11
   5   1  18 575.586 341.883   2
   5   1  19 220.568 330.114  11
   5   1  19-312.592 298.655   2
   5   2 -17 1170.67 440.529   1
   5  -2 -17 1276.90 413.870   1
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   5   2 -16 271.690 289.310   1
   5  -2 -16 28.5779 243.855   1
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   5   2 -15 364.324 311.020   1
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   5  -2 -15 280.871 272.252   1
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   5   2 -14 334.241 248.815   1
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   5  -2 -14 475.933 298.510   1
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   5   2 -13 5523.71 638.037   1
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   5   5   8 17820.0 1089.96   2
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   5   6   3 151.234 57.0202  11
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   5   7 -15-56.7569 219.144   1
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   5   7 -15 196.094 198.983   3
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   5  -7 -13 409.917 289.471   1
   5   7 -13 786.202 310.453   1
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   6   1  11 539.182 249.496  11
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   6   1  12 1630.34 400.112  11
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   6   4   4 43.4774 93.3218  11
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   6   4   5 2584.51 264.629  11
   6  -4   5 2617.00 371.290  11
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   6   6 -11 485.825 270.956   1
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   6   6  12 1816.91 472.524   2
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   6  -6  12 1892.25 449.461  11
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   6   7 -15 486.257 271.748   1
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   6   7 -14 1528.37 387.334   1
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   6  -7 -13 1225.98 381.038   1
   6   7 -13 742.851 323.487   1
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   6   7  -8 3518.66 426.471   1
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   6  -7  -7 1282.49 278.887   7
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   6   7  -6 6732.71 629.839   9
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   6   7  -6 5657.51 574.451   2
   6  -7  -6 6957.02 587.515   7
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   6   7  -6 6102.83 521.505   1
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   6  -7  -6 7649.48 692.864   1
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   6   7  -5 1813.93 346.622   9
   6  -7  -5 1772.23 323.824   7
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   6   7  -5 1661.42 274.079   1
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   6  -7  -5 1432.08 366.288  11
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   6  -7  -4 936.114 244.973   7
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   6   7  -4 1147.05 274.566   2
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   6   7  -4 1615.12 241.396   1
   6  -7  -4 1461.47 311.937  11
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   6  -7  -3 809.978 279.260   7
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   6   7  -3 893.413 276.115   2
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   6  -7  -3 735.620 283.979  11
   6   7  -3 1095.31 195.704   1
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   6   7  -2 9977.76 730.185   9
   6   7  -2 8558.20 656.054   2
   6  -7  -2 9218.35 680.576   7
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   6   7  -2 9751.07 528.314   1
   6  -7  -2 11310.3 781.830  11
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   6   7  -1 164.776 98.6894   1
  -6   7   1 145.984 111.684  13
   6  -7  -1 277.063 243.594   7
   6   7  -1-66.8960 180.898   2
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   6  -7  -1-15.3167 187.728  11
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  -6   7   0 2683.56 438.601  10
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   6  -7   0 3223.98 439.097   7
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   7  -1  15 544.363 328.545  11
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   7   2 -13 2870.07 528.187   1
   7  -2 -12 1434.46 389.781   1
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   7   2 -12 782.274 335.527   1
   7  -2 -11 552.309 291.365   1
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   7   2 -11 654.234 298.795   1
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   7   2 -10 926.968 318.908   1
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   7  -2  -9 3628.54 505.667   1
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   7   2  -8 1838.60 356.773   1
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   7   2  -7 464.510 174.867   9
   7  -2  -7 541.629 300.183   1
   7  -2  -7 570.574 145.533   7
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   7   2  -7 223.711 197.557   1
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   7  -2  -6 1702.99 377.862   1
   7   2  -6 1278.61 229.937   9
   7  -2  -6 1471.82 218.468   7
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   7   2  -6 1278.64 278.550   1
   7   2  -5 6024.50 472.079   9
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   7   2  -5 5419.62 529.343   1
   7  -2  -5 6306.46 595.922   1
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   7   2  -4 90.8366 197.838   2
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   7   2  -4 340.037 176.301   1
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   7  -2   4-5.33959 154.634   2
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   7   2   5 1490.31 328.471   7
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   7   2   5 2303.79 425.234   2
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   7   2   6 831.958 291.851   7
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   7  -2   6 673.399 243.575   2
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   7   2   6 885.437 292.620   2
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   7   2   7 1388.55 326.664   2
   7   2   7 1785.65 293.366  11
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   7  -2   8 647.571 268.718   7
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   7  -2   8 964.366 261.880   2
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   7   2   9 3437.56 524.419   2
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   7  -2   9 2816.46 449.731   7
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   7  -2   9 3690.61 464.472   2
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   7   2   9 2763.32 386.994  11
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   7  -2  11 1245.53 308.534   2
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   7   2  11 1075.60 303.843  11
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   7   3 -14 318.239 267.949   1
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   7  -3 -13 351.221 307.421   1
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   7  -3  -7 6390.66 628.030   1
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   7   3  -5 1330.94 309.558   1
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   7   3  -4 322.306 157.498   1
   7   3  -4 965.020 302.904   2
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   7  -3  -3 9001.40 704.175  11
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   7   3   1 4480.31 499.011   2
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   7   3   1 4788.07 405.673  11
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   7  -3   1 4186.21 472.525  11
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   7  -3   2 1480.61 288.564   2
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   7   3   2 1671.36 333.109   2
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   7   3   2 1499.33 246.858  11
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   7   3   3 4065.04 506.863   2
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   7   3   3 4098.54 392.695  11
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   7  -3   4 416.091 227.985   7
   7  -3   4 241.160 169.642   2
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   7   3   4 196.614 195.479   2
   7   3   4 152.362 141.268  11
   7  -3   4 246.584 207.019  11
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   7  -3   5 6626.36 540.273   2
   7   3   5 6137.89 599.375   2
   7  -3   5 5561.27 534.552   7
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   7   3   5 6096.96 462.874  11
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   7  -3   5 6881.00 598.084  11
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   7  -3   6 980.905 283.738   7
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   7  -3   6 825.324 247.357   2
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   7  -3   6 921.349 300.965  11
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   7  -3   7 2682.26 431.872   7
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   7  -3   7 3939.41 441.860   2
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   7   3   7 3010.96 352.496  11
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   7   3   7 3247.28 494.550   2
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   7  -3   8 128.646 145.517   2
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   7   3   8 371.845 176.419  11
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   7   3   9 1975.76 403.746   2
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   7  -3   9 1601.77 310.495   2
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   7  -4  -9 10421.9 849.425   1
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   7  -4   5 2620.80 412.383   7
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   7  -4   6 946.184 270.350   7
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   7   4   6 1959.50 265.509  11
   7   4   6 1917.99 382.360   2
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   7   4   7 4896.46 417.525  11
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   7  -4   7 5265.95 576.317  11
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   7   4   8 719.457 326.076   2
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   7  -4   8 735.430 293.053  11
   7   4   9 4199.93 618.965   2
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   7  -4   9 3681.76 509.566   7
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   7  -4   9 3585.44 422.168   2
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   7  -4   9 4411.46 589.763  11
   7   4  10 750.796 324.070   2
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   7  -4  10 61.3951 247.681   7
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   7  -4  10 182.337 149.674   2
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   7  -4  10 134.804 261.042  11
   7   4  11 933.694 372.908   2
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   7  -4  11 656.817 283.533   7
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   7  -4  11 1304.94 386.058  11
   7   4  12 272.087 281.533   2
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   7  -4  12 136.122 279.504   7
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   7  -4  12 188.637 288.236  11
   7   4  13 2306.39 542.441   2
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   7  -4  15 391.706 295.058   7
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   7  -4  15 256.089 350.848  11
   7   5 -15 969.874 378.396   1
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   7  -5 -14 327.375 330.494   1
   7   5 -14 166.583 228.091   1
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   7  -5 -13-20.5179 238.512   1
   7   5 -13 27.7438 226.312   1
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   7  -5 -12 360.623 294.072   1
   7   5 -12 370.931 264.930   1
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   7   5 -11 2340.80 444.322   1
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   7   5 -10 2431.76 427.667   1
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   7  -5 -10 3602.78 532.760   1
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   7  -5  -9 83.1018 217.676   1
   7   5  -9 299.077 169.126   9
   7   5  -9-97.0167 143.458  14
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   7   5  -9-164.977 182.849   1
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   7   5  -8 6637.69 587.225   9
   7  -5  -8 6238.82 488.748   7
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   7   5  -8 5257.67 567.412   1
   7  -5  -8 5912.67 670.937   1
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   7   5  -7 1483.19 316.798   1
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   7  -5  -7 2275.20 427.481   1
   7   5  -7 2072.98 352.126   9
   7  -5  -7 2135.34 294.698   7
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   7   5  -5 688.444 222.431   9
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   7   5  -5 544.881 238.097   2
   7  -5  -5 601.655 216.113   7
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   7   5  -4 999.409 266.151   9
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   7   5   2 1827.79 372.532   2
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   7   5   3 1174.12 312.450   2
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   7   5   3 1293.04 229.733  11
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   7  -5   4 1310.54 294.196   7
   7  -5   4 1516.09 254.610   2
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   7   5   4 1454.88 338.504   2
   7  -5   4 1948.21 370.890  11
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   7  -5   5 2452.08 389.552   7
   7  -5   5 3158.27 358.160   2
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   7   5   5 3537.65 470.760   2
   7  -5   5 3035.82 434.944  11
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   7  -5   6 514.628 240.347   7
   7  -5   6 739.422 212.460   2
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   7   5   6 634.175 254.365   2
   7  -5   6 869.591 286.290  11
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   7  -5   7 1807.52 352.042   7
   7  -5   7 1870.78 285.241   2
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   7   5   7 1888.85 405.824   2
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   7   5   8 7526.02 769.118   2
   7  -5   8 6534.25 638.871   7
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   7  -5   8 6981.31 698.418  11
   7   5   9 886.428 333.882   2
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   7  -5   9 1252.66 386.878  11
   7   5  10 455.086 317.053   2
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   7  -5  10 752.393 369.410  11
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   7  -5  11 139.094 265.505  11
   7   5  12 718.802 378.505   2
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   7  -5  12-171.150 249.556   7
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   7  -5  12 539.956 315.678  11
   7   5  13 1055.71 463.225   2
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   7  -5  13 400.540 331.017  11
   7   5  14 404.921 348.541   2
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   7   6 -15-415.163 287.715   1
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   7  -6 -14 2044.86 497.281   1
   7   6 -14 1997.99 463.776   1
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   7   6 -13 102.393 230.220   1
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   7   6 -11 664.596 265.410   1
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   7   6  -5 79.5863 144.009   1
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   7  -6  -4 3029.96 438.769  11
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   7   6  -3 374.925 160.910   1
   7  -6  -3 293.953 190.618   7
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   7   6  -2 8065.87 534.553   1
   7  -6  -2 8434.69 710.663  11
   7   6  -1 587.905 174.967   1
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   7   6   0 1904.85 250.436   1
   7  -6   0 1951.85 339.613   7
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   7  -6   0 1841.45 367.132  11
   7   6   1 730.751 164.226   1
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   7  -6   1 896.715 268.838   7
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   7   6   1 902.650 259.825   2
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   7  -6   1 555.561 228.632  11
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   7   6   2 5194.50 581.659   2
   7  -6   2 4083.93 494.979   7
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   7  -6   2 5808.00 593.150  11
   7   6   2 5205.66 406.200   1
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  -7   6  -3 113.325 237.290  10
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   7  -6   3 197.658 137.756   2
   7  -6   3 437.657 257.251   7
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  -7  -6  -3 252.711 224.375   6
   7   6   3 263.770 233.288   2
  -7   6  -3 3.14077 122.882   6
   7  -6   3 121.095 182.646  11
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   7  -6   4 1077.60 226.560   2
   7  -6   4 1271.25 310.328   7
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   7   6   4 854.480 290.338   2
   7  -6   4 1400.92 343.684  11
  -7   6  -5 88.1081 209.230  10
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  -7   6  -5 272.681 218.562   5
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   7  -6   5 282.028 137.801   2
   7  -6   5 598.602 268.876   7
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   7   6   5 221.005 224.678   2
   7  -6   5 152.034 240.324  11
  -7   6  -6 9984.85 784.264   5
  -7   6  -6 9751.33 826.557  10
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   7  -6   6 8930.96 580.519   2
   7   6   6 9694.53 810.577   2
   7  -6   6 8578.93 710.791   7
  -7  -6  -6 8416.33 742.662  12
  -7  -6  -6 9865.33 823.069   6
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   7  -6   6 9390.79 782.546  11
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  -7  -6  -7 78.1452 195.829   8
   7  -6   7 672.343 269.833   7
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   7  -6   7 581.277 276.166  11
   7   6   7 404.629 281.449   2
   7   6   8 891.815 377.328   2
  -7   6  -8 526.470 307.402  10
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  -7   6  -8 1090.01 335.486   5
  -7  -6  -8 855.216 304.593   8
   7  -6   8 592.781 280.645   7
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   7  -6   9 255.242 234.400   7
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   7   8   2 2035.39 399.940   2
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   7  -8   3 3118.07 468.519   7
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   7  10   5 3678.86 568.999   2
   7 -10   5 5119.17 650.239  11
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   7 -10   6 23.4910 256.861   7
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   7 -10   6-243.413 274.455  11
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   7 -10   7 1141.16 346.670   7
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   8   1  -8 3238.13 484.780   1
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   8   1  -3 387.002 227.738   1
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   8   1  -3 820.628 289.861   2
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   8   1  -3 529.967 165.185   7
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   8   1   1 843.348 274.366   2
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   8   1   1 321.207 173.157  11
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   8  -1   2 7277.60 631.051   2
   8   1   2 8602.44 703.396   2
   8  -1   2 6959.34 591.093   7
   8   1   2 7441.11 604.401   7
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   8   1   2 8369.06 618.909  11
   8  -1   2 7741.47 632.741  11
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   8  -1   3 1306.17 296.873   7
   8   1   3 945.085 244.541   7
   8  -1   3 1310.90 314.352   2
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   8   1   3 1329.66 315.139   2
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   8   1   3 1249.42 276.215  11
   8  -1   3 1735.22 313.445  11
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   8  -1   4 131.524 197.617   7
   8   1   4 346.753 240.902   7
   8  -1   4 616.987 259.827   2
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   8   1   4 118.087 246.558   2
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   8   1   4 181.151 157.111  11
   8  -1   4 484.424 252.513  11
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   8  -1   5-203.733 202.420   7
   8   1   5 28.1783 226.668   7
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   8  -1   5 93.2872 183.800   2
   8   1   5 281.106 243.629   2
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   8   1   5 403.961 203.491  11
   8  -1   5 46.3462 184.566  11
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   8   1   6 1638.77 326.615   7
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   8  -1   6 1452.18 348.755   2
   8   1   6 2830.48 454.584   2
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   8   1   6 1611.89 308.437  11
   8  -1   6 1490.35 338.064  11
   8  -1   7 161.054 199.346   7
   8   1   7 273.260 216.866   7
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   8  -1   7 195.267 219.313   2
   8   1   7 214.067 208.907   2
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   8   1   7 189.300 192.603  11
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   8  -1   8 1262.66 342.711   2
   8   1   8 1448.11 375.309   2
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   8   1   8 701.366 256.519  11
   8  -1   8 1349.20 362.508  11
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   8  -1   9 855.327 261.208   2
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   8   1   9 543.286 276.708   2
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   8   1  10 5469.96 645.820   2
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   8   2 -10 446.836 269.061   1
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   8   2  -7 4308.00 520.573   1
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   8   2  -6 1624.07 354.884   1
   8  -2  -6 1819.37 382.004   1
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   8   2  -6 1377.15 255.492   9
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   8  -2  -5 685.173 279.108   1
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   8   2  -5 811.602 225.756   9
   8   2  -5 700.452 278.893   1
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   8  -2  -4 4427.62 537.715   1
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   8   2  -4 4687.87 517.285   1
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   8   2   0 22.2145 179.115   7
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   8   2   3 1292.65 365.376   2
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   8   2   3 705.905 231.540  11
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   8  -2   4 3934.95 476.301   7
   8   2   4 3852.31 472.334   7
   8  -2   4 4314.43 501.263   2
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   8   2   4 3600.50 514.329   2
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   8   2   4 4427.21 453.094  11
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   8  -2   5 3148.66 444.635   7
   8   2   5 3638.17 470.413   7
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   8  -2   5 5007.35 526.849   2
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   8   2   5 3947.39 515.062   2
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   8   2   5 3545.14 403.962  11
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   8  -2   6 840.186 286.864   2
   8   2   6 615.057 283.547   2
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   8   2   6 651.352 210.340  11
   8  -2   6 467.814 237.346  11
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   8  -2   7 1255.11 314.607   2
   8   2   7 1722.97 408.549   2
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   8   2   7 1687.95 322.042  11
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   8  -2   8-145.585 250.435   7
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   8  -2   8 121.011 181.046   2
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   8   2   8-239.248 262.469   2
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   8  -2   9 590.622 281.811   7
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   8  -2   9 739.362 259.540   2
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   8   2   9 1301.68 356.200   2
   8   2   9 984.582 267.551  11
   8  -2   9 810.930 304.349  11
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   8  -2  10 81.1835 218.266   7
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   8  -2  10 149.707 191.688   2
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   8   2  10 50.6406 224.374   2
   8  -2  10 508.637 272.899  11
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   8  -2  11 655.225 309.347   7
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   8  -2  11 838.879 302.175   2
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   8   2  11 1105.23 432.334   2
   8  -2  11 989.323 374.908  11
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   8  -2  12 1249.87 361.002   7
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   8  -2  12 503.293 263.934   2
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   8  -2  12 1054.52 382.245  11
   8   2  12 1955.68 456.036   2
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   8  -2  13 665.843 310.654   7
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   8  -2  13 1702.84 448.174  11
   8   2  13 1543.79 444.045   2
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   8  -2  14-316.470 308.354  11
   8   2  15 18.6110 252.125   2
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   8   3 -13 2202.35 498.467   1
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   8  -3 -12 515.506 300.788   1
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   8   3 -12 386.616 301.541   1
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   8  -3 -11 677.420 355.804   1
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   8   3 -11 788.485 322.538   1
   8   3 -10 436.336 260.277   1
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   8  -3 -10-203.405 247.634   1
   8  -3  -9 4096.30 575.331   1
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   8   3  -9 3487.74 511.338   1
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   8   3  -8 993.536 318.846   1
   8  -3  -8 573.371 305.651   1
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   8   3  -7 816.158 286.496   1
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   8  -3  -7 727.854 293.058   1
  -8   3   6 219.416 194.770   5
   8   3  -6 76.7516 149.651   9
   8  -3  -6 125.600 248.939   1
   8  -3  -6 153.477 129.029   7
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  -8   3   6 32.7872 173.075   6
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   8   3  -6 179.053 211.646   1
  -8   3   6 62.9293 217.080   4
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   8   3  -5 6742.98 555.152   9
   8  -3  -5 5547.06 457.706   7
   8   3  -5 5048.54 572.858   2
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   8   3  -5 5428.04 555.922   1
   8  -3  -5 7024.55 690.027   1
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   8   3  -4 1372.66 318.677   1
   8   3  -4 914.303 301.633   2
   8  -3  -4 2013.25 285.150   7
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  -8  -3   4 1243.36 341.856   6
   8  -3  -4 867.804 304.699  11
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   8   3  -3 810.095 320.194   2
   8  -3  -3 1388.38 259.110   7
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   8   3  -3 990.070 296.638   1
   8  -3  -3 979.603 353.516  11
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   8  -3  -2 65.0824 173.918   7
   8   3  -2-277.449 212.814   2
   8   3  -2 152.550 168.050   1
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  -8   3   2 95.4903 171.094   6
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   8  -3  -2-115.254 201.352  11
  -8   3   1 7237.32 599.128   5
   8  -3  -1 7067.38 627.970   2
   8   3  -1 6436.26 629.710   2
   8  -3  -1 6623.45 550.874   7
  -8   3   1 6849.67 568.102  13
  -8   3   1 7622.19 601.016   6
  -8  -3   1 6858.12 664.978   6
  -8  -3   1 6312.88 625.031  12
   8  -3  -1 7202.83 655.914  11
   8   3  -1 6697.67 579.901   1
  -8   3   0 885.856 239.333   5
   8  -3   0 855.012 256.677   2
   8  -3   0 790.561 235.504   7
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   8   3   0 1279.36 316.631   2
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  -8   3   0 814.495 233.488   6
   8   3   0 723.563 206.955  11
   8  -3   0 704.343 263.160  11
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   8  -3   1 2189.69 383.686   2
   8  -3   1 2296.94 370.488   7
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   8   3   1 1921.77 410.762   2
  -8  -3  -1 2204.15 427.269  12
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   8   3   1 2048.28 336.397  11
   8  -3   1 1753.73 393.419  11
  -8   3  -2 43.3827 160.077   5
  -8   3  -2 526.092 163.583   3
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   8  -3   2 135.669 161.822   2
   8  -3   2 289.560 192.739   7
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   8   3   2 95.5937 202.590   2
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   8   3   2 92.7154 127.951  11
   8  -3   2 28.8028 189.799  11
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   8  -3   3 5861.70 556.492   7
   8  -3   3 5053.89 515.748   2
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   8   3   3 5362.37 579.180   2
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   8   3   3 5884.56 486.997  11
   8  -3   3 6105.40 586.281  11
  -8   3  -3 5426.15 440.864   3
  -8   3  -4 1539.22 327.432   5
  -8   3  -4 1546.76 269.286   3
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   8  -3   4 1252.59 309.487   7
   8  -3   4 2071.82 356.740   2
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   8   3   4 1526.36 356.732   2
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   8   3   4 1838.21 290.080  11
   8  -3   4 1366.42 319.834  11
  -8   3  -5 1788.30 370.069   5
  -8   3  -5 1178.62 263.714   3
  -8  -3  -5 1331.95 294.047   8
   8  -3   5 1868.08 387.913   7
   8  -3   5 2184.09 374.122   2
  -8  -3  -5 1910.80 418.226  12
   8   3   5 2429.00 443.164   2
  -8  -3  -5 1683.02 411.599   6
  -8   3  -5 2240.36 371.954   6
   8   3   5 1780.21 305.438  11
   8  -3   5 2252.77 429.936  11
  -8   3  -6 196.325 196.397   5
  -8   3  -6-119.658 155.505   3
  -8  -3  -6-28.3305 177.410   8
   8  -3   6 266.005 210.089   7
   8  -3   6-88.1766 171.191   2
  -8  -3  -6-300.120 207.014  12
   8   3   6 115.142 219.802   2
  -8  -3  -6 35.1277 243.008   6
  -8   3  -6-41.8423 148.794   6
   8   3   6 220.331 159.334  11
   8  -3   6 226.761 223.190  11
  -8   3  -7 2697.04 411.849   5
  -8   3  -7 3392.09 418.716   3
  -8  -3  -7 2738.59 378.973   8
   8  -3   7 3207.76 475.595   7
   8  -3   7 3066.24 421.853   2
  -8  -3  -7 2936.04 465.807  12
  -8  -3  -7 3500.43 515.104   6
   8   3   7 3334.13 515.189   2
  -8   3  -7 3271.81 441.534   6
   8  -3   7 3470.35 484.908  11
  -8   3  -8 1521.47 356.331  10
  -8   3  -8 880.836 250.063   3
  -8   3  -8 749.371 261.614   5
   8  -3   8 615.192 282.655   7
  -8  -3  -8 636.497 287.914  12
   8  -3   8 416.502 209.852   2
  -8  -3  -8 776.919 299.769   6
  -8   3  -8 1245.73 327.487   6
   8   3   8 451.159 288.613   2
   8  -3   8 1572.03 365.745  11
  -8   3  -9 2414.82 442.796  10
  -8   3  -9 1982.05 383.334   3
   8  -3   9 1126.88 331.737   7
  -8   3  -9 1579.35 352.442  12
  -8  -3  -9 1990.33 413.198  12
   8  -3   9 2253.11 379.209   2
  -8  -3  -9 2312.32 487.811   6
  -8   3  -9 2390.39 434.100   6
   8   3   9 1866.55 447.349   2
   8  -3   9 1056.42 344.710  11
  -8   3 -10 522.251 269.734  10
  -8   3 -10 428.673 259.396   3
   8  -3  10-239.961 236.792   7
  -8   3 -10 308.630 221.050  12
  -8  -3 -10 316.480 231.050  12
   8  -3  10 149.572 163.181   2
  -8  -3 -10 517.296 288.195   6
  -8   3 -10 869.719 285.443   6
   8   3  10 368.723 299.172   2
   8  -3  10 299.319 295.681  11
  -8   3 -11 1867.65 398.825   3
   8  -3  11 2030.57 444.016   7
  -8   3 -11 1385.49 353.771  12
  -8  -3 -11 1100.96 374.641  12
  -8  -3 -11 1972.52 468.344   6
  -8   3 -11 1860.91 386.071   6
   8  -3  11 2068.18 469.499  11
   8   3  11 2315.95 497.591   2
  -8   3 -12 634.504 303.307   3
   8  -3  12 450.456 283.626   7
  -8   3 -12 317.100 214.942  12
  -8  -3 -12 18.0397 243.466  12
  -8  -3 -12 503.224 341.654   6
  -8   3 -12 647.301 294.102   6
   8  -3  12 432.791 316.898  11
   8   3  12 843.301 368.488   2
   8   3  13 1533.58 456.052   2
  -8   3 -13 1047.76 355.714   3
   8  -3  13 729.846 330.760   7
  -8   3 -13 850.791 328.510  12
  -8  -3 -13 1386.25 388.145  12
  -8  -3 -13 746.689 374.629   6
   8  -3  13 2081.76 511.785  11
   8   3  14-494.571 307.836   2
  -8   3 -14 265.023 248.341   3
  -8   3 -14 374.038 239.311  12
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   8  -3  14-255.830 315.860  11
  -8   4  14 114.457 253.475   5
   8   4 -14 657.223 331.553   1
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  -8   4  13 328.421 282.352   5
   8  -4 -13-73.0907 272.068   1
   8   4 -13 84.0711 225.969   1
  -8  -4  13 355.111 316.182   4
  -8   4  13 1124.69 426.212  13
  -8  -4  13 218.818 310.943  13
  -8   4  13 554.319 327.419   4
  -8   4  12-16.5606 236.175   5
   8  -4 -12 890.858 384.166   1
  -8  -4  12 307.375 277.033   4
  -8   4  12-40.6261 272.010  13
  -8  -4  12 408.057 361.865  13
   8   4 -12 471.089 311.496   1
  -8   4  12 221.729 272.016   4
  -8   4  11 2239.23 453.473   5
   8  -4 -11 3505.92 592.013   1
  -8  -4  11 2455.35 487.244   4
  -8   4  11 2991.06 556.503  13
  -8  -4  11 4174.42 680.316  13
  -8   4  11 2779.28 494.722   4
   8   4 -11 3292.39 526.536   1
  -8   4  10 1238.51 347.178   5
  -8  -4  10 1047.08 338.350   4
  -8   4  10 798.956 331.520  13
  -8  -4  10 1471.31 444.314  13
  -8   4  10 1151.83 339.716   4
   8  -4 -10 1329.55 382.486   1
   8   4 -10 1240.98 338.256   1
   8   4  -9 221.519 253.063   1
  -8   4   9 340.467 266.363   5
   8  -4  -9 329.226 273.896   1
  -8  -4   9 533.604 258.005   4
  -8   4   9 391.766 280.121  13
  -8  -4   9-168.559 262.194  13
  -8  -4   9 461.993 317.330   6
  -8   4   9-49.4502 237.630   4
  -8   4   8 254.702 234.267   5
   8   4  -8 730.172 265.557   1
   8  -4  -8 824.805 345.865   1
  -8  -4   8 720.420 240.157   4
  -8   4   8 587.925 282.073  13
  -8  -4   8 483.676 284.865  13
  -8   4   8 491.825 267.408   4
  -8  -4   8 840.947 328.120   6
   8  -4  -7 4908.18 614.465   1
  -8   4   7 5282.57 602.562   5
   8   4  -7 4565.05 494.449   9
   8   4  -7 5285.67 577.708   1
  -8  -4   7 4799.16 518.455   4
  -8   4   7 5172.57 585.616  13
  -8  -4   7 4664.13 621.657  13
  -8   4   7 5319.90 600.202   4
  -8  -4   7 4423.93 601.479   6
  -8   4   6 53.0689 180.374   5
   8   4  -6 347.523 202.048   9
   8   4  -6 79.9521 207.130   2
   8   4  -6 238.955 195.932   1
   8  -4  -6 169.485 128.011   7
  -8   4   6 50.0682 261.722  13
  -8  -4   6 122.335 174.329   4
  -8   4   6-203.741 202.756   6
  -8  -4   6 364.612 289.487  13
  -8  -4   6 97.7525 226.601   6
   8  -4  -6 224.176 213.401   1
  -8   4   5 922.628 290.020   5
   8   4  -5 714.141 255.145   9
   8   4  -5 895.287 327.493   2
   8  -4  -5 1142.37 240.644   7
   8  -4  -5 1198.51 365.462   1
  -8   4   5 840.820 296.009  13
  -8  -4   5 1196.85 266.540   4
  -8  -4   5 1185.54 377.588  13
   8   4  -5 767.829 307.576   1
  -8   4   5 514.432 244.326   6
  -8  -4   5 1161.10 387.949   6
   8   4  -4 304.693 190.285   1
  -8   4   4-45.6283 163.942   5
   8   4  -4-4.03506 200.413   2
   8  -4  -4 299.990 156.314   7
  -8   4   4 142.879 201.923  13
  -8  -4   4 227.939 238.447  13
  -8   4   4 253.170 179.999   6
  -8  -4   4 459.302 264.761   6
   8  -4  -4-61.1242 208.345  11
  -8   4   3 5648.01 555.947   5
   8  -4  -3 5129.18 471.600   7
  -8   4   3 5749.46 533.649  13
   8   4  -3 5077.67 561.471   2
  -8   4   3 6321.16 551.874   6
  -8  -4   3 5452.21 566.391  12
  -8  -4   3 5935.56 636.702   6
   8   4  -3 5837.18 538.899   1
   8  -4  -3 5097.95 577.702  11
  -8   4   2 785.004 231.107   5
   8  -4  -2 783.559 244.242   7
   8   4  -2 1250.63 303.637   2
  -8   4   2 1270.86 280.943  13
  -8  -4   2 1216.30 298.641  12
  -8   4   2 1237.12 254.161   6
  -8  -4   2 585.447 237.191   6
   8   4  -2 589.803 217.935   1
   8  -4  -2 662.482 259.314  11
  -8   4   1 1512.82 329.350   5
   8  -4  -1 2001.98 343.136   7
   8   4  -1 1966.04 340.840   1
   8   4  -1 1927.66 378.779   2
  -8   4   1 1315.22 280.161  13
  -8  -4   1 1693.74 349.354  12
  -8   4   1 2287.46 336.959   6
  -8  -4   1 1753.77 390.910   6
   8  -4  -1 1696.86 386.605  11
  -8   4   0 899.106 280.660   5
   8  -4   0 805.007 241.415   2
   8   4   0 1427.76 278.863   1
   8  -4   0 1142.25 273.680   7
  -8   4   0 1348.06 270.971  13
   8   4   0 1267.95 313.308   2
  -8  -4   0 818.084 312.385  12
  -8  -4   0 612.365 283.081   6
  -8   4   0 1157.85 268.939   6
   8  -4   0 903.627 283.964  11
  -8   4  -1 3830.69 453.340   5
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   8  -4   1 3863.01 453.800   2
   8  -4   1 4163.21 480.494   7
  -8   4  -1 4248.46 412.529  13
  -8   4  -1 4428.26 444.333   6
   8   4   1 4141.12 508.877   2
  -8  -4  -1 4039.19 514.810  12
  -8  -4  -1 5480.44 605.044   6
   8   4   1 4798.63 429.841  11
   8  -4   1 4354.08 518.976  11
  -8   4  -2-155.430 200.529   5
  -8  -4  -2 297.013 215.999   8
   8  -4   2 190.666 186.489   2
   8  -4   2 249.612 210.914   7
  -8   4  -2 171.953 152.406  13
  -8  -4  -2 137.812 231.133  12
   8   4   2 504.372 280.809   2
  -8  -4  -2 446.852 287.098   6
  -8   4  -2-70.0501 142.610   6
   8   4   2 171.212 156.433  11
   8  -4   2 282.445 206.512  11
  -8   4  -3 1020.26 316.977   5
  -8   4  -3 1198.60 228.878   3
  -8  -4  -3 1530.26 333.910   8
   8  -4   3 1032.04 270.560   2
   8  -4   3 1174.32 338.477   7
  -8   4  -3 973.408 241.836  13
  -8  -4  -3 888.971 325.832  12
   8   4   3 789.801 349.023   2
  -8  -4  -3 1455.62 397.440   6
  -8   4  -3 953.035 304.435   6
   8  -4   3 1286.91 379.758  11
  -8   4  -4 208.934 168.025   5
  -8   4  -4 182.670 139.135   3
  -8  -4  -4 419.173 201.162   8
   8  -4   4 470.128 250.695   7
   8  -4   4 57.9555 167.676   2
  -8  -4  -4 315.615 241.630  12
   8   4   4 68.4221 202.018   2
  -8  -4  -4 246.414 209.328   6
  -8   4  -4 399.899 172.478   6
   8  -4   4 61.2906 178.322  11
  -8   4  -5 3711.03 477.953   5
  -8   4  -5 4079.73 430.438   3
  -8  -4  -5 4297.96 498.284   8
   8  -4   5 3793.16 489.220   7
   8  -4   5 3375.41 417.527   2
  -8   4  -5 4533.62 471.647   6
  -8  -4  -5 3220.30 480.616  12
   8   4   5 3518.92 508.510   2
  -8  -4  -5 3731.06 532.058   6
   8  -4   5 4270.98 530.439  11
  -8   4  -6 384.914 279.502  10
  -8   4  -6 385.532 183.313   3
  -8   4  -6 87.2816 201.124   5
  -8  -4  -6 308.559 213.783   8
   8  -4   6 229.563 209.388   7
   8  -4   6 327.590 164.789   2
  -8  -4  -6 427.118 249.879  12
  -8  -4  -6-107.902 237.231   6
   8   4   6 230.723 256.159   2
  -8   4  -6 540.882 213.616   6
   8  -4   6 105.701 228.491  11
  -8   4  -7 4057.61 560.320  10
  -8   4  -7 3099.85 413.362   3
  -8   4  -7 3776.95 506.993   5
  -8  -4  -7 3590.29 449.460   8
   8  -4   7 3830.70 524.478   7
   8  -4   7 2973.53 403.061   2
  -8  -4  -7 2893.93 466.899  12
  -8  -4  -7 3746.50 561.524   6
   8   4   7 3049.28 506.957   2
  -8   4  -7 3771.76 478.743   6
   8  -4   7 2917.46 478.675  11
  -8   4  -8 731.555 319.308  10
  -8   4  -8 515.225 230.370   3
  -8   4  -8 156.785 233.442   5
  -8  -4  -8 1062.18 288.171   8
   8  -4   8 480.266 260.526   7
   8  -4   8 175.320 180.872   2
  -8  -4  -8 209.318 256.816  12
  -8  -4  -8 202.541 236.372   6
  -8   4  -8 544.477 233.014   6
   8   4   8 722.126 329.026   2
   8  -4   8 348.810 257.381  11
  -8   4  -9 1775.17 399.367  10
  -8   4  -9 1625.80 349.058   3
  -8   4  -9 2740.35 443.085   5
   8  -4   9 1709.23 387.786   7
  -8  -4  -9 1783.68 390.636  12
  -8  -4  -9 2212.39 454.773   6
  -8   4  -9 1718.18 349.953   6
   8   4   9 2342.70 496.117   2
   8  -4   9 2063.30 443.118  11
  -8   4 -10 432.386 256.982  10
  -8   4 -10 432.861 213.996   3
   8  -4  10 242.055 234.625   7
  -8  -4 -10 398.394 259.131  12
  -8  -4 -10 252.661 308.308   6
   8  -4  10 12.2727 280.276  11
   8   4  10-198.526 262.240   2
  -8   4 -11 638.920 297.423  10
  -8   4 -11 782.234 291.767   3
   8  -4  11 770.770 333.643   7
  -8  -4 -11 843.286 325.746  12
  -8  -4 -11 1479.29 442.512   6
   8  -4  11 1464.88 436.289  11
   8   4  11 940.697 417.302   2
   8   4  12 749.399 365.744   2
  -8   4 -12 253.766 227.165   3
  -8  -4 -12 329.000 244.517  12
  -8  -4 -12 565.551 342.822   6
   8  -4  12 1054.30 399.363  11
   8   4  13 805.038 379.117   2
  -8   4 -13 514.793 283.038   3
   8  -4  13 157.991 274.479   7
  -8  -4 -13 770.320 326.847  12
  -8  -4 -13 976.615 409.301   6
   8  -4  13 989.408 407.537  11
   8   5 -14 704.672 362.652   1
  -8  -5  14 0.49676 349.886   4
  -8   5  13 123.158 309.666   5
   8   5 -13 857.964 342.495   1
  -8  -5  13 527.156 318.742   4
  -8   5  12 1176.20 379.301   5
   8  -5 -12 1946.63 481.707   1
   8   5 -12 1632.49 417.150   1
  -8  -5  12 1509.65 404.255   4
  -8   5  12 1399.87 452.799  13
  -8  -5  12 1359.67 475.915  13
  -8   5  12 2160.06 468.773   4
  -8   5  11 267.337 233.541   5
  -8   5  11 100.731 213.637  10
  -8  -5  11 20.2430 256.894   4
  -8   5  11 686.376 349.024  13
   8  -5 -11 381.364 267.654   1
   8   5 -11 86.7552 223.797   1
  -8  -5  11 346.221 308.677  13
  -8   5  11-31.7955 240.396   4
  -8   5  10 1899.72 425.132   5
  -8   5  10 1768.45 392.799  10
  -8  -5  10 1496.73 365.734   4
  -8   5  10 1465.42 406.889  13
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   8   5 -10 1715.52 370.518   1
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   8  -5  -9 3173.65 528.566   1
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   8   5  -9 2532.73 433.079   1
   8   5  -8 1841.08 370.081   1
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   8   5  -8 1836.11 341.263   9
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   8   5  -7 446.870 243.525   1
   8  -5  -7 136.728 265.454   1
   8   5  -7 154.692 187.550   9
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   8  -5  -6 1183.20 366.057   1
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   8  -5  -3 300.978 239.430  11
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   8   5   2 2104.25 427.321   2
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   8   5   3 1056.61 314.862   2
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   8   5   4 1695.43 392.345   2
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   8   5   5 561.791 258.957   2
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   8   5   6 4518.35 592.031   2
   8  -5   6 5320.17 599.790  11
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   8  -5   7 2086.26 403.540   7
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   8   5   7 2231.10 461.634   2
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   8  -5   8 59.8017 231.987   7
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   8   5   8 340.520 326.287   2
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   8  -5  10 733.230 338.498  11
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   8  -5  11 513.220 340.602  11
   8   5  11 137.662 257.960   2
   8   5  12 206.427 307.128   2
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   8  -5  12-135.475 277.574   7
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   8  -5  12 358.882 320.925  11
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   8  -5  13 1393.02 464.120  11
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   8   6 -13-210.337 245.356   1
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   8   6 -10 4850.32 593.000   1
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   8  -6  -7 117.023 259.417   1
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   8   6  -7 406.262 226.169   1
   8   6  -6 1033.53 272.509   1
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   8   6  -6 900.449 276.263   9
   8  -6  -6 1164.87 341.186   1
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   8  -6  -5 502.252 316.508   1
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   8  -6  -5 20.5802 220.385  11
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   8   6  -3 1129.57 248.823   1
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   8   6  -2 4401.36 426.953   1
   8  -6  -2 4364.21 545.403  11
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   8   6   2 1010.58 316.489   2
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   8  -6   2 913.838 346.616  11
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   8  -6   3 101.278 139.690   2
   8  -6   3 376.825 251.733   7
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   8   6   3 618.188 280.220   2
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   8  -6   3 427.376 270.300  11
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   8  -6   4 5437.48 494.729   2
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   8  -6   4 5417.49 590.757   7
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   8   6   4 5386.69 619.442   2
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   8  -6   4 5113.06 589.149  11
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   8   6   5 900.471 307.534   2
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   8  -6   6 453.756 265.066   7
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   8   6   6 614.909 301.239   2
   8  -6   6 627.134 309.211  11
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   8  -6   7-315.504 246.046   7
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   8   6   7 398.596 300.919   2
   8  -6   7 299.429 235.742  11
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   8  -6   8 2388.25 440.877   7
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   8   6   8 1858.20 430.837   2
   8  -6   8 2731.65 506.914  11
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   8  -6   9-34.7435 249.964   7
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   8  -6   9 418.655 265.031  11
   8   6   9 6.85715 249.461   2
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   8  -6  10 185.498 270.468   7
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   8  -6  10 646.209 344.998  11
   8   6  10 1231.13 440.709   2
   8   6  11 43.1261 309.257   2
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   8  -6  11-546.532 291.502   7
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   8  -6  11 425.386 314.403  11
   8   6  12 2700.44 590.808   2
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   8  -6  12 3041.77 549.027   7
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   8  -6  12 2289.65 559.537  11
  -8   6 -13 798.029 317.853   3
   8   7 -13 540.442 294.997   1
  -8   7  13 486.484 369.163  13
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   8   7 -12 2500.95 468.772   1
  -8   7  12 2203.30 514.309  13
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   8   7 -11-385.698 225.968   1
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   8   7   2 3263.65 500.575   2
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   8  -7   3 720.322 276.894   7
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   8   7   3 580.264 301.543   2
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   8  -7   3 865.277 306.345  11
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   8   7   4 1936.34 426.485   2
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   8  -7   5 405.752 265.045   7
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   8   7   5 563.130 263.056   2
   8  -7   5 475.756 277.322  11
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   8  -7   6 5006.33 593.012   7
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   8   7   6 5335.36 660.918   2
   8  -7   6 6273.48 688.679  11
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   8  -7   7 209.608 230.172   7
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   8   7   7 69.0073 261.458   2
   8  -7   7 767.201 313.795  11
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   8  -7   8 5.42755 251.711   7
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   8   7   8 568.244 361.059   2
   8  -7   8 463.601 295.393  11
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   8  -7   9 485.543 297.885   7
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   8  -7   9 116.383 290.022  11
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   8   7  11-34.3377 291.477   2
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   8  -8  -8 3347.90 597.501   1
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   8   8  -7 2198.12 431.536   2
   8  -8  -7 2814.46 508.704   1
   8  -8  -7 2715.66 405.898   7
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   8  -8  -6 1742.83 407.425   1
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   8  -8  -3 3433.91 521.935  11
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   8  -8   0 3560.39 530.058  11
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   8  -8   1 2409.22 422.345  11
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   8   8   2 1249.35 356.208   2
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   8  -8   2 892.930 319.079  11
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   8   8   3 2652.03 466.027   2
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   8  -8   3 2533.27 457.298  11
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   8  -8   4 280.552 228.566   7
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   8   8   4 671.038 318.523   2
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   8  -8   4 820.985 311.123  11
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   8   8   5 1160.70 348.467   2
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   8  -8   6 502.766 307.552   7
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   8   8   6 499.975 274.269   2
   8  -8   6 358.036 284.303  11
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   8  -8   7 470.343 290.985   7
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   8   8   7 525.219 288.960   2
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   8  -8   8 2233.38 464.076   7
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   8   8   8 2599.33 539.497   2
   8  -8   8 3191.43 566.448  11
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   8  -8   9 1533.22 393.516   7
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   8  -8   9 1777.32 495.239  11
   8   8   9 1480.94 415.116   2
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   8  -8  10 773.893 334.974  11
   8   8  10 356.485 337.325   2
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   8  -9 -10 319.451 302.953   1
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   8   9 -10 190.014 223.217  14
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   8   9  -9 2240.14 453.321   9
   8  -9  -9 2114.68 485.584   1
   8   9  -9 2204.77 450.377  14
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   8   9  -8 278.509 236.351   9
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   8  -9  -8 145.280 276.169   1
  -8   9   7 929.951 352.116   5
  -8   9   7 888.341 369.007  10
   8   9  -7 988.436 333.538   9
   8   9  -7 831.190 311.882   2
   8  -9  -7 872.774 355.053   1
   8  -9  -7 849.472 303.699   7
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  -8   9   6-213.001 254.973   5
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   8   9  -6-154.419 216.684   9
   8   9  -6 346.374 253.760   2
   8  -9  -6-2.64402 175.712   7
   8  -9  -6 210.244 244.665   1
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   8   9  -5 3830.15 544.622   9
   8  -9  -5 4523.93 560.742   7
   8   9  -5 3748.54 546.657   2
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   8  -9  -5 4634.90 603.093  11
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   8   9  -4-154.738 203.955   9
   8  -9  -4 428.615 248.992   7
   8   9  -4 179.173 227.087   2
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   8  -9  -4 698.787 324.817  11
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   8   9  -3 967.159 364.649   9
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   8  -9  -3 1071.53 324.671   7
   8   9  -3 729.246 294.914   2
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   8  -9  -3 1021.64 382.204  11
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   8   9  -2 343.691 265.630   9
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   8  -9  -2 118.200 211.492   7
   8   9  -2 174.946 203.559   2
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   8  -9  -2 956.014 334.331  11
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   8   9  -1 3363.81 517.446   9
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   8  -9  -1 3160.49 473.900   7
   8   9  -1 2976.57 473.685   2
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   8 -10  -8 819.121 390.085   1
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   8 -10  -7 4633.53 586.439   7
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   8 -10  -5-15.4980 267.656  11
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   8 -11   6 2404.12 549.342  11
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   8 -12  -8 1651.22 437.183   7
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   8 -12  -7 855.188 350.435   7
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   8 -12  -6 3005.09 557.229   1
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   8 -12  -6 2322.68 476.818   7
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   8  12  -5 116.772 230.370   9
   8 -12  -5 50.0044 222.889   7
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   8 -12  -5 837.131 368.009   1
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   8 -12  -5-250.429 335.004  11
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   8 -12  -4 1816.75 448.396   7
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   8 -12  -4 2517.93 513.822  11
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   8 -12  -3-3.08080 224.855   7
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   8 -12  -3 41.3205 244.505  11
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   8  12  -2 1510.70 421.539   9
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   8 -12  -2 2365.62 477.308   7
   8  12  -2 175.811 233.172   2
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   8 -12  -2 1833.65 457.965  11
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   8  12  -1 96.2929 248.592   9
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   8 -12  -1 319.188 307.055   7
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   8 -12  -1 74.0536 285.871  11
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   8  12   0 2304.06 507.560   9
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   8 -12   0 2301.67 488.355   7
   8  12   0 2126.90 438.213   2
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   8 -12   0 3050.66 542.166  11
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   8  12   1 1042.64 381.420   9
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   8 -12   1 1921.27 436.835   7
   8  12   1 2051.54 435.124   2
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   8 -12   1 2034.93 446.248  11
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   8  12   2 992.627 379.043   9
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   8 -12   2 782.817 362.708   7
  -8 -12  -2 754.113 333.002  12
   8  12   2 558.929 291.156   2
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   8 -12   4 3464.82 602.302  11
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   8  13   1-256.384 224.355   2
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   8  13   2 2384.27 474.861   2
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   9   1 -11 201.024 302.010   1
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   9   1 -10 1467.27 412.645   1
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   9   1  -8 1126.62 349.334   1
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   9   1  -7 892.482 309.880   1
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   9   1  -6 2416.67 437.178   1
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   9  -1  -6 2453.40 465.789   1
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   9  -1  -5 341.623 249.294   1
   9   1  -5 762.877 285.938   1
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   9   1  -4 2504.52 445.493   1
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   9  -1  -4 2295.36 444.164   1
   9   1  -4 2325.13 435.627   2
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   9  -1  -3 22.6786 220.177   2
   9   1  -3-38.3778 206.879   2
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   9   1  -3 183.961 156.064   7
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   9   1  -3 181.287 200.842   1
   9  -1  -3 183.902 217.832   1
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   9   1   0 2572.01 446.084   2
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   9  -1   0 3095.81 464.444  11
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   9  -1   1 1660.17 360.869   2
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   9  -1   2 1469.60 346.948   2
   9  -1   2 283.078 190.463   7
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   9   1   2 839.609 310.228   2
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   9   1   2 950.865 290.419  11
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   9  -1   3 494.539 253.876   7
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   9   1   3 233.596 218.257   7
   9   1   3-96.8610 198.137   2
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   9   1   3 94.0789 159.424  11
   9  -1   3 165.950 180.777  11
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   9  -1   4 2758.24 430.418   7
   9   1   4 2718.55 422.217   7
   9  -1   4 2526.23 435.099   2
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   9   1   4 2175.39 419.814   2
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   9   1   4 2883.92 410.162  11
   9  -1   4 2295.31 395.900  11
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   9  -1   5 177.568 237.131   7
   9   1   5 35.7463 207.441   7
   9  -1   5 234.271 230.971   2
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   9   1   5 181.677 237.968   2
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   9   1   5 299.585 213.545  11
   9  -1   5 435.379 238.934  11
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   9  -1   6 805.899 293.165   7
   9   1   6 708.850 258.169   7
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   9   1   6 1126.77 340.592   2
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   9   1   6 1501.11 315.407  11
   9  -1   6 860.841 270.608  11
   9  -1   7 772.683 303.102   7
   9   1   7 1242.02 355.281   7
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   9  -1   7 1202.79 339.585   2
   9   1   7 1416.71 382.411   2
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   9   1   7 1756.30 345.291  11
   9  -1   7 1419.34 338.771  11
   9  -1   8 3038.87 481.431   7
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   9  -1   8 3771.04 531.643   2
   9   1   8 3419.23 526.622   2
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   9   1   8 3206.52 444.898  11
   9  -1   8 2571.73 430.219  11
   9  -1   9 508.770 265.380   7
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   9  -1   9 1220.32 348.061   2
   9   1   9 886.052 317.887   2
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   9  -1   9 1160.46 346.799  11
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   9  -1  10 168.068 251.006   7
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   9  -1  10-63.2188 194.154   2
   9   1  10 174.099 270.614   2
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   9  -1  10 267.089 254.386  11
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   9  -1  11 399.461 297.499   7
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   9  -1  11-192.704 233.484   2
   9   1  11-357.486 266.594   2
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   9  -1  11 195.573 284.789  11
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   9  -1  12 650.613 302.859   2
   9   1  12 647.359 350.390   2
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   9  -1  12 878.677 354.580  11
   9   1  13 118.181 233.015   2
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   9  -1  13 132.930 256.544  11
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   9   2 -12 35.5790 250.776   1
   9   2 -11 1187.00 381.177   1
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   9  -2 -11 468.988 292.729   1
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  -9   2  11 229.282 315.370   4
  -9   2  10 16.6214 202.011   5
   9   2 -10 243.694 255.304   1
   9  -2 -10 958.884 368.840   1
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  -9   2  10 411.358 249.068   4
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   9   2  -9 1957.66 422.804   1
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  -9   2   9 2482.56 480.896   4
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   9  -2  -9 1685.67 452.451   1
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   9  -2  -8 1543.90 397.668   1
   9   2  -8 1705.72 379.909   1
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  -9   2   8 971.312 332.948   4
  -9   2   8 1080.77 334.020   6
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  -9   2   7-71.2844 159.472   5
   9  -2  -7 903.041 333.223   1
  -9   2   7 294.814 320.778  13
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   9   2  -7 152.911 218.009   1
  -9   2   7 786.540 293.762   4
  -9   2   7 13.5788 194.365   6
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   9   2  -6 3632.82 514.761   1
   9  -2  -6 2754.70 493.367   1
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  -9   2   6 3564.05 518.505  13
  -9  -2   6 3182.02 536.237  13
  -9  -2   6 2704.62 405.601   4
  -9   2   6 2917.75 473.170   6
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  -9   2   5 2511.38 404.050   5
   9   2  -5 2355.38 407.311   1
   9   2  -5 1609.59 365.365   2
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  -9  -2   5 2844.23 381.214   4
   9  -2  -5 3833.62 538.743   1
  -9   2   5 3430.09 496.824   6
  -9  -2   5 3415.23 533.634   6
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   9  -2  -4 342.261 248.579   1
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   9  -3  11 1105.10 403.865  11
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   9  -4  -9 3008.34 534.534   1
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   9   4  -7 525.565 261.662   1
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   9  -4  -6 734.947 341.189   1
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   9  -4  -5 3467.50 541.818   1
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   9   4  -5 2478.12 405.287   1
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   9   4  -4 1053.75 275.174   9
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   9   4  -4 1511.38 333.875   1
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   9   4  -3 826.766 279.622   1
   9   4  -3 726.453 309.924   2
   9  -4  -3 424.915 191.048   7
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   9   6   3 87.8875 210.580   2
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   9  -6   4 1446.27 411.258  11
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   9  -6   5 327.747 257.997   7
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   9   6   5 156.985 276.011   2
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   9  -6   5 531.342 284.776  11
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   9  -6   6 4102.67 573.289   7
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   9   6   6 4950.48 668.770   2
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   9  -6   6 5046.51 633.510  11
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   9  -6   7-297.405 268.343   7
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   9   6   7 166.801 303.364   2
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   9  -6   7 494.414 299.621  11
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   9  -6   8 37.0428 232.754   7
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   9  -6   9 322.059 329.720   7
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   9   6   9 267.769 302.030   2
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   9  -7  -8 493.355 343.366   1
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   9  -7  -6 1121.12 410.996   1
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   9  -7  -5-29.7245 285.054   1
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   9   7   4 5586.95 693.005   2
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   9  -7   5-55.0228 260.992   7
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   9   7   5 85.6699 250.027   2
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   9  -7   5-141.435 236.379  11
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   9   7   6 1271.64 363.106   2
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   9  -7   6 1603.53 436.171  11
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   9  -7   7 266.071 236.406   7
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   9   7   7 584.991 325.816   2
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   9  -7   7 532.545 357.291  11
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   9  -7   8 1016.59 361.070   7
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   9   7   8 286.496 292.004   2
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   9  -7   8 827.548 388.146  11
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   9  -7   9 420.863 325.911  11
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   9   8  -7 131.872 221.800   9
   9  -8  -7 696.388 375.106   1
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   9  -8  -6-183.245 268.055   1
   9   8  -6 249.071 246.969   9
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   9   8  -5 2366.11 455.970   9
   9   8  -5 2063.81 456.043   2
   9  -8  -5 2498.39 423.931   7
   9  -8  -5 3581.80 577.005   1
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   9   8  -4 1260.18 369.876   9
   9  -8  -4 841.093 281.831   7
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   9  -8  -4 1381.44 401.916  11
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   9  -8  -3 353.701 265.954  11
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   9  -8  -2 1415.77 332.382   7
   9   8  -2 1719.55 411.953   2
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   9  -8  -2 2529.16 496.575  11
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   9  -8  -1 2719.45 457.741   7
   9   8  -1 2015.07 428.381   2
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   9  -8  -1 2417.87 492.371  11
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   9   8   0-153.289 249.809   2
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   9  -8   0 355.465 288.705  11
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   9   8   1 817.905 325.588   2
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   9  -8   1 511.603 291.269  11
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   9   8   2 1273.37 379.741   2
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   9   8   3 2662.62 503.634   2
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   9  -8   3 2161.89 454.734  11
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   9  -8   4 914.784 333.573   7
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   9   8   5 915.140 374.004   2
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   9  -8   5 593.042 356.731  11
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   9  -8   6 1191.02 379.602   7
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   9   8   6 881.160 357.469   2
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   9  -8   6 2270.16 487.153  11
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   9  -8   7 1890.22 436.688   7
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   9   8   7 2043.75 493.155   2
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   9  -8   7 3021.57 556.322  11
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   9   9  -8 526.543 290.437   9
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   9   9  -7 4950.04 649.937   9
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   9   9  -6-14.6064 228.402   9
   9  -9  -6-150.506 267.424   1
   9   9  -6 46.6314 203.970   2
   9  -9  -6 125.317 196.600   7
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   9   9  -5-57.8822 227.565   9
   9   9  -5 198.788 263.157   2
   9  -9  -5-298.443 284.013   7
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   9  -9  -5 181.714 264.780   1
  -9   9   4-296.822 285.724   5
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   9   9  -4-170.472 200.924   9
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   9  -9  -4 121.946 199.855   7
   9   9  -4 66.5849 203.637   2
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   9  -9  -4-32.7264 284.453  11
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   9   9  -3 1013.27 356.203   9
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   9   9  -3 1053.62 361.874   2
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   9  -9  -3 1454.33 398.948  11
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   9   9  -2-172.267 289.005   9
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   9  -9  -2 312.477 216.224   7
   9   9  -2-66.8778 235.149   2
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   9  -9  -2 312.421 272.763  11
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   9   9  -1 1141.92 397.808   9
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   9  -9  -1 712.672 319.405   7
   9   9  -1 1126.17 375.132   2
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   9  -9  -1 1033.86 425.917  11
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   9  -9   0 944.416 315.351   7
   9   9   0 1277.41 363.960   2
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   9  -9   0 707.593 311.269  11
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   9  -9   1 6277.92 697.467   7
   9   9   1 4661.76 629.926   2
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   9  -9   1 5130.40 663.551  11
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   9  -9   2 696.104 352.864   7
   9   9   2 898.099 317.415   2
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   9  -9   2 626.008 317.163  11
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   9  -9   3 658.807 296.204   7
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   9   9   3 188.175 298.039   2
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   9  -9   3 659.497 350.672  11
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   9  -9   4-110.373 254.758   7
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   9   9   4 369.653 291.762   2
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   9  -9   4 113.153 245.827  11
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   9  -9   5 738.984 334.476   7
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   9   9   5 803.423 343.537   2
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   9  -9   5 538.841 297.986  11
  -9   9  -6 273.188 317.918  10
  -9   9  -6 200.338 256.894   5
  -9  -9  -6 384.108 262.450   8
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  -9   9  -7 394.151 331.435  10
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  -9   9  -8 163.126 328.958  10
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  -9  -9  -9 3221.44 586.264   8
   9  10  -8 321.580 257.243   9
   9  10  -8 681.247 317.743  14
  -9  10   7 581.400 368.277  10
   9  10  -7 602.220 305.566   9
  -9  10   6-9.26597 276.734  10
   9  10  -6 26.4141 228.777   9
   9  10  -6-28.0137 225.295   2
   9 -10  -6-41.4885 205.432   7
  -9  10   5 2122.45 467.402   5
  -9  10   5 2334.51 551.345  10
   9  10  -5 1897.56 430.832   9
   9  10  -5 1436.50 380.182   2
   9 -10  -5 2035.88 422.096   7
  -9  10   4-83.8228 309.587  10
  -9  10   4-231.457 249.338   5
   9  10  -4 191.023 236.766   9
  -9 -10   4-352.675 302.971   8
   9 -10  -4 51.7177 218.240   7
   9  10  -4 127.596 221.658   2
  -9 -10   4-250.616 264.186   6
  -9  10   3 885.055 432.839  10
  -9  10   3-72.6298 241.249   5
   9  10  -3 533.957 304.605   9
  -9 -10   3 207.385 305.127   8
   9 -10  -3 450.886 240.613   7
   9  10  -3 234.294 270.115   2
  -9 -10   3 346.875 332.828   6
   9 -10  -3 391.412 302.361  11
  -9  10   2 266.443 328.264  10
  -9  10   2 57.3169 255.799   5
   9  10  -2-224.837 241.123   9
  -9 -10   2 12.0560 271.628   8
   9 -10  -2 527.370 346.055   7
   9  10  -2 546.470 335.585   2
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  11  -7  -2 308.818 262.437   7
 -11  -7   2 519.788 308.957  12
 -11   7   1 402.590 298.154   5
 -11   7   0 0.45525 211.375   5
 -11   7  -1 205.219 219.461   5
 -11  -7  -1-173.196 247.017   8
 -11   7  -2 1175.03 391.312   5
 -11  -7  -2 1216.90 402.837   8
 -11   7  -3 274.148 246.929   5
   0   0   0    0.00    0.00   0
;
_shelx_hkl_checksum              42664
_shelx_res_file
;
TITL Kasuar in P2(1)/c
    shelx.res
    created by SHELXL-2019/3 at 09:50:29 on 19-Oct-2023
CELL 0.71073   8.310718  13.482029  14.759108  90.0000  90.4239  90.0000
ZERR    4.00   0.000560   0.00053   0.00092   0.0000   0.0062   0.0000
LATT  1
SYMM -x, y+1/2,-z+1/2
SFAC C H P S Br Au
UNIT 48.00 108.00 4.00 4.00 4.00 4.00
L.S.  6
FMAP  2
PLAN 10
SIZE 0.15 0.04 0.04
TEMP -173
ACTA 58
CONF 2.3
SHEL 999 0.73
BOND $H
EQIV $1 x,0.5-y,0.5+z
EQIV $2 1-x,1-y,1-z
HTAB C13 Br1_$1
HTAB C32 Br1_$2
HTAB C33 Au1
HTAB C23 Au1
HTAB C12 S1
HTAB C33 S1
HTAB C22 S1
TWIN 1 0 0  0 -1 0  0 0 -1
WGHT    0.035700    8.660301
BASF   0.21503
FVAR       0.73525
AU1   6    0.260919    0.328683    0.617593    11.00000    0.02512    0.00978 =
         0.02229   -0.00021    0.00216    0.00194
BR1   5    0.166221    0.231141    0.492717    11.00000    0.03403    0.01592 =
         0.02214   -0.00107    0.00071    0.00047
P1    3    0.255506    0.549195    0.741964    11.00000    0.01724    0.00949 =
         0.01431   -0.00030   -0.00055   -0.00031
S1    4    0.360121    0.412078    0.740159    11.00000    0.03002    0.01369 =
         0.02957   -0.00202   -0.00784    0.00636
C1    1    0.310828    0.596996    0.858853    11.00000    0.03463    0.01595 =
         0.01441   -0.00071   -0.00579   -0.00035
C2    1    0.029516    0.540165    0.726755    11.00000    0.01967    0.01659 =
         0.02368   -0.00247    0.00113   -0.00042
C3    1    0.346259    0.630224    0.650199    11.00000    0.01842    0.01767 =
         0.01691   -0.00252    0.00092    0.00363
C11   1    0.292624    0.710885    0.868075    11.00000    0.03419    0.01463 =
         0.02028   -0.00317   -0.00469   -0.00559
AFIX 137
H11A  2    0.181089    0.729814    0.854734    11.00000   -1.50000
H11B  2    0.364619    0.743914    0.825303    11.00000   -1.50000
H11C  2    0.320645    0.730980    0.930022    11.00000   -1.50000
AFIX   0
C12   1    0.486577    0.569016    0.883801    11.00000    0.04053    0.03438 =
         0.02705    0.00679   -0.01980   -0.00851
AFIX 137
H12A  2    0.511311    0.592143    0.945293    11.00000   -1.50000
H12B  2    0.560227    0.600398    0.840895    11.00000   -1.50000
H12C  2    0.499294    0.496819    0.880986    11.00000   -1.50000
AFIX   0
C13   1    0.207308    0.547541    0.930788    11.00000    0.04824    0.02672 =
         0.01781    0.00144    0.00088   -0.00647
AFIX 137
H13A  2    0.240799    0.570757    0.990957    11.00000   -1.50000
H13B  2    0.220513    0.475413    0.927302    11.00000   -1.50000
H13C  2    0.094085    0.564670    0.920334    11.00000   -1.50000
AFIX   0
C21   1   -0.052054    0.635017    0.761774    11.00000    0.01827    0.03140 =
         0.03165   -0.01276    0.00041    0.00004
AFIX 137
H21A  2   -0.005717    0.692931    0.731479    11.00000   -1.50000
H21B  2   -0.034629    0.640614    0.827318    11.00000   -1.50000
H21C  2   -0.167773    0.631924    0.748830    11.00000   -1.50000
AFIX   0
C22   1   -0.035668    0.448904    0.777890    11.00000    0.02708    0.02032 =
         0.04504   -0.00087    0.00314   -0.01042
AFIX 137
H22A  2   -0.152836    0.445651    0.770510    11.00000   -1.50000
H22B  2   -0.008469    0.454596    0.842403    11.00000   -1.50000
H22C  2    0.012919    0.388527    0.753219    11.00000   -1.50000
AFIX   0
C23   1   -0.018252    0.526748    0.626859    11.00000    0.02384    0.02292 =
         0.03317   -0.01088   -0.00847    0.00285
AFIX 137
H23A  2   -0.134832    0.516853    0.622109    11.00000   -1.50000
H23B  2    0.037342    0.468791    0.602068    11.00000   -1.50000
H23C  2    0.012231    0.586032    0.592612    11.00000   -1.50000
AFIX   0
C31   1    0.261805    0.730712    0.639076    11.00000    0.03727    0.01891 =
         0.01336    0.00499   -0.00063    0.00309
AFIX 137
H31A  2    0.248637    0.761605    0.698667    11.00000   -1.50000
H31B  2    0.155899    0.720763    0.610882    11.00000   -1.50000
H31C  2    0.326927    0.773962    0.600574    11.00000   -1.50000
AFIX   0
C32   1    0.524580    0.647185    0.674638    11.00000    0.02259    0.02341 =
         0.04544    0.00007    0.00699   -0.00272
AFIX 137
H32A  2    0.576746    0.684108    0.625778    11.00000   -1.50000
H32B  2    0.578239    0.583015    0.682606    11.00000   -1.50000
H32C  2    0.532253    0.685230    0.731083    11.00000   -1.50000
AFIX   0
C33   1    0.343333    0.576427    0.557924    11.00000    0.04305    0.02302 =
         0.02009   -0.00203    0.01006    0.00387
AFIX 137
H33A  2    0.231596    0.567315    0.537935    11.00000   -1.50000
H33B  2    0.395457    0.511552    0.564101    11.00000   -1.50000
H33C  2    0.401088    0.616248    0.513129    11.00000   -1.50000
AFIX   0
HKLF 4
REM  Kasuar in P2(1)/c
REM wR2 = 0.0842, GooF = S = 1.043, Restrained GooF = 1.043 for all data
REM R1 = 0.0373 for 3863 Fo > 4sig(Fo) and 0.0486 for all 4445 data
REM 155 parameters refined using 0 restraints
END
WGHT      0.0357      8.6690
REM Highest difference peak  2.677,  deepest hole -1.318,  1-sigma level  0.202
Q1    1   0.1541  0.3247  0.6220  11.00000  0.05    2.68
Q2    1   0.3670  0.2337  0.4963  11.00000  0.05    1.76
Q3    1   0.2878  0.2319  0.4878  11.00000  0.05    1.72
Q4    1  -0.2145  0.6754  0.8537  11.00000  0.05    1.66
Q5    1   0.3769  0.3269  0.6074  11.00000  0.05    1.47
Q6    1   0.7413  0.5135  0.8818  11.00000  0.05    1.24
Q7    1   0.6744  0.6668  0.8520  11.00000  0.05    1.12
Q8    1   0.1925  0.3258  0.6830  11.00000  0.05    1.03
Q9    1   0.3278  0.3385  0.6909  11.00000  0.05    0.88
Q10   1   0.2061  0.3200  0.5456  11.00000  0.05    0.87
;
_shelx_res_checksum              44055
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au Au1 0.26092(4) 0.32868(2) 0.61759(2) 0.01906(7) Uani d 1 . .
Br Br1 0.16622(9) 0.23114(5) 0.49272(5) 0.02403(16) Uani d 1 . .
P P1 0.2555(2) 0.54919(11) 0.74196(11) 0.0137(3) Uani d 1 . .
S S1 0.3601(2) 0.41208(13) 0.74016(14) 0.0245(4) Uani d 1 . .
C C1 0.3108(9) 0.5970(5) 0.8589(5) 0.0217(15) Uani d 1 . .
C C2 0.0295(9) 0.5402(5) 0.7268(5) 0.0200(15) Uani d 1 . .
C C3 0.3463(8) 0.6302(5) 0.6502(5) 0.0177(13) Uani d 1 . .
C C11 0.2926(9) 0.7109(5) 0.8681(5) 0.0231(16) Uani d 1 . .
H H11A 0.181089 0.729814 0.854734 0.035 Uiso calc 1 . .
H H11B 0.364619 0.743914 0.825303 0.035 Uiso calc 1 . .
H H11C 0.320645 0.730980 0.930022 0.035 Uiso calc 1 . .
C C12 0.4866(10) 0.5690(6) 0.8838(6) 0.0341(19) Uani d 1 . .
H H12A 0.511311 0.592143 0.945293 0.051 Uiso calc 1 . .
H H12B 0.560227 0.600398 0.840895 0.051 Uiso calc 1 . .
H H12C 0.499294 0.496819 0.880986 0.051 Uiso calc 1 . .
C C13 0.2073(11) 0.5475(6) 0.9308(5) 0.0309(19) Uani d 1 . .
H H13A 0.240799 0.570757 0.990957 0.046 Uiso calc 1 . .
H H13B 0.220513 0.475413 0.927302 0.046 Uiso calc 1 . .
H H13C 0.094085 0.564670 0.920334 0.046 Uiso calc 1 . .
C C21 -0.0521(9) 0.6350(6) 0.7618(6) 0.0271(17) Uani d 1 . .
H H21A -0.005717 0.692931 0.731479 0.041 Uiso calc 1 . .
H H21B -0.034629 0.640614 0.827318 0.041 Uiso calc 1 . .
H H21C -0.167773 0.631924 0.748830 0.041 Uiso calc 1 . .
C C22 -0.0357(10) 0.4489(6) 0.7779(6) 0.0308(19) Uani d 1 . .
H H22A -0.152836 0.445651 0.770510 0.046 Uiso calc 1 . .
H H22B -0.008469 0.454596 0.842403 0.046 Uiso calc 1 . .
H H22C 0.012919 0.388527 0.753219 0.046 Uiso calc 1 . .
C C23 -0.0183(9) 0.5267(6) 0.6269(6) 0.0267(17) Uani d 1 . .
H H23A -0.134832 0.516853 0.622109 0.040 Uiso calc 1 . .
H H23B 0.037342 0.468791 0.602068 0.040 Uiso calc 1 . .
H H23C 0.012231 0.586032 0.592612 0.040 Uiso calc 1 . .
C C31 0.2618(10) 0.7307(5) 0.6391(4) 0.0232(15) Uani d 1 . .
H H31A 0.248637 0.761605 0.698667 0.035 Uiso calc 1 . .
H H31B 0.155899 0.720763 0.610882 0.035 Uiso calc 1 . .
H H31C 0.326927 0.773962 0.600574 0.035 Uiso calc 1 . .
C C32 0.5246(10) 0.6472(6) 0.6746(6) 0.0304(19) Uani d 1 . .
H H32A 0.576746 0.684108 0.625778 0.046 Uiso calc 1 . .
H H32B 0.578239 0.583015 0.682606 0.046 Uiso calc 1 . .
H H32C 0.532253 0.685230 0.731083 0.046 Uiso calc 1 . .
C C33 0.3433(11) 0.5764(6) 0.5579(5) 0.0287(17) Uani d 1 . .
H H33A 0.231596 0.567315 0.537935 0.043 Uiso calc 1 . .
H H33B 0.395457 0.511552 0.564101 0.043 Uiso calc 1 . .
H H33C 0.401088 0.616248 0.513129 0.043 Uiso calc 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Au1 0.02512(12) 0.00978(10) 0.02229(13) 0.00194(11) 0.00216(12) -0.00021(10)
Br1 0.0340(4) 0.0159(3) 0.0221(4) 0.0005(3) 0.0007(3) -0.0011(3)
P1 0.0172(8) 0.0095(6) 0.0143(7) -0.0003(7) -0.0005(7) -0.0003(5)
S1 0.0300(10) 0.0137(8) 0.0296(10) 0.0064(7) -0.0078(8) -0.0020(7)
C1 0.035(4) 0.016(3) 0.014(3) 0.000(3) -0.006(3) -0.001(3)
C2 0.020(3) 0.017(3) 0.024(4) 0.000(3) 0.001(3) -0.002(3)
C3 0.018(3) 0.018(3) 0.017(3) 0.004(3) 0.001(3) -0.003(3)
C11 0.034(4) 0.015(3) 0.020(4) -0.006(3) -0.005(3) -0.003(3)
C12 0.041(5) 0.034(4) 0.027(4) -0.009(4) -0.020(4) 0.007(4)
C13 0.048(5) 0.027(4) 0.018(4) -0.006(4) 0.001(3) 0.001(3)
C21 0.018(4) 0.031(4) 0.032(5) 0.000(3) 0.000(3) -0.013(3)
C22 0.027(4) 0.020(4) 0.045(5) -0.010(3) 0.003(4) -0.001(4)
C23 0.024(4) 0.023(4) 0.033(5) 0.003(3) -0.008(3) -0.011(3)
C31 0.037(4) 0.019(3) 0.013(3) 0.003(3) -0.001(4) 0.005(2)
C32 0.023(4) 0.023(4) 0.045(5) -0.003(3) 0.007(4) 0.000(4)
C33 0.043(5) 0.023(4) 0.020(4) 0.004(3) 0.010(4) -0.002(3)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
S1 Au1 Br1 . . 176.04(5) y
C2 P1 C1 . . 111.3(3) y
C2 P1 C3 . . 110.5(3) y
C1 P1 C3 . . 111.0(3) y
C2 P1 S1 . . 111.2(2) y
C1 P1 S1 . . 102.7(2) y
C3 P1 S1 . . 109.9(2) y
P1 S1 Au1 . . 107.77(9) y
C13 C1 C11 . . 108.4(6) ?
C13 C1 C12 . . 105.3(6) ?
C11 C1 C12 . . 108.2(6) ?
C13 C1 P1 . . 110.5(5) ?
C11 C1 P1 . . 113.2(5) ?
C12 C1 P1 . . 110.8(5) ?
C23 C2 C21 . . 108.0(6) ?
C23 C2 C22 . . 106.6(6) ?
C21 C2 C22 . . 109.9(6) ?
C23 C2 P1 . . 111.8(5) ?
C21 C2 P1 . . 110.2(5) ?
C22 C2 P1 . . 110.2(5) ?
C31 C3 C32 . . 109.4(6) ?
C31 C3 C33 . . 108.4(6) ?
C32 C3 C33 . . 106.6(6) ?
C31 C3 P1 . . 113.6(5) ?
C32 C3 P1 . . 107.7(5) ?
C33 C3 P1 . . 110.8(5) ?
C1 C11 H11A . . 109.5 ?
C1 C11 H11B . . 109.5 ?
H11A C11 H11B . . 109.5 ?
C1 C11 H11C . . 109.5 ?
H11A C11 H11C . . 109.5 ?
H11B C11 H11C . . 109.5 ?
C1 C12 H12A . . 109.5 ?
C1 C12 H12B . . 109.5 ?
H12A C12 H12B . . 109.5 ?
C1 C12 H12C . . 109.5 ?
H12A C12 H12C . . 109.5 ?
H12B C12 H12C . . 109.5 ?
C1 C13 H13A . . 109.5 ?
C1 C13 H13B . . 109.5 ?
H13A C13 H13B . . 109.5 ?
C1 C13 H13C . . 109.5 ?
H13A C13 H13C . . 109.5 ?
H13B C13 H13C . . 109.5 ?
C2 C21 H21A . . 109.5 ?
C2 C21 H21B . . 109.5 ?
H21A C21 H21B . . 109.5 ?
C2 C21 H21C . . 109.5 ?
H21A C21 H21C . . 109.5 ?
H21B C21 H21C . . 109.5 ?
C2 C22 H22A . . 109.5 ?
C2 C22 H22B . . 109.5 ?
H22A C22 H22B . . 109.5 ?
C2 C22 H22C . . 109.5 ?
H22A C22 H22C . . 109.5 ?
H22B C22 H22C . . 109.5 ?
C2 C23 H23A . . 109.5 ?
C2 C23 H23B . . 109.5 ?
H23A C23 H23B . . 109.5 ?
C2 C23 H23C . . 109.5 ?
H23A C23 H23C . . 109.5 ?
H23B C23 H23C . . 109.5 ?
C3 C31 H31A . . 109.5 ?
C3 C31 H31B . . 109.5 ?
H31A C31 H31B . . 109.5 ?
C3 C31 H31C . . 109.5 ?
H31A C31 H31C . . 109.5 ?
H31B C31 H31C . . 109.5 ?
C3 C32 H32A . . 109.5 ?
C3 C32 H32B . . 109.5 ?
H32A C32 H32B . . 109.5 ?
C3 C32 H32C . . 109.5 ?
H32A C32 H32C . . 109.5 ?
H32B C32 H32C . . 109.5 ?
C3 C33 H33A . . 109.5 ?
C3 C33 H33B . . 109.5 ?
H33A C33 H33B . . 109.5 ?
C3 C33 H33C . . 109.5 ?
H33A C33 H33C . . 109.5 ?
H33B C33 H33C . . 109.5 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Au1 S1 . 2.2791(19) y
Au1 Br1 . 2.3925(8) y
P1 C2 . 1.894(7) ?
P1 C1 . 1.895(7) ?
P1 C3 . 1.900(7) ?
P1 S1 . 2.043(2) y
C1 C13 . 1.525(11) ?
C1 C11 . 1.549(9) ?
C1 C12 . 1.550(11) ?
C2 C23 . 1.535(11) ?
C2 C21 . 1.539(10) ?
C2 C22 . 1.544(10) ?
C3 C31 . 1.534(9) ?
C3 C32 . 1.540(11) ?
C3 C33 . 1.543(10) ?
C11 H11A . 0.9800 ?
C11 H11B . 0.9800 ?
C11 H11C . 0.9800 ?
C12 H12A . 0.9800 ?
C12 H12B . 0.9800 ?
C12 H12C . 0.9800 ?
C13 H13A . 0.9800 ?
C13 H13B . 0.9800 ?
C13 H13C . 0.9800 ?
C21 H21A . 0.9800 ?
C21 H21B . 0.9800 ?
C21 H21C . 0.9800 ?
C22 H22A . 0.9800 ?
C22 H22B . 0.9800 ?
C22 H22C . 0.9800 ?
C23 H23A . 0.9800 ?
C23 H23B . 0.9800 ?
C23 H23C . 0.9800 ?
C31 H31A . 0.9800 ?
C31 H31B . 0.9800 ?
C31 H31C . 0.9800 ?
C32 H32A . 0.9800 ?
C32 H32B . 0.9800 ?
C32 H32C . 0.9800 ?
C33 H33A . 0.9800 ?
C33 H33B . 0.9800 ?
C33 H33C . 0.9800 ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
C13 H13B Br1 4_566 0.98 2.98 3.882(8) 153.1 yes
C32 H32A Br1 3_666 0.98 3.00 3.936(8) 160.8 yes
C33 H33B Au1 . 0.98 2.82 3.523(8) 129.0 yes
C23 H23B Au1 . 0.98 2.66 3.541(7) 149.9 yes
C12 H12C S1 . 0.98 2.63 3.169(9) 114.7 yes
C33 H33B S1 . 0.98 2.94 3.487(8) 116.2 yes
C22 H22C S1 . 0.98 2.91 3.377(9) 110.2 yes
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
C2 P1 S1 Au1 . . . . 48.4(3) y
C1 P1 S1 Au1 . . . . 167.6(3) y
C3 P1 S1 Au1 . . . . -74.3(3) y
C2 P1 C1 C13 . . . . 43.1(6) ?
C3 P1 C1 C13 . . . . 166.7(5) ?
S1 P1 C1 C13 . . . . -76.0(6) ?
C2 P1 C1 C11 . . . . -78.8(6) ?
C3 P1 C1 C11 . . . . 44.8(6) ?
S1 P1 C1 C11 . . . . 162.1(5) ?
C2 P1 C1 C12 . . . . 159.4(5) ?
C3 P1 C1 C12 . . . . -77.0(6) ?
S1 P1 C1 C12 . . . . 40.3(5) ?
C1 P1 C2 C23 . . . . 165.9(5) ?
C3 P1 C2 C23 . . . . 42.1(6) ?
S1 P1 C2 C23 . . . . -80.3(5) ?
C1 P1 C2 C21 . . . . 45.8(6) ?
C3 P1 C2 C21 . . . . -78.1(6) ?
S1 P1 C2 C21 . . . . 159.6(5) ?
C1 P1 C2 C22 . . . . -75.7(6) ?
C3 P1 C2 C22 . . . . 160.4(5) ?
S1 P1 C2 C22 . . . . 38.1(6) ?
C2 P1 C3 C31 . . . . 50.2(6) ?
C1 P1 C3 C31 . . . . -73.8(6) ?
S1 P1 C3 C31 . . . . 173.4(4) ?
C2 P1 C3 C32 . . . . 171.6(5) ?
C1 P1 C3 C32 . . . . 47.6(6) ?
S1 P1 C3 C32 . . . . -65.3(5) ?
C2 P1 C3 C33 . . . . -72.1(6) ?
C1 P1 C3 C33 . . . . 163.8(5) ?
S1 P1 C3 C33 . . . . 51.0(5) ?

_cod_database_fobs_code 2022973