#------------------------------------------------------------------------------ #$Date: 2024-02-05 13:07:49 +0100 (Mon, 05 Feb 2024) $ #$Revision: 289690 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/29/2022970.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022970 loop_ _publ_author_name 'Upmann, Daniel' 'Jones, Peter G.' 'Bockfeld, Dirk' 'Târcoveanu, Eliza' _publ_section_title ; Crystal structures of sixteen phosphane chalcogenide complexes of gold(I) chloride, bromide and iodide. ; _journal_coeditor_code YZ2044 _journal_issue 'Pt 1' _journal_name_full 'Acta crystallographica. Section E, Crystallographic communications' _journal_page_first 34 _journal_page_last 49 _journal_paper_doi 10.1107/S2056989023010459 _journal_volume 80 _journal_year 2024 _chemical_formula_iupac '[Au Cl (C11 H25 P Se)]' _chemical_formula_moiety 'C11 H25 Au Cl P Se' _chemical_formula_sum 'C11 H25 Au Cl P Se' _chemical_formula_weight 499.66 _chemical_name_systematic ; [Bis(tert-butyl)(propan-2-yl)phosphane selenide-\kSe]chloridogold ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2019/3 _cell_angle_alpha 90 _cell_angle_beta 90.4954(12) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 7.64505(10) _cell_length_b 14.6437(2) _cell_length_c 13.7211(2) _cell_measurement_reflns_used 24794 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 30.8179 _cell_measurement_theta_min 2.6590 _cell_volume 1536.04(4) _computing_cell_refinement ; CrysAlisPro, Version 1.171.35.11 (Rigaku OD, 2020) ; _computing_data_collection ; CrysAlisPro, Version 1.171.35.11 (Rigaku OD, 2020) ; _computing_data_reduction ; CrysAlisPro, Version 1.171.35.11 (Rigaku OD, 2020) ; _computing_molecular_graphics ; Bruker XP (Bruker, 1998) ; _computing_publication_material ; SHELXL-2019/3 (Sheldrick, 2015) ; _computing_structure_refinement ; SHELXL-2019/3 (Sheldrick, 2015) ; _computing_structure_solution ; SHELXS-97 (Sheldrick, 2008) ; _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean 16.1419 _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.964 _diffrn_measurement_device_type 'Oxford Diffration Xcalibur, Eos' _diffrn_measurement_method '\w scan' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0473 _diffrn_reflns_av_unetI/netI 0.0212 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 20 _diffrn_reflns_limit_k_min -20 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 64129 _diffrn_reflns_theta_full 30.000 _diffrn_reflns_theta_max 30.887 _diffrn_reflns_theta_min 2.664 _diffrn_source 'Enhance (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 12.198 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.17806 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro, Version 1.171.35.11 (Rigaku OD, 2020) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 2.161 _exptl_crystal_density_method 'not measured' _exptl_crystal_description plate _exptl_crystal_F_000 944 _exptl_crystal_size_max 0.3 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.08 _refine_diff_density_max 2.041 _refine_diff_density_min -1.361 _refine_ls_extinction_coef 0.00130(6) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method ; SHELXL-2019/3 (Sheldrick, 2015) ; _refine_ls_goodness_of_fit_ref 1.058 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 145 _refine_ls_number_reflns 4654 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.058 _refine_ls_R_factor_all 0.0243 _refine_ls_R_factor_gt 0.0203 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0167P)^2^+2.0383P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0408 _refine_ls_wR_factor_ref 0.0423 _reflns_number_gt 4270 _reflns_number_total 4654 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file yz2044sup1.cif _cod_data_source_block 7a _cod_depositor_comments 'Adding full bibliography for 2022965--2022980.cif.' _cod_original_cell_volume 1536.05(4) _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 2022970 _cod_database_fobs_code 2022970 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.121 _shelx_estimated_absorpt_t_max 0.442 _shelx_hkl_file ; 0 0 -2 7874.55 499.715 16 0 0 2 6609.48 401.657 3 0 0 2 5887.68 694.229 21 0 0 -2 6959.33 678.818 12 0 0 2 6610.04 358.298 1 0 0 2 6506.31 480.079 17 0 0 -2 7792.47 424.265 3 0 0 -2 8035.22 498.981 17 0 0 -2 6606.59 710.719 2 0 0 2 5746.71 680.240 2 0 0 2 6775.70 314.844 19 0 0 -2 6828.28 358.225 1 0 0 2 6524.57 675.057 20 0 0 2 7440.85 521.724 16 0 0 2 6239.69 600.130 12 0 0 -2 6990.52 723.315 21 0 0 -2 6006.20 638.100 20 0 0 -3 541.974 93.1132 10 0 0 -3 547.162 160.186 3 0 0 -3 307.254 148.809 16 0 0 3 700.785 251.969 16 0 0 3 1143.05 429.430 21 0 0 3 3014.57 573.301 20 0 0 -3 1869.92 537.393 21 0 0 3 706.562 130.629 7 0 0 -3 2538.66 548.069 12 0 0 -3 442.556 418.628 2 0 0 -3 565.169 201.939 17 0 0 3 353.338 106.098 19 0 0 3 421.662 132.870 1 0 0 3 646.269 363.874 12 0 0 3 519.559 172.473 17 0 0 3 596.816 160.935 3 0 0 3 913.766 340.682 2 0 0 -3 333.564 127.533 1 0 0 4 320579. 7598.95 19 0 0 -4 322214. 7778.90 1 0 0 4 324609. 8498.37 16 0 0 -4 317474. 7404.11 8 0 0 4 306061. 7651.46 7 0 0 -4 309356. 7456.39 10 0 0 -4 313037. 8204.60 17 0 0 -4 364181. 9602.68 12 0 0 4 280643. 9355.02 21 0 0 -4 321197. 8254.76 16 0 0 -4 323926. 7954.53 3 0 0 4 328720. 9372.77 20 0 0 -4 337234. 9629.66 21 0 0 4 300643. 8369.29 17 0 0 -4 339792. 9641.74 2 0 0 4 295584. 8872.85 12 0 0 4 335782. 8022.07 3 0 0 4 275944. 9339.55 2 0 0 4 320320. 7788.91 1 0 0 5-2.83755 83.2279 19 0 0 5 185.434 229.124 16 0 0 -5 89.3048 129.903 1 0 0 -5 202.597 70.0788 8 0 0 5 21.0078 107.826 7 0 0 -5 37.3620 424.521 21 0 0 -5 264.538 495.003 12 0 0 -5 428.879 251.968 17 0 0 -5 83.7165 69.1734 10 0 0 -5 522.066 456.106 2 0 0 5 243.419 200.697 3 0 0 6 282025. 7948.45 7 0 0 -6 314917. 7531.33 10 0 0 -6 324423. 7394.32 8 0 0 -6 310998. 8617.20 17 0 0 6 332839. 8445.44 3 0 0 -6 314865. 8041.41 1 0 0 6 299288. 7251.63 5 0 0 6 326266. 9156.98 16 0 0 -7 229.480 288.743 17 0 0 -7-308.399 371.068 21 0 0 7 528.013 315.076 3 0 0 7 157.219 153.711 7 0 0 -7 72.4594 490.507 2 0 0 -7-11.5986 173.688 1 0 0 7 264.888 60.2996 5 0 0 -7 276.344 92.4881 8 0 0 -7 168.862 95.7679 10 0 0 7-285.360 380.405 16 0 0 8 2427.07 405.683 7 0 0 -8 2380.72 263.553 10 0 0 -8 2090.05 379.804 1 0 0 -8 3376.46 866.293 2 0 0 -8 2327.88 199.977 8 0 0 8 2084.53 147.332 5 0 0 8 1799.37 181.686 5 0 0 8 1515.56 400.019 3 0 0 8 2923.38 683.834 16 0 0 -8 2290.39 548.524 17 0 0 -8 3568.27 895.610 21 0 0 -9-380.537 280.080 17 0 0 -9 557.322 565.335 21 0 0 -9 34.7956 46.0700 8 0 0 9 391.035 222.137 7 0 0 9-196.589 393.104 3 0 0 -9 166.369 527.561 2 0 0 -9 718.818 339.333 1 0 0 9-38.0965 440.574 16 0 0 -9 186.317 91.4656 10 0 0 10 71753.7 2492.34 7 0 0 -10 85556.8 4431.68 21 0 0 -10 81943.0 4333.83 2 0 0 -10 61382.0 2727.81 1 0 0 10 65520.5 3167.19 3 0 0 -10 82753.2 2956.19 13 0 0 -10 60348.2 2005.34 10 0 0 10 64855.7 3609.38 16 0 0 -10 67001.9 3272.37 17 0 0 -10 63775.6 1721.58 8 0 0 -11 440.663 576.062 2 0 0 11 273.885 373.783 3 0 0 11 130.370 136.438 7 0 0 -11 905.942 350.010 17 0 0 -11 368.194 588.487 21 0 0 11-779.462 672.668 16 0 0 -11-438.527 370.285 1 0 0 -12 32978.0 2376.97 17 0 0 12 31890.4 2342.71 3 0 0 -12 42735.7 3138.11 2 0 0 -12 32279.5 2012.90 1 0 0 12 36137.6 2814.30 16 0 0 -12 42292.9 3105.38 21 0 0 12 38309.1 3179.76 18 0 0 -13 185.372 509.820 21 0 0 -13 83.1169 342.861 1 0 0 13 306.763 582.080 18 0 0 13-349.179 527.933 3 0 0 -13-149.981 406.411 17 0 0 13 757.451 560.501 16 0 0 -14 9586.12 1344.11 17 0 0 -14 11369.3 1248.95 1 0 0 14 11603.7 1774.30 18 0 0 14 12094.1 1536.43 3 0 0 14 10174.7 1562.31 16 0 0 15-524.979 582.949 3 0 0 -15-123.483 534.044 17 0 0 15-362.774 492.750 18 0 0 15 995.766 602.367 16 0 0 -15-508.675 473.435 1 0 0 -16 19150.3 1810.29 1 0 0 16 20869.8 2182.74 3 0 0 -16 22468.3 2214.13 17 0 0 16 23719.4 2418.09 16 0 0 16 22328.8 2486.82 18 0 0 17-354.052 545.771 16 0 0 17-349.373 495.014 3 0 0 -17 754.029 590.595 1 0 0 -17-34.0856 518.907 17 0 0 17 722.012 678.953 18 0 0 -18 3207.79 834.440 1 0 0 -18 4135.78 1012.43 17 0 0 18 4865.84 1282.05 18 0 0 18 4281.87 1118.35 16 0 0 18 3543.32 995.450 3 0 0 -19-876.950 686.300 17 0 0 19 18.3528 499.694 16 0 -1 -2 102342. 3641.32 20 0 -1 2 115357. 3298.26 17 0 1 2 89990.2 3582.99 12 0 1 -2 105958. 3127.64 12 0 1 2 110836. 2687.87 9 0 1 -2 104869. 3229.50 17 0 -1 -2 107749. 2716.51 17 0 -1 2 106000. 2928.97 12 0 -1 -2 97787.9 3685.20 12 0 1 -2 106648. 3030.73 7 0 -1 -2 110674. 2690.61 9 0 -1 2 113792. 3000.79 3 0 1 -2 114048. 2943.31 11 0 1 -2 97838.5 3366.42 21 0 1 2 107529. 2951.74 15 0 1 -2 97468.5 3093.44 8 0 1 -2 109823. 2749.27 19 0 -1 2 94281.7 3062.59 20 0 1 -2 109879. 3230.51 16 0 1 -2 97904.7 3366.84 2 0 -1 2 111012. 3232.27 16 0 1 2 87356.4 3572.45 20 0 1 2 106741. 2694.51 1 0 -1 2 102972. 3169.31 7 0 -1 -2 111511. 2699.23 1 0 -1 2 90304.5 3229.49 8 0 -1 -2 86175.5 3488.35 21 0 1 -2 112966. 3007.05 3 0 -1 2 109669. 2935.70 11 0 1 2 113529. 2700.44 3 0 -1 2 110725. 2771.89 19 0 1 2 109355. 2774.50 16 0 -1 -2 111760. 2710.79 16 0 1 2 103456. 2749.12 17 0 -1 3 31232.3 1922.01 2 0 -1 3 34633.6 1536.06 7 0 -1 -3 36112.7 2055.68 20 0 -1 3 36105.3 1786.50 20 0 -1 3 36869.4 1586.03 12 0 1 3 32388.9 2048.49 21 0 -1 3 31777.6 1937.88 21 0 1 3 35417.6 1216.97 1 0 -1 3 36720.5 1717.37 16 0 1 3 29384.8 1991.61 2 0 1 3 36815.5 1483.32 15 0 1 -3 35796.8 1344.62 7 0 -1 -3 37188.6 1302.12 17 0 1 -3 38652.8 2019.46 21 0 1 3 35320.4 1195.82 9 0 -1 -3 32693.7 2078.70 12 0 1 -3 35401.9 1194.71 19 0 -1 -3 35954.8 1207.39 1 0 -1 -3 32928.6 2045.09 21 0 1 3 35470.9 2089.76 12 0 1 -3 38205.9 1827.15 12 0 1 -3 38274.0 1480.49 3 0 -1 3 36062.4 1387.82 11 0 1 3 36831.1 1257.19 3 0 -1 -3 37412.2 1306.78 16 0 1 3 40098.8 1454.35 16 0 -1 -3 38426.8 1235.84 3 0 1 -3 36799.0 1957.21 2 0 1 -3 35194.0 1451.12 8 0 1 -3 36699.3 1687.24 17 0 -1 -3 35685.5 2140.74 2 0 1 3 29648.4 2018.47 20 0 1 -3 38465.1 1702.98 16 0 -1 3 36446.7 1719.08 17 0 1 3 37050.3 1383.39 17 0 -1 3 36733.2 1225.28 19 0 -1 3 37221.5 1464.38 3 0 -1 4 173843. 5927.95 2 0 1 4 147321. 4690.98 17 0 -1 -4 178510. 6147.10 2 0 1 -4 172789. 4733.87 3 0 -1 -4 167570. 4550.35 17 0 -1 4 176551. 4792.66 3 0 1 -4 194136. 5699.22 12 0 1 -4 173549. 5824.20 2 0 1 4 161747. 3985.62 10 0 1 -4 173647. 5821.84 21 0 -1 -4 176986. 6141.16 21 0 -1 -4 178824. 6197.90 12 0 -1 -4 172064. 4580.30 16 0 1 4 161255. 4793.73 15 0 -1 4 152108. 4769.59 7 0 -1 -4 166406. 4363.43 1 0 -1 4 165925. 5054.89 12 0 1 -4 167048. 5090.44 17 0 1 -4 170390. 4309.08 19 0 -1 4 186569. 5604.42 20 0 1 -4 162502. 4389.66 7 0 1 4 170390. 4835.07 16 0 1 4 170987. 4483.41 3 0 1 4 149699. 5710.29 12 0 1 4 165486. 4340.08 9 0 1 -4 171590. 5115.14 16 0 1 4 167762. 4358.63 1 0 -1 4 160718. 5170.04 17 0 1 -4 159077. 4503.31 8 0 -1 4 169447. 4328.29 19 0 -1 -4 174969. 4421.97 3 0 -1 -4 165674. 3924.39 10 0 1 -4 169705. 4464.51 1 0 -1 4 172004. 5244.50 16 0 1 4 161681. 5974.33 20 0 -1 4 157775. 5766.18 21 0 -1 4 174327. 4640.46 11 0 1 -5 287441. 7075.24 7 0 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1 7 36179.7 2228.55 16 0 1 -7 37010.3 2181.64 17 0 -1 -7 36638.7 1130.99 10 0 -1 7 39815.7 1995.74 7 0 1 7 38032.8 1846.59 3 0 -1 -7 49973.5 3166.93 21 0 1 -7 36167.0 1708.47 1 0 1 -7 39181.5 1478.35 10 0 -1 7 37939.5 2394.60 16 0 -1 -7 36534.0 1872.41 17 0 -1 -7 48913.0 3147.49 2 0 1 7 33135.5 1369.52 7 0 1 -7 48879.0 2937.08 2 0 -1 -7 34372.3 1616.87 1 0 -1 7 38125.8 1994.59 3 0 1 -7 37817.3 1420.40 8 0 1 -7 49639.6 2955.09 21 0 -1 -8 52057.8 2455.33 17 0 1 8 54090.9 2439.05 3 0 1 -8 66155.1 3621.79 2 0 1 -8 51756.1 2779.89 17 0 -1 -8 68853.9 3880.66 2 0 -1 -8 50356.9 1534.52 10 0 -1 -8 51068.2 2169.33 1 0 1 -8 66184.1 3610.43 21 0 -1 -8 70700.3 3929.91 21 0 1 8 53147.8 1923.10 7 0 -1 8 60085.0 2566.55 7 0 -1 8 51409.8 2560.83 3 0 1 -8 52224.9 2235.38 1 0 1 8 52010.4 2916.17 16 0 -1 8 48532.6 2901.66 16 0 1 -8 55113.4 1799.09 8 0 -1 -9 108579. 2956.63 10 0 -1 -9 112149. 3818.86 1 0 1 -9 136287. 5591.32 21 0 -1 9 134630. 4220.81 7 0 -1 9 111166. 4908.90 16 0 1 9 109914. 4810.89 16 0 1 9 116653. 3324.00 7 0 -1 -9 147067. 6051.55 21 0 1 9 100722. 3192.44 5 0 1 -9 111649. 4602.16 17 0 -1 9 113902. 4382.52 3 0 1 -9 138614. 5638.84 2 0 -1 -9 145145. 6033.55 2 0 -1 -9 108677. 4210.19 17 0 1 -9 112787. 3906.67 1 0 1 9 112581. 4203.65 3 0 1 -9 116690. 3179.41 8 0 1 -10 36313.3 2431.68 17 0 -1 -10 49162.9 1927.34 13 0 1 -10 44649.6 3050.98 21 0 1 10 35371.9 1130.55 5 0 -1 -10 51860.4 3434.47 2 0 -1 -10 36440.6 1236.40 13 0 -1 -10 37218.4 1931.10 1 0 1 10 34483.0 2570.14 16 0 1 -10 37809.4 2001.27 1 0 -1 10 45662.3 2090.29 7 0 1 -10 38379.1 1350.66 8 0 -1 -10 35657.1 1218.20 10 0 1 10 35043.2 1299.12 5 0 1 10 33728.3 1298.73 7 0 -1 10 39526.6 2739.33 16 0 -1 -10 40432.4 2288.74 17 0 -1 -10 50990.9 3395.23 21 0 1 10 38787.2 2270.01 3 0 -1 10 36234.9 2292.78 3 0 1 -10 45715.6 3093.45 2 0 1 11 46322.5 1411.81 5 0 -1 -11 49007.3 2707.04 17 0 1 11 48556.2 3167.42 16 0 1 11 42226.1 1380.71 7 0 -1 11 54027.6 2241.53 7 0 -1 -11 66425.7 3981.66 2 0 -1 -11 46205.0 2314.60 1 0 -1 -11 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16 0 13 12 4083.93 1203.04 5 0 -13 -12 3587.94 801.644 9 0 -13 13 596.359 565.280 3 0 13 13-449.323 418.770 11 0 13 13-611.590 680.112 5 0 13 -13-0.98474 387.598 8 0 13 -13 286.151 396.881 17 0 13 -13 177.780 374.386 19 0 -13 13 684.394 537.259 7 0 -13 13 821.026 572.067 16 0 -13 -13 730.231 454.566 1 0 13 13 206.283 364.367 4 0 -13 14 3436.37 988.390 7 0 13 -14 2631.45 711.519 19 0 -13 14 3215.30 951.448 3 0 -13 14 4053.39 1031.98 16 0 13 14 3142.99 741.754 4 0 13 -14 3332.35 971.066 17 0 13 -14 2059.86 712.097 8 0 13 14 3077.89 672.204 11 0 13 -15 3241.63 819.811 19 0 13 15 2440.94 631.346 11 0 13 15 2540.35 739.304 4 0 -14 0 16276.3 1549.97 15 0 14 0 16188.6 2159.54 5 0 14 0 14790.9 1543.90 19 0 14 0 17728.4 2299.38 8 0 -14 0 12209.5 1203.26 9 0 -14 0 20151.8 2387.14 6 0 -14 0 12913.4 1797.63 7 0 14 0 14688.6 1380.86 11 0 -14 0 13413.1 1268.31 14 0 -14 -1 24663.2 2013.33 15 0 -14 1 23594.9 1804.37 15 0 -14 1 22411.2 1706.03 9 0 14 1 24587.5 2701.16 5 0 -14 1 22632.3 1703.61 14 0 14 1 20896.7 1609.21 11 0 -14 -1 29990.4 3022.44 6 0 14 -1 24926.4 2041.15 19 0 -14 1 30325.9 2897.05 6 0 -14 -1 22342.3 2198.27 7 0 14 -1 32469.3 3049.63 8 0 -14 -1 21446.1 1598.01 14 0 14 -1 23380.7 1851.16 11 0 14 -1 32416.3 2105.54 17 0 14 1 26751.8 2815.64 8 0 14 1 25584.4 2048.72 19 0 -14 -1 22599.7 1674.62 9 0 14 -1 24150.9 2530.50 5 0 -14 1 26054.8 2505.93 7 0 14 -2 3749.71 825.052 19 0 14 -2 4645.99 1137.10 5 0 14 -2 6147.59 1268.82 8 0 -14 -2 5354.16 1067.24 7 0 14 2 3651.59 1005.78 5 0 -14 -2 3497.51 672.928 14 0 14 2 3715.71 656.018 11 0 14 -2 4296.00 840.302 11 0 -14 2 3870.89 1005.43 7 0 -14 -2 6423.02 1490.51 6 0 14 2 4503.72 884.531 19 0 -14 2 4232.36 762.116 9 0 -14 2 4616.65 752.975 15 0 -14 2 4037.55 731.565 14 0 -14 -2 3201.51 652.380 9 0 14 2 5663.46 1251.47 8 0 14 -2 5200.51 874.108 17 0 -14 2 6499.07 1448.35 6 0 14 -3 75392.0 4625.19 8 0 -14 -3 76906.4 4894.75 6 0 -14 -3 54402.6 2755.98 14 0 -14 3 64279.1 4207.46 7 0 14 3 56726.4 3192.15 19 0 14 -3 60028.4 3384.51 19 0 14 3 68306.7 4765.06 5 0 -14 -3 61526.1 3490.68 7 0 14 3 66493.8 4393.32 8 0 14 -3 66571.4 4008.11 5 0 14 3 54867.6 2715.74 11 0 -14 3 56512.5 3006.69 9 0 14 -3 74208.3 3605.41 17 0 -14 -3 59596.3 2883.58 9 0 14 -3 59253.8 3302.49 11 0 -14 3 56666.9 3021.43 14 0 -14 3 59195.5 2682.68 16 0 14 4 24122.7 1960.69 19 0 14 -4 27587.7 2709.58 8 0 -14 4 22597.6 1816.28 9 0 14 4 30963.8 3207.00 5 0 -14 -4 23191.3 1697.71 9 0 -14 -4 22098.5 1657.19 14 0 -14 4 21742.8 1612.08 16 0 -14 -4 23709.5 2702.93 6 0 14 -4 22341.3 2209.56 5 0 14 -4 21615.9 1992.42 11 0 -14 4 27643.4 2680.59 7 0 14 4 19901.9 1504.64 11 0 14 -4 29726.4 2243.61 17 0 -14 -4 22345.8 1915.06 7 0 14 -4 22820.3 2020.94 19 0 14 4 24500.4 2499.58 8 0 -14 4 23560.7 1870.72 14 0 -14 -5 16546.6 1435.00 14 0 14 -5 20735.2 1930.90 17 0 14 -5 16383.4 1799.44 11 0 14 -5 20912.7 2337.25 8 0 -14 -5 18194.0 1525.88 9 0 -14 5 19305.6 2247.50 7 0 -14 5 17979.1 1531.54 16 0 14 -5 17398.8 1767.17 19 0 14 5 18129.2 2130.48 8 0 -14 -5 17012.9 1565.65 7 0 -14 5 15928.9 1596.42 9 0 14 5 15566.9 1301.02 11 0 14 5 18630.5 1725.01 19 0 14 5 23589.7 2825.37 5 0 -14 5 14838.6 1531.69 14 0 14 -5 19188.1 1961.16 5 0 14 6 6304.00 1663.99 5 0 14 -6 6955.32 1191.50 17 0 14 6 4630.01 703.162 11 0 -14 -6 4051.52 727.928 14 0 -14 6 7614.27 1386.00 7 0 14 6 5737.58 732.750 10 0 -14 6 5258.22 945.139 14 0 -14 6 4423.94 921.595 9 0 14 -6 6667.61 1380.76 8 0 14 6 4668.58 887.049 19 0 14 -6 5774.29 1032.16 5 0 -14 6 4835.74 853.574 16 0 14 -6 6716.42 1111.99 19 0 14 -6 5144.36 1010.43 11 0 -14 -6 6678.58 948.274 7 0 -14 -6 4865.01 802.683 9 0 14 6 5272.93 1121.59 8 0 -14 -7 20225.2 1640.22 9 0 -14 7 25392.5 2587.94 7 0 -14 7 20763.0 1830.13 16 0 14 7 20531.6 1838.53 19 0 14 7 24160.8 2901.44 5 0 -14 -7 18924.7 1589.77 14 0 14 -7 26590.9 2306.62 17 0 14 7 20001.8 1489.73 11 0 14 -7 21491.1 1988.47 19 0 14 -7 25997.8 2570.30 8 0 -14 7 20458.4 1888.45 9 0 14 7 23932.5 2113.79 8 0 14 -7 21556.9 1956.91 5 0 14 -7 19350.9 2004.68 11 0 -14 -7 23899.5 1673.67 7 0 -14 7 20236.1 1870.82 14 0 14 8 146.012 232.695 11 0 -14 8 258.691 583.460 7 0 14 -8 637.908 443.429 5 0 14 8 667.552 773.489 5 0 14 -8 137.425 426.618 8 0 14 -8 1119.98 603.819 19 0 -14 -8 722.993 460.972 14 0 -14 8 407.437 419.324 16 0 14 8 223.762 234.488 4 0 -14 8 1302.82 610.412 9 0 -14 -8 116.711 295.883 9 0 14 -8 137.439 400.978 17 0 -14 8 146.733 374.285 14 0 14 -8-494.901 588.828 11 0 14 8 24.5844 415.902 19 0 14 9 34349.1 2439.24 19 0 -14 9 34545.1 2540.26 16 0 -14 9 34355.5 2995.45 7 0 14 -9 40515.5 3154.74 8 0 14 -9 33237.3 2732.80 11 0 14 9 34554.9 3457.95 5 0 -14 9 31789.0 2483.50 14 0 -14 9 29183.5 2308.05 3 0 14 -9 34088.7 2525.18 19 0 -14 -9 33002.3 2212.59 9 0 14 9 29801.1 1914.12 11 0 14 9 29339.6 1878.05 4 0 14 -9 37895.7 2925.50 17 0 14 -10 12399.3 1677.72 11 0 14 -10 18360.8 2092.70 8 0 14 10 14300.0 1312.18 4 0 14 10 11307.9 1425.42 19 0 -14 10 15767.9 1737.95 16 0 -14 10 17400.8 2146.23 7 0 14 -10 15927.8 1900.81 17 0 14 10 11916.8 1217.04 11 0 14 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4 0 -14 14 723.683 630.717 7 0 14 -14 946.978 576.492 8 0 14 -14 731.442 503.164 19 0 -15 0-191.474 390.385 15 0 -15 0 69.8659 660.618 6 0 15 0-857.822 702.533 8 0 -15 0-585.770 421.850 9 0 -15 0-400.616 640.165 7 0 15 0 332.360 327.708 11 0 15 0 24.8661 644.596 5 0 -15 0-519.583 377.181 14 0 15 0 95.7303 354.298 19 0 15 1 3674.83 1213.87 5 0 -15 -1 2855.88 633.403 14 0 -15 -1 4311.07 1016.70 7 0 15 -1 2977.30 697.465 11 0 15 1 2756.59 898.682 8 0 -15 -1 5004.48 1325.13 6 0 -15 -1 3822.37 672.457 9 0 15 -1 3140.46 963.961 5 0 -15 1 2769.93 635.322 14 0 15 1 3152.83 679.948 11 0 -15 1 3726.54 958.821 7 0 15 1 1940.84 616.165 19 0 15 -1 3485.60 809.771 19 0 -15 1 3543.43 714.416 9 0 15 -1 4397.07 1082.00 8 0 -15 2 33805.3 2233.30 9 0 15 2 38143.1 3480.66 5 0 -15 -2 31340.7 2084.37 14 0 15 -2 36201.9 2634.05 19 0 15 -2 32555.9 3016.66 5 0 -15 -2 34557.5 2734.06 7 0 -15 -2 44946.4 3721.20 6 0 15 -2 47454.5 3688.40 8 0 -15 -2 35582.0 2204.51 9 0 -15 2 39849.2 3255.92 7 0 15 2 31603.1 2428.10 19 0 -15 2 34651.0 2276.05 14 0 15 2 33276.1 2110.26 11 0 15 2 35624.1 3271.31 8 0 15 -2 33842.6 2437.35 11 0 15 -3 2247.81 828.678 5 0 -15 3 2596.52 913.660 7 0 -15 -3 3371.24 823.442 7 0 -15 3 3118.82 711.568 14 0 15 3 3129.87 1164.70 5 0 15 3 2764.20 920.236 8 0 -15 -3 2823.97 604.736 14 0 -15 3 3309.97 592.731 16 0 15 -3 2207.93 898.786 8 0 15 -3 2686.87 789.999 19 0 15 -3 2641.61 734.281 11 0 15 3 1686.74 485.728 11 0 -15 3 3270.93 749.344 9 0 -15 -3 2593.40 634.473 9 0 15 3 2920.99 773.861 19 0 -15 -4 12503.4 1328.27 9 0 15 4 12807.1 2189.48 5 0 -15 4 12102.5 1375.65 9 0 -15 -4 12436.3 1277.99 14 0 15 -4 16746.0 1681.62 17 0 15 -4 15623.0 1867.75 5 0 -15 4 14523.6 1994.45 7 0 -15 -4 12787.7 1503.30 7 0 -15 4 15008.0 1530.24 14 0 15 -4 11824.0 1482.65 19 0 -15 4 12922.0 1229.53 16 0 15 4 11337.2 1155.05 11 0 15 -4 13767.4 1620.98 11 0 15 4 13908.4 1562.99 19 0 15 -4 16861.6 2131.15 8 0 15 4 15353.2 2074.60 8 0 -15 5 1403.17 500.279 16 0 15 -5 1088.83 553.461 5 0 15 5 1021.15 422.514 11 0 15 -5 6.57388 443.474 11 0 15 5 1398.83 815.252 5 0 15 5 1833.75 685.187 8 0 15 -5 155.165 436.859 19 0 15 5 545.702 491.113 19 0 -15 -5 1059.55 497.439 9 0 -15 -5 563.458 300.668 7 0 -15 5 256.968 385.040 14 0 -15 -5 572.496 422.150 14 0 15 -5 1075.09 750.038 8 0 -15 5 682.328 496.364 9 0 -15 5 209.992 575.285 7 0 15 -5 886.509 537.380 17 0 -15 -6 324.284 241.881 7 0 -15 -6 366.238 317.793 14 0 -15 6-361.676 455.184 14 0 15 -6 487.953 556.084 11 0 15 6 844.977 441.293 19 0 15 6 246.661 223.452 10 0 -15 6 676.611 670.490 7 0 15 6 411.633 292.612 11 0 15 -6-79.3493 656.631 8 0 15 -6 776.589 562.639 17 0 -15 -6 393.925 350.678 9 0 15 6 678.312 492.867 8 0 15 6-125.179 739.373 5 0 -15 6 590.634 319.185 16 0 15 -6 940.013 552.858 19 0 15 -6 339.468 346.988 5 0 -15 6-47.2610 333.780 9 0 15 -7 14819.6 1732.40 17 0 -15 -7 11894.2 1295.36 14 0 15 -7 16398.7 1731.58 5 0 15 7 11655.3 1591.79 8 0 -15 -7 12334.7 1330.11 9 0 15 -7 18031.5 2200.81 8 0 15 7 11255.4 1419.64 19 0 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1789.72 11 0 15 -10 15926.1 1919.26 17 0 15 10 10949.4 1200.87 11 0 15 -10 16747.1 2116.91 8 0 15 10 10947.1 1480.26 19 0 -15 10 14270.2 1692.90 16 0 -15 10 15432.8 2036.56 7 0 15 10 11523.8 2045.56 5 0 -15 11 3054.40 866.240 16 0 -15 11 4040.13 958.794 3 0 15 11 2380.17 1060.98 5 0 15 -11 3217.35 844.060 19 0 15 -11 2464.80 853.381 8 0 15 -11 3113.01 936.017 17 0 -15 11 3504.17 988.681 7 0 15 -11 4865.11 1212.65 11 0 -15 11 3325.82 887.620 14 0 -15 -11 3223.16 809.684 9 0 15 11 3497.38 726.197 11 0 15 11 2478.53 727.841 19 0 15 -12 1134.74 520.136 19 0 15 12-39.9317 576.949 5 0 15 -12 1819.46 815.745 17 0 -15 12 1746.24 818.181 7 0 -15 12 677.209 472.230 3 0 -15 12 1379.93 713.955 16 0 15 12 889.155 520.214 19 0 15 -12 386.808 486.365 8 0 15 12 667.957 354.190 11 0 15 13 2393.19 1010.95 5 0 -15 13 5789.70 1282.33 7 0 15 -13 5126.95 1211.28 17 0 15 -13 5331.77 1051.71 19 0 15 -13 5216.10 1131.37 8 0 -16 0 19162.2 2236.26 7 0 -16 0 20147.9 1698.92 14 0 -16 0 17872.9 1626.44 9 0 16 0 23877.2 2666.95 8 0 16 0 20596.5 2016.93 19 0 16 0 22884.9 2623.19 5 0 16 0 21130.3 1846.82 11 0 16 -1 1605.89 688.500 19 0 16 1 1841.64 603.590 11 0 -16 -1 883.161 417.757 7 0 -16 -1 1840.57 578.234 14 0 16 1 1529.36 929.510 5 0 16 -1 1841.49 645.113 11 0 -16 1 364.947 379.506 7 0 16 1 1629.83 673.856 19 0 -16 -1 741.787 305.516 9 0 16 1 2001.34 903.365 8 0 16 -1 1396.98 836.956 5 0 16 -1 3123.93 1099.86 8 0 -16 1 963.471 467.602 14 0 -16 1 1195.85 497.462 9 0 16 2 1648.89 1089.41 5 0 -16 -2 2305.78 585.845 14 0 16 -2 2226.44 693.387 11 0 -16 2 3146.96 718.135 9 0 -16 2 2454.14 644.025 14 0 16 -2 1860.72 878.474 8 0 -16 -2 2037.33 557.782 9 0 16 -2 2074.95 742.714 19 0 -16 -2 1702.00 622.488 7 0 16 2 2814.56 672.287 11 0 16 2 2382.58 739.994 19 0 -16 2 945.534 754.934 7 0 16 2 2465.92 980.669 8 0 16 -2 2241.11 849.212 5 0 16 -3 662.213 547.579 5 0 16 -3 2230.53 901.804 8 0 -16 -3 1844.78 596.213 7 0 16 3 2862.74 798.127 19 0 16 3 1843.83 508.400 11 0 16 -3 1839.47 633.523 19 0 -16 3 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1827.30 420.812 3 1 -2 -8 1247.19 312.926 1 -1 -2 8 2123.50 621.906 16 -1 -2 8 619.237 392.589 18 1 2 -7 507.659 225.661 8 1 -2 -7-46.3863 483.970 12 1 2 -7 57.3220 318.000 17 1 -2 -7 589.940 158.239 6 -1 2 7 449.920 249.460 16 -1 2 7 906.901 410.771 18 1 2 -7 938.182 372.246 12 -1 -2 7 1188.78 352.269 7 1 2 -7 753.124 182.790 19 -1 2 7 597.692 215.700 3 -1 -2 7 501.820 120.160 5 1 2 -7 646.211 309.591 1 1 2 -7 994.137 211.510 6 -1 -2 7 450.470 239.298 3 -1 -2 7 1018.85 479.815 16 -1 -2 7 550.831 389.150 18 1 -2 -7 1026.96 281.738 1 1 -2 -7 1064.39 316.002 17 -1 -2 6 24818.7 961.023 5 -1 2 6 22627.9 1548.96 16 1 2 -6 25821.4 1370.47 13 1 -2 -6 24668.7 1248.90 1 -1 -2 6 23327.4 1657.39 18 1 2 -6 25782.7 1593.52 17 -1 2 6 27915.3 1465.39 3 1 -2 -6 27202.6 1300.91 17 1 -2 -6 25589.5 1474.69 15 1 2 -6 25488.8 1116.39 19 -1 -2 6 26278.6 1638.71 3 1 -2 -6 24790.4 1923.53 12 -1 -2 6 25590.7 1744.25 16 -1 -2 6 23930.0 1356.58 15 1 -2 -6 24940.0 1144.23 6 -1 2 6 27599.0 1767.26 18 -1 -2 6 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90597.7 2902.51 7 1 2 -4 94987.8 3107.98 17 1 -2 -4 97862.2 2726.22 6 1 -2 -4 95098.1 2400.36 8 -1 2 4 96936.1 2969.47 4 1 -2 -4 92257.3 2996.53 15 1 -2 -4 95247.1 2644.35 3 -1 2 4 92587.0 3044.60 18 -1 -2 4 92402.0 3162.47 3 1 -2 -4 87986.3 3533.56 12 1 2 -4 91115.3 2571.70 5 -1 2 4 97062.0 2873.06 16 1 -2 -4 94719.2 2662.88 9 -1 2 4 98392.5 2896.06 3 1 2 -4 94558.1 2886.60 12 -1 -2 4 92651.3 3089.88 18 1 2 -4 88684.1 2856.14 13 -1 2 4 95138.6 2555.96 6 1 -2 -4 93886.8 2721.78 17 -1 -2 4 94352.0 2778.50 19 -1 -2 3 77204.7 2432.97 7 -1 2 3 77544.2 2178.64 9 -1 2 3 75199.9 2216.56 17 1 -2 -3 79059.6 2186.96 9 -1 -2 3 78174.6 2538.01 3 1 -2 -3 76913.5 2061.72 8 -1 -2 3 79069.0 2528.73 16 -1 2 3 75417.6 1983.38 8 1 2 -3 78470.1 2535.66 16 -1 -2 3 76300.5 2036.19 15 -1 2 3 78195.8 2137.46 14 -1 2 3 80030.5 2391.82 4 -1 -2 3 77257.3 2234.67 5 -1 2 3 78083.3 2044.90 19 -1 -2 3 78289.3 2362.27 13 -1 -2 3 80508.2 2256.27 19 -1 2 3 77186.2 2460.65 15 1 2 -3 76666.4 2251.70 19 1 2 -3 79173.6 2563.70 3 1 -2 -3 78397.9 2463.09 15 -1 -2 3 78088.3 2421.35 18 -1 2 3 75939.6 2237.72 1 -1 -2 3 77789.6 2467.77 11 -1 2 3 71849.1 2803.94 12 -1 2 3 74522.7 2371.10 18 1 -2 -3 79428.1 2104.67 3 1 -2 -3 75983.7 2451.81 18 -1 2 3 81614.3 2295.76 3 1 -2 -3 77377.2 2283.24 6 1 -2 -3 68508.7 2281.54 16 1 -2 -3 69399.1 2817.03 12 -1 2 3 79088.3 2144.73 16 1 2 -3 75585.5 2363.83 13 1 2 -3 76486.6 2224.42 5 1 2 -3 80009.7 2311.01 12 -1 2 3 77316.9 2194.52 6 1 -2 -3 78140.3 2240.54 1 1 2 -3 76284.9 2421.50 18 1 -2 -3 76922.9 2198.41 17 -1 -2 3 76980.4 2481.14 17 1 2 -3 77365.1 2491.93 17 1 2 -2 2288.36 250.187 18 1 -2 -2 1988.05 241.932 4 -1 -2 2 2245.68 206.671 4 1 -2 -2 1813.48 207.754 1 -1 2 2 1893.45 183.028 14 -1 2 2 2085.59 201.455 9 -1 -2 2 1778.23 285.549 7 -1 2 2 2060.05 147.885 16 -1 -2 2 2301.10 281.341 3 -1 -2 2 1849.48 231.950 13 1 -2 -2 1864.21 192.175 9 -1 2 2 2043.62 210.539 17 1 -2 -2 1885.52 159.941 16 1 2 -2 2482.70 284.540 3 1 2 -2 1718.19 200.886 19 1 -2 -2 1942.91 172.954 19 -1 2 2 1928.00 187.297 19 -1 -2 2 2252.00 272.531 17 -1 2 2 2165.75 194.923 3 1 -2 -2 1970.93 242.079 18 -1 -2 2 1942.50 257.680 16 -1 -2 2 1782.11 233.206 5 -1 2 2 1976.58 255.357 15 1 -2 -2 1966.77 195.441 14 -1 2 2 2003.87 217.198 1 -1 2 2 1835.83 210.211 18 1 -2 -2 2033.20 144.842 3 -1 -2 2 2297.92 299.408 11 1 -2 -2 2018.00 402.243 12 -1 2 2 2312.74 263.868 4 1 -2 -2 1835.65 277.426 15 -1 2 2 2290.75 172.958 10 1 -2 -2 1916.92 204.086 8 -1 -2 2 2398.28 224.367 19 -1 2 2 2123.82 237.317 6 -1 2 2 1903.46 336.232 12 1 2 -2 1954.94 243.607 13 1 2 -2 1947.17 261.790 17 1 -2 -2 1873.44 260.678 6 1 2 -2 1877.02 250.056 5 -1 2 2 1937.47 188.463 8 1 2 -2 1946.15 265.981 16 -1 -2 2 1921.36 215.940 18 1 -2 -1 4571.27 319.557 4 1 -2 -1 4584.73 271.392 9 -1 -2 1 4326.13 326.919 16 -1 -2 1 4536.11 280.032 18 -1 -2 1 4701.77 393.483 7 -1 -2 1 4837.98 314.479 17 1 2 -1 4930.74 360.435 13 1 2 -1 4586.05 333.204 16 -1 2 1 5392.34 447.379 12 1 -2 -1 4993.68 324.517 19 1 2 -1 4970.21 313.582 17 1 -2 -1 4540.70 328.546 8 1 2 -1 4894.80 308.339 19 1 2 -1 4322.49 392.645 5 -1 2 1 4613.65 278.509 1 1 -2 -1 4454.30 277.059 1 -1 2 1 4240.97 303.233 4 -1 -2 1 4564.43 226.595 4 1 -2 -1 4675.20 260.303 14 1 -2 -1 5222.84 450.648 12 -1 2 1 5058.86 338.913 7 -1 -2 1 4495.36 301.563 14 -1 2 1 4448.31 356.579 15 -1 2 1 4765.71 286.477 18 -1 2 1 4952.86 277.969 9 -1 2 1 4919.61 267.592 14 1 2 -1 4800.56 228.870 4 -1 -2 1 4784.51 365.698 11 -1 -2 1 4351.53 367.768 5 1 -2 -1 4415.32 359.559 15 -1 -2 1 4027.16 332.161 13 -1 2 1 4786.54 349.729 19 1 2 -1 4356.99 352.246 11 -1 2 1 4669.73 321.197 8 1 -2 -1 4564.87 367.459 6 1 2 -1 5066.60 301.701 18 1 -2 -1 4910.40 297.072 18 -1 2 1 4584.42 307.290 11 -1 2 1 5133.34 309.465 10 -1 2 1 4824.45 362.898 6 -1 2 0 6465.71 424.473 6 1 2 0 6909.83 368.160 11 -1 2 0 5761.36 341.470 11 1 -2 0 6143.43 423.173 12 1 2 0 5846.36 371.590 10 1 2 0 6350.28 326.186 9 -1 -2 0 6280.32 465.549 20 1 -2 0 6207.64 412.398 8 1 -2 0 6146.17 325.844 14 -1 -2 0 6780.31 493.688 5 -1 2 0 6213.68 289.812 1 -1 2 0 6069.82 394.069 10 1 2 0 5702.75 263.743 4 1 -2 0 6144.95 442.244 19 -1 -2 0 6536.62 391.877 13 -1 -2 0 6330.64 299.348 11 -1 -2 0 6501.23 328.577 14 1 2 0 6067.51 315.489 18 -1 -2 0 6082.03 333.275 21 1 2 0 6056.44 325.516 14 1 2 0 5298.27 443.353 5 -1 2 0 6245.85 313.816 18 -1 2 0 6100.72 352.440 4 -1 2 0 6091.12 400.242 8 1 -2 0 6063.36 354.913 4 -1 2 0 6282.13 403.994 7 -1 -2 0 5943.19 414.735 7 1 -2 0 6246.90 318.124 18 -1 -2 0 5838.94 274.583 17 -1 -2 0 6102.34 318.750 18 -1 -2 0 5857.88 329.424 2 1 2 0 6330.48 386.812 13 1 -2 0 6529.92 429.666 6 -1 -2 0 6419.15 319.539 9 1 -2 0 6368.93 332.600 9 -1 2 0 5771.82 423.488 19 1 2 0 6417.40 269.989 17 1 -2 0 6160.24 351.501 11 1 -2 0 6326.54 404.660 7 -1 -2 -1 247292. 5685.06 14 -1 -2 -1 244760. 5820.19 2 -1 -2 -1 247216. 5669.10 9 1 2 1 240581. 5672.30 9 -1 -2 -1 223427. 5775.95 7 1 2 1 239534. 6132.97 20 -1 2 -1 241355. 5796.13 11 1 2 1 240370. 5778.01 2 1 2 1 238463. 5780.60 21 -1 -2 -1 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14 1 2 2 499.611 169.335 21 -1 2 -2 479.192 158.530 10 -1 2 -2 515.965 150.783 7 1 -2 2 357.477 145.480 11 1 2 2 253.579 95.4145 9 1 2 2 509.700 180.759 2 -1 -2 -2 75.7943 161.945 21 -1 -2 -2 638.172 146.257 17 1 -2 2 471.197 151.361 19 -1 2 -2 527.721 177.355 8 1 -2 2 290.689 115.008 8 -1 2 -2 736.971 198.976 11 1 -2 2 318.761 112.278 2 -1 -2 -2 355.373 115.511 1 -1 2 -2 528.560 183.666 19 -1 2 -2 260.316 98.0024 6 -1 -2 -2 273.337 106.100 9 1 2 2 667.287 227.098 5 -1 2 -2 853.390 180.949 16 -1 -2 -2 272.406 90.2669 10 -1 -2 -2 382.929 164.875 2 1 -2 2 386.659 141.001 6 -1 -2 -2 297.862 106.046 13 -1 -2 -2 3.71299 127.859 5 1 2 2 216.943 89.0426 1 -1 -2 -2 726.211 288.696 20 1 -2 2 203.125 99.4849 21 -1 2 -3 125239. 3492.52 3 -1 -2 -3 105284. 3458.75 17 1 -2 3 120081. 3474.79 2 1 2 3 122684. 3099.08 10 -1 -2 -3 119696. 4028.57 20 1 2 3 125197. 3247.25 14 -1 2 -3 118374. 3467.58 2 -1 2 -3 122824. 3494.91 21 1 -2 3 120951. 3601.31 16 -1 2 -3 120712. 3278.41 20 -1 -2 -3 117944. 3106.26 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705.392 21 2 -12 10 1884.36 795.689 7 2 12 10 1892.98 573.166 19 -2 -12 -10 1602.42 799.193 2 2 -12 10 2372.27 721.810 6 -2 12 -10 597.316 533.297 11 -2 -12 -11 2048.50 866.178 21 -2 -12 -11 936.728 492.005 9 2 12 11 1100.58 405.242 3 -2 12 -11 1244.44 763.616 17 2 -12 11 1913.86 720.867 16 2 12 11 1850.95 798.845 5 -2 12 -11 63.6301 367.674 19 2 -12 11 1123.46 624.269 7 -2 -12 -11 3107.81 1033.74 2 2 -12 11 1331.76 617.937 3 -2 12 -11 839.747 577.398 11 -2 12 -11 1124.27 554.107 8 2 -12 12 13440.7 1631.09 3 2 -12 12 17159.2 1976.10 7 2 12 12 12588.4 1364.73 3 -2 12 -12 13951.2 1651.45 19 2 12 12 13533.5 1722.15 5 -2 12 -12 14403.4 1935.72 17 -2 12 -12 16624.0 1814.39 8 2 -12 12 14499.8 1816.81 16 2 12 12 13171.6 1453.50 4 -2 -12 -12 16290.6 2264.09 21 -2 -12 -12 15741.6 2201.14 2 -2 12 -12 13920.1 1799.93 11 2 12 13 2695.77 648.169 3 -2 -12 -13 4788.85 1333.94 2 -2 12 -13 4783.31 1197.04 17 -2 -12 -13 3416.43 1096.23 21 2 -12 13 3301.89 969.685 16 -2 12 -13 5289.71 1036.82 8 -2 -12 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10187.2 963.600 4 -2 -13 6 10649.9 1248.16 9 -2 13 6 11013.2 1193.23 8 2 -13 -6 11163.6 1457.29 15 -2 -13 6 10236.6 1635.44 7 2 -13 -6 11216.0 1104.68 14 -2 -13 6 11439.0 1295.13 14 2 -13 -6 12279.0 2014.31 6 -2 13 6 11019.8 1146.73 11 2 13 -6 12678.4 1489.55 11 2 13 -5 4656.37 857.149 19 -2 13 5 6933.25 1035.01 19 2 13 -5 6283.24 1071.97 5 -2 -13 5 6484.61 966.855 9 2 13 -5 4457.84 810.773 17 -2 -13 5 7059.94 974.826 16 2 13 -5 5814.51 1208.72 8 -2 13 5 6370.56 997.234 8 2 -13 -5 5611.48 1026.95 15 2 -13 -5 5460.25 789.838 9 -2 -13 5 5818.91 899.696 14 2 -13 -5 6487.18 820.877 14 -2 13 5 6232.97 719.885 4 -2 -13 5 5823.59 1280.72 7 -2 13 5 5246.79 779.834 11 2 -13 -5 6248.88 1368.54 6 2 13 -5 4822.79 966.675 11 2 13 -4 2818.85 674.488 19 2 -13 -4 3485.98 663.397 9 -2 13 4 2263.98 667.037 19 -2 -13 4 2527.60 605.024 9 2 13 -4 3549.32 911.176 5 2 13 -4 2154.00 532.176 17 2 13 -4 2416.47 880.181 8 2 -13 -4 3486.67 835.242 15 -2 -13 4 1406.80 406.405 14 -2 13 4 3405.85 524.856 4 2 -13 -4 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3 -17 26475.6 2699.97 17 -4 3 -17 24514.7 2819.62 2 4 3 17 24231.0 2616.61 16 -4 -4 17 2800.44 1010.42 3 4 -4 -17 1923.69 634.450 17 -4 -4 17 662.825 597.389 16 -4 -4 17 1412.42 740.601 4 4 -4 -17 2987.32 1325.74 12 -4 -4 16 53742.9 4023.65 18 -4 4 16 44019.4 3725.37 18 4 -4 -16 48856.9 3085.42 17 -4 -4 16 53904.9 4041.45 16 4 4 -16 44680.8 3272.55 1 -4 4 16 50467.3 3753.78 4 -4 -4 16 49218.1 3658.21 4 4 4 -16 46830.6 3584.03 17 -4 -4 16 55860.8 3881.36 3 4 -4 -16 51283.7 4333.86 12 4 -4 -16 50120.4 3188.79 1 -4 -4 15 1757.16 760.614 3 -4 -4 15 1461.39 729.651 18 -4 4 15 1914.32 718.026 18 4 -4 -15 1876.92 609.471 17 4 4 -15 2138.32 713.278 17 -4 -4 15 1109.38 621.909 16 4 -4 -15 1987.75 656.624 1 -4 4 15 2288.04 945.268 4 -4 -4 15 2040.68 738.452 4 4 4 -15 2180.45 628.302 1 4 -4 -15 1696.37 862.413 12 4 4 -14 1668.17 673.812 1 -4 -4 14 640.664 546.221 18 -4 -4 14 544.984 485.215 3 -4 4 14 970.544 521.440 18 4 -4 -14 484.740 340.039 17 4 4 -14-794.320 631.661 17 -4 -4 14-58.6000 387.184 16 4 -4 -14 354.736 377.558 1 -4 -4 14 666.930 462.720 7 -4 4 14 1206.42 687.378 4 -4 -4 14 788.058 483.876 4 4 -4 -14 292.441 505.558 12 4 4 -14 855.421 490.048 12 -4 4 13 5505.84 1111.66 18 4 4 -13 7148.52 1127.84 1 4 -4 -13 8273.46 1092.89 17 4 4 -13 5831.68 1101.35 17 -4 -4 13 6478.76 1181.77 16 4 -4 -13 6287.26 955.138 1 -4 -4 13 6988.57 1075.90 7 -4 4 13 6610.43 1177.78 4 -4 -4 13 6634.89 1135.68 4 4 -4 -13 7576.63 1512.34 12 4 4 -13 6743.81 1132.12 12 -4 -4 13 5963.20 1125.65 3 -4 -4 13 6499.67 1238.48 18 -4 4 12 109301. 5075.62 18 4 -4 -12 117326. 4544.40 17 4 4 -12 117456. 5197.02 17 -4 4 12 115544. 4219.16 16 -4 -4 12 112773. 5334.26 16 4 4 -12 118406. 4994.65 1 4 -4 -12 115129. 4868.13 15 -4 4 12 114840. 5082.54 4 -4 -4 12 108089. 4882.69 4 -4 -4 12 111091. 5232.75 18 -4 -4 12 116095. 4763.37 7 -4 -4 12 115169. 5191.12 3 4 -4 -12 113159. 6090.53 12 4 4 -12 111981. 4924.85 12 4 -4 -12 121951. 4597.25 1 -4 -4 11 3215.35 791.585 18 -4 4 11 3443.02 636.218 3 -4 -4 11 1472.57 523.294 3 4 4 -11 2787.15 517.218 10 4 4 -11 1860.22 563.377 1 4 -4 -11 2800.24 609.371 17 -4 -4 11 3380.82 774.998 16 4 4 -11 2017.05 588.885 17 4 -4 -11 2221.51 573.151 15 4 -4 -11 1993.63 523.983 1 -4 -4 11 2482.03 550.946 7 -4 4 11 2623.85 746.195 4 -4 -4 11 2783.77 663.311 4 4 -4 -11 1390.03 681.415 12 4 4 -11 3110.66 707.446 12 -4 4 11 1555.68 552.071 18 4 -4 -11 2313.87 499.965 6 4 4 -10 75412.0 3070.62 5 -4 -4 10 73087.9 3674.27 18 -4 4 10 69667.6 3468.26 18 4 -4 -10 74278.2 3202.12 17 4 4 -10 71765.7 3587.55 17 -4 -4 10 71916.0 3673.06 16 4 -4 -10 74297.0 3474.14 15 -4 4 10 69122.8 3477.41 4 -4 -4 10 73273.1 3368.35 4 -4 -4 10 72249.1 3352.83 7 4 4 -10 75020.5 3554.56 1 -4 -4 10 75445.8 3159.77 13 4 4 -10 73873.5 2900.25 10 -4 -4 10 73971.9 3649.89 3 -4 4 10 76686.4 3060.38 3 4 -4 -10 73047.3 4374.22 12 4 4 -10 68532.1 3370.00 12 4 -4 -10 78167.0 3269.23 6 4 -4 -10 71493.8 3127.24 1 4 4 -9 8560.02 898.533 5 4 4 -9 6862.03 943.163 1 -4 4 9 7943.26 1009.42 18 4 4 -9 6643.50 953.536 17 -4 -4 9 7222.73 1003.27 16 -4 -4 9 7413.98 995.887 18 4 -4 -9 8326.79 1000.28 15 4 -4 -9 7367.55 852.568 1 -4 -4 9 8516.16 998.496 7 4 4 -9 7628.95 803.737 10 -4 4 9 7282.28 957.967 4 -4 -4 9 8012.76 951.450 4 -4 -4 9 8052.32 867.412 13 -4 4 9 9913.31 853.859 3 4 -4 -9 9405.21 959.404 6 4 -4 -9 6882.38 1269.71 12 4 4 -9 7368.46 953.519 12 4 4 -8 15198.4 1129.12 10 4 4 -8 17101.0 933.788 19 -4 4 8 16527.7 1366.35 18 4 4 -8 14696.2 1315.35 17 -4 -4 8 17645.9 1463.22 16 4 4 -8 14611.8 933.088 15 4 -4 -8 15198.0 1335.10 15 -4 4 8 15034.6 1338.91 4 -4 -4 8 15357.8 1192.87 4 -4 -4 8 13688.5 1262.16 7 -4 -4 8 14796.2 1348.55 18 -4 4 8 15795.0 738.605 13 -4 -4 8 17328.3 1259.72 13 4 4 -8 16117.5 1342.93 12 4 -4 -8 15126.0 1770.96 12 4 -4 -8 17402.8 1308.34 6 4 4 -8 15534.8 1233.19 5 4 -4 -8 17604.6 1219.54 1 4 -4 -7 34.2711 104.136 10 4 4 -7 43.3213 231.958 5 4 4 -7 76.0967 205.004 10 4 4 -7 206.873 156.507 19 -4 4 7 232.724 239.089 18 4 4 -7-19.3146 275.782 17 4 -4 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35248.7 1392.92 9 -4 4 5 36714.7 1796.05 18 -4 -4 5 35757.4 1824.54 18 4 4 -5 36391.9 1816.20 17 -4 -4 5 35857.9 1637.50 4 -4 4 5 35016.0 1866.17 4 4 -4 -5 36366.5 1939.96 15 4 4 -5 34844.8 1367.61 15 -4 4 5 36190.7 1416.25 13 -4 -4 5 35650.7 1747.30 13 4 -4 -5 36195.0 2345.00 12 4 -4 -5 34249.7 1838.59 6 4 -4 -5 37654.6 1591.38 1 4 -4 -5 35740.2 1416.45 3 -4 -4 4 68135.5 2632.74 18 4 4 -4 68497.8 2604.39 10 4 -4 -4 68429.3 2386.16 10 4 4 -4 71922.7 2270.80 19 -4 4 4 67601.1 2105.85 19 -4 4 4 65721.1 2561.30 18 4 -4 -4 69240.8 2119.65 9 4 4 -4 70307.1 2574.82 17 -4 -4 4 69359.2 2415.32 4 -4 4 4 69081.3 2698.44 4 4 4 -4 66747.1 2879.05 5 4 -4 -4 67971.0 2796.84 15 4 4 -4 69689.0 2176.99 15 -4 -4 4 68044.4 2241.71 14 -4 4 4 66870.1 2010.34 14 4 -4 -4 66996.8 2101.59 19 -4 4 4 65824.6 2236.38 13 -4 -4 4 70042.4 2607.86 13 4 -4 -4 69011.3 3279.20 12 4 -4 -4 68330.5 2288.75 1 4 -4 -4 69580.5 2764.29 6 4 -4 -4 59448.3 2093.25 3 -4 4 4 71172.5 2516.54 11 4 -4 -3-53.4947 187.494 6 -4 4 3 208.796 167.119 11 4 4 -3 170.832 180.649 17 4 -4 -3 231.959 119.337 1 -4 4 3 281.144 112.466 9 4 -4 -3 106.984 165.566 10 4 4 -3 879.548 223.840 19 4 4 -3-193.304 161.871 10 4 4 -3 220.799 360.640 5 -4 4 3 170.101 160.889 18 -4 -4 3 41.4871 151.037 18 4 -4 -3 138.537 88.3642 9 -4 -4 3 283.613 118.810 9 4 -4 -3-174.997 278.943 15 -4 -4 3 46.1364 135.502 4 -4 -4 3 274.236 119.913 14 -4 4 3 307.813 264.400 4 4 -4 -3 209.582 92.4443 3 -4 4 3 590.145 192.192 13 -4 -4 3 164.996 228.745 13 -4 4 3 237.611 143.563 19 4 -4 -3-351.137 351.376 12 -4 4 2 58716.8 2219.64 18 4 4 -2 60009.8 2635.31 5 4 4 -2 58450.6 2314.43 10 4 -4 -2 59582.6 2236.42 10 -4 4 2 57650.2 2077.15 19 -4 -4 2 58143.5 2268.73 18 -4 -4 2 58758.7 1784.02 9 -4 4 2 55926.2 1892.83 1 -4 -4 2 59792.6 2114.34 4 -4 4 2 57406.7 2242.04 8 -4 4 2 58676.0 2358.61 4 4 -4 -2 59443.0 2531.22 15 -4 -4 2 59322.9 1872.81 14 4 -4 -2 58176.4 1665.12 14 4 -4 -2 61998.6 1870.55 1 -4 -4 2 61041.5 2350.57 13 4 -4 -2 56845.0 2732.21 12 4 -4 -2 57959.9 2422.88 6 -4 4 2 58432.7 2154.32 11 4 -4 -2 56669.7 1783.15 9 4 -4 -1 2898.02 431.784 10 -4 4 1 2759.98 393.944 11 4 4 -1 2851.70 427.369 10 -4 -4 1 2860.93 274.619 9 4 -4 -1 3093.29 300.364 9 4 4 -1 3505.81 598.240 5 -4 4 1 3007.32 429.310 18 -4 -4 1 2808.10 439.431 18 -4 -4 1 2918.37 465.413 21 4 -4 -1 3276.98 278.331 1 -4 4 1 2499.49 416.088 8 4 -4 -1 3115.48 539.920 15 -4 -4 1 3146.84 414.995 4 4 -4 -1 3512.58 270.030 14 -4 4 1 3967.46 537.007 4 -4 -4 1 3024.21 311.419 14 -4 -4 1 2922.70 451.567 13 -4 4 1 2757.02 416.237 19 -4 4 1 2735.16 274.762 1 4 -4 -1 3235.09 510.747 6 -4 -4 1 3031.88 360.884 11 4 4 0 109191. 3924.25 5 4 -4 0 106317. 3532.15 10 -4 -4 0 108666. 3583.51 21 4 4 0 108425. 3519.48 10 -4 4 0 108889. 3487.01 19 -4 -4 0 112361. 2958.65 9 -4 4 0 107882. 3412.34 18 -4 -4 0 110921. 3480.62 18 4 -4 0 109424. 3010.92 9 -4 4 0 106079. 2786.10 1 -4 4 0 107908. 3584.46 4 -4 4 0 110467. 3593.79 8 4 -4 0 106905. 2935.48 14 -4 -4 0 111959. 3052.44 14 -4 -4 0 113037. 3566.53 13 -4 -4 0 110402. 3588.20 2 4 -4 0 111506. 3710.82 6 -4 -4 0 100712. 2841.81 11 -4 4 0 112815. 3358.95 11 -4 -4 -1 19104.0 1226.51 21 -4 4 -1 19338.3 1151.02 21 -4 -4 -1 20150.7 1564.29 20 4 4 1 20463.8 1398.66 5 4 -4 1 20392.4 939.826 3 4 -4 1 20339.2 1239.49 10 -4 4 -1 19877.3 1212.38 19 -4 4 -1 17910.7 617.423 1 -4 -4 -1 19495.7 864.002 9 -4 4 -1 19003.7 1200.98 4 -4 4 -1 20857.3 1258.65 8 4 -4 1 18650.1 923.425 9 -4 -4 -1 20206.3 928.240 14 -4 -4 -1 21901.5 1224.39 13 -4 -4 -1 19749.3 1238.79 2 -4 4 -1 20550.3 1178.50 2 4 -4 1 17465.0 1173.56 6 4 4 1 20609.6 1189.10 10 -4 4 -1 19646.6 1086.05 11 -4 4 -2 4122.85 506.856 11 -4 -4 -2 3261.10 660.547 20 -4 -4 -2 3677.99 558.933 21 4 -4 2 3380.52 499.925 10 -4 4 -2 3819.08 534.518 19 4 -4 2 3224.94 491.921 6 4 4 2 3189.51 529.216 5 -4 -4 -2 3540.67 356.566 9 4 -4 2 3700.33 418.468 3 -4 -4 -2 2463.99 449.246 2 -4 4 -2 2863.30 458.219 2 -4 4 -2 3215.02 522.174 8 4 4 2 3173.54 473.712 10 -4 -4 -2 3931.32 523.513 13 -4 4 -2 3891.07 502.861 21 4 -4 3 15049.8 1114.62 10 4 4 3 14936.3 999.032 10 4 4 3 15170.2 1197.98 5 -4 4 -3 16384.1 1182.69 19 -4 -4 -3 14616.1 833.220 9 -4 -4 -3 15642.1 1193.43 21 -4 -4 -3 17098.9 1485.29 20 -4 4 -3 15748.3 1136.92 8 4 -4 3 17091.7 1094.27 16 -4 4 -3 14224.8 546.722 1 -4 4 -3 14583.9 532.140 1 -4 4 -3 16686.7 1088.82 21 -4 -4 -3 17497.7 1250.12 2 4 -4 3 15724.6 943.337 3 -4 -4 -3 15580.6 1056.52 13 -4 4 -3 16104.1 1071.48 2 4 -4 3 15285.5 1065.01 6 -4 4 -3 14765.3 1024.75 11 4 -4 4 55803.3 2179.58 3 4 4 4 52619.9 2135.35 10 -4 -4 -4 53614.6 2531.65 21 -4 4 -4 53373.7 2295.19 21 4 -4 4 54007.8 2359.61 10 -4 -4 -4 56098.2 2965.16 20 -4 4 -4 55238.5 2461.70 19 -4 4 -4 52128.5 1571.30 1 -4 4 -4 54626.8 2356.84 8 4 -4 4 57852.5 2348.90 16 -4 -4 -4 56855.7 2587.01 2 -4 4 -4 51395.3 2262.94 2 -4 -4 -4 51607.4 2170.85 13 4 4 4 51364.3 2408.86 5 4 -4 4 53447.6 2239.56 6 -4 4 -4 53974.5 2368.52 11 4 -4 5 739.983 264.513 6 -4 4 -5 1399.79 407.746 19 4 -4 5 607.143 305.420 10 -4 -4 -5 555.178 333.634 21 -4 -4 -5 767.975 539.443 20 -4 4 -5 783.542 316.345 20 4 4 5 876.326 259.003 10 -4 4 -5 1607.03 437.097 21 -4 -4 -5 616.288 330.975 2 4 -4 5 826.722 285.993 3 4 -4 5 487.021 308.807 16 -4 4 -5 489.999 283.795 8 4 4 5 394.290 222.710 5 -4 4 -5 796.822 310.400 2 -4 4 -5 631.047 166.416 1 -4 -4 -5 546.419 228.633 13 -4 4 -5 860.662 369.423 11 -4 -4 -6 35445.2 2217.97 21 -4 4 -6 36743.2 1986.90 21 4 -4 6 37874.2 1981.02 10 4 4 6 34318.3 1687.03 10 4 4 6 35158.9 1873.86 5 -4 4 -6 35681.3 1889.44 20 -4 4 -6 36321.7 1388.85 1 -4 -4 -6 37386.8 1909.53 17 -4 4 -6 36344.1 1908.15 8 4 -4 6 34808.4 1951.87 16 -4 -4 -6 36367.1 2237.65 2 -4 4 -6 37810.8 2008.72 2 -4 -4 -6 35099.5 1718.58 13 4 -4 6 35232.3 1752.53 6 -4 -4 -6 33219.1 2408.91 20 -4 4 -6 33073.1 2054.70 11 4 4 6 32600.4 1375.56 11 4 -4 6 35885.2 1866.86 3 4 4 7 7737.15 743.951 10 -4 -4 -7 7073.76 1157.61 20 -4 4 -7 6168.09 818.951 2 -4 4 -7 7195.88 876.870 21 -4 -4 -7 8205.15 1145.52 21 4 -4 7 6389.91 791.777 3 -4 -4 -7 7109.53 884.608 17 4 4 7 8486.00 859.955 5 4 -4 7 6385.75 858.859 16 -4 4 -7 6261.23 781.275 8 -4 4 -7 7834.98 872.549 20 -4 -4 -7 7240.34 699.295 1 -4 -4 -7 6701.86 720.200 13 4 -4 7 7027.47 734.317 6 -4 -4 -7 8013.60 1068.32 2 -4 4 -7 8037.72 1001.52 11 -4 4 -7 7791.09 619.046 1 4 -4 8 183.626 193.969 6 -4 4 -8 514.266 310.779 20 -4 -4 -8 606.568 467.209 21 -4 4 -8 883.150 459.741 21 -4 -4 -8 1346.47 631.170 2 -4 -4 -8 668.976 473.482 20 4 4 8 158.888 179.340 10 4 -4 8 1064.55 466.112 3 4 4 8 445.832 302.299 5 -4 4 -8 245.706 153.951 1 -4 -4 -8-205.376 439.638 17 -4 4 -8 919.626 549.947 17 4 -4 8 726.653 394.534 16 -4 4 -8 302.399 241.221 8 -4 -4 -8 334.717 188.252 7 -4 4 -8 779.640 494.028 2 -4 -4 -8 569.956 281.393 13 -4 -4 -8 118.581 203.179 1 -4 4 -8-5.29123 366.830 11 -4 -4 -9 2578.44 858.354 20 -4 4 -9 3636.96 793.816 2 4 4 9 2789.57 483.251 10 -4 4 -9 2631.84 437.271 1 4 -4 9 2767.46 625.465 3 4 4 9 3531.11 586.110 5 4 4 9 3266.51 602.018 3 -4 -4 -9 3499.93 702.416 17 -4 -4 -9 2719.75 803.950 21 4 -4 9 3520.65 700.085 16 4 4 9 2755.13 574.964 16 -4 4 -9 3909.02 633.109 8 -4 4 -9 2851.23 693.564 21 -4 -4 -9 2795.91 496.793 13 -4 -4 -9 3032.89 501.410 1 -4 4 -9 2739.46 580.951 20 -4 4 -9 2060.69 678.946 17 -4 4 -9 2735.88 602.878 11 -4 -4 -9 3940.83 933.209 2 4 -4 9 2632.25 466.682 6 -4 4 -10 31504.0 2384.97 21 4 4 10 31788.6 1993.13 3 4 4 10 32207.4 1705.33 10 4 4 10 29259.3 1642.45 5 -4 4 -10 33378.5 2148.57 20 -4 -4 -10 31137.2 2776.94 20 -4 4 -10 30837.0 1676.56 1 -4 -4 -10 35362.6 2429.42 17 -4 4 -10 32846.3 2546.85 17 -4 4 -10 32708.2 1886.91 8 4 -4 10 28446.4 2215.80 16 4 4 10 30767.1 2024.81 16 -4 -4 -10 31574.8 2695.64 2 -4 4 -10 31012.1 2366.53 2 -4 -4 -10 31704.2 1780.27 1 -4 -4 -10 30238.7 1698.94 13 -4 -4 -10 31561.9 2716.26 21 4 -4 10 31378.1 1692.88 6 4 -4 10 32607.3 2157.19 3 -4 -4 -11 14090.8 1922.50 2 -4 4 -11 13110.3 1615.18 2 4 4 11 15788.0 1176.62 10 -4 -4 -11 13476.0 1846.04 21 -4 4 -11 15130.9 1528.74 20 -4 -4 -11 14434.8 1933.39 20 4 4 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4198.94 8 4 10 -3 114935. 4161.77 19 -4 10 3 109526. 3973.74 4 -4 -10 3 112677. 3807.76 21 4 -10 -3 111604. 4593.33 15 -4 -10 3 112328. 5105.22 7 -4 -10 3 109922. 3945.96 14 4 -10 -3 112374. 3694.83 14 -4 -10 3 122566. 4563.66 20 -4 -10 3 115530. 4539.65 13 -4 -10 3 114274. 3817.55 2 4 10 -3 108748. 4480.10 10 4 -10 -3 108853. 5034.89 12 4 -10 -3 106409. 4915.23 6 -4 10 3 115335. 4156.36 11 -4 -10 2 4560.75 604.544 21 -4 -10 2 5053.30 865.354 20 4 10 -2 5030.66 710.317 19 4 10 -2 5126.91 870.283 10 -4 10 2 5843.87 976.291 19 -4 -10 2 4490.49 570.930 18 -4 10 2 4821.00 721.109 11 4 10 -2 5197.76 1076.38 5 4 10 -2 5329.67 534.031 17 4 -10 -2 5376.91 655.319 9 -4 -10 2 5088.76 676.174 9 -4 -10 2 5073.38 625.542 2 -4 10 2 4699.02 732.254 8 4 -10 -2 5294.41 899.904 15 -4 10 2 4281.85 639.748 4 -4 -10 2 5869.10 725.709 14 4 -10 -2 4708.00 585.602 14 -4 -10 2 4824.40 989.559 7 -4 -10 2 5180.59 847.857 13 4 -10 -2 5265.95 940.319 12 4 -10 -2 3888.49 759.286 6 -4 10 1 718.111 381.456 11 -4 -10 1 953.621 339.678 21 -4 -10 1 1654.21 629.753 20 4 10 -1 379.504 246.172 19 4 10 -1 616.640 430.957 10 -4 10 1 660.862 451.461 19 -4 -10 1 687.985 297.286 2 4 10 -1 547.919 452.766 5 -4 -10 1 441.301 242.907 9 4 -10 -1 17.8492 215.762 9 4 -10 -1 526.975 185.690 16 -4 10 1 692.201 465.729 8 4 -10 -1 58.0086 341.393 15 -4 10 1 191.413 263.003 4 4 -10 -1 311.540 212.044 14 -4 -10 1 158.371 208.316 14 -4 -10 1 1121.74 567.976 7 -4 -10 1 834.693 399.880 13 4 -10 -1 715.974 358.616 12 4 10 -1 525.986 292.625 11 4 -10 -1-922.153 689.132 6 -4 10 0 53.3942 296.390 11 -4 10 0 290.920 182.371 21 4 10 0 4.65458 261.641 19 4 10 0-220.565 328.466 10 -4 -10 0 314.252 284.227 21 -4 -10 0 164.704 217.659 2 4 10 0 404.579 480.578 5 -4 -10 0 102.143 194.024 9 4 -10 0 374.389 273.596 9 -4 10 0-494.530 442.712 19 4 -10 0-31.6704 158.861 16 -4 10 0 139.240 154.957 2 -4 10 0 1393.70 598.609 8 4 -10 0-333.246 367.384 15 -4 10 0 130.140 244.342 4 4 -10 0 144.432 216.036 14 -4 -10 0-151.373 287.381 14 -4 -10 0 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2458.91 587.101 5 -5 -4 -3 2981.95 605.648 2 5 -4 3 2203.86 392.889 3 -5 4 -3 2321.47 460.042 2 5 -4 3 1829.28 402.494 6 -5 4 -3 3040.18 573.099 8 -5 -4 -3 3089.17 531.298 13 5 -4 4 73939.1 2742.32 3 5 -4 4 68927.9 2965.48 10 5 4 4 68433.0 2790.06 10 -5 -4 -4 74500.2 3248.41 21 5 4 4 70275.6 3111.07 5 -5 4 -4 73891.4 3014.05 8 5 -4 4 77113.5 2978.39 16 -5 -4 -4 72752.1 3204.21 2 -5 4 -4 70823.5 2944.40 2 -5 -4 -4 74665.2 2891.98 13 5 -4 4 69778.4 2876.06 6 -5 -4 -4 71086.6 3647.44 20 -5 4 -4 74576.7 3010.19 21 -5 4 -4 70562.8 2909.79 11 5 -4 5 877.851 321.869 6 -5 -4 -5 329.380 358.531 21 -5 4 -5 575.954 332.423 21 -5 -4 -5 1150.33 656.061 20 5 -4 5 1359.07 416.577 10 5 4 5 667.310 288.796 10 -5 -4 -5 815.061 388.800 2 5 4 5 957.344 432.868 5 -5 4 -5 770.823 429.373 2 5 -4 5 1034.66 322.364 3 -5 4 -5 1598.62 555.118 20 5 -4 5 416.809 267.804 16 -5 4 -5 1274.75 413.471 8 -5 -4 -5 769.453 293.825 13 -5 4 -5 1451.97 444.753 11 5 -4 6 4790.93 638.695 6 -5 -4 -6 5360.13 876.382 21 -5 4 -6 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21 7 10 10 232.640 280.905 10 7 10 10-354.954 410.671 5 7 -10 10-326.373 342.839 16 -7 10 -10 186.922 355.964 8 -7 -10 -10-99.6772 379.691 13 -7 10 -10 354.857 497.348 11 7 -10 11 1332.58 635.551 16 7 10 11 1215.47 614.657 16 7 11 -11 4188.65 1014.35 10 7 11 -11 6187.87 1201.66 17 -7 -11 11 6203.05 1240.28 13 7 11 -10 1206.36 583.887 10 -7 -11 10 1365.07 561.441 13 7 -11 -10 2510.55 1030.02 6 7 11 -9 1746.98 660.062 10 7 11 -9 3676.38 960.968 5 -7 11 9 2250.06 704.201 4 -7 -11 9 1524.06 669.929 13 7 -11 -9 4105.60 1213.43 12 7 -11 -9 3022.97 920.666 6 7 11 -8 19272.2 2137.55 5 7 11 -8 16337.7 1884.45 10 -7 -11 8 18634.3 1803.42 18 -7 11 8 19150.0 1920.25 4 7 -11 -8 18858.2 2143.59 15 -7 -11 8 18157.3 2207.57 7 -7 -11 8 19347.5 1986.78 13 7 -11 -8 20102.7 2732.44 12 -7 11 8 20421.7 1818.01 11 7 -11 -8 18618.8 2283.51 6 -7 11 7 108.779 389.658 11 7 11 -7-236.568 504.362 10 7 11 -7 516.526 719.767 5 -7 -11 7 158.246 325.270 18 7 -11 -7 130.287 405.497 15 -7 11 7 214.538 360.321 4 -7 -11 7 591.437 652.217 7 -7 -11 7 259.171 329.313 13 7 -11 -7 787.975 803.751 12 7 -11 -7-667.740 566.399 6 7 11 -6 39123.8 3149.49 5 7 11 -6 35455.6 2714.99 10 -7 -11 6 36159.7 2450.23 18 -7 11 6 37087.3 2627.81 4 7 -11 -6 38292.4 2974.75 15 -7 -11 6 38511.5 3164.40 7 -7 -11 6 35431.5 2659.99 13 7 -11 -6 33873.5 3332.30 12 7 -11 -6 35347.4 3019.51 6 -7 11 6 33955.6 2355.55 11 -7 11 5 2243.07 614.724 11 -7 -11 5 2174.20 786.999 20 7 11 -5 2121.51 673.554 10 7 11 -5 2349.45 879.624 5 -7 11 5 1485.67 448.800 18 -7 -11 5 3326.39 746.610 18 7 -11 -5 3084.92 909.042 15 -7 11 5 3042.83 799.269 4 -7 -11 5 2224.88 848.412 7 -7 -11 5 2972.31 853.299 13 7 -11 -5 2529.46 983.634 12 7 -11 -5 1502.68 680.695 6 -7 11 4 5784.88 957.051 11 -7 -11 4 4905.00 1059.72 20 7 11 -4 6746.86 1113.02 10 7 11 -4 4019.27 1027.99 5 7 -11 -4 8240.85 1388.30 15 -7 11 4 5288.16 968.701 4 -7 11 4 5356.57 817.914 13 -7 -11 4 4864.55 1111.49 7 -7 -11 4 6398.18 1142.59 13 7 -11 -4 5250.13 1254.31 12 7 -11 -4 4232.20 1042.51 6 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801.592 13 -8 -4 1 5432.86 821.930 13 -8 -4 0 87398.4 4097.58 21 -8 4 0 82033.8 3852.31 21 8 -4 0 86715.0 3869.98 10 8 4 0 91133.0 3915.06 10 -8 -4 0 88797.1 4850.43 20 8 4 0 86404.3 4278.78 5 -8 4 0 90131.5 3803.16 13 -8 -4 0 91338.3 3874.42 13 -8 -4 0 88952.8 4120.70 2 -8 4 0 87632.5 3935.92 2 8 -4 0 88962.6 4062.97 6 -8 4 0 91303.1 3431.84 11 8 -4 1 2446.91 650.746 6 -8 -4 -1 2275.85 647.860 21 -8 4 -1 3097.28 673.327 21 -8 -4 -1 2413.64 931.504 20 8 -4 1 1584.56 474.997 10 8 4 1 1955.39 559.369 10 8 4 1 1642.50 557.049 5 -8 -4 -1 1931.35 573.935 2 -8 4 -1 1730.04 576.156 2 -8 4 -1 1769.02 545.953 13 -8 -4 -1 1853.25 534.882 13 8 -4 2 1000.80 493.166 6 -8 -4 -2-41.7055 463.974 21 -8 4 -2 976.839 437.779 21 -8 -4 -2 818.775 656.319 20 8 -4 2 502.553 350.330 10 8 4 2 700.790 415.261 10 8 4 2 443.292 381.566 5 -8 -4 -2 1171.08 535.967 2 -8 4 -2 994.844 485.429 2 -8 4 -2 548.862 316.274 13 -8 -4 -2 317.434 343.197 13 8 -4 3 5553.53 913.820 6 -8 -4 -3 6357.37 1119.76 21 -8 4 -3 6470.81 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7168.52 1084.39 6 8 -5 7 3987.04 832.630 10 -8 -5 -7 5222.72 1108.70 21 -8 5 -7 5771.29 1051.56 21 -8 5 -7 4383.57 913.230 20 -8 -5 -7 5248.29 1289.09 20 8 5 7 5718.55 935.214 10 -8 -5 -7 4331.69 991.463 2 -8 5 -7 4847.96 991.649 2 8 5 7 6654.31 1045.45 5 8 -5 7 4419.75 764.650 3 8 -5 7 4746.40 933.427 16 -8 5 -7 4242.10 872.065 13 -8 -5 -7 5071.77 888.405 13 -8 -5 -8 23531.6 2370.54 21 -8 5 -8 24238.4 2186.06 21 8 5 8 23642.2 1904.51 10 8 5 8 25872.5 2097.40 5 -8 5 -8 23051.9 2149.88 20 -8 -5 -8 27139.4 2830.25 20 8 -5 8 23829.9 2144.61 16 -8 -5 -8 27068.2 2530.88 2 -8 5 -8 24391.1 2161.23 2 -8 5 -8 23540.2 2104.70 13 -8 -5 -8 25565.8 2028.88 13 8 -5 8 24284.7 1973.06 6 8 -5 8 24358.7 1977.84 3 8 -5 9 3887.18 815.944 6 -8 -5 -9 2812.41 992.334 21 -8 5 -9 1024.87 493.596 21 -8 5 -9 2324.19 727.760 20 -8 -5 -9 667.623 545.580 20 -8 -5 -9 288.452 573.820 2 8 5 9 1945.63 609.083 10 -8 5 -9 1758.82 638.483 2 8 5 9 2032.46 647.130 5 8 -5 9 2545.69 710.557 3 8 -5 9 2119.05 724.359 16 -8 5 -9 1377.33 561.920 13 -8 -5 -9 2871.26 686.082 13 -8 -5 -10 10604.9 1743.11 21 -8 5 -10 9713.90 1510.58 21 -8 -5 -10 12196.3 1858.81 2 -8 -5 -10 8712.26 1676.75 20 -8 5 -10 8047.74 1327.54 2 8 5 10 10720.6 1317.24 10 8 -5 10 8211.47 1257.93 3 8 5 10 10365.3 1389.55 3 -8 5 -10 9385.87 1598.10 17 8 -5 10 11800.0 1612.66 16 8 5 10 12021.1 1531.44 16 -8 5 -10 8484.45 1300.17 13 -8 -5 -10 8628.19 1224.42 13 -8 5 -11 11534.2 1667.87 21 8 5 11 14868.9 1599.62 10 -8 5 -11 11643.2 1686.28 2 8 -5 11 13356.1 1645.39 3 -8 -5 -11 12723.4 1489.14 13 8 5 12 9236.99 1252.73 10 8 -5 12 7881.77 1347.81 3 -8 -5 -12 10487.8 1372.54 13 -8 6 11 1796.17 668.758 11 -8 6 11 3459.44 898.792 18 8 -6 -11 2864.94 824.807 15 8 6 -11 1574.04 712.239 12 8 -6 -10 908.059 497.802 6 -8 6 10 681.809 411.340 11 8 6 -10 730.023 420.406 5 -8 6 10 1999.54 741.903 18 -8 -6 10 1026.66 552.959 18 8 -6 -10 1683.64 749.190 15 -8 6 10 1494.26 659.685 4 -8 -6 10 2189.47 670.916 7 8 6 -10 1437.14 666.209 12 8 6 -9 16217.9 1600.41 10 8 6 -9 14410.2 1784.89 5 -8 6 9 18152.7 1840.97 18 -8 -6 9 16620.1 1869.03 18 8 -6 -9 17480.2 1887.45 15 -8 -6 9 15565.4 1811.92 7 -8 6 9 17669.4 1865.71 4 -8 -6 9 17135.8 1668.58 13 8 6 -9 15370.4 1835.72 12 8 -6 -9 19002.3 2005.04 6 8 -6 -9 16957.7 2400.62 12 -8 6 9 16111.5 1568.35 11 8 -6 -8 897.168 471.168 6 -8 6 8 243.008 334.841 11 8 6 -8 348.802 286.442 10 8 6 -8 432.498 335.102 5 -8 6 8 666.621 495.240 18 -8 -6 8 1230.03 685.031 18 8 -6 -8 104.964 415.151 15 -8 6 8 637.330 518.157 4 -8 -6 8 546.949 525.211 7 -8 -6 8-437.952 442.538 13 8 -6 -8 690.559 691.231 12 8 6 -8 877.829 564.526 12 8 -6 -7 5890.46 1107.19 6 -8 6 7 3731.26 714.682 11 8 6 -7 4716.08 846.341 10 8 6 -7 4756.69 1073.14 5 -8 6 7 4233.98 876.850 18 -8 -6 7 6199.79 1078.62 18 8 -6 -7 5350.39 1050.85 15 -8 6 7 4076.08 843.437 4 -8 -6 7 5116.00 1036.29 7 -8 -6 7 5127.26 873.544 13 8 -6 -7 3121.99 903.901 12 8 6 -7 6309.20 1160.66 12 8 -6 -6 1142.07 527.720 6 -8 6 6 1965.23 536.233 11 8 6 -6 2314.65 640.827 10 8 6 -6 1912.97 765.692 5 -8 6 6 2552.72 651.919 18 -8 -6 6 2091.45 639.278 18 8 -6 -6 1567.42 622.777 15 -8 6 6 1962.95 589.192 4 -8 -6 6 2784.41 779.519 7 -8 -6 6 1213.88 496.714 13 8 -6 -6 558.273 578.651 12 8 -6 -5 1546.57 533.384 6 -8 6 5 1673.77 461.677 11 -8 -6 5 1465.77 547.812 21 8 -6 -5 1332.36 459.968 10 8 6 -5 2217.85 619.921 10 8 6 -5 1841.03 697.857 5 -8 6 5 2567.99 633.396 18 -8 -6 5 1960.83 620.603 18 -8 -6 5 2004.93 663.117 7 8 -6 -5 1963.06 622.497 15 -8 6 5 2756.26 755.344 4 -8 6 5 1983.44 488.804 13 -8 -6 5 1725.69 567.149 13 8 -6 -5 1846.74 722.443 12 8 -6 -4 482.488 470.967 6 -8 6 4 776.449 280.340 11 -8 -6 4 551.657 425.516 21 8 -6 -4-264.726 487.648 10 8 6 -4 385.040 420.266 10 8 6 -4 378.432 440.884 5 -8 6 4 524.593 317.809 18 -8 -6 4 2.13041 341.025 18 -8 -6 4 509.295 470.711 2 -8 -6 4 1356.97 584.978 7 8 -6 -4 15.2011 442.310 15 -8 6 4 778.647 520.992 4 -8 6 4 313.727 331.017 13 -8 -6 4 485.229 388.189 13 8 -6 -4 394.165 522.766 12 -8 -6 3 24150.8 1995.42 21 8 -6 -3 19134.1 1664.44 10 8 6 -3 20140.5 2118.11 5 8 6 -3 19662.3 1730.32 10 -8 6 3 20726.9 1698.36 18 -8 -6 3 20029.5 1755.36 18 -8 6 3 20225.8 1839.55 4 8 -6 -3 22517.5 2057.71 15 -8 6 3 21670.9 1608.55 13 -8 -6 3 22851.9 1851.11 13 -8 -6 3 21359.2 1866.11 2 8 -6 -3 22806.6 2005.24 6 8 -6 -3 16753.0 2048.32 12 -8 6 3 22178.8 1604.27 11 -8 6 2 562.527 371.055 11 8 -6 -2-268.779 482.307 6 -8 -6 2 826.154 435.585 21 -8 6 2 274.322 396.882 21 -8 -6 2 1258.99 801.595 20 8 -6 -2 557.909 368.676 10 8 6 -2 383.056 423.822 10 8 6 -2 132.499 387.421 5 -8 -6 2-154.296 369.108 2 8 -6 -2 275.549 327.130 15 -8 6 2 251.910 340.449 4 -8 6 2 609.997 388.444 13 -8 -6 2-190.206 396.537 13 8 -6 -2 17.5459 451.842 12 8 -6 -1 10842.1 1335.74 6 -8 -6 1 11067.8 1346.44 21 -8 6 1 9546.87 1159.16 21 -8 -6 1 10831.6 1678.94 20 8 -6 -1 9017.68 1154.05 10 8 6 -1 11467.9 1282.78 10 8 6 -1 10835.7 1499.39 5 -8 6 1 10976.1 1243.78 2 8 -6 -1 10905.0 1423.56 15 -8 6 1 10075.7 1271.84 4 -8 6 1 11536.9 1233.21 13 -8 -6 1 12539.4 1432.73 2 -8 -6 1 11929.5 1330.34 13 8 -6 -1 11868.8 1631.43 12 -8 6 1 10127.3 1067.00 11 -8 6 0 6990.32 904.052 11 8 -6 0 7511.78 1097.82 6 -8 -6 0 8027.03 1161.94 21 -8 6 0 7071.40 1000.74 21 -8 -6 0 7235.26 1362.88 20 8 -6 0 5391.89 894.271 10 8 6 0 7293.71 1026.59 10 8 6 0 9713.86 1420.93 5 -8 -6 0 6500.59 1057.19 2 -8 6 0 6910.56 996.938 2 8 -6 0 6690.87 1143.92 15 -8 6 0 7314.04 1005.54 13 -8 -6 0 8040.74 1079.30 13 8 -6 0 6548.71 1209.60 12 -8 6 -1 5234.19 791.323 11 8 -6 1 3615.83 794.379 6 -8 -6 -1 3527.93 786.466 21 -8 6 -1 5322.29 881.158 21 -8 -6 -1 5067.47 1132.66 20 8 -6 1 3668.59 750.127 10 8 6 1 3609.74 749.621 10 8 6 1 5267.16 1049.79 5 -8 -6 -1 6311.53 1030.32 2 -8 6 -1 4980.04 856.424 2 8 -6 1 4062.75 943.686 15 -8 6 -1 5050.39 835.287 13 -8 -6 -1 3867.73 777.137 13 -8 6 -2 922.823 407.588 11 8 -6 2 246.837 328.543 6 -8 -6 -2 1001.23 528.268 21 -8 6 -2 37.9424 372.521 21 -8 -6 -2 775.558 648.221 20 8 -6 2 911.716 440.678 10 8 6 2 392.309 299.250 10 8 6 2 925.912 618.858 5 -8 -6 -2 412.230 434.141 2 -8 6 -2 745.020 464.903 2 -8 6 -2 839.195 504.499 13 -8 -6 -2 1711.70 597.551 13 -8 -6 -3 51109.6 3206.02 21 -8 6 -3 51013.6 2931.70 21 8 -6 3 51302.0 3023.91 10 8 6 3 51785.9 2879.45 10 -8 -6 -3 54015.8 3881.80 20 8 6 3 50459.3 3207.15 5 8 -6 3 53504.2 2835.28 16 -8 -6 -3 53599.9 3256.26 2 -8 6 -3 52256.5 2990.02 13 -8 6 -3 49840.6 2882.62 2 -8 -6 -3 54968.6 2964.31 13 8 -6 3 49409.7 2986.82 6 -8 6 -3 53720.8 2794.02 11 8 -6 4 71.1360 268.766 6 -8 -6 -4-99.4500 396.357 21 -8 6 -4 617.924 431.285 21 -8 -6 -4 1383.15 819.652 20 8 -6 4-470.069 394.355 10 8 6 4 7.25331 293.993 10 8 6 4 768.536 510.465 5 -8 -6 -4 152.834 334.141 2 -8 6 -4 556.004 452.175 2 8 -6 4 482.712 378.273 16 -8 6 -4-268.471 415.174 13 -8 -6 -4-51.0116 365.701 13 -8 6 -5 14714.7 1522.91 21 8 -6 5 13761.8 1529.52 10 -8 -6 -5 14888.3 1745.35 21 8 6 5 13789.0 1431.70 10 -8 6 -5 16378.5 1724.96 20 8 6 5 16297.5 1732.89 5 -8 -6 -5 14420.1 2069.45 20 8 -6 5 15042.6 1552.92 16 -8 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5 8 -6 8-281.972 392.174 16 -8 6 -8 412.334 324.924 13 -8 -6 -8 20.2738 387.356 13 -8 -6 -9 59783.5 4142.67 21 -8 6 -9 52863.6 3433.77 21 8 6 9 57906.5 3183.22 10 8 6 9 57515.1 3306.84 5 -8 -6 -9 51222.3 4151.20 20 8 -6 9 58059.5 3606.10 16 -8 -6 -9 56559.5 4030.23 2 -8 6 -9 56100.1 3507.75 2 -8 6 -9 54925.2 3473.34 13 -8 -6 -9 59220.5 3305.37 13 8 -6 9 55614.9 3208.38 6 8 -6 9 55134.5 3244.88 3 -8 -6 -10 672.384 736.348 21 -8 6 -10 1290.78 617.476 21 -8 -6 -10 798.170 762.411 2 -8 6 -10 1624.60 779.019 2 8 6 10 199.554 257.570 10 8 -6 10 113.402 328.947 3 -8 6 -10 477.231 438.276 17 8 -6 10 344.399 336.945 16 8 6 10 946.325 523.218 16 -8 6 -10 237.517 472.120 13 -8 -6 -10-59.8942 372.165 13 -8 6 -11 1249.67 648.434 21 -8 6 -11 572.139 523.068 2 8 6 11 330.997 361.509 10 8 -6 11 57.1277 407.971 3 -8 -6 -11 851.056 405.780 13 8 6 12 1686.25 649.579 10 8 -6 12 1273.22 658.185 3 8 7 -12 145.328 490.145 1 8 7 -11 12290.4 1667.96 1 8 -7 -10 6583.82 1263.58 6 -8 7 10 7707.23 1130.89 11 8 7 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1728.42 515.145 4 -8 -7 7 1930.99 567.592 7 -8 -7 7 3073.13 746.030 13 8 -7 -7 1003.35 532.101 12 8 7 -7 2937.59 881.057 12 8 -7 -6 285.930 494.615 6 -8 7 6 143.912 270.219 11 -8 -7 6-335.545 475.846 21 8 7 -6 108.559 413.431 10 8 7 -6 336.689 446.205 5 -8 7 6 25.9256 309.179 18 -8 -7 6-73.3680 328.712 18 8 -7 -6 360.748 449.813 15 -8 7 6-228.887 310.847 4 -8 -7 6 656.429 545.290 7 -8 -7 6 91.7240 336.421 13 8 -7 -6-253.761 536.919 12 -8 -7 5 18405.6 1814.19 21 8 7 -5 19054.8 2101.89 5 8 7 -5 20073.4 1792.92 10 -8 7 5 20324.5 1763.73 18 -8 -7 5 19342.6 1805.60 18 -8 7 5 19604.4 1872.37 4 8 -7 -5 20408.6 1982.72 15 -8 -7 5 23986.4 2152.63 7 -8 7 5 21080.4 1541.46 13 -8 -7 5 19752.8 1810.59 13 -8 -7 5 21405.4 1932.06 2 8 -7 -5 18328.5 1921.34 6 8 -7 -5 21509.0 2450.51 12 -8 7 5 20350.9 1624.61 11 8 -7 -4 5130.15 1026.05 6 -8 7 4 5606.09 849.575 11 -8 -7 4 5395.07 971.214 21 8 7 -4 5849.90 991.696 10 8 7 -4 6694.01 1312.26 5 -8 7 4 6251.79 978.739 18 -8 -7 4 7007.57 1078.25 18 -8 -7 4 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3348.81 6 -8 10 3 43318.9 2670.68 11 -8 10 2 2270.54 649.414 11 -8 -10 2 3594.95 822.737 21 -8 10 2 3176.86 709.822 21 -8 -10 2 2626.05 863.382 20 8 10 -2 2945.52 793.040 10 8 10 -2 1287.75 728.789 5 -8 -10 2 2314.31 641.242 2 -8 10 2 1707.46 548.571 2 8 -10 -2 2901.39 833.152 15 -8 10 2 2474.54 744.870 4 -8 -10 2 1826.25 661.999 7 -8 10 2 2246.24 634.076 13 -8 -10 2 2646.76 774.460 13 8 -10 -2 2509.63 890.158 12 8 -10 -2 2715.61 803.572 6 -8 10 1 13958.5 1413.90 21 -8 -10 1 13508.7 1595.75 21 8 10 -1 15670.5 1675.86 10 -8 -10 1 10698.3 1694.66 20 8 10 -1 15251.2 1475.45 19 8 10 -1 12969.8 1916.31 5 -8 -10 1 14102.4 1607.82 2 -8 10 1 13749.1 1543.64 4 8 -10 -1 14832.3 1826.14 15 -8 -10 1 13550.6 1754.01 7 -8 10 1 12539.3 1418.49 13 -8 10 1 14790.2 1446.51 2 -8 -10 1 14805.0 1636.61 13 8 -10 -1 14452.3 1900.33 12 -8 10 1 13832.9 1435.09 11 8 -10 -1 13204.1 1702.42 6 -8 10 0 4453.15 846.701 11 -8 -10 0 5494.69 1103.17 21 -8 10 0 3728.51 738.779 21 -8 -10 0 5638.73 1330.65 20 8 10 0 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5-555.226 556.374 6 -8 -10 -6 335.750 573.459 21 -8 -10 -6-314.224 761.349 20 -8 -10 -6 73.9031 460.650 2 8 10 6 232.876 358.038 10 8 10 6-363.662 518.981 5 -8 10 -6 1856.53 856.088 8 -8 -10 -6 541.291 468.070 13 -8 10 -6-355.990 570.492 11 8 -10 6 732.505 533.208 6 -8 -10 -7 24616.6 2704.15 21 8 10 7 22362.3 1980.87 10 8 10 7 25880.8 2466.52 5 8 -10 7 23227.8 2179.64 16 -8 -10 -7 25795.8 2736.54 2 -8 -10 -7 22787.8 2099.87 13 8 -10 7 23691.4 2263.48 6 -8 -10 -8 615.176 688.518 21 -8 -10 -8 388.962 640.943 2 8 10 8-97.7057 350.418 10 8 10 8 836.606 580.290 5 8 -10 8 747.646 520.622 16 -8 -10 -8 718.212 461.852 13 8 -10 8-475.321 473.236 6 8 10 9 2266.98 755.362 5 8 -10 9 3971.59 1038.38 16 8 11 -8 38877.1 3241.56 5 8 11 -7 1317.22 817.357 5 -8 11 6 1636.55 597.409 11 8 11 -6 2567.35 788.992 10 8 11 -6 1428.65 818.275 5 -8 -11 6 3385.31 954.517 13 8 -11 -6 1983.72 1140.87 12 8 -11 -6 214.903 516.852 6 -8 11 5 5686.81 995.612 11 -8 -11 5 7574.45 1342.77 20 8 11 -5 6999.57 1266.56 10 8 11 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5567.82 1173.23 2 8 11 4 8658.08 1575.67 5 -8 11 -4 8416.07 1420.87 8 8 -11 4 8125.12 1427.74 15 -8 -11 -4 9277.62 1530.46 7 -8 -11 -4 7615.77 1219.18 13 8 -11 4 8655.74 1384.93 6 -8 11 -4 6441.07 1190.02 11 -8 -11 -5 5745.66 1178.80 21 -8 -11 -5 5729.34 1546.35 20 -8 -11 -5 4625.61 1109.13 2 8 11 5 6174.25 1062.18 10 8 11 5 8264.33 1559.70 5 8 -11 5 6316.34 1265.22 15 -8 -11 -5 5456.86 1083.61 13 8 -11 5 5736.78 1137.39 6 -8 11 -5 6292.58 1212.69 11 -8 -11 -6 4574.47 1217.64 21 -8 -11 -6 3830.90 1105.62 2 8 11 6 3948.81 845.503 10 8 11 6 4627.78 1146.96 5 -8 -11 -6 4392.17 1000.04 13 8 -11 6 4033.74 962.027 6 -8 11 -6 3201.15 835.992 11 -8 -11 -7 3488.05 1174.77 21 -8 -11 -7 4397.95 1217.85 2 -8 11 -7 4046.22 1017.40 11 8 -11 7 4025.58 906.801 6 -8 -11 -8 9546.27 1841.36 21 -8 -11 -8 10939.3 1964.41 2 8 -11 8 8543.70 1406.55 6 8 -12 -5-457.664 443.083 12 -8 12 4 6050.01 1047.10 11 -8 12 4 8252.00 1290.36 4 8 -12 -4 6076.97 1376.40 12 -8 12 3 1935.98 622.795 11 -8 -12 3 2810.28 940.737 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2 951.076 575.781 11 -8 -13 2 659.380 566.545 20 -8 13 2 756.729 508.107 13 -8 13 1 4042.37 985.155 11 -8 -13 1 3740.79 1098.48 20 8 13 -1 4253.17 862.996 19 -8 13 0 403.994 402.178 11 -8 -13 0 897.166 675.232 20 8 13 0 665.630 542.655 19 -8 -13 0-170.962 506.570 7 -8 -13 -1 18903.5 2432.07 20 8 13 1 20815.2 1968.89 19 -8 -13 -1 21495.8 2476.68 7 -8 13 -1 19459.2 1955.73 11 -8 -13 -2 3607.37 1193.60 20 8 13 2 4384.05 893.179 19 -8 13 -2 2779.51 877.613 19 -8 -13 -2 2690.39 932.135 7 -8 13 -2 4394.75 957.917 11 -8 -13 -3 27.8801 560.329 20 -8 13 -3 200.567 507.152 19 -8 -13 -3 275.505 552.786 7 -8 13 -3 627.116 548.282 11 -8 13 -4 1857.22 870.761 11 8 14 -1 3502.60 861.769 19 -8 -14 0 256.023 665.831 20 8 14 0-109.927 401.039 19 -8 -14 -1 19172.3 2478.57 20 -8 14 -2 15395.9 2005.72 19 9 0 -10-144.458 407.115 6 -9 0 10 26.8811 457.844 4 9 0 -9-513.757 495.995 6 -9 0 9-143.269 451.506 4 9 0 -9-711.571 842.487 12 -9 0 8 35301.0 2709.80 18 -9 0 8 32549.0 2586.89 4 9 0 -8 32261.3 3006.29 12 9 0 -8 33748.8 2611.26 6 9 0 -7-506.881 534.457 6 -9 0 7 34.4043 326.005 18 -9 0 7 293.130 521.908 4 9 0 -7 1138.88 709.874 12 9 0 -6 1917.52 627.501 6 9 0 -6 599.677 279.221 10 -9 0 6 151.680 339.743 18 9 0 -6 1164.54 514.561 15 -9 0 6 1039.40 544.147 4 -9 0 6 1163.07 489.554 13 9 0 -6 1793.36 886.706 12 9 0 -5-419.360 446.827 6 9 0 -5-20.9012 418.366 10 -9 0 5 657.403 394.047 18 9 0 -5-109.774 316.195 15 -9 0 5-393.905 379.840 4 -9 0 5-355.142 369.069 13 9 0 -5-34.0836 461.403 12 9 0 -4 16.5068 357.960 6 -9 0 4-739.849 446.369 21 9 0 -4 88.8481 293.415 10 -9 0 4 778.567 536.986 18 9 0 -4 790.806 394.085 15 -9 0 4 468.867 465.880 4 -9 0 4-309.159 376.464 13 9 0 -3 16.1913 397.526 6 -9 0 3-197.080 371.150 21 9 0 -3-68.3324 348.791 10 -9 0 3 311.376 436.943 18 -9 0 3 149.393 434.198 2 9 0 -3 195.972 305.895 15 -9 0 3 879.073 539.258 4 -9 0 3 14.6534 286.679 13 -9 0 2 26228.3 2159.60 21 9 0 -2 25461.1 1985.84 10 9 0 -2 26912.5 2106.95 15 -9 0 2 26243.0 1915.61 13 -9 0 2 26064.7 2150.07 2 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360.147 13 -9 0 -6 29233.7 2543.02 21 9 0 6 30984.2 2199.57 3 9 0 6 25818.4 2160.82 10 -9 0 -6 28951.4 2718.25 20 -9 0 -6 31057.8 2591.19 2 -9 0 -6 28194.5 2218.17 13 9 0 6 30374.6 2208.84 6 9 0 7 666.135 430.870 6 -9 0 -7 550.697 509.964 21 -9 0 -7 208.996 606.683 20 9 0 7 80.8254 404.793 10 -9 0 -7 798.642 504.357 2 9 0 7-78.1181 274.490 3 -9 0 -7 586.634 416.112 13 9 0 8 9626.19 1232.35 6 -9 0 -8 8120.31 1406.45 21 -9 0 -8 10858.0 1741.35 20 9 0 8 11245.0 1425.55 10 -9 0 -8 12203.5 1704.08 2 9 0 8 10060.5 1345.22 3 9 0 8 11127.6 1461.22 16 -9 0 -8 8344.72 1245.78 13 9 0 9-298.422 332.628 10 9 0 9-89.3492 442.313 3 9 0 10 46054.9 3111.61 3 -9 0 -10 46259.2 3648.58 20 -9 0 -10 46700.4 3418.05 17 9 -1 -10 13689.1 1697.25 6 9 1 -10 12257.6 1585.89 6 -9 -1 10 11449.1 1587.97 4 -9 1 10 13924.3 1814.11 4 9 -1 -9 6541.54 1127.30 6 9 1 -9 6068.63 1110.63 6 -9 -1 9 7965.79 1322.34 4 -9 1 9 4402.63 977.617 4 9 1 -9 6219.31 1262.16 12 9 -1 -8 3838.24 927.309 6 9 1 -8 3408.30 829.682 6 -9 1 8 3412.85 866.284 18 -9 -1 8 4572.06 1062.00 18 9 -1 -8 3226.40 749.479 15 -9 -1 8 5083.78 1064.60 4 -9 1 8 5478.82 1091.22 4 9 -1 -8 4217.32 1205.22 12 9 1 -8 3994.91 1095.19 12 9 -1 -7 7835.23 1222.05 6 9 1 -7 8928.00 1322.42 6 9 1 -7 6610.26 960.677 10 -9 1 7 8029.62 1210.07 18 -9 -1 7 7283.11 1194.76 18 9 -1 -7 7136.80 1077.99 15 -9 -1 7 7220.84 1187.47 4 -9 1 7 6913.57 1185.55 4 -9 -1 7 8519.34 1068.72 13 9 -1 -7 7862.01 1554.65 12 9 1 -7 7201.55 1438.84 12 9 -1 -6 7097.13 1144.92 6 9 1 -6 5525.49 1031.91 6 9 -1 -6 5767.56 899.078 10 9 1 -6 5966.53 937.721 10 -9 1 6 7261.93 1146.39 18 -9 -1 6 4606.20 926.478 18 9 -1 -6 4543.58 843.883 15 -9 -1 6 5965.50 1047.66 4 -9 1 6 5646.42 1031.73 4 -9 1 6 6034.59 886.748 13 -9 -1 6 6807.52 980.418 13 9 -1 -6 5470.70 1192.57 12 9 1 -6 5161.48 1169.97 12 9 -1 -5 2183.06 690.510 6 9 1 -5 821.795 390.915 6 9 -1 -5 1141.39 527.383 10 9 1 -5 1588.47 516.386 10 -9 1 5 1164.87 541.103 18 -9 -1 5 1531.05 549.785 18 9 -1 -5 1789.80 642.766 15 9 1 -5 1697.26 585.126 15 -9 -1 5 2005.69 648.085 4 -9 1 5 976.574 543.047 4 -9 1 5 922.086 399.968 13 -9 -1 5 1292.52 468.355 13 9 -1 -5 1275.76 669.590 12 9 1 -5 1312.69 695.470 12 -9 -1 4 20488.1 1969.06 21 9 -1 -4 20337.5 1716.18 10 9 1 -4 20254.1 1726.50 10 -9 1 4 19194.4 1851.22 18 -9 -1 4 20858.5 1895.31 18 -9 -1 4 19118.4 1832.53 4 -9 1 4 19841.4 1877.26 4 9 -1 -4 19785.4 1817.96 15 9 1 -4 17815.0 1633.59 15 -9 1 4 19565.6 1624.24 13 -9 -1 4 18757.6 1618.59 13 9 -1 -4 18374.2 2239.24 12 9 -1 -4 19320.9 1854.39 6 9 1 -4 22724.5 2043.26 6 9 -1 -3 2436.50 721.591 6 -9 -1 3 1737.92 621.247 21 -9 1 3 1992.74 624.724 21 9 -1 -3 1759.88 531.944 10 9 1 -3 1043.09 456.313 10 -9 -1 3 1276.22 489.402 18 -9 -1 3 2235.38 689.114 4 -9 -1 3 1531.73 625.408 2 -9 1 3 1752.82 626.211 2 9 -1 -3 1516.47 583.487 15 9 1 -3 1087.56 399.708 15 -9 1 3 1645.11 697.695 4 -9 1 3 2102.14 568.913 13 -9 -1 3 1475.69 434.393 13 9 -1 -2 488.598 352.528 6 9 1 -2-160.334 422.570 5 -9 -1 2-345.315 445.554 21 -9 1 2 748.872 406.248 21 9 -1 -2 57.8132 293.859 10 9 1 -2 179.760 353.441 10 -9 -1 2 195.907 423.405 2 -9 1 2-314.045 372.093 2 9 -1 -2 920.262 533.417 15 9 1 -2 1120.60 556.628 15 -9 1 2 450.444 363.413 13 -9 -1 2-153.755 346.309 13 -9 1 1 14865.1 1605.95 21 9 -1 -1 11340.8 1386.64 6 9 1 -1 12947.4 1562.88 5 -9 -1 1 13007.3 1509.20 21 9 -1 -1 11524.6 1327.77 10 9 1 -1 10962.5 1275.44 10 -9 -1 1 12921.4 1492.89 2 -9 1 1 12207.4 1434.03 2 9 -1 -1 15076.8 1626.42 15 -9 1 1 11108.8 1243.13 13 -9 -1 1 12686.3 1318.90 13 -9 -1 0 22287.9 2017.50 21 -9 1 0 25116.9 2093.00 21 9 1 0 24758.7 2156.76 5 9 -1 0 25370.3 1995.97 10 9 1 0 24257.5 1922.66 10 -9 1 0 25603.0 1898.39 13 -9 -1 0 25043.4 1900.15 13 -9 -1 0 25646.7 2117.18 2 -9 1 0 23069.8 1998.83 2 9 -1 0 26910.9 2136.68 6 9 -1 1 2952.25 741.305 6 -9 -1 -1 2913.04 726.149 21 -9 1 -1 2536.06 734.230 21 9 -1 1 2313.91 629.937 10 9 1 1 2456.63 642.737 10 9 1 1 3884.73 907.518 5 -9 -1 -1 2378.59 693.495 2 -9 1 -1 4297.78 925.555 2 -9 1 -1 3288.34 764.969 13 -9 -1 -1 3707.96 748.073 13 -9 -1 -2 20206.3 1933.45 21 -9 1 -2 19561.9 1865.51 21 9 -1 2 19338.2 1777.21 10 9 1 2 20579.8 1921.23 5 9 1 2 22835.8 1849.86 10 -9 -1 -2 19400.3 2220.68 20 -9 1 -2 19205.2 1707.32 13 -9 -1 -2 18101.3 1656.41 13 -9 -1 -2 19384.8 1905.19 2 -9 1 -2 19809.4 1872.37 2 9 -1 2 20114.8 1839.80 6 9 -1 3-91.2681 271.142 6 9 1 3 974.721 487.336 6 -9 -1 -3 777.047 426.130 21 -9 1 -3 762.717 459.288 21 -9 1 -3 1499.67 723.071 20 -9 -1 -3 736.125 619.665 20 9 -1 3 599.409 407.344 10 9 1 3 753.800 465.732 10 9 1 3 949.901 502.529 5 -9 -1 -3 1486.27 566.025 2 -9 1 -3-102.101 517.447 2 -9 1 -3 1234.14 555.076 13 -9 -1 -3 453.571 448.390 13 9 -1 4 2120.65 667.600 6 9 1 4 2273.61 706.224 6 -9 -1 -4 3034.96 884.495 21 -9 1 -4 2247.32 751.408 21 -9 1 -4 1990.80 694.773 20 -9 -1 -4 2671.43 945.552 20 9 -1 4 1551.63 613.175 10 9 1 4 1915.76 604.763 10 9 1 4 1257.24 512.179 5 -9 -1 -4 1236.02 587.400 2 -9 1 -4 3144.99 843.034 2 -9 1 -4 1314.59 531.147 13 -9 -1 -4 1585.25 572.795 13 -9 -1 -5 33563.6 2648.96 21 -9 1 -5 31769.6 2568.03 21 9 -1 5 34937.6 2242.49 3 9 -1 5 31971.8 2378.71 10 9 1 5 30742.0 2376.12 5 9 1 5 31864.5 2335.62 10 -9 1 -5 29057.1 2692.13 20 -9 -1 -5 32016.5 2876.90 20 -9 -1 -5 34303.8 2673.46 2 -9 1 -5 32552.4 2584.47 2 -9 1 -5 33131.6 2396.79 13 -9 -1 -5 32288.8 2337.50 13 9 -1 5 33184.0 2341.77 6 9 1 5 30451.4 2273.82 6 -9 -1 -6 19652.9 2047.88 21 -9 1 -6 18950.7 1978.86 21 9 -1 6 18858.6 1683.06 3 9 -1 6 19715.0 1870.98 10 9 1 6 17459.9 1727.31 5 9 1 6 17602.1 1753.04 10 -9 1 -6 16951.4 2033.78 20 -9 -1 -6 16411.5 2050.42 20 -9 -1 -6 19998.7 2042.21 2 -9 1 -6 17932.0 1934.00 2 -9 1 -6 19811.5 1848.64 13 -9 -1 -6 17483.5 1728.82 13 9 -1 6 18783.3 1730.61 6 9 1 6 21627.0 1851.54 6 9 -1 7 1415.93 565.373 6 9 1 7 779.743 466.714 6 9 1 7 1865.57 612.411 5 -9 -1 -7 584.389 533.860 21 -9 1 -7 1171.21 605.008 21 -9 1 -7 1526.38 627.443 20 -9 -1 -7 2156.77 877.688 20 9 -1 7 921.216 583.948 10 9 1 7 1382.03 511.278 10 -9 -1 -7 1307.32 650.409 2 -9 1 -7 712.377 576.663 2 9 -1 7 898.635 458.598 3 9 1 7 2094.46 654.445 3 9 -1 7 1796.09 625.177 16 -9 1 -7 1982.26 630.903 13 -9 -1 -7 944.318 443.806 13 9 -1 8 10509.2 1312.70 6 9 1 8 9329.84 1189.26 6 -9 -1 -8 9670.84 1561.26 21 -9 1 -8 9876.43 1524.39 21 -9 1 -8 10350.3 1689.19 20 -9 -1 -8 8398.23 1603.33 20 9 -1 8 10745.7 1423.13 10 9 1 8 11290.6 1432.35 10 -9 -1 -8 10670.8 1581.95 2 -9 1 -8 8374.67 1433.86 2 9 -1 8 10784.3 1362.10 3 9 1 8 12537.6 1461.85 3 9 -1 8 11971.4 1536.56 16 9 1 8 13374.8 1604.69 16 -9 1 -8 10534.2 1394.40 13 -9 -1 -8 9346.65 1297.00 13 9 -1 9 16799.7 1745.39 3 9 1 9 15778.4 1686.69 3 -9 1 -9 13435.1 1877.84 20 -9 -1 -9 14026.3 2013.79 20 9 1 9 14894.8 1669.58 10 -9 -1 -9 15376.8 1687.26 13 -9 1 -10 197.409 498.956 20 9 -1 10 951.245 549.304 3 -9 1 -10 2015.98 824.040 17 -9 1 -11 20683.5 2351.83 17 -9 -2 11 26592.1 2495.29 4 9 -2 -10 1752.85 572.416 6 9 2 -10 2586.06 787.309 6 -9 -2 10 1922.04 735.304 4 -9 -2 9 27207.1 2382.68 4 -9 2 9 24742.1 2318.06 4 9 -2 -9 27100.8 2230.43 15 9 2 -9 27537.0 2743.46 12 9 -2 -9 23595.3 2263.70 6 9 2 -9 26871.3 2369.51 6 9 -2 -8 291.957 417.097 6 9 2 -8 563.568 453.662 6 -9 2 8 599.636 548.547 18 -9 -2 8 274.645 470.625 18 9 -2 -8 500.696 394.044 15 -9 -2 8 808.394 605.701 4 -9 2 8 572.170 364.090 4 9 -2 -8 2121.51 969.312 12 9 2 -8 1237.27 804.717 12 9 -2 -7 514.537 389.997 6 9 2 -7 719.322 444.607 6 9 2 -7-97.6771 260.248 10 -9 2 7 400.563 397.107 18 -9 -2 7 615.002 476.086 18 9 -2 -7 401.562 360.838 15 -9 -2 7 875.820 535.213 4 -9 2 7 1134.65 576.879 4 -9 -2 7 630.311 430.900 13 9 -2 -7 905.681 717.307 12 9 2 -7 738.933 566.903 12 9 -2 -6 3546.06 793.542 6 9 -2 -6 3898.40 765.765 10 9 2 -6 4804.00 868.643 10 -9 2 6 3873.76 842.669 18 -9 -2 6 4563.59 930.148 18 9 -2 -6 3132.97 742.642 15 -9 -2 6 5185.98 984.936 4 -9 2 6 2559.32 761.934 4 -9 2 6 4633.11 775.781 13 -9 -2 6 5941.61 947.248 13 9 -2 -6 4252.45 1149.22 12 9 2 -6 4906.25 1182.50 12 9 -2 -5 65170.5 3330.10 10 9 2 -5 66487.4 3394.65 10 -9 2 5 69693.2 3703.66 18 -9 -2 5 68587.1 3742.22 18 -9 -2 5 66737.4 3666.30 4 -9 2 5 67843.7 3740.59 4 9 -2 -5 66023.1 3588.28 15 -9 2 5 67851.4 3190.08 13 -9 -2 5 67616.4 3356.23 13 9 -2 -5 70894.2 4544.18 12 9 -2 -5 68310.0 3778.85 6 9 -2 -4 1680.31 664.179 6 9 2 -4 1010.31 510.964 5 -9 -2 4 1346.24 588.018 21 9 -2 -4 578.540 400.104 10 9 2 -4 1471.59 527.086 10 -9 2 4 1139.20 579.253 18 -9 -2 4 943.473 563.454 18 -9 -2 4 1820.44 701.377 2 9 -2 -4 2038.99 614.357 15 9 2 -4 1533.89 506.842 15 -9 -2 4 796.290 403.443 4 -9 2 4 907.300 553.058 4 -9 2 4 1938.11 499.177 13 -9 -2 4 1098.94 432.038 13 9 -2 -4 1287.46 894.520 12 -9 -2 3 19371.7 1901.99 21 -9 2 3 18581.9 1817.49 21 9 -2 -3 18400.2 1653.52 10 9 2 -3 19023.9 1995.50 5 9 2 -3 19996.7 1709.80 10 -9 2 3 19527.1 1892.76 4 9 -2 -3 17992.8 1784.25 15 9 2 -3 18125.6 1639.76 15 -9 2 3 20799.5 1642.35 13 -9 -2 3 19149.8 1658.44 13 -9 -2 3 18835.7 1874.13 2 -9 2 3 17259.2 1753.71 2 9 -2 -3 21574.1 2368.17 12 9 -2 -3 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28078.7 2323.56 6 9 -5 0 627.905 414.786 6 -9 -5 0-103.933 401.363 21 -9 5 0 801.515 402.072 21 -9 -5 0 970.096 777.146 20 9 -5 0 741.921 561.231 10 9 5 0 1714.15 552.812 10 9 5 0 64.5024 498.359 5 -9 -5 0 415.518 307.254 2 -9 5 0 460.937 405.068 2 9 -5 0 871.419 575.312 15 -9 5 0 115.931 350.033 13 -9 -5 0 509.458 437.523 13 9 -5 1 1028.50 516.354 6 -9 -5 -1 764.786 440.358 21 -9 5 -1 758.868 417.965 21 -9 -5 -1 2498.89 915.218 20 9 -5 1 549.842 429.949 10 9 5 1 224.040 343.934 10 9 5 1 1532.11 660.794 5 -9 -5 -1 1373.06 598.017 2 -9 5 -1-288.866 368.870 2 9 -5 1 1059.65 607.864 15 -9 5 -1 1187.62 487.693 13 -9 -5 -1 1016.35 477.615 13 9 -5 2 5304.74 987.882 6 -9 -5 -2 5983.02 1117.66 21 -9 5 -2 5467.91 1019.93 21 -9 -5 -2 4468.35 1118.00 20 9 -5 2 6416.21 1051.30 10 9 5 2 5445.34 962.963 10 9 5 2 5483.16 1056.36 5 -9 -5 -2 5455.90 965.601 2 -9 5 -2 4634.42 932.359 2 -9 5 -2 5658.48 994.366 13 -9 -5 -2 5787.81 1011.68 13 -9 5 -3 18140.9 1791.26 21 9 -5 3 17697.2 1781.39 10 -9 -5 -3 15262.3 1809.38 21 9 5 3 18589.8 1749.48 10 9 5 3 19044.6 1961.19 5 -9 -5 -3 14741.8 2118.30 20 -9 -5 -3 17490.1 1951.47 2 -9 5 -3 17265.4 1716.59 13 -9 5 -3 19261.8 1846.93 2 -9 -5 -3 19506.7 1776.27 13 9 -5 3 17087.9 1751.91 6 9 -5 4 7141.71 1133.89 6 -9 -5 -4 9092.26 1386.73 21 -9 5 -4 9020.97 1285.81 21 -9 5 -4 7281.07 1310.35 20 -9 -5 -4 6087.00 1304.80 20 9 -5 4 6953.55 1096.47 10 9 5 4 7330.79 1117.34 10 9 5 4 8437.66 1316.46 5 -9 -5 -4 6620.60 1204.76 2 -9 5 -4 9790.85 1342.93 2 9 -5 4 10423.0 1313.24 16 -9 5 -4 7819.47 1161.08 13 -9 -5 -4 8272.02 1163.12 13 -9 -5 -5 19123.2 2144.32 21 -9 5 -5 22689.6 2097.01 21 9 -5 5 19303.8 1965.07 10 9 5 5 22304.8 1952.08 10 9 5 5 23905.1 2163.93 5 -9 5 -5 21443.8 2143.37 20 -9 -5 -5 22578.3 2618.01 20 9 -5 5 21783.6 1985.31 16 -9 -5 -5 23730.6 2337.05 2 -9 5 -5 23060.0 2118.68 2 -9 5 -5 24622.0 2139.25 13 -9 -5 -5 22773.1 1985.17 13 9 -5 5 22352.4 2019.15 6 9 -5 6 9368.28 1294.89 6 -9 -5 -6 8909.58 1462.41 21 -9 5 -6 8798.86 1337.47 21 -9 5 -6 9807.15 1479.19 20 -9 -5 -6 9211.22 1699.09 20 9 -5 6 9237.64 1362.24 10 9 5 6 8433.47 1190.72 10 -9 -5 -6 10332.9 1560.83 2 9 5 6 10739.0 1489.74 5 -9 5 -6 8785.78 1324.44 2 9 -5 6 9225.77 1344.80 16 -9 5 -6 9255.44 1313.13 13 -9 -5 -6 8074.09 1217.05 13 9 -5 7 4175.85 885.035 6 9 -5 7 2254.28 729.447 10 -9 -5 -7 2570.39 847.017 21 -9 5 -7 3160.24 874.740 21 -9 5 -7 2267.35 789.113 20 -9 -5 -7 2839.71 1091.54 20 9 5 7 2800.43 737.306 10 -9 -5 -7 3896.83 1017.91 2 -9 5 -7 2615.22 808.877 2 9 5 7 1899.30 706.476 5 9 -5 7 3272.12 855.775 16 -9 5 -7 3136.09 816.840 13 -9 -5 -7 4045.20 867.369 13 9 -5 8 8100.99 1221.14 6 -9 5 -8 7813.34 1351.92 21 -9 5 -8 8823.55 1489.79 20 -9 5 -8 7139.79 1264.29 2 9 5 8 11009.2 1411.44 5 9 -5 8 10084.7 1459.88 16 9 -6 -9 8301.96 1415.16 6 -9 6 9 9855.53 1285.91 11 9 6 -9 6277.56 1229.82 5 9 6 -9 8175.52 1461.08 12 9 -6 -8-245.889 341.487 6 -9 6 8 101.769 282.894 11 9 6 -8-222.798 441.280 10 9 6 -8-629.689 588.455 5 -9 6 8 641.985 529.836 18 9 -6 -8 97.6510 543.480 15 -9 -6 8-213.802 521.731 13 9 6 -8-57.2079 399.868 12 9 -6 -7 3097.82 944.459 6 -9 6 7 1775.56 570.988 11 -9 -6 7 1861.07 793.571 21 9 6 -7 1242.43 550.624 10 9 6 -7 1084.40 614.425 5 -9 6 7 1496.99 554.994 18 -9 -6 7 1556.89 539.581 18 9 -6 -7 2118.86 720.077 15 -9 -6 7 1835.83 593.054 13 9 6 -7 1096.27 687.093 12 9 -6 -6-111.142 502.764 6 -9 6 6 103.651 269.540 11 -9 -6 6 404.527 490.003 21 9 6 -6 220.962 415.447 10 9 6 -6 309.212 537.298 5 -9 6 6 1128.71 661.404 18 -9 -6 6 166.151 439.313 18 -9 -6 6 413.743 466.314 2 9 -6 -6-307.050 425.654 15 -9 6 6 842.608 530.778 4 -9 -6 6 403.269 519.276 7 -9 -6 6 185.871 426.216 13 9 -6 -6 529.034 629.352 12 9 -6 -5 10706.5 1529.01 6 -9 6 5 9636.19 1143.17 11 -9 -6 5 9876.80 1453.71 21 9 6 -5 9852.13 1279.11 10 9 6 -5 10011.9 1591.12 5 -9 6 5 9942.53 1313.92 18 -9 -6 5 9432.78 1348.62 18 -9 -6 5 11854.7 1555.10 2 9 -6 -5 7898.79 1286.20 15 -9 6 5 10964.9 1486.49 4 -9 -6 5 13187.7 1665.18 7 -9 -6 5 10496.9 1376.50 13 9 -6 -5 11033.7 1836.09 12 9 -6 -4 3258.68 862.671 6 -9 6 4 3036.35 652.262 11 -9 -6 4 2479.08 775.415 21 9 -6 -4 1736.46 521.927 10 9 6 -4 2564.62 701.138 10 9 6 -4 1936.14 848.791 5 -9 -6 4 3898.31 915.897 18 -9 -6 4 2296.00 766.335 2 -9 -6 4 2528.80 828.427 7 9 -6 -4 2835.79 786.893 15 -9 6 4 2423.37 773.317 4 -9 6 4 3326.40 688.329 13 -9 -6 4 2807.74 767.232 13 9 -6 -4 2438.99 966.993 12 9 -6 -3 8698.83 1283.65 6 -9 -6 3 7495.31 1256.89 21 -9 6 3 6773.87 1101.62 21 -9 -6 3 9930.35 1779.32 20 9 -6 -3 7940.24 1170.30 10 9 6 -3 7415.80 1135.48 10 9 6 -3 7168.25 1292.64 5 -9 -6 3 8629.50 1307.90 2 -9 6 3 8958.78 1254.35 2 9 -6 -3 8386.41 1346.81 15 -9 6 3 8542.33 1297.34 4 -9 6 3 8402.07 1097.11 13 -9 -6 3 8288.65 1168.70 13 9 -6 -3 8345.67 1583.13 12 9 -6 -2 6075.84 1103.16 6 -9 -6 2 7472.12 1241.16 21 -9 6 2 8321.15 1197.19 21 -9 -6 2 7724.36 1501.74 20 9 -6 -2 5159.63 951.208 10 9 6 -2 7944.76 1185.81 10 9 6 -2 8566.53 1440.57 5 -9 -6 2 6724.58 1201.58 2 -9 6 2 8118.51 1202.83 2 9 -6 -2 8179.72 1344.54 15 -9 6 2 9609.29 1392.50 4 -9 6 2 7029.08 1004.27 13 -9 -6 2 7696.45 1157.98 13 9 -6 -2 7303.34 1430.36 12 9 -6 -1 1102.50 504.095 6 -9 -6 1 1851.47 719.364 21 -9 6 1 754.842 429.984 21 -9 -6 1 2037.36 961.486 20 9 -6 -1 2005.40 537.407 10 9 6 -1 1423.36 651.417 10 9 6 -1 871.316 566.380 5 -9 -6 1 2385.65 754.890 2 -9 6 1 900.336 517.453 2 9 -6 -1 1026.43 561.330 15 -9 6 1 1394.70 537.613 13 -9 -6 1 1435.52 550.915 13 9 -6 -1 2616.12 951.915 12 9 -6 0 60.7205 345.774 6 -9 -6 0 1174.76 643.659 21 -9 6 0 684.336 483.925 21 -9 -6 0-45.4063 477.949 20 9 -6 0-130.894 417.426 10 9 6 0-275.991 459.963 10 9 6 0 708.380 351.902 5 -9 -6 0-869.050 558.482 2 -9 6 0 670.537 436.621 2 9 -6 0-31.9172 527.336 15 -9 6 0 873.227 558.344 13 -9 -6 0 969.167 531.485 13 9 -6 0 1306.17 776.607 12 -9 -6 -1 20693.4 2076.88 21 -9 6 -1 22405.3 1982.98 21 9 -6 1 21712.9 1967.63 10 9 6 1 21603.9 1939.07 10 9 6 1 23047.0 2274.34 5 -9 -6 -1 19040.3 2341.74 20 9 -6 1 24443.8 2384.36 15 -9 6 -1 22365.6 1932.07 13 -9 -6 -1 21386.3 2094.44 2 -9 -6 -1 23442.6 2007.39 13 -9 6 -1 21295.1 1925.24 2 9 -6 1 24480.6 2495.18 12 9 -6 1 23593.3 2146.56 6 9 -6 2-286.802 485.120 6 -9 -6 -2 779.469 592.842 21 -9 6 -2 939.598 486.595 21 -9 -6 -2 31.8122 597.432 20 9 -6 2 648.945 445.366 10 9 6 2 1008.87 634.225 10 9 6 2 640.089 430.634 5 -9 -6 -2 865.303 643.252 2 -9 6 -2 871.288 456.232 2 9 -6 2 429.370 398.223 16 9 -6 2 862.504 617.033 15 -9 6 -2 655.534 432.992 13 -9 -6 -2 1132.25 551.466 13 -9 -6 -3 21483.4 2151.41 21 -9 6 -3 22010.9 1981.36 21 9 -6 3 19750.0 1946.35 10 9 6 3 18556.9 1791.76 10 9 6 3 17695.8 1945.20 5 -9 -6 -3 21778.6 2543.60 20 9 -6 3 18160.0 1720.76 16 -9 -6 -3 22401.4 2192.99 2 -9 6 -3 18612.4 1824.32 13 -9 6 -3 19110.8 1830.09 2 -9 -6 -3 18090.5 1773.99 13 9 -6 3 20605.9 1975.53 6 9 -6 4 3581.05 899.583 6 9 -6 4 2988.46 749.341 10 -9 -6 -4 3307.27 893.215 21 -9 6 -4 2325.38 713.947 21 -9 6 -4 2836.05 910.880 20 -9 -6 -4 3919.96 1099.87 20 9 6 4 1920.82 591.670 10 9 6 4 2950.95 883.842 5 -9 -6 -4 4269.05 1041.44 2 -9 6 -4 3887.73 855.464 2 9 -6 4 3757.09 833.284 16 -9 6 -4 3445.71 813.536 13 -9 -6 -4 3273.55 824.424 13 9 -6 5 4180.97 931.214 6 -9 -6 -5 2952.87 875.548 21 -9 6 -5 2755.67 783.376 21 -9 6 -5 3842.53 944.388 20 -9 -6 -5 2959.14 1051.94 20 9 6 5 2896.02 775.250 10 -9 -6 -5 4373.61 1017.01 2 9 6 5 3851.87 949.840 5 -9 6 -5 2510.05 728.983 2 9 -6 5 2398.06 722.787 16 -9 6 -5 3088.84 848.020 13 -9 -6 -5 3640.18 837.422 13 9 -6 6-39.8820 353.376 6 -9 -6 -6 148.848 406.961 21 -9 6 -6 674.306 576.082 21 -9 6 -6 812.799 553.899 20 -9 -6 -6 718.989 777.751 20 9 6 6-258.058 301.980 10 -9 -6 -6 178.563 413.750 2 9 6 6 597.530 550.245 5 -9 6 -6 530.202 475.728 2 9 -6 6 288.662 347.234 16 -9 6 -6 104.403 397.650 13 -9 -6 -6-55.4042 411.028 13 -9 -6 -7 41460.1 3360.22 21 -9 6 -7 43053.4 3063.99 21 9 6 7 42169.3 2807.46 10 9 6 7 44637.3 3122.44 5 -9 6 -7 38775.0 2976.70 20 9 -6 7 44815.8 3090.43 16 -9 -6 -7 44462.2 3455.05 2 -9 6 -7 45575.1 3127.88 2 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1199.96 514.846 21 -9 7 2 1420.92 554.243 21 -9 -7 2 2370.67 1042.70 20 9 7 -2 1007.54 603.541 10 9 7 -2 1939.71 831.711 5 -9 -7 2 1238.43 615.086 2 -9 7 2 1908.28 619.488 2 9 -7 -2 1006.58 513.478 15 -9 7 2 918.539 528.776 4 -9 -7 2 1807.07 732.992 7 -9 7 2 2058.13 548.270 13 -9 -7 2 1049.81 496.935 13 9 -7 -2 861.342 677.567 12 9 -7 -1 6919.30 1235.10 6 -9 -7 1 5264.37 1034.58 21 -9 7 1 5891.45 1011.46 21 -9 -7 1 6282.85 1388.63 20 9 7 -1 4978.37 981.931 10 9 7 -1 7331.87 1374.62 5 -9 -7 1 6622.45 1177.31 2 -9 7 1 5957.04 1010.24 2 9 -7 -1 6390.18 1208.34 15 -9 -7 1 6528.03 1182.78 7 -9 7 1 6990.33 1040.35 13 -9 -7 1 6021.37 1020.39 13 9 -7 -1 6121.68 1312.21 12 9 -7 0 2000.25 786.730 6 -9 -7 0 1973.58 673.123 21 -9 7 0 1538.37 521.157 21 -9 -7 0 1415.55 751.702 20 9 7 0 3014.54 757.358 10 9 7 0 1861.51 833.631 5 -9 -7 0 2079.54 764.087 2 -9 7 0 2173.82 649.540 2 9 -7 0 1904.28 868.407 15 -9 -7 0 2009.84 701.289 7 -9 7 0 1894.49 571.345 13 -9 -7 0 2194.96 685.204 13 9 -7 0 1645.71 770.632 12 9 -7 1 133.611 491.985 6 -9 -7 -1 1176.12 659.932 21 -9 7 -1 185.123 332.620 21 -9 -7 -1 264.565 565.599 20 9 7 1-178.121 398.646 10 9 7 1 302.977 660.000 5 -9 -7 -1-144.034 454.105 2 -9 7 -1-283.173 444.791 2 9 -7 1 440.484 490.315 15 -9 -7 -1 538.740 466.884 7 -9 7 -1 1198.03 646.957 13 -9 -7 -1-113.290 354.676 13 9 -7 1 483.387 541.712 12 -9 -7 -2 18250.0 2023.46 21 -9 7 -2 15086.1 1613.82 21 9 7 2 18702.7 1803.30 10 9 7 2 17994.7 2049.46 5 -9 -7 -2 13019.4 2168.55 20 9 -7 2 18244.8 1665.54 16 9 -7 2 20010.9 2216.37 15 -9 -7 -2 18117.7 1926.19 7 -9 -7 -2 18626.8 2006.79 2 -9 7 -2 18356.7 1803.23 13 -9 7 -2 15561.5 1638.32 2 -9 -7 -2 17898.7 1774.49 13 9 -7 2 19189.8 2154.65 12 9 -7 2 17376.2 1878.00 6 -9 -7 -3 20500.8 2151.92 21 -9 7 -3 22149.8 1982.11 21 9 7 3 22898.6 2016.74 10 -9 -7 -3 26333.2 2875.00 20 9 7 3 22767.6 2321.66 5 9 -7 3 23026.1 1907.05 16 -9 -7 -3 22273.0 2112.66 7 -9 -7 -3 23154.8 2264.59 2 -9 7 -3 20167.6 1964.74 13 -9 7 -3 22000.9 1985.87 2 -9 -7 -3 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10 -6 -1 6942.94 1199.49 10 -10 6 1 7330.39 1133.44 13 -10 6 0 32.9859 432.458 21 10 -6 0-548.427 454.832 10 -10 6 0 355.345 440.870 2 -10 6 0-186.335 391.688 13 10 -6 0-145.531 506.117 12 -10 6 -1 8433.51 1298.43 21 10 -6 1 10204.2 1527.57 10 -10 6 -1 8668.93 1307.82 2 -10 6 -1 11294.4 1469.62 13 10 -6 1 10093.2 1751.41 12 10 -6 2 67.0045 511.998 12 -10 6 -3 1864.99 854.911 20 10 -6 3 638.913 381.069 16 -10 6 -4 6015.38 1238.47 20 10 -6 4 6296.44 1106.49 16 -10 -6 -4 6830.98 1218.48 7 -10 6 -5 16533.2 2001.34 20 10 -6 5 15623.5 1790.82 16 -10 7 3 3499.57 787.933 13 -10 7 2 1781.45 612.437 13 -10 7 1 2123.43 634.098 13 -10 7 0 5986.93 1074.46 13 10 -7 1 12132.6 1930.63 12 -10 -7 -2 4743.63 1045.35 7 10 -7 2 5649.14 1343.89 12 -10 -7 -3 3269.12 892.144 7 10 -7 3 5065.04 1259.75 12 -10 7 -4 1341.78 696.395 20 -10 -7 -4 1464.15 702.908 7 -10 8 2 13224.9 1524.02 13 10 -8 2 28351.0 2807.12 12 10 -8 3 3407.30 986.780 12 ; _shelx_hkl_checksum 25450 _shelx_res_file ; TITL Jens in P2(1)/c shelx.res created by SHELXL-2019/3 at 10:52:50 on 15-Oct-2023 CELL 0.71073 7.645053 14.643742 13.721069 90.0000 90.4954 90.0000 ZERR 4.00 0.00010 0.0002 0.0002 0.0000 0.0012 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H P Cl Se Au UNIT 44.00 100.00 4.00 4.00 4.00 4.00 L.S. 6 FMAP 2 PLAN 10 TEMP -173 SIZE 0.3 0.2 0.08 ACTA 60 CONF 2.4 BOND $H HTAB C13 AU1 HTAB C23 AU1 HTAB C32 SE1 EQIV $1 -x, -0.5+y, 0.5-z EQIV $2 -x, 1-y, -z HTAB C3 Cl1_$1 RTAB cont Se1 Au1_$2 RTAB CONT Se1 Se1_$2 RTAB angl Au1 Se1 Au1_$2 RTAB angl Se1 Au1_$2 Se1_$2 WGHT 0.016700 2.038300 EXTI 0.001302 FVAR 2.05783 AU1 6 0.127028 0.621413 0.089734 11.00000 0.01726 0.02062 = 0.01251 0.00362 0.00192 0.00498 CL1 4 0.153365 0.772642 0.050038 11.00000 0.03211 0.01938 = 0.01718 0.00064 0.00432 0.00558 P1 3 0.264317 0.422413 0.235003 11.00000 0.01098 0.00953 = 0.01090 0.00010 0.00133 -0.00019 SE1 5 0.083480 0.462954 0.116878 11.00000 0.01578 0.02326 = 0.01381 0.00283 -0.00414 -0.00408 C1 1 0.238458 0.496814 0.345330 11.00000 0.01908 0.01679 = 0.01138 -0.00316 0.00154 -0.00437 C2 1 0.492179 0.417819 0.186064 11.00000 0.01126 0.02116 = 0.02110 0.00496 0.00499 0.00345 C3 1 0.182371 0.308567 0.271793 11.00000 0.02461 0.01059 = 0.02109 0.00201 0.00742 -0.00149 AFIX 13 H3 2 0.086991 0.321412 0.319288 11.00000 -1.20000 AFIX 0 C11 1 0.304959 0.449344 0.438299 11.00000 0.02539 0.03658 = 0.01471 0.00334 -0.00167 -0.00616 AFIX 137 H11A 2 0.426791 0.430479 0.429488 11.00000 -1.50000 H11B 2 0.232742 0.395501 0.451376 11.00000 -1.50000 H11C 2 0.297788 0.491755 0.493370 11.00000 -1.50000 AFIX 0 C12 1 0.041836 0.515018 0.359366 11.00000 0.02185 0.01526 = 0.01982 -0.00276 0.00833 0.00188 AFIX 137 H12A 2 0.025236 0.553189 0.417219 11.00000 -1.50000 H12B 2 -0.019542 0.456852 0.367911 11.00000 -1.50000 H12C 2 -0.005278 0.546595 0.301899 11.00000 -1.50000 AFIX 0 C13 1 0.333461 0.588277 0.333027 11.00000 0.03156 0.01979 = 0.01899 -0.00596 0.00462 -0.01149 AFIX 137 H13A 2 0.302037 0.629288 0.386532 11.00000 -1.50000 H13B 2 0.298923 0.615991 0.270763 11.00000 -1.50000 H13C 2 0.460131 0.577997 0.333924 11.00000 -1.50000 AFIX 0 C21 1 0.628546 0.399357 0.266133 11.00000 0.01273 0.05893 = 0.03668 0.02200 0.00295 0.00776 AFIX 137 H21A 2 0.744569 0.393917 0.236878 11.00000 -1.50000 H21B 2 0.599553 0.342403 0.299840 11.00000 -1.50000 H21C 2 0.628745 0.449941 0.312897 11.00000 -1.50000 AFIX 0 C22 1 0.495299 0.340472 0.109919 11.00000 0.03848 0.01948 = 0.04006 -0.00126 0.02407 0.00610 AFIX 137 H22A 2 0.402133 0.350485 0.061589 11.00000 -1.50000 H22B 2 0.476918 0.281716 0.142451 11.00000 -1.50000 H22C 2 0.608830 0.340036 0.077301 11.00000 -1.50000 AFIX 0 C23 1 0.539078 0.507047 0.134400 11.00000 0.01659 0.02158 = 0.02232 0.00145 0.00689 -0.00330 AFIX 137 H23A 2 0.540991 0.557103 0.181804 11.00000 -1.50000 H23B 2 0.451620 0.519995 0.083621 11.00000 -1.50000 H23C 2 0.654649 0.501173 0.104697 11.00000 -1.50000 AFIX 0 C31 1 0.312286 0.246965 0.327362 11.00000 0.03842 0.01853 = 0.04549 0.01658 0.01757 0.01259 AFIX 137 H31A 2 0.249080 0.195800 0.356711 11.00000 -1.50000 H31B 2 0.370693 0.282460 0.378704 11.00000 -1.50000 H31C 2 0.399812 0.223407 0.282055 11.00000 -1.50000 AFIX 0 C32 1 0.094456 0.253509 0.190014 11.00000 0.05337 0.01794 = 0.03291 -0.00853 0.01265 -0.01622 AFIX 137 H32A 2 0.183385 0.232432 0.144179 11.00000 -1.50000 H32B 2 0.009513 0.292198 0.155597 11.00000 -1.50000 H32C 2 0.034243 0.200684 0.217962 11.00000 -1.50000 AFIX 0 HKLF 4 REM Jens in P2(1)/c REM wR2 = 0.0423, GooF = S = 1.058, Restrained GooF = 1.058 for all data REM R1 = 0.0203 for 4270 Fo > 4sig(Fo) and 0.0243 for all 4654 data REM 145 parameters refined using 0 restraints END WGHT 0.0167 2.0386 REM Highest difference peak 2.041, deepest hole -1.361, 1-sigma level 0.128 Q1 1 0.2335 0.6231 0.0869 11.00000 0.05 2.04 Q2 1 0.0234 0.6223 0.0927 11.00000 0.05 2.03 Q3 1 -0.0142 0.4595 0.1220 11.00000 0.05 0.96 Q4 1 0.1611 0.6537 0.1260 11.00000 0.05 0.86 Q5 1 0.1965 0.4628 0.1177 11.00000 0.05 0.84 Q6 1 0.0600 0.6139 0.0163 11.00000 0.05 0.78 Q7 1 0.1850 0.6226 0.1647 11.00000 0.05 0.77 Q8 1 0.1273 0.5822 0.1012 11.00000 0.05 0.69 Q9 1 0.0530 0.5743 0.0423 11.00000 0.05 0.66 Q10 1 0.3671 0.4167 0.2240 11.00000 0.05 0.65 ; _shelx_res_checksum 27232 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Au Au1 0.12703(2) 0.62141(2) 0.08973(2) 0.01679(4) Uani d 1 . . Cl Cl1 0.15337(9) 0.77264(4) 0.05004(5) 0.02287(13) Uani d 1 . . P P1 0.26432(7) 0.42241(4) 0.23500(4) 0.01046(11) Uani d 1 . . Se Se1 0.08348(3) 0.46295(2) 0.11688(2) 0.01764(6) Uani d 1 . . C C1 0.2385(3) 0.49681(16) 0.34533(18) 0.0157(5) Uani d 1 . . C C2 0.4922(3) 0.41782(17) 0.18606(19) 0.0178(5) Uani d 1 . . C C3 0.1824(3) 0.30857(16) 0.27179(19) 0.0187(5) Uani d 1 . . H H3 0.086991 0.321412 0.319288 0.022 Uiso calc 1 . . C C11 0.3050(4) 0.4493(2) 0.4383(2) 0.0256(6) Uani d 1 . . H H11A 0.426791 0.430479 0.429488 0.038 Uiso calc 1 . . H H11B 0.232742 0.395501 0.451376 0.038 Uiso calc 1 . . H H11C 0.297788 0.491755 0.493370 0.038 Uiso calc 1 . . C C12 0.0418(3) 0.51502(17) 0.3594(2) 0.0189(5) Uani d 1 . . H H12A 0.025236 0.553189 0.417219 0.028 Uiso calc 1 . . H H12B -0.019542 0.456852 0.367911 0.028 Uiso calc 1 . . H H12C -0.005278 0.546595 0.301899 0.028 Uiso calc 1 . . C C13 0.3335(4) 0.58828(18) 0.3330(2) 0.0234(6) Uani d 1 . . H H13A 0.302037 0.629288 0.386532 0.035 Uiso calc 1 . . H H13B 0.298923 0.615991 0.270763 0.035 Uiso calc 1 . . H H13C 0.460131 0.577997 0.333924 0.035 Uiso calc 1 . . C C21 0.6285(4) 0.3994(3) 0.2661(3) 0.0361(8) Uani d 1 . . H H21A 0.744569 0.393917 0.236878 0.054 Uiso calc 1 . . H H21B 0.599553 0.342403 0.299840 0.054 Uiso calc 1 . . H H21C 0.628745 0.449941 0.312897 0.054 Uiso calc 1 . . C C22 0.4953(4) 0.34047(19) 0.1099(2) 0.0325(7) Uani d 1 . . H H22A 0.402133 0.350485 0.061589 0.049 Uiso calc 1 . . H H22B 0.476918 0.281716 0.142451 0.049 Uiso calc 1 . . H H22C 0.608830 0.340036 0.077301 0.049 Uiso calc 1 . . C C23 0.5391(3) 0.50705(18) 0.1344(2) 0.0201(5) Uani d 1 . . H H23A 0.540991 0.557103 0.181804 0.030 Uiso calc 1 . . H H23B 0.451620 0.519995 0.083621 0.030 Uiso calc 1 . . H H23C 0.654649 0.501173 0.104697 0.030 Uiso calc 1 . . C C31 0.3123(4) 0.24696(19) 0.3274(3) 0.0340(7) Uani d 1 . . H H31A 0.249080 0.195800 0.356711 0.051 Uiso calc 1 . . H H31B 0.370693 0.282460 0.378704 0.051 Uiso calc 1 . . H H31C 0.399812 0.223407 0.282055 0.051 Uiso calc 1 . . C C32 0.0945(5) 0.2535(2) 0.1900(2) 0.0347(7) Uani d 1 . . H H32A 0.183385 0.232432 0.144179 0.052 Uiso calc 1 . . H H32B 0.009513 0.292198 0.155597 0.052 Uiso calc 1 . . H H32C 0.034243 0.200684 0.217962 0.052 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Au1 0.01726(5) 0.02062(6) 0.01251(5) 0.00498(3) 0.00192(3) 0.00362(3) Cl1 0.0321(3) 0.0194(3) 0.0172(3) 0.0056(2) 0.0043(2) 0.0006(2) P1 0.0110(3) 0.0095(2) 0.0109(3) -0.00019(19) 0.0013(2) 0.0001(2) Se1 0.01578(11) 0.02326(13) 0.01381(12) -0.00408(9) -0.00414(8) 0.00283(9) C1 0.0191(11) 0.0168(11) 0.0114(11) -0.0044(9) 0.0015(8) -0.0032(9) C2 0.0113(10) 0.0212(12) 0.0211(13) 0.0034(9) 0.0050(9) 0.0050(10) C3 0.0246(12) 0.0106(10) 0.0211(13) -0.0015(9) 0.0074(10) 0.0020(9) C11 0.0254(14) 0.0366(16) 0.0147(13) -0.0062(11) -0.0017(10) 0.0033(11) C12 0.0218(12) 0.0153(11) 0.0198(13) 0.0019(9) 0.0083(9) -0.0028(9) C13 0.0316(14) 0.0198(12) 0.0190(13) -0.0115(10) 0.0046(11) -0.0060(10) C21 0.0127(12) 0.059(2) 0.0367(18) 0.0078(13) 0.0029(11) 0.0220(16) C22 0.0385(17) 0.0195(13) 0.0401(19) 0.0061(12) 0.0241(14) -0.0013(12) C23 0.0166(11) 0.0216(12) 0.0223(13) -0.0033(9) 0.0069(9) 0.0015(10) C31 0.0384(17) 0.0185(13) 0.045(2) 0.0126(12) 0.0176(14) 0.0166(13) C32 0.053(2) 0.0179(13) 0.0329(17) -0.0162(13) 0.0126(14) -0.0085(12) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag Cl1 Au1 Se1 . . 174.465(18) y C3 P1 C2 . . 112.52(11) y C3 P1 C1 . . 105.33(11) y C2 P1 C1 . . 114.50(12) y C3 P1 Se1 . . 103.38(9) y C2 P1 Se1 . . 109.00(8) y C1 P1 Se1 . . 111.54(8) y P1 Se1 Au1 . . 106.911(18) y C13 C1 C11 . . 109.5(2) ? C13 C1 C12 . . 109.0(2) ? C11 C1 C12 . . 106.9(2) ? C13 C1 P1 . . 111.40(17) ? C11 C1 P1 . . 111.77(18) ? C12 C1 P1 . . 108.12(16) ? C23 C2 C21 . . 108.8(2) ? C23 C2 C22 . . 108.0(2) ? C21 C2 C22 . . 110.0(2) ? C23 C2 P1 . . 110.95(16) ? C21 C2 P1 . . 112.23(19) ? C22 C2 P1 . . 106.81(18) ? C32 C3 C31 . . 109.4(2) ? C32 C3 P1 . . 114.91(19) ? C31 C3 P1 . . 116.4(2) ? C32 C3 H3 . . 105.0 ? C31 C3 H3 . . 105.0 ? P1 C3 H3 . . 105.0 ? C1 C11 H11A . . 109.5 ? C1 C11 H11B . . 109.5 ? H11A C11 H11B . . 109.5 ? C1 C11 H11C . . 109.5 ? H11A C11 H11C . . 109.5 ? H11B C11 H11C . . 109.5 ? C1 C12 H12A . . 109.5 ? C1 C12 H12B . . 109.5 ? H12A C12 H12B . . 109.5 ? C1 C12 H12C . . 109.5 ? H12A C12 H12C . . 109.5 ? H12B C12 H12C . . 109.5 ? C1 C13 H13A . . 109.5 ? C1 C13 H13B . . 109.5 ? H13A C13 H13B . . 109.5 ? C1 C13 H13C . . 109.5 ? H13A C13 H13C . . 109.5 ? H13B C13 H13C . . 109.5 ? C2 C21 H21A . . 109.5 ? C2 C21 H21B . . 109.5 ? H21A C21 H21B . . 109.5 ? C2 C21 H21C . . 109.5 ? H21A C21 H21C . . 109.5 ? H21B C21 H21C . . 109.5 ? C2 C22 H22A . . 109.5 ? C2 C22 H22B . . 109.5 ? H22A C22 H22B . . 109.5 ? C2 C22 H22C . . 109.5 ? H22A C22 H22C . . 109.5 ? H22B C22 H22C . . 109.5 ? C2 C23 H23A . . 109.5 ? C2 C23 H23B . . 109.5 ? H23A C23 H23B . . 109.5 ? C2 C23 H23C . . 109.5 ? H23A C23 H23C . . 109.5 ? H23B C23 H23C . . 109.5 ? C3 C31 H31A . . 109.5 ? C3 C31 H31B . . 109.5 ? H31A C31 H31B . . 109.5 ? C3 C31 H31C . . 109.5 ? H31A C31 H31C . . 109.5 ? H31B C31 H31C . . 109.5 ? C3 C32 H32A . . 109.5 ? C3 C32 H32B . . 109.5 ? H32A C32 H32B . . 109.5 ? C3 C32 H32C . . 109.5 ? H32A C32 H32C . . 109.5 ? H32B C32 H32C . . 109.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Au1 Cl1 . 2.2898(6) y Au1 Se1 . 2.3740(3) y P1 C3 . 1.853(2) ? P1 C2 . 1.874(2) ? P1 C1 . 1.877(2) ? P1 Se1 . 2.2027(6) y C1 C13 . 1.534(3) ? C1 C11 . 1.535(4) ? C1 C12 . 1.540(3) ? C2 C23 . 1.531(3) ? C2 C21 . 1.532(4) ? C2 C22 . 1.541(4) ? C3 C32 . 1.532(4) ? C3 C31 . 1.539(4) ? C3 H3 . 1.0000 ? C11 H11A . 0.9800 ? C11 H11B . 0.9800 ? C11 H11C . 0.9800 ? C12 H12A . 0.9800 ? C12 H12B . 0.9800 ? C12 H12C . 0.9800 ? C13 H13A . 0.9800 ? C13 H13B . 0.9800 ? C13 H13C . 0.9800 ? C21 H21A . 0.9800 ? C21 H21B . 0.9800 ? C21 H21C . 0.9800 ? C22 H22A . 0.9800 ? C22 H22B . 0.9800 ? C22 H22C . 0.9800 ? C23 H23A . 0.9800 ? C23 H23B . 0.9800 ? C23 H23C . 0.9800 ? C31 H31A . 0.9800 ? C31 H31B . 0.9800 ? C31 H31C . 0.9800 ? C32 H32A . 0.9800 ? C32 H32B . 0.9800 ? C32 H32C . 0.9800 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C13 H13B Au1 . 0.98 2.80 3.712(3) 154.9 yes C23 H23B Au1 . 0.98 2.89 3.615(3) 131.2 yes C32 H32B Se1 . 0.98 2.62 3.228(3) 120.4 yes C3 H3 Cl1 2_545 1.00 2.68 3.599(3) 153.6 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C3 P1 Se1 Au1 . . . . 166.02(8) y C2 P1 Se1 Au1 . . . . -74.09(9) y C1 P1 Se1 Au1 . . . . 53.31(8) y C3 P1 C1 C13 . . . . 168.86(19) ? C2 P1 C1 C13 . . . . 44.7(2) ? Se1 P1 C1 C13 . . . . -79.65(19) ? C3 P1 C1 C11 . . . . 46.1(2) ? C2 P1 C1 C11 . . . . -78.1(2) ? Se1 P1 C1 C11 . . . . 157.55(15) ? C3 P1 C1 C12 . . . . -71.34(19) ? C2 P1 C1 C12 . . . . 164.51(16) ? Se1 P1 C1 C12 . . . . 40.14(18) ? C3 P1 C2 C23 . . . . 166.43(18) ? C1 P1 C2 C23 . . . . -73.3(2) ? Se1 P1 C2 C23 . . . . 52.4(2) ? C3 P1 C2 C21 . . . . -71.6(2) ? C1 P1 C2 C21 . . . . 48.6(2) ? Se1 P1 C2 C21 . . . . 174.31(19) ? C3 P1 C2 C22 . . . . 49.0(2) ? C1 P1 C2 C22 . . . . 169.23(18) ? Se1 P1 C2 C22 . . . . -65.06(19) ? C2 P1 C3 C32 . . . . -87.3(2) ? C1 P1 C3 C32 . . . . 147.3(2) ? Se1 P1 C3 C32 . . . . 30.1(2) ? C2 P1 C3 C31 . . . . 42.3(2) ? C1 P1 C3 C31 . . . . -83.0(2) ? Se1 P1 C3 C31 . . . . 159.79(19) ?