#------------------------------------------------------------------------------ #$Date: 2023-12-01 04:12:49 +0100 (Fri, 01 Dec 2023) $ #$Revision: 287923 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/29/2022958.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022958 loop_ _publ_author_name 'Weil, Matthias' 'Missen, Owen P.' 'Mills, Stuart J.' _publ_section_title ; Dimorphism of [Bi2O2(OH)](NO3) -- the ordered Pna21 structure at 100 K ; _journal_coeditor_code HB8084 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E Crystallographic Communications' _journal_page_first 1223 _journal_page_last 1227 _journal_paper_doi 10.1107/S205698902301023X _journal_volume 79 _journal_year 2023 _chemical_formula_iupac '[Bi2 O2 (O H)] (N O3)' _chemical_formula_moiety 'Bi2 H O3 +, N O3 -' _chemical_formula_sum 'Bi2 H N O6' _chemical_formula_weight 528.98 _chemical_name_systematic ; Dioxidodibismuth(III) hydroxide nitrate ; _space_group_crystal_system orthorhombic _space_group_IT_number 33 _space_group_name_Hall 'P 2c -2n' _space_group_name_H-M_alt 'P n a 21' _audit_creation_method SHELXL-2019/3 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 5.3854(13) _cell_length_b 5.3676(13) _cell_length_c 17.051(4) _cell_measurement_reflns_used 3403 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 36.313 _cell_measurement_theta_min 2.889 _cell_volume 492.9(2) _computing_cell_refinement ; SAINT (Bruker, 2016) ; _computing_data_collection ; APEX3 (Bruker, 2016) ; _computing_data_reduction ; SAINT (Bruker, 2016) ; _computing_molecular_graphics ; ATOMS (Dowty, 2005) ; _computing_publication_material ; publCIF (Westrip, 2010) ; _computing_structure_refinement ; SHELXL2018/3 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.965 _diffrn_measurement_device_type 'Bruker APEXII CCD' _diffrn_measurement_method \w-scans _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0620 _diffrn_reflns_av_unetI/netI 0.0498 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_k_max 8 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_l_max 29 _diffrn_reflns_limit_l_min -29 _diffrn_reflns_number 9853 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 38.759 _diffrn_reflns_theta_min 1.194 _exptl_absorpt_coefficient_mu 71.268 _exptl_absorpt_correction_T_max 0.5236 _exptl_absorpt_correction_T_min 0.0169 _exptl_absorpt_correction_type numerical _exptl_absorpt_process_details ; (HABITUS; Herrendorf, 1997) ; _exptl_crystal_colour 'light yellow' _exptl_crystal_density_diffrn 7.129 _exptl_crystal_description plate _exptl_crystal_F_000 888 _exptl_crystal_size_max 0.090 _exptl_crystal_size_mid 0.080 _exptl_crystal_size_min 0.010 _refine_diff_density_max 3.128 _refine_diff_density_min -3.609 _refine_ls_abs_structure_details ; Twinning involves inversion, so Flack parameter cannot be determined ; _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.984 _refine_ls_hydrogen_treatment undef _refine_ls_matrix_type full _refine_ls_number_parameters 48 _refine_ls_number_reflns 2798 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 0.983 _refine_ls_R_factor_all 0.0380 _refine_ls_R_factor_gt 0.0298 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0213P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0550 _refine_ls_wR_factor_ref 0.0574 _reflns_number_gt 2407 _reflns_number_total 2798 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file hb8084sup1.cif _cod_data_source_block I _cod_database_code 2022958 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.060 _shelx_estimated_absorpt_t_max 0.536 _shelx_hkl_file ; 0 0 -1 43.11 9.09 0 0 0 -1 -.24 1.63 0 0 0 -1 25.71 6.90 0 0 0 1 3.27 2.41 0 0 0 1 2.00 4.76 0 0 0 1 1.63 .89 0 0 0 -2 3342.75 46.75 0 0 0 -2 3159.75 43.26 0 0 0 -2 3124.18 32.02 0 0 0 2 3460.97 47.25 0 0 0 2 3015.76 42.20 0 0 0 2 1.86 2.42 0 0 0 2 2885.16 41.87 0 0 0 -3 48.59 10.72 0 0 0 -3 51.08 8.61 0 0 0 3 24.46 9.18 0 0 0 3 34.97 6.76 0 0 0 3 29.24 10.84 0 0 0 -4 509.74 21.95 0 0 0 -4 509.92 15.84 0 0 0 4 556.01 21.50 0 0 0 4 531.13 14.93 0 0 0 4 493.35 23.24 0 0 0 -5 1.25 7.26 0 0 0 5 -1.17 7.01 0 0 0 5 1.65 5.20 0 0 0 5 .61 8.97 0 0 0 -6 7571.04 73.01 0 0 0 6 7442.15 67.22 0 0 0 6 7398.17 48.00 0 0 0 -7 19.87 8.01 0 0 0 7 8.84 6.84 0 0 0 7 4.30 3.85 0 0 0 -8 2379.06 42.31 0 0 0 8 2370.24 39.02 0 0 0 8 2280.97 26.84 0 0 0 -9 9.00 6.50 0 0 0 9 4.78 6.05 0 0 0 9 1.63 3.41 0 0 0 -10 37.50 9.30 0 0 0 10 50.77 9.05 0 0 0 10 44.64 5.64 0 0 0 -11 1.84 6.19 0 0 0 11 3.78 5.97 0 0 0 11 2.81 3.28 0 0 0 -12 4479.53 59.97 0 0 0 12 4613.12 55.35 0 0 0 12 4259.12 35.49 0 0 0 -13 5.58 6.62 0 0 0 13 8.58 6.25 0 0 0 13 2.36 3.28 0 0 0 -14 4104.34 58.77 0 0 0 14 4365.25 54.79 0 0 0 14 4306.10 34.79 0 0 0 -15 8.52 7.25 0 0 0 15 13.54 7.17 0 0 0 15 9.56 3.62 0 0 0 -16 366.43 20.19 0 0 0 16 356.61 17.99 0 0 0 16 365.50 10.42 0 0 0 -17 2.57 7.14 0 0 0 17 7.75 6.73 0 0 0 -18 1546.38 38.85 0 0 0 18 1475.08 33.56 0 0 0 -19 13.28 8.21 0 0 0 19 8.22 6.78 0 0 0 -20 2523.67 50.58 0 0 0 20 2345.44 42.36 0 0 0 -21 12.15 9.05 0 0 0 21 16.85 7.56 0 0 0 -22 507.64 25.94 0 0 0 22 440.35 20.65 0 0 0 -23 10.27 9.75 0 0 0 23 6.96 10.24 0 0 0 -24 526.08 27.30 0 0 0 -25 3.98 9.99 0 0 0 -26 1523.38 44.00 0 0 0 -27 16.53 11.06 0 0 0 -28 814.75 34.79 0 0 0 -29 10.63 12.81 0 0 -1 0 13.45 1.69 0 0 -1 0 63.88 19.22 0 0 1 0 18.05 3.27 0 0 -1 -1 26.44 1.88 0 0 -1 -1 57.37 13.88 0 0 -1 1 38.30 22.85 0 0 1 -1 38.79 2.99 0 0 1 -1 23.44 1.84 0 0 1 -1 31.30 1.92 0 0 1 1 22.63 4.84 0 0 1 1 27.24 1.92 0 0 -1 -2 2.08 1.14 0 0 -1 -2 7.11 6.54 0 0 -1 2 17.01 19.32 0 0 -1 2 7.81 8.49 0 0 1 -2 .68 1.22 0 0 1 2 -1.15 5.52 0 0 1 2 1.07 1.06 0 0 1 2 25.66 15.47 0 0 -1 -3 70.67 3.18 0 0 -1 -3 85.10 6.54 0 0 -1 3 123.92 18.20 0 0 -1 3 107.84 17.28 0 0 1 -3 67.24 2.03 0 0 1 -3 74.39 3.90 0 0 1 3 96.31 12.82 0 0 1 3 75.00 3.07 0 0 1 3 140.25 14.70 0 0 -1 -4 5.75 2.00 0 0 -1 -4 7.82 1.78 0 0 -1 4 22.04 11.24 0 0 -1 4 8.71 12.37 0 0 1 -4 8.62 2.00 0 0 1 -4 2.81 2.30 0 0 1 4 4.80 10.97 0 0 1 4 18.81 5.54 0 0 -1 -5 23.70 3.55 0 0 -1 5 16.52 9.23 0 0 -1 5 16.40 10.58 0 0 1 -5 28.78 4.59 0 0 1 5 37.11 15.42 0 0 -1 -6 4.29 3.20 0 0 -1 6 3.19 3.04 0 0 -1 6 6.91 7.45 0 0 -1 6 -.36 8.54 0 0 1 -6 5.80 4.42 0 0 1 6 3.44 15.67 0 0 -1 -7 7.34 4.32 0 0 -1 7 12.33 5.09 0 0 -1 7 15.91 7.17 0 0 -1 7 -.38 9.26 0 0 1 -7 17.88 6.98 0 0 1 7 16.96 15.44 0 0 -1 -8 6.74 5.61 0 0 -1 8 -1.21 6.26 0 0 -1 8 -1.73 5.25 0 0 1 -8 -.57 7.05 0 0 1 8 -1.04 10.79 0 0 -1 -9 37.80 9.63 0 0 -1 9 27.08 9.25 0 0 -1 9 37.38 7.72 0 0 1 -9 30.13 11.70 0 0 1 9 19.08 10.70 0 0 -1 -10 10.40 8.97 0 0 -1 10 8.75 9.36 0 0 -1 10 1.01 5.01 0 0 1 -10 -5.15 10.33 0 0 1 10 -.02 7.98 0 0 -1 -11 8.88 11.55 0 0 -1 11 28.86 9.31 0 0 -1 11 20.44 6.40 0 0 1 -11 33.08 15.55 0 0 1 11 20.90 9.20 0 0 -1 -12 -.66 9.66 0 0 -1 12 -2.84 6.61 0 0 -1 12 .51 4.94 0 0 1 -12 -.71 9.93 0 0 1 12 7.83 7.67 0 0 -1 -13 22.46 10.62 0 0 -1 13 1.79 6.28 0 0 -1 13 -.67 5.06 0 0 1 -13 -1.30 9.17 0 0 1 13 4.16 7.04 0 0 -1 -14 3.26 8.21 0 0 -1 14 1.71 6.00 0 0 -1 14 3.77 5.08 0 0 1 -14 6.06 8.76 0 0 1 14 1.27 6.93 0 0 -1 -15 13.00 8.82 0 0 -1 15 22.19 7.60 0 0 -1 15 13.25 6.00 0 0 1 -15 20.98 9.85 0 0 1 15 16.58 8.28 0 0 -1 -16 2.60 7.55 0 0 -1 16 1.26 5.82 0 0 -1 16 1.18 4.86 0 0 1 -16 4.17 7.96 0 0 1 16 -2.73 6.97 0 0 -1 -17 15.75 8.86 0 0 -1 17 18.63 7.39 0 0 -1 17 22.07 6.33 0 0 1 -17 23.31 9.85 0 0 1 17 35.80 9.99 0 0 -1 -18 .26 7.47 0 0 -1 18 -.76 5.83 0 0 -1 18 -1.60 4.86 0 0 1 -18 8.14 8.50 0 0 1 18 2.85 7.38 0 0 -1 -19 -1.13 7.79 0 0 -1 19 .87 5.97 0 0 1 -19 17.37 9.57 0 0 1 19 5.97 7.80 0 0 -1 -20 .67 8.34 0 0 1 -20 3.64 8.60 0 0 1 20 4.73 7.55 0 0 -1 -21 3.93 8.93 0 0 1 -21 13.10 9.64 0 0 1 21 6.37 8.43 0 0 -1 -22 3.34 8.93 0 0 1 -22 3.09 9.09 0 0 1 22 4.27 8.04 0 0 -1 -23 22.24 10.72 0 0 1 -23 16.39 11.31 0 0 1 23 15.83 9.26 0 0 -1 -24 -.53 9.12 0 0 1 -24 5.71 10.57 0 0 1 24 4.58 8.54 0 0 -1 -25 1.17 9.47 0 0 1 -25 15.76 11.37 0 0 1 25 3.41 8.52 0 0 -1 -26 2.80 9.78 0 0 1 -26 10.92 10.80 0 0 -1 -27 .18 10.06 0 0 1 -27 13.31 11.71 0 0 -1 -28 7.40 11.81 0 0 1 -28 3.67 12.01 0 0 -1 -29 11.75 12.63 0 0 1 -29 1.08 12.65 0 0 -2 0 7839.32 33.16 0 0 -2 0 9000.05 141.21 0 0 2 0 6987.56 56.04 0 0 -2 -1 594.49 35.83 0 0 -2 1 226.25 6.88 0 0 -2 1 791.66 61.81 0 0 2 -1 223.16 10.74 0 0 2 1 232.05 14.64 0 0 -2 -2 1724.91 14.52 0 0 -2 -2 1887.63 46.05 0 0 -2 2 1574.39 81.59 0 0 -2 2 1624.24 39.76 0 0 2 -2 1471.46 19.21 0 0 2 -2 1692.18 14.73 0 0 2 2 1624.57 36.25 0 0 -2 -3 19.55 2.48 0 0 -2 -3 46.95 9.69 0 0 -2 3 38.05 21.19 0 0 -2 3 39.57 14.64 0 0 2 -3 11.10 3.05 0 0 2 -3 16.12 2.51 0 0 2 3 30.01 11.08 0 0 -2 -4 1671.42 15.56 0 0 -2 -4 1815.32 30.21 0 0 2 -4 963.67 10.94 0 0 2 -4 1697.79 17.79 0 0 2 4 1721.33 47.11 0 0 -2 5 250.96 24.11 0 0 2 5 216.02 26.02 0 0 -2 -6 6467.74 36.36 0 0 -2 -6 6538.46 36.18 0 0 -2 6 6452.70 85.88 0 0 -2 6 6679.82 76.28 0 0 2 -6 6219.25 41.50 0 0 2 6 6470.39 106.98 0 0 2 7 276.06 33.36 0 0 -2 -8 3614.23 33.98 0 0 -2 8 3784.46 61.25 0 0 2 -8 3433.57 38.62 0 0 2 8 3838.38 96.79 0 0 -2 -9 60.05 6.79 0 0 2 -9 30.06 6.48 0 0 2 9 58.81 18.56 0 0 -2 -10 24.64 5.92 0 0 -2 10 13.84 8.00 0 0 2 -10 22.09 7.33 0 0 2 10 76.80 17.94 0 0 -2 -11 59.61 9.37 0 0 -2 11 37.94 9.44 0 0 2 -11 25.38 8.87 0 0 2 11 40.42 13.35 0 0 -2 -12 2426.41 46.99 0 0 -2 12 2441.26 45.48 0 0 2 -12 2659.39 57.03 0 0 2 12 2401.58 58.26 0 0 2 -13 58.31 16.14 0 0 2 13 105.93 16.42 0 0 -2 -14 3147.98 68.99 0 0 -2 14 3398.37 52.14 0 0 2 -14 3318.89 79.85 0 0 2 14 3145.48 62.88 0 0 -2 -15 134.89 23.69 0 0 -2 15 44.79 9.28 0 0 2 -15 14.54 16.63 0 0 2 15 42.01 11.69 0 0 -2 -16 138.80 23.77 0 0 -2 16 99.68 12.96 0 0 2 -16 125.55 25.59 0 0 2 16 114.07 16.76 0 0 -2 -17 21.12 13.31 0 0 -2 17 20.98 8.36 0 0 2 -17 28.06 14.62 0 0 2 17 6.69 9.03 0 0 -2 -18 1451.37 47.25 0 0 -2 18 1438.13 33.46 0 0 2 -18 1252.72 45.93 0 0 2 18 1457.24 42.20 0 0 -2 19 69.71 10.46 0 0 2 -19 66.51 15.55 0 0 2 19 71.26 13.85 0 0 -2 -20 2655.99 58.81 0 0 -2 20 2758.93 44.42 0 0 2 -20 2383.07 58.30 0 0 2 20 2711.40 56.24 0 0 -2 -21 58.29 14.00 0 0 2 -21 65.09 15.32 0 0 2 21 50.31 12.35 0 0 -2 -22 473.52 27.53 0 0 2 -22 439.78 28.34 0 0 2 22 481.76 26.25 0 0 -2 -23 2.63 10.18 0 0 2 -23 14.49 11.42 0 0 2 23 6.08 9.74 0 0 -2 -24 300.86 23.81 0 0 2 -24 346.79 25.53 0 0 2 24 322.41 22.74 0 0 -2 -25 30.62 12.31 0 0 2 -25 28.36 12.96 0 0 2 25 13.33 10.28 0 0 -2 -26 1451.37 44.29 0 0 2 -26 1390.41 44.75 0 0 2 26 1398.50 41.42 0 0 -2 -27 37.91 13.76 0 0 2 -27 41.91 15.72 0 0 2 27 36.33 11.48 0 0 -2 -28 692.36 32.90 0 0 2 -28 575.03 32.68 0 0 -2 -29 9.95 13.01 0 0 -3 0 1.95 2.21 0 0 -3 0 4.45 19.10 0 0 3 0 10.64 9.10 0 0 -3 -1 158.75 6.26 0 0 -3 -1 166.40 26.24 0 0 -3 1 166.81 7.09 0 0 -3 1 190.95 43.29 0 0 3 -1 139.70 16.32 0 0 3 1 165.22 20.02 0 0 -3 -2 3.13 2.10 0 0 -3 -2 6.37 11.24 0 0 -3 2 4.36 2.87 0 0 -3 2 10.89 30.61 0 0 3 -2 3.16 7.67 0 0 3 2 -4.78 9.86 0 0 -3 -3 373.91 8.85 0 0 -3 -3 410.87 24.56 0 0 -3 3 381.96 11.90 0 0 -3 3 301.16 56.06 0 0 3 -3 342.01 18.14 0 0 3 -3 362.87 8.76 0 0 3 3 339.17 28.93 0 0 -3 -4 3.40 2.24 0 0 -3 -4 14.00 7.60 0 0 -3 4 14.82 20.38 0 0 3 -4 6.32 6.84 0 0 3 -4 .37 2.16 0 0 3 4 3.71 12.91 0 0 -3 -5 177.88 6.78 0 0 -3 -5 197.26 13.48 0 0 -3 5 198.57 26.99 0 0 3 -5 146.73 12.11 0 0 3 -5 170.64 7.32 0 0 3 5 194.69 28.75 0 0 -3 -6 2.06 2.37 0 0 -3 -6 2.43 4.40 0 0 -3 6 -1.20 10.93 0 0 3 -6 1.11 2.65 0 0 3 6 13.22 17.43 0 0 -3 -7 55.96 5.06 0 0 -3 -7 62.28 6.71 0 0 -3 7 45.96 14.58 0 0 3 -7 55.45 5.88 0 0 3 7 79.74 24.87 0 0 -3 -8 3.70 2.84 0 0 -3 -8 4.36 2.89 0 0 -3 8 8.41 9.70 0 0 3 -8 1.44 3.35 0 0 3 8 .96 17.95 0 0 -3 -9 211.97 9.57 0 0 -3 -9 201.78 6.68 0 0 -3 9 193.38 19.77 0 0 3 -9 207.15 10.87 0 0 3 9 237.20 36.62 0 0 -3 -10 2.48 3.72 0 0 -3 -10 .04 1.51 0 0 -3 10 -3.54 8.80 0 0 3 -10 2.81 4.36 0 0 3 10 -14.20 12.79 0 0 -3 -11 152.16 10.31 0 0 -3 11 174.91 18.80 0 0 3 -11 143.38 12.06 0 0 3 11 137.61 23.08 0 0 -3 -12 3.63 5.35 0 0 -3 12 5.33 8.91 0 0 3 -12 -5.05 5.52 0 0 3 12 -5.12 10.78 0 0 -3 -13 17.61 7.63 0 0 -3 13 22.67 10.17 0 0 3 -13 11.38 8.36 0 0 3 13 9.29 11.93 0 0 -3 -14 1.74 6.73 0 0 -3 14 .71 8.51 0 0 3 -14 -1.33 9.02 0 0 3 14 4.36 10.23 0 0 -3 -15 117.09 17.89 0 0 -3 15 119.97 16.08 0 0 3 -15 102.76 19.07 0 0 3 15 112.31 19.18 0 0 -3 -16 5.56 11.66 0 0 -3 16 8.09 8.98 0 0 3 -16 -.36 13.57 0 0 3 16 14.36 10.62 0 0 -3 -17 134.86 23.92 0 0 -3 17 158.17 17.22 0 0 3 -17 137.86 27.80 0 0 3 17 162.12 21.42 0 0 -3 -18 9.92 17.59 0 0 -3 18 1.27 8.80 0 0 3 -18 -4.96 18.10 0 0 3 18 7.37 10.45 0 0 -3 -19 30.97 17.63 0 0 -3 19 39.48 11.10 0 0 3 -19 21.85 19.20 0 0 3 19 40.98 13.28 0 0 -3 -20 -6.63 12.71 0 0 -3 20 -5.43 8.22 0 0 3 -20 -.78 14.38 0 0 3 20 2.64 10.41 0 0 -3 -21 54.75 17.11 0 0 -3 21 89.43 14.27 0 0 3 -21 43.63 17.48 0 0 3 21 60.65 14.79 0 0 -3 -22 -2.66 11.24 0 0 3 -22 5.35 13.23 0 0 3 22 -2.75 10.28 0 0 -3 -23 98.63 18.34 0 0 3 -23 125.81 21.44 0 0 3 23 105.19 17.34 0 0 -3 -24 -2.92 11.35 0 0 3 -24 7.64 12.77 0 0 3 24 3.74 10.89 0 0 -3 -25 30.20 14.40 0 0 3 -25 24.67 15.10 0 0 3 25 41.48 14.05 0 0 3 -26 2.91 13.38 0 0 3 26 -10.91 10.07 0 0 -3 27 17.78 14.46 0 0 3 -27 31.45 15.82 0 0 3 27 15.82 12.81 0 0 3 28 21.34 12.53 0 0 -4 0 4759.15 37.60 0 0 -4 0 4968.53 120.62 0 0 4 0 4472.74 105.33 0 0 -4 -1 264.46 9.42 0 0 -4 -1 636.03 43.98 0 0 -4 1 275.93 10.35 0 0 4 -1 440.09 41.19 0 0 4 1 325.71 39.04 0 0 -4 -2 1954.13 23.13 0 0 -4 -2 2050.27 62.09 0 0 -4 2 1958.74 26.53 0 0 -4 2 2349.05 118.08 0 0 4 -2 1587.27 62.16 0 0 4 2 2039.77 77.00 0 0 -4 -3 9.13 3.11 0 0 -4 -3 17.04 11.54 0 0 -4 3 8.48 3.91 0 0 -4 3 14.98 39.46 0 0 4 -3 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112.97 26.91 0 -1 -6 16 2.98 26.08 0 -1 -6 16 42.26 17.09 0 -1 6 -16 18.83 10.67 0 -1 6 16 31.61 15.49 0 1 -6 16 21.31 27.73 0 1 -6 16 14.44 16.40 0 1 6 -16 32.30 12.83 0 1 6 16 4.40 16.51 0 -1 -6 17 44.80 34.05 0 -1 -6 17 45.76 17.16 0 -1 6 -17 52.31 14.00 0 -1 6 17 27.28 15.31 0 1 -6 17 35.30 24.44 0 1 -6 17 82.35 19.68 0 1 6 -17 62.80 16.39 0 1 6 17 57.76 20.91 0 -1 -6 18 2.33 35.46 0 -1 -6 18 50.62 17.00 0 -1 6 -18 36.17 14.55 0 -1 6 18 38.75 15.91 0 1 -6 18 28.63 21.81 0 1 -6 18 24.97 16.68 0 1 6 -18 41.63 16.29 0 1 6 18 26.77 17.06 0 -1 -6 19 194.12 41.39 0 -1 -6 19 205.41 25.65 0 -1 6 -19 212.87 26.38 0 -1 6 19 215.33 26.51 0 1 -6 19 226.51 31.63 0 1 -6 19 220.28 28.24 0 1 6 -19 232.39 30.29 0 1 6 19 208.92 29.25 0 -1 -6 20 72.50 29.07 0 -1 -6 20 84.25 18.25 0 -1 6 -20 78.47 21.66 0 -1 6 20 77.15 20.52 0 1 -6 20 48.38 20.20 0 1 -6 20 68.65 18.76 0 1 6 -20 80.62 24.59 0 1 6 20 66.27 21.15 0 -1 -6 21 95.54 27.75 0 -1 -6 21 121.74 21.20 0 -1 6 -21 104.36 25.64 0 -1 6 21 110.23 21.79 0 1 -6 21 107.89 23.19 0 1 -6 21 130.06 23.44 0 1 6 -21 133.77 32.31 0 1 6 21 156.53 28.34 0 -1 -6 22 26.52 26.44 0 -1 -6 22 33.54 14.61 0 -1 6 -22 25.76 24.27 0 -1 6 22 30.84 23.26 0 1 -6 22 29.77 17.07 0 1 -6 22 18.57 15.71 0 1 6 -22 12.46 32.23 0 -1 -6 23 3.62 20.05 0 -1 -7 0 42.60 9.31 0 -1 -7 0 63.98 23.67 0 1 -7 0 11.41 32.50 0 1 7 0 87.60 51.89 0 -1 -7 -1 89.41 11.47 0 -1 -7 -1 139.87 26.92 0 -1 -7 1 101.25 11.91 0 -1 -7 1 163.42 33.81 0 1 -7 -1 137.62 36.78 0 1 -7 1 176.44 50.82 0 1 7 -1 165.39 66.73 0 1 7 1 158.33 56.39 0 -1 -7 -2 866.13 25.38 0 -1 -7 -2 886.02 44.87 0 -1 -7 2 826.54 26.23 0 -1 -7 2 976.94 69.70 0 -1 7 2 744.15 47.93 0 1 -7 -2 920.21 60.22 0 1 -7 2 866.72 96.61 0 1 7 2 890.99 97.54 0 -1 -7 -3 194.61 14.02 0 -1 -7 -3 209.70 24.94 0 -1 -7 3 193.78 15.14 0 -1 -7 3 249.86 50.45 0 -1 7 3 247.03 37.59 0 1 -7 -3 185.69 31.38 0 1 -7 3 219.80 67.03 0 1 7 3 158.02 55.30 0 -1 -7 -4 1171.79 29.83 0 -1 -7 -4 1155.17 43.16 0 -1 -7 4 1181.19 32.35 0 -1 -7 4 1191.45 98.40 0 -1 7 4 1104.53 70.65 0 1 -7 -4 1208.70 54.78 0 1 -7 4 1140.05 112.13 0 1 7 4 1248.94 106.22 0 -1 -7 -5 178.74 20.68 0 -1 -7 5 134.15 14.26 0 -1 -7 5 204.48 65.15 0 -1 7 5 172.99 40.60 0 1 -7 -5 134.15 23.39 0 1 -7 5 109.89 45.25 0 1 7 5 140.55 50.73 0 -1 -7 -6 156.83 19.17 0 -1 -7 6 145.24 15.66 0 -1 -7 6 86.79 66.10 0 -1 7 6 137.54 39.63 0 1 -7 6 153.49 42.34 0 1 7 6 146.82 46.05 0 -1 -7 7 69.95 13.31 0 -1 -7 7 126.05 72.57 0 -1 7 7 115.82 35.53 0 1 -7 7 77.29 30.45 0 1 7 7 53.69 32.36 0 -1 -7 8 492.30 25.93 0 -1 -7 8 476.10 67.17 0 -1 7 8 476.75 47.99 0 1 -7 8 504.33 49.72 0 1 7 8 554.31 60.53 0 -1 -7 9 162.17 20.10 0 -1 -7 9 180.63 43.26 0 -1 7 9 200.33 33.02 0 1 -7 9 144.68 31.69 0 1 7 9 151.38 37.34 0 -1 -7 10 1105.11 40.54 0 -1 -7 10 1100.79 65.53 0 -1 7 10 1071.08 55.13 0 1 -7 10 1039.72 57.47 0 1 7 10 1057.29 67.50 0 -1 -7 11 144.83 21.21 0 -1 -7 11 143.61 30.69 0 -1 7 11 151.35 27.15 0 1 -7 11 148.78 29.85 0 1 7 11 120.34 30.43 0 -1 -7 12 253.25 27.61 0 -1 -7 12 296.37 36.93 0 -1 7 12 320.66 33.53 0 1 -7 12 274.40 32.03 0 1 -7 12 305.41 36.61 0 1 7 12 308.32 41.54 0 -1 -7 13 45.23 19.42 0 -1 -7 13 56.49 20.72 0 -1 7 13 40.04 18.01 0 1 -7 13 76.28 23.78 0 1 -7 13 69.55 20.86 0 1 7 13 33.45 20.60 0 -1 -7 14 132.41 28.56 0 -1 -7 14 201.68 30.06 0 -1 7 14 159.50 25.93 0 1 -7 14 149.83 32.66 0 1 -7 14 221.88 32.05 0 1 7 14 197.69 32.95 0 -1 -7 15 66.80 27.72 0 -1 -7 15 109.83 24.35 0 -1 7 15 77.33 20.30 0 1 -7 15 111.07 34.15 0 1 -7 15 118.32 25.76 0 1 7 15 86.02 23.56 0 -1 -7 16 682.70 59.22 0 -1 -7 16 724.85 43.23 0 -1 7 16 734.59 41.76 0 1 -7 16 687.17 43.88 0 1 7 16 659.10 46.17 0 -1 -7 17 102.33 37.66 0 -1 -7 17 127.46 25.58 0 -1 7 17 148.25 25.03 0 1 -7 17 108.54 40.88 0 1 -7 17 107.05 25.44 0 1 7 17 129.91 26.39 0 -1 -7 18 342.81 60.95 0 -1 -7 18 457.61 35.62 0 -1 7 18 440.34 35.67 0 1 -7 18 436.20 38.46 0 1 7 18 518.63 42.36 0 -1 -7 19 36.20 55.65 0 1 -7 19 62.79 28.11 0 1 -7 19 35.74 20.46 0 -1 -8 0 167.04 31.55 0 1 -8 0 147.57 41.72 0 -1 -8 -1 322.78 36.25 0 -1 -8 1 346.24 45.98 0 1 -8 -1 283.18 44.21 0 1 -8 1 328.67 58.90 0 -1 -8 -2 84.22 22.20 0 -1 -8 2 82.88 34.53 0 1 -8 -2 41.75 25.26 0 1 -8 2 18.02 42.54 0 -1 -8 -3 46.41 16.85 0 -1 -8 3 51.87 37.18 0 1 -8 -3 26.04 20.60 0 1 -8 3 38.80 51.15 0 -1 -8 -4 32.32 17.27 0 -1 -8 4 20.44 13.79 0 -1 -8 4 79.38 45.14 0 1 -8 4 -3.37 51.44 0 1 8 4 30.37 30.42 0 -1 -8 5 244.56 19.60 0 -1 -8 5 182.16 61.70 0 1 -8 5 181.92 70.02 0 1 8 5 193.54 40.04 0 -1 -8 6 86.32 14.94 0 -1 -8 6 126.55 70.40 0 1 -8 6 60.01 48.08 0 1 8 6 94.59 32.72 0 -1 -8 7 411.39 24.82 0 -1 -8 7 447.35 103.55 0 -1 8 7 308.19 53.63 0 1 -8 7 470.36 65.55 0 1 8 7 441.59 48.61 0 -1 -8 8 68.62 14.77 0 -1 -8 8 24.06 51.07 0 -1 8 8 28.89 34.62 0 1 -8 8 37.23 29.64 0 1 8 8 63.70 25.83 0 -1 -8 9 89.68 16.70 0 -1 -8 9 86.92 43.03 0 -1 8 9 78.98 30.72 0 1 -8 9 104.98 32.28 0 1 8 9 111.55 28.96 0 -1 -8 10 36.76 14.19 0 -1 -8 10 14.68 28.81 0 -1 8 10 -3.25 21.81 0 1 -8 10 10.89 24.36 0 1 8 10 32.50 22.67 0 -1 -8 11 122.98 22.51 0 -1 -8 11 134.80 35.03 0 -1 8 11 88.52 25.84 0 1 -8 11 151.46 35.23 0 1 8 11 115.68 28.06 0 -1 -8 12 54.13 19.84 0 -1 -8 12 91.52 31.54 0 -1 8 12 70.74 23.04 0 1 -8 12 78.37 28.42 0 1 8 12 83.88 25.74 0 -1 -8 13 270.68 33.40 0 -1 -8 13 370.80 44.88 0 -1 8 13 309.38 35.52 0 1 -8 13 343.58 42.63 0 1 8 13 316.73 38.13 0 -1 -8 14 25.59 22.88 0 -1 -8 14 50.57 28.62 0 -1 8 14 68.21 23.14 0 1 -8 14 72.81 34.86 0 1 8 14 94.47 25.56 0 -1 -8 15 107.73 35.98 0 -1 8 15 113.80 35.62 0 -1 -9 0 76.11 26.71 0 1 -9 0 55.67 32.71 0 -1 -9 -1 60.18 23.97 0 -1 -9 1 106.33 31.76 0 1 -9 -1 92.49 31.44 0 1 -9 1 49.68 38.04 0 -1 -9 2 442.01 57.26 0 1 -9 2 346.14 63.76 0 -1 -9 3 70.00 40.03 0 1 -9 3 66.52 51.82 0 -1 -9 4 454.27 70.78 0 1 -9 4 502.69 84.89 0 -1 -9 5 136.02 60.19 0 1 -9 5 97.60 62.00 0 -1 -9 6 59.70 91.65 0 1 -9 6 157.01 88.00 0 -2 0 0 4161.22 26.25 0 -2 0 -1 2521.44 23.44 0 -2 0 1 2471.19 18.40 0 2 0 -1 2736.47 17.31 0 2 0 1 2597.78 20.74 0 -2 0 -2 975.21 17.28 0 -2 0 2 962.80 11.02 0 2 0 -2 993.31 10.82 0 2 0 2 1006.36 13.46 0 -2 0 -3 226.78 10.93 0 -2 0 3 186.18 5.19 0 2 0 -3 225.66 5.80 0 2 0 3 196.75 6.67 0 -2 0 -4 1201.14 26.15 0 -2 0 4 1259.70 19.84 0 -2 0 4 1261.24 12.96 0 -2 0 4 1244.96 25.56 0 2 0 -4 1196.17 13.97 0 2 0 4 1304.24 17.02 0 -2 0 -5 2008.67 38.37 0 -2 0 5 2044.25 27.31 0 -2 0 5 2019.11 17.46 0 -2 0 5 1922.16 33.18 0 2 0 -5 2145.30 20.96 0 2 0 5 2018.72 22.65 0 -2 0 -6 3890.73 60.53 0 -2 0 6 3553.20 39.56 0 -2 0 6 3589.71 25.31 0 -2 0 6 3611.22 48.12 0 2 0 -6 3615.81 31.06 0 2 0 6 3641.55 32.83 0 -2 0 -7 2663.34 56.95 0 -2 0 7 2754.05 38.85 0 -2 0 7 2745.43 24.49 0 -2 0 7 2662.89 44.09 0 2 0 -7 2858.28 32.16 0 2 0 7 2438.54 25.54 0 2 0 7 2746.28 31.17 0 -2 0 -8 2304.70 59.01 0 -2 0 8 2161.91 39.02 0 -2 0 8 2074.36 23.79 0 -2 0 8 2091.95 41.19 0 2 0 -8 2206.30 33.29 0 2 0 8 1913.31 24.53 0 2 0 8 2023.21 29.57 0 -2 0 -9 554.82 35.67 0 -2 0 9 618.29 25.43 0 -2 0 9 566.31 14.52 0 -2 0 9 531.32 23.07 0 2 0 -9 674.90 22.64 0 2 0 9 610.08 15.88 0 2 0 9 590.83 18.69 0 -2 0 -10 181.42 24.38 0 -2 0 10 198.04 19.98 0 -2 0 10 168.47 10.32 0 -2 0 10 154.21 15.24 0 2 0 -10 220.05 17.66 0 2 0 10 172.43 10.74 0 2 0 10 168.65 13.45 0 -2 0 -11 582.09 31.71 0 -2 0 11 558.21 32.43 0 -2 0 11 533.63 18.47 0 -2 0 11 518.91 20.77 0 2 0 -11 631.64 30.83 0 2 0 11 579.30 19.39 0 2 0 11 620.58 24.27 0 -2 0 -12 1410.46 44.07 0 -2 0 12 1338.77 51.50 0 -2 0 12 1263.88 31.15 0 -2 0 12 1163.65 27.28 0 2 0 -12 1377.32 49.90 0 2 0 12 1307.93 31.84 0 2 0 12 1193.89 36.20 0 -2 0 -13 1834.87 48.12 0 -2 0 13 1492.82 59.00 0 -2 0 13 1531.47 38.75 0 -2 0 13 1718.76 30.67 0 2 0 -13 2024.76 66.33 0 2 0 13 1943.88 44.43 0 2 0 13 1725.03 48.19 0 -2 0 -14 1812.19 46.97 0 -2 0 14 1798.76 60.43 0 -2 0 14 1705.67 45.78 0 -2 0 14 1705.54 29.13 0 2 0 -14 1752.65 57.36 0 2 0 14 1985.91 52.95 0 2 0 14 1953.37 44.85 0 2 0 14 1847.23 56.12 0 -2 0 -15 720.54 30.50 0 -2 0 15 714.86 36.78 0 -2 0 15 581.79 32.62 0 -2 0 15 673.74 18.05 0 2 0 -15 785.41 36.72 0 2 0 15 809.62 42.60 0 2 0 15 809.68 31.84 0 2 0 15 704.74 42.52 0 -2 0 -16 167.50 17.91 0 -2 0 16 154.03 20.53 0 -2 0 16 135.11 23.57 0 -2 0 16 157.24 9.75 0 2 0 -16 173.37 19.94 0 2 0 16 230.29 29.66 0 2 0 16 167.83 19.74 0 2 0 16 150.85 28.63 0 -2 0 -17 273.51 20.91 0 -2 0 17 237.40 22.25 0 -2 0 17 203.18 24.39 0 2 0 -17 226.94 20.58 0 2 0 17 248.57 24.26 0 2 0 17 255.86 19.70 0 2 0 17 292.83 35.29 0 -2 0 -18 739.63 31.04 0 -2 0 18 771.53 31.70 0 -2 0 18 770.04 33.97 0 2 0 -18 737.73 31.44 0 2 0 18 766.63 32.44 0 2 0 18 760.52 41.50 0 -2 0 -19 1056.40 36.34 0 -2 0 19 1088.96 35.87 0 -2 0 19 1090.19 36.87 0 2 0 -19 1101.88 36.94 0 2 0 19 1096.81 35.38 0 -2 0 -20 1517.30 43.12 0 -2 0 20 1518.80 40.91 0 -2 0 20 1589.53 41.73 0 2 0 -20 1514.19 42.45 0 2 0 20 1477.16 38.52 0 -2 0 -21 698.72 30.97 0 -2 0 21 782.04 30.21 0 -2 0 21 760.13 29.70 0 2 0 -21 726.96 30.61 0 -2 0 -22 312.36 23.58 0 -2 0 22 310.69 21.41 0 -2 0 22 360.98 22.00 0 2 0 -22 350.63 23.30 0 -2 0 -23 46.98 13.76 0 -2 0 23 31.58 11.35 0 -2 0 23 56.87 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44.99 0 -3 3 -23 1146.50 42.34 0 -3 3 23 1035.02 40.83 0 3 3 -23 1154.99 64.22 0 3 3 23 1138.08 58.13 0 -3 -3 -24 244.76 35.47 0 -3 -3 24 208.84 24.69 0 -3 3 -24 196.60 23.93 0 -3 3 24 173.93 22.52 0 3 3 -24 230.49 36.26 0 3 3 24 193.80 29.08 0 -3 -3 -25 355.87 36.78 0 -3 -3 25 317.71 26.71 0 -3 3 -25 331.46 27.54 0 -3 3 25 359.13 27.81 0 3 3 -25 327.92 36.76 0 3 3 25 342.67 33.90 0 -3 -3 -26 204.10 33.07 0 -3 -3 26 180.47 22.42 0 -3 3 -26 184.28 23.75 0 -3 3 26 193.92 23.87 0 3 3 -26 180.69 29.09 0 3 3 26 196.86 26.76 0 -3 -4 0 284.08 13.43 0 -3 -4 0 272.06 20.86 0 -3 4 0 270.40 12.12 0 3 -4 0 313.14 56.90 0 3 -4 0 299.36 11.10 0 3 4 0 284.17 7.90 0 -3 -4 -1 21.18 5.71 0 -3 -4 -1 23.24 9.19 0 -3 -4 1 32.22 6.62 0 -3 -4 1 35.77 12.44 0 -3 4 -1 21.60 4.93 0 -3 4 1 25.79 6.20 0 3 -4 -1 22.61 31.87 0 3 -4 -1 16.17 4.46 0 3 -4 1 30.40 30.99 0 3 -4 1 21.92 4.93 0 3 4 -1 19.91 3.08 0 3 4 1 44.93 9.34 0 3 4 1 20.03 3.50 0 -3 -4 -2 152.61 10.46 0 -3 -4 -2 159.25 15.55 0 -3 -4 2 156.26 10.73 0 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46.61 0 3 -4 6 276.06 13.92 0 3 4 6 252.72 18.14 0 3 4 6 263.10 15.90 0 -3 -4 -7 17.66 5.90 0 -3 -4 -7 21.84 6.83 0 -3 -4 7 13.32 6.40 0 -3 -4 7 46.60 25.59 0 -3 4 7 28.47 15.48 0 3 -4 -7 42.75 13.84 0 3 -4 7 14.57 23.88 0 3 -4 7 22.66 7.14 0 3 4 7 19.39 9.12 0 3 4 7 18.79 9.59 0 -3 -4 -8 188.38 12.66 0 -3 -4 -8 206.80 12.90 0 -3 -4 8 195.73 14.84 0 -3 -4 8 125.62 33.18 0 -3 4 -8 194.32 6.38 0 -3 4 8 159.24 27.43 0 3 -4 -8 205.96 21.82 0 3 -4 8 196.36 40.59 0 3 -4 8 191.32 14.41 0 3 4 -8 200.46 12.62 0 3 4 8 164.47 17.01 0 3 4 8 212.62 21.66 0 -3 -4 -9 15.91 6.66 0 -3 -4 -9 21.68 6.17 0 -3 -4 9 13.62 7.81 0 -3 -4 9 14.59 22.50 0 -3 4 -9 15.91 3.95 0 -3 4 9 19.93 20.91 0 3 -4 -9 17.77 11.22 0 3 -4 9 15.00 22.92 0 3 -4 9 21.44 8.56 0 3 4 -9 22.75 6.95 0 3 4 9 2.11 7.84 0 3 4 9 13.72 13.01 0 -3 -4 -10 68.18 10.52 0 -3 -4 10 57.54 11.64 0 -3 -4 10 68.80 22.89 0 -3 4 -10 62.16 7.03 0 -3 4 10 40.16 25.61 0 3 -4 -10 83.88 15.92 0 3 -4 10 50.35 26.29 0 3 -4 10 53.61 12.20 0 3 4 -10 75.17 10.59 0 3 4 10 53.00 13.02 0 3 4 10 75.38 18.49 0 -3 -4 -11 7.95 6.66 0 -3 -4 11 10.74 8.98 0 -3 -4 11 6.79 15.66 0 -3 4 -11 9.41 5.29 0 -3 4 11 -10.74 23.89 0 3 -4 11 19.96 23.35 0 3 -4 11 17.93 10.99 0 3 4 -11 11.89 6.88 0 3 4 11 9.69 9.58 0 3 4 11 15.34 12.23 0 -3 -4 -12 187.14 15.72 0 -3 -4 12 140.85 19.04 0 -3 -4 12 139.78 23.57 0 -3 4 -12 166.88 12.24 0 -3 4 12 176.92 34.58 0 3 -4 12 160.10 36.30 0 3 -4 12 165.04 20.72 0 3 4 -12 143.34 14.04 0 3 4 12 128.10 18.97 0 3 4 12 191.05 21.66 0 -3 -4 -13 28.48 9.80 0 -3 -4 13 26.10 13.23 0 -3 -4 13 24.73 14.07 0 -3 4 -13 24.61 8.47 0 -3 4 13 22.51 18.98 0 3 -4 13 42.47 24.35 0 3 -4 13 22.81 14.30 0 3 4 -13 25.90 9.37 0 3 4 13 20.46 13.17 0 -3 -4 -14 189.57 18.22 0 -3 -4 14 117.89 21.57 0 -3 -4 14 202.96 23.55 0 -3 4 -14 163.57 15.84 0 -3 4 14 177.46 28.43 0 3 -4 14 153.19 30.50 0 3 -4 14 188.16 27.56 0 3 4 -14 177.75 17.69 0 3 4 14 139.06 23.23 0 -3 -4 -15 23.59 10.85 0 -3 -4 15 22.06 17.40 0 -3 -4 15 10.87 11.98 0 -3 4 -15 13.67 10.26 0 -3 4 15 5.71 14.66 0 3 -4 15 25.36 19.92 0 3 -4 15 -7.63 15.67 0 3 4 -15 17.01 10.53 0 3 4 15 6.68 15.01 0 -3 -4 -16 54.47 15.06 0 -3 -4 16 20.43 21.00 0 -3 -4 16 47.06 14.47 0 -3 4 -16 56.17 15.55 0 -3 4 16 49.04 17.41 0 3 -4 16 59.27 21.96 0 3 -4 16 54.16 23.50 0 3 4 -16 53.37 14.60 0 3 4 16 47.39 21.77 0 -3 -4 -17 20.47 13.37 0 -3 -4 17 -6.44 23.06 0 -3 -4 17 5.79 11.61 0 -3 4 -17 13.17 14.56 0 -3 4 17 11.83 14.14 0 3 -4 17 19.80 18.32 0 3 -4 17 10.02 20.60 0 3 4 -17 19.10 13.45 0 3 4 17 -3.50 19.64 0 -3 -4 -18 96.27 22.55 0 -3 -4 18 65.73 33.18 0 -3 -4 18 92.75 16.69 0 -3 4 -18 93.63 22.49 0 -3 4 18 113.63 20.60 0 3 -4 18 113.84 24.29 0 3 -4 18 122.13 29.38 0 3 4 -18 109.73 23.23 0 3 4 18 127.72 34.58 0 -3 -4 -19 10.83 18.56 0 -3 -4 19 -3.82 28.99 0 -3 -4 19 5.81 11.40 0 -3 4 -19 12.65 19.37 0 -3 4 19 .27 12.63 0 3 -4 19 15.63 16.18 0 3 -4 19 17.37 16.78 0 3 4 -19 6.14 16.92 0 3 4 19 6.83 29.17 0 -3 -4 -20 188.40 34.89 0 -3 -4 20 116.15 31.12 0 -3 -4 20 146.96 19.34 0 -3 4 -20 132.21 28.59 0 -3 4 20 118.92 20.30 0 3 -4 20 154.79 26.97 0 3 4 -20 160.48 33.90 0 3 4 20 128.02 43.87 0 -3 -4 -21 20.57 24.14 0 -3 -4 21 3.93 18.73 0 -3 -4 21 12.04 10.84 0 -3 4 -21 19.07 18.36 0 -3 4 21 11.98 13.26 0 3 -4 21 -9.89 13.70 0 3 4 -21 -13.20 21.62 0 3 4 21 21.18 27.79 0 -3 -4 -22 27.20 31.05 0 -3 -4 22 18.76 17.76 0 -3 4 -22 56.32 19.96 0 -3 4 22 40.27 15.35 0 3 -4 22 41.35 17.53 0 3 4 -22 45.77 33.46 0 3 4 22 47.91 27.17 0 -3 -4 -23 14.54 26.58 0 -3 -4 23 11.68 15.45 0 -3 4 -23 56.59 18.46 0 -3 4 23 -8.21 12.60 0 3 4 -23 9.81 30.88 0 3 4 23 14.10 21.66 0 -3 -4 -24 55.50 26.85 0 -3 -4 24 52.28 17.93 0 -3 4 -24 67.12 18.51 0 -3 4 24 26.74 16.57 0 3 4 -24 30.15 28.54 0 3 4 24 37.27 22.18 0 -3 4 -25 25.97 17.04 0 3 4 25 2.38 21.81 0 -3 -5 0 270.73 14.65 0 -3 -5 0 297.27 25.74 0 -3 5 0 269.41 13.12 0 3 -5 0 312.43 63.39 0 3 -5 0 270.24 11.60 0 3 5 0 253.57 19.78 0 -3 -5 -1 360.32 16.65 0 -3 -5 -1 371.11 25.30 0 -3 -5 1 362.80 16.79 0 -3 -5 1 356.66 29.80 0 -3 5 -1 354.07 13.62 0 -3 5 1 332.02 15.95 0 3 -5 -1 374.58 59.50 0 3 -5 -1 327.55 12.22 0 3 -5 1 363.15 64.53 0 3 -5 1 337.64 13.05 0 3 5 -1 240.60 19.85 0 3 5 1 351.21 21.85 0 -3 -5 -2 385.44 17.09 0 -3 -5 -2 387.69 23.94 0 -3 -5 2 368.19 16.93 0 -3 -5 2 373.82 32.86 0 -3 5 -2 353.73 12.30 0 -3 5 2 346.06 18.01 0 3 -5 -2 384.59 53.37 0 3 -5 -2 342.90 12.33 0 3 -5 2 364.43 65.68 0 3 -5 2 342.44 13.68 0 3 5 -2 395.68 23.12 0 3 5 2 355.86 22.35 0 -3 -5 -3 1877.28 35.10 0 -3 -5 -3 1865.26 44.93 0 -3 -5 3 1812.96 35.78 0 -3 -5 3 1720.37 65.39 0 -3 5 3 1679.96 39.21 0 3 -5 -3 1772.39 85.25 0 3 -5 -3 1718.26 25.32 0 3 -5 3 1762.36 107.53 0 3 -5 3 1794.44 29.23 0 3 5 -3 732.39 28.96 0 3 5 3 1673.80 42.97 0 -3 -5 -4 419.53 17.85 0 -3 -5 -4 403.98 22.04 0 -3 -5 4 382.36 18.22 0 -3 -5 4 351.35 39.92 0 -3 5 4 353.05 22.61 0 3 -5 -4 436.82 48.54 0 3 -5 -4 371.59 12.69 0 3 -5 4 407.87 66.66 0 3 -5 4 384.81 15.75 0 3 5 -4 375.43 23.44 0 3 5 4 390.20 24.01 0 -3 -5 -5 880.42 24.82 0 -3 -5 -5 847.94 28.80 0 -3 -5 5 814.02 25.87 0 -3 -5 5 834.02 59.36 0 -3 5 5 780.16 34.76 0 3 -5 -5 1044.07 66.24 0 3 -5 -5 839.25 18.41 0 3 -5 5 909.98 78.56 0 3 -5 5 790.30 22.44 0 3 5 5 809.58 32.85 0 -3 -5 -6 318.47 16.25 0 -3 -5 -6 324.33 18.64 0 -3 -5 6 309.09 17.77 0 -3 -5 6 306.07 47.33 0 -3 5 6 279.09 27.55 0 3 -5 -6 368.47 46.51 0 3 -5 6 331.10 52.81 0 3 -5 6 296.63 16.58 0 3 5 6 262.33 21.95 0 -3 -5 -7 75.94 10.92 0 -3 -5 -7 89.07 12.02 0 -3 -5 7 78.72 12.29 0 -3 -5 7 68.57 34.57 0 -3 5 7 112.78 23.48 0 3 -5 -7 99.57 26.47 0 3 -5 7 45.54 31.35 0 3 -5 7 72.52 11.75 0 3 5 7 75.26 14.96 0 -3 -5 -8 334.98 17.32 0 -3 -5 -8 345.06 17.39 0 -3 -5 8 316.41 19.54 0 -3 -5 8 330.59 54.73 0 -3 5 8 308.41 38.41 0 3 -5 -8 347.49 36.74 0 3 -5 8 296.41 48.77 0 3 -5 8 330.42 20.79 0 3 5 8 290.74 24.55 0 -3 -5 -9 1407.68 33.77 0 -3 -5 -9 1359.18 30.55 0 -3 -5 9 1267.83 36.95 0 -3 -5 9 1292.15 77.46 0 -3 5 9 1175.79 64.45 0 3 -5 9 1251.22 73.02 0 3 -5 9 1217.54 36.84 0 3 5 9 1312.58 46.66 0 -3 -5 -10 333.90 18.94 0 -3 -5 10 337.13 22.76 0 -3 -5 10 341.52 44.12 0 -3 5 10 231.29 41.79 0 3 -5 10 268.18 40.66 0 3 -5 10 329.45 25.24 0 3 5 10 279.59 27.21 0 -3 -5 -11 1083.45 31.94 0 -3 -5 11 973.62 37.10 0 -3 -5 11 1040.95 55.52 0 -3 5 11 830.08 66.63 0 3 -5 11 1059.74 62.55 0 3 -5 11 979.92 40.99 0 3 5 11 1029.45 46.70 0 -3 -5 -12 262.43 18.43 0 -3 -5 12 252.71 24.42 0 -3 -5 12 282.41 33.83 0 -3 5 12 263.10 40.34 0 3 -5 12 249.06 35.83 0 3 -5 12 285.32 30.42 0 3 5 -12 300.92 19.40 0 3 5 12 246.48 29.49 0 -3 -5 -13 17.31 9.02 0 -3 -5 13 18.56 14.04 0 -3 -5 13 17.48 16.82 0 -3 5 13 14.78 19.80 0 3 -5 13 11.60 19.77 0 3 -5 13 16.02 18.06 0 3 5 -13 22.28 9.85 0 3 5 13 30.43 17.79 0 -3 -5 -14 221.07 19.48 0 -3 -5 14 184.62 26.68 0 -3 -5 14 227.91 28.33 0 -3 5 -14 192.96 14.27 0 -3 5 14 250.74 33.10 0 3 -5 14 252.18 36.93 0 3 -5 14 227.79 33.85 0 3 5 -14 205.43 19.49 0 3 5 14 201.93 31.89 0 -3 -5 -15 697.36 32.16 0 -3 -5 15 588.20 42.17 0 -3 -5 15 759.78 39.49 0 -3 5 -15 698.84 23.19 0 -3 5 15 629.70 41.01 0 3 -5 15 739.19 49.17 0 3 -5 15 675.86 50.85 0 3 5 -15 672.59 31.41 0 3 5 15 656.72 52.33 0 -3 -5 -16 216.71 23.14 0 -3 -5 16 148.85 31.44 0 -3 -5 16 202.23 25.36 0 -3 5 -16 205.25 17.25 0 -3 5 16 167.82 25.86 0 3 -5 16 178.70 29.42 0 3 -5 16 216.78 32.76 0 3 5 -16 192.86 22.36 0 3 5 16 206.16 38.43 0 -3 -5 -17 1054.52 43.85 0 -3 -5 17 909.44 64.30 0 -3 -5 17 962.62 41.29 0 -3 5 -17 1000.67 32.95 0 -3 5 17 926.21 44.79 0 3 -5 17 1032.62 53.48 0 3 -5 17 1039.33 50.73 0 3 5 -17 1010.38 43.21 0 3 5 17 1091.63 76.15 0 -3 -5 -18 223.09 27.69 0 -3 -5 18 165.26 43.89 0 -3 -5 18 220.25 24.65 0 -3 5 -18 218.55 22.21 0 -3 5 18 220.57 27.24 0 3 -5 18 154.27 27.03 0 3 5 -18 229.58 30.43 0 3 5 18 213.99 49.33 0 -3 -5 -19 154.62 28.05 0 -3 -5 19 55.22 39.67 0 -3 -5 19 137.51 20.67 0 -3 5 -19 121.15 20.17 0 -3 5 19 123.42 21.36 0 3 -5 19 120.60 25.63 0 3 5 -19 141.77 27.43 0 3 5 19 134.84 46.38 0 -3 -5 -20 201.93 33.29 0 -3 -5 20 132.57 36.61 0 -3 -5 20 205.58 24.37 0 -3 5 -20 188.62 25.74 0 -3 5 20 187.84 25.66 0 3 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7 87.86 22.63 0 3 -7 7 83.50 29.50 0 3 7 7 68.44 25.77 0 -3 -7 -8 181.50 16.95 0 -3 -7 8 168.07 20.96 0 -3 -7 8 99.06 51.87 0 -3 7 8 176.73 31.97 0 3 -7 8 125.02 31.87 0 3 7 8 197.50 37.69 0 -3 -7 -9 673.39 28.20 0 -3 -7 9 616.14 31.97 0 -3 -7 9 528.34 77.18 0 -3 7 9 440.21 47.57 0 3 -7 9 595.81 51.50 0 3 7 9 678.03 58.76 0 -3 -7 -10 220.15 19.19 0 -3 -7 10 199.55 23.41 0 -3 -7 10 205.49 45.85 0 -3 7 10 138.03 35.35 0 3 -7 10 155.38 32.44 0 3 7 10 258.31 43.77 0 -3 -7 -11 574.89 27.74 0 -3 -7 11 509.03 33.20 0 -3 -7 11 527.81 55.06 0 -3 7 11 465.14 57.32 0 3 -7 11 543.60 47.86 0 3 7 11 610.57 62.68 0 -3 -7 -12 202.34 19.88 0 -3 -7 12 170.20 26.02 0 -3 -7 12 203.52 36.37 0 -3 7 12 182.85 42.07 0 3 -7 12 218.59 36.83 0 3 7 12 201.27 45.25 0 -3 -7 -13 48.98 13.95 0 -3 -7 13 37.44 18.48 0 -3 -7 13 39.54 22.39 0 -3 7 13 92.45 29.66 0 3 -7 13 33.16 21.29 0 3 7 13 20.40 34.82 0 -3 -7 -14 134.59 21.24 0 -3 -7 14 78.49 24.21 0 -3 -7 14 138.57 29.40 0 -3 7 14 110.42 28.40 0 3 -7 14 110.35 29.45 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768.23 17.83 0 -4 0 -5 1487.57 44.32 0 -4 0 5 1431.98 20.49 0 4 0 -5 1538.86 20.91 0 4 0 5 1500.78 25.23 0 -4 0 6 368.14 10.93 0 4 0 -6 344.59 10.88 0 4 0 6 312.95 12.76 0 -4 0 -7 2568.53 67.62 0 -4 0 7 2610.21 26.96 0 4 0 -7 2841.53 30.78 0 4 0 7 2665.85 35.66 0 -4 0 -8 631.32 40.44 0 -4 0 8 483.32 12.45 0 4 0 -8 457.11 13.74 0 4 0 8 453.39 16.40 0 -4 0 -9 325.10 35.33 0 -4 0 9 332.15 10.96 0 4 0 -9 365.44 13.24 0 4 0 9 352.20 15.61 0 -4 0 -10 690.55 45.59 0 -4 0 10 644.40 15.23 0 4 0 -10 670.90 18.79 0 4 0 10 816.07 21.18 0 4 0 10 667.10 21.55 0 -4 0 -11 730.89 42.19 0 -4 0 11 683.06 16.48 0 4 0 -11 689.58 20.67 0 4 0 11 706.18 20.63 0 4 0 11 674.78 23.10 0 -4 0 -12 425.73 32.48 0 -4 0 12 386.18 13.77 0 4 0 -12 327.70 16.51 0 4 0 12 294.83 15.35 0 4 0 12 308.13 18.31 0 -4 0 -13 2588.06 65.27 0 -4 0 13 2357.11 33.33 0 4 0 -13 2621.41 47.08 0 4 0 13 2562.47 40.65 0 4 0 13 2420.17 47.21 0 -4 0 -14 465.68 30.74 0 -4 0 14 417.07 16.63 0 4 0 -14 329.77 21.07 0 4 0 14 299.41 17.36 0 4 0 14 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0 4 2 0 145.51 8.13 0 -4 -2 -1 2300.86 33.15 0 -4 -2 -1 2276.41 43.96 0 -4 -2 1 2306.00 32.46 0 -4 -2 1 2304.53 47.98 0 4 -2 1 2261.69 30.48 0 4 2 1 2427.85 28.68 0 -4 -2 -2 572.34 17.41 0 -4 -2 -2 551.90 22.18 0 -4 -2 2 634.32 17.56 0 -4 -2 2 586.72 26.92 0 4 -2 2 665.40 17.22 0 4 2 2 636.87 15.32 0 -4 -2 -3 25.12 5.78 0 -4 -2 3 21.40 5.34 0 -4 -2 3 27.54 11.01 0 4 -2 3 23.45 5.16 0 4 2 3 21.81 4.41 0 -4 -2 -4 653.38 19.42 0 -4 -2 4 648.10 18.03 0 -4 -2 4 657.48 32.16 0 4 -2 4 674.18 17.87 0 4 2 4 719.58 16.94 0 -4 -2 -5 1747.35 32.27 0 -4 -2 5 1693.38 28.73 0 -4 -2 5 1712.42 52.74 0 -4 2 5 1687.38 34.65 0 4 -2 5 1851.73 29.60 0 4 2 5 1799.26 27.07 0 -4 -2 -6 212.94 13.32 0 -4 -2 6 213.84 11.73 0 -4 -2 6 317.55 29.38 0 -4 2 -6 197.53 9.17 0 -4 2 6 205.47 15.23 0 4 -2 6 194.43 11.47 0 4 2 -6 205.88 10.91 0 4 2 6 210.68 10.90 0 -4 -2 -7 2787.10 44.03 0 -4 -2 7 2703.85 37.94 0 -4 -2 7 2679.70 74.04 0 -4 2 -7 2972.25 36.60 0 -4 2 7 2640.80 49.91 0 4 -2 7 2868.75 39.10 0 4 2 -7 3084.33 38.43 0 4 2 7 3005.40 37.92 0 -4 -2 -8 380.98 18.55 0 -4 -2 8 372.06 15.64 0 -4 -2 8 381.10 36.00 0 -4 2 -8 401.59 18.50 0 -4 2 8 379.27 23.07 0 4 -2 8 373.65 16.18 0 4 2 -8 416.56 15.67 0 4 2 8 396.25 18.38 0 4 2 8 405.77 16.00 0 -4 -2 -9 495.62 22.09 0 -4 -2 9 472.93 18.28 0 -4 -2 9 351.89 35.68 0 -4 2 -9 520.44 24.38 0 -4 2 9 439.19 27.17 0 4 -2 9 470.32 18.68 0 4 2 -9 550.57 18.42 0 4 2 9 463.96 20.21 0 4 2 9 489.42 18.41 0 -4 -2 -10 646.97 26.72 0 -4 -2 10 613.01 21.50 0 -4 -2 10 496.78 40.04 0 -4 2 -10 662.09 31.20 0 -4 2 10 606.56 35.40 0 4 -2 10 592.74 15.08 0 4 -2 10 635.12 22.48 0 4 2 -10 726.72 21.96 0 4 2 10 599.02 22.80 0 4 2 10 688.31 22.88 0 -4 -2 -11 464.63 24.88 0 -4 -2 11 467.04 20.34 0 -4 -2 11 417.30 33.16 0 -4 2 -11 478.15 31.54 0 -4 2 11 451.42 36.40 0 4 -2 11 494.02 21.47 0 4 2 -11 538.54 20.35 0 4 2 11 479.24 21.66 0 4 2 11 485.53 21.55 0 -4 -2 -12 301.62 23.37 0 -4 -2 12 268.31 17.56 0 -4 -2 12 301.38 27.01 0 -4 2 -12 271.54 29.36 0 -4 2 12 333.66 40.16 0 4 -2 12 280.72 18.92 0 4 2 -12 306.32 17.21 0 4 2 12 265.29 18.31 0 4 2 12 281.31 19.49 0 -4 -2 -13 1975.02 54.94 0 -4 -2 13 1901.60 43.92 0 -4 -2 13 2088.94 54.49 0 -4 2 -13 1944.88 56.67 0 -4 2 13 1693.94 78.84 0 4 -2 13 2004.20 44.91 0 4 2 -13 2102.34 43.13 0 4 2 13 2014.33 44.30 0 4 2 13 2013.22 47.19 0 -4 -2 -14 153.23 23.30 0 -4 -2 14 168.08 18.61 0 -4 -2 14 170.67 19.80 0 -4 2 -14 135.96 20.48 0 -4 2 14 189.97 44.59 0 4 -2 14 145.92 18.30 0 4 2 -14 137.06 15.91 0 4 2 14 171.57 18.03 0 4 2 14 149.67 19.49 0 -4 -2 -15 731.27 42.74 0 -4 -2 15 663.95 32.51 0 -4 -2 15 734.12 31.54 0 -4 2 -15 739.19 34.40 0 -4 2 15 609.52 63.14 0 4 -2 15 772.40 46.71 0 4 -2 15 712.66 33.52 0 4 2 -15 769.93 32.22 0 4 2 15 741.82 31.80 0 4 2 15 746.44 38.07 0 -4 -2 -16 405.86 39.70 0 -4 -2 16 421.20 30.19 0 -4 -2 16 473.36 25.56 0 -4 2 -16 491.17 28.78 0 -4 2 16 405.18 44.55 0 4 -2 16 515.81 42.68 0 4 -2 16 445.59 31.52 0 4 2 -16 470.06 29.18 0 4 2 16 485.60 29.34 0 4 2 16 508.21 37.87 0 -4 -2 -17 198.61 36.84 0 -4 -2 17 150.05 24.48 0 -4 -2 17 198.18 18.44 0 -4 2 -17 163.37 20.81 0 -4 2 17 157.89 29.19 0 4 -2 17 190.10 32.89 0 4 -2 17 174.40 25.53 0 4 2 -17 153.92 23.26 0 4 2 17 196.83 24.00 0 4 2 17 196.03 30.94 0 -4 -2 -18 233.41 42.06 0 -4 -2 18 177.59 28.37 0 -4 -2 18 223.59 18.29 0 -4 2 -18 217.73 21.64 0 -4 2 18 165.96 26.60 0 4 -2 18 227.24 36.07 0 4 -2 18 190.88 29.17 0 4 2 -18 198.76 29.94 0 4 2 18 180.93 26.18 0 4 2 18 212.30 35.81 0 -4 -2 -19 1340.26 68.79 0 -4 -2 19 1116.43 55.75 0 -4 -2 19 1466.08 38.14 0 -4 2 -19 1348.71 42.37 0 -4 2 19 1273.18 51.18 0 4 -2 19 1605.44 72.20 0 4 -2 19 1551.17 67.49 0 4 2 -19 1396.64 64.91 0 4 2 19 1484.48 61.01 0 4 2 19 1456.00 72.21 0 -4 -2 -20 102.25 27.31 0 -4 -2 20 92.89 22.85 0 -4 2 20 42.11 17.44 0 4 -2 20 54.43 23.79 0 4 -2 20 91.48 29.16 0 4 2 -20 30.75 25.56 0 4 2 20 88.90 26.18 0 4 2 20 79.95 23.54 0 -4 -2 -21 994.19 53.46 0 -4 -2 21 806.48 41.06 0 -4 2 -21 927.60 36.55 0 -4 2 21 867.27 41.12 0 4 -2 21 930.90 65.77 0 4 2 -21 871.52 68.44 0 4 2 21 1050.36 68.97 0 4 2 21 1036.02 52.48 0 -4 -2 -22 318.82 33.98 0 -4 -2 22 307.90 26.45 0 -4 2 -22 319.26 25.48 0 -4 2 22 261.92 27.35 0 4 -2 22 344.97 46.76 0 4 2 -22 333.33 51.53 0 4 2 22 413.15 55.67 0 -4 -2 -23 13.83 16.68 0 -4 2 -23 3.25 11.89 0 -4 2 23 12.14 13.70 0 4 -2 23 24.27 20.70 0 4 2 -23 26.79 23.17 0 4 2 23 -9.37 23.28 0 -4 -2 -24 239.06 30.99 0 -4 -2 24 258.92 21.41 0 -4 2 -24 220.65 22.90 0 -4 2 24 173.54 23.15 0 4 2 -24 223.16 35.34 0 -4 -2 -25 581.05 38.73 0 -4 2 -25 604.52 32.02 0 -4 2 25 494.77 32.05 0 4 2 -25 586.02 42.15 0 -4 2 26 38.37 24.85 0 4 2 -26 38.79 19.34 0 -4 -3 0 25.65 6.04 0 -4 -3 0 38.71 10.85 0 4 -3 0 29.97 5.67 0 4 3 0 27.40 4.38 0 -4 -3 -1 27.72 6.18 0 -4 -3 -1 25.21 9.14 0 -4 -3 1 33.59 6.78 0 -4 -3 1 34.07 11.53 0 4 -3 -1 23.00 5.25 0 4 -3 1 28.06 5.48 0 4 3 -1 24.80 4.33 0 4 3 1 23.71 4.31 0 -4 -3 -2 116.07 9.65 0 -4 -3 -2 132.70 13.94 0 -4 -3 2 104.49 9.37 0 -4 -3 2 123.13 18.68 0 4 -3 2 118.84 8.83 0 4 3 2 120.12 7.39 0 -4 -3 -3 7.99 4.85 0 -4 -3 -3 8.65 6.68 0 -4 -3 3 12.31 5.08 0 -4 -3 3 19.24 10.95 0 -4 3 3 10.85 5.83 0 4 -3 3 9.50 4.45 0 4 3 3 7.15 3.52 0 -4 -3 -4 143.16 10.96 0 -4 -3 -4 163.18 13.56 0 -4 -3 4 138.73 10.46 0 -4 -3 4 142.99 21.37 0 -4 3 4 132.96 12.68 0 4 -3 4 154.67 10.21 0 4 3 4 145.20 8.54 0 -4 -3 -5 20.99 6.05 0 -4 -3 -5 22.88 7.18 0 -4 -3 5 25.22 6.29 0 -4 -3 5 18.80 15.09 0 -4 3 5 24.03 7.77 0 4 -3 5 24.69 6.08 0 4 3 5 24.72 5.20 0 -4 -3 -6 42.14 7.90 0 -4 -3 6 36.04 7.24 0 -4 -3 6 40.19 16.40 0 -4 3 6 52.34 11.62 0 4 -3 6 42.55 7.29 0 4 3 6 39.22 9.09 0 4 3 6 42.23 6.74 0 -4 -3 -7 39.79 8.48 0 -4 -3 7 40.01 7.79 0 -4 -3 7 23.15 17.66 0 -4 3 7 40.12 12.00 0 4 -3 7 39.26 7.78 0 4 3 7 44.30 9.89 0 4 3 7 43.89 7.29 0 -4 -3 -8 90.41 12.03 0 -4 -3 8 62.43 9.71 0 -4 -3 8 66.19 23.64 0 -4 3 8 81.04 15.63 0 4 -3 8 71.48 9.94 0 4 3 -8 81.99 9.64 0 4 3 8 76.30 12.09 0 4 3 8 83.01 10.22 0 -4 -3 -9 19.19 7.63 0 -4 -3 9 12.75 6.86 0 -4 -3 9 28.77 21.06 0 -4 3 -9 14.92 4.43 0 -4 3 9 23.51 13.94 0 4 -3 9 21.44 7.52 0 4 3 -9 11.82 6.07 0 4 3 9 12.72 8.13 0 4 3 9 15.25 6.99 0 -4 -3 -10 130.40 14.10 0 -4 -3 10 114.31 13.05 0 -4 -3 10 91.65 25.96 0 -4 3 -10 134.76 10.20 0 -4 3 10 117.55 23.19 0 4 -3 10 135.38 14.30 0 4 3 -10 146.71 12.55 0 4 3 10 129.74 15.64 0 4 3 10 124.32 14.32 0 -4 -3 -11 32.26 9.78 0 -4 -3 11 15.45 8.07 0 -4 -3 11 17.98 16.83 0 -4 3 -11 25.38 7.69 0 -4 3 11 36.92 20.92 0 4 -3 11 19.26 9.02 0 4 3 -11 18.59 7.63 0 4 3 11 23.24 9.65 0 4 3 11 21.39 9.70 0 -4 -3 -12 27.34 10.35 0 -4 -3 12 28.87 10.10 0 -4 -3 12 31.13 16.10 0 -4 3 -12 37.76 10.17 0 -4 3 12 51.26 26.57 0 4 -3 12 43.46 22.49 0 4 -3 12 42.94 11.40 0 4 3 -12 47.30 9.79 0 4 3 12 45.36 11.98 0 4 3 12 48.21 13.34 0 -4 -3 -13 38.42 12.32 0 -4 -3 13 46.79 12.60 0 -4 -3 13 42.42 15.48 0 -4 3 -13 37.65 12.45 0 -4 3 13 41.04 28.87 0 4 -3 13 34.53 23.22 0 4 -3 13 33.06 12.37 0 4 3 -13 43.11 10.32 0 4 3 13 39.92 11.89 0 4 3 13 47.97 14.70 0 -4 -3 -14 56.39 14.99 0 -4 -3 14 32.57 13.07 0 -4 -3 14 32.90 13.79 0 -4 3 -14 42.30 14.83 0 -4 3 14 48.51 33.68 0 4 -3 14 25.45 22.48 0 4 -3 14 24.84 13.00 0 4 3 -14 46.26 11.75 0 4 3 14 47.83 13.50 0 4 3 14 40.66 16.65 0 -4 -3 -15 25.59 13.74 0 -4 -3 15 30.01 14.59 0 -4 -3 15 15.53 11.71 0 -4 3 -15 27.33 16.47 0 -4 3 15 30.52 24.22 0 4 -3 15 31.62 23.81 0 4 -3 15 20.19 13.96 0 4 3 -15 22.91 11.10 0 4 3 15 21.95 12.81 0 4 3 15 22.67 17.18 0 -4 -3 -16 88.19 20.74 0 -4 -3 16 90.65 21.53 0 -4 -3 16 97.55 16.75 0 -4 3 -16 65.45 20.72 0 -4 3 16 90.94 25.47 0 4 -3 16 101.52 31.80 0 4 -3 16 78.52 19.84 0 4 3 -16 100.47 18.26 0 4 3 16 93.23 19.57 0 4 3 16 106.84 27.33 0 -4 -3 -17 6.87 16.37 0 -4 -3 17 26.91 19.35 0 -4 -3 17 13.79 11.01 0 -4 3 -17 16.44 19.29 0 -4 3 17 8.92 17.49 0 4 -3 17 20.53 24.05 0 4 -3 17 14.82 17.82 0 4 3 -17 8.41 12.79 0 4 3 17 24.56 15.59 0 4 3 17 11.73 18.98 0 -4 -3 -18 59.89 23.65 0 -4 -3 18 36.85 23.36 0 -4 -3 18 52.76 13.41 0 -4 3 -18 75.94 20.51 0 -4 3 18 54.26 19.16 0 4 -3 18 54.61 26.12 0 4 -3 18 64.40 24.06 0 4 3 -18 34.03 17.64 0 4 3 18 53.34 21.18 0 4 3 18 41.84 18.91 0 -4 -3 -19 32.00 23.50 0 -4 -3 19 -4.72 22.58 0 -4 -3 19 23.45 11.78 0 -4 3 -19 46.76 17.47 0 -4 3 19 33.97 17.00 0 4 -3 19 -2.16 20.80 0 4 -3 19 15.79 23.43 0 4 3 -19 15.47 18.32 0 4 3 19 26.72 20.14 0 4 3 19 1.63 14.31 0 -4 -3 -20 -20.77 24.68 0 -4 -3 20 14.61 21.49 0 -4 -3 20 .42 9.82 0 -4 3 -20 42.93 16.53 0 -4 3 20 26.73 15.18 0 4 -3 20 24.38 19.34 0 4 -3 20 8.83 24.11 0 4 3 -20 9.53 22.16 0 4 3 20 22.75 24.03 0 -4 -3 -21 -19.61 22.41 0 -4 -3 21 20.48 17.26 0 -4 3 -21 13.71 13.97 0 -4 3 21 14.02 15.09 0 4 -3 21 -2.69 17.93 0 4 -3 21 11.10 23.08 0 4 3 -21 -12.57 24.23 0 4 3 21 41.27 29.07 0 -4 -3 -22 74.04 30.16 0 -4 -3 22 61.86 18.63 0 -4 3 -22 63.68 17.74 0 -4 3 22 45.51 17.62 0 4 -3 22 78.02 26.34 0 4 3 -22 2.82 29.72 0 4 3 22 69.99 37.96 0 -4 -3 -23 -8.54 22.68 0 -4 -3 23 37.07 14.83 0 -4 3 -23 3.43 12.94 0 -4 3 23 -15.19 14.05 0 4 -3 23 36.99 21.43 0 4 3 -23 -14.17 27.34 0 4 3 23 19.27 28.21 0 -4 -3 -24 47.75 24.96 0 -4 -3 24 74.26 16.33 0 -4 3 -24 45.53 16.30 0 -4 3 24 21.69 17.04 0 4 3 -24 23.05 27.30 0 4 3 24 43.36 26.45 0 -4 -3 25 41.71 13.13 0 -4 3 -25 19.78 15.44 0 4 3 25 24.79 39.03 0 -4 -4 0 68.58 9.86 0 -4 -4 0 57.47 13.82 0 4 -4 0 47.84 7.51 0 4 4 0 51.53 5.64 0 -4 -4 -1 1901.00 35.26 0 -4 -4 -1 2072.79 49.41 0 -4 -4 1 2041.96 36.73 0 -4 -4 1 1904.79 52.63 0 4 -4 -1 1988.40 30.60 0 4 -4 1 2031.04 31.28 0 4 4 -1 2001.04 24.67 0 4 4 1 2081.41 25.77 0 -4 -4 -2 420.63 17.62 0 -4 -4 -2 479.63 24.83 0 -4 -4 2 429.81 18.05 0 -4 -4 2 440.24 29.97 0 -4 4 2 422.08 17.82 0 4 -4 -2 388.67 14.54 0 4 -4 2 415.59 15.42 0 4 4 -2 438.87 12.08 0 4 4 2 416.32 12.56 0 -4 -4 -3 73.46 10.17 0 -4 -4 -3 83.25 13.23 0 -4 -4 3 54.46 8.77 0 -4 -4 3 68.61 18.49 0 -4 4 3 65.86 10.15 0 4 -4 -3 64.51 8.02 0 4 -4 3 74.25 9.01 0 4 4 -3 70.89 5.90 0 4 4 3 85.11 12.61 0 4 4 3 60.93 6.66 0 -4 -4 -4 530.04 19.90 0 -4 -4 -4 524.93 23.57 0 -4 -4 4 461.50 19.13 0 -4 -4 4 438.91 35.25 0 -4 4 4 463.96 21.60 0 4 -4 4 517.40 17.77 0 4 4 4 489.45 23.45 0 4 4 4 469.89 14.69 0 -4 -4 -5 992.03 26.98 0 -4 -4 -5 1015.96 30.61 0 -4 -4 5 877.29 25.78 0 -4 -4 5 899.63 50.23 0 -4 4 5 883.74 30.51 0 4 -4 5 996.17 24.55 0 4 4 5 925.57 30.38 0 4 4 5 974.58 21.83 0 -4 -4 -6 55.35 9.37 0 -4 -4 -6 60.11 10.69 0 -4 -4 6 52.01 9.57 0 -4 -4 6 39.21 21.01 0 -4 4 6 66.98 13.61 0 4 -4 6 55.82 8.91 0 4 4 6 61.30 12.04 0 4 4 6 63.73 9.10 0 -4 -4 -7 1765.08 36.97 0 -4 -4 -7 1767.86 37.61 0 -4 -4 7 1585.94 36.11 0 -4 -4 7 1477.96 70.86 0 -4 4 7 1628.93 47.80 0 4 -4 7 1762.66 34.42 0 4 4 7 1631.69 40.95 0 4 4 7 1721.47 33.67 0 -4 -4 -8 202.03 15.29 0 -4 -4 8 199.72 15.67 0 -4 -4 8 190.02 36.29 0 -4 4 8 203.84 24.63 0 4 -4 8 248.10 44.41 0 4 -4 8 217.26 15.66 0 4 4 8 223.79 19.01 0 4 4 8 220.14 16.46 0 -4 -4 -9 283.86 17.72 0 -4 -4 9 212.84 16.85 0 -4 -4 9 252.84 43.84 0 -4 4 9 228.89 28.55 0 4 -4 9 241.83 44.93 0 4 -4 9 216.75 16.65 0 4 4 9 224.90 19.83 0 4 4 9 257.27 19.90 0 -4 -4 -10 471.70 22.58 0 -4 -4 10 378.53 21.96 0 -4 -4 10 420.42 45.81 0 -4 4 10 433.33 40.32 0 4 -4 10 418.56 49.93 0 4 -4 10 462.25 23.01 0 4 4 -10 422.38 19.71 0 4 4 10 378.09 24.44 0 4 4 10 465.89 27.22 0 -4 -4 -11 474.05 23.60 0 -4 -4 11 460.15 25.07 0 -4 -4 11 429.49 41.31 0 -4 4 11 402.44 45.98 0 4 -4 11 518.00 53.34 0 4 -4 11 465.08 24.87 0 4 4 -11 490.09 22.08 0 4 4 11 489.02 28.09 0 4 4 11 586.31 34.01 0 -4 -4 -12 134.22 16.69 0 -4 -4 12 114.45 17.86 0 -4 -4 12 102.69 23.45 0 -4 4 12 105.13 34.41 0 4 -4 12 148.78 38.12 0 4 -4 12 143.85 18.66 0 4 4 -12 136.34 14.64 0 4 4 12 125.83 19.24 0 4 4 12 180.13 26.16 0 -4 -4 -13 1717.30 46.12 0 -4 -4 13 1531.59 48.44 0 -4 -4 13 1706.85 58.95 0 -4 4 -13 1702.02 38.45 0 -4 4 13 1454.54 83.69 0 4 -4 13 1943.21 90.15 0 4 -4 13 1591.42 47.02 0 4 4 -13 1646.87 41.49 0 4 4 13 1636.80 51.33 0 4 4 13 1894.19 66.66 0 -4 -4 -14 100.93 18.05 0 -4 -4 14 69.73 17.42 0 -4 -4 14 102.35 21.03 0 -4 4 -14 89.89 11.41 0 -4 4 14 66.09 31.15 0 4 -4 14 117.62 36.28 0 4 -4 14 85.61 18.82 0 4 4 -14 115.92 17.02 0 4 4 14 77.89 17.70 0 4 4 14 106.78 23.33 0 -4 -4 -15 715.79 35.31 0 -4 -4 15 592.24 38.34 0 -4 -4 15 783.28 38.62 0 -4 4 -15 646.63 24.52 0 -4 4 15 614.61 50.96 0 4 -4 15 841.07 65.19 0 4 -4 15 667.24 39.31 0 4 4 -15 678.26 31.62 0 4 4 15 640.06 39.44 0 4 4 15 812.48 42.51 0 -4 -4 -16 442.70 32.69 0 -4 -4 16 416.82 38.40 0 -4 -4 16 441.76 30.23 0 -4 4 -16 423.55 24.26 0 -4 4 16 392.43 40.10 0 4 -4 16 495.24 52.49 0 4 -4 16 425.85 37.40 0 4 4 -16 483.86 30.11 0 4 4 16 410.84 36.53 0 4 4 16 482.88 32.47 0 -4 -4 -17 137.43 24.84 0 -4 -4 17 109.17 29.13 0 -4 -4 17 91.08 18.17 0 -4 4 -17 115.06 18.60 0 -4 4 17 98.10 24.10 0 4 -4 17 98.97 30.16 0 4 -4 17 106.35 28.09 0 4 4 -17 105.16 21.00 0 4 4 17 110.36 25.31 0 -4 -4 -18 221.51 33.14 0 -4 -4 18 158.15 35.13 0 -4 -4 18 178.81 22.23 0 -4 4 -18 169.96 23.22 0 -4 4 18 194.53 28.54 0 4 -4 18 183.25 33.10 0 4 -4 18 212.63 39.29 0 4 4 -18 211.07 29.99 0 4 4 18 159.54 31.86 0 -4 -4 -19 1033.24 57.42 0 -4 -4 19 783.13 63.12 0 -4 -4 19 967.41 38.08 0 -4 4 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1 54.70 9.63 0 -4 -5 1 60.33 16.89 0 -4 5 1 72.73 9.54 0 4 -5 -1 65.15 41.14 0 4 -5 -1 64.56 8.25 0 4 -5 1 -2.28 38.27 0 4 -5 1 63.41 8.65 0 4 5 -1 79.36 14.98 0 4 5 1 81.15 14.82 0 -4 -5 -2 180.98 13.91 0 -4 -5 -2 212.81 20.59 0 -4 -5 2 183.67 14.52 0 -4 -5 2 226.11 29.93 0 -4 5 2 200.68 14.65 0 4 -5 -2 237.47 51.05 0 4 -5 -2 186.64 11.35 0 4 -5 2 226.93 56.82 0 4 -5 2 196.69 12.51 0 4 5 2 192.57 19.38 0 -4 -5 -3 22.12 7.26 0 -4 -5 -3 23.81 10.15 0 -4 -5 3 23.97 7.65 0 -4 -5 3 38.31 18.82 0 -4 5 3 33.61 9.10 0 4 -5 -3 10.72 22.51 0 4 -5 -3 26.18 6.09 0 4 -5 3 -8.62 32.04 0 4 -5 3 20.83 6.94 0 4 5 3 11.05 10.02 0 -4 -5 -4 235.74 15.58 0 -4 -5 -4 257.74 20.24 0 -4 -5 4 239.86 16.19 0 -4 -5 4 197.49 31.10 0 -4 5 4 240.89 18.33 0 4 -5 -4 262.29 40.65 0 4 -5 -4 256.39 12.94 0 4 -5 4 328.52 65.59 0 4 -5 4 242.94 14.82 0 4 5 4 234.34 20.84 0 -4 -5 -5 48.21 9.57 0 -4 -5 -5 54.61 11.69 0 -4 -5 5 40.49 9.55 0 -4 -5 5 54.36 24.55 0 -4 5 5 44.25 11.98 0 4 -5 -5 36.51 20.09 0 4 -5 -5 49.19 7.83 0 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0 7 1 7 916.49 29.84 0 -7 -1 -8 540.63 61.99 0 7 -1 8 378.28 22.07 0 7 1 8 378.22 21.16 0 -7 -1 -9 368.61 55.04 0 7 -1 9 252.19 19.51 0 7 1 9 273.37 19.81 0 -7 -1 -10 723.93 56.74 0 7 -1 10 654.22 28.68 0 7 1 10 553.28 28.26 0 7 1 10 656.93 28.22 0 -7 -1 -11 436.70 43.67 0 7 -1 11 332.03 23.19 0 7 1 11 298.71 22.98 0 7 1 11 330.86 22.86 0 -7 -1 -12 307.23 36.59 0 7 -1 12 220.13 21.45 0 7 1 12 230.92 21.39 0 7 1 12 241.20 21.64 0 -7 -1 -13 797.32 47.46 0 7 -1 13 718.21 33.42 0 7 1 13 662.62 30.03 0 7 1 13 766.66 34.22 0 -7 -1 -14 194.03 30.41 0 7 -1 14 159.88 21.53 0 7 1 14 160.50 19.23 0 7 1 14 166.94 22.36 0 -7 -1 -15 302.92 32.08 0 7 -1 15 269.72 27.20 0 7 1 15 284.52 23.04 0 7 1 15 292.01 27.87 0 -7 -1 -16 544.19 36.49 0 7 -1 16 496.24 34.64 0 7 1 16 541.98 35.68 0 -7 -1 -17 161.39 25.40 0 7 -1 17 133.34 25.26 0 7 1 17 126.71 24.41 0 -7 -1 -18 316.53 29.72 0 7 -1 18 320.12 37.14 0 7 1 18 258.88 33.35 0 -7 -1 -19 587.43 36.43 0 7 1 19 553.27 53.28 0 -7 -2 0 5.69 10.55 0 7 -2 0 4.99 6.55 0 7 2 0 5.36 5.76 0 -7 -2 -1 32.79 13.99 0 -7 -2 1 19.59 11.84 0 7 -2 -1 30.48 8.53 0 7 -2 1 33.63 8.90 0 7 2 -1 33.10 7.96 0 7 2 1 26.90 7.47 0 -7 -2 -2 33.78 13.66 0 -7 -2 2 29.45 12.21 0 7 -2 -2 22.49 8.40 0 7 -2 2 26.03 8.55 0 7 2 -2 27.59 7.59 0 7 2 2 28.64 7.75 0 -7 -2 -3 40.58 15.01 0 -7 -2 3 28.50 12.31 0 7 -2 -3 37.56 9.64 0 7 -2 3 34.24 9.43 0 7 2 -3 36.38 8.43 0 7 2 3 32.86 8.24 0 -7 -2 -4 69.32 17.56 0 -7 -2 4 40.67 12.35 0 7 -2 -4 32.78 9.41 0 7 -2 4 33.75 9.17 0 7 2 -4 28.74 7.98 0 7 2 4 24.95 7.88 0 -7 -2 -5 39.34 16.64 0 -7 -2 5 33.13 12.48 0 7 -2 -5 24.99 9.06 0 7 -2 5 26.86 8.98 0 7 2 -5 16.26 6.87 0 7 2 5 13.86 7.12 0 -7 -2 -6 10.41 15.05 0 -7 -2 6 2.51 10.13 0 7 -2 6 9.08 7.77 0 7 2 6 3.09 6.50 0 -7 -2 -7 29.38 16.43 0 -7 -2 7 23.25 12.12 0 7 -2 7 20.45 9.53 0 7 2 7 38.07 10.05 0 -7 -2 -8 14.94 18.24 0 -7 -2 8 9.66 12.30 0 7 -2 8 16.96 9.38 0 7 2 8 9.48 8.08 0 -7 -2 -9 30.32 20.97 0 7 -2 9 19.54 10.05 0 7 2 9 6.65 11.44 0 7 2 9 15.72 8.88 0 -7 -2 -10 38.06 22.10 0 7 -2 10 31.14 11.98 0 7 2 10 15.74 12.04 0 7 2 10 16.38 9.84 0 -7 -2 -11 17.49 23.09 0 7 -2 11 25.09 11.58 0 7 2 11 15.62 11.78 0 7 2 11 16.31 10.69 0 -7 -2 -12 29.68 25.28 0 7 -2 12 -2.65 10.26 0 7 2 12 4.99 10.23 0 7 2 12 2.70 10.08 0 -7 -2 -13 30.10 29.49 0 7 -2 13 10.90 12.24 0 7 2 13 31.15 12.40 0 7 2 13 14.31 12.11 0 -7 -2 -14 3.12 29.20 0 7 -2 14 11.51 13.00 0 7 2 14 8.40 10.29 0 7 2 14 -.35 12.62 0 -7 -2 -15 25.33 27.32 0 7 -2 15 8.54 14.18 0 7 2 15 28.59 12.38 0 7 2 15 2.74 13.75 0 -7 -2 -16 23.02 23.02 0 7 -2 16 15.04 17.21 0 7 2 16 27.27 12.91 0 7 2 16 12.16 15.56 0 -7 -2 -17 -8.65 21.32 0 7 -2 17 2.15 17.66 0 7 2 17 38.79 14.17 0 7 2 17 18.06 18.06 0 -7 -2 -18 12.76 21.93 0 7 -2 18 13.52 26.12 0 7 -2 18 9.41 28.06 0 7 2 18 26.87 20.70 0 -7 -3 0 154.15 19.15 0 7 -3 0 132.41 14.64 0 7 3 0 125.98 12.42 0 -7 -3 -1 664.17 30.72 0 -7 -3 1 667.29 29.74 0 7 -3 -1 706.06 26.77 0 7 -3 1 701.44 26.69 0 7 3 -1 679.15 23.48 0 7 3 1 733.95 24.52 0 -7 -3 -2 498.11 27.72 0 -7 -3 2 455.58 25.53 0 7 -3 -2 503.67 23.30 0 7 -3 2 467.12 22.76 0 7 3 -2 465.77 19.91 0 7 3 2 489.52 20.93 0 -7 -3 -3 217.35 21.83 0 -7 -3 3 195.09 19.27 0 7 -3 -3 200.58 16.76 0 7 -3 3 201.19 17.25 0 7 3 -3 205.96 14.48 0 7 3 3 193.91 14.99 0 -7 -3 -4 531.78 30.29 0 -7 -3 4 488.29 26.53 0 7 -3 -4 505.92 23.94 0 7 -3 4 567.93 25.23 0 7 3 -4 521.61 21.33 0 7 3 4 537.20 22.42 0 -7 -3 -5 553.21 31.69 0 -7 -3 5 539.82 28.04 0 7 -3 -5 560.34 25.38 0 7 -3 5 600.57 26.17 0 7 3 -5 547.83 22.06 0 7 3 5 566.93 23.54 0 -7 -3 -6 170.54 23.46 0 -7 -3 6 159.66 20.12 0 7 -3 -6 110.81 14.93 0 7 -3 6 168.64 17.53 0 7 3 -6 144.38 13.51 0 7 3 6 150.62 15.25 0 -7 -3 -7 805.16 39.70 0 -7 -3 7 624.00 31.28 0 7 -3 -7 736.73 29.00 0 7 -3 7 767.52 30.28 0 7 3 -7 771.09 26.56 0 7 3 7 686.90 33.17 0 7 3 7 772.75 28.32 0 -7 -3 -8 308.44 29.51 0 -7 -3 8 241.75 22.96 0 7 -3 8 296.22 22.08 0 7 3 8 248.63 24.34 0 7 3 8 261.84 19.72 0 -7 -3 -9 291.40 31.32 0 -7 -3 9 219.32 23.74 0 7 -3 9 251.79 21.67 0 7 3 9 230.66 23.43 0 7 3 9 253.23 20.33 0 -7 -3 -10 534.84 39.01 0 -7 -3 10 420.79 30.11 0 7 -3 10 490.23 27.85 0 7 3 10 484.47 29.59 0 7 3 10 488.21 26.37 0 -7 -3 -11 397.93 38.26 0 -7 -3 11 300.34 28.19 0 7 -3 11 329.20 25.23 0 7 3 11 339.78 26.69 0 7 3 11 343.09 24.84 0 -7 -3 -12 234.94 36.45 0 -7 -3 12 173.86 26.34 0 7 -3 12 195.54 23.05 0 7 3 12 201.08 23.17 0 7 3 12 190.63 22.67 0 -7 -3 -13 633.61 51.08 0 7 -3 13 611.36 34.24 0 7 3 13 662.50 34.64 0 7 3 13 601.88 34.53 0 -7 -3 -14 149.50 36.59 0 7 -3 14 94.20 20.66 0 7 3 14 136.93 21.18 0 7 3 14 97.53 21.22 0 -7 -3 -15 342.79 52.81 0 7 -3 15 213.89 42.51 0 7 -3 15 240.50 29.16 0 7 3 15 250.86 26.93 0 7 3 15 258.20 30.82 0 -7 -3 -16 442.65 64.31 0 7 -3 16 427.51 57.78 0 7 -3 16 382.18 35.61 0 7 3 16 455.79 33.47 0 7 3 16 436.28 38.55 0 7 -3 17 138.50 41.57 0 7 3 17 194.59 28.02 0 7 3 17 182.60 35.03 0 -7 -4 0 4.02 8.66 0 7 -4 0 4.89 7.61 0 -7 -4 -1 85.34 15.55 0 -7 -4 1 83.03 15.31 0 7 -4 -1 81.71 13.23 0 7 -4 1 81.99 13.39 0 -7 -4 -2 46.80 13.04 0 -7 -4 2 53.64 13.94 0 7 -4 -2 48.73 11.31 0 7 -4 2 61.78 12.33 0 -7 -4 -3 56.92 13.97 0 -7 -4 3 51.78 13.64 0 7 -4 -3 50.58 11.20 0 7 -4 3 56.93 12.21 0 -7 -4 -4 74.81 15.91 0 -7 -4 4 61.05 14.50 0 7 -4 -4 65.55 11.94 0 7 -4 4 77.09 13.84 0 7 4 4 56.29 16.33 0 -7 -4 -5 64.86 15.94 0 -7 -4 5 50.19 14.15 0 7 -4 -5 77.13 13.17 0 7 -4 5 71.36 13.55 0 7 4 5 64.16 16.30 0 -7 -4 -6 16.15 12.17 0 -7 -4 6 -3.22 9.74 0 7 -4 -6 9.64 8.52 0 7 -4 6 5.19 9.70 0 7 4 6 .73 11.71 0 -7 -4 -7 83.08 18.74 0 -7 -4 7 69.45 16.01 0 7 -4 -7 75.34 13.61 0 7 -4 7 86.05 15.45 0 7 4 7 69.55 16.29 0 -7 -4 -8 43.52 15.98 0 -7 -4 8 12.48 12.34 0 7 -4 -8 42.88 12.09 0 7 -4 8 26.20 12.27 0 7 4 8 32.26 13.62 0 -7 -4 -9 48.03 17.55 0 -7 -4 9 41.41 15.48 0 7 -4 -9 43.88 11.97 0 7 -4 9 13.69 12.13 0 7 4 9 28.71 13.36 0 -7 -4 -10 61.54 18.98 0 -7 -4 10 52.01 17.09 0 7 -4 10 59.90 15.37 0 7 4 10 73.23 16.96 0 -7 -4 -11 27.78 19.35 0 -7 -4 11 25.39 15.96 0 7 -4 11 36.99 32.11 0 7 -4 11 31.98 14.28 0 7 4 11 25.51 14.27 0 -7 -4 -12 26.30 20.31 0 -7 -4 12 16.13 16.20 0 7 -4 12 12.36 34.36 0 7 -4 12 8.08 13.95 0 7 4 12 23.15 13.69 0 -7 -4 -13 66.02 25.26 0 -7 -4 13 31.45 18.03 0 7 -4 13 83.52 41.69 0 7 -4 13 38.99 17.86 0 7 4 13 75.29 19.12 0 -7 -4 -14 -12.54 27.22 0 -7 -4 14 28.28 18.60 0 7 -4 14 19.61 36.92 0 7 -4 14 -6.49 15.66 0 7 4 14 19.71 14.64 0 -7 -5 0 53.65 14.83 0 7 -5 0 46.60 11.82 0 7 5 0 34.87 18.99 0 -7 -5 -1 527.11 29.76 0 -7 -5 1 478.13 28.63 0 7 -5 -1 536.15 25.70 0 7 -5 1 431.86 24.32 0 7 5 1 419.69 33.40 0 -7 -5 -2 285.06 23.63 0 -7 -5 2 284.00 23.87 0 7 -5 -2 266.62 19.75 0 7 -5 2 273.91 21.02 0 7 5 2 219.00 26.80 0 -7 -5 -3 187.04 20.91 0 -7 -5 3 170.14 20.63 0 7 -5 -3 174.32 17.58 0 7 -5 3 152.77 18.63 0 7 5 3 155.66 23.53 0 -7 -5 -4 327.95 25.65 0 -7 -5 4 325.78 25.56 0 7 -5 -4 346.97 22.07 0 7 -5 4 322.72 71.40 0 7 -5 4 330.00 23.39 0 7 5 4 328.89 29.07 0 -7 -5 -5 397.65 28.52 0 -7 -5 5 359.71 26.96 0 7 -5 -5 408.57 23.44 0 7 -5 5 324.04 66.06 0 7 -5 5 399.30 25.60 0 7 5 5 385.76 30.56 0 -7 -5 -6 117.87 21.32 0 -7 -5 6 76.56 16.74 0 7 -5 -6 102.00 15.47 0 7 -5 6 118.34 56.28 0 7 -5 6 86.30 16.48 0 7 5 6 95.33 19.91 0 -7 -5 -7 549.40 34.72 0 -7 -5 7 496.71 31.94 0 7 -5 -7 517.73 26.12 0 7 -5 7 770.60 91.02 0 7 -5 7 489.74 29.25 0 7 5 7 490.86 33.49 0 -7 -5 -8 193.32 26.91 0 -7 -5 8 188.33 25.98 0 7 -5 -8 155.63 18.38 0 7 -5 8 212.03 60.79 0 7 -5 8 173.52 22.68 0 7 5 8 164.53 24.22 0 -7 -5 -9 238.90 29.20 0 -7 -5 9 183.91 26.18 0 -7 -5 9 161.55 54.80 0 7 -5 -9 244.45 20.87 0 7 -5 9 246.45 61.07 0 7 -5 9 164.83 22.51 0 7 5 9 222.19 27.03 0 -7 -5 -10 307.26 34.20 0 -7 -5 10 279.99 30.50 0 -7 -5 10 154.68 55.94 0 7 -5 -10 281.83 22.74 0 7 -5 10 360.33 71.36 0 7 -5 10 288.63 27.76 0 7 5 10 341.10 32.89 0 -7 -5 11 235.48 32.09 0 7 -5 -11 232.52 23.16 0 7 -5 11 258.47 28.71 0 7 -5 12 124.70 29.79 0 -7 -6 0 .02 18.07 0 7 -6 0 12.58 55.44 0 7 6 0 3.88 16.20 0 -7 -6 -1 153.57 34.29 0 -7 -6 1 178.22 35.02 0 7 -6 -1 272.34 75.92 0 7 -6 1 149.74 65.95 0 7 6 -1 128.36 27.11 0 7 6 1 165.86 28.06 0 -7 -6 2 114.38 33.17 0 7 -6 -2 103.04 51.20 0 7 -6 2 82.27 70.67 0 7 6 -2 61.13 22.92 0 7 6 2 56.52 20.48 0 7 -6 -3 52.11 40.89 0 7 6 -3 40.79 23.51 0 7 -6 -4 121.56 46.15 0 7 6 -4 -23.00 21.89 0 7 6 -5 46.80 34.28 0 8 0 0 579.57 25.63 0 8 0 -1 315.02 20.29 0 8 0 1 298.73 19.79 0 8 0 -2 249.57 18.48 0 8 0 2 246.78 18.77 0 8 0 -3 1126.33 34.78 0 8 0 3 1077.92 34.06 0 8 0 -4 73.82 13.14 0 8 0 4 61.87 12.58 0 8 0 -5 530.34 25.63 0 8 0 5 497.68 25.32 0 8 0 -6 488.00 24.89 0 8 0 6 505.91 25.79 0 8 0 -7 50.52 11.68 0 8 0 7 62.07 13.60 0 8 0 -8 349.09 22.56 0 8 0 8 351.69 23.52 0 8 0 9 790.23 32.84 0 8 0 10 12.62 11.38 0 8 0 11 617.75 31.67 0 8 0 12 350.39 27.41 0 8 0 13 19.46 14.23 0 8 0 14 378.04 31.50 0 8 -1 0 15.02 8.34 0 8 1 0 10.65 7.41 0 8 -1 -1 25.91 9.75 0 8 -1 1 34.70 10.08 0 8 1 -1 14.10 7.54 0 8 1 1 24.27 8.92 0 8 -1 -2 5.00 7.62 0 8 -1 2 14.51 8.46 0 8 1 -2 16.38 7.97 0 8 1 2 2.06 6.89 0 8 -1 -3 4.12 7.39 0 8 -1 3 5.51 7.60 0 8 1 -3 7.88 7.21 0 8 1 3 10.60 8.01 0 8 -1 -4 -2.53 7.30 0 8 -1 4 -6.96 6.90 0 8 1 -4 4.99 7.36 0 8 1 4 -1.51 7.15 0 8 -1 -5 14.09 8.98 0 8 -1 5 .00 7.95 0 8 1 -5 8.58 7.60 0 8 1 5 11.37 8.25 0 8 -1 -6 9.34 8.49 0 8 -1 6 5.05 8.49 0 8 1 -6 12.32 8.13 0 8 1 6 6.64 8.27 0 8 -1 -7 16.35 9.20 0 8 -1 7 24.96 10.73 0 8 1 -7 25.32 9.69 0 8 1 7 19.33 9.93 0 8 -1 -8 9.42 8.92 0 8 -1 8 11.45 9.97 0 8 1 -8 3.92 7.94 0 8 1 8 10.65 9.60 0 8 -1 9 2.42 9.76 0 8 1 9 -24.17 12.82 0 8 1 9 1.46 9.58 0 8 -1 10 -1.78 9.94 0 8 1 10 -10.79 11.89 0 8 1 10 1.17 10.41 0 8 -1 11 .85 11.47 0 8 1 11 7.34 12.48 0 8 1 11 1.64 10.59 0 8 -1 12 10.53 12.95 0 8 1 12 8.38 11.86 0 8 1 12 2.52 11.57 0 8 -1 13 23.09 14.28 0 8 1 13 23.70 12.95 0 8 1 13 11.27 13.78 0 8 -1 14 -1.82 16.04 0 8 1 14 .45 13.79 0 8 -2 0 472.17 24.60 0 8 2 0 477.93 23.16 0 8 -2 -1 270.06 20.27 0 8 -2 1 267.53 20.11 0 8 2 -1 267.28 18.42 0 8 2 1 293.56 19.23 0 -8 -2 -2 225.90 37.18 0 8 -2 -2 190.10 18.01 0 8 -2 2 170.74 17.63 0 8 2 -2 167.84 15.73 0 8 2 2 166.53 16.29 0 -8 -2 -3 879.85 58.73 0 8 -2 -3 1063.04 35.03 0 8 -2 3 1064.29 35.17 0 8 2 -3 980.48 31.74 0 8 2 3 1017.19 32.78 0 -8 -2 -4 80.31 31.05 0 8 -2 -4 64.08 12.70 0 8 -2 4 65.18 13.22 0 8 2 -4 72.16 12.18 0 8 2 4 84.31 13.46 0 -8 -2 -5 435.98 50.20 0 8 -2 -5 393.35 23.66 0 8 -2 5 429.79 24.96 0 8 2 -5 426.45 22.74 0 8 2 5 458.08 24.16 0 -8 -2 -6 434.17 51.04 0 8 -2 -6 458.58 25.28 0 8 -2 6 454.82 26.10 0 8 2 -6 458.02 23.65 0 8 2 6 460.34 24.54 0 -8 -2 -7 124.07 36.39 0 8 -2 -7 89.34 15.25 0 8 -2 7 81.77 15.15 0 8 2 -7 69.73 12.78 0 8 2 7 79.81 14.61 0 -8 -2 -8 405.62 55.14 0 8 -2 -8 280.55 22.44 0 8 -2 8 305.85 23.81 0 8 2 -8 317.28 21.51 0 8 2 8 252.01 26.65 0 8 2 8 296.56 22.36 0 -8 -2 -9 798.49 69.43 0 8 -2 -9 752.29 33.00 0 8 -2 9 723.13 33.24 0 8 2 -9 790.63 31.72 0 8 2 9 806.71 36.96 0 8 2 9 743.76 32.23 0 -8 -2 -10 5.60 32.97 0 8 -2 10 -3.25 11.47 0 8 2 10 5.17 12.63 0 8 2 10 3.68 11.07 0 -8 -2 -11 705.73 61.53 0 8 -2 11 580.91 32.84 0 8 2 11 596.92 32.80 0 8 2 11 610.74 31.91 0 -8 -2 -12 379.88 48.41 0 8 -2 12 271.91 27.41 0 8 2 12 300.41 26.19 0 8 2 12 270.22 26.18 0 -8 -2 -13 59.28 23.88 0 8 -2 13 15.23 18.84 0 8 2 13 34.36 12.76 0 8 2 13 5.96 13.86 0 -8 -2 -14 363.73 42.57 0 8 2 14 355.64 30.30 0 8 2 14 285.53 34.43 0 -8 -3 0 70.43 19.94 0 8 -3 0 74.80 13.49 0 8 3 0 64.60 11.57 0 -8 -3 -1 -13.47 14.09 0 -8 -3 1 -10.48 14.25 0 8 -3 -1 8.42 8.99 0 8 -3 1 2.21 8.68 0 8 3 -1 9.73 7.40 0 8 3 1 -4.17 6.79 0 -8 -3 -2 22.72 17.95 0 -8 -3 2 37.80 17.74 0 8 -3 -2 31.82 11.35 0 8 -3 2 53.23 12.86 0 8 3 -2 37.98 9.67 0 8 3 2 29.95 9.71 0 -8 -3 -3 23.10 16.54 0 -8 -3 3 16.25 16.84 0 8 -3 -3 29.24 11.07 0 8 -3 3 26.54 11.39 0 8 3 -3 32.70 9.64 0 8 3 3 14.54 8.87 0 -8 -3 -4 25.02 18.61 0 -8 -3 4 16.05 18.93 0 8 -3 -4 21.55 10.58 0 8 -3 4 23.69 11.41 0 8 3 -4 22.22 8.40 0 8 3 4 16.75 9.67 0 -8 -3 -5 -7.57 17.17 0 8 -3 -5 27.63 11.10 0 8 -3 5 4.16 10.20 0 8 3 -5 12.84 7.69 0 8 3 5 1.36 8.12 0 -8 -3 -6 63.14 22.73 0 8 -3 -6 55.26 13.37 0 8 -3 6 66.61 14.93 0 8 3 -6 79.78 12.96 0 8 3 6 55.35 18.62 0 8 3 6 80.25 14.72 0 -8 -3 -7 14.36 19.13 0 8 -3 -7 16.07 10.58 0 8 -3 7 9.95 11.59 0 8 3 -7 11.44 8.22 0 8 3 7 .11 14.14 0 8 3 7 2.96 9.29 0 -8 -3 -8 39.01 25.17 0 8 -3 -8 45.32 13.83 0 8 -3 8 44.47 15.02 0 8 3 -8 30.32 9.61 0 8 3 8 34.76 16.41 0 8 3 8 44.72 13.52 0 -8 -3 -9 20.57 25.15 0 8 -3 -9 17.97 12.20 0 8 -3 9 12.16 12.70 0 8 3 -9 27.66 9.88 0 8 3 9 18.02 14.53 0 8 3 9 15.79 11.92 0 -8 -3 -10 20.92 25.10 0 8 -3 -10 15.61 11.90 0 8 -3 10 -3.94 12.92 0 8 3 -10 7.95 8.23 0 8 3 10 .00 12.97 0 8 3 10 -13.65 10.12 0 -8 -3 -11 11.76 29.39 0 8 -3 -11 24.94 13.95 0 8 -3 11 8.64 16.19 0 8 3 -11 20.69 10.06 0 8 3 11 20.90 13.84 0 8 3 11 13.27 20.97 0 -8 -3 -12 28.80 39.89 0 -8 -4 0 400.62 31.35 0 8 -4 0 400.71 25.16 0 -8 -4 -1 236.64 27.53 0 -8 -4 1 202.82 25.31 0 8 -4 -1 266.14 21.71 0 8 -4 1 231.53 21.53 0 -8 -4 -2 179.87 26.09 0 -8 -4 2 164.98 24.55 0 8 -4 -2 135.63 18.04 0 8 -4 2 148.26 19.47 0 -8 -4 -3 748.19 41.38 0 -8 -4 3 724.72 38.59 0 8 -4 -3 741.89 31.78 0 8 -4 3 762.88 32.69 0 8 4 3 637.23 39.84 0 -8 -4 -4 79.45 21.56 0 -8 -4 4 42.91 16.47 0 8 -4 -4 40.90 13.07 0 8 -4 4 37.26 13.65 0 8 4 4 26.76 18.07 0 -8 -4 -5 371.86 35.51 0 -8 -4 5 342.20 30.38 0 8 -4 -5 337.91 23.96 0 8 -4 5 352.31 25.86 0 8 4 5 296.06 30.12 0 -8 -4 -6 291.35 33.33 0 -8 -4 6 249.02 28.66 0 8 -4 -6 311.78 23.76 0 8 -4 6 269.52 24.57 0 8 4 6 292.05 29.10 0 -8 -4 -7 73.31 23.59 0 -8 -4 7 78.14 20.80 0 8 -4 -7 57.67 14.95 0 8 -4 7 38.18 15.06 0 8 4 7 49.25 26.79 0 -8 -4 -8 196.72 47.36 0 8 -4 -8 165.37 24.06 0 8 -4 8 159.31 29.63 0 9 0 0 1.88 8.90 0 9 0 -1 9.85 9.80 0 9 0 1 6.60 9.74 0 9 0 -2 4.67 8.87 0 9 0 2 -8.49 8.92 0 9 0 -3 16.00 10.08 0 9 0 3 19.51 11.51 0 9 0 -4 .93 8.75 0 9 0 4 -14.01 9.11 0 9 0 -5 15.43 9.96 0 9 0 5 9.18 11.54 0 9 0 -6 -3.87 9.17 0 9 0 6 -7.00 10.68 0 9 -1 0 193.95 20.63 0 9 1 0 182.16 19.39 0 9 -1 -1 605.08 30.13 0 9 -1 1 605.28 30.20 0 9 1 -1 660.30 30.11 0 9 1 1 617.60 29.55 0 9 -1 -2 265.92 22.39 0 9 -1 2 270.68 23.28 0 9 1 -2 259.51 21.23 0 9 1 2 242.40 21.58 0 9 -1 -3 70.69 15.15 0 9 -1 3 45.01 13.86 0 9 1 -3 55.64 13.21 0 9 1 3 27.92 11.77 0 9 -1 -4 277.46 23.48 0 9 -1 4 248.30 22.92 0 9 1 -4 243.55 21.41 0 9 1 4 265.73 22.69 0 9 -1 -5 502.42 34.35 0 9 -1 5 440.03 37.00 0 9 1 -5 432.75 26.31 0 9 1 5 434.76 27.07 0 9 1 -6 181.91 22.86 0 9 1 6 192.62 22.77 0 9 -2 0 10.13 14.62 0 9 2 0 5.00 9.00 0 9 -2 -1 13.56 15.75 0 9 2 -1 -3.12 7.66 0 9 2 1 3.79 9.19 0 9 2 -2 21.64 9.98 0 9 2 2 9.13 9.66 0 9 2 -3 8.69 8.76 0 9 2 3 6.96 9.87 0 9 2 -4 18.34 9.99 0 9 2 4 16.37 11.68 0 9 2 -5 12.39 10.64 0 9 2 5 5.26 10.98 0 ; _shelx_hkl_checksum 71844 _shelx_res_file ; TITL test3_b.res in Pna2(1) habitus.res created by SHELXL-2019/3 at 17:40:05 on 25-Aug-2023 REM Old TITL test3 in Pna2(1) REM SHELXT solution in Pna2(1) REM R1 0.145, Rweak 0.003, Alpha 0.018, Orientation as input REM Flack x = 0.367 ( 0.083 ) from Parsons' quotients REM Formula found by SHELXT: Bi O2 CELL 0.71073 5.3854 5.3676 17.0506 90.000 90.000 90.000 ZERR 4.000 0.0013 0.0013 0.0041 0.000 0.000 0.000 LATT -1 SYMM -X, -Y, 1/2+Z SYMM 1/2+X, 1/2-Y, Z SYMM 1/2-X, 1/2+Y, 1/2+Z SFAC H BI N O UNIT 4 8 4 24 TEMP -173 twin 0 -1 0 1 0 0 0 0 -1 size 0.09 0.08 0.01 rem synthesis Owen Missen A0top rem yellowish plate rem coordinaten entsprechend Henry aufgestellt um group-subgroup relations rem Cmc21 -->Pna21 mit transformationsmatrix -b,a,c verwandt (k2 uebergang acta L.S. 100 conn 10 3.0 $Bi conn 8 3.0 O2 BOND $H LIST 4 FMAP 2 PLAN 20 WGHT 0.021300 BASF 0.07039 FVAR 0.16914 BI1 2 0.043616 -0.007846 0.236583 11.00000 0.00314 0.00303 = 0.00279 0.00006 0.00001 -0.00018 BI2 2 0.082171 0.481988 0.084417 11.00000 0.00461 0.00439 = 0.00395 0.00100 -0.00086 -0.00002 O1A 4 0.286611 0.246778 0.167820 11.00000 0.00410 O1B 4 0.284038 0.739413 0.168324 11.00000 0.00527 O2 4 0.493685 0.453864 0.042306 11.00000 0.00966 N1 3 0.021392 0.496893 0.375935 11.00000 0.00915 O3 4 0.036257 0.497701 0.300366 11.00000 0.00888 O4 4 0.865017 0.635147 0.408370 11.00000 0.01484 O5 4 0.162565 0.360429 0.415300 11.00000 0.01447 HKLF 4 REM test3_b.res in Pna2(1) REM wR2 = 0.0574, GooF = S = 0.984, Restrained GooF = 0.983 for all data REM R1 = 0.0298 for 2407 Fo > 4sig(Fo) and 0.0380 for all 2798 data REM 48 parameters refined using 1 restraints END WGHT 0.0213 0.0000 REM Highest difference peak 3.128, deepest hole -3.609, 1-sigma level 0.638 Q1 1 0.5856 0.3000 0.0492 11.00000 0.05 3.13 Q2 1 0.0381 -0.0084 0.2891 11.00000 0.05 3.02 Q3 1 0.0902 0.6256 0.0568 11.00000 0.05 2.88 Q4 1 -0.1018 0.5648 0.2441 11.00000 0.05 2.73 Q5 1 0.0701 0.4641 0.2163 11.00000 0.05 2.63 Q6 1 0.9351 0.5276 0.4510 11.00000 0.05 2.59 Q7 1 0.6889 0.5055 0.0390 11.00000 0.05 2.51 Q8 1 0.0834 0.4727 0.0399 11.00000 0.05 2.43 Q9 1 0.0861 0.6304 0.1124 11.00000 0.05 2.40 Q10 1 0.0504 -0.0024 0.1814 11.00000 0.05 2.37 Q11 1 0.0748 0.2106 0.1197 11.00000 0.05 2.36 Q12 1 0.2941 0.8470 0.1580 11.00000 0.05 2.36 Q13 1 0.2985 0.0827 0.1080 11.00000 0.05 2.36 Q14 1 0.2110 0.5272 0.0863 11.00000 0.05 2.34 Q15 1 -0.0204 0.5336 0.0907 11.00000 0.05 2.26 Q16 1 0.0550 -0.1831 0.2618 11.00000 0.05 2.26 Q17 1 0.0402 0.6904 0.2686 11.00000 0.05 2.22 Q18 1 0.0438 0.1310 0.2552 11.00000 0.05 2.20 Q19 1 0.4509 0.5244 0.1509 11.00000 0.05 2.17 Q20 1 0.1686 0.9748 0.1321 11.00000 0.05 2.16 ; _shelx_res_checksum 47215 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Bi Bi1 0.04362(7) -0.00785(7) 0.23658(3) 0.00299(7) Uani d 1 . . Bi Bi2 0.08217(8) 0.48199(6) 0.08442(4) 0.00432(8) Uani d 1 . . O O1A 0.2866(15) 0.2468(15) 0.1678(5) 0.0041(15) Uiso d 1 . . O O1B 0.2840(15) 0.7394(15) 0.1683(5) 0.0053(15) Uiso d 1 . . O O2 0.4937(17) 0.4539(16) 0.0423(6) 0.0097(15) Uiso d 1 . . N N1 0.021(2) 0.4969(18) 0.3759(6) 0.0091(19) Uiso d 1 . . O O3 0.0363(16) 0.4977(15) 0.3004(5) 0.0089(14) Uiso d 1 . . O O4 0.8650(17) 0.6351(17) 0.4084(6) 0.0148(19) Uiso d 1 . . O O5 0.1626(17) 0.3604(16) 0.4153(6) 0.0145(18) Uiso d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Bi1 0.00314(12) 0.00303(15) 0.00279(14) -0.00018(11) 0.00001(12) 0.0001(2) Bi2 0.00461(13) 0.00439(16) 0.00395(15) -0.00002(11) -0.00086(14) 0.0010(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Bi Bi -4.1077 10.2566 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O1B Bi1 O1B 3_455 1_545 75.34(18) ? O1B Bi1 O1A 3_455 . 116.2(3) ? O1B Bi1 O1A 1_545 . 75.8(3) ? O1B Bi1 O1A 3_455 3_455 72.0(3) ? O1B Bi1 O1A 1_545 3_455 117.4(3) ? O1A Bi1 O1A . 3_455 73.15(16) ? O1A Bi2 O1B . . 72.6(3) ? O1A Bi2 O2 . . 71.7(3) ? O1B Bi2 O2 . . 77.2(3) ? O1A Bi2 O1A . 3_455 70.34(18) ? O1B Bi2 O1A . 3_455 104.4(3) ? O2 Bi2 O1A . 3_455 139.4(3) ? O1A Bi2 O2 . 3_455 75.1(3) ? O1B Bi2 O2 . 3_455 147.7(3) ? O2 Bi2 O2 . 3_455 91.8(3) ? O1A Bi2 O2 3_455 3_455 64.8(3) ? O1A Bi2 O1B . 3_465 106.4(3) ? O1B Bi2 O1B . 3_465 66.50(16) ? O2 Bi2 O1B . 3_465 141.9(3) ? O1A Bi2 O1B 3_455 3_465 64.7(3) ? O2 Bi2 O1B 3_455 3_465 125.2(3) ? Bi2 O1A Bi1 . . 113.5(3) ? Bi2 O1A Bi1 . 3 106.4(3) ? Bi1 O1A Bi1 . 3 117.4(4) ? Bi2 O1A Bi2 . 3 103.7(3) ? Bi1 O1A Bi2 . 3 112.2(3) ? Bi1 O1A Bi2 3 3 102.1(3) ? Bi1 O1B Bi1 3 1_565 116.1(4) ? Bi1 O1B Bi2 3 . 107.1(3) ? Bi1 O1B Bi2 1_565 . 115.2(4) ? Bi1 O1B Bi2 3 3_565 102.8(3) ? Bi1 O1B Bi2 1_565 3_565 107.3(3) ? Bi2 O1B Bi2 . 3_565 107.3(3) ? Bi2 O2 Bi2 . 3 98.8(3) ? O5 N1 O4 . 1_455 121.3(11) ? O5 N1 O3 . . 120.0(10) ? O4 N1 O3 1_455 . 118.7(10) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Bi1 O1B 3_455 2.203(8) ? Bi1 O1B 1_545 2.207(8) ? Bi1 O1A . 2.226(8) ? Bi1 O1A 3_455 2.292(8) ? Bi1 O3 3 2.868(9) ? Bi1 O3 1_545 2.868(8) ? Bi1 O3 . 2.924(8) ? Bi1 O3 3_455 2.941(9) ? Bi2 O1A . 2.197(8) ? Bi2 O1B . 2.267(8) ? Bi2 O2 . 2.334(9) ? Bi2 O1A 3_455 2.462(8) ? Bi2 O2 3_455 2.493(9) ? Bi2 O1B 3_465 2.619(8) ? N1 O5 . 1.251(14) ? N1 O4 1_455 1.251(13) ? N1 O3 . 1.291(14) ? _cod_database_fobs_code 2022958