#------------------------------------------------------------------------------ #$Date: 2023-11-22 03:59:01 +0100 (Wed, 22 Nov 2023) $ #$Revision: 287720 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/29/2022949.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022949 loop_ _publ_author_name 'Zouhair, Mustapha' 'El Ghayati, Lhoussaine' 'El Monfalouti, Hanae' 'Abchihi, Hicham' 'H\"okelek, Tuncer' 'Ahmed, Mazzah' 'Mague, Joel T.' 'Sebbar, Nada Kheira' _publ_section_title ; Synthesis, structure and Hirshfeld surface analysis of 1,3-bis[(1-octyl-1H-1,2,3-triazol-4-yl)methyl]-1H-benzo[d]imidazol-2(3H)-one ; _journal_coeditor_code HB8081 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E Crystallographic Communications' _journal_paper_doi 10.1107/S2056989023009891 _journal_volume 79 _journal_year 2023 _chemical_absolute_configuration unk _chemical_formula_moiety 'C29 H44 N8 O' _chemical_formula_sum 'C29 H44 N8 O' _chemical_formula_weight 520.72 _chemical_name_systematic 1,3-Bis[(1-octyl-1H-1,2,3-triazol-4-yl)methyl]-1H-benzo[d]imidazol-2(3H)-one _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_Hall 'P 2yb' _space_group_name_H-M_alt 'P 1 21 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2019/1 _cell_angle_alpha 90 _cell_angle_beta 94.9620(10) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 5.5229(2) _cell_length_b 11.9579(5) _cell_length_c 22.5767(9) _cell_measurement_reflns_used 9942 _cell_measurement_temperature 150(2) _cell_measurement_theta_max 28.245 _cell_measurement_theta_min 2.468 _cell_volume 1485.43(10) _computing_cell_refinement ; SAINT (Bruker, 2020) ; _computing_data_collection ; APEX3 (Bruker, 2020) ; _computing_data_reduction ; SAINT (Bruker, 2020) ; _computing_molecular_graphics ; DIAMOND (Brandenburg & Putz, 2012) ; _computing_publication_material ; SHELXTL (Sheldrick, 2008) ; _computing_structure_refinement ; SHELXL2018/1 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 150(2) _diffrn_detector_area_resol_mean 7.3910 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device 'Bruker D8 QUEST PHOTON 3 diffractometer' _diffrn_measurement_device_type 'Bruker D8 QUEST PHOTON 3 diffractometer' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0403 _diffrn_reflns_av_unetI/netI 0.0292 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_h_min -7 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 30 _diffrn_reflns_limit_l_min -30 _diffrn_reflns_number 44175 _diffrn_reflns_theta_full 28.300 _diffrn_reflns_theta_max 28.328 _diffrn_reflns_theta_min 1.811 _diffrn_source 'fine-focus sealed tube' _diffrn_source_current 30.0 _diffrn_source_power 1.50 _diffrn_source_voltage 50 _exptl_absorpt_coefficient_mu 0.074 _exptl_absorpt_correction_T_max 1.00 _exptl_absorpt_correction_T_min 0.97 _exptl_absorpt_correction_type numerical _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.164 _exptl_crystal_density_method 'not measured' _exptl_crystal_description plate _exptl_crystal_F_000 564 _exptl_crystal_size_max 0.427 _exptl_crystal_size_mid 0.236 _exptl_crystal_size_min 0.044 _refine_diff_density_max 0.211 _refine_diff_density_min -0.150 _refine_ls_abs_structure_details ; Refined as an inversion twin ; _refine_ls_abs_structure_Flack 0.2(13) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.049 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 346 _refine_ls_number_reflns 7403 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.049 _refine_ls_R_factor_all 0.0422 _refine_ls_R_factor_gt 0.0356 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0469P)^2^+0.1166P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0860 _refine_ls_wR_factor_ref 0.0900 _reflns_number_gt 6607 _reflns_number_total 7403 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file hb8081sup1.cif _cod_data_source_block I _cod_original_sg_symbol_H-M 'P 21' _cod_database_code 2022949 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.969 _shelx_estimated_absorpt_t_max 0.997 _shelx_hkl_file ; -1 0 0 167.08 7.50 1 0 0 168.28 7.50 -1 0 0 183.08 7.40 -1 0 0 173.28 7.60 1 0 0 176.38 7.60 1 0 0 166.08 7.40 -1 0 0 167.28 7.20 -1 0 0 169.58 7.40 1 0 0 177.18 7.50 1 0 0 165.38 7.70 -1 0 0 183.48 7.50 1 0 0 176.78 7.30 2 0 0 894.01 35.80 2 0 0 918.51 36.30 -2 0 0 856.51 36.20 2 0 0 854.41 36.60 2 0 0 858.31 36.50 -2 0 0 889.01 35.80 -2 0 0 895.31 36.00 -2 0 0 856.01 36.70 2 0 0 878.31 36.20 -2 0 0 860.31 36.50 -2 0 0 838.42 36.00 2 0 0 869.41 36.30 -2 0 0 848.72 36.30 -3 0 0 185.28 8.30 3 0 0 188.08 8.70 -3 0 0 179.78 8.00 -3 0 0 168.08 8.60 3 0 0 184.98 9.20 -3 0 0 169.58 9.50 3 0 0 185.08 9.30 3 0 0 174.88 8.40 -3 0 0 171.38 9.30 3 0 0 180.78 8.00 -3 0 0 181.08 8.80 3 0 0 184.18 8.70 3 0 0 185.58 9.10 4 0 0 27.40 2.80 4 0 0 27.10 2.80 4 0 0 23.90 2.00 4 0 0 27.00 3.50 -4 0 0 23.50 2.80 -4 0 0 21.20 3.40 4 0 0 23.50 3.10 5 0 0 3.30 2.40 5 0 0 4.30 2.10 5 0 0 4.00 1.90 -5 0 0 6.80 2.10 -5 0 0 7.00 2.60 -6 0 0 102.39 7.30 6 0 0 103.29 8.30 6 0 0 107.29 8.00 6 0 0 98.19 7.30 -6 0 0 112.99 8.50 6 0 0 116.59 7.40 7 0 0 9.80 3.20 7 0 0 9.50 3.30 7 0 0 16.30 4.40 -7 0 0 13.40 4.30 0 -1 0 0.10 0.20 0 1 0 -0.10 0.30 1 -1 0 1308.37 57.29 -1 -1 0 1379.76 57.59 -1 -1 0 1455.45 57.59 1 -1 0 1492.45 57.59 1 -1 0 1461.35 57.29 1 -1 0 1346.07 57.49 -1 -1 0 1414.46 57.69 -1 -1 0 1410.26 57.59 1 -1 0 1442.86 57.69 -1 -1 0 1358.96 57.69 1 -1 0 1441.66 57.79 -1 -1 0 1455.35 57.49 1 -1 0 1333.77 57.79 1 -1 0 1363.96 57.39 -1 -1 0 1427.26 57.39 -1 1 0 1393.96 57.49 1 1 0 1431.66 57.69 1 1 0 1399.26 57.59 -1 1 0 1368.86 57.39 -1 1 0 1438.06 57.49 1 1 0 1446.76 57.59 -1 1 0 1249.47 57.99 -1 1 0 1398.56 57.69 -1 1 0 1351.86 57.89 1 1 0 1418.66 57.69 1 1 0 1473.05 57.39 1 1 0 1437.06 57.69 1 1 0 1417.36 57.49 -1 1 0 1444.86 57.59 1 1 0 1431.06 57.59 2 -1 0 16.60 1.40 -2 -1 0 14.60 1.70 2 -1 0 14.40 1.50 2 -1 0 15.00 2.00 2 -1 0 11.80 1.20 2 -1 0 14.30 1.80 -2 -1 0 13.00 1.70 -2 -1 0 15.90 1.20 2 -1 0 12.50 1.40 -2 -1 0 12.50 1.60 -2 -1 0 14.20 1.50 2 -1 0 17.30 1.60 -2 -1 0 14.60 1.20 -2 -1 0 16.90 1.60 -2 1 0 14.40 1.50 -2 1 0 12.80 1.20 2 1 0 13.20 1.60 2 1 0 14.00 1.70 2 1 0 15.20 1.70 -2 1 0 12.50 1.40 2 1 0 14.20 1.70 2 1 0 12.10 1.60 -2 1 0 14.70 1.20 -2 1 0 12.70 1.80 2 1 0 13.40 1.80 2 1 0 15.50 1.20 -2 1 0 18.30 1.30 2 1 0 10.60 1.70 -2 1 0 13.30 2.00 -3 -1 0 180.98 7.90 -3 -1 0 183.98 8.30 -3 -1 0 160.88 8.60 -3 -1 0 179.78 9.00 -3 -1 0 169.28 8.50 -3 -1 0 173.38 9.10 3 -1 0 180.18 8.90 3 -1 0 171.08 8.30 3 -1 0 187.38 8.00 3 -1 0 176.08 8.50 3 -1 0 179.08 8.30 3 -1 0 164.18 9.10 -3 -1 0 174.98 7.70 3 1 0 185.18 8.90 -3 1 0 173.48 7.90 3 1 0 180.58 8.60 3 1 0 175.88 8.60 -3 1 0 183.58 9.40 3 1 0 188.98 8.70 -3 1 0 163.38 8.40 3 1 0 192.98 9.20 3 1 0 169.08 7.90 -3 1 0 179.68 7.90 -3 1 0 164.78 8.50 4 -1 0 10.10 1.90 4 -1 0 9.80 2.60 -4 -1 0 10.40 2.10 4 -1 0 8.00 2.10 4 -1 0 8.80 1.90 -4 -1 0 11.60 2.60 4 -1 0 7.70 1.40 -4 1 0 9.30 1.80 4 1 0 9.30 1.50 4 1 0 11.40 2.50 4 1 0 7.50 1.80 4 1 0 8.50 2.20 4 1 0 9.80 2.10 -4 1 0 8.50 2.40 -4 1 0 8.30 1.80 -5 -1 0 23.20 3.30 5 -1 0 18.60 3.60 5 -1 0 19.20 3.10 5 -1 0 14.70 3.10 5 1 0 22.20 3.10 -5 1 0 16.50 3.50 5 1 0 17.50 3.90 5 1 0 16.60 3.30 -5 1 0 12.20 2.60 6 -1 0 31.30 4.00 -6 -1 0 31.50 4.20 6 -1 0 31.20 4.90 6 -1 0 37.30 4.90 -6 -1 0 36.10 5.20 6 -1 0 36.80 4.40 -6 1 0 36.40 5.30 6 1 0 29.30 4.60 6 1 0 45.00 5.40 6 1 0 35.70 4.30 6 1 0 31.70 4.20 7 -1 0 57.59 5.50 -7 -1 0 51.19 6.60 7 -1 0 34.10 6.20 7 -1 0 43.30 5.40 7 1 0 47.30 5.50 -7 1 0 50.19 6.80 7 1 0 50.19 5.80 7 1 0 47.20 6.20 0 -2 0 306.97 13.30 0 -2 0 307.27 13.20 0 -2 0 317.77 13.00 0 -2 0 319.27 13.20 0 -2 0 303.07 12.90 0 -2 0 319.77 13.20 0 -2 0 312.97 13.20 0 2 0 315.77 13.20 0 2 0 307.37 13.20 0 2 0 308.47 12.90 0 2 0 308.67 12.90 0 2 0 303.97 13.00 0 2 0 320.77 13.20 0 2 0 315.87 13.20 0 2 0 331.87 13.20 0 2 0 312.77 13.30 1 -2 0 278.87 11.60 -1 -2 0 258.77 11.30 -1 -2 0 265.97 11.60 -1 -2 0 271.47 11.60 1 -2 0 257.47 12.00 -1 -2 0 274.17 11.40 -1 -2 0 274.87 11.60 1 -2 0 264.77 11.80 1 -2 0 278.47 11.40 1 -2 0 258.47 11.50 -1 -2 0 270.57 11.60 -1 -2 0 282.47 11.60 1 -2 0 250.67 11.40 1 2 0 262.47 11.60 1 2 0 282.17 11.60 1 2 0 256.87 11.70 -1 2 0 254.97 11.50 1 2 0 274.57 11.40 -1 2 0 286.67 11.40 1 2 0 278.17 11.90 1 2 0 267.17 11.40 -1 2 0 251.57 11.50 -1 2 0 248.98 11.70 1 2 0 263.57 11.60 1 2 0 280.97 11.60 -1 2 0 266.47 12.00 -1 2 0 280.97 11.30 -1 2 0 286.07 11.60 -1 2 0 263.37 11.60 1 2 0 264.17 11.40 -1 2 0 256.77 11.80 -2 -2 0 65.19 3.20 2 -2 0 63.09 3.80 -2 -2 0 61.69 3.60 2 -2 0 64.09 3.40 -2 -2 0 66.89 3.90 2 -2 0 62.19 4.10 -2 -2 0 56.69 3.60 -2 -2 0 62.69 3.60 2 -2 0 63.69 3.40 -2 -2 0 67.69 3.80 -2 -2 0 62.59 3.40 2 -2 0 61.29 3.20 2 -2 0 59.69 3.10 2 -2 0 62.99 3.20 2 -2 0 62.19 3.60 -2 -2 0 64.39 3.80 2 2 0 71.79 3.80 -2 2 0 68.29 3.40 2 2 0 60.19 3.70 2 2 0 63.39 3.60 2 2 0 65.29 3.20 -2 2 0 64.59 3.90 -2 2 0 77.19 4.50 2 2 0 71.79 3.90 -2 2 0 63.19 3.30 -2 2 0 64.99 3.60 2 2 0 65.39 3.80 -2 2 0 62.39 3.10 2 2 0 65.69 3.70 -2 2 0 60.19 4.10 -2 2 0 61.39 3.20 2 2 0 66.39 3.40 -3 -2 0 188.88 8.80 3 -2 0 179.58 9.20 -3 -2 0 164.58 9.70 -3 -2 0 187.88 8.30 -3 -2 0 185.58 9.20 3 -2 0 183.98 8.40 3 -2 0 179.48 8.30 -3 -2 0 198.18 9.00 3 -2 0 180.08 8.50 -3 -2 0 201.68 9.50 -3 -2 0 188.18 8.20 3 -2 0 179.18 8.50 3 -2 0 189.08 8.90 -3 2 0 175.38 8.30 -3 2 0 177.28 8.60 -3 2 0 169.58 8.80 3 2 0 186.48 9.20 3 2 0 187.08 8.20 3 2 0 179.88 8.20 3 2 0 176.88 9.70 -3 2 0 179.18 9.60 3 2 0 194.88 8.90 3 2 0 181.08 9.00 3 2 0 192.58 9.00 3 2 0 161.58 8.80 -4 -2 0 2.50 1.70 4 -2 0 2.20 1.40 4 -2 0 3.10 1.20 4 -2 0 4.60 1.80 4 -2 0 2.70 1.90 -4 -2 0 3.10 1.50 4 -2 0 0.40 1.10 -4 2 0 0.20 1.70 4 2 0 3.20 1.40 4 2 0 5.80 2.10 -4 2 0 1.00 1.20 4 2 0 0.00 1.30 4 2 0 3.60 1.50 4 2 0 2.70 1.40 5 -2 0 49.80 5.40 5 -2 0 47.20 4.00 -5 -2 0 46.10 5.00 5 -2 0 53.99 5.00 -5 -2 0 43.30 4.40 5 -2 0 46.20 4.20 5 2 0 42.40 4.80 -5 2 0 43.60 4.00 5 2 0 42.00 4.50 -5 2 0 50.39 5.50 5 2 0 48.70 4.30 6 -2 0 25.30 4.50 6 -2 0 26.60 3.90 6 -2 0 22.00 3.50 -6 -2 0 21.10 3.90 6 -2 0 30.60 4.80 -6 -2 0 34.60 4.90 6 2 0 25.80 4.50 6 2 0 25.80 4.20 6 2 0 25.80 4.10 -6 2 0 34.50 5.20 6 2 0 29.10 4.70 7 -2 0 5.70 2.50 7 -2 0 10.40 3.30 7 2 0 5.60 3.40 7 2 0 6.90 3.00 7 2 0 2.20 2.70 -7 2 0 11.50 4.10 0 -3 0 0.60 0.50 0 -3 0 0.40 0.40 0 -3 0 -0.50 0.90 0 -3 0 1.00 0.80 0 -3 0 1.60 1.50 0 3 0 4.60 1.10 0 3 0 1.60 0.80 0 3 0 -0.10 0.50 0 3 0 1.40 0.60 0 3 0 0.30 1.00 0 3 0 0.90 0.50 0 3 0 0.30 0.80 1 -3 0 612.74 25.10 -1 -3 0 609.44 25.50 -1 -3 0 596.34 24.90 -1 -3 0 617.44 25.50 1 -3 0 578.04 25.40 -1 -3 0 611.44 25.30 -1 -3 0 609.14 25.40 1 -3 0 617.34 25.30 1 -3 0 619.64 25.50 -1 -3 0 619.94 25.40 1 -3 0 569.94 25.30 1 -3 0 578.34 25.80 -1 -3 0 617.44 25.20 -1 3 0 596.04 25.10 1 3 0 605.34 25.50 -1 3 0 632.14 25.50 -1 3 0 602.34 25.30 1 3 0 628.14 25.40 1 3 0 610.94 25.50 1 3 0 642.64 25.40 -1 3 0 563.84 25.40 -1 3 0 572.34 25.30 1 3 0 603.24 24.90 -1 3 0 570.34 25.50 1 3 0 620.74 25.30 1 3 0 604.04 25.30 -1 3 0 574.34 25.30 -1 3 0 604.84 25.40 1 3 0 614.74 25.20 2 -3 0 520.95 21.80 -2 -3 0 532.95 22.70 -2 -3 0 545.25 22.60 2 -3 0 524.45 23.00 2 -3 0 504.65 22.20 -2 -3 0 537.65 22.90 2 -3 0 497.45 22.30 -2 -3 0 529.95 22.40 2 -3 0 516.65 22.80 -2 -3 0 558.44 22.20 2 -3 0 536.95 22.50 -2 -3 0 531.45 22.40 -2 -3 0 531.85 22.50 2 -3 0 523.65 21.80 2 3 0 516.05 23.40 -2 3 0 515.35 22.30 2 3 0 540.85 22.40 -2 3 0 513.55 22.50 -2 3 0 493.35 22.20 2 3 0 557.24 22.20 2 3 0 530.25 22.40 2 3 0 545.15 22.60 2 3 0 542.65 22.50 -2 3 0 521.45 22.20 -2 3 0 515.35 23.00 2 3 0 536.15 22.70 -2 3 0 473.75 22.10 -2 3 0 535.75 23.30 2 3 0 524.65 22.60 2 3 0 547.25 22.10 -3 -3 0 71.59 4.50 -3 -3 0 69.69 4.20 3 -3 0 62.39 3.60 -3 -3 0 63.89 4.30 -3 -3 0 68.09 4.50 3 -3 0 58.49 4.70 3 -3 0 63.89 4.50 3 -3 0 68.49 3.90 -3 -3 0 65.89 3.60 3 -3 0 69.19 4.20 -3 -3 0 68.99 3.90 3 -3 0 63.99 3.80 3 -3 0 62.69 3.50 3 3 0 68.99 4.30 -3 3 0 67.49 3.50 -3 3 0 65.39 3.90 3 3 0 73.79 4.40 -3 3 0 66.09 3.90 3 3 0 73.69 4.50 3 3 0 69.39 3.80 -3 3 0 62.89 3.40 3 3 0 72.19 4.40 -3 3 0 63.99 3.80 3 3 0 67.09 4.20 3 3 0 64.49 3.60 -3 3 0 58.89 4.80 4 -3 0 15.00 3.10 -4 -3 0 10.10 2.40 -4 -3 0 10.80 1.70 4 -3 0 13.20 2.30 -4 -3 0 14.00 2.60 4 -3 0 12.80 1.90 4 -3 0 13.70 2.70 -4 3 0 9.00 1.90 -4 3 0 16.20 3.30 -4 3 0 10.10 1.90 4 3 0 12.40 2.60 4 3 0 15.80 2.80 4 3 0 14.10 2.50 4 3 0 7.40 2.10 5 -3 0 81.79 6.50 5 -3 0 79.69 5.40 -5 -3 0 94.79 6.70 5 -3 0 91.39 6.10 5 -3 0 86.99 7.10 -5 -3 0 86.29 6.30 -5 3 0 98.49 7.50 5 3 0 87.99 6.40 5 3 0 96.19 6.80 5 3 0 77.89 5.80 -5 3 0 78.49 5.60 6 -3 0 110.29 7.00 6 -3 0 98.09 7.30 -6 -3 0 105.59 8.20 6 -3 0 113.79 8.80 6 -3 0 106.89 8.10 -6 -3 0 110.89 7.80 6 3 0 102.59 7.50 -6 3 0 120.09 9.00 6 3 0 105.19 8.00 6 3 0 121.09 8.50 -7 -3 0 13.10 4.30 7 -3 0 9.90 3.00 7 -3 0 13.00 4.00 7 -3 0 13.70 3.70 -7 3 0 11.90 4.30 7 3 0 8.80 3.20 7 3 0 16.20 5.50 7 3 0 12.10 3.70 0 -4 0 6747.32 308.67 0 -4 0 7568.64 308.27 0 -4 0 7983.50 308.77 0 -4 0 7552.24 309.07 0 4 0 7860.81 308.27 0 4 0 7580.84 308.77 0 4 0 7591.44 308.97 0 4 0 7765.02 308.77 -1 -4 0 8.70 1.50 -1 -4 0 8.70 1.40 1 -4 0 5.00 1.40 1 -4 0 12.00 1.50 -1 -4 0 6.40 1.20 1 -4 0 5.70 1.40 -1 -4 0 9.10 1.50 1 -4 0 11.80 2.10 1 -4 0 8.00 1.40 1 -4 0 8.40 1.60 -1 -4 0 3.60 1.30 -1 -4 0 8.20 1.30 -1 4 0 7.30 1.40 -1 4 0 12.10 1.60 1 4 0 8.80 1.50 -1 4 0 7.40 1.30 1 4 0 8.20 1.40 -1 4 0 13.40 1.70 -1 4 0 8.40 1.50 -1 4 0 4.70 1.40 1 4 0 9.50 1.40 1 4 0 6.50 1.30 1 4 0 9.10 1.40 1 4 0 7.90 1.50 -1 4 0 4.80 1.40 1 4 0 7.20 1.50 -1 4 0 13.20 1.60 1 4 0 6.80 1.30 -1 4 0 6.90 1.50 2 -4 0 1493.55 63.19 -2 -4 0 1587.44 62.99 2 -4 0 1509.95 62.89 -2 -4 0 1555.64 63.29 -2 -4 0 1573.34 63.69 2 -4 0 1475.55 63.49 2 -4 0 1443.76 63.09 -2 -4 0 1598.64 63.49 -2 -4 0 1521.65 63.29 -2 -4 0 1580.44 63.59 2 -4 0 1558.64 63.29 2 -4 0 1500.15 63.79 -2 -4 0 1601.24 63.49 -2 -4 0 1489.85 62.89 2 4 0 1519.85 63.39 -2 4 0 1454.35 63.19 -2 4 0 1432.76 63.09 -2 4 0 1493.55 62.89 2 4 0 1574.74 63.29 -2 4 0 1512.95 63.59 2 4 0 1532.75 63.69 2 4 0 1565.84 62.99 -2 4 0 1501.35 63.79 -2 4 0 1439.36 63.09 2 4 0 1593.24 63.49 -2 4 0 1472.85 62.79 -2 4 0 1521.45 63.49 2 4 0 1551.04 63.39 2 4 0 1582.84 62.99 2 4 0 1510.95 63.39 2 4 0 1610.54 62.99 3 -4 0 103.69 6.60 -3 -4 0 117.79 5.50 3 -4 0 103.29 5.10 3 -4 0 103.09 5.40 -3 -4 0 114.89 6.10 -3 -4 0 120.89 6.50 3 -4 0 110.59 5.80 -3 -4 0 112.59 6.00 -3 -4 0 115.49 5.90 3 -4 0 103.29 5.90 3 -4 0 104.29 6.40 -3 -4 0 106.59 6.10 -3 4 0 104.29 5.50 3 4 0 108.49 6.20 3 4 0 108.29 5.90 3 4 0 121.59 5.50 -3 4 0 101.29 5.60 -3 4 0 99.19 6.70 3 4 0 112.69 6.10 3 4 0 95.49 5.90 3 4 0 110.49 6.20 3 4 0 105.09 5.30 -3 4 0 99.69 5.30 -3 4 0 99.29 5.40 3 4 0 114.79 5.80 -3 4 0 100.49 5.50 4 -4 0 8.20 1.70 4 -4 0 11.80 2.20 -4 -4 0 10.20 1.90 4 -4 0 4.70 2.10 4 -4 0 7.80 1.60 -4 -4 0 4.90 1.90 -4 -4 0 6.90 2.10 4 -4 0 6.00 2.10 4 4 0 11.30 2.40 4 4 0 15.20 2.70 -4 4 0 8.00 1.70 4 4 0 10.30 2.40 4 4 0 8.10 1.90 -4 4 0 11.30 3.00 5 -4 0 32.60 4.70 5 -4 0 30.90 3.80 5 -4 0 33.20 3.30 -5 -4 0 42.60 4.50 -5 -4 0 35.50 4.10 5 -4 0 33.70 4.50 5 4 0 33.70 4.30 -5 4 0 47.00 5.30 5 4 0 39.50 4.20 5 4 0 31.70 4.10 6 -4 0 5.80 1.90 6 -4 0 11.10 3.60 -6 -4 0 6.40 2.80 -6 -4 0 9.30 3.40 6 -4 0 8.60 3.40 6 -4 0 11.90 3.00 6 4 0 8.60 2.80 6 4 0 3.10 2.40 -6 4 0 8.90 3.40 6 4 0 7.10 2.90 6 4 0 6.20 3.10 7 -4 0 -0.10 2.50 7 -4 0 2.00 2.30 7 -4 0 1.80 2.80 -7 -4 0 6.00 3.40 7 4 0 -1.00 2.50 -7 4 0 2.30 3.20 7 4 0 -0.20 3.20 0 -5 0 0.10 1.00 0 -5 0 -0.20 0.60 0 -5 0 2.40 1.00 0 -5 0 2.00 0.80 0 -5 0 0.50 0.60 0 -5 0 2.30 1.00 0 -5 0 -1.70 0.90 0 -5 0 1.10 1.00 0 5 0 0.40 1.00 0 5 0 0.50 0.90 0 5 0 -2.00 1.00 0 5 0 0.20 0.90 0 5 0 4.00 1.10 0 5 0 2.20 0.60 0 5 0 -0.50 0.60 0 5 0 1.60 1.00 0 5 0 -0.20 0.70 0 5 0 1.00 0.70 0 5 0 3.00 1.10 1 -5 0 1757.72 75.79 -1 -5 0 1934.11 76.19 -1 -5 0 1874.51 75.69 -1 -5 0 1871.81 75.59 1 -5 0 1824.32 74.79 -1 -5 0 1880.71 75.89 -1 -5 0 1884.71 75.49 -1 -5 0 1902.51 75.59 1 -5 0 1802.72 75.69 1 -5 0 1874.71 75.59 1 -5 0 1715.33 75.59 1 -5 0 1837.42 75.29 -1 -5 0 1852.91 75.49 1 -5 0 1807.12 75.39 1 5 0 1907.21 75.69 1 5 0 1884.61 75.59 -1 5 0 1735.93 75.59 -1 5 0 1802.52 75.69 1 5 0 1829.42 75.49 -1 5 0 1790.52 75.49 -1 5 0 1796.02 75.29 -1 5 0 1711.23 75.79 1 5 0 1875.81 75.89 -1 5 0 1778.02 75.59 1 5 0 1822.92 76.69 -1 5 0 1758.42 75.49 -1 5 0 1762.62 75.99 1 5 0 1894.41 75.59 -1 5 0 1805.82 75.69 1 5 0 1942.61 75.59 1 5 0 1885.91 75.59 2 -5 0 11.70 2.10 -2 -5 0 7.40 1.70 -2 -5 0 10.30 1.70 -2 -5 0 8.50 1.50 -2 -5 0 8.80 1.90 2 -5 0 7.20 1.50 -2 -5 0 7.60 1.20 2 -5 0 7.30 1.50 -2 -5 0 5.50 1.60 2 -5 0 10.40 1.80 2 -5 0 7.70 1.30 2 -5 0 6.10 1.80 -2 -5 0 6.10 1.70 2 5 0 6.40 1.40 2 5 0 9.00 1.80 2 5 0 4.50 1.60 -2 5 0 7.40 1.60 2 5 0 8.90 1.50 -2 5 0 7.40 1.30 -2 5 0 5.90 1.60 2 5 0 7.50 1.60 -2 5 0 6.00 1.50 2 5 0 6.80 1.60 -2 5 0 6.10 1.30 -2 5 0 9.40 1.80 -2 5 0 10.20 1.90 2 5 0 8.00 1.30 2 5 0 7.60 1.60 -2 5 0 9.50 1.90 3 -5 0 132.49 7.60 3 -5 0 124.79 6.80 -3 -5 0 143.89 6.80 3 -5 0 133.09 6.30 3 -5 0 129.79 7.90 -3 -5 0 149.69 7.90 3 -5 0 124.79 6.20 3 -5 0 134.19 8.00 -3 -5 0 136.19 7.30 -3 -5 0 134.19 7.40 -3 -5 0 139.29 7.30 -3 -5 0 154.68 7.20 3 -5 0 129.79 7.00 3 5 0 139.49 7.40 3 5 0 142.99 6.70 -3 5 0 122.99 6.60 -3 5 0 133.29 7.60 -3 5 0 135.49 8.00 -3 5 0 124.09 6.60 3 5 0 142.69 7.10 -3 5 0 130.39 6.90 3 5 0 130.99 7.20 3 5 0 149.09 7.40 3 5 0 129.29 7.30 -3 5 0 127.59 6.80 3 5 0 132.89 7.10 3 5 0 153.88 7.60 4 -5 0 99.79 7.20 -4 -5 0 104.59 6.80 4 -5 0 96.59 6.20 4 -5 0 100.79 5.30 4 -5 0 100.19 5.90 -4 -5 0 99.79 5.90 -4 -5 0 109.19 6.50 4 -5 0 101.19 6.80 4 5 0 99.39 6.30 4 5 0 100.79 6.50 -4 5 0 92.19 6.60 4 5 0 97.19 6.40 -4 5 0 101.19 7.30 4 5 0 107.19 6.30 -4 5 0 93.39 5.50 -5 -5 0 169.28 12.40 -5 -5 0 143.99 9.20 5 -5 0 150.78 10.00 5 -5 0 141.59 8.60 5 5 0 143.59 8.70 5 5 0 148.49 9.20 -5 5 0 152.48 10.10 5 5 0 145.09 8.90 6 -5 0 15.50 3.40 6 -5 0 20.90 4.30 6 -5 0 18.80 3.10 -6 -5 0 18.90 4.10 6 5 0 19.60 4.00 -6 5 0 16.10 4.10 -6 5 0 16.30 4.00 6 5 0 18.50 3.90 0 -6 0 899.71 35.60 0 -6 0 765.62 35.60 0 -6 0 855.91 36.00 0 -6 0 862.21 35.40 0 -6 0 869.91 36.60 0 -6 0 887.71 36.20 0 -6 0 866.51 36.00 0 6 0 870.41 35.20 0 6 0 859.51 35.30 0 6 0 793.22 36.00 0 6 0 908.71 36.20 0 6 0 828.22 36.10 0 6 0 817.02 37.80 0 6 0 880.51 35.30 0 6 0 841.42 36.00 0 6 0 855.51 36.50 0 6 0 842.32 35.30 0 6 0 874.41 36.20 1 -6 0 1.40 0.90 1 -6 0 1.50 1.10 -1 -6 0 0.30 1.30 -1 -6 0 1.60 1.10 1 -6 0 0.30 1.20 -1 -6 0 0.60 1.00 -1 -6 0 0.90 1.00 1 -6 0 1.60 1.10 1 -6 0 0.10 1.00 -1 -6 0 0.80 1.30 1 -6 0 0.40 0.90 -1 -6 0 0.90 1.00 -1 -6 0 0.40 1.00 1 -6 0 0.20 0.60 -1 6 0 1.30 1.10 -1 6 0 -1.70 0.80 1 6 0 -0.90 1.10 -1 6 0 1.90 1.10 -1 6 0 0.80 1.10 1 6 0 1.70 1.10 -1 6 0 1.70 1.00 1 6 0 1.50 0.90 1 6 0 3.00 1.20 -1 6 0 0.30 1.10 -1 6 0 0.70 1.00 1 6 0 -0.20 0.70 1 6 0 0.20 1.40 1 6 0 2.00 1.00 1 6 0 1.30 1.20 -1 6 0 -2.50 1.10 2 -6 0 30.00 3.00 -2 -6 0 31.40 3.00 2 -6 0 34.00 3.00 2 -6 0 37.30 2.60 -2 -6 0 31.70 3.00 -2 -6 0 34.20 3.00 2 -6 0 32.40 2.90 -2 -6 0 38.20 3.30 -2 -6 0 35.80 3.30 2 -6 0 38.20 3.20 2 6 0 30.00 3.20 2 6 0 36.50 3.10 -2 6 0 38.60 3.10 2 6 0 38.60 2.80 2 6 0 36.90 2.90 2 6 0 36.70 3.10 -2 6 0 31.20 3.10 -2 6 0 33.90 3.20 2 6 0 31.50 2.90 -2 6 0 34.10 2.60 2 6 0 33.30 2.20 -2 6 0 30.20 3.10 -2 6 0 36.30 2.60 3 -6 0 181.38 9.20 -3 -6 0 185.68 8.90 3 -6 0 173.08 9.90 -3 -6 0 189.78 9.50 -3 -6 0 191.08 9.40 3 -6 0 174.78 8.10 -3 -6 0 199.08 10.00 3 -6 0 180.88 9.30 3 -6 0 182.88 9.70 3 -6 0 168.18 8.00 3 -6 0 174.28 9.00 3 6 0 189.38 8.80 -3 6 0 160.38 8.90 3 6 0 185.68 8.80 3 6 0 195.38 9.60 -3 6 0 174.58 9.90 3 6 0 181.18 9.40 3 6 0 197.18 9.60 -3 6 0 184.58 9.70 -3 6 0 175.68 8.60 4 -6 0 156.28 9.00 4 -6 0 150.38 8.60 4 -6 0 146.69 9.40 4 -6 0 181.98 12.40 -4 -6 0 184.38 9.90 -4 -6 0 179.28 9.00 4 -6 0 159.48 7.90 4 6 0 163.98 9.20 -4 6 0 189.28 11.80 4 6 0 170.58 9.30 4 6 0 168.38 8.90 -4 6 0 158.08 9.50 4 6 0 178.18 9.50 -5 -6 0 9.10 3.00 5 -6 0 9.70 3.00 5 -6 0 13.10 3.00 5 -6 0 7.40 1.80 5 6 0 11.30 4.20 -5 6 0 5.40 3.00 -5 6 0 7.10 2.80 5 6 0 8.40 2.70 6 -6 0 7.60 3.20 -6 -6 0 4.90 2.80 6 -6 0 0.60 2.30 6 -6 0 6.80 2.20 -6 6 0 4.40 3.30 6 6 0 3.20 2.70 -6 6 0 6.50 3.20 6 6 0 6.60 2.90 0 -7 0 -0.30 1.50 0 -7 0 1.30 1.30 0 -7 0 0.40 0.90 0 -7 0 0.90 1.30 0 -7 0 4.10 1.30 0 7 0 2.50 1.30 0 7 0 4.80 1.50 0 7 0 0.60 0.90 0 7 0 1.60 0.80 -1 -7 0 341.07 15.60 1 -7 0 336.87 15.30 1 -7 0 336.07 15.40 -1 -7 0 345.97 15.20 1 -7 0 326.77 15.00 -1 -7 0 338.47 15.20 -1 -7 0 340.47 15.10 1 -7 0 343.77 14.40 -1 -7 0 341.37 15.30 1 -7 0 326.77 15.70 -1 -7 0 351.36 16.00 1 -7 0 338.77 14.50 -1 7 0 332.47 15.00 -1 7 0 310.37 15.30 1 7 0 340.67 15.30 1 7 0 355.86 15.40 -1 7 0 310.67 14.90 -1 7 0 322.77 15.30 1 7 0 343.17 15.30 2 -7 0 69.79 3.70 2 -7 0 75.19 4.90 -2 -7 0 79.39 4.90 -2 -7 0 78.49 5.30 -2 -7 0 75.59 5.30 2 -7 0 68.29 5.20 2 -7 0 72.09 5.00 2 -7 0 74.69 4.40 2 -7 0 79.49 3.80 2 7 0 80.29 5.00 2 7 0 81.19 5.00 2 7 0 82.59 4.70 -2 7 0 74.89 4.90 -2 7 0 74.99 5.00 -2 7 0 82.29 5.00 2 7 0 72.79 4.70 -3 -7 0 38.30 4.30 3 -7 0 40.20 3.50 3 -7 0 31.60 3.70 3 -7 0 32.00 2.30 3 -7 0 34.90 2.30 3 -7 0 35.00 3.30 -3 -7 0 39.00 3.70 3 -7 0 36.20 3.50 -3 -7 0 30.20 3.50 3 7 0 34.80 3.50 -3 7 0 36.40 3.90 3 7 0 38.10 3.20 -3 7 0 34.90 2.90 -3 7 0 40.70 4.00 3 7 0 40.20 3.60 3 7 0 35.80 3.50 4 -7 0 12.10 1.80 4 -7 0 10.50 2.40 -4 -7 0 10.00 2.80 4 -7 0 13.30 2.80 4 -7 0 18.00 3.40 -4 -7 0 9.00 2.50 -4 7 0 9.40 2.80 -4 7 0 7.20 2.70 4 7 0 15.00 3.00 4 7 0 14.10 2.90 5 -7 0 40.80 5.20 5 -7 0 38.90 4.40 -5 -7 0 35.40 4.80 5 -7 0 37.00 3.30 -5 7 0 37.30 5.30 -5 7 0 42.70 5.00 5 7 0 51.39 4.90 5 7 0 46.90 6.20 6 -7 0 15.90 3.80 -6 -7 0 28.30 4.90 6 -7 0 23.40 3.30 6 -7 0 22.00 4.60 6 7 0 22.40 4.30 -6 7 0 23.40 4.80 6 7 0 18.80 4.30 -6 7 0 22.50 4.70 0 -8 0 2387.26 94.79 0 -8 0 2315.67 95.29 0 -8 0 2220.98 95.99 0 -8 0 2424.66 95.59 0 8 0 2210.58 95.39 0 8 0 2369.66 95.39 0 8 0 2216.58 94.19 0 8 0 2248.58 94.09 0 8 0 2337.87 95.39 1 -8 0 33.10 3.30 1 -8 0 35.40 3.10 1 -8 0 35.50 3.70 -1 -8 0 39.20 4.10 -1 -8 0 37.50 3.90 1 -8 0 41.20 2.60 -1 -8 0 36.80 3.30 -1 -8 0 40.80 3.10 1 -8 0 35.60 2.60 -1 8 0 41.90 3.40 -1 8 0 37.60 3.00 1 8 0 37.80 3.70 1 8 0 39.90 3.30 -1 8 0 38.60 3.20 -1 8 0 42.30 3.50 1 8 0 34.80 3.30 1 8 0 47.40 3.60 -2 -8 0 42.40 4.20 2 -8 0 38.20 3.90 2 -8 0 44.40 3.70 2 -8 0 42.40 3.20 2 -8 0 38.20 2.50 2 -8 0 45.10 3.80 -2 -8 0 48.80 4.10 -2 -8 0 47.50 4.30 2 -8 0 43.50 2.50 -2 8 0 36.80 3.20 2 8 0 43.50 3.70 -2 8 0 35.40 3.50 -2 8 0 32.70 3.60 2 8 0 43.70 4.00 -2 8 0 44.30 3.70 2 8 0 40.00 3.40 3 -8 0 46.00 4.10 3 -8 0 42.90 2.80 3 -8 0 52.89 5.10 -3 -8 0 44.40 4.40 3 -8 0 49.50 4.10 -3 -8 0 43.30 4.50 -3 8 0 48.90 4.20 3 8 0 53.19 4.40 -3 8 0 49.50 4.60 -3 8 0 41.40 4.40 3 8 0 49.70 4.30 -3 8 0 40.80 3.30 3 8 0 55.49 3.90 4 -8 0 23.70 2.40 -4 -8 0 31.10 4.10 4 -8 0 30.70 3.60 4 -8 0 22.00 3.50 4 -8 0 22.90 3.90 -4 -8 0 19.40 3.50 -4 8 0 29.70 4.20 4 8 0 31.80 3.90 -4 8 0 27.70 4.30 4 8 0 33.30 4.00 5 -8 0 25.00 4.10 5 -8 0 28.00 4.70 5 -8 0 31.70 3.00 -5 -8 0 25.40 4.50 5 8 0 30.50 4.40 -5 8 0 31.60 5.10 -5 8 0 37.90 5.00 5 8 0 28.50 4.30 6 -8 0 2.30 2.70 6 -8 0 6.00 3.60 -6 -8 0 4.10 3.00 6 -8 0 0.70 1.80 -6 8 0 3.80 3.10 -6 8 0 4.20 3.80 6 8 0 4.20 3.00 6 8 0 0.70 2.60 0 -9 0 0.70 1.80 0 -9 0 1.60 1.20 0 -9 0 1.30 1.60 0 9 0 4.60 2.70 0 9 0 2.10 1.70 0 9 0 3.90 1.80 -1 -9 0 181.18 10.30 1 -9 0 199.68 9.90 -1 -9 0 194.28 9.70 -1 -9 0 185.68 9.90 1 -9 0 182.28 10.20 -1 -9 0 185.38 9.30 1 -9 0 181.18 8.60 1 -9 0 174.08 9.20 -1 9 0 169.18 8.90 -1 9 0 192.28 9.90 1 9 0 183.78 9.50 -1 9 0 177.28 9.60 1 9 0 195.28 9.80 -1 9 0 184.28 9.70 1 9 0 182.68 9.60 2 -9 0 14.50 2.40 -2 -9 0 19.50 3.30 2 -9 0 17.80 3.10 -2 -9 0 20.80 3.20 2 -9 0 15.80 2.80 -2 -9 0 17.40 2.80 2 -9 0 15.70 1.80 2 -9 0 20.40 2.90 -2 9 0 17.50 3.00 -2 9 0 19.50 2.90 -2 9 0 19.10 2.80 2 9 0 19.70 2.70 2 9 0 17.50 2.80 2 9 0 16.00 2.80 3 -9 0 9.30 2.40 3 -9 0 5.50 2.20 -3 -9 0 9.30 2.40 -3 -9 0 9.30 2.70 3 -9 0 6.50 1.30 -3 -9 0 10.80 2.80 3 -9 0 5.70 2.10 3 9 0 9.10 2.50 3 9 0 7.30 2.40 -3 9 0 8.90 2.50 3 9 0 7.30 2.00 -3 9 0 11.90 2.70 -3 9 0 9.20 2.40 4 -9 0 5.50 1.50 -4 -9 0 4.90 2.40 4 -9 0 8.20 2.60 -4 -9 0 7.40 2.70 4 -9 0 3.20 2.70 -4 9 0 10.50 3.20 4 9 0 6.60 2.50 4 9 0 6.50 2.50 -4 9 0 5.40 2.60 -4 9 0 7.20 3.00 -5 -9 0 8.20 3.10 5 -9 0 6.80 2.70 5 -9 0 3.20 2.70 5 -9 0 5.30 1.60 -5 9 0 6.50 3.20 -5 9 0 4.50 2.60 5 9 0 1.10 2.30 -5 9 0 7.70 3.20 5 9 0 5.90 2.80 6 -9 0 12.00 4.20 -6 -9 0 6.20 3.30 6 -9 0 14.30 6.20 6 -9 0 6.50 2.20 -6 9 0 7.40 3.60 -6 9 0 5.00 3.70 6 9 0 14.30 4.20 6 9 0 6.50 3.40 0 -10 0 63.59 4.90 0 -10 0 59.99 4.90 0 -10 0 62.19 4.20 0 -10 0 66.59 5.60 0 10 0 62.29 5.00 0 10 0 61.99 4.80 0 10 0 66.49 5.00 1 -10 0 310.07 13.90 -1 -10 0 318.77 15.30 -1 -10 0 308.97 15.00 -1 -10 0 308.07 15.80 -1 -10 0 301.67 14.50 1 -10 0 295.57 14.60 1 -10 0 313.97 15.20 1 -10 0 333.37 15.90 1 10 0 301.77 15.00 -1 10 0 296.67 15.00 -1 10 0 323.67 15.20 1 10 0 299.87 15.00 -1 10 0 314.67 15.20 1 10 0 307.67 14.90 2 -10 0 1.50 1.80 -2 -10 0 8.60 2.70 2 -10 0 8.10 1.40 2 -10 0 10.30 2.40 -2 -10 0 2.90 2.10 2 -10 0 6.40 2.40 -2 -10 0 9.20 2.20 2 10 0 6.00 2.00 -2 10 0 9.10 2.50 -2 10 0 3.10 1.90 2 10 0 8.20 2.20 -2 10 0 3.80 2.10 2 10 0 3.60 1.90 -3 -10 0 88.59 7.40 -3 -10 0 84.69 6.50 3 -10 0 80.19 6.00 -3 -10 0 76.59 5.80 3 -10 0 66.09 5.80 3 -10 0 75.29 5.80 3 -10 0 73.69 4.20 -3 10 0 76.69 6.10 3 10 0 82.79 5.50 -3 10 0 75.09 6.00 3 10 0 76.59 6.50 3 10 0 78.99 5.90 -3 10 0 69.19 5.70 4 -10 0 16.60 4.30 4 -10 0 15.90 2.20 4 -10 0 16.80 3.30 -4 -10 0 18.30 3.70 -4 -10 0 12.20 3.30 -4 10 0 15.10 3.50 -4 10 0 19.00 3.60 -4 10 0 16.40 3.60 4 10 0 19.90 4.40 4 10 0 17.40 3.50 5 -10 0 17.70 2.80 -5 -10 0 20.30 4.50 5 -10 0 28.80 4.70 5 10 0 26.30 4.70 5 10 0 21.50 4.20 -5 10 0 20.80 4.60 -5 10 0 23.50 4.70 -5 10 0 21.30 4.20 0 -11 0 1.10 1.70 0 -11 0 -1.10 1.80 0 -11 0 1.60 1.40 0 -11 0 -1.60 1.60 0 11 0 3.10 1.90 0 11 0 3.20 1.90 0 11 0 1.90 1.90 -1 -11 0 298.87 14.10 1 -11 0 307.27 15.50 1 -11 0 291.07 14.20 1 -11 0 299.67 13.50 -1 -11 0 294.07 14.80 -1 -11 0 296.57 15.60 1 -11 0 305.57 14.90 -1 -11 0 307.07 14.70 1 11 0 288.37 14.50 1 11 0 296.67 14.80 -1 11 0 276.17 14.60 -1 11 0 287.07 14.80 1 11 0 275.57 14.50 -1 11 0 283.77 14.60 2 -11 0 28.40 3.80 2 -11 0 30.10 4.20 -2 -11 0 28.30 4.10 2 -11 0 28.80 2.50 -2 -11 0 25.90 3.60 -2 -11 0 23.60 4.20 -2 11 0 22.60 3.40 -2 11 0 27.10 3.80 2 11 0 25.80 3.70 2 11 0 25.40 3.50 2 11 0 23.70 3.50 -2 11 0 18.50 3.40 3 -11 0 29.80 4.10 3 -11 0 33.50 4.20 3 -11 0 28.30 2.60 -3 -11 0 25.80 4.00 3 -11 0 25.80 4.10 -3 -11 0 37.20 4.70 -3 -11 0 33.10 4.70 -3 11 0 31.40 4.30 -3 11 0 28.00 5.00 3 11 0 28.40 4.10 -3 11 0 38.20 4.30 -3 11 0 31.40 4.40 3 11 0 39.20 4.40 3 11 0 25.40 3.60 -4 -11 0 5.80 2.90 -4 -11 0 10.20 3.30 4 -11 0 4.00 2.40 4 -11 0 7.80 2.90 4 -11 0 5.00 1.50 -4 11 0 5.90 2.90 4 11 0 9.50 3.10 4 11 0 7.20 2.80 -4 11 0 8.50 3.20 -4 11 0 3.70 2.40 5 -11 0 40.80 3.60 5 -11 0 35.10 5.20 -5 -11 0 50.49 6.10 -5 11 0 49.00 8.80 5 11 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3 4 66.59 5.40 4 3 -4 68.89 4.90 4 3 -4 66.09 4.80 -4 3 4 64.69 3.90 4 3 -4 69.79 4.20 4 3 -4 59.89 4.60 3 -3 -4 108.59 5.40 -3 -3 4 113.69 6.50 -3 -3 4 122.19 6.10 -3 -3 4 124.99 5.90 3 -3 -4 107.29 5.90 3 -3 -4 125.39 6.30 3 -3 -4 111.79 6.30 3 -3 -4 106.39 5.80 -3 -3 4 118.49 6.50 -3 -3 4 136.29 6.60 -3 -3 4 122.69 6.40 3 -3 -4 105.59 5.40 -3 -3 4 132.89 6.50 3 -3 -4 123.89 6.80 -3 3 4 114.79 7.00 -3 3 4 107.59 5.40 3 3 -4 134.09 6.60 3 3 -4 126.49 6.60 3 3 -4 116.59 6.30 3 3 -4 118.79 5.90 -3 3 4 106.99 5.40 -3 3 4 119.49 6.70 -3 3 4 116.69 6.10 3 3 -4 131.69 6.50 -3 3 4 111.09 5.40 3 3 -4 123.69 6.10 -3 3 4 111.29 5.50 -2 -3 4 9.40 1.40 -2 -3 4 7.90 1.60 -2 -3 4 8.60 1.50 -2 -3 4 7.70 1.50 2 -3 -4 7.30 2.20 2 -3 -4 8.00 1.20 2 -3 -4 9.10 1.70 -2 -3 4 11.40 1.80 -2 -3 4 8.90 1.50 2 -3 -4 10.50 1.70 2 -3 -4 9.20 1.60 -2 -3 4 7.50 1.40 -2 -3 4 10.10 1.50 -2 -3 4 9.30 1.50 2 3 -4 8.50 1.50 2 3 -4 9.30 1.50 -2 3 4 8.60 1.60 2 3 -4 11.90 1.70 -2 3 4 7.00 1.10 -2 3 4 11.50 1.80 2 3 -4 7.80 1.50 -2 3 4 6.80 1.60 2 3 -4 6.60 1.40 2 3 -4 9.80 1.70 -2 3 4 8.00 1.10 2 3 -4 9.00 1.50 1 -3 -4 410.16 18.90 -1 -3 4 440.76 18.90 1 -3 -4 414.36 19.00 1 -3 -4 476.35 19.00 1 -3 -4 457.95 19.00 -1 -3 4 428.16 18.90 -1 -3 4 472.05 18.90 -1 -3 4 460.05 18.50 1 -3 -4 407.36 19.50 -1 -3 4 462.15 19.10 -1 -3 4 451.45 18.50 -1 -3 4 439.96 18.90 -1 3 4 424.56 18.90 1 3 -4 464.55 19.00 -1 3 4 452.85 19.10 1 3 -4 467.65 19.00 1 3 -4 454.85 18.80 -1 3 4 436.16 18.50 -1 3 4 417.36 18.60 -1 3 4 421.86 18.90 -1 3 4 410.26 19.10 1 3 -4 463.55 19.20 1 3 -4 455.35 19.10 -1 3 4 422.56 18.90 1 3 -4 455.55 18.50 -1 3 4 438.26 19.10 1 3 -4 456.85 18.60 1 3 -4 458.05 18.80 0 -3 4 391.56 16.60 0 -3 4 380.86 16.10 0 -3 4 379.06 15.90 0 -3 -4 408.96 16.30 0 -3 -4 389.06 16.20 0 -3 4 381.96 15.90 0 -3 -4 383.26 16.30 0 -3 4 369.06 16.00 0 -3 4 367.26 16.30 0 -3 -4 393.96 16.20 0 -3 -4 369.16 16.50 0 -3 4 387.86 16.40 0 -3 -4 361.06 16.40 0 -3 -4 349.47 16.20 0 -3 4 420.86 16.50 0 -3 -4 360.06 16.10 0 -3 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-3 -4 74.09 4.10 -2 -3 -4 70.39 4.20 2 -3 4 65.89 4.80 -2 -3 -4 70.69 4.20 -2 -3 -4 66.59 3.70 -2 -3 -4 68.59 4.00 -2 3 -4 55.19 3.40 2 3 4 69.09 3.20 2 3 4 70.19 3.90 2 3 4 61.79 4.00 2 3 4 63.49 3.20 -2 3 -4 63.89 3.80 -2 3 -4 65.59 3.60 -2 3 -4 57.29 3.70 -2 3 -4 60.59 3.60 -2 3 -4 63.79 4.00 -2 3 -4 61.89 3.80 2 3 4 68.89 4.00 2 3 4 70.59 4.20 2 3 4 70.29 3.80 2 3 4 65.19 3.80 2 3 4 69.99 4.00 -2 3 -4 58.39 3.70 -3 -3 -4 79.99 5.10 3 -3 4 72.59 3.90 3 -3 4 64.49 4.30 3 -3 4 73.69 5.20 3 -3 4 66.09 3.70 3 -3 4 74.99 4.30 3 -3 4 79.09 5.00 -3 -3 -4 82.09 5.50 3 -3 4 69.49 3.70 -3 -3 -4 67.39 4.30 -3 -3 -4 74.49 4.40 -3 3 -4 72.39 3.90 3 3 4 73.49 4.60 3 3 4 75.09 4.80 -3 3 -4 78.29 4.10 3 3 4 78.69 5.40 3 3 4 70.19 4.40 3 3 4 71.39 4.60 -3 3 -4 65.29 4.40 3 3 4 63.79 4.20 -3 3 -4 75.29 4.20 -3 3 -4 77.49 4.40 -3 3 -4 75.49 4.50 -4 -3 -4 28.10 3.20 -4 -3 -4 21.70 2.50 4 -3 4 24.70 3.40 4 -3 4 28.80 3.70 4 -3 4 29.90 3.00 4 -3 4 23.90 2.40 4 3 4 25.10 3.40 -4 3 -4 23.10 2.40 -4 3 -4 26.40 3.50 4 3 4 25.10 2.90 -4 3 -4 27.20 3.80 4 3 4 31.00 3.60 4 3 4 30.10 3.30 5 -3 4 7.10 1.90 -5 -3 -4 6.40 2.50 5 -3 4 1.30 2.10 5 -3 4 5.70 2.10 -5 -3 -4 4.60 2.30 5 -3 4 6.60 2.60 5 3 4 1.30 1.80 5 3 4 7.30 2.20 5 3 4 2.50 2.20 5 3 4 6.40 2.40 -5 3 -4 6.30 2.30 -5 3 -4 -0.30 2.00 -6 -3 -4 0.40 2.20 6 -3 4 1.40 1.90 6 -3 4 3.20 2.60 6 -3 4 -0.40 2.00 6 -3 4 0.30 2.40 -6 -3 -4 1.20 2.50 -6 3 -4 1.70 2.60 6 3 4 0.00 2.20 6 3 4 -2.30 1.80 6 3 4 -0.70 2.10 6 3 4 2.80 2.40 -7 -3 -4 22.90 5.10 -7 -3 -4 18.10 4.40 7 -3 4 23.30 5.40 7 -3 4 18.20 3.60 7 -3 4 11.90 4.20 7 3 4 9.20 4.00 7 3 4 15.20 4.30 -7 3 -4 20.90 5.20 7 -4 -4 3.60 3.80 7 -4 -4 1.70 2.90 7 -4 -4 3.50 2.40 7 4 -4 2.40 2.80 -7 4 4 1.90 3.00 -7 4 4 4.30 3.30 7 4 -4 7.10 3.50 6 -4 -4 59.09 6.00 6 -4 -4 40.20 4.90 -6 -4 4 57.99 5.60 6 -4 -4 61.49 4.90 6 4 -4 50.69 5.50 -6 4 4 65.19 6.70 -6 4 4 48.00 5.90 6 4 -4 56.29 5.60 -5 -4 4 173.88 10.10 5 -4 -4 178.48 9.30 -5 -4 4 190.58 10.40 5 -4 -4 161.28 9.80 5 -4 -4 166.58 10.40 5 4 -4 171.28 10.00 -5 4 4 188.08 10.60 -5 4 4 196.68 11.40 5 4 -4 172.48 10.00 5 4 -4 194.68 10.20 -4 -4 4 85.89 5.70 -4 -4 4 75.39 4.50 4 -4 -4 73.59 4.70 4 -4 -4 77.89 5.40 -4 -4 4 77.29 5.40 4 -4 -4 72.39 5.70 -4 -4 4 79.09 6.60 4 -4 -4 75.29 5.20 4 4 -4 94.69 5.00 4 4 -4 83.49 5.50 4 4 -4 85.49 5.50 -4 4 4 85.29 5.80 4 4 -4 84.89 5.60 -4 4 4 76.59 6.10 -3 -4 4 152.18 7.30 3 -4 -4 136.29 6.80 -3 -4 4 148.89 7.60 -3 -4 4 144.29 7.50 3 -4 -4 140.19 8.20 -3 -4 4 147.59 7.20 3 -4 -4 139.79 6.90 3 -4 -4 153.18 8.80 3 -4 -4 134.29 7.20 -3 -4 4 140.39 7.80 -3 -4 4 136.29 7.60 -3 -4 4 159.48 7.50 3 -4 -4 147.89 7.40 -3 4 4 136.09 6.40 -3 4 4 136.79 6.40 3 4 -4 140.39 7.10 3 4 -4 142.39 7.50 -3 4 4 142.89 8.50 -3 4 4 134.49 6.70 3 4 -4 151.08 7.70 3 4 -4 153.38 8.40 -3 4 4 139.69 8.10 3 4 -4 143.69 7.20 3 4 -4 145.39 7.50 2 -4 -4 41.20 2.90 -2 -4 4 29.30 2.40 -2 -4 4 31.90 2.80 -2 -4 4 31.60 2.70 2 -4 -4 37.30 2.30 2 -4 -4 38.70 2.40 -2 -4 4 33.40 2.70 2 -4 -4 29.60 2.50 -2 -4 4 35.70 3.00 -2 -4 4 28.20 2.30 -2 -4 4 33.60 2.60 2 -4 -4 29.50 2.60 -2 -4 4 30.10 2.20 -2 -4 4 35.00 2.80 2 -4 -4 40.80 3.20 2 4 -4 34.80 2.70 -2 4 4 30.60 1.90 2 4 -4 32.90 2.80 -2 4 4 27.00 2.60 2 4 -4 31.20 2.70 2 4 -4 32.70 2.90 2 4 -4 37.10 3.40 -2 4 4 34.80 2.60 -2 4 4 36.30 3.00 -2 4 4 30.30 2.60 2 4 -4 38.20 2.60 2 4 -4 34.90 2.60 -2 4 4 32.60 3.10 -2 4 4 43.90 3.20 1 -4 -4 27.10 2.40 1 -4 -4 31.40 2.30 -1 -4 4 28.50 2.30 -1 -4 4 33.60 2.30 1 -4 -4 30.20 2.50 -1 -4 4 28.00 2.50 -1 -4 4 30.40 2.20 -1 -4 4 31.60 1.90 1 -4 -4 29.60 2.00 -1 -4 4 26.10 2.40 1 -4 -4 26.50 2.30 1 -4 -4 24.90 1.70 -1 4 4 23.40 2.30 -1 4 4 21.40 2.20 1 4 -4 33.80 2.20 1 4 -4 34.10 2.60 1 4 -4 28.90 2.10 -1 4 4 26.80 2.40 -1 4 4 33.30 2.40 1 4 -4 32.10 2.30 1 4 -4 25.90 2.20 1 4 -4 30.80 2.30 1 4 -4 28.00 1.90 1 4 -4 33.00 2.50 -1 4 4 29.30 2.40 -1 4 4 23.40 1.80 -1 4 4 29.50 1.70 -1 4 4 28.10 2.40 -1 4 4 28.50 2.50 0 -4 -4 150.68 7.00 0 -4 4 148.59 6.70 0 -4 -4 158.18 7.10 0 -4 -4 160.68 7.00 0 -4 -4 142.29 6.90 0 -4 4 152.18 7.20 0 -4 4 148.99 6.70 0 -4 -4 146.89 7.00 0 -4 4 147.59 6.60 0 -4 -4 154.38 7.10 0 -4 4 144.49 6.60 0 -4 -4 145.59 7.40 0 -4 4 147.39 7.40 0 -4 4 152.98 7.30 0 -4 4 143.59 6.90 0 4 -4 147.99 6.70 0 4 4 158.08 7.30 0 4 -4 136.39 6.90 0 4 -4 149.09 7.20 0 4 4 160.48 7.10 0 4 4 158.78 6.90 0 4 4 147.59 6.90 0 4 4 168.28 7.20 0 4 4 143.69 6.90 0 4 4 147.79 7.10 0 4 -4 148.59 6.70 0 4 -4 154.18 7.50 0 4 -4 147.39 7.10 0 4 -4 141.99 6.60 0 4 4 158.28 7.50 1 -4 4 262.07 11.20 1 -4 4 253.57 11.20 -1 -4 -4 255.27 11.00 -1 -4 -4 256.67 11.20 -1 -4 -4 259.57 11.30 -1 -4 -4 249.78 11.90 -1 -4 -4 246.38 11.60 -1 -4 -4 245.78 11.40 1 -4 4 255.07 11.50 1 -4 4 259.37 11.40 1 -4 4 244.98 11.30 -1 -4 -4 234.78 11.00 -1 -4 -4 251.87 11.20 1 -4 4 254.97 11.10 1 4 4 251.97 11.60 1 4 4 248.58 11.20 1 4 4 263.97 11.10 -1 4 -4 253.07 11.20 1 4 4 247.88 11.10 1 4 4 257.47 11.20 1 4 4 242.38 11.30 -1 4 -4 255.97 11.30 1 4 4 248.38 11.40 -1 4 -4 239.28 11.00 -1 4 -4 237.28 11.20 -1 4 -4 244.98 11.50 -1 4 -4 240.28 11.50 1 4 4 248.78 11.50 -1 4 -4 247.28 11.20 -1 4 -4 230.18 11.60 -1 4 -4 257.37 11.10 -1 4 -4 259.07 11.10 2 -4 4 10.10 1.80 2 -4 4 8.20 1.50 -2 -4 -4 11.00 1.70 -2 -4 -4 7.10 1.60 -2 -4 -4 10.70 1.80 2 -4 4 7.10 1.80 -2 -4 -4 13.80 2.20 -2 -4 -4 11.10 1.30 2 -4 4 10.10 1.70 -2 -4 -4 11.40 1.80 -2 -4 -4 6.30 1.40 2 -4 4 9.00 1.50 2 -4 4 8.60 1.50 -2 4 -4 7.80 1.50 2 4 4 7.60 1.50 -2 4 -4 11.50 1.70 2 4 4 10.10 1.90 -2 4 -4 7.10 1.40 2 4 4 7.10 1.50 -2 4 -4 8.90 1.40 -2 4 -4 8.10 1.60 2 4 4 11.50 2.00 2 4 4 10.30 1.60 2 4 4 13.10 1.90 -2 4 -4 7.80 2.30 2 4 4 8.80 1.30 2 4 4 8.60 1.30 -2 4 -4 8.30 1.50 -2 4 -4 7.00 1.60 2 4 4 9.90 1.70 -3 -4 -4 105.29 6.20 3 -4 4 96.29 5.30 3 -4 4 89.79 4.40 -3 -4 -4 96.49 5.50 3 -4 4 91.29 6.40 3 -4 4 87.39 5.00 -3 -4 -4 102.39 5.60 3 -4 4 94.39 6.20 3 -4 4 88.49 5.10 -3 4 -4 78.79 5.80 3 4 4 105.49 5.80 3 4 4 94.49 5.50 3 4 4 98.59 6.00 -3 4 -4 87.19 6.40 3 4 4 102.09 5.80 -3 4 -4 93.59 5.40 -3 4 -4 96.29 5.20 3 4 4 93.69 5.70 -3 4 -4 91.99 5.30 3 4 4 98.49 4.60 3 4 4 102.39 5.60 -4 -4 -4 295.87 15.20 4 -4 4 310.87 14.40 4 -4 4 315.57 15.80 4 -4 4 306.17 15.10 -4 -4 -4 320.07 14.30 4 -4 4 298.17 13.60 4 4 4 328.87 15.00 4 4 4 306.97 14.50 -4 4 -4 276.87 14.50 4 4 4 311.57 15.10 4 4 4 292.27 15.00 -4 4 -4 313.87 15.90 5 -4 4 217.98 11.90 5 -4 4 262.07 14.00 -5 -4 -4 230.48 12.90 5 -4 4 234.48 13.00 5 -4 4 246.78 13.50 -5 -4 -4 218.28 15.60 -5 4 -4 241.98 13.80 5 4 4 236.68 12.30 5 4 4 231.68 13.00 -5 4 -4 235.78 12.20 5 4 4 256.97 12.80 6 -4 4 18.30 4.40 -6 -4 -4 23.20 4.50 6 -4 4 18.40 3.60 -6 -4 -4 20.60 4.10 6 -4 4 22.70 4.60 6 4 4 27.20 4.60 6 4 4 24.10 4.20 6 4 4 12.50 3.00 6 4 4 14.90 3.80 -6 4 -4 35.20 5.40 6 -5 -4 16.40 3.80 6 -5 -4 15.10 2.90 -6 -5 4 19.60 3.90 6 -5 -4 11.20 3.10 6 5 -4 13.40 3.40 6 5 -4 14.70 3.60 -6 5 4 12.70 3.70 -6 5 4 21.10 4.60 -5 -5 4 3.90 2.20 5 -5 -4 1.00 1.80 5 -5 -4 0.60 2.30 5 5 -4 3.90 2.10 5 5 -4 2.60 2.80 -5 5 4 -1.40 2.10 4 -5 -4 55.09 3.80 -4 -5 4 43.50 5.20 -4 -5 4 53.89 3.90 4 -5 -4 54.49 4.20 -4 -5 4 54.19 4.60 4 -5 -4 46.10 4.20 -4 -5 4 53.39 4.20 4 -5 -4 45.70 4.60 4 5 -4 52.09 4.50 4 5 -4 58.29 4.00 4 5 -4 62.79 4.60 -4 5 4 53.89 4.80 4 5 -4 52.59 4.30 -4 5 4 57.89 5.20 3 -5 -4 112.99 6.30 -3 -5 4 118.49 6.80 -3 -5 4 120.79 6.00 -3 -5 4 111.09 6.40 3 -5 -4 108.79 5.90 -3 -5 4 115.39 6.30 -3 -5 4 108.09 6.80 3 -5 -4 117.69 6.50 3 -5 -4 109.69 5.70 -3 -5 4 114.09 6.60 3 -5 -4 111.69 6.80 3 5 -4 116.29 6.50 3 5 -4 121.49 6.50 -3 5 4 98.29 5.10 -3 5 4 103.79 5.10 3 5 -4 120.69 6.10 3 5 -4 108.39 6.20 -3 5 4 113.39 7.00 -3 5 4 101.59 5.70 3 5 -4 119.19 6.30 -3 5 4 117.39 6.80 -2 -5 4 1954.20 79.09 -2 -5 4 1933.51 79.39 -2 -5 4 1974.60 79.59 2 -5 -4 1810.82 79.19 -2 -5 4 2007.00 78.49 2 -5 -4 1833.42 78.69 2 -5 -4 1918.51 79.39 2 -5 -4 1906.51 78.29 -2 -5 4 1926.01 79.29 -2 -5 4 1959.30 79.29 -2 -5 4 1849.42 78.49 -2 -5 4 1971.00 79.79 2 -5 -4 1892.81 78.69 2 -5 -4 1923.01 79.39 -2 5 4 1824.42 78.29 2 5 -4 1968.50 79.29 2 5 -4 1931.51 79.19 -2 5 4 2005.20 79.79 2 5 -4 1954.20 79.19 2 5 -4 2007.80 79.29 -2 5 4 1828.62 79.69 -2 5 4 1793.42 79.09 2 5 -4 1965.50 79.49 2 5 -4 1959.70 79.49 -2 5 4 1782.42 78.19 2 5 -4 1980.70 79.09 1 -5 -4 103.99 5.10 -1 -5 4 106.29 5.30 1 -5 -4 97.09 5.60 -1 -5 4 104.99 5.50 1 -5 -4 97.49 5.70 -1 -5 4 108.69 5.10 -1 -5 4 105.89 5.80 -1 -5 4 108.59 5.90 -1 -5 4 101.39 5.50 1 -5 -4 95.69 4.90 1 -5 -4 107.29 5.60 -1 -5 4 107.89 5.60 1 -5 -4 110.09 5.60 1 5 -4 110.29 5.20 -1 5 4 105.39 5.80 -1 5 4 101.79 5.70 1 5 -4 109.39 5.90 1 5 -4 99.09 5.50 1 5 -4 106.09 5.10 -1 5 4 104.69 5.60 1 5 -4 102.29 5.50 -1 5 4 98.09 5.50 1 5 -4 108.49 5.60 -1 5 4 105.19 5.50 -1 5 4 99.99 4.90 1 5 -4 102.29 5.10 -1 5 4 102.39 4.90 1 5 -4 105.19 5.80 -1 5 4 98.49 4.80 0 -5 -4 257.87 12.30 0 -5 4 264.37 11.50 0 -5 -4 280.77 11.90 0 -5 4 265.97 12.10 0 -5 -4 249.68 12.00 0 -5 4 260.97 11.40 0 -5 -4 289.17 12.50 0 -5 -4 252.37 11.60 0 -5 -4 276.77 11.70 0 -5 -4 269.47 12.00 0 -5 4 267.57 11.80 0 -5 -4 261.67 11.80 0 -5 4 252.47 11.30 0 -5 4 262.87 12.00 0 -5 4 257.97 12.00 0 -5 4 266.27 11.40 0 -5 4 265.37 12.40 0 5 -4 261.97 12.00 0 5 -4 272.87 12.30 0 5 -4 269.77 11.50 0 5 4 240.58 13.20 0 5 -4 254.77 11.90 0 5 -4 257.07 11.80 0 5 -4 251.67 11.80 0 5 4 277.17 12.20 0 5 4 264.67 12.30 0 5 -4 250.77 11.20 0 5 -4 259.37 12.30 0 5 4 261.07 11.80 0 5 4 247.28 11.60 0 5 4 288.17 12.00 0 5 4 264.37 11.50 0 5 4 266.77 11.70 0 5 -4 274.27 11.60 -1 -5 -4 7.70 1.40 -1 -5 -4 5.70 1.40 -1 -5 -4 9.70 1.50 1 -5 4 6.50 1.40 1 -5 4 6.70 1.40 1 -5 4 4.80 1.30 -1 -5 -4 7.30 1.40 -1 -5 -4 6.20 1.40 1 -5 4 3.60 1.20 1 -5 4 5.80 1.30 1 -5 4 5.30 1.40 -1 -5 -4 8.40 1.30 -1 -5 -4 7.30 1.60 -1 -5 -4 7.20 1.60 1 5 4 7.50 1.60 -1 5 -4 6.60 1.50 -1 5 -4 5.10 1.20 1 5 4 3.70 1.40 -1 5 -4 10.10 1.70 -1 5 -4 4.50 1.50 -1 5 -4 9.00 1.50 1 5 4 5.20 1.30 -1 5 -4 6.40 1.70 -1 5 -4 6.30 1.30 1 5 4 5.60 1.30 1 5 4 6.70 1.50 1 5 4 8.40 1.50 -1 5 -4 5.20 1.40 1 5 4 6.60 1.30 -2 -5 -4 17.70 2.20 2 -5 4 22.10 2.20 -2 -5 -4 19.90 2.30 2 -5 4 25.20 2.30 2 -5 4 20.20 2.40 -2 -5 -4 24.90 2.00 -2 -5 -4 25.40 2.60 2 -5 4 18.80 2.50 2 -5 4 19.40 2.40 -2 -5 -4 17.10 2.40 -2 -5 -4 22.00 2.50 2 -5 4 22.50 2.30 -2 5 -4 24.20 2.20 -2 5 -4 23.40 2.40 2 5 4 25.20 2.40 -2 5 -4 20.60 2.10 2 5 4 21.70 1.90 -2 5 -4 22.40 2.20 2 5 4 22.60 2.60 2 5 4 21.80 2.00 -2 5 -4 21.00 2.30 -2 5 -4 22.80 2.30 2 5 4 20.90 2.30 -2 5 -4 23.10 2.20 -2 5 -4 22.20 2.40 -2 5 -4 24.50 2.30 2 5 4 24.40 2.50 2 5 4 21.20 2.50 -2 5 -4 17.30 2.30 2 5 4 21.50 2.20 3 -5 4 23.20 2.40 -3 -5 -4 24.50 2.90 -3 -5 -4 26.40 2.80 3 -5 4 21.50 2.40 3 -5 4 18.70 3.10 -3 -5 -4 20.70 2.50 3 -5 4 21.60 2.80 3 -5 4 20.70 2.50 3 5 4 23.50 1.90 3 5 4 21.30 2.80 3 5 4 26.10 2.70 3 5 4 25.40 3.00 -3 5 -4 13.30 2.40 -3 5 -4 23.70 2.40 -3 5 -4 23.70 2.50 -3 5 -4 17.10 3.00 -3 5 -4 19.60 2.30 4 -5 4 302.77 13.60 -4 -5 -4 324.07 15.60 4 -5 4 309.27 16.40 4 -5 4 301.57 14.60 4 -5 4 293.57 15.20 -4 -5 -4 319.57 14.70 -4 5 -4 298.27 16.20 4 5 4 326.67 15.20 -4 5 -4 297.87 14.60 4 5 4 307.17 14.80 4 5 4 317.47 15.10 4 5 4 301.97 15.30 5 -5 4 56.49 6.10 5 -5 4 55.19 4.10 5 -5 4 60.19 5.00 -5 -5 -4 64.99 6.20 5 -5 4 58.19 6.30 -5 -5 -4 69.79 7.60 5 5 4 62.49 5.90 -5 5 -4 53.19 6.10 5 5 4 64.89 5.70 -5 5 -4 60.09 5.00 5 5 4 67.39 5.60 5 5 4 68.19 5.30 -6 -5 -4 29.50 4.80 6 -5 4 26.80 4.90 6 -5 4 26.40 5.20 6 -5 4 32.00 3.60 6 5 4 27.20 4.80 6 5 4 30.60 4.30 6 5 4 28.50 5.00 -6 5 -4 36.30 5.80 -6 -6 4 11.90 3.40 6 -6 -4 10.10 2.70 6 -6 -4 11.90 3.10 6 -6 -4 9.50 3.40 6 6 -4 6.50 3.00 -6 6 4 13.10 3.70 6 6 -4 13.80 3.60 -6 6 4 18.70 4.60 5 -6 -4 158.58 8.40 5 -6 -4 160.88 9.40 5 -6 -4 178.78 9.80 -5 -6 4 166.98 10.00 5 -6 -4 158.58 10.00 -5 6 4 159.28 10.00 -5 6 4 147.49 10.10 5 6 -4 149.88 9.30 5 6 -4 144.19 9.20 4 -6 -4 11.70 2.60 4 -6 -4 11.90 2.40 4 -6 -4 16.00 3.30 4 -6 -4 14.40 2.30 -4 -6 4 11.70 2.60 -4 -6 4 9.60 2.20 4 6 -4 11.70 2.70 4 6 -4 13.20 2.60 4 6 -4 11.00 2.10 -4 6 4 8.80 3.10 -4 6 4 10.40 2.80 3 -6 -4 204.48 10.20 3 -6 -4 211.68 10.10 -3 -6 4 205.78 10.60 3 -6 -4 206.38 9.20 3 -6 -4 188.98 9.70 -3 -6 4 216.68 10.30 3 -6 -4 215.98 10.70 -3 -6 4 202.58 10.10 -3 6 4 185.78 9.60 -3 6 4 187.98 10.60 -3 6 4 173.38 8.70 3 6 -4 198.38 9.70 3 6 -4 199.08 10.00 3 6 -4 192.68 10.10 3 6 -4 195.58 9.80 -3 6 4 204.58 10.60 -2 -6 4 63.29 4.00 -2 -6 4 66.09 4.50 2 -6 -4 63.89 4.10 -2 -6 4 60.99 4.10 2 -6 -4 54.89 3.00 2 -6 -4 51.89 3.20 2 -6 -4 52.89 3.50 -2 -6 4 60.49 4.30 2 -6 -4 51.09 4.00 2 -6 -4 56.49 4.30 -2 6 4 49.40 3.90 2 6 -4 61.19 4.10 2 6 -4 59.69 3.90 -2 6 4 62.69 4.40 -2 6 4 58.59 4.20 -2 6 4 52.69 2.90 2 6 -4 59.59 3.70 2 6 -4 55.89 3.70 -2 6 4 51.89 3.00 1 -6 -4 143.49 7.30 -1 -6 4 171.18 8.60 1 -6 -4 160.88 8.10 -1 -6 4 165.78 7.60 -1 -6 4 160.58 7.70 1 -6 -4 164.58 8.00 1 -6 -4 154.48 7.40 1 -6 -4 151.68 8.20 -1 -6 4 158.28 7.80 -1 -6 4 169.58 8.30 1 -6 -4 159.08 7.50 -1 -6 4 172.98 8.50 -1 6 4 165.58 8.00 -1 6 4 168.08 8.30 1 6 -4 167.18 8.60 1 6 -4 166.08 7.50 1 6 -4 161.18 7.50 -1 6 4 144.69 7.30 -1 6 4 153.78 7.10 1 6 -4 153.18 7.90 1 6 -4 159.88 8.00 -1 6 4 152.68 8.20 -1 6 4 145.39 7.90 0 -6 -4 362.06 16.40 0 -6 4 353.06 16.00 0 -6 -4 372.86 16.00 0 -6 4 341.87 15.50 0 -6 4 357.86 15.30 0 -6 -4 369.86 15.60 0 -6 4 358.26 16.40 0 -6 -4 334.67 15.50 0 -6 -4 363.46 15.90 0 -6 -4 355.66 15.80 0 -6 4 373.36 16.20 0 -6 -4 345.17 16.00 0 -6 -4 367.26 15.70 0 -6 4 354.06 15.80 0 6 4 378.96 16.20 0 6 -4 329.67 15.00 0 6 4 331.47 15.70 0 6 4 355.56 15.90 0 6 -4 356.86 16.00 0 6 4 362.06 15.90 0 6 -4 343.97 15.90 0 6 -4 357.06 16.00 0 6 -4 375.16 15.90 0 6 -4 352.76 16.40 0 6 4 371.16 15.60 0 6 4 381.26 16.00 0 6 -4 353.66 15.50 0 6 4 349.77 15.40 0 6 -4 363.86 15.60 0 6 4 349.96 16.30 0 6 4 356.26 15.50 1 -6 4 115.79 6.30 -1 -6 -4 123.69 6.30 1 -6 4 121.39 6.30 -1 -6 -4 113.29 6.10 -1 -6 -4 116.59 6.10 -1 -6 -4 127.99 6.40 -1 -6 -4 126.99 6.80 1 -6 4 112.99 6.60 -1 -6 -4 122.49 6.50 -1 -6 -4 114.29 5.70 1 -6 4 112.29 6.10 -1 6 -4 118.09 6.30 -1 6 -4 121.09 7.90 -1 6 -4 112.59 6.70 -1 6 -4 118.19 6.10 -1 6 -4 111.19 6.70 -1 6 -4 115.89 6.30 1 6 4 122.09 6.20 1 6 4 120.99 6.50 1 6 4 118.19 6.10 1 6 4 116.49 5.70 1 6 4 127.49 6.60 -1 6 -4 109.99 6.10 1 6 4 126.49 6.20 1 6 4 122.59 6.10 -1 6 -4 118.89 6.20 -1 6 -4 106.89 6.00 -2 -6 -4 13.10 1.70 2 -6 4 8.70 1.80 -2 -6 -4 17.30 3.70 2 -6 4 13.70 2.40 -2 -6 -4 12.30 2.10 2 -6 4 13.30 2.00 2 -6 4 10.80 2.00 2 -6 4 9.60 2.00 2 -6 4 10.60 2.10 -2 -6 -4 12.40 2.10 -2 -6 -4 11.30 2.10 -2 6 -4 10.60 1.90 -2 6 -4 10.30 1.80 -2 6 -4 11.20 2.10 2 6 4 12.30 1.80 -2 6 -4 11.60 2.00 2 6 4 12.50 3.00 2 6 4 10.00 2.10 2 6 4 13.10 1.90 -2 6 -4 13.40 2.20 -2 6 -4 9.20 1.80 2 6 4 10.00 2.00 -2 6 -4 9.60 2.20 2 6 4 12.50 1.80 2 6 4 13.00 2.00 3 -6 4 170.18 9.20 3 -6 4 175.18 10.00 3 -6 4 180.98 9.10 3 -6 4 175.28 9.10 3 -6 4 178.58 9.60 -3 -6 -4 189.58 9.60 -3 -6 -4 175.28 9.30 -3 -6 -4 183.88 10.00 -3 6 -4 166.98 9.90 3 6 4 192.98 8.60 3 6 4 189.08 9.40 3 6 4 199.18 9.30 3 6 4 190.18 9.90 -3 6 -4 181.28 9.10 -3 6 -4 178.08 9.20 3 6 4 189.38 9.60 -3 6 -4 170.08 9.50 -3 6 -4 168.98 9.10 4 -6 4 94.79 6.30 -4 -6 -4 115.29 7.40 4 -6 4 108.49 7.60 4 -6 4 103.29 7.10 4 -6 4 100.89 5.20 -4 -6 -4 117.19 6.80 -4 6 -4 97.59 6.80 4 6 4 100.69 6.50 -4 6 -4 111.39 7.10 4 6 4 102.19 7.00 -4 6 -4 100.69 7.60 -4 6 -4 102.19 6.30 4 6 4 103.79 6.70 5 -6 4 181.28 11.20 5 -6 4 167.48 10.50 -5 -6 -4 173.48 10.70 5 -6 4 167.58 9.60 -5 6 -4 178.08 10.60 5 6 4 170.28 10.10 5 6 4 174.18 10.40 -5 6 -4 170.18 11.20 5 6 4 164.98 9.80 6 -6 4 8.50 2.20 -6 -6 -4 7.10 3.30 6 -6 4 3.70 3.10 6 -6 4 5.50 3.00 -6 6 -4 7.90 3.70 6 6 4 6.20 3.20 -6 6 -4 5.70 3.00 6 6 4 2.80 2.50 6 -7 -4 20.50 4.60 6 -7 -4 10.90 3.10 -6 -7 4 19.20 4.20 6 -7 -4 12.40 2.70 6 7 -4 13.50 3.80 -6 7 4 13.90 4.10 6 7 -4 17.50 3.90 -6 7 4 13.40 4.00 5 -7 -4 5.40 2.70 5 -7 -4 1.20 2.00 5 -7 -4 8.00 2.70 5 -7 -4 4.80 1.80 -5 -7 4 9.20 3.10 5 7 -4 5.50 2.60 5 7 -4 7.50 2.80 -5 7 4 5.90 2.80 -5 7 4 2.80 2.40 4 -7 -4 83.69 5.70 -4 -7 4 82.19 5.70 4 -7 -4 78.89 4.80 4 -7 -4 92.19 6.60 -4 -7 4 78.69 6.30 4 -7 -4 83.19 5.90 4 7 -4 81.99 5.30 -4 7 4 74.79 6.20 4 7 -4 79.29 5.90 -4 7 4 77.59 6.50 4 7 -4 79.09 5.60 3 -7 -4 50.89 3.30 3 -7 -4 57.19 4.30 -3 -7 4 39.00 6.20 3 -7 -4 55.09 4.20 3 -7 -4 42.30 3.80 -3 -7 4 45.50 4.10 -3 -7 4 50.39 4.50 3 7 -4 44.50 3.80 -3 7 4 55.09 4.70 3 7 -4 49.70 3.90 3 7 -4 43.00 4.00 -3 7 4 45.50 4.40 2 -7 -4 13.70 2.30 2 -7 -4 11.00 2.20 -2 -7 4 16.00 2.70 2 -7 -4 16.70 1.80 -2 -7 4 16.00 2.20 2 -7 -4 15.20 2.40 2 -7 -4 14.40 1.60 -2 -7 4 18.70 2.70 -2 -7 4 17.60 2.40 2 7 -4 20.50 2.30 -2 7 4 16.50 2.50 2 7 -4 16.30 2.50 -2 7 4 13.40 2.40 2 7 -4 19.20 4.20 2 7 -4 11.90 2.10 -2 7 4 17.30 2.80 -1 -7 4 773.42 32.10 1 -7 -4 788.82 32.70 1 -7 -4 749.53 32.70 -1 -7 4 747.33 32.30 1 -7 -4 754.42 32.00 -1 -7 4 777.62 32.30 -1 -7 4 800.92 33.30 1 -7 -4 750.12 33.00 1 -7 -4 723.73 31.90 -1 -7 4 786.52 32.90 1 -7 -4 746.93 32.00 -1 7 4 719.23 31.40 1 7 -4 762.12 32.10 -1 7 4 713.53 31.90 1 7 -4 782.22 32.70 -1 7 4 687.63 32.60 -1 7 4 802.42 33.00 -1 7 4 760.62 32.40 1 7 -4 802.62 32.70 1 7 -4 768.52 31.80 0 -7 4 24.00 2.90 0 -7 -4 23.70 2.60 0 -7 -4 26.80 2.30 0 -7 4 28.80 2.70 0 -7 4 28.20 2.80 0 -7 4 20.90 2.10 0 -7 4 21.80 2.30 0 -7 4 27.60 2.10 0 -7 -4 18.00 2.30 0 -7 -4 26.60 2.40 0 -7 -4 19.80 3.00 0 7 4 19.40 2.40 0 7 -4 25.50 2.30 0 7 4 20.90 2.40 0 7 -4 26.30 2.50 0 7 4 18.80 3.10 0 7 -4 28.00 2.70 0 7 -4 26.30 2.40 0 7 4 26.60 2.70 0 7 4 22.20 2.10 1 -7 4 41.60 3.30 1 -7 4 35.40 2.10 -1 -7 -4 38.60 3.10 1 -7 4 36.10 3.50 -1 -7 -4 38.30 3.20 -1 -7 -4 39.80 3.10 1 -7 4 39.50 3.20 1 -7 4 36.10 3.00 -1 -7 -4 37.30 3.30 -1 -7 -4 38.20 3.70 -1 7 -4 35.00 2.90 1 7 4 35.00 2.50 1 7 4 40.80 3.20 -1 7 -4 36.60 2.90 -1 7 -4 34.90 3.00 1 7 4 31.90 2.90 1 7 4 44.40 3.40 -1 7 -4 39.40 3.10 -1 7 -4 35.80 3.20 1 7 4 38.30 3.10 -2 -7 -4 47.10 3.20 -2 -7 -4 38.80 3.80 -2 -7 -4 40.90 3.50 -2 -7 -4 40.10 3.80 2 -7 4 41.60 3.40 2 -7 4 39.90 3.50 2 -7 4 39.20 3.70 2 -7 4 33.50 3.50 -2 7 -4 41.20 3.70 -2 7 -4 43.20 3.70 2 7 4 44.00 3.50 -2 7 -4 40.00 3.30 2 7 4 41.20 3.00 2 7 4 47.10 3.80 2 7 4 46.00 3.30 -2 7 -4 43.30 3.60 -2 7 -4 41.70 3.90 2 7 4 41.00 3.30 -3 -7 -4 238.48 11.60 -3 -7 -4 246.68 12.10 3 -7 4 215.38 11.70 3 -7 4 223.28 11.30 3 -7 4 209.98 11.20 -3 -7 -4 253.57 12.30 3 -7 4 234.68 12.30 3 -7 4 222.58 11.30 3 -7 4 217.18 11.50 -3 7 -4 229.48 11.50 3 7 4 240.48 11.60 -3 7 -4 213.28 11.20 -3 7 -4 227.28 11.70 3 7 4 236.68 11.80 -3 7 -4 235.18 12.30 -3 7 -4 220.18 11.30 3 7 4 230.58 10.80 3 7 4 231.18 11.20 -3 7 -4 232.48 11.40 3 7 4 246.88 12.10 4 -7 4 7.60 2.40 4 -7 4 10.50 3.10 -4 -7 -4 14.40 3.20 4 -7 4 9.00 2.80 -4 -7 -4 11.10 2.70 4 7 4 11.40 2.60 -4 7 -4 9.10 2.30 -4 7 -4 9.50 2.70 4 7 4 13.20 3.00 -4 7 -4 9.80 2.90 -4 7 -4 10.50 2.40 5 -7 4 62.69 6.10 -5 -7 -4 65.89 6.30 5 -7 4 74.19 6.90 5 -7 4 67.29 4.20 5 -7 4 70.59 7.60 5 7 4 70.89 5.80 -5 7 -4 70.89 6.30 5 7 4 60.49 6.00 -5 7 -4 66.19 6.70 6 -7 4 5.80 3.30 -6 -7 -4 8.30 3.50 6 -7 4 7.00 1.90 6 -7 4 6.80 3.60 -6 7 -4 7.00 3.60 6 7 4 10.30 3.30 6 7 4 9.50 3.40 -6 7 -4 5.00 3.20 -6 -8 4 12.80 3.80 6 -8 -4 9.40 3.30 6 8 -4 7.90 3.40 -6 8 4 10.40 3.90 5 -8 -4 -0.30 2.00 -5 -8 4 4.00 2.60 5 -8 -4 1.30 1.60 5 -8 -4 2.60 2.40 5 -8 -4 0.30 2.40 -5 8 4 4.10 2.90 5 8 -4 1.40 2.10 -5 8 4 3.00 2.50 5 8 -4 2.80 2.20 4 -8 -4 33.30 4.00 4 -8 -4 36.20 3.30 -4 -8 4 41.30 4.70 4 -8 -4 38.50 4.30 -4 -8 4 36.40 4.10 -4 8 4 39.00 4.90 4 8 -4 42.00 4.10 4 8 -4 37.30 4.70 -4 8 4 45.10 5.10 4 8 -4 38.80 3.80 3 -8 -4 218.88 11.60 3 -8 -4 214.48 10.40 -3 -8 4 234.08 11.70 3 -8 -4 234.48 11.80 -3 -8 4 244.18 12.40 -3 -8 4 237.88 12.00 -3 8 4 209.98 11.70 3 8 -4 221.78 11.80 3 8 -4 234.38 11.40 3 8 -4 240.38 11.50 -3 8 4 216.28 12.00 -3 8 4 230.38 12.10 2 -8 -4 50.69 4.10 2 -8 -4 42.20 4.10 2 -8 -4 38.30 3.70 -2 -8 4 55.59 4.50 -2 -8 4 47.90 4.40 2 -8 -4 47.10 3.10 -2 -8 4 41.70 3.70 2 8 -4 47.40 4.00 -2 8 4 52.89 4.40 -2 8 4 45.50 4.00 2 8 -4 43.90 3.60 -2 8 4 46.40 4.00 2 8 -4 47.40 3.80 1 -8 -4 31.60 2.60 1 -8 -4 34.60 3.60 -1 -8 4 32.50 2.80 1 -8 -4 33.60 3.20 1 -8 -4 36.30 2.80 -1 -8 4 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179.78 9.30 -2 -4 10 171.58 8.70 2 -4 -10 168.08 8.60 -2 -4 10 179.48 8.40 -2 -4 10 171.48 8.70 -2 -4 10 176.68 9.00 2 4 -10 168.78 8.70 2 4 -10 167.98 8.80 -2 4 10 169.68 8.30 2 4 -10 181.18 7.70 -2 4 10 183.88 9.00 2 4 -10 179.88 8.50 2 4 -10 161.38 8.50 2 4 -10 167.08 8.80 -2 4 10 158.78 8.50 -2 4 10 184.78 9.50 1 -4 -10 124.19 6.40 1 -4 -10 126.29 5.80 1 -4 -10 124.49 6.30 -1 -4 10 133.69 6.30 1 -4 -10 118.39 6.80 1 -4 -10 127.19 6.80 1 -4 -10 127.09 5.70 -1 -4 10 118.49 6.70 -1 -4 10 128.19 6.40 1 -4 -10 129.39 6.50 -1 -4 10 119.39 6.30 1 -4 -10 133.59 6.70 -1 4 10 119.99 6.60 1 4 -10 130.29 6.90 1 4 -10 117.29 6.20 -1 4 10 131.69 6.80 -1 4 10 116.09 6.30 1 4 -10 129.79 6.60 -1 4 10 114.79 6.20 -1 4 10 116.99 6.80 -1 4 10 119.09 6.30 1 4 -10 128.79 6.10 -1 4 10 120.49 5.70 1 4 -10 120.09 7.40 0 -4 -10 49.70 3.70 0 -4 -10 53.89 3.60 0 -4 -10 56.49 3.50 0 -4 -10 55.89 3.60 0 -4 -10 57.29 3.40 0 -4 -10 59.09 3.70 0 -4 10 68.89 4.30 0 -4 -10 59.69 4.10 0 -4 10 51.69 3.20 0 -4 10 55.79 3.60 0 -4 10 54.99 3.70 0 -4 10 51.79 3.10 0 -4 10 58.39 3.30 0 4 -10 52.79 3.20 0 4 10 53.49 3.50 0 4 10 51.99 3.30 0 4 -10 55.29 2.80 0 4 -10 56.59 3.70 0 4 10 55.39 3.90 0 4 10 60.39 3.40 0 4 -10 54.69 3.00 0 4 10 57.79 4.00 0 4 -10 57.59 4.00 0 4 10 51.29 3.30 0 4 10 56.69 3.60 -1 -4 -10 54.79 3.70 1 -4 10 45.90 2.80 1 -4 10 42.70 3.50 -1 -4 -10 57.39 4.00 1 -4 10 43.00 2.90 -1 -4 -10 49.40 3.00 -1 -4 -10 55.09 3.20 1 -4 10 45.30 3.30 -1 -4 -10 50.99 3.50 -1 -4 -10 56.59 3.60 1 -4 10 47.00 3.70 1 4 10 50.69 3.50 -1 4 -10 51.89 2.90 1 4 10 49.80 3.00 1 4 10 54.79 3.90 1 4 10 46.30 3.00 -1 4 -10 46.10 3.30 1 4 10 50.59 3.70 -1 4 -10 48.40 3.30 1 4 10 49.40 3.10 -1 4 -10 48.60 3.80 -1 4 -10 44.20 2.90 -1 4 -10 45.60 2.80 1 4 10 45.80 3.50 1 4 10 48.80 3.60 -1 4 -10 59.69 3.90 2 -4 10 650.33 27.80 2 -4 10 663.83 29.40 2 -4 10 658.83 27.80 2 -4 10 646.94 29.30 2 -4 10 685.53 28.10 -2 -4 -10 701.63 29.40 -2 -4 -10 717.53 29.40 2 -4 10 632.64 28.60 -2 -4 -10 678.63 28.00 -2 -4 -10 606.14 28.60 2 4 10 688.43 29.40 -2 4 -10 703.73 29.30 -2 4 -10 661.13 28.60 2 4 10 711.93 29.70 -2 4 -10 663.13 28.40 2 4 10 649.43 28.20 2 4 10 687.23 29.30 2 4 10 709.83 29.10 -2 4 -10 623.64 28.00 -2 4 -10 676.93 29.10 -2 4 -10 646.14 28.00 -2 4 -10 638.24 28.30 -3 -4 -10 83.99 6.20 3 -4 10 85.09 6.30 -3 -4 -10 99.09 6.00 3 -4 10 90.09 5.90 3 -4 10 90.59 4.60 3 -4 10 87.99 4.90 -3 4 -10 91.89 6.00 3 4 10 95.69 6.20 -3 4 -10 84.19 5.70 3 4 10 93.09 6.20 3 4 10 85.79 5.80 -3 4 -10 89.09 4.90 3 4 10 88.49 5.20 -4 -4 -10 109.69 7.00 4 -4 10 109.39 6.00 -4 -4 -10 122.39 8.00 4 -4 10 108.89 8.10 4 -4 10 106.09 7.30 4 4 10 116.89 8.60 4 4 10 123.49 7.80 4 4 10 118.99 7.30 -4 4 -10 108.89 6.70 -4 4 -10 116.59 7.40 5 -4 10 22.00 3.00 5 -4 10 32.10 5.00 -5 -4 -10 25.60 4.30 5 -4 10 16.50 3.60 5 4 10 26.50 4.50 5 4 10 26.20 4.00 5 4 10 19.80 4.20 6 -4 10 28.30 3.90 -6 -4 -10 27.80 5.10 6 -4 10 36.70 5.50 6 -4 10 34.00 5.80 6 4 10 26.40 5.10 -6 4 -10 27.20 4.80 6 4 10 35.60 5.10 6 4 10 39.80 5.70 -6 4 -10 47.80 6.50 6 -5 -10 -0.50 2.10 6 -5 -10 0.60 2.80 6 -5 -10 1.80 2.20 -6 5 10 2.70 2.80 -6 5 10 -0.40 2.80 6 5 -10 0.20 2.40 -5 -5 10 1.40 2.30 5 -5 -10 4.20 2.30 5 -5 -10 6.20 2.40 5 -5 -10 10.80 3.30 5 -5 -10 5.40 2.10 5 5 -10 4.00 2.20 -5 5 10 8.90 3.30 -5 5 10 6.90 3.10 5 5 -10 2.10 2.10 4 -5 -10 18.10 3.20 -4 -5 10 14.80 3.10 4 -5 -10 17.10 2.80 4 -5 -10 15.20 2.80 4 -5 -10 12.40 3.10 4 5 -10 18.70 2.70 -4 5 10 19.00 3.50 4 5 -10 16.10 2.80 -4 5 10 14.80 3.40 4 5 -10 18.70 3.00 3 -5 -10 111.19 6.50 3 -5 -10 107.99 6.50 -3 -5 10 119.09 6.90 3 -5 -10 105.29 6.80 -3 -5 10 133.49 7.20 -3 -5 10 129.29 7.40 3 -5 -10 119.69 7.10 3 5 -10 128.49 7.00 3 5 -10 120.19 6.20 -3 5 10 109.69 7.20 3 5 -10 125.59 6.90 3 5 -10 118.49 6.90 -3 5 10 122.09 7.90 -2 -5 10 39.60 3.50 -2 -5 10 37.40 3.50 2 -5 -10 39.10 3.40 -2 -5 10 37.20 3.40 2 -5 -10 38.40 3.40 -2 -5 10 43.40 2.90 2 5 -10 42.50 3.40 2 5 -10 41.30 2.40 -2 5 10 34.40 2.80 -2 5 10 40.30 3.60 -2 5 10 43.70 4.20 2 5 -10 40.30 3.50 2 5 -10 37.60 3.10 2 5 -10 40.10 3.40 -1 -5 10 189.78 8.90 1 -5 -10 182.28 8.90 1 -5 -10 182.58 8.90 1 -5 -10 181.08 8.90 -1 -5 10 179.98 8.80 -1 -5 10 200.38 9.60 1 -5 -10 191.58 9.20 1 -5 -10 184.68 9.40 -1 -5 10 191.08 9.60 -1 -5 10 186.78 8.90 -1 -5 10 177.68 8.50 -1 5 10 163.48 8.90 1 5 -10 193.48 9.50 -1 5 10 165.28 8.70 -1 5 10 185.98 9.50 1 5 -10 180.78 9.10 -1 5 10 179.08 8.90 -1 5 10 177.48 8.10 -1 5 10 186.68 9.40 1 5 -10 175.38 8.70 0 -5 -10 142.19 7.00 0 -5 10 134.99 7.70 0 -5 10 133.79 6.70 0 -5 10 133.69 6.90 0 -5 -10 147.49 7.20 0 -5 10 137.39 6.70 0 -5 -10 142.69 7.10 0 -5 -10 137.59 7.20 0 -5 10 129.39 6.60 0 -5 -10 146.19 7.70 0 -5 10 147.69 7.70 0 5 10 131.59 6.80 0 5 10 145.19 7.00 0 5 -10 132.09 6.70 0 5 10 140.69 7.40 0 5 -10 140.79 7.60 0 5 10 133.49 7.10 0 5 -10 149.09 7.40 0 5 10 131.29 7.10 0 5 10 133.19 6.80 0 5 10 136.69 7.10 0 5 10 152.88 7.60 -1 -5 -10 86.39 5.30 -1 -5 -10 87.59 4.90 1 -5 10 97.29 7.60 1 -5 10 85.99 4.50 -1 -5 -10 94.69 5.30 1 -5 10 88.39 4.70 -1 -5 -10 102.79 5.60 1 -5 10 87.39 4.40 1 -5 10 89.39 5.40 -1 -5 -10 95.29 5.00 1 5 10 91.59 5.00 1 5 10 94.99 6.90 -1 5 -10 116.89 7.90 1 5 10 90.09 5.30 -1 5 -10 92.79 5.20 -1 5 -10 90.29 4.70 1 5 10 89.69 5.40 -1 5 -10 94.09 4.80 -1 5 -10 92.99 5.70 1 5 10 85.69 5.00 1 5 10 94.79 5.50 -1 5 -10 85.69 4.60 1 5 10 85.89 4.90 -1 5 -10 87.89 4.70 -2 -5 -10 17.80 2.20 -2 -5 -10 16.90 2.50 -2 -5 -10 23.00 3.00 -2 -5 -10 20.90 2.80 2 -5 10 22.40 3.00 -2 -5 -10 20.90 2.10 2 -5 10 21.30 2.50 2 -5 10 24.30 2.90 -2 5 -10 22.20 3.00 -2 5 -10 26.60 3.00 2 5 10 22.00 2.80 -2 5 -10 16.70 2.20 2 5 10 23.90 2.90 -2 5 -10 24.50 2.10 2 5 10 24.10 3.10 -2 5 -10 20.00 2.50 2 5 10 25.20 2.40 -2 5 -10 22.90 2.30 3 -5 10 32.40 3.50 3 -5 10 28.00 2.10 -3 -5 -10 31.30 3.70 3 -5 10 26.00 3.90 3 -5 10 32.20 3.40 -3 -5 -10 31.50 3.60 3 5 10 33.80 3.10 -3 5 -10 25.40 3.40 3 5 10 32.60 5.90 -3 5 -10 25.40 2.80 3 5 10 32.70 3.60 -3 5 -10 26.90 3.40 3 5 10 34.30 3.80 -3 5 -10 34.90 2.80 -4 -5 -10 0.10 1.50 4 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22.20 3.00 3 6 -10 21.20 3.00 -3 6 10 21.90 3.80 -3 6 10 28.40 3.60 3 6 -10 22.00 3.00 3 6 -10 20.50 2.40 -2 -6 10 197.28 10.60 2 -6 -10 209.98 10.40 2 -6 -10 202.98 10.20 2 -6 -10 194.18 10.40 -2 -6 10 205.08 10.70 2 -6 -10 204.18 9.90 -2 -6 10 201.38 10.20 2 6 -10 199.28 10.30 -2 6 10 200.78 10.70 2 6 -10 198.28 10.10 -2 6 10 204.38 10.80 2 6 -10 223.08 10.60 -1 -6 10 89.09 5.10 -1 -6 10 96.69 5.90 1 -6 -10 93.49 6.50 -1 -6 10 93.99 4.60 1 -6 -10 88.99 5.20 1 -6 -10 76.09 4.40 1 -6 -10 94.69 5.50 1 -6 -10 85.79 5.20 1 6 -10 81.79 4.50 1 6 -10 94.19 5.80 -1 6 10 76.59 4.90 1 6 -10 90.89 5.50 1 6 -10 90.79 5.20 -1 6 10 88.99 5.20 -1 6 10 85.89 5.60 -1 6 10 80.19 5.60 0 -6 10 27.90 2.30 0 -6 10 31.00 2.40 0 -6 10 33.30 3.20 0 -6 10 36.40 3.50 0 -6 -10 34.70 2.90 0 -6 10 27.30 2.50 0 -6 10 31.20 2.60 0 -6 -10 33.50 2.90 0 -6 -10 26.30 3.10 0 -6 -10 27.40 2.50 0 6 -10 32.00 3.40 0 6 -10 30.90 3.40 0 6 -10 25.30 2.40 0 6 10 28.60 3.00 0 6 10 28.90 2.80 0 6 10 34.30 2.80 0 6 10 26.00 3.00 0 6 -10 29.90 2.50 0 6 10 29.20 2.60 -1 -6 -10 67.99 4.40 -1 -6 -10 75.89 5.20 1 -6 10 68.49 4.80 -1 -6 -10 74.29 4.60 1 -6 10 68.49 4.50 1 -6 10 64.09 3.50 1 -6 10 54.79 3.40 1 -6 10 65.59 3.80 -1 -6 -10 60.89 4.10 1 -6 10 58.59 4.80 -1 -6 -10 65.69 4.70 -1 6 -10 59.89 3.70 1 6 10 54.89 4.10 -1 6 -10 59.49 3.70 -1 6 -10 67.39 4.40 1 6 10 64.39 4.50 -1 6 -10 79.89 5.10 1 6 10 68.59 4.80 1 6 10 72.89 4.20 1 6 10 64.89 4.70 1 6 10 67.99 4.50 -1 6 -10 63.69 3.90 -1 6 -10 66.69 4.00 2 -6 10 17.00 2.80 -2 -6 -10 21.80 2.70 -2 -6 -10 14.90 2.10 2 -6 10 17.40 2.40 -2 -6 -10 18.20 3.00 -2 -6 -10 18.50 2.80 2 -6 10 15.20 2.80 -2 6 -10 18.10 2.70 2 6 10 21.90 2.50 -2 6 -10 17.70 2.10 2 6 10 20.10 2.70 -2 6 -10 13.90 2.40 -2 6 -10 18.60 2.90 2 6 10 22.60 2.90 2 6 10 19.40 3.00 -2 6 -10 15.50 2.30 -3 -6 -10 119.19 7.60 3 -6 10 121.09 7.90 -3 -6 -10 129.69 7.60 3 -6 10 97.99 6.80 -3 6 -10 114.79 7.10 3 6 10 119.39 7.60 -3 6 -10 112.69 7.30 3 6 10 121.49 6.70 3 6 10 114.69 7.20 -3 6 -10 110.59 6.30 3 6 10 124.29 7.30 -3 6 -10 112.99 6.50 4 -6 10 23.70 4.20 -4 -6 -10 19.80 3.60 4 -6 10 20.80 3.70 -4 -6 -10 19.90 3.60 4 -6 10 22.30 2.20 4 6 10 23.70 3.80 -4 6 -10 22.20 3.60 4 6 10 21.70 3.90 4 6 10 22.10 4.00 -5 -6 -10 72.39 6.70 5 -6 10 74.89 7.20 5 -6 10 57.59 6.00 5 -6 10 66.69 4.50 5 6 10 71.19 6.70 -5 6 -10 64.79 6.00 -5 6 -10 65.79 6.90 5 6 10 78.19 6.70 6 -6 10 4.60 3.30 -6 -6 -10 10.30 3.80 6 -6 10 7.20 3.80 6 -6 10 5.40 2.10 -6 6 -10 13.00 4.20 6 6 10 10.80 4.10 -6 -7 10 0.30 2.90 6 -7 -10 0.50 2.50 -6 7 10 1.60 3.30 -6 7 10 -1.60 2.90 -5 -7 10 4.60 2.70 5 -7 -10 7.00 2.40 5 -7 -10 6.30 2.80 5 -7 -10 4.90 2.70 -5 7 10 8.60 3.60 -5 7 10 8.50 3.00 5 7 -10 6.10 2.80 4 -7 -10 23.90 3.60 4 -7 -10 27.30 3.70 -4 -7 10 23.40 4.00 4 7 -10 25.00 4.10 -4 7 10 27.70 4.80 4 7 -10 24.50 3.50 3 -7 -10 57.79 4.80 3 -7 -10 56.19 4.40 -3 -7 10 63.89 5.20 -3 -7 10 65.49 5.10 3 -7 -10 66.09 5.10 -3 -7 10 66.79 5.50 3 -7 -10 68.59 5.20 -3 7 10 71.29 5.60 3 7 -10 67.09 5.00 3 7 -10 76.89 5.40 -3 7 10 58.79 5.80 3 7 -10 65.99 5.00 2 -7 -10 254.77 12.60 2 -7 -10 236.08 12.30 -2 -7 10 261.57 13.00 -2 -7 10 245.38 12.20 2 -7 -10 233.58 11.90 -2 -7 10 259.77 13.00 2 -7 -10 251.27 12.70 2 7 -10 260.97 12.60 -2 7 10 242.78 12.40 2 7 -10 254.97 12.40 -2 7 10 258.87 13.00 2 7 -10 263.47 12.90 -2 7 10 254.97 13.00 1 -7 -10 51.39 4.40 -1 -7 10 42.30 4.20 1 -7 -10 49.60 4.10 1 -7 -10 45.70 3.70 1 -7 -10 45.60 3.80 -1 -7 10 52.89 4.40 -1 -7 10 61.79 3.90 -1 7 10 53.19 4.20 -1 7 10 48.10 3.90 -1 7 10 51.69 4.40 1 7 -10 51.19 4.10 1 7 -10 58.09 4.50 0 -7 10 56.59 3.60 0 -7 -10 63.19 4.80 0 -7 -10 65.19 4.30 0 -7 10 59.69 3.70 0 -7 10 50.89 4.40 0 -7 -10 58.29 3.90 0 -7 -10 59.49 4.10 0 -7 10 52.69 4.70 0 7 10 56.69 5.50 0 7 10 51.89 3.80 0 7 -10 57.59 3.90 0 7 10 61.69 4.30 0 7 -10 55.39 4.20 0 7 10 61.19 4.60 0 7 -10 59.79 4.80 -1 -7 -10 4.70 1.60 1 -7 10 2.70 1.70 -1 -7 -10 3.40 1.50 1 -7 10 5.90 2.00 1 -7 10 5.80 1.10 -1 -7 -10 5.20 1.90 1 -7 10 4.00 1.50 1 -7 10 3.30 1.00 -1 7 -10 4.30 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135.39 7.00 -2 3 -14 130.39 8.10 2 3 14 141.29 8.40 2 3 14 141.29 7.90 3 -3 14 383.66 18.70 3 -3 14 424.86 19.90 -3 -3 -14 418.66 19.50 -3 -3 -14 393.36 19.10 3 -3 14 403.56 18.00 3 3 14 400.16 18.90 -3 3 -14 410.06 19.50 -3 3 -14 406.96 19.10 3 3 14 396.66 19.30 4 -3 14 4.10 2.40 -4 -3 -14 2.30 2.20 4 -3 14 9.00 2.00 -4 -3 -14 9.40 3.00 4 -3 14 16.70 3.70 4 3 14 14.00 3.40 -4 3 -14 11.90 2.70 4 3 14 12.00 2.90 5 -3 14 11.20 3.60 5 -3 14 17.60 2.90 5 -3 14 11.30 3.50 -5 -3 -14 15.50 3.90 5 3 14 19.30 4.50 5 3 14 15.40 3.50 5 3 14 13.20 3.70 -5 3 -14 13.10 3.60 6 -3 14 -1.10 2.10 -6 -3 -14 -3.30 2.60 6 -3 14 -0.10 2.70 6 -3 14 3.60 3.60 6 3 14 2.60 2.80 6 3 14 0.60 2.90 -6 3 -14 4.80 4.20 6 3 14 2.30 2.90 6 -4 -14 7.70 3.10 6 -4 -14 6.40 2.90 6 -4 -14 11.30 3.90 6 -4 -14 1.30 2.40 -6 4 14 7.00 3.40 6 4 -14 2.40 2.50 -6 4 14 7.50 4.00 5 -4 -14 6.80 2.70 5 -4 -14 2.80 2.30 5 -4 -14 0.00 2.00 -5 4 14 6.00 3.40 5 4 -14 4.70 2.40 5 4 -14 8.20 2.80 -5 4 14 8.00 3.00 4 -4 -14 246.58 13.20 4 -4 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20.90 3.90 4 -4 14 20.90 3.70 4 -4 14 19.90 4.20 -4 -4 -14 19.20 3.70 4 -4 14 25.20 2.90 4 4 14 19.20 3.50 -4 4 -14 24.20 3.60 4 4 14 19.20 4.00 4 4 14 28.20 4.20 -4 4 -14 16.40 3.50 -5 -4 -14 33.50 5.20 5 -4 14 29.60 4.70 5 -4 14 33.90 3.70 5 -4 14 48.00 6.00 5 4 14 32.70 5.20 -5 4 -14 29.10 4.60 5 4 14 40.40 5.50 5 4 14 30.70 4.70 6 -5 -14 1.10 2.60 6 -5 -14 3.90 2.90 6 -5 -14 3.90 3.70 -6 5 14 2.90 3.20 -6 5 14 0.80 3.50 6 5 -14 5.00 2.90 5 -5 -14 9.10 2.90 -5 -5 14 8.10 2.90 5 -5 -14 7.50 2.80 5 -5 -14 7.40 2.90 -5 5 14 8.30 3.10 5 5 -14 4.80 2.40 -5 5 14 6.10 3.50 5 5 -14 10.30 2.90 4 -5 -14 97.59 6.80 4 -5 -14 102.29 6.70 4 -5 -14 100.89 7.00 -4 -5 14 104.69 7.10 -4 5 14 105.09 8.30 -4 5 14 111.09 7.50 4 5 -14 102.69 7.00 4 5 -14 104.49 7.00 -3 -5 14 10.00 2.60 3 -5 -14 7.90 2.30 -3 -5 14 9.60 2.40 3 -5 -14 14.70 2.60 3 -5 -14 9.30 2.30 3 -5 -14 8.90 2.60 -3 5 14 7.10 3.10 -3 5 14 11.70 2.90 3 5 -14 7.80 2.20 3 5 -14 11.80 2.40 3 5 -14 9.20 2.40 2 -5 -14 108.49 7.00 -2 -5 14 122.99 6.70 2 -5 -14 124.19 6.90 2 -5 -14 128.09 7.30 -2 -5 14 120.39 7.40 2 -5 -14 112.49 6.80 -2 -5 14 113.59 6.90 2 5 -14 123.39 7.30 2 5 -14 133.99 7.30 2 5 -14 118.69 6.70 -2 5 14 114.59 7.70 -2 5 14 131.39 7.50 -1 -5 14 4.80 1.50 1 -5 -14 5.30 1.60 -1 -5 14 5.50 1.70 1 -5 -14 5.00 1.70 1 -5 -14 3.10 1.50 -1 -5 14 3.90 1.80 1 -5 -14 0.70 1.40 -1 5 14 7.20 2.10 1 5 -14 6.30 1.60 1 5 -14 5.20 1.80 1 5 -14 4.90 1.80 -1 5 14 3.20 1.50 -1 5 14 2.10 1.40 -1 5 14 4.90 1.80 0 -5 14 33.10 3.50 0 -5 14 33.50 2.90 0 -5 14 36.70 3.30 0 -5 -14 48.10 4.10 0 -5 -14 31.50 3.70 0 -5 -14 37.50 3.10 0 -5 -14 34.20 3.30 0 5 14 35.40 2.80 0 5 -14 38.30 3.30 0 5 14 36.40 3.50 0 5 14 33.90 3.60 0 5 14 28.50 3.10 0 5 -14 32.40 2.60 0 5 14 26.50 2.80 0 5 -14 42.30 3.90 -1 -5 -14 92.19 5.80 -1 -5 -14 100.39 5.50 1 -5 14 90.09 6.20 -1 -5 -14 97.39 6.40 -1 -5 -14 102.79 6.00 1 -5 14 93.19 6.10 1 -5 14 90.19 5.10 -1 5 -14 94.79 6.30 1 5 14 97.99 6.00 -1 5 -14 91.99 5.60 1 5 14 90.59 6.10 1 5 14 93.19 5.10 -1 5 -14 87.99 4.70 -1 5 -14 94.59 6.20 1 5 14 88.59 6.10 -2 -5 -14 148.49 9.00 2 -5 14 159.18 9.20 -2 -5 -14 156.88 8.90 -2 -5 -14 146.89 7.60 2 -5 14 155.88 9.20 2 -5 14 151.68 7.50 -2 5 -14 144.79 8.00 2 5 14 162.08 9.10 -2 5 -14 156.08 9.00 -2 5 -14 159.88 9.10 2 5 14 169.18 9.40 2 5 14 162.28 8.90 3 -5 14 119.49 8.30 -3 -5 -14 118.19 7.90 3 -5 14 120.49 9.70 3 -5 14 119.29 6.20 -3 -5 -14 123.29 7.80 -3 5 -14 112.99 7.50 3 5 14 114.79 7.50 3 5 14 113.89 7.80 3 5 14 118.69 8.00 -3 5 -14 121.99 7.90 4 -5 14 1.90 2.10 -4 -5 -14 1.40 1.90 4 -5 14 0.30 2.20 4 -5 14 -0.90 1.10 -4 -5 -14 -3.10 1.80 -4 5 -14 2.90 2.40 -4 5 -14 1.20 1.90 4 5 14 2.50 2.30 4 5 14 -1.30 1.90 4 5 14 0.90 2.30 -5 -5 -14 7.00 3.20 5 -5 14 12.30 4.80 5 -5 14 15.40 6.40 5 -5 14 15.00 2.60 5 5 14 7.30 3.40 5 5 14 9.40 3.50 5 5 14 5.80 3.20 -5 5 -14 12.90 3.80 6 -6 -14 13.50 3.90 6 -6 -14 15.60 4.10 6 -6 -14 21.40 4.30 -6 6 14 19.50 5.20 -6 6 14 10.50 4.50 6 6 -14 10.70 3.50 5 -6 -14 19.80 3.70 -5 -6 14 14.90 3.70 5 -6 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74.89 4.80 0 -6 -14 67.89 4.50 0 -6 -14 69.89 4.80 0 -6 14 66.89 4.30 0 -6 -14 66.99 4.80 0 6 -14 64.99 4.20 0 6 14 73.99 4.50 0 6 -14 67.99 5.30 0 6 14 71.69 5.30 0 6 14 75.29 5.40 0 6 -14 68.79 5.00 1 -6 14 9.00 1.60 1 -6 14 6.20 2.10 -1 -6 -14 10.20 2.10 -1 -6 -14 9.00 2.40 -1 -6 -14 9.40 2.20 -1 -6 -14 6.00 2.00 1 -6 14 3.40 1.90 1 6 14 12.60 2.00 1 6 14 8.50 2.40 -1 6 -14 8.60 1.60 1 6 14 12.80 2.70 -1 6 -14 9.40 2.40 -1 6 -14 8.20 2.10 -1 6 -14 9.30 2.40 1 6 14 9.50 2.20 2 -6 14 68.39 5.70 2 -6 14 74.49 4.20 -2 -6 -14 79.49 5.80 2 -6 14 71.69 5.80 -2 -6 -14 71.99 5.80 -2 6 -14 68.79 5.50 -2 6 -14 69.79 4.90 -2 6 -14 68.69 5.60 2 6 14 75.69 5.80 2 6 14 75.79 5.60 2 6 14 78.19 5.80 3 -6 14 50.29 3.30 -3 -6 -14 43.90 4.80 -3 -6 -14 57.29 5.20 3 -6 14 42.30 5.10 3 6 14 56.99 5.10 3 6 14 59.49 5.20 3 6 14 45.00 5.10 -3 6 -14 49.90 5.00 -3 6 -14 44.70 4.70 -4 -6 -14 46.90 5.50 -4 -6 -14 63.79 5.80 4 -6 14 63.29 6.40 4 -6 14 49.99 3.70 4 6 14 48.70 5.60 4 6 14 55.49 5.70 -4 6 -14 58.29 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6.30 0 -9 -21 55.99 5.40 0 -9 21 44.80 4.80 0 -9 21 50.79 6.30 0 9 21 56.59 6.30 0 9 -21 56.99 6.20 0 9 -21 61.89 6.50 0 9 -21 54.49 5.60 0 9 21 57.39 6.10 -1 -9 -21 66.99 6.90 1 -9 21 50.59 6.20 1 -9 21 58.19 4.90 -1 9 -21 58.19 6.20 -1 9 -21 68.49 6.90 -1 9 -21 60.89 6.00 1 9 21 80.09 7.20 1 9 21 57.79 6.40 -2 -9 -21 4.10 3.10 2 -9 21 5.20 4.00 2 -9 21 6.40 2.30 2 9 21 3.30 3.00 -2 9 -21 7.00 3.20 2 9 21 2.80 3.30 -2 9 -21 4.60 3.90 3 -10 -21 40.10 5.80 3 10 -21 38.00 7.40 3 10 -21 36.00 5.70 -2 -10 21 1.10 2.40 2 -10 -21 -2.30 2.30 -2 -10 21 -2.00 2.40 2 -10 -21 1.30 2.80 -2 10 21 -0.10 2.60 -2 10 21 1.90 2.80 2 10 -21 -1.10 2.50 1 -10 -21 50.99 6.40 -1 -10 21 42.50 5.10 1 -10 -21 55.19 5.80 -1 -10 21 46.50 6.30 1 10 -21 48.10 5.70 -1 10 21 62.09 6.60 1 10 -21 61.49 6.50 -1 10 21 52.89 6.40 0 -10 21 31.20 5.30 0 -10 -21 35.10 5.60 0 -10 -21 34.60 4.80 0 -10 21 31.80 4.20 0 10 -21 27.90 5.00 0 10 21 33.80 5.50 0 10 21 32.50 5.40 0 10 -21 30.30 5.40 0 10 -21 38.50 5.30 1 -10 21 -2.90 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2.00 1 0 22 8.10 2.50 -1 0 -22 4.00 2.50 -1 0 -22 6.20 2.40 1 0 22 6.90 2.70 -2 0 -22 1.90 2.30 2 0 22 6.50 2.80 2 0 22 2.40 2.20 -2 0 -22 1.00 2.00 -3 0 -22 4.00 2.40 3 0 22 -0.90 2.20 -3 0 -22 2.10 2.30 3 0 22 2.60 2.00 4 0 22 0.80 2.30 -4 0 -22 0.70 2.80 -4 0 -22 -2.80 2.10 4 0 22 1.10 2.70 5 -1 -22 5.90 2.90 -5 -1 22 10.40 4.50 5 -1 -22 11.90 3.60 5 1 -22 10.20 3.40 5 1 -22 9.50 3.20 -5 1 22 14.90 3.90 4 -1 -22 4.20 2.40 -4 -1 22 5.40 2.60 4 -1 -22 3.90 2.40 4 1 -22 6.20 3.20 -4 1 22 3.90 2.50 4 1 -22 2.10 2.30 3 -1 -22 4.30 2.40 -3 -1 22 4.80 2.50 -3 1 22 2.30 2.10 3 1 -22 4.20 3.60 3 1 -22 3.60 2.20 2 -1 -22 1.10 1.90 -2 -1 22 2.40 2.20 -2 -1 22 1.90 1.80 -2 -1 22 4.30 2.30 2 1 -22 1.70 2.00 -2 1 22 1.40 2.20 1 -1 -22 44.00 4.40 1 -1 -22 49.99 5.00 -1 -1 22 40.80 4.40 -1 -1 22 48.40 4.70 -1 -1 22 55.09 5.40 1 1 -22 39.80 4.30 1 1 -22 46.60 4.50 -1 1 22 49.80 4.80 -1 1 22 60.29 5.50 1 1 -22 46.10 4.90 0 -1 -22 28.60 4.10 0 -1 22 34.80 3.90 0 -1 -22 29.40 3.80 0 -1 -22 31.30 3.60 0 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3.10 3 2 -22 7.90 2.60 -3 2 22 8.20 3.00 3 2 -22 7.60 2.70 -2 -2 22 37.40 4.30 2 -2 -22 41.70 6.30 2 -2 -22 38.20 4.50 -2 -2 22 36.90 4.40 -2 -2 22 36.30 4.60 2 2 -22 47.20 4.60 -2 2 22 40.00 5.00 2 2 -22 37.70 4.50 2 2 -22 44.30 4.50 -1 -2 22 89.49 7.00 -1 -2 22 93.59 6.50 1 -2 -22 97.59 7.10 -1 -2 22 91.19 6.70 1 -2 -22 84.19 6.20 1 2 -22 102.69 7.20 1 2 -22 90.69 6.40 -1 2 22 104.89 7.50 1 2 -22 99.99 6.60 0 -2 -22 102.69 6.80 0 -2 -22 100.09 6.80 0 -2 22 102.99 7.00 0 -2 22 114.89 7.50 0 -2 22 106.89 7.80 0 -2 -22 111.79 7.80 0 2 -22 115.69 8.00 0 2 22 107.49 7.30 0 2 -22 112.99 7.40 0 2 -22 106.99 6.90 0 2 22 115.79 8.00 -1 -2 -22 0.10 2.00 1 -2 22 1.80 2.30 -1 -2 -22 1.90 2.20 1 -2 22 3.90 1.90 1 2 22 0.90 2.00 -1 2 -22 1.80 2.20 1 2 22 1.50 1.90 -1 2 -22 0.70 1.60 -1 2 -22 0.80 2.00 2 -2 22 14.00 2.70 2 -2 22 9.30 3.20 -2 -2 -22 17.30 3.50 -2 -2 -22 18.90 3.70 2 2 22 10.40 3.30 -2 2 -22 12.00 3.20 2 2 22 6.60 2.50 -2 2 -22 13.90 3.30 3 -2 22 9.30 2.50 3 -2 22 9.80 3.60 -3 -2 -22 11.30 3.20 -3 -2 -22 8.30 3.10 3 2 22 6.00 3.00 3 2 22 5.80 2.80 -3 2 -22 12.10 3.50 -3 2 -22 13.10 3.70 -4 -2 -22 7.20 3.30 4 -2 22 2.20 3.10 -4 -2 -22 7.90 4.70 4 -2 22 7.60 3.20 4 2 22 5.10 3.40 -4 2 -22 8.90 3.40 4 2 22 8.40 3.30 5 -3 -22 2.00 2.60 5 -3 -22 0.00 2.70 5 3 -22 4.80 2.80 -5 3 22 6.50 3.40 4 -3 -22 0.90 2.20 4 -3 -22 0.30 2.40 4 3 -22 2.50 2.30 -4 3 22 2.70 2.40 -3 -3 22 9.60 3.00 3 -3 -22 6.60 2.80 3 3 -22 6.60 2.60 3 3 -22 5.30 2.40 -3 3 22 8.30 3.10 2 -3 -22 41.90 4.70 2 -3 -22 42.50 4.70 -2 -3 22 42.40 4.60 -2 -3 22 36.00 4.50 -2 -3 22 47.90 4.90 2 3 -22 45.10 4.50 2 3 -22 35.30 4.50 -2 3 22 43.20 5.20 2 3 -22 42.50 4.60 -1 -3 22 0.50 1.90 1 -3 -22 -0.10 1.80 1 -3 -22 -0.50 1.60 -1 -3 22 1.10 2.10 -1 -3 22 -0.50 1.70 1 3 -22 1.10 1.80 -1 3 22 1.40 2.00 1 3 -22 3.20 2.10 1 3 -22 -1.30 1.80 0 -3 22 56.49 5.60 0 -3 22 65.49 5.70 0 -3 -22 57.59 8.40 0 -3 -22 51.59 6.40 0 -3 22 53.59 4.70 0 -3 -22 48.90 4.60 0 3 22 39.10 6.70 0 3 -22 54.99 4.80 0 3 -22 54.09 6.20 0 3 22 67.69 5.90 0 3 -22 60.09 5.30 1 -3 22 25.30 4.10 -1 -3 -22 29.60 4.40 -1 -3 -22 25.80 3.80 1 -3 22 20.90 3.20 1 3 22 24.00 4.40 -1 3 -22 24.60 4.10 -1 3 -22 22.00 3.20 1 3 22 21.30 3.60 -1 3 -22 22.20 3.80 -2 -3 -22 5.60 2.70 2 -3 22 8.10 2.40 -2 -3 -22 8.80 2.80 2 -3 22 12.70 3.40 -2 3 -22 7.00 2.80 2 3 22 11.00 3.00 -2 3 -22 9.80 3.00 2 3 22 14.70 3.70 2 3 22 8.50 2.70 3 -3 22 2.50 2.60 -3 -3 -22 2.90 2.60 -3 -3 -22 6.40 3.00 3 -3 22 4.50 2.10 3 3 22 3.70 2.80 3 3 22 1.20 2.20 -3 3 -22 1.10 2.30 -3 3 -22 6.70 3.00 3 3 22 3.20 2.50 4 -3 22 103.99 9.00 -4 -3 -22 99.49 8.40 4 -3 22 110.59 7.80 4 3 22 91.89 8.20 4 3 22 94.89 8.70 4 3 22 95.79 8.00 -4 3 -22 87.99 8.60 -4 3 -22 88.99 8.40 5 -4 -22 19.70 4.10 5 -4 -22 19.70 4.30 5 4 -22 13.70 4.00 5 4 -22 16.60 3.70 -5 4 22 23.90 5.20 4 -4 -22 1.60 2.20 4 -4 -22 1.70 2.50 4 4 -22 3.20 2.60 -3 -4 22 11.60 3.20 3 -4 -22 8.10 2.90 3 4 -22 6.00 2.70 3 4 -22 12.00 3.30 -3 4 22 16.10 3.90 2 -4 -22 66.39 6.00 -2 -4 22 80.19 6.40 -2 -4 22 73.79 6.20 2 -4 -22 81.69 6.60 -2 -4 22 73.39 6.10 2 4 -22 78.09 6.20 -2 4 22 86.39 7.10 2 4 -22 87.19 6.40 1 -4 -22 3.90 2.20 -1 -4 22 4.40 2.40 -1 -4 22 2.20 2.10 -1 -4 22 0.70 1.70 1 4 -22 6.90 2.50 1 4 -22 5.70 2.90 1 4 -22 4.10 2.40 -1 4 22 6.20 2.80 0 -4 -22 13.00 3.10 0 -4 22 12.60 3.40 0 -4 -22 14.30 2.90 0 -4 22 14.90 3.40 0 -4 22 10.00 2.90 0 4 -22 18.40 3.60 0 4 22 15.90 3.60 0 4 -22 27.60 5.80 0 4 22 15.50 3.20 0 4 -22 19.60 3.30 1 -4 22 2.60 2.40 -1 -4 -22 1.20 1.80 1 -4 22 2.90 1.80 -1 -4 -22 2.90 2.30 1 4 22 4.60 2.70 -1 4 -22 0.40 2.10 1 4 22 3.70 2.40 -1 4 -22 3.20 2.30 -1 4 -22 4.40 2.00 -2 -4 -22 3.50 2.70 2 -4 22 9.60 3.40 2 -4 22 3.90 2.00 -2 -4 -22 6.50 2.70 2 4 22 3.20 2.70 2 4 22 6.10 3.20 -2 4 -22 5.00 2.70 2 4 22 6.60 3.00 -2 4 -22 6.70 2.80 3 -4 22 28.00 3.80 -3 -4 -22 23.40 4.60 -3 -4 -22 19.90 4.30 3 -4 22 25.80 4.90 3 4 22 20.00 4.50 3 4 22 17.90 4.00 -3 4 -22 16.90 4.10 3 4 22 17.60 5.10 -3 4 -22 24.90 4.50 -4 -4 -22 75.09 7.50 -4 -4 -22 63.99 6.90 4 -4 22 67.99 5.70 4 -4 22 74.49 7.90 4 4 22 66.39 7.10 4 4 22 74.59 7.70 -4 4 -22 66.49 7.10 4 -5 -22 0.60 2.50 4 -5 -22 0.30 2.40 4 5 -22 2.10 2.60 -4 5 22 1.80 2.40 -3 -5 22 24.90 4.50 3 -5 -22 26.70 4.40 -3 5 22 30.70 4.90 3 5 -22 29.10 4.40 3 5 -22 24.70 4.20 2 -5 -22 16.30 3.40 2 -5 -22 9.20 3.60 -2 -5 22 10.50 2.90 2 5 -22 8.60 2.80 -2 5 22 11.40 3.40 2 5 -22 12.20 3.30 1 -5 -22 -0.20 1.90 -1 -5 22 4.40 2.40 1 -5 -22 -1.40 3.00 -1 -5 22 0.90 2.70 -1 -5 22 2.40 3.30 1 5 -22 4.50 2.40 1 5 -22 -0.70 1.70 1 5 -22 3.20 2.30 -1 5 22 0.40 2.00 -1 5 22 0.40 2.10 0 -5 -22 35.20 4.70 0 -5 22 26.70 4.20 0 -5 -22 26.90 3.80 0 -5 22 36.50 4.80 0 -5 22 30.00 3.70 0 5 22 35.10 4.40 0 5 22 32.10 4.80 0 5 -22 27.30 3.80 0 5 -22 33.60 4.50 0 5 -22 26.60 4.50 1 -5 22 18.20 2.90 1 -5 22 7.00 2.90 -1 -5 -22 11.60 3.30 1 -5 22 6.30 2.80 -1 -5 -22 13.20 3.30 1 5 22 17.30 3.90 1 5 22 16.60 3.60 -1 5 -22 13.60 3.30 -1 5 -22 8.00 2.40 -1 5 -22 10.60 3.10 -2 -5 -22 12.60 3.30 -2 -5 -22 12.90 3.60 2 -5 22 12.60 3.70 2 -5 22 10.20 2.40 2 5 22 16.20 3.70 -2 5 -22 7.00 3.00 -2 5 -22 9.20 3.00 2 5 22 16.60 3.90 3 -5 22 8.00 2.40 -3 -5 -22 12.20 3.60 -3 -5 -22 14.60 3.80 3 -5 22 11.20 3.70 3 5 22 12.60 4.30 3 5 22 9.50 3.40 -3 5 -22 18.00 4.20 -3 5 -22 7.50 3.10 4 5 22 13.90 4.30 4 -6 -22 1.30 2.90 4 -6 -22 0.40 2.40 4 6 -22 5.70 3.00 -4 6 22 4.80 2.80 -3 -6 22 -1.00 2.20 3 -6 -22 4.20 2.60 -3 6 22 5.40 2.80 3 6 -22 2.20 2.30 3 6 -22 0.30 2.10 -2 -6 22 27.80 4.60 -2 -6 22 28.50 4.40 2 -6 -22 36.50 4.90 2 -6 -22 26.40 4.10 -2 6 22 23.30 4.80 2 6 -22 24.30 4.30 -2 6 22 38.00 5.20 2 6 -22 27.80 4.30 -1 -6 22 19.20 4.10 1 -6 -22 17.90 3.80 -1 -6 22 27.80 3.90 1 -6 -22 19.80 3.90 1 6 -22 18.50 3.70 1 6 -22 14.90 3.40 1 6 -22 24.50 4.10 -1 6 22 19.80 4.20 -1 6 22 18.20 3.70 0 -6 22 43.10 5.30 0 -6 -22 51.99 5.70 0 -6 -22 48.10 4.80 0 -6 22 45.00 4.50 0 6 22 43.90 6.40 0 6 -22 45.70 5.20 0 6 22 43.40 5.30 0 6 -22 51.89 5.30 0 6 -22 51.19 4.90 1 -6 22 22.00 4.00 1 -6 22 14.40 3.60 1 -6 22 10.30 2.40 -1 -6 -22 12.00 3.40 1 6 22 9.80 3.30 -1 6 -22 15.90 3.30 -1 6 -22 15.00 3.50 1 6 22 17.90 3.90 -1 6 -22 13.40 3.30 2 -6 22 9.30 3.30 -2 -6 -22 13.00 3.70 -2 -6 -22 15.80 3.50 2 -6 22 19.00 3.10 2 6 22 11.00 3.60 2 6 22 16.70 4.10 -2 6 -22 20.40 4.20 -2 6 -22 14.90 3.70 3 -6 22 -2.30 1.60 -3 -6 -22 2.20 2.70 3 -6 22 0.80 3.10 -3 -6 -22 -0.10 2.60 3 6 22 -2.10 2.70 -3 6 -22 -2.80 2.20 -3 6 -22 2.30 2.70 3 6 22 1.30 4.30 4 -7 -22 3.00 2.70 4 -7 -22 0.30 2.40 -4 7 22 7.10 3.10 4 7 -22 1.60 2.70 -3 -7 22 0.50 2.60 -3 -7 22 3.00 3.00 3 -7 -22 3.40 2.80 -3 7 22 10.90 3.70 3 7 -22 2.00 2.50 3 7 -22 2.10 2.40 -3 7 22 1.70 2.50 -2 -7 22 18.20 4.10 2 -7 -22 7.70 3.00 2 -7 -22 18.00 3.80 -2 -7 22 10.30 3.00 2 7 -22 16.00 3.60 -2 7 22 20.50 4.30 -2 7 22 8.20 3.00 2 7 -22 15.50 3.60 -1 -7 22 63.99 6.50 1 -7 -22 62.29 5.80 1 -7 -22 72.89 6.60 -1 -7 22 59.29 5.50 1 7 -22 63.69 6.20 -1 7 22 73.49 6.40 1 7 -22 61.09 5.90 1 7 -22 60.39 6.30 -1 7 22 74.49 6.80 0 -7 -22 10.70 3.40 0 -7 -22 12.90 4.60 0 -7 22 17.60 3.90 0 -7 22 12.60 2.80 0 7 -22 15.40 3.40 0 7 -22 12.80 3.50 0 7 22 12.20 3.50 0 7 22 11.20 3.30 0 7 -22 17.40 3.80 1 -7 22 6.40 2.90 -1 -7 -22 -0.20 2.30 1 -7 22 0.90 1.70 1 7 22 -1.80 1.90 -1 7 -22 0.00 2.10 -1 7 -22 -0.20 2.10 -1 7 -22 5.00 2.60 1 7 22 1.30 2.30 -2 -7 -22 27.40 5.00 2 -7 22 18.40 3.30 2 -7 22 22.90 4.60 2 7 22 29.50 5.00 -2 7 -22 22.60 4.60 2 7 22 37.30 5.40 -2 7 -22 22.10 4.50 3 -7 22 88.09 6.20 3 -7 22 86.29 10.40 -3 -7 -22 87.19 8.20 -3 -7 -22 100.39 8.10 3 7 22 107.99 8.70 -3 7 -22 90.69 8.20 -3 7 -22 95.39 8.30 3 7 22 77.79 8.00 3 -8 -22 -0.50 2.40 -3 -8 22 3.30 3.20 -3 -8 22 -0.70 2.50 3 8 -22 4.00 3.30 -3 8 22 2.80 2.90 3 8 -22 3.60 2.90 -3 8 22 3.30 3.00 2 -8 -22 -1.70 2.20 -2 -8 22 -2.90 2.20 2 -8 -22 0.20 2.30 -2 -8 22 -0.60 2.10 2 8 -22 -1.50 2.20 -2 8 22 3.10 2.70 -2 8 22 4.40 2.80 2 8 -22 0.60 2.20 1 -8 -22 6.30 2.70 1 -8 -22 6.50 2.90 -1 -8 22 0.10 2.10 -1 -8 22 4.70 3.00 1 8 -22 0.80 2.30 -1 8 22 2.60 2.60 -1 8 22 4.10 2.60 1 8 -22 7.20 2.90 0 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4 -27 1.00 2.60 0 4 -27 1.50 2.50 0 4 -27 0.90 2.40 -1 -4 -27 3.00 3.90 1 -4 27 7.60 2.80 -1 4 -27 3.40 3.50 -1 4 -27 9.90 3.60 1 4 27 4.40 3.40 2 -4 27 7.00 3.40 -2 -4 -27 1.90 2.80 2 -4 27 1.40 2.60 -2 4 -27 3.90 3.10 2 4 27 2.80 3.10 -2 4 -27 7.70 3.60 2 -5 -27 2.40 3.00 2 -5 -27 -1.60 2.40 -2 -5 27 1.90 3.00 -2 5 27 0.20 2.50 2 5 -27 0.40 2.80 2 5 -27 5.00 4.60 -1 -5 27 13.10 3.30 1 -5 -27 19.60 4.10 -1 -5 27 16.10 4.10 1 -5 -27 16.50 4.10 -1 5 27 10.60 4.30 1 5 -27 16.30 4.00 1 5 -27 21.40 4.20 1 5 -27 12.30 3.60 0 -5 27 11.70 3.70 0 -5 27 15.30 5.00 0 -5 -27 10.90 3.60 0 -5 27 2.60 2.50 0 5 -27 8.30 3.20 0 5 27 15.90 4.30 0 5 -27 6.50 3.40 0 5 -27 5.00 3.10 1 -5 27 18.70 5.90 -1 -5 -27 19.80 4.50 1 5 27 15.10 4.30 -1 5 -27 15.90 4.20 -2 -6 27 12.60 3.70 2 -6 -27 17.90 5.60 -2 -6 27 27.30 5.20 2 -6 -27 21.60 4.60 2 6 -27 13.10 3.90 -2 6 27 20.20 4.70 2 6 -27 19.00 5.10 1 -6 -27 14.70 3.80 1 -6 -27 10.30 4.20 -1 -6 27 13.30 4.30 -1 -6 27 11.40 3.40 1 6 -27 15.60 6.20 -1 6 27 22.00 4.90 1 6 -27 19.90 4.50 1 6 -27 14.70 3.80 0 -6 -27 10.40 3.70 0 -6 27 3.90 3.20 0 -6 27 4.30 3.70 0 6 -27 6.00 3.10 0 6 27 0.90 2.80 0 6 -27 6.80 4.90 0 6 -27 8.90 3.50 1 -6 27 4.80 2.70 -1 -6 -27 7.20 3.50 1 6 27 7.40 3.70 -1 6 -27 4.30 3.30 -1 6 -27 4.10 3.10 1 -7 -27 16.90 4.30 1 -7 -27 15.60 4.00 -1 -7 27 6.60 3.80 -1 7 27 18.70 5.20 1 7 -27 9.70 3.30 1 7 -27 5.70 3.40 1 7 -27 14.10 4.10 3 0 -28 -1.80 2.30 -3 0 28 -2.20 2.30 2 0 -28 35.20 5.40 2 0 -28 31.50 4.90 -2 0 28 42.60 5.90 1 0 -28 -1.10 2.40 1 0 -28 1.70 2.30 -1 0 28 2.90 3.10 0 0 28 0.70 2.90 0 0 -28 -1.80 2.10 1 0 28 15.80 3.60 1 0 28 36.90 5.90 -1 0 -28 26.20 5.90 -1 0 -28 24.70 4.70 -2 0 -28 12.20 5.70 2 0 28 12.80 4.40 -2 0 -28 7.20 3.60 2 0 28 4.30 3.00 -3 -1 28 10.50 3.80 3 -1 -28 16.40 3.90 -3 1 28 19.00 4.80 3 1 -28 11.40 3.70 -2 -1 28 12.70 4.30 2 -1 -28 11.90 3.50 2 -1 -28 7.10 3.20 2 1 -28 6.70 3.10 -2 1 28 10.20 3.70 2 1 -28 12.10 3.50 1 -1 -28 39.80 5.70 1 -1 -28 42.70 5.20 -1 1 28 46.30 6.10 1 1 -28 47.20 5.40 1 1 -28 41.30 5.70 0 -1 -28 10.00 3.60 0 -1 28 12.10 4.00 0 -1 28 4.70 2.90 0 1 28 11.90 3.90 0 1 -28 10.60 3.60 -1 -1 -28 34.50 7.50 -1 -1 -28 32.30 5.80 1 -1 28 36.30 5.30 1 -1 28 44.50 6.20 1 1 28 38.60 6.10 -1 1 -28 37.50 5.50 -1 1 -28 39.60 8.40 2 -1 28 0.00 2.80 -2 -1 -28 2.40 3.10 2 1 28 -0.80 2.60 -2 1 -28 4.70 3.00 2 1 28 0.70 2.80 -2 1 -28 4.50 3.60 3 -2 -28 7.40 3.40 -3 -2 28 8.20 3.50 -3 2 28 4.30 3.20 3 2 -28 8.30 3.40 2 -2 -28 15.50 3.90 2 -2 -28 12.10 3.80 -2 2 28 22.60 4.90 2 2 -28 28.40 5.10 2 2 -28 18.40 4.00 -1 -2 28 2.90 3.20 1 -2 -28 -0.10 2.40 1 -2 -28 -0.10 2.50 1 2 -28 -0.40 2.30 1 2 -28 0.00 2.60 -1 2 28 -0.10 2.70 0 -2 -28 39.80 5.80 0 -2 28 36.00 5.10 0 -2 28 42.40 8.10 0 2 28 44.00 6.20 0 2 -28 38.00 5.20 0 2 -28 37.20 5.80 1 -2 28 3.30 2.60 -1 -2 -28 2.80 4.20 1 -2 28 3.00 3.00 1 2 28 4.10 3.30 -1 2 -28 4.10 3.10 -1 2 -28 1.30 3.60 -2 -3 28 0.10 3.00 2 -3 -28 -1.00 2.50 2 -3 -28 0.60 2.40 2 3 -28 -0.10 2.50 -2 3 28 -0.30 2.50 2 3 -28 -2.80 2.20 1 -3 -28 -0.80 2.40 1 -3 -28 4.10 2.80 -1 -3 28 1.00 2.70 -1 -3 28 -0.20 2.30 1 3 -28 1.50 2.70 1 3 -28 -3.20 2.00 -1 3 28 1.90 2.90 0 -3 -28 9.40 3.60 0 -3 28 10.80 3.30 0 3 -28 4.00 2.90 0 3 28 13.80 4.20 0 3 -28 6.10 3.10 1 -3 28 19.10 4.70 -1 -3 -28 13.40 4.00 1 -3 28 12.90 3.40 -1 3 -28 12.80 4.00 1 3 28 13.70 4.40 -1 3 -28 14.30 4.00 2 -4 -28 9.50 3.40 2 -4 -28 1.60 3.70 2 4 -28 5.50 3.20 2 4 -28 3.50 3.30 -2 4 28 2.40 2.90 1 -4 -28 2.60 2.90 -1 -4 28 5.80 3.40 1 -4 -28 3.70 2.90 -1 -4 28 1.60 2.40 -1 -4 28 2.80 3.10 1 4 -28 2.60 3.00 1 4 -28 11.20 3.40 -1 4 28 -1.00 2.60 1 4 -28 2.90 2.80 0 -4 -28 -0.50 4.40 0 -4 28 3.20 2.60 0 4 28 4.80 3.40 0 4 -28 -0.70 2.50 0 4 -28 1.10 4.00 0 4 -28 1.00 3.10 1 -4 28 -1.50 2.60 -1 -4 -28 3.60 3.30 1 -4 28 1.70 2.70 -1 4 -28 1.30 2.90 1 4 28 2.30 3.30 -1 4 -28 1.70 3.00 2 -5 -28 0.20 2.90 2 -5 -28 -1.50 2.70 2 5 -28 0.40 3.40 -2 5 28 3.00 3.10 2 5 -28 -0.90 2.50 -1 -5 28 1.40 2.20 1 -5 -28 0.50 2.80 -1 -5 28 1.50 2.90 -1 5 28 -1.10 2.50 1 5 -28 0.50 2.70 1 5 -28 1.50 2.90 1 5 -28 0.60 2.60 0 -5 28 -0.20 3.70 0 -5 -28 -0.40 2.70 0 -5 28 -2.50 2.30 0 5 -28 0.30 3.70 0 5 28 0.00 2.90 0 5 -28 0.00 2.70 0 5 -28 4.40 3.20 2 0 -29 1.60 4.40 2 0 -29 -0.70 2.60 -2 0 29 -0.30 2.60 1 0 -29 4.70 2.90 1 0 -29 5.90 3.10 -1 0 29 4.40 3.30 0 0 29 4.00 3.20 0 0 -29 2.80 3.60 -1 0 -29 49.10 5.90 1 0 29 25.80 4.70 -1 0 -29 32.80 5.80 2 -1 -29 3.80 4.70 -2 -1 29 1.50 2.90 2 -1 -29 5.20 3.00 2 1 -29 2.00 2.70 -2 1 29 2.00 3.00 -1 -1 29 -0.10 2.70 1 -1 -29 1.60 2.70 1 -1 -29 0.00 2.50 -1 1 29 -0.70 3.10 1 1 -29 1.20 2.50 1 1 -29 0.10 2.30 0 -1 -29 4.90 3.50 0 -1 29 2.70 3.10 0 1 29 3.60 3.40 0 1 -29 3.10 3.40 1 -1 29 0.70 2.40 1 -1 29 -1.90 2.60 -1 -1 -29 -0.20 2.70 -1 1 -29 1.90 2.80 1 1 29 -0.40 2.70 -1 1 -29 -2.80 2.30 2 -2 -29 5.60 3.00 -2 -2 29 3.90 3.30 -2 2 29 9.00 3.90 2 2 -29 2.10 2.90 2 2 -29 1.90 2.70 -1 -2 29 5.40 3.10 1 -2 -29 4.50 3.00 1 -2 -29 3.40 3.00 -1 2 29 5.10 3.40 1 2 -29 6.90 3.40 1 2 -29 1.70 4.50 0 -2 29 10.60 4.00 0 -2 -29 7.10 3.30 0 -2 29 4.70 2.90 0 2 -29 3.30 3.00 0 2 -29 9.30 4.40 0 2 29 13.20 4.30 1 -2 29 0.60 2.80 1 -2 29 1.60 3.20 -1 -2 -29 2.40 3.00 1 2 29 -1.00 3.00 -1 2 -29 1.50 2.80 2 -3 -29 -1.50 2.70 -2 -3 29 0.20 2.90 2 -3 -29 1.90 3.00 -2 3 29 3.80 3.20 2 3 -29 0.10 2.60 -1 -3 29 1.90 3.00 1 -3 -29 5.90 3.10 1 3 -29 6.10 3.10 -1 3 29 12.90 4.40 1 3 -29 6.30 3.50 0 -3 -29 35.20 5.90 0 -3 29 36.90 5.40 0 -3 29 43.60 6.20 0 3 29 44.10 6.40 0 3 -29 35.60 5.70 0 3 -29 30.90 5.40 -1 -4 29 -0.40 2.70 1 -4 -29 -1.60 2.70 -1 -4 29 1.50 2.70 1 -4 -29 -0.90 2.40 -1 4 29 3.40 3.20 1 4 -29 1.60 2.90 1 4 -29 3.00 3.00 0 -4 29 3.40 3.10 0 -4 -29 7.80 3.70 0 4 29 14.20 4.40 0 4 -29 9.40 3.70 1 0 -30 6.00 3.20 -1 0 30 5.10 3.60 1 0 -30 8.20 3.30 0 0 -30 33.50 6.00 0 0 30 42.60 6.20 -1 -1 30 -1.60 2.70 1 -1 -30 2.80 3.20 1 -1 -30 1.90 2.70 1 1 -30 2.50 2.80 1 1 -30 2.10 2.90 -1 1 30 1.80 3.50 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 4489 _shelx_res_file ; TITL JTM1571_0m_a.res in P2(1) JTM1571_0m_a.res created by SHELXL-2019/1 at 07:09:39 on 15-Aug-2022 REM Old TITL JTM1571_0m in P2(1) REM SHELXT solution in P2(1): R1 0.099, Rweak 0.023, Alpha 0.001 REM 2.398 for 7 systematic absences, Orientation as input REM Flack x = 0.241 ( 0.358 ) from 2544 Parsons' quotients REM Formula found by SHELXT: C31 N6 O CELL 0.71073 5.5229 11.9579 22.5767 90.000 94.962 90.000 ZERR 2.000 0.0002 0.0005 0.0009 0.000 0.001 0.000 LATT -1 SYMM -X, 1/2+Y, -Z SFAC C H N O UNIT 58 88 16 2 TEMP -123 SIZE 0.044 0.236 0.427 L.S. 5 BOND $H LIST 4 FMAP 2 PLAN 5 TWIN MPLA C9 C10 N3 > N5 MPLA C1 > C7 N1 N2 MPLA C20 C21 N6 > N8 CONF EQIV $1 -x+1, y-1/2, -z+1 HTAB C2 O1_$1 EQIV $2 x-1, y, z HTAB C10 N5_$2 HTAB C19 O1_$1 ACTA 56.6 WGHT 0.046900 0.116600 BASF 0.24318 FVAR 0.80729 O1 4 0.516493 0.450335 0.464481 11.00000 0.02947 0.02862 = 0.04088 -0.00241 0.00461 0.00492 N1 3 0.842180 0.381620 0.415921 11.00000 0.02735 0.02209 = 0.03064 0.00234 0.00410 0.00140 N2 3 0.654626 0.266105 0.473151 11.00000 0.02516 0.02327 = 0.02836 0.00161 0.00242 -0.00155 N3 3 0.710531 0.489120 0.232036 11.00000 0.02765 0.03125 = 0.03338 0.00294 0.00123 0.00532 N4 3 0.952835 0.490115 0.230315 11.00000 0.02806 0.04293 = 0.03649 0.00464 0.00579 0.00314 N5 3 1.048301 0.487643 0.285794 11.00000 0.02679 0.03943 = 0.03716 0.00456 0.00526 0.00054 N6 3 0.778939 0.261194 0.663056 11.00000 0.02517 0.02907 = 0.02831 -0.00163 0.00128 -0.00424 N7 3 0.544051 0.254148 0.672788 11.00000 0.02720 0.06054 = 0.03313 -0.00567 0.00411 -0.00840 N8 3 0.420460 0.242096 0.620513 11.00000 0.02542 0.05527 = 0.03263 -0.00652 0.00434 -0.00580 C1 1 0.832525 0.204182 0.447908 11.00000 0.02503 0.02628 = 0.02631 -0.00121 -0.00204 0.00052 C2 1 0.897827 0.092477 0.453730 11.00000 0.03695 0.02405 = 0.03249 -0.00060 -0.00521 -0.00100 AFIX 43 H2 2 0.816702 0.042829 0.478248 11.00000 -1.20000 AFIX 0 C3 1 1.088216 0.056781 0.421839 11.00000 0.04260 0.02606 = 0.03702 -0.00649 -0.00609 0.00722 AFIX 43 H3 2 1.138081 -0.019205 0.424677 11.00000 -1.20000 AFIX 0 C4 1 1.207033 0.128957 0.386076 11.00000 0.03493 0.03924 = 0.03393 -0.01041 -0.00135 0.00893 AFIX 43 H4 2 1.337097 0.101465 0.365294 11.00000 -1.20000 AFIX 0 C5 1 1.139807 0.241383 0.379878 11.00000 0.03011 0.03379 = 0.02834 -0.00221 0.00194 0.00166 AFIX 43 H5 2 1.219570 0.290810 0.354969 11.00000 -1.20000 AFIX 0 C6 1 0.952255 0.276925 0.411668 11.00000 0.02486 0.02477 = 0.02637 -0.00151 -0.00238 0.00146 C7 1 0.655655 0.375033 0.452793 11.00000 0.02336 0.02562 = 0.02705 -0.00194 -0.00109 -0.00110 C8 1 0.918229 0.485046 0.388862 11.00000 0.02834 0.02433 = 0.03266 0.00211 -0.00020 -0.00280 AFIX 23 H8A 2 1.094756 0.495617 0.398973 11.00000 -1.20000 H8B 2 0.832786 0.548675 0.405854 11.00000 -1.20000 AFIX 0 C9 1 0.867297 0.486135 0.322692 11.00000 0.02300 0.02335 = 0.03443 0.00507 0.00376 0.00022 C10 1 0.649663 0.487103 0.288382 11.00000 0.02498 0.03311 = 0.03349 0.00379 0.00433 0.00196 AFIX 43 H10 2 0.490916 0.486484 0.301568 11.00000 -1.20000 AFIX 0 C11 1 0.550063 0.495582 0.177284 11.00000 0.03804 0.03655 = 0.03319 -0.00125 -0.00417 0.00791 AFIX 23 H11A 2 0.424118 0.436762 0.177800 11.00000 -1.20000 H11B 2 0.645578 0.481045 0.142950 11.00000 -1.20000 AFIX 0 C12 1 0.427843 0.608391 0.169482 11.00000 0.02924 0.03251 = 0.03256 0.00334 0.00045 0.00309 AFIX 23 H12A 2 0.553863 0.666846 0.167562 11.00000 -1.20000 H12B 2 0.337533 0.624078 0.204577 11.00000 -1.20000 AFIX 0 C13 1 0.252912 0.614681 0.113554 11.00000 0.03303 0.03291 = 0.03122 -0.00011 0.00022 0.00377 AFIX 23 H13A 2 0.347180 0.612977 0.078210 11.00000 -1.20000 H13B 2 0.145729 0.548191 0.111835 11.00000 -1.20000 AFIX 0 C14 1 0.096959 0.719739 0.111399 11.00000 0.03149 0.03119 = 0.03405 -0.00082 -0.00148 0.00274 AFIX 23 H14A 2 0.205307 0.785813 0.114617 11.00000 -1.20000 H14B 2 0.000482 0.720037 0.146372 11.00000 -1.20000 AFIX 0 C15 1 -0.075760 0.731328 0.055446 11.00000 0.03459 0.03391 = 0.03265 -0.00102 -0.00186 0.00344 AFIX 23 H15A 2 0.020707 0.736967 0.020592 11.00000 -1.20000 H15B 2 -0.176824 0.663028 0.050563 11.00000 -1.20000 AFIX 0 C16 1 -0.241710 0.832631 0.056452 11.00000 0.03367 0.03344 = 0.03593 0.00156 -0.00176 0.00260 AFIX 23 H16A 2 -0.140055 0.900797 0.060959 11.00000 -1.20000 H16B 2 -0.335843 0.827341 0.091726 11.00000 -1.20000 AFIX 0 C17 1 -0.418697 0.845273 0.001213 11.00000 0.04369 0.04254 = 0.03768 0.00322 -0.00517 0.00809 AFIX 23 H17A 2 -0.325170 0.855305 -0.033890 11.00000 -1.20000 H17B 2 -0.514793 0.775659 -0.004678 11.00000 -1.20000 AFIX 0 C18 1 -0.590922 0.943098 0.004974 11.00000 0.04575 0.04432 = 0.04523 0.00951 -0.00046 0.01089 AFIX 137 H18A 2 -0.697235 0.948212 -0.031997 11.00000 -1.50000 H18B 2 -0.497132 1.012380 0.010853 11.00000 -1.50000 H18C 2 -0.689828 0.931993 0.038498 11.00000 -1.50000 AFIX 0 C19 1 0.485650 0.226107 0.513946 11.00000 0.02554 0.03173 = 0.02906 0.00162 0.00119 -0.00701 AFIX 23 H19A 2 0.453376 0.145736 0.506273 11.00000 -1.20000 H19B 2 0.329889 0.266739 0.506328 11.00000 -1.20000 AFIX 0 C20 1 0.577533 0.241091 0.577825 11.00000 0.02444 0.02307 = 0.02990 -0.00014 0.00328 -0.00147 C21 1 0.808161 0.252523 0.604653 11.00000 0.02360 0.02610 = 0.02833 0.00035 0.00343 -0.00115 AFIX 43 H21 2 0.956179 0.254009 0.586136 11.00000 -1.20000 AFIX 0 C22 1 0.961681 0.280572 0.712864 11.00000 0.03211 0.03307 = 0.02716 0.00027 -0.00464 -0.00684 AFIX 23 H22A 2 1.096178 0.226424 0.710619 11.00000 -1.20000 H22B 2 0.887647 0.267285 0.750639 11.00000 -1.20000 AFIX 0 C23 1 1.063950 0.398882 0.713014 11.00000 0.03009 0.02935 = 0.02909 -0.00112 -0.00190 -0.00308 AFIX 23 H23A 2 1.146748 0.411157 0.676381 11.00000 -1.20000 H23B 2 0.929314 0.453473 0.713353 11.00000 -1.20000 AFIX 0 C24 1 1.242909 0.417557 0.767061 11.00000 0.03256 0.03102 = 0.02950 -0.00158 -0.00103 -0.00502 AFIX 23 H24A 2 1.356372 0.353377 0.771095 11.00000 -1.20000 H24B 2 1.152369 0.419553 0.803024 11.00000 -1.20000 AFIX 0 C25 1 1.389877 0.525116 0.764211 11.00000 0.03171 0.03133 = 0.03665 -0.00105 -0.00140 -0.00653 AFIX 23 H25A 2 1.478246 0.524128 0.727887 11.00000 -1.20000 H25B 2 1.277315 0.589698 0.761315 11.00000 -1.20000 AFIX 0 C26 1 1.571762 0.540237 0.818286 11.00000 0.03423 0.03361 = 0.03813 -0.00144 -0.00226 -0.00675 AFIX 23 H26A 2 1.677894 0.473452 0.822144 11.00000 -1.20000 H26B 2 1.481523 0.544120 0.854257 11.00000 -1.20000 AFIX 0 C27 1 1.731414 0.643933 0.816324 11.00000 0.03379 0.03333 = 0.04425 -0.00267 -0.00216 -0.00682 AFIX 23 H27A 2 1.819955 0.641269 0.780050 11.00000 -1.20000 H27B 2 1.626618 0.711228 0.813756 11.00000 -1.20000 AFIX 0 C28 1 1.913948 0.654070 0.870380 11.00000 0.04234 0.03972 = 0.04802 -0.00342 -0.00531 -0.01022 AFIX 23 H28A 2 1.824831 0.657064 0.906555 11.00000 -1.20000 H28B 2 2.017259 0.586294 0.873072 11.00000 -1.20000 AFIX 0 C29 1 2.076166 0.756372 0.869099 11.00000 0.04355 0.04272 = 0.06488 -0.00773 -0.00939 -0.01246 AFIX 137 H29A 2 2.192124 0.756753 0.904500 11.00000 -1.50000 H29B 2 1.976150 0.824116 0.868607 11.00000 -1.50000 H29C 2 2.164945 0.754289 0.833362 11.00000 -1.50000 AFIX 0 HKLF 4 REM JTM1571_0m_a.res in P2(1) REM wR2 = 0.0900, GooF = S = 1.049, Restrained GooF = 1.049 for all data REM R1 = 0.0356 for 6607 Fo > 4sig(Fo) and 0.0422 for all 7403 data REM 346 parameters refined using 1 restraints END WGHT 0.0469 0.1166 REM Highest difference peak 0.211, deepest hole -0.150, 1-sigma level 0.031 Q1 1 0.8720 0.4840 0.3516 11.00000 0.05 0.21 Q2 1 0.6929 0.2318 0.5840 11.00000 0.05 0.19 Q3 1 0.5550 0.2377 0.5500 11.00000 0.05 0.18 Q4 1 0.8034 0.2484 0.6318 11.00000 0.05 0.15 Q5 1 0.7624 0.4595 0.3109 11.00000 0.05 0.15 ; _shelx_res_checksum 94194 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O O1 0.5165(2) 0.45034(11) 0.46448(6) 0.0329(3) Uani d 1 . . N N1 0.8422(3) 0.38162(12) 0.41592(6) 0.0266(3) Uani d 1 . . N N2 0.6546(3) 0.26610(12) 0.47315(6) 0.0256(3) Uani d 1 . . N N3 0.7105(3) 0.48912(14) 0.23204(7) 0.0308(3) Uani d 1 . . N N4 0.9528(3) 0.49012(15) 0.23032(7) 0.0357(4) Uani d 1 . . N N5 1.0483(3) 0.48764(14) 0.28579(7) 0.0343(4) Uani d 1 . . N N6 0.7789(3) 0.26119(13) 0.66306(6) 0.0276(3) Uani d 1 . . N N7 0.5441(3) 0.25415(17) 0.67279(7) 0.0402(4) Uani d 1 . . N N8 0.4205(3) 0.24210(16) 0.62051(7) 0.0377(4) Uani d 1 . . C C1 0.8325(3) 0.20418(14) 0.44791(8) 0.0261(4) Uani d 1 . . C C2 0.8978(4) 0.09248(15) 0.45373(9) 0.0316(4) Uani d 1 . . H H2 0.816702 0.042829 0.478248 0.038 Uiso calc 1 . . C C3 1.0882(4) 0.05678(16) 0.42184(9) 0.0358(4) Uani d 1 . . H H3 1.138081 -0.019205 0.424677 0.043 Uiso calc 1 . . C C4 1.2070(4) 0.12896(17) 0.38608(9) 0.0363(4) Uani d 1 . . H H4 1.337097 0.101465 0.365294 0.044 Uiso calc 1 . . C C5 1.1398(3) 0.24138(16) 0.37988(8) 0.0308(4) Uani d 1 . . H H5 1.219570 0.290810 0.354969 0.037 Uiso calc 1 . . C C6 0.9523(3) 0.27692(14) 0.41167(7) 0.0256(3) Uani d 1 . . C C7 0.6557(3) 0.37503(15) 0.45279(7) 0.0255(3) Uani d 1 . . C C8 0.9182(3) 0.48505(15) 0.38886(8) 0.0286(4) Uani d 1 . . H H8A 1.094756 0.495617 0.398973 0.034 Uiso calc 1 . . H H8B 0.832786 0.548675 0.405854 0.034 Uiso calc 1 . . C C9 0.8673(3) 0.48614(15) 0.32269(8) 0.0269(3) Uani d 1 . . C C10 0.6497(3) 0.48710(16) 0.28838(8) 0.0304(4) Uani d 1 . . H H10 0.490916 0.486484 0.301568 0.037 Uiso calc 1 . . C C11 0.5501(4) 0.49558(17) 0.17728(9) 0.0363(4) Uani d 1 . . H H11A 0.424118 0.436762 0.177800 0.044 Uiso calc 1 . . H H11B 0.645578 0.481045 0.142950 0.044 Uiso calc 1 . . C C12 0.4278(3) 0.60839(16) 0.16948(8) 0.0316(4) Uani d 1 . . H H12A 0.553863 0.666846 0.167562 0.038 Uiso calc 1 . . H H12B 0.337533 0.624078 0.204577 0.038 Uiso calc 1 . . C C13 0.2529(4) 0.61468(16) 0.11355(8) 0.0325(4) Uani d 1 . . H H13A 0.347180 0.612977 0.078210 0.039 Uiso calc 1 . . H H13B 0.145729 0.548191 0.111835 0.039 Uiso calc 1 . . C C14 0.0970(4) 0.71974(16) 0.11140(9) 0.0325(4) Uani d 1 . . H H14A 0.205307 0.785813 0.114617 0.039 Uiso calc 1 . . H H14B 0.000482 0.720037 0.146372 0.039 Uiso calc 1 . . C C15 -0.0758(4) 0.73133(16) 0.05545(9) 0.0340(4) Uani d 1 . . H H15A 0.020707 0.736967 0.020592 0.041 Uiso calc 1 . . H H15B -0.176824 0.663028 0.050563 0.041 Uiso calc 1 . . C C16 -0.2417(4) 0.83263(17) 0.05645(9) 0.0346(4) Uani d 1 . . H H16A -0.140055 0.900797 0.060959 0.042 Uiso calc 1 . . H H16B -0.335843 0.827341 0.091726 0.042 Uiso calc 1 . . C C17 -0.4187(4) 0.84527(18) 0.00121(9) 0.0418(5) Uani d 1 . . H H17A -0.325170 0.855305 -0.033890 0.050 Uiso calc 1 . . H H17B -0.514793 0.775659 -0.004678 0.050 Uiso calc 1 . . C C18 -0.5909(4) 0.9431(2) 0.00497(10) 0.0454(5) Uani d 1 . . H H18A -0.697235 0.948212 -0.031997 0.068 Uiso calc 1 . . H H18B -0.497132 1.012380 0.010853 0.068 Uiso calc 1 . . H H18C -0.689828 0.931993 0.038498 0.068 Uiso calc 1 . . C C19 0.4857(3) 0.22611(15) 0.51395(8) 0.0288(4) Uani d 1 . . H H19A 0.453376 0.145736 0.506273 0.035 Uiso calc 1 . . H H19B 0.329889 0.266739 0.506328 0.035 Uiso calc 1 . . C C20 0.5775(3) 0.24109(14) 0.57782(8) 0.0257(3) Uani d 1 . . C C21 0.8082(3) 0.25252(15) 0.60465(7) 0.0259(3) Uani d 1 . . H H21 0.956179 0.254009 0.586136 0.031 Uiso calc 1 . . C C22 0.9617(3) 0.28057(16) 0.71286(8) 0.0312(4) Uani d 1 . . H H22A 1.096178 0.226424 0.710619 0.037 Uiso calc 1 . . H H22B 0.887647 0.267285 0.750639 0.037 Uiso calc 1 . . C C23 1.0639(3) 0.39888(15) 0.71301(8) 0.0298(4) Uani d 1 . . H H23A 1.146748 0.411157 0.676381 0.036 Uiso calc 1 . . H H23B 0.929314 0.453473 0.713353 0.036 Uiso calc 1 . . C C24 1.2429(4) 0.41756(16) 0.76706(8) 0.0312(4) Uani d 1 . . H H24A 1.356372 0.353377 0.771095 0.037 Uiso calc 1 . . H H24B 1.152369 0.419553 0.803024 0.037 Uiso calc 1 . . C C25 1.3899(4) 0.52512(16) 0.76421(9) 0.0335(4) Uani d 1 . . H H25A 1.478246 0.524128 0.727887 0.040 Uiso calc 1 . . H H25B 1.277315 0.589698 0.761315 0.040 Uiso calc 1 . . C C26 1.5718(4) 0.54024(17) 0.81829(9) 0.0356(4) Uani d 1 . . H H26A 1.677894 0.473452 0.822144 0.043 Uiso calc 1 . . H H26B 1.481523 0.544120 0.854257 0.043 Uiso calc 1 . . C C27 1.7314(4) 0.64393(17) 0.81632(9) 0.0374(4) Uani d 1 . . H H27A 1.819955 0.641269 0.780050 0.045 Uiso calc 1 . . H H27B 1.626618 0.711228 0.813756 0.045 Uiso calc 1 . . C C28 1.9139(4) 0.65407(19) 0.87038(10) 0.0439(5) Uani d 1 . . H H28A 1.824831 0.657064 0.906555 0.053 Uiso calc 1 . . H H28B 2.017259 0.586294 0.873072 0.053 Uiso calc 1 . . C C29 2.0762(4) 0.7564(2) 0.86910(11) 0.0512(6) Uani d 1 . . H H29A 2.192124 0.756753 0.904500 0.077 Uiso calc 1 . . H H29B 1.976150 0.824116 0.868607 0.077 Uiso calc 1 . . H H29C 2.164945 0.754289 0.833362 0.077 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.0295(7) 0.0286(6) 0.0409(8) 0.0049(5) 0.0046(6) -0.0024(6) N1 0.0274(7) 0.0221(7) 0.0306(8) 0.0014(6) 0.0041(6) 0.0023(6) N2 0.0252(7) 0.0233(7) 0.0284(7) -0.0016(6) 0.0024(6) 0.0016(6) N3 0.0276(7) 0.0312(8) 0.0334(8) 0.0053(7) 0.0012(6) 0.0029(7) N4 0.0281(8) 0.0429(9) 0.0365(9) 0.0031(7) 0.0058(7) 0.0046(8) N5 0.0268(7) 0.0394(9) 0.0372(9) 0.0005(7) 0.0053(7) 0.0046(7) N6 0.0252(7) 0.0291(7) 0.0283(7) -0.0042(6) 0.0013(6) -0.0016(6) N7 0.0272(8) 0.0605(11) 0.0331(8) -0.0084(8) 0.0041(7) -0.0057(8) N8 0.0254(8) 0.0553(11) 0.0326(8) -0.0058(7) 0.0043(6) -0.0065(8) C1 0.0250(8) 0.0263(8) 0.0263(9) 0.0005(7) -0.0020(7) -0.0012(7) C2 0.0370(10) 0.0240(8) 0.0325(10) -0.0010(8) -0.0052(8) -0.0006(7) C3 0.0426(11) 0.0261(9) 0.0370(11) 0.0072(8) -0.0061(9) -0.0065(8) C4 0.0349(10) 0.0392(11) 0.0339(10) 0.0089(8) -0.0013(8) -0.0104(8) C5 0.0301(9) 0.0338(10) 0.0283(9) 0.0017(7) 0.0019(7) -0.0022(7) C6 0.0249(8) 0.0248(8) 0.0264(8) 0.0015(7) -0.0024(7) -0.0015(7) C7 0.0234(8) 0.0256(8) 0.0271(8) -0.0011(7) -0.0011(7) -0.0019(7) C8 0.0283(8) 0.0243(8) 0.0327(9) -0.0028(7) -0.0002(7) 0.0021(7) C9 0.0230(8) 0.0234(7) 0.0344(9) 0.0002(7) 0.0038(7) 0.0051(7) C10 0.0250(8) 0.0331(9) 0.0335(9) 0.0020(8) 0.0043(7) 0.0038(8) C11 0.0380(10) 0.0366(10) 0.0332(10) 0.0079(9) -0.0042(8) -0.0013(8) C12 0.0292(9) 0.0325(9) 0.0326(9) 0.0031(7) 0.0005(8) 0.0033(7) C13 0.0330(10) 0.0329(10) 0.0312(9) 0.0038(7) 0.0002(8) -0.0001(7) C14 0.0315(9) 0.0312(9) 0.0341(10) 0.0027(8) -0.0015(8) -0.0008(7) C15 0.0346(10) 0.0339(10) 0.0326(10) 0.0034(8) -0.0019(8) -0.0010(7) C16 0.0337(10) 0.0334(9) 0.0359(10) 0.0026(8) -0.0018(8) 0.0016(8) C17 0.0437(12) 0.0425(12) 0.0377(11) 0.0081(9) -0.0052(9) 0.0032(9) C18 0.0457(12) 0.0443(12) 0.0452(13) 0.0109(10) -0.0005(10) 0.0095(10) C19 0.0255(8) 0.0317(9) 0.0291(9) -0.0070(7) 0.0012(7) 0.0016(7) C20 0.0244(8) 0.0231(8) 0.0299(9) -0.0015(6) 0.0033(7) -0.0001(6) C21 0.0236(8) 0.0261(8) 0.0283(8) -0.0012(7) 0.0034(7) 0.0004(7) C22 0.0321(9) 0.0331(9) 0.0272(9) -0.0068(8) -0.0046(7) 0.0003(7) C23 0.0301(9) 0.0294(9) 0.0291(9) -0.0031(7) -0.0019(7) -0.0011(7) C24 0.0326(10) 0.0310(9) 0.0295(9) -0.0050(7) -0.0010(8) -0.0016(7) C25 0.0317(10) 0.0313(9) 0.0367(11) -0.0065(8) -0.0014(8) -0.0010(8) C26 0.0342(10) 0.0336(10) 0.0381(11) -0.0068(8) -0.0023(9) -0.0014(8) C27 0.0338(10) 0.0333(10) 0.0443(11) -0.0068(8) -0.0022(9) -0.0027(9) C28 0.0423(12) 0.0397(11) 0.0480(12) -0.0102(10) -0.0053(10) -0.0034(9) C29 0.0436(12) 0.0427(12) 0.0649(15) -0.0125(10) -0.0094(11) -0.0077(11) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C7 N1 C6 . . 109.97(14) ? C7 N1 C8 . . 123.91(14) ? C6 N1 C8 . . 126.02(14) ? C7 N2 C1 . . 110.01(14) ? C7 N2 C19 . . 122.99(15) ? C1 N2 C19 . . 126.99(15) ? N4 N3 C10 . . 111.05(15) ? N4 N3 C11 . . 120.59(15) ? C10 N3 C11 . . 128.28(15) ? N5 N4 N3 . . 106.89(14) ? N4 N5 C9 . . 109.21(15) ? N7 N6 C21 . . 110.88(14) ? N7 N6 C22 . . 119.89(14) ? C21 N6 C22 . . 129.19(15) ? N8 N7 N6 . . 107.11(15) ? N7 N8 C20 . . 108.94(15) ? C2 C1 N2 . . 131.37(18) ? C2 C1 C6 . . 121.48(17) ? N2 C1 C6 . . 107.15(15) ? C1 C2 C3 . . 116.63(18) ? C1 C2 H2 . . 121.7 ? C3 C2 H2 . . 121.7 ? C4 C3 C2 . . 121.84(17) ? C4 C3 H3 . . 119.1 ? C2 C3 H3 . . 119.1 ? C3 C4 C5 . . 121.48(18) ? C3 C4 H4 . . 119.3 ? C5 C4 H4 . . 119.3 ? C6 C5 C4 . . 116.72(18) ? C6 C5 H5 . . 121.6 ? C4 C5 H5 . . 121.6 ? C5 C6 N1 . . 131.52(16) ? C5 C6 C1 . . 121.85(16) ? N1 C6 C1 . . 106.63(15) ? O1 C7 N2 . . 126.84(16) ? O1 C7 N1 . . 126.95(16) ? N2 C7 N1 . . 106.20(14) ? N1 C8 C9 . . 112.95(15) ? N1 C8 H8A . . 109.0 ? C9 C8 H8A . . 109.0 ? N1 C8 H8B . . 109.0 ? C9 C8 H8B . . 109.0 ? H8A C8 H8B . . 107.8 ? N5 C9 C10 . . 108.03(16) ? N5 C9 C8 . . 121.92(16) ? C10 C9 C8 . . 130.05(16) ? N3 C10 C9 . . 104.82(15) ? N3 C10 H10 . . 127.6 ? C9 C10 H10 . . 127.6 ? N3 C11 C12 . . 112.22(15) ? N3 C11 H11A . . 109.2 ? C12 C11 H11A . . 109.2 ? N3 C11 H11B . . 109.2 ? C12 C11 H11B . . 109.2 ? H11A C11 H11B . . 107.9 ? C11 C12 C13 . . 112.66(15) ? C11 C12 H12A . . 109.1 ? C13 C12 H12A . . 109.1 ? C11 C12 H12B . . 109.1 ? C13 C12 H12B . . 109.1 ? H12A C12 H12B . . 107.8 ? C14 C13 C12 . . 112.57(15) ? C14 C13 H13A . . 109.1 ? C12 C13 H13A . . 109.1 ? C14 C13 H13B . . 109.1 ? C12 C13 H13B . . 109.1 ? H13A C13 H13B . . 107.8 ? C13 C14 C15 . . 114.46(15) ? C13 C14 H14A . . 108.6 ? C15 C14 H14A . . 108.6 ? C13 C14 H14B . . 108.6 ? C15 C14 H14B . . 108.6 ? H14A C14 H14B . . 107.6 ? C16 C15 C14 . . 113.30(16) ? C16 C15 H15A . . 108.9 ? C14 C15 H15A . . 108.9 ? C16 C15 H15B . . 108.9 ? C14 C15 H15B . . 108.9 ? H15A C15 H15B . . 107.7 ? C15 C16 C17 . . 114.31(17) ? C15 C16 H16A . . 108.7 ? C17 C16 H16A . . 108.7 ? C15 C16 H16B . . 108.7 ? C17 C16 H16B . . 108.7 ? H16A C16 H16B . . 107.6 ? C18 C17 C16 . . 113.09(17) ? C18 C17 H17A . . 109.0 ? C16 C17 H17A . . 109.0 ? C18 C17 H17B . . 109.0 ? C16 C17 H17B . . 109.0 ? H17A C17 H17B . . 107.8 ? C17 C18 H18A . . 109.5 ? C17 C18 H18B . . 109.5 ? H18A C18 H18B . . 109.5 ? C17 C18 H18C . . 109.5 ? H18A C18 H18C . . 109.5 ? H18B C18 H18C . . 109.5 ? N2 C19 C20 . . 112.93(14) ? N2 C19 H19A . . 109.0 ? C20 C19 H19A . . 109.0 ? N2 C19 H19B . . 109.0 ? C20 C19 H19B . . 109.0 ? H19A C19 H19B . . 107.8 ? N8 C20 C21 . . 108.28(16) ? N8 C20 C19 . . 120.19(15) ? C21 C20 C19 . . 131.51(16) ? N6 C21 C20 . . 104.79(15) ? N6 C21 H21 . . 127.6 ? C20 C21 H21 . . 127.6 ? N6 C22 C23 . . 112.32(14) ? N6 C22 H22A . . 109.1 ? C23 C22 H22A . . 109.1 ? N6 C22 H22B . . 109.1 ? C23 C22 H22B . . 109.1 ? H22A C22 H22B . . 107.9 ? C24 C23 C22 . . 110.72(15) ? C24 C23 H23A . . 109.5 ? C22 C23 H23A . . 109.5 ? C24 C23 H23B . . 109.5 ? C22 C23 H23B . . 109.5 ? H23A C23 H23B . . 108.1 ? C23 C24 C25 . . 113.69(15) ? C23 C24 H24A . . 108.8 ? C25 C24 H24A . . 108.8 ? C23 C24 H24B . . 108.8 ? C25 C24 H24B . . 108.8 ? H24A C24 H24B . . 107.7 ? C26 C25 C24 . . 112.51(16) ? C26 C25 H25A . . 109.1 ? C24 C25 H25A . . 109.1 ? C26 C25 H25B . . 109.1 ? C24 C25 H25B . . 109.1 ? H25A C25 H25B . . 107.8 ? C25 C26 C27 . . 114.60(17) ? C25 C26 H26A . . 108.6 ? C27 C26 H26A . . 108.6 ? C25 C26 H26B . . 108.6 ? C27 C26 H26B . . 108.6 ? H26A C26 H26B . . 107.6 ? C28 C27 C26 . . 112.76(17) ? C28 C27 H27A . . 109.0 ? C26 C27 H27A . . 109.0 ? C28 C27 H27B . . 109.0 ? C26 C27 H27B . . 109.0 ? H27A C27 H27B . . 107.8 ? C29 C28 C27 . . 113.62(19) ? C29 C28 H28A . . 108.8 ? C27 C28 H28A . . 108.8 ? C29 C28 H28B . . 108.8 ? C27 C28 H28B . . 108.8 ? H28A C28 H28B . . 107.7 ? C28 C29 H29A . . 109.5 ? C28 C29 H29B . . 109.5 ? H29A C29 H29B . . 109.5 ? C28 C29 H29C . . 109.5 ? H29A C29 H29C . . 109.5 ? H29B C29 H29C . . 109.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag O1 C7 . 1.227(2) ? N1 C7 . 1.382(2) ? N1 C6 . 1.399(2) ? N1 C8 . 1.457(2) ? N2 C7 . 1.381(2) ? N2 C1 . 1.391(2) ? N2 C19 . 1.448(2) ? N3 N4 . 1.342(2) ? N3 C10 . 1.344(2) ? N3 C11 . 1.459(2) ? N4 N5 . 1.317(2) ? N5 C9 . 1.356(2) ? N6 N7 . 1.337(2) ? N6 C21 . 1.346(2) ? N6 C22 . 1.463(2) ? N7 N8 . 1.319(2) ? N8 C20 . 1.351(2) ? C1 C2 . 1.387(2) ? C1 C6 . 1.399(2) ? C2 C3 . 1.392(3) ? C2 H2 . 0.9500 ? C3 C4 . 1.385(3) ? C3 H3 . 0.9500 ? C4 C5 . 1.399(3) ? C4 H4 . 0.9500 ? C5 C6 . 1.377(3) ? C5 H5 . 0.9500 ? C8 C9 . 1.496(3) ? C8 H8A . 0.9900 ? C8 H8B . 0.9900 ? C9 C10 . 1.373(2) ? C10 H10 . 0.9500 ? C11 C12 . 1.512(3) ? C11 H11A . 0.9900 ? C11 H11B . 0.9900 ? C12 C13 . 1.524(3) ? C12 H12A . 0.9900 ? C12 H12B . 0.9900 ? C13 C14 . 1.522(3) ? C13 H13A . 0.9900 ? C13 H13B . 0.9900 ? C14 C15 . 1.522(2) ? C14 H14A . 0.9900 ? C14 H14B . 0.9900 ? C15 C16 . 1.520(3) ? C15 H15A . 0.9900 ? C15 H15B . 0.9900 ? C16 C17 . 1.524(3) ? C16 H16A . 0.9900 ? C16 H16B . 0.9900 ? C17 C18 . 1.515(3) ? C17 H17A . 0.9900 ? C17 H17B . 0.9900 ? C18 H18A . 0.9800 ? C18 H18B . 0.9800 ? C18 H18C . 0.9800 ? C19 C20 . 1.498(2) ? C19 H19A . 0.9900 ? C19 H19B . 0.9900 ? C20 C21 . 1.369(2) ? C21 H21 . 0.9500 ? C22 C23 . 1.523(3) ? C22 H22A . 0.9900 ? C22 H22B . 0.9900 ? C23 C24 . 1.519(2) ? C23 H23A . 0.9900 ? C23 H23B . 0.9900 ? C24 C25 . 1.525(3) ? C24 H24A . 0.9900 ? C24 H24B . 0.9900 ? C25 C26 . 1.523(3) ? C25 H25A . 0.9900 ? C25 H25B . 0.9900 ? C26 C27 . 1.524(3) ? C26 H26A . 0.9900 ? C26 H26B . 0.9900 ? C27 C28 . 1.519(3) ? C27 H27A . 0.9900 ? C27 H27B . 0.9900 ? C28 C29 . 1.518(3) ? C28 H28A . 0.9900 ? C28 H28B . 0.9900 ? C29 H29A . 0.9800 ? C29 H29B . 0.9800 ? C29 H29C . 0.9800 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C2 H2 O1 2_646 0.95 2.59 3.502(2) 162 yes C10 H10 N5 1_455 0.95 2.44 3.317(2) 153 yes C19 H19A O1 2_646 0.99 2.43 3.334(2) 152 yes C21 H21 N8 1_655 0.95 2.62 3.372(2) 137 y C22 H22A Cg2 2_746 0.99 2.89 3.664(2) 135 y loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C10 N3 N4 N5 . . . . 0.6(2) ? C11 N3 N4 N5 . . . . 177.67(15) ? N3 N4 N5 C9 . . . . -0.6(2) ? C21 N6 N7 N8 . . . . -0.7(2) ? C22 N6 N7 N8 . . . . 177.02(16) ? N6 N7 N8 C20 . . . . 0.2(2) ? C7 N2 C1 C2 . . . . -178.80(18) ? C19 N2 C1 C2 . . . . 0.0(3) ? C7 N2 C1 C6 . . . . 1.31(19) ? C19 N2 C1 C6 . . . . -179.84(15) ? N2 C1 C2 C3 . . . . -179.77(18) ? C6 C1 C2 C3 . . . . 0.1(3) ? C1 C2 C3 C4 . . . . 0.0(3) ? C2 C3 C4 C5 . . . . -0.5(3) ? C3 C4 C5 C6 . . . . 0.9(3) ? C4 C5 C6 N1 . . . . 179.66(17) ? C4 C5 C6 C1 . . . . -0.7(3) ? C7 N1 C6 C5 . . . . 178.61(18) ? C8 N1 C6 C5 . . . . -4.8(3) ? C7 N1 C6 C1 . . . . -1.08(18) ? C8 N1 C6 C1 . . . . 175.52(16) ? C2 C1 C6 C5 . . . . 0.2(3) ? N2 C1 C6 C5 . . . . -179.86(15) ? C2 C1 C6 N1 . . . . 179.96(16) ? N2 C1 C6 N1 . . . . -0.14(18) ? C1 N2 C7 O1 . . . . 177.12(17) ? C19 N2 C7 O1 . . . . -1.8(3) ? C1 N2 C7 N1 . . . . -1.95(18) ? C19 N2 C7 N1 . . . . 179.15(14) ? C6 N1 C7 O1 . . . . -177.20(17) ? C8 N1 C7 O1 . . . . 6.1(3) ? C6 N1 C7 N2 . . . . 1.86(18) ? C8 N1 C7 N2 . . . . -174.83(15) ? C7 N1 C8 C9 . . . . -113.03(18) ? C6 N1 C8 C9 . . . . 70.8(2) ? N4 N5 C9 C10 . . . . 0.3(2) ? N4 N5 C9 C8 . . . . -179.02(16) ? N1 C8 C9 N5 . . . . -113.96(19) ? N1 C8 C9 C10 . . . . 66.8(2) ? N4 N3 C10 C9 . . . . -0.4(2) ? C11 N3 C10 C9 . . . . -177.17(17) ? N5 C9 C10 N3 . . . . 0.0(2) ? C8 C9 C10 N3 . . . . 179.31(18) ? N4 N3 C11 C12 . . . . -107.0(2) ? C10 N3 C11 C12 . . . . 69.6(2) ? N3 C11 C12 C13 . . . . -177.95(16) ? C11 C12 C13 C14 . . . . 169.67(17) ? C12 C13 C14 C15 . . . . 178.35(16) ? C13 C14 C15 C16 . . . . 175.90(17) ? C14 C15 C16 C17 . . . . -179.27(17) ? C15 C16 C17 C18 . . . . 176.78(18) ? C7 N2 C19 C20 . . . . -88.9(2) ? C1 N2 C19 C20 . . . . 92.4(2) ? N7 N8 C20 C21 . . . . 0.3(2) ? N7 N8 C20 C19 . . . . 178.80(16) ? N2 C19 C20 N8 . . . . 159.08(17) ? N2 C19 C20 C21 . . . . -22.8(3) ? N7 N6 C21 C20 . . . . 0.8(2) ? C22 N6 C21 C20 . . . . -176.61(16) ? N8 C20 C21 N6 . . . . -0.6(2) ? C19 C20 C21 N6 . . . . -178.96(17) ? N7 N6 C22 C23 . . . . -106.9(2) ? C21 N6 C22 C23 . . . . 70.3(2) ? N6 C22 C23 C24 . . . . 177.04(15) ? C22 C23 C24 C25 . . . . 168.59(16) ? C23 C24 C25 C26 . . . . -178.67(17) ? C24 C25 C26 C27 . . . . 177.38(17) ? C25 C26 C27 C28 . . . . -178.60(18) ? C26 C27 C28 C29 . . . . 179.6(2) ? _cod_database_fobs_code 2022949