#------------------------------------------------------------------------------
#$Date: 2023-12-20 04:03:28 +0100 (Wed, 20 Dec 2023) $
#$Revision: 288434 $
#$URL: svn://www.crystallography.net/cod/cif/2/02/29/2022965.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2022965
loop_
_publ_author_name
'Upmann, Daniel'
'Jones, Peter G.'
'Bockfeld, Dirk'
'T\^arcoveanu, Eliza'
_publ_section_title
;
 Crystal structures of sixteen phosphane chalcogenide complexes of gold(I)
 chloride, bromide and iodide
;
_journal_coeditor_code           YZ2044
_journal_issue                   1
_journal_name_full
'Acta Crystallographica Section E Crystallographic Communications'
_journal_paper_doi               10.1107/S2056989023010459
_journal_volume                  80
_journal_year                    2023
_chemical_formula_iupac          '[Au Cl (C9 H21 P S)]'
_chemical_formula_moiety         'C9 H21 Au Cl P S'
_chemical_formula_sum            'C9 H21 Au Cl P S'
_chemical_formula_weight         424.70
_chemical_name_systematic
;
Chlorido(tripropylphosphane sulfide-\k<i>S</i>)gold
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-2019/3
_cell_angle_alpha                90
_cell_angle_beta                 97.004(2)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   8.05892(17)
_cell_length_b                   11.1342(2)
_cell_length_c                   15.0596(4)
_cell_measurement_reflns_used    14045
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      30.8176
_cell_measurement_theta_min      2.2763
_cell_volume                     1341.21(5)
_computing_cell_refinement
;
CrysAlisPro, Version 1.171.35.21 (Rigaku OD, 2020)
;
_computing_data_collection
;
CrysAlisPro, Version 1.171.35.21 (Rigaku OD, 2020)
;
_computing_data_reduction
;
CrysAlisPro, Version 1.171.35.21 (Rigaku OD, 2020)
;
_computing_molecular_graphics
;
Bruker XP (Bruker, 1998)
;
_computing_publication_material
;
SHELXL-2019/3 (Sheldrick, 2015)
;
_computing_structure_refinement
;
SHELXL-2019/3 (Sheldrick, 2015)
;
_computing_structure_solution
;
SHELXS-97 (Sheldrick, 2008)
;
_diffrn_ambient_temperature      100(2)
_diffrn_detector_area_resol_mean 16.1419
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.955
_diffrn_measurement_device_type  'Oxford Diffraction Xcalibur, Eos'
_diffrn_measurement_method       '\w scan'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0286
_diffrn_reflns_av_unetI/netI     0.0151
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            39799
_diffrn_reflns_theta_full        30.000
_diffrn_reflns_theta_max         30.887
_diffrn_reflns_theta_min         2.281
_diffrn_source                   'fine-focus sealed tube'
_exptl_absorpt_coefficient_mu    11.404
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.38863
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro, Version 1.171.35.21 (Rigaku OD, 2020)
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    2.103
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             808
_exptl_crystal_size_max          0.4
_exptl_crystal_size_mid          0.2
_exptl_crystal_size_min          0.2
_refine_diff_density_max         1.327
_refine_diff_density_min         -0.754
_refine_ls_extinction_coef       0.00169(5)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_extinction_method
;
SHELXL-2019/3 (Sheldrick, 2015)
;
_refine_ls_goodness_of_fit_ref   1.077
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     125
_refine_ls_number_reflns         4047
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.077
_refine_ls_R_factor_all          0.0191
_refine_ls_R_factor_gt           0.0148
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0111P)^2^+0.8830P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0301
_refine_ls_wR_factor_ref         0.0315
_reflns_number_gt                3612
_reflns_number_total             4047
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            yz2044sup1.cif
_cod_data_source_block           1a
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               2022965
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.092
_shelx_estimated_absorpt_t_max   0.209
_shelx_hkl_file
;
   0   0  -2 222627. 3778.66  16
   0   0  -2 224577. 3621.15   6
   0   0  -2 227874. 3755.86   1
   0   0  -2 224758. 3816.45  10
   0   0   2 228947. 3671.89  11
   0   0   2 232738. 3624.81   6
   0   0   2 222738. 4134.51   2
   0   0  -2 227676. 3650.31  11
   0   0  -3 44.6137 53.8915  11
   0   0   3 83.8846 60.1763  15
   0   0  -3 30.3530 51.2798   6
   0   0  -3 149.840 70.1991  15
   0   0   3 93.1188 64.5235  11
   0   0  -3 81.1362 66.4899  16
   0   0  -3 187.930 89.5288  12
   0   0  -3 9.07831 99.1009  10
   0   0   3 132.117 85.3004   1
   0   0   3 95.5962 53.2061   6
   0   0  -3 29.7522 60.9551   1
   0   0   3-32.9499 160.787   2
   0   0   3 134.825 77.2048  16
   0   0  -3 179.004 144.218   2
   0   0   4 8326.91 360.124   6
   0   0  -4 9291.11 537.156  10
   0   0  -4 8477.98 478.203  16
   0   0  -4 8783.56 464.655   1
   0   0  -4 8622.01 454.491  12
   0   0   4 8242.98 403.561  11
   0   0   4 8908.72 463.347   1
   0   0  -4 8433.71 386.479  11
   0   0  -4 8282.60 364.400   6
   0   0  -4 8898.00 483.674  15
   0   0   4 8943.92 395.991  15
   0   0   4 9475.18 501.196  16
   0   0  -4 9106.32 698.818   2
   0   0   4 8389.48 662.761   2
   0   0   4 8363.53 496.713  10
   0   0   5 547.421 133.675  11
   0   0  -5 753.120 231.278  10
   0   0   5 183.483 135.974   1
   0   0   5 415.333 106.350   6
   0   0   5 192.117 216.918   2
   0   0  -5 184.830 96.5630  12
   0   0  -5 202.918 138.814  16
   0   0  -5 364.717 89.5276   6
   0   0   5 462.622 124.051  15
   0   0  -5 595.513 123.430  11
   0   0  -6 25200.9 1120.31  10
   0   0  -6 27250.1 886.841  11
   0   0   6 26855.1 1044.56   1
   0   0   6 26352.9 1483.79   2
   0   0   6 27380.9 949.655  11
   0   0  -6 25057.0 1063.77  16
   0   0   6 28025.4 853.367   6
   0   0   6 27471.0 882.079  15
   0   0   7 151.153 104.013  11
   0   0  -7-75.3217 120.456  11
   0   0   7 86.8730 92.6547  15
   0   0  -7 193.816 210.230  16
   0   0   7 178.919 157.111   1
   0   0   7-4.70992 70.5922   6
   0   0  -7 24.1423 209.008  10
   0   0  -8 503062. 9141.06  16
   0   0  -8 500389. 8522.47  11
   0   0  -8 513206. 9332.91  10
   0   0   8 509879. 8486.59  15
   0   0   8 505961. 8984.82   1
   0   0   9 636.400 194.596  15
   0   0  -9 632.988 335.896  16
   0   0  -9 24.9264 248.252  10
   0   0  -9 883.903 217.987  11
   0   0   9 593.851 287.301   1
   0   0  10 367788. 6404.54  15
   0   0 -10 351231. 7203.60  16
   0   0  10 353217. 7043.88   1
   0   0 -10 356872. 6482.97  11
   0   0 -10 351805. 7442.89  10
   0   0 -11 265.729 178.510  11
   0   0 -11 964.030 444.378  16
   0   0  11 410.715 268.199   1
   0   0  11 643.530 199.460  15
   0   0 -11 841.444 458.255  10
   0   0  12 27402.5 1104.30  15
   0   0 -12 25222.6 1518.96  16
   0   0  12 26480.1 1463.51   1
   0   0 -12 26453.5 1161.56  11
   0   0 -12 26738.4 1653.26  10
   0   0 -13 50.0252 361.027  10
   0   0 -13-227.829 172.947  11
   0   0 -13 60.6022 304.298  16
   0   0  13 208.349 332.011   1
   0   0  13 46.8091 128.109  15
   0   0 -14 2660.36 390.992  11
   0   0 -14 2446.80 581.070  16
   0   0 -14 2391.46 624.016  10
   0   0  14 1456.74 457.258   1
   0   0 -15 283.859 431.279  16
   0   0 -15-118.176 170.452  11
   0   0 -15-34.8005 444.954  10
   0   0  15-515.399 432.476   1
   0   0 -16 21659.1 1835.35  10
   0   0 -16 21257.3 1667.71  16
   0   0  16 19507.7 1498.43   1
   0   0  17 636.140 436.800   1
   0   0 -17 673.238 482.438  10
   0   0 -17-138.026 496.695  16
   0   0 -18 120888. 4864.92  10
   0   0 -18 111647. 4378.51  16
   0   0  18 112518. 4205.01   1
   0   0 -19 1123.07 649.416  16
   0   0  19 746.310 557.312   1
   0   0 -19 997.934 625.795  10
   0   0  20 17076.5 1659.23   1
   0   0 -20 17677.6 1946.31  10
   0   1  -1 116391. 2106.32  10
   0  -1  -1 118773. 2129.62   3
   0  -1   1 108024. 2149.43   3
   0   1   1 114712. 2051.88   8
   0  -1  -1 114342. 2034.25   1
   0   1  -1 113263. 2101.81  14
   0  -1  -1 117647. 2052.14  16
   0  -1  -2 60819.3 1312.67  10
   0  -1  -2 60643.3 1312.57   8
   0   1   2 63229.4 1318.87  10
   0   1   2 60771.0 1323.56   8
   0  -1   2 62608.8 1373.49  14
   0  -1   2 63261.3 1427.19  10
   0   1   2 64070.7 1342.64  16
   0   1   2 60449.3 1153.23  11
   0   1  -2 62314.9 1374.53  14
   0   1   2 57825.2 1553.17   2
   0   1  -2 61248.4 1420.01  10
   0   1   2 62585.2 1310.92   3
   0  -1  -2 62265.9 1539.50   2
   0  -1   2 60144.6 1329.84   3
   0  -1   2 61288.4 1207.19  12
   0   1   2 61390.7 1260.07   6
   0   1  -2 61968.4 1209.63  12
   0   1   2 62246.7 1292.85   1
   0   1  -2 59759.3 1347.23  16
   0  -1   2 61038.3 1348.17  16
   0  -1   2 63915.3 1556.00  13
   0  -1  -2 62101.2 1303.02   1
   0   1  -2 60922.7 1445.19  11
   0  -1  -2 60567.3 1336.08  16
   0   1  -2 62570.4 1312.56   3
   0  -1   2 56350.9 1444.34  11
   0  -1  -2 62002.0 1242.14   6
   0  -1  -3 283224. 5174.76  10
   0   1  -3 298413. 5660.87   2
   0   1   3 315039. 4976.89   6
   0   1  -3 296550. 5183.83  16
   0   1  -3 292074. 5205.28  11
   0  -1   3 304893. 5195.79  16
   0   1   3 293637. 5688.35   2
   0   1   3 305463. 5148.44   8
   0  -1  -3 294102. 5170.59  16
   0   1  -3 304575. 5194.85  14
   0  -1  -3 309197. 5143.71   8
   0   1   3 295147. 5455.69  15
   0  -1  -3 311998. 5643.48   2
   0  -1   3 299078. 5181.71  14
   0   1   3 317686. 5198.95  16
   0   1  -3 293763. 5290.72  10
   0   1   3 309392. 4864.95  11
   0  -1  -3 303044. 4935.96   6
   0   1   3 317431. 5200.61  10
   0  -1  -3 301262. 4847.81  11
   0   1  -3 303293. 4976.90  12
   0  -1   3 298063. 5045.25   3
   0  -1  -3 306618. 5100.71   1
   0  -1   3 308019. 5002.20  12
   0   1   3 303991. 5095.70   1
   0  -1   3 310376. 5312.56  10
   0  -1   3 289060. 5276.82  11
   0  -1   4 1541.18 242.695  10
   0  -1  -4 1518.39 320.985   2
   0   1   4 1258.88 208.423  16
   0  -1   4 1267.72 209.776   1
   0   1   4 1224.57 204.499  10
   0   1   4 1103.87 230.141  15
   0   1  -4 1023.58 226.291  10
   0   1   4 1155.10 280.828   2
   0  -1   4 1323.71 186.743  12
   0   1   4 800.826 159.736   1
   0   1  -4 1105.76 204.869  16
   0   1  -4 1210.97 193.804  11
   0  -1  -4 1356.94 203.047   8
   0  -1  -4 1228.69 208.220  10
   0   1   4 1180.68 132.722  11
   0  -1  -4 946.069 135.091   6
   0   1  -4 1800.40 356.287   2
   0  -1   4 1336.07 215.707  11
   0   1  -4 1043.57 152.679  12
   0  -1  -4 1024.42 125.826  11
   0   1  -4 902.669 177.910  14
   0  -1  -4 1131.41 174.402   1
   0  -1  -4 941.101 196.535  16
   0  -1   4 1256.51 205.793  16
   0   1   4 1050.41 139.361   6
   0   1  -4 1125.04 112.560  15
   0   1  -5 279240. 5180.03  16
   0  -1   5 283548. 4861.14   6
   0   1   5 287085. 4797.40   6
   0   1   5 281115. 5255.56  15
   0   1   5 287275. 5072.24   1
   0  -1   5 291998. 4557.51  15
   0  -1  -5 274498. 5170.42  16
   0  -1   5 275810. 5181.76  11
   0   1  -5 277364. 4678.80  15
   0   1  -5 278166. 5320.50  10
   0   1   5 275339. 5998.86   2
   0  -1  -5 274263. 5232.31  10
   0  -1   5 280993. 5136.93   1
   0   1  -5 270863. 5039.89  11
   0   1   5 287106. 4759.73  11
   0   1  -5 277804. 4933.20  12
   0  -1  -5 277065. 4758.57   6
   0  -1   5 284484. 5022.91  12
   0  -1  -5 282153. 4702.12  11
   0   1  -6 130.791 100.316  12
   0  -1  -6-22.1092 164.576  10
   0   1  -6 372.760 241.915  16
   0  -1   6 17.0401 135.726   1
   0   1  -6 329.129 89.8489  15
   0   1   6-19.2478 133.784   1
   0  -1   6 155.962 81.8789  15
   0   1  -6 200.768 113.023  11
   0   1   6 329.617 175.375  15
   0   1   6-95.9229 289.721   2
   0   1   6 488.294 110.176  11
   0  -1  -6 81.8067 94.6702   6
   0   1   6 160.811 94.9124   6
   0  -1   6 105.600 88.0572   6
   0  -1  -6 148.058 96.7558  11
   0   1  -6 749.483 278.773  10
   0  -1  -6 35.1541 161.697  16
   0   1   7 331386. 7581.24   2
   0  -1  -7 347436. 5894.15   6
   0  -1  -7 345240. 5849.44  11
   0   1   7 351635. 5918.85   6
   0   1  -7 335815. 6642.21  10
   0  -1  -7 338128. 6477.47  16
   0  -1   7 339516. 6406.05   1
   0   1   7 345938. 6331.69   1
   0   1  -7 337245. 6180.63  11
   0   1   7 333921. 6305.25  15
   0   1  -7 343545. 6484.83  16
   0   1  -7 328182. 6059.77  15
   0  -1   7 356291. 5668.78  15
   0   1   7 349738. 5958.78  11
   0  -1  -7 345708. 6609.76  10
   0  -1   8 3170.65 255.554  15
   0   1   8 3102.44 397.337   1
   0   1  -8 2919.15 493.451  10
   0   1   8 3278.02 328.220  11
   0  -1  -8 2821.50 286.072   6
   0  -1   8 2795.27 394.374   1
   0   1  -8 3109.00 356.612  11
   0  -1  -8 3422.61 469.105  16
   0   1   8 3164.77 379.272  15
   0  -1  -8 3132.40 292.662  11
   0   1   8 2765.83 627.760   2
   0  -1  -8 3123.51 458.571  10
   0   1  -8 2572.05 442.243  16
   0  -1  -9 16638.9 767.040   6
   0   1  -9 19157.1 1190.45  10
   0   1  -9 19394.6 935.423  11
   0  -1  -9 16893.6 760.301  11
   0  -1  -9 19361.6 1196.52  10
   0   1   9 17194.3 1467.34   2
   0   1   9 18503.9 1027.98   1
   0  -1  -9 18140.9 1107.14  16
   0  -1   9 18976.6 1077.65   1
   0   1  -9 16915.6 1083.24  16
   0  -1   9 17825.1 671.421  15
   0   1   9 17471.0 914.701  15
   0   1 -10 37703.6 1811.05  10
   0   1 -10 37032.2 1414.12  11
   0   1  10 38344.9 1448.10  15
   0  -1 -10 38191.4 1254.76  11
   0  -1 -10 35136.0 1248.47   6
   0   1 -10 35318.3 1642.14  16
   0  -1 -10 36280.5 1678.89  16
   0  -1  10 41201.7 1691.32   1
   0  -1  10 38246.7 1099.82  15
   0   1  10 36766.0 1570.92   1
   0  -1 -10 38226.8 1801.93  10
   0  -1 -11 33468.0 1684.56  16
   0   1 -11 34893.0 1700.44  16
   0   1 -11 32828.1 1365.68  11
   0  -1  11 34269.6 1067.54  15
   0  -1  11 31887.1 1573.96   1
   0  -1 -11 32587.0 1201.98  11
   0   1 -11 35194.6 1824.15  10
   0   1  11 34687.9 1401.64  15
   0   1  11 34350.1 1590.19   1
   0  -1 -11 32659.5 1765.80  10
   0   1  12 350.008 269.360   1
   0   1 -12 346.551 338.848  10
   0   1  12 321.062 164.649  15
   0  -1  12 402.106 300.177   1
   0  -1 -12 311.463 321.192  16
   0  -1 -12 307.117 172.816  11
   0  -1 -12 210.943 331.061  10
   0  -1  12 348.794 132.962  15
   0   1 -12-48.5502 372.587  16
   0   1 -12 312.047 179.388  11
   0  -1  13 59083.4 2024.04   3
   0  -1 -13 60611.7 2698.50  10
   0  -1 -13 59798.8 1867.01  11
   0  -1 -13 62273.1 2574.91  16
   0   1 -13 59175.8 2673.02  10
   0   1  13 61616.4 2038.27  15
   0   1  13 59586.1 2373.10   1
   0   1 -13 61526.2 2059.53  11
   0  -1  13 58410.6 2397.00   1
   0   1 -13 61067.1 2541.91  16
   0   1  14 1582.99 458.805   1
   0   1  14 2003.43 342.152  15
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   2   7   9-215.778 310.266   1
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   2   7  10 11977.9 1363.67   2
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   3  11   8 78774.7 3807.72   2
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   3 -11  11 5852.88 1058.38  14
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   3  11  11 6053.80 941.070   8
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   4   2 -20 35586.5 2434.11  16
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   4  -2 -19 605.130 629.374  10
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   4   2 -19 1283.64 592.110  16
   4  -2 -18 22698.5 2002.64  10
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   4  -2 -18 23192.6 1864.57  16
   4   2 -18 24497.3 1846.23  16
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   4  -2 -17 1204.42 612.625  10
   4   2 -17 1345.96 558.629  10
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   4   2 -17 1108.49 479.892  16
   4  -2 -16 30345.6 2166.15  10
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   4   4   8 168656. 4478.74  13
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   4   7   5 131143. 3538.58   8
   4   7   5 132824. 4093.21  13
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   4   7   5 131868. 4196.82   2
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   4   7   5 131216. 4246.20   4
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   4  -7   5 133475. 3260.55   2
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   4   8   5 7631.79 996.128   4
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   4  -8   8 69361.2 3373.29   3
   4   8   8 69755.8 2720.22   8
   4   8   8 67930.1 2958.37  13
   4  -8   8 70216.6 3021.99  12
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   4  -8   9 781.933 539.642  14
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   4   8   9-70.8857 286.590  13
   4  -8   9 166.443 441.075   3
   4   8   9-695.528 627.726   2
   4  -8   9 550.253 314.483  12
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   4  -8  10 166462. 5746.93   3
   4   8  10 162446. 5040.65  13
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   4   8  10 174464. 6074.32   2
   4  -8  10 164302. 5129.32  12
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   4  -8  10 169477. 5333.04  14
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   4  -8  11 294.378 397.428  14
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   4   8  12 35622.4 2170.60  13
   4  -8  12 36816.4 2266.88  12
   4   8  12 33508.7 2656.33   2
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   4  -8  12 34657.9 2307.46  14
   4  -8  12 37075.5 2600.40   3
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   4   9 -13 58622.5 3023.05   5
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   4   9  -8 5711.53 1065.66  13
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   4  -9  -7 113161. 4035.35  10
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   4   9  -7 113875. 4022.25   5
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   4   9  -6 17383.3 1326.10   8
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   4   9  -3 67015.7 2643.89   2
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   4   9  -3 66124.8 2573.91   8
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   4   9   0 26127.1 1897.43  13
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   4   9   0 24122.6 1534.56   2
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   4   9   0 25771.2 1765.93   4
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   4   9   0 22910.2 1399.50   8
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   4   9   2 2814.81 666.110   4
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   4  -9   3 175657. 5178.00  14
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   4   9   3 172583. 5277.24  13
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   4   9   3 176638. 5030.77   2
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   4   9   3 177023. 5341.64   4
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   4   9   3 165443. 4496.40   8
   4   9   4 19573.9 1332.03   8
   4  -9   4 20556.8 1802.01   3
   4   9   4 17425.3 1525.00  13
   4  -9   4 17380.2 1461.38  12
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   4   9   4 19590.7 1539.65   2
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   4  -9   4 18703.1 1562.80  14
   4   9   5 126240. 3829.43   8
   4  -9   5 131134. 4789.57   3
   4  -9   5 126737. 4294.50  12
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   4  -9   5 124093. 4358.08  14
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   4   9   5 135062. 4638.93   4
   4   9   5 121860. 4286.00  13
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   4  -9   6-114.486 391.825  14
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   4   9   6-61.5452 272.150   8
   4   9   6 309.115 333.430  13
   4   9   6 773.567 470.339   2
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   4  -9   6-236.649 620.575   3
   4  -9   6 279.852 330.634  12
   4   9   6-31.1512 473.232   4
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   4  -9   7 60571.4 3231.03   3
   4   9   7 61418.7 2568.95   8
   4   9   7 58307.7 2832.47  13
   4  -9   7 62166.5 2867.18  12
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   4   9   7 65194.0 3244.32   2
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   4  -9   7 60529.8 2976.96  14
   4   9   8 19702.5 1429.32   8
   4   9   8 17849.2 1751.13   2
   4   9   8 17602.8 1511.50  13
   4  -9   8 17673.9 1524.51  12
   4  -9   8 17743.6 1762.56   3
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   4  -9   8 16584.1 1538.94  14
   4  -9   9 12004.5 1375.69  14
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   4   9   9 11935.4 1158.59   8
   4   9   9 12825.2 1301.96  13
   4  -9   9 12704.2 1508.91   3
   4   9   9 14156.8 1640.11   2
   4  -9   9 13024.2 1304.96  12
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   4  -9  10 1719.28 523.028  14
   4   9  10 2246.35 521.691   8
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   4   9  10 2677.90 618.503  13
   4  -9  10 3514.97 822.034   3
   4  -9  10 2690.52 640.446  12
   4   9  10 2878.39 864.255   2
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   4  -9  11 31109.9 2430.79   3
   4   9  11 26211.9 1897.75  13
   4  -9  11 29107.7 2005.97  12
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   4   9  11 29704.4 2489.06   2
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   4  -9  11 30974.4 2185.19  14
   4  -9  12 11348.4 1388.00  14
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   4  -9  12 12490.2 1612.90   3
   4  -9  12 10217.3 1197.04  12
   4   9  12 10714.1 1582.39   2
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   4  -9  13 66256.3 3722.66   3
   4   9  13 63839.7 3906.32   2
   4  -9  13 55174.4 2905.24  12
  -4   9 -13 63011.7 3623.82  11
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  -4   9 -13 60973.9 3618.25   9
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   4  -9  13 60310.9 3234.35  14
   4  -9  14 447.275 526.971   3
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   4  -9  14 1359.70 660.269   1
   4   9  14 389.436 498.925  15
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   4  10 -15 141.494 364.954   5
   4  10 -15 625.006 474.467  11
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   4  10 -14 11103.2 1432.43  11
   4  10 -14 9821.63 1300.46   5
   4 -10 -14 12001.5 1491.40  10
   4 -10 -13 18402.8 1765.99  14
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   4  10 -13 21266.0 1993.42  11
   4 -10 -13 19107.5 1800.30  10
   4  10 -13 19612.3 1740.50   5
   4 -10 -13 17550.8 1766.13  16
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   4 -10 -12 43143.1 2661.28  14
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   4  10 -12 42952.5 2872.21  11
   4 -10 -12 45861.7 2766.12  10
   4  10 -12 49979.0 2755.06   5
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   4 -10 -12 41955.4 2650.35  16
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   4  10 -12 42096.1 2523.63   8
   4  10 -11 1940.47 650.532   8
   4 -10 -11 3916.95 832.701  14
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   4  10 -11 4422.17 1000.46  13
   4 -10 -11 4576.66 910.164  10
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   4 -10 -11 2531.96 673.189  16
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   4 -10 -10 102235. 4099.31  14
   4  10 -10 112365. 5029.68  13
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   4 -10 -10 102670. 4129.89  10
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   4  10 -10 108274. 4139.53   5
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   4  10 -10 98214.9 3871.48   8
   4 -10 -10 101977. 4132.26  16
   4  10  -9 6728.69 964.085   8
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   4 -10  -9 5513.72 923.668  14
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   5   8   3 142855. 3764.03   8
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   6  -3   7 146902. 4751.74   2
   6  -3   7 150080. 4031.40  14
   6  -3   8 341.844 289.569  14
   6   3   8 334.327 462.671   2
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   6   3   9 1748.94 503.121  13
   6   3   9 2776.52 794.288   2
   6  -3   9 2999.14 670.447  12
   6  -3   9 2696.37 617.052   2
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   6   4  12 25383.2 2366.90   2
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   6   6 -10 146942. 4925.62   5
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   6  -6 -10 144781. 4632.62  16
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   6   6  -9 2003.94 633.767  13
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   6   6  12 29231.3 2578.52   2
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   6   6  13 3246.81 750.174  13
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   6   6  15 431.410 374.537  13
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   6  -7 -15 51835.4 3108.79  10
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   6   7 -11 22057.2 1967.11  13
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   6  -7  -7 86077.8 3546.91  10
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   6   7  -5 111986. 4101.21   5
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   6   7  -4 6141.08 872.922   2
   6  -7  -3 101263. 3526.98  14
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   6   7  -3 101471. 3943.85  13
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   6   7  -3 101691. 3657.48   2
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   6  -7  -2 1310.04 404.593  14
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   6   8   4 15027.3 1507.11   4
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   6  -8   4 16542.7 1464.47  14
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   6  -8   5 6817.68 1054.49  12
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   6   8   5 9900.47 1217.11   4
   6   8   6 26044.8 1978.40  13
   6  -8   6 28955.8 2101.12  12
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   6   8   6 25495.0 1974.35   4
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   6  -8   6 24463.7 1821.93  14
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   6  -8   7 1102.05 502.459  14
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   6   8   7 1728.51 695.420   4
   6   8   8 111868. 4422.84  13
   6  -8   8 122635. 4639.70  12
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   6   8   8 125799. 5111.21   2
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   6  -8   8 123437. 4467.90  14
   6  -8   8 128635. 5071.96   3
   6  -8   9 3566.39 832.570  14
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   6   8   9 2015.01 648.026  13
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   6   8  10 35018.6 2392.70  13
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   7   1   4 4244.56 606.699   4
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   7   2  11 12895.3 1408.33  13
   7  -2  11 13609.7 1554.07  12
   7   2  11 11910.3 1609.43   2
   7  -2  11 12473.8 1573.88   2
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   7   2  12 726.776 524.910  13
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   7   2  13 96024.7 4174.18  13
   7  -2  13 98332.3 4504.66  12
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   7   2  13 95875.4 4918.57   2
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   7   3 -18 29259.3 2238.30  10
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   7   3 -17 71.9823 445.830  10
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   7   6   3 107755. 3965.72   4
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   7   6   4-17.8192 436.490   4
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   7   6   5 151082. 5198.55   2
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   7   6   5 154233. 4970.18   4
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   7  -6   6 669.021 380.159  14
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   7  -6   6 634.082 549.356  12
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   7   6   6 216.383 390.613   4
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   7   6   7 42900.3 2767.00   2
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   7   6   7 39024.8 2450.36   4
   7  -6   7 43269.9 2670.58   3
   7  -6   7 42257.4 2287.89  14
   7  -6   8 2229.01 573.068  14
   7   6   8 2097.46 782.893   2
   7   6   8 2628.50 683.978  13
   7  -6   8 1750.31 733.573   3
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   7   6   9 289.632 410.293  13
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   7   6   9 1012.13 624.696   2
   7  -6   9 1341.28 610.007  12
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   7   6  11 20283.7 1834.29  13
   7  -6  11 21149.7 1965.07  12
   7   6  11 21552.1 2254.51   2
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   7  -6  11 21459.7 2039.44   3
   7   6  12 449.912 425.600  13
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   7  -7 -14 3963.40 821.550  16
   7   7 -13 135.906 398.804  13
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   7  -7 -12 70445.0 3418.66  14
   7   7 -12 71332.5 3712.01  13
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   7  -7 -12 67664.4 3475.76  10
   7   7 -12 71940.7 3617.89   5
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   7   7 -10 120405. 4820.94  13
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   7  -7 -10 117282. 4554.75  10
   7   7 -10 114231. 4560.62   5
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   7  -7 -10 113976. 4296.27  16
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   7  -7  -9 5548.32 894.453  14
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   7   7  -9 5421.43 1014.38  13
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   7  -7  -9 4893.81 924.233  10
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   7   7  -9 4131.53 858.635   5
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   7  -7  -8 38689.6 2310.30  14
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   7   7  -8 36674.8 2499.05  13
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   7  -7  -8 39604.3 2467.92  10
   7   7  -8 36439.6 2399.75   5
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   7  -7  -8 35653.0 2212.30  16
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   7  -7  -7 1597.59 479.552  14
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   7   7  -7 2814.32 735.184  13
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   7  -7  -7 1778.40 590.530  10
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   7   7  -7 1198.87 431.481   5
   7  -7  -7 2382.81 564.985  16
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   7  -7  -6 12615.3 1278.48   3
   7  -7  -6 12903.4 1278.37  14
   7   7  -6 11704.8 1414.53  13
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   7   7  -6 12514.5 1365.50   5
   7  -7  -6 11789.6 1217.74  16
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   7   7  -6 11413.7 1288.52   2
   7  -7  -5 2576.76 576.513  14
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   7   7  -5 1616.75 586.899  13
  -7  -7   5 1853.74 526.039   7
   7  -7  -5 2604.08 656.486   3
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  -7   7   5 2439.32 702.570  15
   7   7  -5 1243.84 465.872   2
  -7   7   4 29814.4 1692.80   8
   7  -7  -4 24886.7 1728.42  14
   7  -7  -4 25565.7 1898.20   3
   7   7  -4 29127.3 2130.71  13
  -7  -7   4 26951.1 1744.36   7
  -7  -7   4 26063.5 1845.09   6
   7   7  -4 25965.6 1920.51   2
  -7  -7   4 25590.7 1962.61  17
  -7   7   4 27188.7 1954.85   9
  -7   7   4 28064.5 2091.51  15
   7  -7  -3 849.791 449.935  14
  -7   7   3-56.9039 304.081   8
   7   7  -3 48.8063 423.756  13
   7  -7  -3 475.156 401.288   3
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  -7   7   3 209.123 274.339  11
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   7   7  -3 229.374 491.436   2
   7  -7  -2 142269. 4903.40   3
   7  -7  -2 146340. 4499.29  14
   7   7  -2 149804. 5155.04  13
  -7  -7   2 145029. 4333.74   7
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   7   7  -2 147554. 4811.40   2
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  -7   7   2 134678. 4747.40  15
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   7   7  -1 5080.03 907.621   2
   7  -7  -1 6221.84 872.115  14
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   7   7  -1 7625.17 1137.63  13
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   7   7  -1 7184.51 1011.05   4
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   7  -7   0 87188.0 3325.50  14
   7   7   0 83676.3 3702.18  13
   7  -7   0 81352.0 3716.92  12
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   7   7   0 86816.1 3564.19   2
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  -7   7   0 83408.4 3538.22   9
   7   7   0 84348.4 3505.26   4
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   7  -7   0 79852.1 3561.99   3
   7   7   1 8995.55 1149.80   2
   7  -7   1 8556.73 1023.05  14
  -7   7  -1 9459.64 918.864   8
   7   7   1 9487.06 1214.77  13
   7  -7   1 9164.69 1174.70   3
   7  -7   1 9914.46 1287.53  12
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   7   7   1 9822.01 1164.84   4
  -7   7  -1 9955.74 1195.38   9
   7   7   2 50981.9 2806.31  13
   7  -7   2 50649.3 2879.96  12
  -7   7  -2 47179.8 2580.79  11
  -7  -7  -2 50024.6 2758.57   6
   7   7   2 51877.8 2738.30   2
  -7  -7  -2 51284.7 2763.89  17
  -7   7  -2 49788.2 2761.76   9
   7   7   2 51865.7 2709.09   4
  -7   7  -2 52258.1 2264.80   8
   7  -7   2 49006.4 2784.83   3
   7  -7   2 49671.9 2502.50  14
   7  -7   3 2569.78 555.222  14
   7   7   3 1609.38 520.929   2
   7   7   3 1821.79 668.019  13
   7  -7   3 2073.22 668.112   3
   7  -7   3 2676.07 795.852  12
  -7   7  -3 1168.69 451.769  11
  -7  -7  -3 1917.25 631.925   6
  -7  -7  -3 1753.39 619.111  17
  -7   7  -3 1778.39 624.763   9
   7   7   3 1335.79 576.821   4
   7  -7   4 2928.45 678.570  14
   7   7   4 2927.83 727.975   2
   7   7   4 2250.17 703.209  13
   7  -7   4 2760.58 726.283   3
   7  -7   4 3391.38 735.580  12
  -7   7  -4 2000.24 615.708  11
  -7  -7  -4 3434.27 826.938   6
  -7  -7  -4 3527.39 792.047  17
  -7   7  -4 4172.67 874.300   9
   7   7   4 2446.80 602.078   4
   7  -7   5 2274.99 600.491  14
   7   7   5 2054.16 751.720   2
   7   7   5 2601.38 715.937  13
   7  -7   5 2298.10 729.325   3
   7  -7   5 1948.47 737.327  12
  -7   7  -5 2547.35 688.214  11
  -7  -7  -5 1849.23 612.282   6
  -7  -7  -5 2074.41 712.331  17
  -7   7  -5 1243.18 525.033   9
   7   7   5 1418.87 562.042   4
   7   7   6 37852.6 2470.92  13
   7  -7   6 38065.5 2532.62  12
  -7   7  -6 40238.9 2613.55  11
  -7  -7  -6 43261.7 2638.29   6
  -7  -7  -6 40012.3 2423.65  17
   7   7   6 38880.6 2621.92   2
  -7   7  -6 35788.8 2563.90   9
   7   7   6 38606.9 2459.56   4
   7  -7   6 41827.4 2700.28   3
   7  -7   6 41926.9 2357.51  14
   7  -7   7 881.655 455.872  14
   7   7   7 1386.64 639.245   2
   7   7   7 891.022 582.649  13
   7  -7   7 1416.20 640.725   3
   7  -7   7 889.875 542.338  12
  -7   7  -7 2212.20 734.398  11
  -7  -7  -7 1662.67 671.752   6
  -7  -7  -7 1195.04 523.721  17
  -7   7  -7 418.964 524.281   9
   7   7   7 600.644 416.525   4
   7   7   8 56742.0 3115.00  13
   7  -7   8 54401.1 3115.06  12
  -7   7  -8 59348.0 3330.44  11
  -7  -7  -8 58104.3 3177.04   6
  -7  -7  -8 56741.2 2898.24  17
   7   7   8 56480.9 3416.01   2
  -7   7  -8 54704.1 3414.51   9
   7  -7   8 56864.8 3289.51   3
   7  -7   8 65478.2 3022.31  14
   7  -7   9 7871.75 1054.87  14
   7   7   9 5580.16 980.313  13
   7  -7   9 7456.35 1235.22   3
   7   7   9 7426.44 1301.80   2
   7  -7   9 8132.57 1202.33  12
  -7   7  -9 9460.01 1399.44  11
  -7  -7  -9 8400.73 1228.24   6
  -7  -7  -9 7623.10 1026.69  17
  -7   7  -9 7237.46 1304.79   9
   7   7  10 51075.6 2980.70  13
   7  -7  10 50685.2 3047.21  12
  -7   7 -10 50831.3 3186.44  11
  -7  -7 -10 47439.2 2915.62   6
  -7   7 -10 43461.3 3137.06   9
   7   7  10 53683.7 3500.62   2
   7  -7  10 51179.5 2739.05  14
   7  -7  10 44595.7 3034.02   3
   7  -7  11 3688.50 814.979  14
   7   7  11 2445.80 707.582  13
   7  -8 -13 65006.7 3403.24  14
   7   8 -13 56624.2 3475.16  13
  -7  -8  13 54796.3 3507.72   7
   7  -8 -13 54511.8 3109.18  16
   7  -8 -12 1192.90 491.065  14
   7   8 -12 2229.75 795.574  13
  -7   8  12 1905.19 555.484   8
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   7  -8 -12 810.152 590.963  10
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   7   8 -12 1601.89 570.309   5
   7  -8 -12 1133.30 516.754  16
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   7  -8 -11 2448.58 720.619  14
  -7   8  11 3523.12 741.939   8
   7   8 -11 2724.83 803.964  13
  -7  -8  11 1997.08 723.660   7
   7  -8 -11 3311.46 863.686  10
   7   8 -11 3329.48 866.332   5
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   7  -8 -11 1964.62 670.986  16
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   7  -8 -10 6391.43 1038.54  14
  -7   8  10 5391.87 840.080   8
   7   8 -10 4768.23 1043.47  13
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   7  -8 -10 5672.28 1091.96  10
  -7  -8  10 5316.43 1051.76  17
   7   8 -10 5309.02 1044.07   5
   7  -8 -10 4946.45 961.347  16
  -7   8  10 5502.96 1120.84  15
   7  -8  -9 23704.1 1911.48  14
  -7   8   9 25797.9 1804.76   8
   7   8  -9 24106.7 2160.49  13
  -7  -8   9 24615.7 1994.90   7
   7  -8  -9 24019.9 1997.65  10
   7   8  -9 27743.7 2173.20   5
  -7  -8   9 22975.7 1960.64  17
   7  -8  -9 25452.3 1979.98  16
  -7   8   9 22949.9 2149.81  15
   7  -8  -8 5658.54 951.491  14
  -7   8   8 4910.75 788.547   8
   7   8  -8 3869.01 850.803  13
  -7  -8   8 5740.42 946.518   7
  -7   8   8 6157.77 841.216   7
  -7  -8   8 5721.59 898.528   6
   7  -8  -8 4680.00 924.181  10
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   7   8  -8 4882.30 870.010   5
   7  -8  -8 4983.37 856.267  16
  -7   8   8 6551.11 1174.82  15
  -7   8   7 27138.9 1788.55   8
   7  -8  -7 26415.4 1943.56  14
   7   8  -7 28135.8 2234.73  13
  -7  -8   7 27216.4 1930.43   7
  -7  -8   7 25050.6 1865.87   6
   7  -8  -7 27787.6 2098.26  10
   7   8  -7 26063.5 2037.56   2
  -7  -8   7 27774.5 2154.69  17
   7   8  -7 24858.2 2008.74   5
   7  -8  -7 26529.0 1962.89  16
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  -7   8   7 24153.6 2156.87  15
   7  -8  -6 3603.21 764.462  14
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   7   8  -6 5899.65 1100.59  13
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   7  -8  -6 4767.95 798.292   3
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   7  -8  -6 3435.65 735.255  16
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  -7   8   6 5069.82 1092.37  15
   7   8  -6 4402.14 854.083   2
  -7   8   5 152276. 4538.81   8
   7  -8  -5 151007. 4900.48  14
   7  -8  -5 150876. 5082.32   3
   7   8  -5 151523. 5485.29  13
  -7  -8   5 145310. 4611.24   7
  -7  -8   5 140216. 4908.09   6
   7   8  -5 146053. 5036.95   2
  -7  -8   5 141626. 5180.21  17
  -7   8   5 142975. 5006.76   9
  -7   8   5 139827. 5342.47  15
   7  -8  -4 5296.46 895.811  14
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   7   8  -4 3798.09 870.472  13
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   7  -8  -4 4292.87 852.898   3
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   7   8  -4 3935.17 834.123   2
   7  -8  -3 99819.3 3778.25  14
   7  -8  -3 94571.5 4004.98   3
   7   8  -3 95119.9 4177.85  13
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   7   8  -3 94383.2 3846.41   2
  -7  -8   3 89323.3 3990.79  17
  -7   8   3 92535.9 3876.80   9
  -7   8   3 91104.8 4018.56  15
  -7   8   3 95351.6 3388.73   8
   7   8  -2 325.986 369.464   2
   7  -8  -2 1376.87 563.265  14
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   7   8  -2-19.8332 480.213  13
   7  -8  -2-701.154 564.757   3
  -7  -8   2-33.1022 297.367   7
  -7   8   2 496.019 332.850  11
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  -7   8   2 826.485 509.471   9
  -7   8   2 343.427 325.568  15
   7   8  -1 469.686 356.333   2
   7  -8  -1 193.750 341.261  14
  -7   8   1 359.542 325.375   8
   7   8  -1 960.527 481.369  13
   7  -8  -1 539.536 393.358   3
   7  -8  -1 31.7312 483.956  12
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  -7  -8   1 1227.14 665.411  17
   7   8  -1 495.229 450.296   4
  -7   8   1 780.561 383.316   9
  -7   8   1 2124.44 614.032  15
   7   8   0 1810.26 591.092   2
   7  -8   0 1976.00 608.209  14
  -7   8   0 1668.95 470.140   8
   7   8   0 1916.90 666.088  13
   7  -8   0 2421.64 677.090   3
   7  -8   0 1830.27 684.737  12
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  -7  -8   0 1841.47 645.607   6
  -7  -8   0 2444.61 744.638  17
   7   8   0 1306.77 588.368   4
  -7   8   0 2472.80 662.059   9
  -7   8   0 1789.30 556.484  15
   7  -8   1 7993.36 1016.69  14
   7   8   1 10458.7 1299.61   2
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   7   8   1 9857.61 1265.16  13
   7  -8   1 10124.6 1288.85   3
   7  -8   1 8377.38 1191.56  12
  -7   8  -1 9492.51 1137.17  11
  -7  -8  -1 8291.91 1149.89   6
  -7  -8  -1 7420.08 1164.07  17
  -7   8  -1 8092.88 1176.97   9
   7   8   1 9631.64 1254.78   4
   7  -8   2 146.810 370.447  14
   7   8   2 315.416 391.171   2
  -7   8  -2-233.252 321.661   8
   7   8   2 215.712 449.697  13
   7  -8   2-305.008 489.650   3
   7  -8   2-125.226 432.937  12
  -7   8  -2 518.470 365.269  11
  -7  -8  -2 515.938 474.381   6
  -7  -8  -2 712.356 598.572  17
  -7   8  -2 383.983 509.273   9
   7   8   2 224.257 480.746   4
   7   8   3 87125.1 3869.07  13
   7  -8   3 80812.2 3794.58  12
  -7   8  -3 81599.4 3719.24  11
  -7  -8  -3 73834.9 3605.00   6
   7   8   3 85791.6 3787.49   2
  -7  -8  -3 80345.1 3724.30  17
  -7   8  -3 84160.9 3808.89   9
   7   8   3 84447.8 3715.74   4
   7  -8   3 78017.8 3411.42  14
   7  -8   3 79052.5 3814.91   3
   7  -8   4 230.681 417.497  14
   7   8   4 1131.52 569.946   2
   7   8   4 380.995 455.520  13
   7  -8   4 1219.51 597.046   3
   7  -8   4 51.6530 493.603  12
  -7   8  -4 999.619 609.796  11
  -7  -8  -4 148.468 474.073   6
  -7  -8  -4 1051.02 700.488  17
  -7   8  -4 1039.77 454.705   9
   7   8   4 1184.87 527.285   4
   7   8   5 142715. 5164.11  13
   7  -8   5 144390. 5247.04  12
  -7   8  -5 135196. 5172.01  11
  -7  -8  -5 142717. 5219.92   6
  -7  -8  -5 138926. 5038.74  17
   7   8   5 138855. 5230.68   2
  -7   8  -5 139780. 5313.06   9
   7   8   5 139828. 5109.30   4
   7  -8   5 140075. 4832.60  14
   7  -8   5 138454. 5318.97   3
   7  -8   6 477.578 430.813  14
   7   8   6 949.268 650.256   2
   7   8   6 729.365 527.412  13
   7  -8   6 868.525 643.996   3
   7  -8   6 30.2504 456.696  12
  -7   8  -6 777.014 565.761  11
  -7  -8  -6 1123.46 655.109   6
  -7  -8  -6 620.179 411.429  17
  -7   8  -6-582.976 620.919   9
   7   8   6 59.1184 437.801   4
   7   8   7 25829.2 2087.99  13
   7  -8   7 25340.4 2101.96  12
  -7   8  -7 24269.4 2142.25  11
  -7  -8  -7 24522.6 2117.89   6
  -7  -8  -7 25386.1 1992.21  17
   7   8   7 25284.7 2248.91   2
  -7   8  -7 21196.3 2062.01   9
   7   8   7 24153.9 2069.11   4
   7  -8   7 22923.5 1859.23  14
   7  -8   7 24233.4 2183.36   3
   7  -8   8 978.585 506.842  14
   7   8   8 950.465 503.217  13
   7   8   8 964.892 503.966   2
   7  -8   8 1750.43 781.252   3
   7  -8   8 374.496 429.077  12
  -7   8  -8 444.472 446.757  11
  -7  -8  -8 1367.77 638.341   6
  -7  -8  -8 1665.95 565.642  17
  -7   8  -8 748.345 558.224   9
   7  -8   9-951.081 571.626  14
   7   8   9-70.6417 389.750  13
   7   8   9-29.1646 494.663   2
   7  -8   9-447.005 627.397   3
   7  -8   9 97.5165 387.989  12
  -7   8  -9 243.329 471.366  11
  -7  -8  -9 231.176 449.442   6
  -7  -8  -9-172.543 423.761  17
  -7   8  -9-278.370 681.646   9
   7  -8  10 3379.76 759.403  14
   7   8  10 4040.54 917.041  13
   7  -8  11 7244.63 1121.20  14
   7   9 -13 1215.67 584.706  13
  -7  -9  13 62.6018 476.346   7
  -7   9  12 57615.8 3005.74   8
   7   9 -12 58301.8 3655.94  13
  -7  -9  12 50491.9 3222.16   7
  -7  -9  12 51068.0 3000.02  17
   7  -9 -11 6622.13 1070.71  14
  -7   9  11 5733.52 937.135   8
   7   9 -11 5800.55 1178.58  13
  -7  -9  11 5743.05 1109.95   7
  -7  -9  11 4526.23 930.821  17
   7  -9 -11 6520.00 1128.33  16
   7  -9 -10 67924.0 3461.58  14
  -7   9  10 78208.7 3417.84   8
   7   9 -10 74092.0 4073.23  13
  -7  -9  10 76063.7 3713.94   7
   7  -9 -10 70374.9 3630.59  10
   7   9 -10 71277.7 3642.19   5
  -7  -9  10 64929.3 3505.32  17
   7  -9 -10 70989.0 3552.24  16
  -7   9  10 73123.1 4219.53  15
   7  -9  -9-49.7898 551.657  14
  -7   9   9 527.974 411.530   8
   7   9  -9 457.206 600.301  13
  -7  -9   9 439.805 500.916   7
   7  -9  -9 90.7152 500.981  10
  -7  -9   9 128.603 442.332  17
   7   9  -9 345.752 484.717   5
   7  -9  -9 16.4007 429.820  16
  -7   9   9 6.76950 437.795  15
   7  -9  -8 36851.2 2455.76  14
  -7   9   8 39742.0 2311.39   8
   7   9  -8 38727.1 2832.41  13
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   7 -11   2 31669.6 2527.82  12
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   7  11   2 34759.4 2508.31   2
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   7  11   2 31058.5 2507.47   4
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   7 -11   2 35633.3 2540.76  14
   7 -11   3 10728.4 1405.41  14
   7  11   3 10466.5 1375.92   2
   7 -11   3 9427.03 1444.35   3
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   7  12  -6 2802.92 738.122   2
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   7 -12  -5 59669.6 3556.62   3
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   7 -12  -3 45593.0 3111.17   3
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   8   0 -17-723.314 548.134  10
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   8   0  -7 92.7830 235.275  13
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   8   0  -4 30253.9 1684.01  12
   8   0  -4 31407.4 1622.31  10
   8   0  -4 33294.9 1990.70   2
   8   0  -4 29928.4 1711.78   5
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   8   0   0 72799.8 3036.45   2
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   8   0   2 46367.7 2426.99   2
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   8   0   6 18020.1 1688.17   2
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   8   0   7 532.520 509.146   2
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   8   0   8 68936.2 3587.67   2
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   8   0  12 52771.5 3539.79   2
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   8   1 -17 23518.9 2020.79  10
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   8  -1 -15 69725.6 3453.32  10
   8   1 -15 68320.5 3267.15  10
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   8  -1 -13 82492.9 3594.31  10
   8   1 -13 84561.8 3451.97  10
   8   1 -13 80252.6 3987.13   5
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   8  -1 -12 2956.45 718.827  10
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   8  -1 -11 9573.75 1133.45  10
   8   1 -11 11112.9 1121.02  10
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   8   1 -11 11118.3 1373.72   5
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   8  -1 -10 840.425 405.550  10
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   8  -1  -9 14917.5 1318.41  10
   8   1  -9 16704.4 1252.02  10
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   8  -1  -9 14211.2 1440.91   5
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   8   1  -9 15172.8 1503.18   5
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   8   1  -8 2994.56 566.093  13
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   8  -1  -8 2648.46 532.807  12
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   8  -1  -8 4708.63 737.333  10
   8   1  -8 3940.57 619.538  10
   8  -1  -8 3896.51 755.356   5
   8   1  -8 3105.00 700.563   5
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   8   1  -7 110684. 3694.38  13
   8  -1  -7 116245. 3489.57  13
  -8  -1   7 103892. 4048.09   7
  -8   1   7 107695. 4113.53   7
   8  -1  -7 109514. 3635.51  12
   8  -1  -7 107492. 3642.93  10
   8   1  -7 110881. 3377.92  10
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   8  -1  -7 105592. 3843.90   5
   8   1  -7 103931. 3931.20   5
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   8   1  -6 40.7013 316.362  13
   8  -1  -6-0.53598 230.129  13
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   8  -1  -6 834.329 436.092  12
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   8   1  -6 241.238 330.370   5
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   8   1  -5 216657. 5738.43  13
   8  -1  -5 217731. 5503.50  13
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   8   1  -5 230295. 5219.83  12
   8  -1  -5 221657. 5653.82  12
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   8  -1  -5 223599. 5554.03  10
   8   1  -5 225159. 5109.03  10
   8   1  -5 215022. 6011.63   2
   8  -1  -5 205399. 5788.75   2
   8  -1  -5 210358. 5507.80   5
   8   1  -5 206906. 5677.53   5
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  -8   1   5 213384. 5812.46  17
  -8   1   5 212505. 6003.77   9
   8   1  -4 272.847 300.044  13
   8  -1  -4 149.416 265.288  13
   8   1  -4 94.5201 228.585  12
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   8  -1  -4 292.179 270.596  10
   8   1  -4 446.850 270.874  10
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   8   1  -4 152.740 361.524   5
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   8   1  -4 158.075 369.953   2
   8  -1  -4-438.133 361.955   2
   8   1  -3 102401. 3627.84  13
   8  -1  -3 100724. 3464.56  13
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   8   1  -3 103817. 3261.85  12
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   8  -1  -3 103228. 3549.78  12
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   8   1  -3 106715. 2988.06  10
   8   1  -3 96448.8 3658.69   2
   8  -1  -3 98639.0 3577.69   2
   8  -1  -3 104933. 3219.23   5
   8   1  -3 99670.9 3405.20   5
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   8   1  -2 1038.14 443.450  13
   8  -1  -2 558.733 314.445  13
   8   1  -2 335.272 233.485  12
   8  -1  -2 896.675 415.906  12
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   8   1  -2 959.914 354.646   2
   8  -1  -2 304.615 324.372   2
   8   1  -1 402.245 331.866   2
   8  -1  -1-689.978 492.294   2
   8   1  -1-52.6209 384.475  13
   8  -1  -1 505.808 373.650  13
   8   1  -1 686.151 288.031  12
   8  -1  -1 271.992 339.694  12
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  -8   1   1 840.719 408.883  17
  -8   1   1-67.5069 388.982   9
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   8   1   0 3600.77 710.561   2
   8  -1   0 5033.60 786.200   2
   8   1   0 3457.14 703.479  13
   8  -1   0 4334.01 753.321  13
   8   1   0 4764.01 690.900  12
   8  -1   0 3582.45 680.330  12
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  -8   1   0 3381.30 628.611  17
   8  -1   0 4690.54 563.757   4
  -8   1   0 4130.84 705.936   9
  -8  -1   0 3437.49 580.969   9
   8   1   1 32020.1 1959.11  13
   8   1   1 28445.1 1736.31  12
   8  -1   1 29429.5 1876.69  12
  -8  -1  -1 30926.9 1829.78   6
   8   1   1 29757.5 1923.40   2
   8  -1   1 29825.2 1846.98   2
  -8  -1  -1 33836.3 1972.35  17
  -8   1  -1 33412.0 1956.69  17
  -8   1  -1 28373.1 1855.93   9
  -8  -1  -1 34389.0 1933.38   9
   8   1   1 29453.5 1597.81   4
   8   1   2-259.855 463.035   2
   8  -1   2 462.302 395.001   2
   8   1   2 1128.19 513.219  13
   8   1   2 703.292 418.278  12
   8  -1   2 1157.95 415.402  12
  -8   1  -2 1145.72 482.958  11
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  -8  -1  -2 1546.91 544.292  17
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  -8   1  -2 631.989 372.987   9
  -8  -1  -2 1181.60 445.118   9
   8   1   2 501.338 244.549   4
   8   1   3 160410. 4999.21  13
   8   1   3 162367. 4844.83  12
   8  -1   3 150605. 4859.66  12
  -8   1  -3 154151. 4766.88  11
  -8  -1  -3 159527. 4795.65   6
   8   1   3 163898. 5096.72   2
   8  -1   3 155861. 4904.15   2
  -8  -1  -3 159874. 4757.87  17
  -8   1  -3 162447. 4821.32  17
  -8   1  -3 155358. 4921.83   9
  -8  -1  -3 154675. 4697.37   9
   8   1   3 167790. 4415.40   4
   8   1   4 251.201 442.706   2
   8  -1   4-33.9337 368.221   2
   8   1   4 959.734 570.246  13
   8   1   4 1058.83 462.233  12
   8  -1   4 178.477 381.037  12
  -8   1  -4 382.500 375.389  11
  -8  -1  -4 1461.44 592.216   6
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   8   1   4 557.610 340.058   4
   8   1   5 148043. 4914.32  13
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   8   1   5 151911. 5118.95   2
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   8  -1   5 157658. 5098.81   2
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   8   1   6 1108.60 637.083   2
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   8   1   7 26574.3 2110.04   2
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   8  -1  11 25787.9 2227.69  12
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   8   1  11 22995.0 2316.55   2
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   8  -2 -12 102538. 4064.06  10
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   8   2 -12 102034. 4429.97   5
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   8   2 -10 41383.1 2615.78   5
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   8   2  -9 2632.22 568.732  13
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   8  -2  -9 1588.35 435.822  12
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   8   2  -8 57932.3 2610.36  13
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   8  -2  -8 58627.1 2695.14  12
   8  -2  -8 52634.7 2554.44  10
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   8  -2  -8 48181.8 2576.43   5
   8   2  -8 51620.5 2782.75   5
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   8  -2  -5 432.817 371.322   2
   8   2  -4 41248.1 2246.58  13
   8  -2  -4 41462.6 2018.98  13
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   8   2  -4 42661.6 1832.84  12
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   8  -2  -4 43765.5 2304.86  12
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   8  -2  -4 40862.0 2081.62  10
   8   2  -4 38149.4 2225.97   2
   8  -2  -4 41672.6 2159.65   2
   8  -2  -4 42795.9 1919.10   5
   8   2  -4 38566.2 2126.75   5
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   8  -2  -4 42303.9 1836.81  16
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   8  -2  -4 42732.5 2031.83   3
   8   2  -3 234.120 388.890  13
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   8  -2  -3 1076.17 359.004   5
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   8   2  -3 1033.27 421.663   5
   8  -2  -3 1152.48 327.480  16
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   8   2  -3 595.398 376.935   2
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   8  -2  -2 83756.5 3322.97  12
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   8   2  -2 83869.3 3364.97   2
   8  -2  -2 83870.9 3150.60   2
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   8   2  -1 2735.97 611.252   2
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   8  -2  -1 2588.45 639.232  12
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   8   2   0 90324.3 3504.50  13
   8   2   0 86888.4 3101.28  12
   8  -2   0 87867.0 3454.20  12
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   8   2   0 89818.9 3515.04   2
   8  -2   0 93698.5 3358.29   2
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   8   2   0 86116.6 3074.11   4
  -8   2   0 88778.7 3466.30   9
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   8   2   1-210.031 442.598   2
   8  -2   1-280.187 364.780   2
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   8  -2   1-139.237 440.031  12
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   8   2   1-274.389 367.544   4
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   8   2   2 107605. 3956.84  13
   8   2   2 107462. 3675.67  12
   8  -2   2 109006. 3977.46  12
  -8   2  -2 104271. 3720.50  11
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   8   2   2 107776. 3979.73   2
   8  -2   2 106707. 3771.08   2
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  -8   2  -2 105435. 3780.19  17
  -8   2  -2 104753. 3895.25   9
  -8  -2  -2 108845. 3603.75   9
   8   2   2 109785. 3535.15   4
   8   2   3-532.830 384.988   2
   8  -2   3 14.2090 347.844   2
   8   2   3 103.559 381.905  13
   8   2   3 966.016 490.701  12
   8  -2   3-154.682 467.931  12
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   8   2   3 541.733 369.616   4
   8   2   4 3550.34 771.763   2
   8  -2   4 3957.39 747.971   2
   8   2   4 2457.49 633.514  13
   8   2   4 2751.18 625.763  12
   8  -2   4 3459.94 753.325  12
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   8   2   4 3375.21 635.846   4
   8   2   5 14.1170 479.571   2
   8  -2   5 296.919 414.373   2
   8   2   5-99.6672 398.370  13
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   8   2   5 615.728 356.235   4
   8   2   6 26638.7 1954.23  13
   8   2   6 31220.0 2057.84  12
   8  -2   6 30635.3 2133.08  12
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   8   2   6 28931.7 2178.94   2
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   8  -2   6 30043.5 2147.75   2
  -8   2  -6 26795.5 2032.60   9
  -8  -2  -6 28800.0 1866.98   9
   8   2   6 29488.3 1809.96   4
   8   2   7 2684.20 777.751   2
   8   2   7 3037.83 724.143  13
   8  -2   7 2162.64 653.689   2
   8   2   7 2577.45 692.642  12
   8  -2   7 1774.43 594.747  12
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   8   2   8 26132.0 2030.57  13
   8  -2   8 26300.5 2077.14  12
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   8   2   8 30107.8 2368.31   2
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  -8  -2  -8 25537.3 1870.07   9
   8  -2   8 28167.8 2229.25   2
   8   2   9 551.753 497.435  13
   8   2   9 94.3000 492.297   2
   8  -2   9 693.585 556.276   2
   8  -2   9-322.587 514.694  12
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   8   2  10 104260. 4370.97  13
   8  -2  10 105144. 4570.86  12
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  -8   2 -10 96706.0 4623.30   9
   8   2  10 97978.9 4747.02   2
   8  -2  10 103642. 4769.12   2
   8   2  11-200.572 473.867  13
   8  -2  11-317.819 521.606  12
   8   2  11-165.249 628.586   2
   8  -2  11 174.465 510.641   2
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   8  -2  12 30467.1 2648.98   2
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   8  -3 -15 70979.8 3644.97  10
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   8  -3 -14 1395.98 658.246  10
  -8   3  14 743.648 510.934   1
   8   3 -14 1468.52 615.896   5
  -8  -3  13 62724.5 3727.97   7
  -8   3  13 63473.7 3464.61   7
   8  -3 -13 63661.4 3289.28  10
   8   3 -13 67740.5 3616.13   5
  -8   3  13 64694.9 3154.45   1
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  -8  -3  12 1190.82 666.302   7
  -8   3  12 1159.05 633.562   7
  -8   3  12 823.917 426.994   1
   8  -3 -12 1327.12 562.208  10
   8   3 -12 1257.28 632.569   5
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   8  -3 -12 619.886 379.598  16
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   8  -3 -11 3629.42 757.142  10
   8   3 -11 4846.80 974.973   5
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   8  -3 -11 5005.84 760.995  16
  -8  -3  10 918.753 601.367   7
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   8  -3 -10-65.4994 434.548  10
   8   3 -10 921.398 604.204   5
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   8  -3 -10 973.313 370.117  16
   8   3  -9 3544.98 661.458  13
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  -8   3   9 3592.05 791.813   7
  -8   3   9 4160.99 712.581   1
   8  -3  -9 5463.30 847.716  10
   8   3  -9 2739.34 705.783   5
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  -8   3   9 2299.52 528.344  17
   8  -3  -9 3495.67 621.635  16
   8  -3  -8 127.993 373.182  14
   8   3  -8 510.212 414.365  13
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  -8   3   8-685.980 467.521   7
   8  -3  -8-11.8370 394.338  10
   8   3  -8 247.921 390.430   5
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   8  -3  -8 644.591 277.834  16
   8  -3  -7 90057.1 3217.66  14
   8   3  -7 99526.6 3736.04  13
  -8  -3   7 90438.9 3778.00   7
  -8   3   7 99697.2 3885.25   7
   8  -3  -7 93881.9 3747.04  12
   8  -3  -7 97426.3 3637.36  10
   8  -3  -7 92371.2 3434.89   5
   8   3  -7 91125.2 3760.97   5
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   8  -3  -7 100302. 3286.94  16
   8  -3  -6 160.736 287.580  14
   8   3  -6 302.495 366.522  13
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   8  -3  -6-555.527 428.715  12
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   8  -3  -6-546.617 502.828  10
   8  -3  -6 114.114 292.647   5
   8   3  -6 79.9402 387.651   5
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   8  -3  -5 241310. 5689.81  14
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   8  -3  -5 247618. 5752.66  13
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   8  -3  -5 242566. 6620.29  12
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   8  -3  -5 243318. 6334.81  10
   8   3  -5 233812. 6597.48   2
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   8   3  -5 237367. 6452.37   5
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   8   3   1 19593.1 1618.40   2
   8  -3   1 19457.6 1446.26   2
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   8   3   1 18474.4 1398.37   4
   8   3   2 1382.95 572.924   2
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   8   3   2 1372.07 428.674   4
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   8   3   3 222216. 6325.60   2
   8  -3   3 218710. 5962.06   2
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   8   3   3 222435. 5786.55   4
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   8   3   5 113711. 4398.27   2
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   8  -3   5 111874. 4154.93   2
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   8   3   5 105989. 3780.89   4
   8   3   6 692.999 595.307   2
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   8   3   6-566.135 446.152   4
   8   3   7 17860.0 1661.66  13
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   8   3   7 17516.0 1789.92   2
   8  -3   7 16568.3 1666.53   2
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   8   3   8 2488.20 792.250   2
   8   3   8 1757.03 579.004  13
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   8   3  11 38309.5 2608.30  13
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   8   3  11 41796.2 3135.38   2
   8  -3  11 38781.6 2876.55   2
   8  -3  12 254.059 435.996   2
   8  -3  13 73176.5 4192.84   2
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   8  -4 -15 665.958 466.137  16
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   8  -4 -14 13478.5 1551.52  10
   8   4 -14 12931.5 1634.79   5
   8  -4 -14 13384.5 1393.57  16
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   8  -4 -13 3693.40 889.665  10
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   8  -4 -12 66450.6 3338.57  10
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   8   4 -12 67623.9 3583.96   5
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   8  -4 -12 66173.5 2995.64  16
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   8   4 -10 79474.0 3773.25   5
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   8  -4  -6 10599.0 1075.60   2
   8  -4  -6 11195.2 1199.40  10
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   8   4  -6 11101.5 1258.91   5
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   8  -4  -4 33847.5 2269.62  12
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   8   4  -4 37353.9 2293.56   2
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   8   4  -4 36591.4 2200.05   5
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   8  -4  -4 37212.2 1951.99  16
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   8  -4  -4 36840.3 2085.04   3
   8  -4  -3 3365.44 537.600  14
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   8   4   0 81203.9 3526.57  13
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   8   4   0 85124.3 3532.36   2
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   8   4   0 82569.8 3246.22   4
   8  -4   0 86493.0 3410.19   3
   8   4   1 17035.7 1529.65   2
   8   4   1 17677.4 1567.49  13
   8  -4   1 16720.2 1578.64  12
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   8  -4   1 17451.4 1349.39   2
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   8   4   1 16427.4 1385.39   4
   8  -4   1 17879.1 1497.58   3
   8   4   2 76353.2 3395.05  13
   8  -4   2 74959.9 3464.53  12
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   8   4   2 78366.6 3434.99   2
   8  -4   2 77351.3 3058.08   2
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   8   4   2 77065.4 3137.16   4
   8  -4   2 79604.4 3339.13   3
   8   4   3 1643.33 533.790   2
   8  -4   3 1686.36 451.915   2
   8  -4   3 2246.73 613.746   3
   8   4   3 2721.86 667.738  13
   8  -4   3 1786.54 547.052  12
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   8   4   3 2157.40 559.673   4
   8   4   4 431.558 539.253   2
   8  -4   4 1468.55 512.556   2
   8  -4   4 588.376 485.421   3
   8   4   4 517.542 398.140  13
   8  -4   4-920.623 567.696  12
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   8   4   4 302.067 333.164   4
   8   4   5 7073.74 1099.81   2
   8  -4   5 7655.89 1096.11   3
   8  -4   5 7795.90 1064.23   2
   8   4   5 5899.10 985.562  13
   8  -4   5 7984.57 1167.01  12
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   8   4   5 6950.54 955.940   4
   8   4   6 25307.0 1975.03  13
   8  -4   6 25044.1 2058.22  12
  -8   4  -6 26271.3 1989.90  11
  -8  -4  -6 26514.8 1974.24   6
  -8  -4  -6 22534.2 1719.94  17
   8   4   6 26337.1 2170.99   2
  -8   4  -6 24323.5 2067.09   9
   8  -4   6 27984.8 2046.12   2
   8   4   6 27315.0 1900.49   4
   8  -4   6 25882.9 1993.55   3
   8   4   7 948.632 635.009   2
   8  -4   7 508.080 394.635   3
   8   4   7 843.547 618.631  13
   8  -4   7 596.599 474.096   2
   8  -4   7 400.983 421.800  12
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  -8  -4  -7 662.131 398.704  17
  -8   4  -7 339.653 415.418   9
   8   4   8 42364.9 2622.06  13
   8  -4   8 39373.7 2649.59  12
  -8   4  -8 42186.8 2633.33  11
  -8  -4  -8 42983.0 2626.81   6
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   8   4   8 41574.3 2872.44   2
  -8   4  -8 39997.6 2810.86   9
   8  -4   8 39776.6 2643.22   2
   8  -4   8 45707.8 2752.15   3
   8  -4   9 2666.39 793.154   3
   8   4   9 2964.82 750.602  13
   8   4   9 2021.57 686.415   2
   8  -4   9 2791.54 892.948  12
   8  -4   9 3982.85 913.839   2
  -8   4  -9 2570.90 764.965  11
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  -8   4  -9 1555.14 688.792   9
   8   4  10 66214.8 3475.04  13
   8  -4  10 67895.2 3656.04  12
  -8   4 -10 66419.8 3483.08  11
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  -8   4 -10 62988.8 3806.47   9
   8   4  10 62663.5 3839.63   2
   8  -4  10 65275.5 3615.06   2
   8  -4  10 72454.6 3665.29   3
   8  -4  11 3321.70 888.698   2
   8  -5 -16 126.065 449.043  16
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   8  -5 -15 47263.2 2769.25  16
  -8   5  14 369.775 448.466   7
  -8   5  14-108.255 412.263   1
   8  -5 -14 808.327 457.282  16
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   8  -5 -13 62835.3 3376.16  10
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   8   5 -13 68116.3 3691.46   5
   8  -5 -13 63629.7 3124.15  16
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   8   5 -12-766.041 668.097   5
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   8  -5  -9 20573.2 1766.31  10
   8   5  -9 21694.9 1893.48   5
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   8  -5  -9 20694.5 1618.77  16
   8  -5  -8 1268.77 486.012  14
   8   5  -8 1174.64 514.520  13
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   8   5  -8 567.927 434.765   5
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   8   5  -7 68090.2 3296.32  13
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   8  -5  -7 71956.5 3251.52  10
   8   5  -7 69197.8 3343.13   5
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   8  -5  -7 70714.9 2988.85  16
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   8  -5  -6-184.155 421.850  10
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   8  -5  -6 507.297 293.492   2
   8  -5  -5 147940. 4772.90   3
   8  -5  -5 148484. 4479.41  14
   8   5  -5 151934. 5182.64  13
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   8  -5  -5 146407. 5269.78  12
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   8   5  -5 154315. 5168.14   2
   8  -5  -5 150372. 4337.12   2
   8   5  -5 142849. 4921.28   5
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   8  -5  -5 151141. 4587.87  16
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   8   5  -4 1357.30 580.658  13
   8  -5  -4 441.856 348.946   3
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   8   5  -4 364.282 424.942   2
   8  -5  -4 917.866 369.451   2
   8  -5  -3 128658. 3958.30  14
   8   5  -3 128219. 4689.79  13
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   8  -5  -3 124155. 4740.06  12
  -8   5   3 123760. 3869.94  11
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   8   5  -3 123863. 4506.23   2
   8  -5  -3 134214. 3896.87   2
  -8  -5   3 124587. 4442.30  17
  -8   5   3 124216. 4525.94   9
   8  -5  -3 125780. 4364.87   3
   8  -5  -2 784.735 325.096   2
   8  -5  -2 1555.52 455.292  14
   8   5  -2 1403.06 554.816  13
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   8   5  -2 944.863 478.113   2
   8   5  -1 1507.63 568.207   2
   8  -5  -1 1414.66 375.486   2
   8  -5  -1 845.845 336.852  14
   8   5  -1 1042.80 407.142  13
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   8  -5  -1 428.186 430.662  12
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   8   5   0 1229.94 527.909   2
   8  -5   0 1940.72 485.653  14
   8  -5   0 2038.13 436.082   2
   8   5   0 2191.24 520.766  13
   8  -5   0 1820.01 533.278   3
   8  -5   0 1839.79 623.501  12
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   8   5   0 1490.92 497.397   4
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   8   5   1 28517.6 2079.39  13
   8  -5   1 30642.5 2216.76  12
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   8   5   1 29966.7 2104.97   2
   8  -5   1 31320.9 1784.39   2
  -8  -5  -1 25310.5 1870.81  17
  -8   5  -1 30403.9 2136.69   9
   8   5   1 31439.5 1997.61   4
   8  -5   1 32310.4 2114.59   3
   8  -5   1 31436.1 1788.38  14
   8  -5   2-137.062 330.768  14
   8   5   2-111.639 539.168   2
   8  -5   2 588.544 383.432   2
   8   5   2-392.322 410.702  13
   8  -5   2 54.9873 385.116   3
   8  -5   2-313.347 420.406  12
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  -8  -5  -2-684.531 554.255  17
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   8   5   2-381.209 424.741   4
   8   5   3 90563.5 3849.32  13
   8  -5   3 90512.0 3970.97  12
  -8   5  -3 93209.7 3703.82  11
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   8   5   3 93311.5 3909.99   2
  -8  -5  -3 88536.5 3654.72  17
  -8   5  -3 92171.7 3921.90   9
   8   5   3 90268.9 3623.89   4
   8  -5   3 91690.9 3797.51   3
   8   5   4 697.680 393.708   2
   8  -5   4 492.862 459.548   3
   8   5   4-179.663 369.778  13
   8  -5   4 710.025 478.634  12
  -8   5  -4 785.533 444.604  11
  -8  -5  -4 622.495 515.623   6
  -8  -5  -4 375.827 359.280  17
  -8   5  -4 926.406 552.720   9
   8   5   4 652.263 417.386   4
   8   5   5 133663. 4909.49  13
   8  -5   5 141737. 5161.27  12
  -8   5  -5 131075. 4781.63  11
  -8  -5  -5 143667. 4977.82   6
   8   5   5 145034. 5244.62   2
  -8  -5  -5 141898. 4774.99  17
  -8   5  -5 131389. 5092.35   9
   8   5   5 144616. 4841.96   4
   8  -5   5 139668. 4985.19   3
   8   5   6 865.156 569.654   2
   8  -5   6 449.937 487.701   3
   8   5   6 71.9228 400.672  13
   8  -5   6 343.303 602.564  12
  -8   5  -6-136.415 320.418  11
  -8  -5  -6-97.2463 367.292   6
  -8  -5  -6 104.218 355.783  17
  -8   5  -6-227.171 435.679   9
   8   5   6 566.181 513.360   4
   8   5   7 29242.2 2194.09  13
   8  -5   7 27946.8 2210.04  12
  -8   5  -7 33094.8 2333.44  11
  -8  -5  -7 31597.9 2262.69   6
  -8  -5  -7 29034.4 1998.04  17
   8   5   7 32849.9 2515.63   2
  -8   5  -7 28669.5 2334.75   9
   8   5   7 30814.4 2153.04   4
   8  -5   7 29118.8 2240.52   3
   8  -5   8 1153.95 495.405   3
   8   5   8 774.159 503.412   2
   8   5   8 1055.98 512.300  13
   8  -5   8 2815.93 821.605  12
  -8   5  -8 1555.58 670.568  11
  -8  -5  -8 1810.29 606.396   6
  -8  -5  -8 1636.01 545.374  17
  -8   5  -8 685.217 432.917   9
   8  -5   9 2327.24 836.187   3
   8   5   9 655.581 468.702  13
   8   5   9 1346.44 760.180   2
   8  -5   9 809.865 528.204  12
  -8   5  -9 1563.53 585.650  11
  -8  -5  -9 1162.89 515.975   6
  -8  -5  -9 1231.83 415.799  17
  -8   5  -9 1195.61 631.165   9
   8   5  10 4414.22 930.424  13
  -8   6  15 974.371 512.961   7
  -8   6  14 5421.77 938.506   7
   8  -6 -14 8810.74 1209.48  16
  -8  -6  13 1089.91 783.392   7
  -8   6  13-68.7241 398.718   7
   8  -6 -13 1127.02 696.450  10
   8  -6 -13 544.081 464.983  16
   8  -6 -12 58050.2 3112.20  14
  -8  -6  12 52964.0 3384.61   7
  -8   6  12 53743.6 2963.74   7
   8  -6 -12 55965.7 3174.55  10
   8   6 -12 60009.2 3397.80   5
  -8  -6  12 53784.4 2915.57  17
   8  -6 -12 55455.9 2949.87  16
   8  -6 -11 7894.80 1136.14  14
   8   6 -11 8950.97 1263.37  13
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  -8   6  11 8103.37 1109.25   7
   8  -6 -11 8890.19 1222.56  10
   8   6 -11 8549.06 1289.37   5
  -8  -6  11 8107.64 1158.94  17
   8  -6 -11 8080.43 1116.00  16
   8  -6 -10 74692.1 3409.74  14
   8   6 -10 75032.9 3672.43  13
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  -8   6  10 77784.7 3484.05   7
   8  -6 -10 77790.0 3659.71  10
   8   6 -10 68837.2 3624.74   5
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   8  -6 -10 72357.8 3320.93  16
   8  -6  -9 3814.53 770.022  14
   8   6  -9 4243.15 877.430  13
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  -8   6   9 5057.57 905.319   7
   8  -6  -9 3216.09 766.697  10
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   8   6  -9 4031.18 798.397   5
   8  -6  -9 4625.09 850.497  16
   8  -6  -8 36291.0 2221.62  14
   8   6  -8 33450.7 2346.38  13
  -8  -6   8 33750.2 2291.85   7
  -8   6   8 32934.8 2172.35   7
   8  -6  -8 30012.2 2168.22  10
   8   6  -8 30360.0 2282.13   5
  -8  -6   8 32864.5 2238.95  17
   8  -6  -8 31187.0 2043.81  16
   8  -6  -7 2229.20 628.797  14
   8   6  -7 3699.05 899.450  13
  -8  -6   7 2518.35 704.056   7
  -8   6   7 3679.67 738.680   7
   8   6  -7 2657.46 738.359   2
   8  -6  -7 2061.11 594.441  10
  -8  -6   7 3366.80 795.178  17
   8   6  -7 2053.23 587.481   5
   8  -6  -7 3071.15 684.508  16
  -8   6   7 2822.94 760.971   9
   8  -6  -6 5110.95 828.352  14
   8   6  -6 6191.67 1109.79  13
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   8  -6  -6 3917.77 841.910  10
  -8  -6   6 5666.60 830.591   6
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   8   6  -6 6090.74 1018.94   5
   8  -6  -6 4748.24 818.570  16
  -8   6   6 7368.45 1119.57   9
   8   6  -6 5244.51 966.095   2
   8  -6  -5 2327.44 614.133  14
   8   6  -5 2226.14 680.543  13
   8  -6  -5 4413.47 813.347   3
  -8  -6   5 2293.42 623.141   7
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  -8  -6   5 2837.37 693.312  17
   8  -6  -5 2901.78 675.102  16
  -8   6   5 2670.72 715.230   9
   8   6  -5 3028.65 709.966   2
   8  -6  -4 24155.4 1851.30   3
   8  -6  -4 19522.1 1513.94  14
   8   6  -4 21251.1 1878.23  13
  -8  -6   4 22300.2 1710.35   7
   8  -6  -4 20875.7 1912.94  12
  -8  -6   4 20724.2 1608.84   6
   8   6  -4 21428.3 1802.11   2
  -8  -6   4 21210.8 1779.41  17
  -8   6   4 20838.5 1779.29   9
   8  -6  -3 3095.72 605.806  14
   8   6  -3 4464.61 939.515  13
   8  -6  -3 2551.55 644.480   3
   8  -6  -3 4047.49 933.838  12
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  -8  -6   3 2766.82 651.463   6
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  -8   6   3 2371.06 655.036   9
   8   6  -3 3543.95 804.992   2
   8  -6  -2 86890.6 3278.61  14
   8   6  -2 94335.2 4028.55  13
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   8  -6  -2 92758.1 4091.70  12
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   8   6  -2 90081.1 3786.77   2
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  -8   6   2 83551.5 3683.40   9
   8  -6  -2 91183.2 3787.48   3
   8   6  -1 12328.6 1343.31   2
   8  -6  -1 12520.3 1174.18  14
   8   6  -1 12701.4 1438.62  13
   8  -6  -1 12648.4 1387.95   3
   8  -6  -1 13488.8 1524.28  12
  -8   6   1 12635.2 1231.42  11
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  -8  -6   1 11050.7 1270.10  17
   8   6  -1 12803.8 1334.64   4
  -8   6   1 11578.0 1332.30   9
   8  -6   0 78560.9 3115.61  14
   8   6   0 84447.9 3768.29  13
   8  -6   0 84260.0 3861.26  12
  -8   6   0 77865.2 3270.31  11
  -8  -6   0 80398.3 3477.43   6
   8   6   0 77674.0 3515.61   2
  -8  -6   0 76801.5 3501.83  17
  -8   6   0 78300.5 3554.83   9
   8   6   0 79201.3 3423.70   4
   8  -6   0 84920.5 3662.04   3
   8   6   1 601.064 398.513   2
   8  -6   1 252.162 326.890  14
   8   6   1 125.972 393.694  13
   8  -6   1 862.420 419.152   3
   8  -6   1-432.296 587.974  12
  -8   6  -1 172.631 346.868  11
  -8  -6  -1 795.622 522.657   6
  -8  -6  -1-1300.08 708.316  17
   8   6   1 566.268 444.023   4
  -8   6  -1-533.440 505.058   9
   8   6   2 59064.1 3116.39  13
   8  -6   2 52424.9 3054.25  12
  -8   6  -2 51052.3 2722.75  11
  -8  -6  -2 54599.8 2907.08   6
   8   6   2 59004.1 3070.67   2
  -8  -6  -2 52056.2 2838.34  17
  -8   6  -2 56087.0 3022.65   9
   8   6   2 56153.0 2850.14   4
   8  -6   2 55891.8 2994.16   3
   8  -6   2 61020.5 2700.43  14
   8  -6   3 1816.99 534.539  14
   8   6   3 1808.77 579.004   2
   8   6   3 2030.80 677.765  13
   8  -6   3 1076.72 567.545   3
   8  -6   3 3097.54 855.875  12
  -8   6  -3 2577.85 690.784  11
  -8  -6  -3 2208.39 742.308   6
  -8  -6  -3 1082.55 461.021  17
  -8   6  -3 1784.47 684.075   9
   8   6   3 2169.87 626.714   4
   8   6   4 4027.09 885.761   2
   8   6   4 4609.78 889.019  13
   8  -6   4 4589.20 911.710   3
   8  -6   4 4507.81 938.915  12
  -8   6  -4 3775.14 790.669  11
  -8  -6  -4 4408.75 869.876   6
  -8  -6  -4 3015.98 698.069  17
  -8   6  -4 3730.10 879.216   9
   8   6   4 4892.12 865.181   4
   8   6   5 2160.92 755.633   2
   8   6   5 601.402 371.840  13
   8  -6   5 1233.99 561.976   3
   8  -6   5 1879.29 656.035  12
  -8   6  -5 1674.21 659.682  11
  -8  -6  -5 1468.11 628.863   6
  -8  -6  -5 1653.33 601.585  17
  -8   6  -5 2193.07 733.128   9
   8   6   5 2186.95 692.100   4
   8   6   6 23801.5 2010.28  13
   8  -6   6 20741.4 1921.50  12
  -8   6  -6 19582.5 1831.69  11
  -8  -6  -6 22943.4 1967.01   6
  -8  -6  -6 21934.1 1798.18  17
   8   6   6 26748.5 2252.79   2
   8   6   6 22657.3 1901.03   4
  -8   6  -6 19702.7 1915.16   9
   8  -6   6 23397.7 2033.66   3
   8   6   7 8195.67 1298.12   2
   8   6   7 7677.65 1162.01  13
   8  -6   7 6912.25 1172.59   3
   8  -6   7 8233.20 1251.29  12
  -8   6  -7 5850.27 1068.61  11
  -8  -6  -7 7612.68 1176.58   6
  -8  -6  -7 7541.11 1088.01  17
  -8   6  -7 6419.78 1169.27   9
   8   6   7 6521.11 989.586   4
   8   6   8 54106.9 3106.17  13
   8  -6   8 53769.0 3200.37  12
  -8   6  -8 47031.1 2968.93  11
  -8  -6  -8 54314.2 3139.57   6
  -8  -6  -8 49185.0 2745.87  17
   8   6   8 57293.4 3480.03   2
  -8   6  -8 49615.6 3277.47   9
   8  -6   8 52133.9 3167.09   3
   8   6   9 95.6613 504.051  13
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   8  -7 -13 48051.5 2937.78  14
   8  -7 -13 42903.6 2708.49  16
   8  -7 -12-160.670 446.685  14
   8   7 -12-510.278 448.559  13
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  -8   7  12-165.360 372.650   7
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   8  -7 -12-185.676 432.940  16
   8  -7 -11 721.841 562.561  14
   8   7 -11 2303.81 691.754  13
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   8  -7 -11 1040.29 558.995  10
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   8   7 -11 1119.44 455.639   5
   8  -7 -11 2281.27 701.639  16
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   8   7 -10-464.679 597.567  13
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   8  -7 -10 1224.43 502.867  10
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   8   7 -10 1444.27 608.929   5
   8  -7 -10 173.868 401.931  16
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   8   7  -9 7685.02 1223.78  13
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   8  -7  -9 8457.17 1230.41  10
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   8   7  -9 8364.08 1247.72   5
   8  -7  -9 8407.75 1133.89  16
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   8  -7  -8 868.753 387.857  14
   8   7  -8 123.814 501.826  13
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   8   7  -8 200.303 587.421   2
   8  -7  -8 431.728 503.575  10
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   8   7  -8 459.492 505.301   5
   8  -7  -8 854.388 482.353  16
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   8  -7  -7 61658.1 3035.32  14
   8   7  -7 69258.6 3597.81  13
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   8  -7  -7 66438.9 3330.53  10
   8   7  -7 61549.7 3351.62   2
   8   7  -7 63115.7 3337.73   5
  -8  -7   7 55858.9 3131.73  17
   8  -7  -7 65116.1 3123.10  16
  -8   7   7 64495.9 3392.20   9
  -8   7   7 66755.2 3625.41  15
   8  -7  -6-0.79985 482.040  14
   8   7  -6 157.402 392.401  13
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   8  -7  -6 568.391 469.524  16
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   8   7  -6-298.200 480.360   2
   8  -7  -5 132248. 4503.75  14
   8  -7  -5 131587. 4729.73   3
   8   7  -5 129151. 5073.89  13
  -8  -7   5 128716. 4511.05   7
  -8  -7   5 126423. 4466.12   6
   8   7  -5 133088. 4931.98   2
  -8  -7   5 125091. 4828.52  17
   8  -7  -5 127034. 4498.63  16
  -8   7   5 126121. 4811.46   9
   8  -7  -4 1184.11 521.149  14
   8   7  -4 413.602 573.581  13
   8  -7  -4 855.208 540.169   3
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   8  -7  -4-791.119 653.184  12
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   8   7  -4 173.030 420.994   2
   8  -7  -3 35337.8 2373.96   3
   8  -7  -3 38602.8 2209.78  14
   8   7  -3 38445.3 2602.32  13
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   8  -7  -3 35149.6 2524.34  12
  -8  -7   3 37616.6 2344.43   6
   8   7  -3 37298.4 2430.91   2
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  -8   7   3 36881.4 2446.65   9
   8   7  -2 1953.57 589.362   2
   8  -7  -2 1415.48 530.691  14
   8   7  -2 838.036 528.903  13
   8  -7  -2 1552.91 548.134   3
   8  -7  -2 2012.34 617.627  12
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  -8   7   2 193.904 427.474   9
   8   7  -1 4928.73 898.699   2
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   8   7  -1 5102.48 989.885  13
   8  -7  -1 4675.91 898.961   3
   8  -7  -1 6175.22 1103.46  12
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   8   7  -1 6102.43 1002.29   4
  -8   7   1 5913.02 1004.04   9
   8   7   0 308.187 405.875   2
   8  -7   0-574.040 432.929  14
   8   7   0-280.837 569.776  13
   8  -7   0-162.077 486.617   3
   8  -7   0 425.294 436.472  12
  -8   7   0-133.338 278.651  11
  -8  -7   0-71.2168 355.056   6
  -8  -7   0 1052.52 407.766  17
   8   7   0 0.88181 459.019   4
  -8   7   0 395.214 443.967   9
   8   7   1 14661.4 1537.36   2
   8   7   1 17569.6 1733.40  13
   8  -7   1 15365.9 1601.14   3
   8  -7   1 16711.2 1750.72  12
  -8   7  -1 13370.8 1372.23  11
  -8  -7  -1 15354.4 1579.87   6
  -8  -7  -1 15045.6 1562.12  17
   8   7   1 14075.5 1491.92   4
  -8   7  -1 13881.9 1503.41   9
   8  -7   1 15792.4 1417.35  14
   8  -7   2 2984.59 650.965  14
   8   7   2 4019.97 866.968   2
   8   7   2 4567.70 971.618  13
   8  -7   2 3995.97 858.920   3
   8  -7   2 3223.72 920.288  12
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  -8   7  -2 4148.60 871.968   9
   8   7   2 4624.93 808.760   4
   8   7   3 103286. 4406.54  13
   8  -7   3 104701. 4534.94  12
  -8   7  -3 103698. 4244.00  11
  -8  -7  -3 108115. 4438.52   6
   8   7   3 108438. 4478.99   2
  -8  -7  -3 102783. 4283.23  17
  -8   7  -3 106482. 4513.74   9
   8   7   3 107536. 4278.38   4
   8  -7   3 101749. 4384.10   3
   8  -7   3 103929. 3914.73  14
   8  -7   4 1477.03 452.407  14
   8   7   4 1961.93 745.316   2
   8   7   4 2557.39 727.928  13
   8  -7   4 1446.06 666.489   3
   8  -7   4 2373.82 790.741  12
  -8   7  -4 1537.86 609.087  11
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  -8  -7  -4 198.435 380.354  17
  -8   7  -4 684.827 593.699   9
   8   7   4 2121.22 652.021   4
   8   7   5 85547.7 3965.72  13
   8  -7   5 82343.0 3990.25  12
  -8   7  -5 74161.4 3687.45  11
  -8  -7  -5 80584.2 3870.39   6
  -8  -7  -5 80197.8 3733.41  17
   8   7   5 81396.5 4009.12   2
  -8   7  -5 81126.9 4037.44   9
   8   7   5 78740.5 3724.91   4
   8  -7   5 82935.3 4022.05   3
   8  -7   5 80439.0 3424.94  14
   8   7   6 1313.11 632.885   2
   8   7   6 3102.37 790.847  13
   8  -7   6 2044.74 803.503   3
   8  -7   6 1986.63 755.233  12
  -8   7  -6 1117.90 513.499  11
  -8  -7  -6 2010.82 671.219   6
  -8  -7  -6 1015.98 525.786  17
  -8   7  -6 1455.89 656.063   9
   8   7   6 1994.23 635.535   4
   8   7   7 17367.1 1903.56   2
   8   7   7 18040.0 1813.96  13
   8  -7   7 17091.7 1847.40   3
   8  -7   7 17562.3 1829.56  12
  -8   7  -7 14783.8 1695.40  11
  -8  -7  -7 15712.0 1688.75   6
  -8  -7  -7 16113.9 1604.79  17
  -8   7  -7 20913.2 2103.75   9
   8   7   7 19027.4 1833.39   4
   8   7   8 753.706 621.115  13
  -8  -7  -8 1659.69 617.477  17
  -8  -7  -9 3774.73 800.567  17
   8   8 -12 62625.4 3702.70  13
  -8  -8  12 60723.2 3647.68   7
  -8  -8  12 56755.6 3221.94  17
   8  -8 -12 60178.4 3275.37  16
   8  -8 -11 1576.46 556.910  14
   8   8 -11 1927.42 680.219  13
  -8  -8  11 4228.50 998.518   7
  -8  -8  11 2871.85 760.069  17
   8  -8 -11 4099.91 925.634  16
   8  -8 -10 45861.5 2794.08  14
   8   8 -10 45264.5 3075.01  13
  -8  -8  10 44660.6 2918.16   7
   8  -8 -10 44902.8 2876.68  10
  -8  -8  10 40483.8 2734.88  17
   8  -8 -10 43312.1 2705.07  16
   8  -8  -9 826.488 429.730  14
   8   8  -9 1750.03 675.680  13
  -8  -8   9 2791.71 698.499   7
   8   8  -9 365.490 472.552   2
   8  -8  -9 396.282 489.331  10
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   8   8  -9 1828.66 725.283   5
   8  -8  -9 1054.61 535.620  16
  -8   8   9 2468.82 895.839  15
   8  -8  -8 58504.3 3100.09  14
   8   8  -8 61255.2 3529.24  13
  -8  -8   8 56757.7 3077.52   7
   8  -8  -8 54940.4 3155.55  10
   8   8  -8 56246.6 3267.83   2
  -8  -8   8 53928.9 3194.35  17
   8   8  -8 55701.1 3253.11   5
   8  -8  -8 55485.6 3014.30  16
  -8   8   8 56810.2 3517.57  15
   8  -8  -7 4865.51 897.807  14
   8   8  -7 5127.62 1064.07  13
  -8  -8   7 4304.03 864.930   7
   8  -8  -7 5426.08 1042.94  10
  -8  -8   7 5213.35 1021.71  17
   8  -8  -7 4011.13 892.882  16
  -8   8   7 4600.59 930.974   9
  -8   8   7 4348.11 988.621  15
   8   8  -7 4163.42 884.252   2
   8  -8  -6 3759.72 840.168  14
   8   8  -6 2801.01 784.586  13
  -8  -8   6 3710.82 741.387   7
  -8  -8   6 4356.36 840.184   6
  -8  -8   6 4223.32 928.466  17
   8  -8  -6 2212.33 670.366  16
  -8   8   6 4709.87 966.730   9
  -8   8   6 5050.07 1082.70  15
   8   8  -6 4091.82 904.971   2
   8  -8  -5 116.077 403.848  14
   8   8  -5 383.212 524.587  13
  -8  -8   5 34.1167 356.889   7
   8  -8  -5-91.1410 380.549   3
  -8  -8   5 578.500 343.346   6
  -8  -8   5 1399.55 705.140  17
   8  -8  -5-221.780 489.181  16
  -8   8   5 132.162 430.113   9
  -8   8   5 769.700 543.948  15
   8   8  -5 631.424 522.635   2
   8  -8  -4 43371.8 2502.29  14
   8  -8  -4 43670.5 2723.22   3
   8   8  -4 43148.2 2899.80  13
  -8  -8   4 40462.2 2334.58   7
  -8  -8   4 39480.6 2511.61   6
   8   8  -4 42341.6 2677.04   2
  -8  -8   4 39000.1 2709.24  17
  -8   8   4 42328.9 2688.71   9
  -8   8   4 40700.1 2783.11  15
   8  -8  -3 6663.53 978.314  14
   8   8  -3 8171.39 1278.37  13
   8  -8  -3 6984.79 1174.81   3
   8  -8  -3 7277.56 1188.70  12
  -8  -8   3 6942.53 954.277   7
  -8  -8   3 6248.68 1038.07   6
  -8  -8   3 10064.2 1402.86  17
  -8   8   3 6480.31 1043.50   9
   8   8  -3 8083.45 1182.27   2
   8  -8  -2 47797.9 2612.91  14
   8  -8  -2 50203.7 2990.83   3
   8   8  -2 49756.8 3074.75  13
   8  -8  -2 53282.8 3230.17  12
  -8  -8   2 44507.6 2747.43   6
   8   8  -2 47475.5 2801.82   2
  -8  -8   2 53617.6 3139.56  17
   8   8  -2 45286.6 2763.53   4
  -8   8   2 50586.1 2939.12   9
   8   8  -1 1826.17 637.816   2
   8  -8  -1 1389.48 510.149  14
   8   8  -1 1729.81 585.821  13
   8  -8  -1 1425.67 626.644   3
   8  -8  -1 1534.01 633.585  12
  -8   8   1 1334.48 423.563  11
  -8  -8   1 1688.12 684.961   6
  -8  -8   1 2915.48 863.673  17
   8   8  -1 2050.89 608.366   4
  -8   8   1 307.308 430.725   9
   8  -8   0 79661.6 3413.76  14
   8  -8   0 74767.3 3751.88   3
   8   8   0 74092.2 3790.76  13
   8  -8   0 70552.5 3773.29  12
  -8   8   0 73043.7 3381.27  11
  -8  -8   0 67891.4 3491.92   6
   8   8   0 78364.8 3666.67   2
  -8  -8   0 67888.8 3609.96  17
  -8   8   0 69953.9 3578.93   9
   8   8   0 74925.4 3606.72   4
   8  -8   1 14553.5 1434.80  14
   8   8   1 14108.7 1550.94   2
   8   8   1 15504.7 1725.34  13
   8  -8   1 13083.3 1562.13   3
   8  -8   1 14491.7 1668.83  12
  -8   8  -1 11029.7 1311.71  11
  -8  -8  -1 14509.4 1610.51   6
  -8  -8  -1 13358.8 1617.98  17
  -8   8  -1 13559.6 1564.67   9
   8   8   1 13804.6 1507.21   4
   8   8   2 71274.8 3671.05  13
   8  -8   2 73766.8 3789.05  12
  -8   8  -2 62996.7 3325.11  11
  -8  -8  -2 64700.0 3480.95   6
   8   8   2 72865.5 3620.73   2
  -8  -8  -2 68877.4 3607.86  17
  -8   8  -2 69882.1 3609.44   9
   8   8   2 67052.0 3439.72   4
   8  -8   2 68403.6 3210.50  14
   8  -8   2 68046.0 3645.58   3
   8  -8   3 3271.96 718.723  14
   8   8   3 3047.74 826.936   2
   8   8   3 5119.55 1035.30  13
   8  -8   3 3594.21 857.815   3
   8  -8   3 3145.03 849.709  12
  -8   8  -3 2797.28 729.025  11
  -8  -8  -3 3418.89 929.961   6
  -8  -8  -3 4279.52 989.678  17
  -8   8  -3 3283.61 827.535   9
   8   8   3 3564.23 867.318   4
   8  -8   4 1073.64 502.305  14
   8   8   4 1065.44 638.073   2
   8   8   4 1305.92 620.501  13
   8  -8   4 158.400 449.700   3
   8  -8   4 466.957 577.948  12
  -8   8  -4 461.033 522.587  11
  -8  -8  -4 245.772 393.028   6
  -8  -8  -4 510.844 408.041  17
  -8   8  -4-582.964 681.651   9
   8   8   4 121.667 436.288   4
   8  -8   5 788.625 490.565  14
   8   8   5 1906.89 758.672   2
   8   8   5 1681.16 717.354  13
   8  -8   5 998.518 571.709   3
   8  -8   5 323.054 455.859  12
  -8   8  -5 76.9513 503.585  11
  -8  -8  -5 1512.05 677.383   6
  -8  -8  -5-377.697 596.241  17
  -8   8  -5 473.648 548.630   9
   8   8   5-322.286 608.383   4
   8   8   6 21482.1 2022.08  13
   8  -8   6 22631.6 2109.00  12
  -8   8  -6 20104.4 1969.88  11
  -8  -8  -6 24626.0 2173.46   6
  -8  -8  -6 21009.2 1909.93  17
   8   8   6 21162.0 2102.10   2
  -8   8  -6 22437.5 2186.39   9
   8   8   6 25470.6 2171.38   4
   8  -8   6 25518.5 1936.33  14
   8  -8   6 23983.5 2210.56   3
  -8  -8  -7 785.430 419.714  17
   8   8   7-148.570 624.484   4
  -8  -8  -8 21898.8 1914.82  17
  -8  -9  11 2708.21 844.443   7
   8   9 -10 1802.73 765.515  13
  -8  -9  10 1023.92 515.352   7
  -8  -9  10 222.410 442.249  17
   8  -9 -10 1078.77 541.074  16
   8  -9  -9 8274.17 1232.65  14
   8   9  -9 9508.78 1490.54  13
  -8  -9   9 6819.41 1076.33   7
  -8  -9   9 8382.46 1268.69  17
   8  -9  -9 9788.54 1322.51  16
   8   9  -9 6026.33 1094.93   2
   8  -9  -8-197.018 548.460  14
   8   9  -8 1193.91 705.555  13
  -8  -9   8 32.1922 407.593   7
  -8  -9   8 693.773 609.714  17
   8  -9  -8 206.971 440.405  16
  -8   9   8 1786.86 858.022  15
   8   9  -8 386.189 443.554   2
   8  -9  -7 54251.8 3021.54  14
   8   9  -7 51722.6 3387.35  13
  -8  -9   7 55204.5 2950.00   7
   8  -9  -7 55665.3 3239.96  10
   8   9  -7 51453.1 3128.98   2
  -8  -9   7 52502.1 3265.00  17
   8  -9  -7 46411.4 2844.98  16
  -8   9   7 51386.1 3137.72   9
  -8   9   7 52193.9 3461.17  15
   8  -9  -6 2740.55 763.375  14
   8   9  -6 2544.12 749.144  13
  -8  -9   6 2738.17 693.775   6
  -8  -9   6 4357.16 976.972  17
   8  -9  -6 2204.12 633.553  16
  -8   9   6 2093.31 656.497   9
   8   9  -6 2478.82 717.699   2
   8  -9  -5 107657. 4312.68  14
   8   9  -5 111667. 4981.69  13
  -8  -9   5 87263.5 4095.50   6
   8   9  -5 103007. 4430.97   2
  -8  -9   5 94272.3 4528.34  17
   8  -9  -5 101009. 4246.28  16
  -8   9   5 105429. 4519.77   9
  -8   9   5 101636. 4772.40  15
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   9   1   0 119956. 4348.49  13
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   9  -1   0 117358. 4185.32  12
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   9   1   0 115681. 4297.43   2
   9  -1   0 113457. 4151.31   2
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   9   1   0 116360. 3685.41   4
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   9   1   1 1658.90 608.901   2
   9  -1   1 1237.65 417.305   2
   9   1   1 443.186 420.067  13
   9  -1   1 451.621 358.180  13
   9   1   1 760.561 424.528  12
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   9   2  -9 8730.20 1247.88   5
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   9   2  -3 33526.6 2205.07   2
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   9   2   1 47770.5 2707.20   2
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   9   2   1 49631.4 2372.52   4
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   9   2   3 116083. 4460.00  13
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   9   2   3 117477. 4534.04   2
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   9   2   4 3409.88 760.796   2
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   9   2   5 48245.9 2840.63  13
   9   2   5 46525.9 2661.97  12
   9  -2   5 49356.6 2907.89  12
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   9   2   5 51482.3 3034.69   2
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   9  -2   5 50692.5 2892.35   2
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   9   2   6-119.989 459.001   2
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   9   2   7 33333.3 2399.00  13
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   9   2   7 30094.8 2457.37   2
   9  -2   7 31132.7 2429.25   2
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   9   2   8 289.548 569.688   2
   9   2   8 329.083 441.148  13
   9  -2   8-470.821 449.059   2
   9  -2   8 4.43824 429.777  12
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   9  -2   9 830.232 559.948   2
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   9  -2  10 262.047 574.996   2
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   9  -3 -14 14896.6 1665.15  10
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   9  -3 -13 1307.44 632.222  10
   9   3 -13 806.899 589.610   5
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   9  -3 -12 26353.8 2093.09  10
   9   3 -12 24634.2 2216.82   5
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   9  -3 -11-318.158 426.160  10
   9  -3 -11 137.327 384.244   5
   9   3 -11-168.041 458.329   5
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   9  -3 -10 68649.8 3286.21  10
   9   3 -10 69884.2 3644.30   5
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   9  -3  -9 1812.83 597.133  10
   9   3  -9 2021.73 663.849   5
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   9   3  -8 77188.6 3422.49  13
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   9  -3  -8 82045.9 3607.08  12
   9  -3  -8 83565.8 3502.37  10
   9   3  -8 74625.4 3633.83   5
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   9   3  -7 811.849 368.431  13
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   9  -3  -7 944.815 438.017  12
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   9  -3  -7 1225.96 463.368  10
   9   3  -7 971.337 532.367   5
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   9   3  -7 1356.07 591.156   2
   9  -3  -7 205.994 386.027   2
   9   3  -6 1464.23 542.226  13
   9  -3  -6 596.346 345.195  12
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   9  -3  -6 616.200 426.544  10
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   9   3  -6 1159.80 514.564   5
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   9   3  -6 348.298 483.484   2
   9  -3  -6 785.664 383.697   2
   9   3  -5 971.618 493.392  13
   9  -3  -5 1297.33 555.979  12
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   9  -3  -5 1143.42 485.690  10
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   9   3  -5 1754.28 588.673   5
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   9   3  -5 566.011 531.618   2
   9  -3  -5 822.655 366.575   2
   9   3  -4 15512.7 1539.58  13
   9  -3  -4 14826.4 1267.68  13
   9  -3  -4 16688.1 1573.70  12
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   9  -3  -4 15003.4 1377.01  10
   9  -3  -4 14746.1 1362.21   2
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  -9   3   4 15664.4 1553.68   9
   9  -3  -4 16303.9 1386.82   3
   9   3  -4 14272.6 1498.76   2
   9  -3  -3 120.739 314.399   2
   9   3  -3 137.346 396.800  13
   9  -3  -3 173.389 286.799   3
   9  -3  -3-7.49986 309.878  13
   9  -3  -3 201.907 407.690  12
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  -9  -3   3 189.763 326.181   6
  -9  -3   3 11.4735 377.371  17
  -9   3   3-2.52152 430.052  17
  -9   3   3 41.6056 383.209   9
   9   3  -3-177.728 464.662   2
   9   3  -2 43315.4 2587.87  13
   9  -3  -2 43410.1 2326.44  13
   9  -3  -2 42100.9 2553.18  12
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   9   3  -2 41448.4 2537.30   2
   9  -3  -2 43725.1 2329.76   2
  -9  -3   2 41645.2 2460.86  17
  -9   3   2 39923.9 2427.37  17
  -9   3   2 41625.3 2502.20   9
  -9  -3   2 44664.9 2284.66   9
   9  -3  -2 42317.9 2323.70   3
   9   3  -1 2873.25 704.919   2
   9  -3  -1 3311.88 662.216   2
   9  -3  -1 4705.15 822.035   3
   9   3  -1 2747.14 658.740  13
   9  -3  -1 4269.94 786.854  13
   9   3  -1 3665.57 625.226  12
   9  -3  -1 3990.53 825.566  12
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  -9  -3   1 3625.59 689.696   6
  -9  -3   1 4377.00 897.598  17
  -9   3   1 4148.17 826.540  17
  -9   3   1 2810.89 665.311   9
  -9  -3   1 3818.60 644.614   9
   9   3   0 145852. 5052.53  13
   9   3   0 144463. 4395.31  12
   9  -3   0 144079. 5083.98  12
  -9   3   0 135222. 4590.61  11
  -9  -3   0 146160. 4738.79   6
   9   3   0 148462. 5112.87   2
   9  -3   0 149930. 4699.09   2
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  -9   3   0 147128. 5075.12   9
   9   3   0 147035. 4599.01   4
   9  -3   0 146008. 4778.65   3
   9   3   1 367.488 499.891   2
   9  -3   1-368.639 368.672   2
   9   3   1-87.9807 426.803  13
   9   3   1-114.832 334.676  12
   9  -3   1-511.335 515.281  12
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   9   3   1-20.8224 298.450   4
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   9  -3   1 884.963 480.388   3
   9   3   2 55784.7 2991.03  13
   9   3   2 54944.2 2638.85  12
   9  -3   2 53854.4 2982.86  12
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   9   3   2 51275.1 2904.88   2
   9  -3   2 55271.0 2776.37   2
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  -9   3  -2 53481.2 2933.51   9
   9   3   2 57780.6 2687.41   4
   9  -3   2 55391.2 2844.01   3
   9   3   3-1034.07 625.478   2
   9  -3   3-395.417 473.335   2
   9   3   3 433.758 406.596  13
   9   3   3 568.914 398.144  12
   9  -3   3 266.697 436.010  12
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   9   3   3 159.604 294.657   4
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   9   3   4-33.3086 344.624   4
   9   3   5-307.989 624.833   2
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   9   3   5-381.334 561.935  13
   9  -3   5 35.6482 363.932  12
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   9   3   6 6409.60 1158.15   2
   9   3   6 3731.60 858.962  13
   9  -3   6 3597.47 838.041   2
   9  -3   6 4399.79 961.565  12
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   9   3   8 69699.8 3627.01  13
   9  -3   8 65111.6 3622.36  12
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   9   3   8 69843.5 3917.92   2
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   9  -3   9-307.763 441.669   2
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   9  -3  10 77910.7 4223.89   2
   9  -3  11 228.792 504.979   2
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  -9   4  13 36816.9 2692.30   7
   9  -4 -13 34924.5 2537.47  10
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   9  -4 -12 278.018 419.030  10
   9   4 -12 529.841 541.774   5
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   9  -4 -11 2123.75 660.434  10
   9   4 -11 1839.40 711.982   5
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   9  -4 -10 4266.52 884.160  10
   9   4 -10 4427.27 973.859   5
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   9   4  -9 19052.9 1712.20  13
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   9  -4  -9 15585.0 1614.42  12
   9  -4  -9 18685.3 1723.34  10
   9   4  -9 18688.4 1839.44   5
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   9   4  -8-262.839 390.282  13
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   9   4  -8 204.619 550.217   2
   9  -4  -8 593.167 445.878  10
   9   4  -8 637.573 477.237   5
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   9   4  -7 101039. 4140.24  13
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  -9   4   7 102229. 4244.30   7
   9  -4  -7 99746.6 4269.52  12
   9  -4  -7 104258. 4074.79  10
   9   4  -7 100005. 4341.40   2
   9  -4  -7 101042. 3826.09   2
   9   4  -7 93167.1 4107.30   5
  -9  -4   7 102775. 4132.23  17
   9   4  -6 758.080 533.531  13
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   9  -4  -6-169.749 451.363  12
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   9   4  -6-273.415 576.364   2
   9  -4  -6 188.416 318.388   2
   9   4  -5 115860. 4525.15  13
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   9  -4  -5 119617. 4687.57  12
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   9  -4  -5 120607. 4363.77  10
   9   4  -5 110424. 4512.60   2
   9  -4  -5 122927. 4139.09   2
   9   4  -5 117383. 4455.88   5
  -9  -4   5 113334. 4373.70  17
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   9   4  -4 3039.66 781.631  13
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   9  -4  -4 2170.18 629.529  12
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   9   4  -4 2630.46 731.365   2
   9  -4  -4 2964.42 630.327   2
   9   4  -3 25926.0 2020.44  13
   9  -4  -3 27289.8 1782.42  13
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   9  -4  -3 26294.3 2098.44  12
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   9   4  -3 26216.6 2030.22   2
   9  -4  -3 28452.4 1806.65   2
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   9  -4  -3 31073.6 2056.83   3
   9   4  -2 8093.50 1143.19   2
   9  -4  -2 9976.38 1084.54   2
   9   4  -2 9232.32 1221.22  13
   9  -4  -2 8878.34 1142.41   3
   9  -4  -2 8411.34 1195.37  12
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   9   4  -1 4232.79 811.364   2
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   9   4  -1 2499.71 716.786  13
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   9  -4  -1 3192.23 771.465  12
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   9   4  -1 3174.54 687.347   4
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   9   4   0 1428.34 633.389   2
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   9   4   0 1005.47 496.786   4
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   9   4   1 29371.5 2174.44  13
   9  -4   1 27948.4 2186.43  12
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   9   4   1 26880.0 2077.04   2
   9  -4   1 29160.4 1902.43   2
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  -9   4  -1 25547.1 2053.38   9
   9   4   1 28249.6 1913.56   4
   9  -4   1 29984.3 2096.25   3
   9   4   2 8798.41 1218.39   2
   9  -4   2 6574.94 937.926   2
   9  -4   2 7386.24 1101.49   3
   9   4   2 8731.93 1202.90  13
   9  -4   2 6221.03 1076.50  12
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   9   4   2 7626.11 1018.20   4
   9   4   3 92492.3 4075.28  13
   9  -4   3 92672.9 4172.16  12
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   9   4   3 94302.5 4160.62   2
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   9  -4   3 100134. 3884.37   2
  -9   4  -3 97299.4 4230.86   9
   9   4   3 97968.3 3802.76   4
   9  -4   3 92056.3 3942.36   3
   9   4   4 111.192 508.667   2
   9  -4   4 1692.62 625.630   2
   9  -4   4 1343.88 616.029   3
   9   4   4 1097.59 641.917  13
   9  -4   4 474.376 488.843  12
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   9   4   4 261.795 369.549   4
   9   4   5 48760.9 2936.39  13
   9  -4   5 48039.1 2992.74  12
  -9   4  -5 44896.9 2727.99  11
  -9  -4  -5 49979.3 2882.07   6
   9   4   5 43650.4 2918.94   2
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   9  -4   5 47015.1 2748.90   2
  -9   4  -5 46323.4 2947.27   9
   9   4   5 46408.6 2599.13   4
   9  -4   5 54287.4 3025.26   3
   9   4   6 2019.52 718.258   2
   9  -4   6 1805.34 692.518   3
   9   4   6 1911.72 772.755  13
   9  -4   6 1697.02 636.390  12
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  -9   4  -6 1408.86 621.890   9
   9   4   6 2077.68 650.236   4
   9   4   7 24402.8 2120.27  13
   9  -4   7 21119.6 1993.78  12
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  -9  -4  -7 22461.2 1944.58   6
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   9   4   7 21634.9 2124.91   2
  -9   4  -7 20821.4 2037.91   9
   9  -4   7 22173.6 1992.27   3
  -9  -4  -8 8778.07 1178.76  17
  -9   4  -8 8244.32 1348.15   9
   9  -5 -13 1469.52 573.011  14
   9  -5 -12 64703.1 3317.36  14
  -9   5  12 65275.9 3525.03   7
   9  -5 -12 65581.3 3513.22  10
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   9  -5 -11 1874.83 650.132  14
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  -9   5  11 980.591 545.783   7
   9  -5 -11 1950.66 695.058  10
   9   5 -11 2721.46 782.406   5
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   9  -5 -10 38128.4 2382.58  14
  -9  -5  10 36434.7 2679.88   7
  -9   5  10 37584.3 2555.98   7
   9  -5 -10 39573.8 2592.95  10
   9   5 -10 35980.6 2637.49   5
  -9  -5  10 36910.4 2479.66  17
   9   5  -9 1910.32 642.254  13
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  -9   5   9 3072.89 779.010   7
   9  -5  -9 1998.37 636.020  10
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   9   5  -9 1770.36 722.628   5
   9   5  -8 29716.4 2268.89  13
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  -9   5   8 38276.0 2508.90   7
   9  -5  -8 32809.0 2520.81  12
   9  -5  -8 33290.8 2312.97  10
   9   5  -8 36918.6 2667.83   2
   9   5  -8 30002.4 2358.52   5
  -9  -5   8 37854.8 2514.80  17
   9   5  -7-723.658 500.509  13
  -9  -5   7-139.307 489.558   7
   9  -5  -7-648.208 635.319  12
  -9   5   7-231.847 527.554   7
   9  -5  -7-104.167 372.146  10
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   9   5  -7 588.936 534.752   5
  -9   5   7 347.346 478.683   9
   9   5  -7 669.562 493.681   2
   9   5  -6 13154.7 1527.09  13
  -9  -5   6 11361.9 1377.73   7
   9  -5  -6 11710.9 1472.68  12
   9  -5  -6 9545.79 1213.91  10
  -9  -5   6 11254.2 1357.12  17
   9   5  -6 11028.1 1363.93   5
  -9   5   6 10659.2 1386.52   9
   9   5  -6 11958.8 1460.76   2
   9   5  -5 1594.12 597.810  13
   9  -5  -5 2510.23 841.972  12
  -9  -5   5 2522.31 697.713   7
   9  -5  -5 2418.48 650.768  10
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  -9  -5   5 1651.28 558.833  17
   9  -5  -5 2202.58 552.182  16
  -9   5   5 2399.31 705.486   9
   9   5  -5 2363.83 708.129   2
   9   5  -4 23306.6 2031.83  13
  -9  -5   4 25547.9 1966.00   7
   9  -5  -4 26414.8 2204.23  12
  -9  -5   4 28269.3 1877.93   6
   9   5  -4 24074.6 2041.16   2
  -9  -5   4 22428.0 1900.42  17
   9  -5  -4 26698.4 1773.04  16
  -9   5   4 27063.7 2132.10   9
   9  -5  -4 23501.9 1854.92   3
   9   5  -3 1327.21 578.477  13
   9  -5  -3 1628.67 608.927   3
   9  -5  -3 992.523 539.106  12
  -9  -5   3 876.980 435.247   7
  -9  -5   3 1361.06 485.833   6
  -9  -5   3 700.098 434.011  17
  -9   5   3 570.386 456.472   9
   9   5  -3 640.246 548.946   2
   9   5  -2 68358.9 3468.25  13
   9  -5  -2 68540.9 3550.23  12
  -9   5   2 63469.0 2882.14  11
  -9  -5   2 64706.2 3045.46   6
   9   5  -2 64899.8 3312.57   2
  -9  -5   2 60697.4 3178.77  17
  -9   5   2 62602.5 3286.14   9
   9  -5  -2 66670.4 3240.62   3
   9   5  -1 400.182 491.769   2
   9   5  -1 929.956 544.546  13
   9  -5  -1 11.6103 360.387   3
   9  -5  -1 772.654 432.937  12
  -9   5   1 378.742 323.585  11
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  -9  -5   1 825.506 547.579  17
   9   5  -1 165.694 365.390   4
  -9   5   1 82.2677 446.417   9
   9   5   0 66495.7 3423.84  13
   9  -5   0 62248.1 3400.58  12
  -9   5   0 61154.1 2963.55  11
  -9  -5   0 63775.1 3103.33   6
   9   5   0 62745.9 3284.78   2
  -9  -5   0 60277.2 3132.13  17
  -9   5   0 61113.2 3246.53   9
   9   5   0 62966.8 3056.98   4
   9  -5   0 66632.9 3256.61   3
   9   5   1 1513.62 612.977   2
   9   5   1 967.686 554.622  13
   9  -5   1 2093.35 611.660   3
   9  -5   1 2847.10 821.792  12
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  -9  -5  -1 896.988 568.379  17
   9   5   1 2199.74 600.883   4
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   9   5   2 77858.5 3737.95  13
   9  -5   2 71694.5 3705.84  12
  -9   5  -2 67959.4 3298.10  11
  -9  -5  -2 75546.6 3512.80   6
   9   5   2 74144.4 3643.65   2
  -9  -5  -2 73664.2 3504.67  17
  -9   5  -2 71734.3 3601.89   9
   9   5   2 74016.6 3368.64   4
   9  -5   2 76563.4 3602.24   3
   9   5   3 98.5271 476.142   2
   9   5   3 476.167 461.215  13
   9  -5   3 388.132 474.310   3
   9  -5   3 478.284 484.030  12
  -9   5  -3 21.8336 381.346  11
  -9  -5  -3-88.5414 466.247   6
  -9  -5  -3 12.9511 491.979  17
  -9   5  -3 700.321 563.302   9
   9   5   3 113.577 356.059   4
   9   5   4 2226.98 732.405   2
   9   5   4 1118.80 546.232  13
   9  -5   4 966.716 443.442   3
   9  -5   4 1609.90 699.247  12
  -9   5  -4 2262.53 686.743  11
  -9  -5  -4 1893.00 628.088   6
  -9  -5  -4 1774.81 615.251  17
  -9   5  -4 2467.85 799.194   9
   9   5   4 2425.60 652.650   4
   9   5   5-424.410 629.331   2
   9  -5   5 120.535 479.339   3
   9   5   5-527.116 564.142  13
   9  -5   5 52.4739 500.439  12
  -9   5  -5-90.0793 442.824  11
  -9  -5  -5 316.363 425.597   6
  -9  -5  -5 632.998 540.005  17
  -9   5  -5-181.524 472.562   9
   9   5   5-303.842 516.776   4
   9   5   6 24105.7 2077.46  13
   9  -5   6 22880.9 2117.48  12
  -9   5  -6 26191.0 2138.24  11
  -9  -5  -6 27154.7 2205.56   6
  -9  -5  -6 23077.8 1913.21  17
   9   5   6 22007.9 2124.49   2
  -9   5  -6 23221.9 2168.75   9
   9   5   6 20146.6 1805.76   4
   9  -5   6 24643.7 2136.60   3
  -9  -5  -7 204.413 441.194  17
  -9   5  -7-481.072 554.614   9
  -9  -5  -8 33652.1 2306.69  17
   9  -6 -12 633.482 457.159  14
  -9   6  12 711.531 519.220   7
  -9  -6  12-265.341 506.067  17
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;
_shelx_hkl_checksum              99435
_shelx_res_file
;
TITL gelb in P2(1)/n
    shelx.res
    created by SHELXL-2019/3 at 10:59:54 on 13-Oct-2023
CELL 0.71073   8.058916  11.134197  15.059598  90.0000  97.0038  90.0000
ZERR    4.00   0.00017   0.0002   0.0004   0.0000   0.0020   0.0000
LATT  1
SYMM -x+1/2, y+1/2,-z+1/2
SFAC C H P S Cl Au
UNIT 36.00 84.00 4.00 4.00 4.00 4.00
OMIT    -3   1   1
OMIT    -1   3   1
OMIT     0   1   4
L.S. 6
FMAP 2
PLAN 10
SIZE 0.4 0.2 0.2
TEMP -173
ACTA 60
CONF  2.3
BOND $H
HTAB C32 AU1
EQIV $1 1.5-x, 0.5+y, 0.5-z
HTAB C3 Cl1_$1
EQIV $2 1-x,1-y,1-z
HTAB C12 AU1_$2
EQIV $3 2-x,1-y,1-z
HTAB C1 S1_$3
WGHT    0.011100    0.883000
EXTI    0.001693
FVAR       2.85411
AU1   6    0.503290    0.503339    0.301413    11.00000    0.01461    0.01095 =
         0.01748   -0.00205    0.00225   -0.00199
CL1   5    0.304985    0.472958    0.181878    11.00000    0.02049    0.02211 =
         0.01787   -0.00512    0.00087   -0.00076
P1    3    0.780990    0.689644    0.421901    11.00000    0.01148    0.00917 =
         0.01192    0.00056   -0.00008    0.00053
S1    4    0.699319    0.516930    0.422834    11.00000    0.02072    0.01016 =
         0.02431    0.00323   -0.00425   -0.00212
C1    1    0.919973    0.706188    0.526820    11.00000    0.01544    0.01511 =
         0.01302    0.00232   -0.00057    0.00065
AFIX  13
H1    2    1.000594    0.637699    0.528670    11.00000   -1.20000
AFIX   0
C2    1    0.604696    0.794772    0.407854    11.00000    0.01249    0.01324 =
         0.02019    0.00297    0.00115    0.00218
AFIX  13
H2    2    0.542816    0.777882    0.347485    11.00000   -1.20000
AFIX   0
C3    1    0.908608    0.718842    0.331964    11.00000    0.01645    0.01719 =
         0.01246   -0.00136    0.00305   -0.00153
AFIX  13
H3    2    0.955630    0.801612    0.341415    11.00000   -1.20000
AFIX   0
C11   1    1.026840    0.821086    0.531052    11.00000    0.01933    0.02503 =
         0.01292   -0.00045   -0.00157   -0.00769
AFIX 137
H11A  2    0.955951    0.890946    0.538644    11.00000   -1.50000
H11B  2    1.077490    0.829499    0.475430    11.00000   -1.50000
H11C  2    1.115123    0.815969    0.581775    11.00000   -1.50000
AFIX   0
C12   1    0.830645    0.693310    0.610616    11.00000    0.02748    0.02606 =
         0.01283    0.00343    0.00069   -0.00610
AFIX 137
H12A  2    0.912987    0.675916    0.662427    11.00000   -1.50000
H12B  2    0.749564    0.627477    0.602008    11.00000   -1.50000
H12C  2    0.772311    0.768311    0.620949    11.00000   -1.50000
AFIX   0
C21   1    0.479015    0.775290    0.475223    11.00000    0.02175    0.03048 =
         0.03622    0.00977    0.01338    0.00980
AFIX 137
H21A  2    0.527202    0.804115    0.534274    11.00000   -1.50000
H21B  2    0.453446    0.689493    0.478704    11.00000   -1.50000
H21C  2    0.376102    0.819815    0.455734    11.00000   -1.50000
AFIX   0
C22   1    0.659979    0.926219    0.406151    11.00000    0.02088    0.01302 =
         0.04527    0.00209    0.00358    0.00325
AFIX 137
H22A  2    0.562907    0.977030    0.386965    11.00000   -1.50000
H22B  2    0.743040    0.935382    0.364215    11.00000   -1.50000
H22C  2    0.709377    0.950386    0.466181    11.00000   -1.50000
AFIX   0
C31   1    1.056668    0.632018    0.335959    11.00000    0.02455    0.03612 =
         0.02692   -0.00136    0.00980    0.00996
AFIX 137
H31A  2    1.015170    0.550101    0.324260    11.00000   -1.50000
H31B  2    1.121047    0.635606    0.395463    11.00000   -1.50000
H31C  2    1.128551    0.654776    0.290711    11.00000   -1.50000
AFIX   0
C32   1    0.807391    0.716572    0.239502    11.00000    0.02915    0.02286 =
         0.01298   -0.00136    0.00172   -0.00628
AFIX 137
H32A  2    0.882117    0.729766    0.193739    11.00000   -1.50000
H32B  2    0.722677    0.780119    0.235633    11.00000   -1.50000
H32C  2    0.752369    0.638374    0.229744    11.00000   -1.50000
AFIX   0
HKLF 4
REM  gelb in P2(1)/n
REM wR2 = 0.0315, GooF = S = 1.077, Restrained GooF = 1.077 for all data
REM R1 = 0.0148 for 3612 Fo > 4sig(Fo) and 0.0191 for all 4047 data
REM 125 parameters refined using 0 restraints
END
WGHT      0.0112      0.8791
REM Highest difference peak  1.327,  deepest hole -0.754,  1-sigma level  0.100
Q1    1   0.6000  0.5031  0.2929  11.00000  0.05    1.33
Q2    1   0.3977  0.5044  0.3094  11.00000  0.05    0.90
Q3    1   0.4903  0.5660  0.2682  11.00000  0.05    0.67
Q4    1   0.4853  0.4436  0.2803  11.00000  0.05    0.67
Q5    1   0.5000  0.5000  0.5000  10.50000  0.05    0.58
Q6    1   0.5665  0.4177  0.2810  11.00000  0.05    0.56
Q7    1   0.5087  0.5806  0.3263  11.00000  0.05    0.56
Q8    1   0.5276  0.4338  0.3462  11.00000  0.05    0.48
Q9    1   0.5884  0.5668  0.3611  11.00000  0.05    0.47
Q10   1   0.8733  0.7020  0.4875  11.00000  0.05    0.45
;
_shelx_res_checksum              99329
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au Au1 0.50329(2) 0.50334(2) 0.30141(2) 0.01432(3) Uani d 1 . .
Cl Cl1 0.30499(6) 0.47296(4) 0.18188(3) 0.02028(9) Uani d 1 . .
P P1 0.78099(5) 0.68964(4) 0.42190(3) 0.01098(9) Uani d 1 . .
S S1 0.69932(6) 0.51693(4) 0.42283(4) 0.01897(10) Uani d 1 . .
C C1 0.9200(2) 0.70619(16) 0.52682(12) 0.0147(3) Uani d 1 . .
H H1 1.000594 0.637699 0.528670 0.018 Uiso calc 1 . .
C C2 0.6047(2) 0.79477(16) 0.40785(13) 0.0154(4) Uani d 1 . .
H H2 0.542816 0.777882 0.347485 0.018 Uiso calc 1 . .
C C3 0.9086(2) 0.71884(17) 0.33196(12) 0.0153(3) Uani d 1 . .
H H3 0.955630 0.801612 0.341415 0.018 Uiso calc 1 . .
C C11 1.0268(2) 0.82109(18) 0.53105(13) 0.0194(4) Uani d 1 . .
H H11A 0.955951 0.890946 0.538644 0.029 Uiso calc 1 . .
H H11B 1.077490 0.829499 0.475430 0.029 Uiso calc 1 . .
H H11C 1.115123 0.815969 0.581775 0.029 Uiso calc 1 . .
C C12 0.8306(3) 0.69331(19) 0.61062(13) 0.0223(4) Uani d 1 . .
H H12A 0.912987 0.675916 0.662427 0.033 Uiso calc 1 . .
H H12B 0.749564 0.627477 0.602008 0.033 Uiso calc 1 . .
H H12C 0.772311 0.768311 0.620949 0.033 Uiso calc 1 . .
C C21 0.4790(3) 0.7753(2) 0.47522(16) 0.0287(5) Uani d 1 . .
H H21A 0.527202 0.804115 0.534274 0.043 Uiso calc 1 . .
H H21B 0.453446 0.689493 0.478704 0.043 Uiso calc 1 . .
H H21C 0.376102 0.819815 0.455734 0.043 Uiso calc 1 . .
C C22 0.6600(3) 0.92622(17) 0.40615(16) 0.0264(5) Uani d 1 . .
H H22A 0.562907 0.977030 0.386965 0.040 Uiso calc 1 . .
H H22B 0.743040 0.935382 0.364215 0.040 Uiso calc 1 . .
H H22C 0.709377 0.950386 0.466181 0.040 Uiso calc 1 . .
C C31 1.0567(3) 0.6320(2) 0.33596(15) 0.0286(5) Uani d 1 . .
H H31A 1.015170 0.550101 0.324260 0.043 Uiso calc 1 . .
H H31B 1.121047 0.635606 0.395463 0.043 Uiso calc 1 . .
H H31C 1.128551 0.654776 0.290711 0.043 Uiso calc 1 . .
C C32 0.8074(3) 0.71657(18) 0.23950(13) 0.0217(4) Uani d 1 . .
H H32A 0.882117 0.729766 0.193739 0.033 Uiso calc 1 . .
H H32B 0.722677 0.780119 0.235633 0.033 Uiso calc 1 . .
H H32C 0.752369 0.638374 0.229744 0.033 Uiso calc 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Au1 0.01461(4) 0.01095(4) 0.01748(5) -0.00199(2) 0.00225(3) -0.00205(2)
Cl1 0.0205(2) 0.0221(2) 0.0179(2) -0.00076(18) 0.00087(17) -0.00512(18)
P1 0.0115(2) 0.0092(2) 0.0119(2) 0.00053(15) -0.00008(16) 0.00056(16)
S1 0.0207(2) 0.0102(2) 0.0243(3) -0.00212(16) -0.00425(19) 0.00323(17)
C1 0.0154(8) 0.0151(8) 0.0130(9) 0.0007(6) -0.0006(7) 0.0023(7)
C2 0.0125(8) 0.0132(8) 0.0202(10) 0.0022(6) 0.0012(7) 0.0030(7)
C3 0.0164(9) 0.0172(9) 0.0125(9) -0.0015(7) 0.0030(7) -0.0014(7)
C11 0.0193(9) 0.0250(10) 0.0129(9) -0.0077(8) -0.0016(7) -0.0005(8)
C12 0.0275(10) 0.0261(10) 0.0128(9) -0.0061(8) 0.0007(8) 0.0034(8)
C21 0.0218(10) 0.0305(12) 0.0362(13) 0.0098(8) 0.0134(9) 0.0098(10)
C22 0.0209(10) 0.0130(9) 0.0453(14) 0.0032(7) 0.0036(9) 0.0021(9)
C31 0.0246(11) 0.0361(12) 0.0269(12) 0.0100(9) 0.0098(9) -0.0014(9)
C32 0.0291(10) 0.0229(10) 0.0130(9) -0.0063(8) 0.0017(8) -0.0014(7)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
S1 Au1 Cl1 . . 175.217(16) y
C3 P1 C1 . . 106.34(8) y
C3 P1 C2 . . 107.41(9) y
C1 P1 C2 . . 114.79(9) y
C3 P1 S1 . . 112.67(6) y
C1 P1 S1 . . 104.69(6) y
C2 P1 S1 . . 110.96(6) y
P1 S1 Au1 . . 104.56(2) y
C12 C1 C11 . . 111.10(16) ?
C12 C1 P1 . . 113.67(13) ?
C11 C1 P1 . . 113.55(13) ?
C12 C1 H1 . . 105.9 ?
C11 C1 H1 . . 105.9 ?
P1 C1 H1 . . 105.9 ?
C22 C2 C21 . . 111.30(17) ?
C22 C2 P1 . . 112.91(13) ?
C21 C2 P1 . . 113.48(13) ?
C22 C2 H2 . . 106.2 ?
C21 C2 H2 . . 106.2 ?
P1 C2 H2 . . 106.2 ?
C32 C3 C31 . . 110.65(16) ?
C32 C3 P1 . . 112.77(13) ?
C31 C3 P1 . . 111.41(14) ?
C32 C3 H3 . . 107.2 ?
C31 C3 H3 . . 107.2 ?
P1 C3 H3 . . 107.2 ?
C1 C11 H11A . . 109.5 ?
C1 C11 H11B . . 109.5 ?
H11A C11 H11B . . 109.5 ?
C1 C11 H11C . . 109.5 ?
H11A C11 H11C . . 109.5 ?
H11B C11 H11C . . 109.5 ?
C1 C12 H12A . . 109.5 ?
C1 C12 H12B . . 109.5 ?
H12A C12 H12B . . 109.5 ?
C1 C12 H12C . . 109.5 ?
H12A C12 H12C . . 109.5 ?
H12B C12 H12C . . 109.5 ?
C2 C21 H21A . . 109.5 ?
C2 C21 H21B . . 109.5 ?
H21A C21 H21B . . 109.5 ?
C2 C21 H21C . . 109.5 ?
H21A C21 H21C . . 109.5 ?
H21B C21 H21C . . 109.5 ?
C2 C22 H22A . . 109.5 ?
C2 C22 H22B . . 109.5 ?
H22A C22 H22B . . 109.5 ?
C2 C22 H22C . . 109.5 ?
H22A C22 H22C . . 109.5 ?
H22B C22 H22C . . 109.5 ?
C3 C31 H31A . . 109.5 ?
C3 C31 H31B . . 109.5 ?
H31A C31 H31B . . 109.5 ?
C3 C31 H31C . . 109.5 ?
H31A C31 H31C . . 109.5 ?
H31B C31 H31C . . 109.5 ?
C3 C32 H32A . . 109.5 ?
C3 C32 H32B . . 109.5 ?
H32A C32 H32B . . 109.5 ?
C3 C32 H32C . . 109.5 ?
H32A C32 H32C . . 109.5 ?
H32B C32 H32C . . 109.5 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Au1 S1 . 2.2711(5) y
Au1 Cl1 . 2.2820(5) y
P1 C3 . 1.8269(18) ?
P1 C1 . 1.8312(19) ?
P1 C2 . 1.8330(18) ?
P1 S1 . 2.0332(6) y
C1 C12 . 1.534(3) ?
C1 C11 . 1.539(3) ?
C1 H1 . 1.0000 ?
C2 C22 . 1.531(3) ?
C2 C21 . 1.534(3) ?
C2 H2 . 1.0000 ?
C3 C32 . 1.526(3) ?
C3 C31 . 1.531(3) ?
C3 H3 . 1.0000 ?
C11 H11A . 0.9800 ?
C11 H11B . 0.9800 ?
C11 H11C . 0.9800 ?
C12 H12A . 0.9800 ?
C12 H12B . 0.9800 ?
C12 H12C . 0.9800 ?
C21 H21A . 0.9800 ?
C21 H21B . 0.9800 ?
C21 H21C . 0.9800 ?
C22 H22A . 0.9800 ?
C22 H22B . 0.9800 ?
C22 H22C . 0.9800 ?
C31 H31A . 0.9800 ?
C31 H31B . 0.9800 ?
C31 H31C . 0.9800 ?
C32 H32A . 0.9800 ?
C32 H32B . 0.9800 ?
C32 H32C . 0.9800 ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
C32 H32C Au1 . 0.98 2.83 3.615(2) 138.2 yes
C3 H3 Cl1 2_655 1.00 2.77 3.6734(19) 151.1 yes
C12 H12B Au1 3_666 0.98 3.02 3.8290(19) 140.9 yes
C1 H1 S1 3_766 1.00 2.99 3.9487(19) 161.9 yes
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
C3 P1 S1 Au1 . . . . -71.54(7) y
C1 P1 S1 Au1 . . . . 173.32(6) y
C2 P1 S1 Au1 . . . . 48.95(7) y
C3 P1 C1 C12 . . . . 175.97(14) ?
C2 P1 C1 C12 . . . . 57.35(16) ?
S1 P1 C1 C12 . . . . -64.55(14) ?
C3 P1 C1 C11 . . . . 47.67(15) ?
C2 P1 C1 C11 . . . . -70.95(15) ?
S1 P1 C1 C11 . . . . 167.15(12) ?
C3 P1 C2 C22 . . . . -56.09(17) ?
C1 P1 C2 C22 . . . . 61.92(17) ?
S1 P1 C2 C22 . . . . -179.64(13) ?
C3 P1 C2 C21 . . . . 176.07(15) ?
C1 P1 C2 C21 . . . . -65.92(17) ?
S1 P1 C2 C21 . . . . 52.51(16) ?
C1 P1 C3 C32 . . . . -176.22(13) ?
C2 P1 C3 C32 . . . . -52.86(15) ?
S1 P1 C3 C32 . . . . 69.64(14) ?
C1 P1 C3 C31 . . . . 58.65(16) ?
C2 P1 C3 C31 . . . . -177.99(14) ?
S1 P1 C3 C31 . . . . -55.49(15) ?

_cod_database_fobs_code 2022965