#------------------------------------------------------------------------------
#$Date: 2023-10-20 04:06:54 +0200 (Fri, 20 Oct 2023) $
#$Revision: 287049 $
#$URL: svn://www.crystallography.net/cod/cif/2/02/29/2022919.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2022919
loop_
_publ_author_name
'Rharmili, Nohaila'
'Abdellaoui, Omar'
'Haoudi, Amal'
'Mague, Joel T.'
'H\"okelek, Tuncer'
'Ouazzani Chahdi, Fouad'
'Kandri Rodi, Youssef'
'Mazzah, Ahmed'
'Sebbar, Nada Kheira'
_publ_section_title
;
Synthesis, crystal structure and Hirshfeld surface analysis of
1-(12-bromododecyl)indoline-2,3-dione
;
_journal_coeditor_code HB8077
_journal_issue 11
_journal_name_full
'Acta Crystallographica Section E Crystallographic Communications'
_journal_paper_doi 10.1107/S2056989023009052
_journal_volume 79
_journal_year 2023
_chemical_formula_iupac 'C20 H28 Br N O2'
_chemical_formula_moiety 'C20 H28 Br N O2'
_chemical_formula_sum 'C20 H28 Br N O2'
_chemical_formula_weight 394.34
_chemical_name_systematic
;
1-(12-Bromododecyl)indoline-2,3-dione
;
_space_group_crystal_system monoclinic
_space_group_IT_number 14
_space_group_name_Hall '-P 2ybc'
_space_group_name_H-M_alt 'P 1 21/c 1'
_atom_sites_solution_hydrogens geom
_atom_sites_solution_primary dual
_atom_sites_solution_secondary difmap
_audit_creation_method SHELXL-2019/1
_cell_angle_alpha 90
_cell_angle_beta 105.2310(10)
_cell_angle_gamma 90
_cell_formula_units_Z 4
_cell_length_a 20.5385(5)
_cell_length_b 8.1977(2)
_cell_length_c 12.3185(3)
_cell_measurement_reflns_used 9620
_cell_measurement_temperature 150.(2)
_cell_measurement_theta_max 74.6592
_cell_measurement_theta_min 6.6070
_cell_volume 2001.19(8)
_computing_cell_refinement
;
SAINT (Bruker, 2021)
;
_computing_data_collection
;
APEX4 (Bruker, 2021)
;
_computing_data_reduction
;
SAINT (Bruker, 2021)
;
_computing_molecular_graphics
;
DIAMOND (Brandenburg & Putz, 2012)
;
_computing_publication_material
;
SHELXTL (Sheldrick, 2008)
;
_computing_structure_refinement
;
SHELXL2019/1 (Sheldrick, 2015b)
;
_computing_structure_solution
;
SHELXT (Sheldrick, 2015a)
;
_diffrn_ambient_temperature 150(2)
_diffrn_detector_area_resol_mean 7.3910
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device 'Bruker D8 VENTURE PHOTON 3 CPAD'
_diffrn_measurement_device_type 'Bruker D8 VENTURE PHOTON 3 CPAD'
_diffrn_measurement_method '\f and \w scans'
_diffrn_radiation_monochromator mirror
_diffrn_radiation_type CuK\a
_diffrn_radiation_wavelength 1.54178
_diffrn_reflns_av_R_equivalents 0.0380
_diffrn_reflns_av_unetI/netI 0.0200
_diffrn_reflns_limit_h_max 25
_diffrn_reflns_limit_h_min -25
_diffrn_reflns_limit_k_max 10
_diffrn_reflns_limit_k_min -10
_diffrn_reflns_limit_l_max 15
_diffrn_reflns_limit_l_min -15
_diffrn_reflns_number 42466
_diffrn_reflns_theta_full 74.700
_diffrn_reflns_theta_max 74.717
_diffrn_reflns_theta_min 5.841
_diffrn_source 'INCOATEC I\mS micro----focus source'
_diffrn_source_current 1.0
_diffrn_source_power 0.05
_diffrn_source_voltage 50
_exptl_absorpt_coefficient_mu 2.878
_exptl_absorpt_correction_T_max 0.87
_exptl_absorpt_correction_T_min 0.74
_exptl_absorpt_correction_type multi-scan
_exptl_absorpt_process_details
;
(SADABS; Krause et al., 2015)
;
_exptl_crystal_colour yellow
_exptl_crystal_density_diffrn 1.309
_exptl_crystal_density_method 'not measured'
_exptl_crystal_description column
_exptl_crystal_F_000 824
_exptl_crystal_size_max 0.228
_exptl_crystal_size_mid 0.068
_exptl_crystal_size_min 0.048
_refine_diff_density_max 0.441
_refine_diff_density_min -0.660
_refine_ls_extinction_method none
_refine_ls_goodness_of_fit_ref 1.060
_refine_ls_hydrogen_treatment constr
_refine_ls_matrix_type full
_refine_ls_number_parameters 217
_refine_ls_number_reflns 4091
_refine_ls_number_restraints 0
_refine_ls_restrained_S_all 1.060
_refine_ls_R_factor_all 0.0323
_refine_ls_R_factor_gt 0.0303
_refine_ls_shift/su_max 0.001
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0459P)^2^+0.8387P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.0822
_refine_ls_wR_factor_ref 0.0839
_reflns_number_gt 3810
_reflns_number_total 4091
_reflns_threshold_expression 'I > 2\s(I)'
_cod_data_source_file hb8077sup1.cif
_cod_data_source_block I
_cod_original_sg_symbol_H-M 'P 21/c'
_cod_database_code 2022919
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min 0.560
_shelx_estimated_absorpt_t_max 0.874
_shelx_hkl_file
;
0 0 -1 -0.20 0.40
0 0 1 3.50 0.80
0 0 1 0.00 0.40
0 0 3 1.30 1.30
0 0 -3 2.30 1.70
0 0 3 2.20 1.50
0 0 4 3206.08 105.19
0 0 -4 3057.59 106.19
0 0 -5 4.40 2.60
0 0 5 0.30 1.60
0 0 -6 1220.68 49.00
0 0 6 1225.78 47.10
0 0 7 1.60 2.30
0 0 -7 -3.00 1.90
0 0 8 107.69 13.40
0 0 -8 87.59 7.40
0 0 -8 89.19 13.10
0 0 -8 94.39 8.90
0 0 -8 85.29 6.70
0 0 -9 -4.20 2.50
0 0 -9 0.50 3.00
0 0 -9 0.20 2.50
0 0 -9 4.10 5.20
0 0 9 0.20 4.00
0 0 9 0.30 3.40
0 0 -9 3.40 2.80
0 0 -9 -2.30 3.10
0 0 -9 0.30 3.00
0 0 -9 -2.80 3.60
0 0 9 -2.00 3.60
0 0 -10 4.80 2.80
0 0 -10 2.80 2.80
0 0 10 4.40 4.00
0 0 10 7.60 3.10
0 0 -10 4.30 6.00
0 0 -10 4.80 3.50
0 0 -10 6.40 3.30
0 0 -10 12.30 4.10
0 0 -10 6.10 3.00
0 0 -10 -0.20 2.90
0 0 10 7.40 6.40
0 0 -11 3.40 2.80
0 0 -11 -0.20 2.80
0 0 -11 -0.40 8.00
0 0 -11 -10.50 3.20
0 0 -11 0.70 2.80
0 0 11 -4.90 3.90
0 0 11 -4.70 7.00
0 0 11 1.50 2.40
0 0 -11 -0.60 2.30
0 0 -11 2.70 2.90
0 0 -12 4.70 2.50
0 0 -12 5.90 2.80
0 0 12 8.50 2.70
0 0 -12 3.10 2.80
0 0 -12 6.00 3.00
0 0 -12 5.70 2.30
0 0 -13 1.20 1.80
0 0 13 -1.10 1.50
0 0 -13 -3.50 2.10
0 0 -13 -0.10 1.60
0 0 -13 -3.30 1.70
0 0 13 0.40 2.00
0 0 -13 3.80 2.40
0 0 -14 -1.40 2.20
0 0 14 0.40 1.30
0 0 -14 2.90 1.60
0 0 -14 7.30 2.70
0 0 -14 0.80 1.20
0 0 14 2.50 1.40
0 1 0 0.90 0.60
0 1 0 0.30 0.60
0 -1 0 1.00 0.50
0 1 2 257.27 11.10
0 1 2 265.17 11.90
0 1 -2 261.97 9.80
0 1 -2 268.57 9.80
0 -1 -2 262.87 11.90
0 -1 -2 266.97 11.40
0 1 3 602.24 24.10
0 1 3 607.44 23.10
0 1 -3 643.24 22.40
0 1 -3 569.04 22.00
0 -1 -3 582.24 23.00
0 -1 3 569.44 21.30
0 -1 -3 598.04 24.00
0 -1 3 620.04 21.60
0 1 -4 1412.26 48.80
0 1 4 1431.16 50.59
0 1 4 1405.36 49.30
0 1 -4 1253.27 48.60
0 -1 4 1393.36 48.00
0 -1 -4 1353.86 50.49
0 -1 -4 1352.36 48.80
0 1 -5 1507.25 56.39
0 1 5 1360.26 50.39
0 1 5 1348.77 51.49
0 1 -5 1356.06 50.19
0 -1 -5 1255.57 49.20
0 -1 -5 1377.16 52.19
0 -1 5 1356.66 49.30
0 1 6 358.66 19.00
0 1 6 337.47 23.00
0 1 -6 382.46 19.40
0 -1 6 381.06 18.40
0 -1 -6 358.86 20.50
0 1 7 574.64 28.00
0 1 -7 569.74 28.50
0 -1 7 583.64 27.30
0 -1 -7 579.04 30.30
0 1 8 316.07 20.50
0 1 -8 319.37 14.70
0 1 -8 312.77 15.00
0 1 -8 318.77 14.90
0 1 -8 307.17 21.00
0 1 -8 322.17 14.90
0 1 -8 312.67 15.00
0 1 -8 334.77 14.60
0 -1 -8 326.07 14.90
0 -1 8 347.87 20.50
0 -1 -8 316.47 14.70
0 -1 -8 355.46 23.80
0 -1 -8 312.27 14.40
0 1 -9 6.60 3.00
0 1 -9 3.20 3.00
0 1 -9 9.80 3.20
0 1 9 3.80 4.40
0 1 -9 6.10 3.10
0 1 9 4.70 2.70
0 1 9 0.60 5.00
0 1 -9 4.60 3.10
0 1 -9 0.80 3.80
0 1 -9 6.10 3.40
0 -1 -9 3.70 3.30
0 -1 -9 7.30 4.40
0 -1 -9 0.30 4.40
0 -1 9 -2.30 5.00
0 -1 -9 5.00 3.30
0 -1 -9 8.90 3.70
0 -1 -9 5.90 3.10
0 -1 -9 5.90 3.10
0 -1 9 0.80 3.80
0 -1 -9 7.00 3.00
0 1 -10 36.80 5.30
0 1 -10 44.70 10.70
0 1 -10 52.39 6.60
0 1 -10 57.49 7.10
0 1 10 38.50 10.70
0 1 10 42.90 6.40
0 1 -10 44.40 5.90
0 1 -10 48.10 5.30
0 1 -10 42.40 5.60
0 1 10 46.20 5.30
0 -1 -10 40.80 6.00
0 -1 10 41.30 5.80
0 -1 -10 48.20 6.30
0 -1 -10 47.10 5.90
0 -1 10 44.20 9.60
0 -1 -10 47.30 13.20
0 -1 -10 36.30 5.20
0 -1 10 43.70 6.40
0 -1 -10 48.30 5.70
0 -1 -10 36.90 5.00
0 1 -11 -4.10 6.40
0 1 -11 4.70 2.50
0 1 -11 3.30 2.80
0 1 -11 -1.90 2.90
0 1 -11 3.60 2.40
0 1 11 -0.80 4.40
0 1 -11 1.80 2.30
0 1 11 6.50 2.60
0 1 -11 0.80 2.60
0 1 11 3.50 2.90
0 -1 -11 4.60 3.00
0 -1 -11 -2.50 2.30
0 -1 -11 5.40 2.70
0 -1 -11 3.10 2.60
0 -1 -11 -3.00 3.00
0 -1 11 6.00 4.00
0 -1 -11 2.00 3.70
0 -1 11 2.70 3.10
0 -1 11 -1.00 6.40
0 1 -12 535.75 21.60
0 1 -12 521.75 22.00
0 1 12 533.45 20.40
0 1 -12 525.25 21.70
0 1 -12 556.14 21.30
0 1 -12 529.25 21.90
0 1 12 527.15 22.30
0 1 -12 522.75 21.80
0 -1 -12 535.15 21.80
0 -1 -12 498.35 21.10
0 -1 -12 523.75 21.30
0 -1 -12 519.75 21.90
0 -1 -12 520.75 20.60
0 -1 12 534.75 21.00
0 -1 -12 517.65 21.20
0 1 -13 5.30 2.40
0 1 -13 3.60 2.10
0 1 13 5.20 1.80
0 1 -13 4.10 1.80
0 1 -13 6.60 2.40
0 1 13 5.30 2.40
0 1 -13 7.20 2.30
0 -1 13 6.00 2.30
0 -1 13 6.10 2.20
0 -1 -13 2.70 1.90
0 -1 -13 3.00 2.20
0 -1 -13 14.10 2.90
0 -1 -13 0.20 3.00
0 1 -14 6.90 1.90
0 1 -14 4.60 1.60
0 1 -14 3.80 1.40
0 1 -14 1.40 1.70
0 1 14 4.90 1.80
0 1 -14 7.30 2.00
0 1 14 5.00 1.90
0 -1 14 6.90 1.80
0 -1 -14 8.50 2.00
0 -1 14 4.10 1.70
0 -1 -14 3.20 1.40
0 2 2 200.78 9.60
0 2 2 219.68 11.30
0 -2 -2 210.48 10.30
0 -2 -2 195.98 10.40
0 2 4 523.25 22.30
0 2 4 492.25 23.90
0 2 -4 572.34 21.20
0 -2 -4 526.95 23.80
0 -2 4 553.74 20.00
0 -2 4 483.35 19.70
0 -2 -4 514.25 22.70
0 2 5 458.35 21.40
0 2 5 454.65 23.20
0 2 -5 486.15 20.90
0 -2 -5 435.06 21.50
0 -2 -5 478.55 23.20
0 -2 5 464.75 19.60
0 -2 5 434.06 19.90
0 2 6 752.42 35.30
0 2 6 729.53 32.40
0 2 -6 774.12 32.00
0 -2 -6 699.33 32.40
0 -2 -6 760.42 34.80
0 -2 6 764.42 30.90
0 2 7 474.75 25.50
0 2 -7 498.75 25.30
0 -2 -7 510.65 28.40
0 -2 7 517.85 24.60
0 2 -8 5.50 4.20
0 2 -8 0.70 2.70
0 2 -8 9.10 3.60
0 2 -8 2.90 3.20
0 2 8 -2.00 4.80
0 2 -8 4.60 3.10
0 2 -8 9.60 3.20
0 2 -8 2.00 2.80
0 2 8 4.40 2.40
0 2 8 5.50 3.00
0 -2 -8 3.40 2.70
0 -2 -8 5.80 3.50
0 -2 8 -0.20 2.80
0 -2 -8 2.40 3.00
0 -2 -8 11.90 6.10
0 2 9 904.51 45.60
0 2 -9 894.71 35.40
0 2 -9 961.40 35.70
0 2 -9 964.10 34.80
0 2 9 869.31 35.50
0 2 -9 984.90 35.70
0 2 -9 998.60 36.10
0 2 -9 948.01 45.50
0 2 9 961.30 35.90
0 2 -9 950.70 35.40
0 2 9 951.30 33.90
0 2 -9 977.80 35.80
0 -2 -9 927.91 34.80
0 -2 -9 945.81 50.09
0 -2 -9 980.20 35.20
0 -2 -9 902.31 35.00
0 -2 -9 970.90 35.60
0 -2 -9 904.91 35.20
0 -2 9 996.80 43.80
0 2 -10 22.90 8.30
0 2 -10 19.40 4.40
0 2 10 17.40 3.20
0 2 -10 17.10 3.70
0 2 -10 20.90 4.40
0 2 -10 24.20 4.20
0 2 -10 17.70 4.20
0 2 10 16.50 4.30
0 2 -10 18.00 4.20
0 2 10 23.40 5.10
0 -2 -10 13.10 4.20
0 -2 10 20.50 7.40
0 -2 10 12.70 5.50
0 -2 -10 14.60 4.00
0 -2 -10 25.10 4.50
0 -2 -10 7.70 4.40
0 -2 -10 15.30 3.80
0 2 -11 69.39 6.80
0 2 -11 79.39 7.00
0 2 -11 76.89 6.80
0 2 -11 86.99 7.30
0 2 -11 68.59 6.70
0 2 -11 76.79 6.70
0 2 11 84.79 5.70
0 2 11 93.59 7.50
0 -2 -11 80.39 7.10
0 -2 11 69.59 7.50
0 -2 -11 76.09 7.00
0 -2 -11 79.49 6.60
0 -2 11 84.09 14.70
0 -2 -11 84.79 6.80
0 -2 -11 87.79 7.90
0 -2 11 76.99 7.30
0 2 -12 8.80 2.90
0 2 -12 8.00 2.50
0 2 -12 5.10 2.60
0 2 -12 8.50 2.70
0 2 12 5.00 2.60
0 2 -12 4.80 2.40
0 2 -12 5.90 2.20
0 2 12 6.90 1.90
0 -2 -12 5.20 2.40
0 -2 12 3.60 2.80
0 -2 -12 9.00 2.90
0 -2 -12 4.20 2.50
0 2 -13 139.89 7.90
0 2 13 133.39 7.60
0 2 -13 133.79 7.80
0 2 -13 138.19 7.00
0 2 -13 134.89 7.70
0 2 13 136.79 8.10
0 2 -13 131.29 7.60
0 -2 -13 138.79 7.60
0 -2 -13 142.89 7.60
0 -2 13 136.59 7.30
0 -2 -13 137.89 7.10
0 2 -14 -0.60 1.20
0 2 -14 1.50 1.30
0 2 -14 -2.70 1.40
0 2 14 -1.50 1.50
0 2 -14 -1.50 1.50
0 2 -14 0.20 1.20
0 2 14 -0.10 1.60
0 -2 14 0.60 1.30
0 -2 14 -1.60 1.10
0 -2 -14 -0.10 1.20
0 3 0 0.60 1.30
0 3 0 2.50 2.00
0 -3 0 2.30 1.60
0 -3 0 6.10 2.50
0 3 1 585.04 23.70
0 3 -1 583.24 21.50
0 3 -1 562.64 21.40
0 -3 1 540.75 20.10
0 -3 1 493.85 20.40
0 -3 -1 603.44 22.40
0 3 -2 714.73 26.00
0 3 2 704.03 29.80
0 -3 -2 738.23 28.80
0 3 3 116.09 9.70
0 3 -3 133.09 6.60
0 -3 -3 101.99 8.90
0 -3 -3 109.79 8.60
0 3 -4 1880.91 60.09
0 3 4 1614.54 61.99
0 3 4 1519.05 64.69
0 -3 4 1757.02 58.59
0 -3 -4 1744.53 64.49
0 -3 -4 1818.22 64.09
0 -3 4 1757.12 58.99
0 3 5 1442.56 56.19
0 3 5 1411.46 59.49
0 3 -5 1567.04 54.29
0 -3 -5 1418.26 58.59
0 -3 -5 1547.55 57.89
0 -3 5 1588.94 53.39
0 -3 5 1454.15 53.29
0 3 -6 19.70 5.00
0 3 6 13.90 5.90
0 -3 -6 11.70 7.20
0 -3 -6 13.30 5.50
0 -3 6 17.90 4.40
0 3 -7 282.47 14.00
0 3 -7 301.27 14.10
0 3 -7 332.07 18.50
0 3 -7 304.67 14.40
0 3 7 307.77 14.30
0 3 -7 293.47 14.00
0 3 7 304.77 12.20
0 3 -7 313.57 14.10
0 -3 -7 305.57 14.10
0 -3 -7 278.77 11.80
0 -3 -7 310.47 14.00
0 -3 7 340.37 17.90
0 3 -8 287.77 14.00
0 3 8 298.17 12.00
0 3 -8 306.77 14.40
0 3 -8 285.47 14.00
0 3 -8 282.17 13.90
0 3 -8 299.87 14.30
0 3 -8 283.87 14.10
0 3 -8 315.77 13.90
0 3 -8 288.87 19.00
0 3 8 275.47 14.60
0 3 8 302.67 14.30
0 -3 8 304.27 18.50
0 -3 -8 257.07 13.50
0 -3 -8 287.77 13.50
0 -3 -8 298.07 13.90
0 3 -9 21.80 4.50
0 3 9 17.70 4.20
0 3 -9 19.60 3.90
0 3 -9 17.50 4.10
0 3 9 18.40 2.90
0 3 -9 15.90 3.60
0 3 -9 23.30 7.30
0 3 -9 19.50 4.10
0 3 -9 26.10 4.50
0 3 -9 25.00 4.40
0 3 9 12.40 3.60
0 -3 9 19.30 6.40
0 -3 -9 15.80 3.40
0 -3 -9 16.80 3.50
0 -3 -9 9.90 4.50
0 3 10 185.28 8.40
0 3 -10 173.18 17.10
0 3 -10 184.98 10.70
0 3 10 189.98 11.60
0 3 10 173.28 10.80
0 3 -10 195.58 10.90
0 3 -10 186.98 10.90
0 3 -10 208.18 11.30
0 3 -10 192.18 10.00
0 3 -10 194.28 11.00
0 3 -10 196.68 11.00
0 -3 -10 187.58 10.60
0 -3 -10 196.78 10.60
0 -3 -10 168.48 10.90
0 -3 10 178.68 15.90
0 3 -11 165.58 9.80
0 3 -11 174.88 10.10
0 3 -11 187.18 10.40
0 3 -11 171.08 10.10
0 3 -11 175.98 9.10
0 3 11 178.48 10.70
0 3 -11 159.58 10.00
0 3 11 185.08 10.10
0 -3 -11 187.18 10.00
0 -3 -11 189.68 10.00
0 -3 11 174.08 10.60
0 -3 -11 168.28 10.10
0 3 -12 25.30 3.70
0 3 -12 23.40 3.60
0 3 -12 29.10 4.30
0 3 -12 33.40 4.30
0 3 12 25.70 3.80
0 3 12 28.70 4.30
0 3 -12 30.20 4.10
0 3 -12 32.20 3.70
0 -3 -12 23.60 3.40
0 -3 12 22.70 3.80
0 -3 -12 24.30 3.70
0 3 13 30.50 3.40
0 3 -13 38.50 3.70
0 3 -13 27.50 3.50
0 3 13 30.10 3.80
0 3 -13 27.80 3.30
0 3 -13 26.30 3.30
0 -3 13 39.80 3.70
0 -3 -13 28.20 3.30
0 -3 -13 38.80 3.60
0 3 -14 15.30 2.10
0 3 -14 11.70 1.80
0 3 -14 9.70 1.50
0 3 -14 11.40 1.80
0 3 14 8.30 1.80
0 -3 14 13.70 1.80
0 -3 -14 8.20 1.60
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-10 1 -11 3.00 1.90
10 -1 11 3.70 1.60
-10 -1 -11 3.90 1.80
-10 -1 -11 3.20 1.80
10 -1 11 1.80 1.60
10 1 12 42.10 3.40
10 -1 12 50.79 3.20
-10 -1 -12 50.49 3.50
10 -1 12 45.70 3.20
10 2 -14 29.00 3.10
-10 2 14 19.60 2.80
10 2 -14 25.70 3.00
10 2 -14 20.90 2.70
-10 2 14 26.60 2.50
10 2 -14 27.70 3.20
-10 -2 14 27.90 3.10
10 -2 -14 26.70 3.40
10 -2 -14 23.90 2.70
-10 2 13 91.39 6.30
10 2 -13 86.29 6.10
-10 2 13 88.39 5.30
10 2 -13 82.49 6.00
10 2 -13 77.29 6.00
10 2 -13 100.39 5.70
10 2 -13 87.99 5.70
10 2 -13 87.99 5.70
10 -2 -13 78.89 6.00
10 -2 -13 87.49 6.20
10 -2 -13 88.09 6.20
10 -2 -13 91.09 5.80
-10 -2 13 92.49 6.40
10 -2 -13 80.09 6.30
10 2 -12 2.10 2.20
10 2 -12 1.10 2.20
10 2 -12 4.20 2.30
10 2 -12 -1.70 1.80
10 2 -12 -0.60 2.10
10 2 -12 2.60 2.10
-10 2 12 0.70 2.10
-10 2 12 -2.40 2.10
10 -2 -12 3.90 3.10
10 -2 -12 0.60 2.50
10 -2 -12 -2.70 2.70
10 -2 -12 1.10 2.50
10 -2 -12 2.00 2.10
10 -2 -12 -2.40 2.20
-10 -2 12 8.40 4.30
-10 2 11 244.98 12.70
10 2 -11 251.97 12.10
10 2 -11 242.98 12.80
-10 2 11 249.08 11.60
10 2 -11 249.58 12.70
10 2 -11 240.28 12.00
10 2 -11 249.88 12.70
10 2 -11 257.67 12.40
10 -2 -11 243.48 12.50
-10 -2 11 257.17 18.30
10 -2 -11 243.08 12.10
10 -2 -11 258.07 13.10
10 -2 -11 265.87 13.00
10 -2 -11 237.78 12.10
10 -2 -11 254.97 12.20
-10 2 10 4.30 8.90
-10 2 10 0.40 2.70
10 2 -10 1.80 2.20
10 2 -10 -2.50 2.30
10 2 -10 5.20 4.30
10 2 -10 2.10 2.30
10 2 -10 0.60 1.90
10 2 -10 1.60 2.50
10 2 -10 2.20 4.10
10 2 -10 5.60 3.20
-10 2 10 0.20 2.40
10 -2 -10 -0.40 2.50
10 -2 -10 2.20 2.40
10 -2 -10 -2.90 8.10
-10 -2 10 2.00 4.00
10 -2 -10 0.30 2.90
10 -2 -10 4.10 2.60
10 -2 -10 2.00 2.50
10 -2 -10 5.00 3.40
-10 2 9 1295.57 57.29
-10 2 9 1303.37 45.10
10 2 -9 1258.87 52.59
-10 2 9 1274.07 46.10
10 2 -9 1343.67 46.60
10 2 -9 1228.08 45.20
10 2 -9 1305.77 46.30
10 2 -9 1259.87 46.20
10 2 -9 1291.37 45.90
10 2 -9 1276.67 46.70
10 2 -9 1237.18 45.40
10 -2 -9 1277.67 45.60
10 -2 -9 1272.37 45.90
10 -2 -9 1306.77 46.40
10 -2 -9 1323.17 46.70
10 -2 -9 1283.57 59.99
10 -2 -9 1239.08 45.80
-10 -2 9 1337.07 51.69
10 -2 -9 1341.37 46.10
10 2 -8 31.00 5.00
10 2 -8 30.20 4.90
-10 2 8 30.00 8.40
10 2 -8 27.40 4.50
10 2 -8 30.70 6.60
10 2 -8 30.70 4.80
-10 2 8 22.90 4.20
10 2 -8 32.30 4.50
-10 2 8 29.40 4.20
10 2 -8 27.10 5.40
10 2 -8 28.60 4.40
10 -2 -8 20.10 4.20
10 -2 -8 24.40 3.90
-10 -2 8 29.70 5.90
10 -2 -8 12.90 5.70
10 -2 -8 28.40 4.80
10 -2 -8 26.70 4.60
10 -2 -8 27.90 4.90
10 -2 -8 30.40 5.00
-10 2 7 61.39 10.60
10 2 -7 60.59 5.80
10 2 -7 66.89 8.90
10 2 -7 70.59 7.10
10 2 -7 81.09 7.10
-10 2 7 57.19 5.50
10 2 -7 71.49 6.70
-10 2 7 67.39 6.70
10 2 -7 66.09 5.50
10 2 -7 68.19 6.80
10 -2 -7 65.69 6.40
10 -2 -7 56.59 10.90
10 -2 -7 66.09 5.90
10 -2 -7 65.09 6.50
10 -2 -7 57.49 6.40
-10 -2 7 59.09 7.80
10 2 -6 4.60 2.60
-10 2 6 9.10 5.00
-10 -2 6 9.80 3.30
10 -2 -6 2.90 4.20
-10 2 5 1339.67 54.49
10 2 -5 1389.86 51.29
-10 -2 5 1386.96 50.29
10 -2 -5 1398.36 56.49
-10 2 4 28.50 6.80
-10 -2 4 42.00 5.90
-10 2 3 4305.37 151.28
-10 2 3 4295.77 149.88
10 -2 -3 4082.49 149.39
-10 -2 3 4771.42 147.29
-10 2 2 1571.84 60.19
-10 2 2 1586.24 61.59
-10 -2 2 1624.24 58.29
10 -2 -2 1562.54 60.19
-10 2 1 6.70 4.20
-10 2 1 10.20 4.60
-10 -2 1 6.70 3.00
10 -2 -1 9.90 4.20
-10 2 0 803.22 34.20
-10 2 0 614.74 30.80
10 -2 0 701.83 31.80
-10 -2 0 747.83 31.70
-10 2 -1 1355.16 57.59
10 -2 1 1460.55 56.39
-10 -2 -1 1471.75 56.19
-10 2 -2 63.29 10.80
-10 -2 -2 82.39 12.10
10 -2 2 85.69 12.00
10 2 3 341.17 23.20
-10 2 -3 343.27 22.80
-10 2 -3 303.37 18.80
10 2 3 385.66 19.00
-10 -2 -3 325.47 21.20
10 -2 3 334.17 20.90
10 2 4 146.19 9.90
-10 2 -4 149.88 9.40
-10 2 -4 164.28 9.60
10 2 4 174.78 9.50
-10 2 -4 178.78 9.70
10 2 4 167.48 10.00
-10 2 -4 183.48 17.20
-10 2 -4 170.38 10.10
10 2 4 161.98 9.20
-10 2 -4 174.08 10.10
10 2 4 130.69 17.70
-10 -2 -4 166.28 16.30
-10 -2 -4 181.08 10.60
-10 -2 -4 156.58 8.20
10 -2 4 154.68 14.50
10 -2 4 158.28 8.60
10 -2 4 178.08 9.20
-10 2 -5 1019.50 38.20
-10 2 -5 1058.49 38.50
-10 2 -5 1045.70 38.20
-10 2 -5 994.40 50.69
10 2 5 1042.50 38.00
-10 2 -5 1081.49 39.10
-10 2 -5 1053.99 39.20
10 2 5 1035.20 38.20
-10 2 -5 1009.70 37.90
10 2 5 1060.99 39.60
10 2 5 1105.99 38.50
-10 -2 -5 1057.19 36.50
10 -2 5 1040.30 37.20
10 -2 5 1076.79 48.90
10 -2 5 1029.40 38.00
-10 -2 -5 1118.89 38.80
-10 -2 -5 1065.29 39.10
-10 2 -6 252.57 12.70
-10 2 -6 216.88 12.40
-10 2 -6 222.78 12.00
10 2 6 238.08 12.10
-10 2 -6 228.08 23.60
-10 2 -6 228.38 11.90
10 2 6 212.58 11.70
-10 2 -6 251.87 13.00
10 2 6 245.58 12.90
-10 2 -6 246.88 12.30
10 -2 6 230.68 11.60
10 -2 6 248.08 11.20
-10 -2 -6 231.98 12.60
-10 -2 -6 249.48 12.40
-10 -2 -6 210.18 9.50
10 -2 6 244.48 20.80
10 2 7 236.98 12.10
-10 2 -7 230.08 12.10
10 2 7 222.48 12.10
-10 2 -7 230.28 12.30
10 2 7 220.98 12.80
-10 2 -7 233.18 12.10
-10 2 -7 249.48 12.80
-10 2 -7 214.68 11.80
-10 2 -7 254.77 12.80
10 -2 7 238.68 11.50
-10 -2 -7 237.48 12.70
10 -2 7 251.37 11.20
-10 -2 -7 252.17 12.50
-10 -2 -7 206.18 11.50
-10 2 -8 54.79 5.70
10 2 8 48.40 5.50
-10 2 -8 41.60 5.50
-10 2 -8 40.40 5.30
10 2 8 48.10 6.40
-10 2 -8 37.80 4.80
-10 2 -8 33.70 5.00
-10 -2 -8 41.30 5.90
-10 -2 -8 42.80 5.40
10 -2 8 48.30 4.70
-10 -2 -8 40.10 4.90
-10 2 -9 8.80 2.80
10 2 9 4.10 2.10
-10 2 -9 7.40 3.10
-10 2 -9 7.30 2.60
-10 2 -9 7.70 3.00
10 2 9 8.00 2.60
-10 2 -9 12.90 3.30
-10 -2 -9 10.10 3.30
10 -2 9 7.20 2.70
-10 -2 -9 6.20 2.50
10 -2 9 5.20 2.10
10 2 10 11.40 2.50
10 2 10 14.50 3.10
-10 2 -10 15.50 3.00
-10 2 -10 16.20 3.10
-10 2 -10 8.40 2.30
-10 2 -10 14.70 2.90
-10 2 -10 8.00 3.40
-10 -2 -10 9.20 2.30
10 -2 10 11.90 2.10
-10 -2 -10 11.80 2.90
10 -2 10 9.40 2.40
-10 2 -11 53.89 4.00
10 2 11 56.09 4.00
10 2 11 59.29 4.30
-10 2 -11 60.19 4.30
-10 -2 -11 60.49 4.60
10 -2 11 57.29 4.10
10 -2 11 58.19 4.30
-10 -2 -11 57.09 4.10
10 3 -14 10.10 2.00
-10 3 14 12.40 2.20
-10 3 14 13.20 2.30
10 3 -14 10.30 1.80
10 3 -14 11.80 2.00
10 3 -14 13.60 2.00
-10 -3 14 11.60 2.30
10 -3 -14 10.20 2.10
10 -3 -14 15.20 2.00
-10 3 13 11.00 2.60
10 3 -13 5.20 1.90
10 3 -13 5.60 2.00
10 3 -13 9.30 2.20
-10 3 13 7.20 2.40
10 3 -13 8.30 2.20
10 3 -13 11.70 2.60
10 -3 -13 8.30 2.30
-10 -3 13 2.70 3.20
10 -3 -13 7.50 2.20
-10 3 12 117.39 7.70
10 3 -12 127.09 7.10
10 3 -12 125.69 7.30
-10 3 12 125.19 6.10
10 3 -12 121.19 7.50
10 3 -12 124.09 7.50
10 3 -12 121.39 7.50
10 3 -12 114.69 6.80
10 -3 -12 114.79 6.90
10 -3 -12 108.49 6.90
10 -3 -12 124.29 7.80
-10 3 11 8.50 2.90
10 3 -11 5.40 2.60
10 3 -11 8.40 2.90
10 3 -11 8.90 2.80
-10 3 11 6.30 2.20
10 3 -11 11.30 2.90
10 3 -11 9.30 2.80
10 3 -11 9.00 2.80
10 -3 -11 13.80 3.40
10 -3 -11 4.10 3.80
10 -3 -11 8.50 2.90
10 -3 -11 10.40 3.00
-10 3 10 249.08 11.20
-10 3 10 251.87 12.90
10 3 -10 264.97 13.00
10 3 -10 264.17 12.90
10 3 -10 235.88 16.30
10 3 -10 247.08 12.10
10 3 -10 262.57 13.10
10 3 -10 255.27 12.40
10 3 -10 259.57 12.40
10 -3 -10 251.77 12.60
10 -3 -10 273.27 12.90
10 -3 -10 244.08 12.10
-10 -3 10 259.77 16.40
10 -3 -10 245.98 13.00
10 -3 -10 252.67 12.90
10 3 -9 130.99 9.00
-10 3 9 150.98 8.10
10 3 -9 151.08 9.40
10 3 -9 164.28 9.00
10 3 -9 148.09 9.10
10 3 -9 151.88 9.20
-10 3 9 158.78 9.70
10 3 -9 155.68 9.30
10 3 -9 154.48 12.00
10 3 -9 136.49 9.20
-10 -3 9 160.98 11.80
10 -3 -9 148.59 8.90
10 -3 -9 155.98 9.40
10 -3 -9 161.88 9.80
10 -3 -9 166.98 9.70
10 3 -8 57.09 5.40
10 3 -8 42.90 5.30
-10 3 8 47.70 4.60
10 3 -8 52.09 5.50
10 3 -8 56.39 8.00
10 3 -8 51.29 6.00
10 3 -8 57.69 6.40
10 3 -8 61.69 6.50
-10 3 8 66.09 6.80
10 -3 -8 51.59 5.70
-10 -3 8 47.30 7.10
10 -3 -8 62.49 6.10
10 -3 -8 68.19 6.70
10 -3 -8 58.99 6.20
10 -3 -8 49.70 5.70
10 -3 -8 62.39 6.70
-10 3 7 1096.19 37.70
10 3 -7 1081.59 39.20
10 3 -7 1102.89 39.40
10 3 -7 1053.79 38.70
10 3 -7 1068.79 39.10
10 3 -7 1104.79 42.10
-10 3 7 1102.09 39.30
10 3 -7 1131.39 39.10
10 3 -7 1070.49 39.50
10 -3 -7 1064.79 39.10
10 -3 -7 1088.99 39.50
10 -3 -7 1121.29 39.40
10 -3 -7 1065.09 38.80
10 -3 -7 1013.40 51.29
10 -3 -7 1042.50 38.40
-10 -3 7 1120.99 41.40
10 3 -6 35.40 4.60
10 3 -6 33.10 4.50
10 3 -6 33.10 4.70
10 3 -6 35.70 4.60
-10 3 6 34.60 3.90
10 3 -6 37.80 5.90
-10 3 6 26.50 8.00
-10 3 6 35.30 4.80
10 3 -6 38.90 5.20
-10 -3 6 41.40 5.50
10 -3 -6 41.90 4.90
10 -3 -6 27.60 4.80
10 -3 -6 42.30 9.70
10 -3 -6 35.90 4.30
10 3 -5 107.29 8.90
10 3 -5 96.89 10.70
-10 3 5 75.99 12.00
-10 3 5 88.59 5.60
10 -3 -5 94.49 6.90
-10 -3 5 94.09 7.10
-10 3 4 959.90 44.90
-10 -3 4 1053.29 38.40
-10 3 3 759.32 36.00
10 -3 -3 728.73 34.70
-10 -3 3 777.42 30.90
-10 3 2 402.76 23.70
10 -3 -2 410.66 22.80
-10 -3 2 408.46 20.10
-10 3 1 1205.18 51.69
10 -3 -1 1208.28 50.59
-10 -3 1 1270.07 48.50
-10 3 0 62.39 11.10
-10 -3 0 55.19 9.10
10 -3 0 50.99 9.60
-10 3 -1 53.59 10.70
10 -3 1 48.10 9.30
-10 -3 -1 52.09 9.40
10 3 2 362.16 14.90
10 3 2 300.47 14.30
-10 3 -2 328.07 14.40
10 3 2 349.57 23.10
-10 3 -2 355.16 23.00
-10 3 -2 311.97 15.50
-10 3 -2 332.37 14.80
10 3 2 340.97 15.70
10 -3 2 328.27 21.00
-10 -3 -2 357.46 21.70
-10 3 -3 527.65 21.90
-10 3 -3 566.34 21.70
10 3 3 539.45 21.40
-10 3 -3 525.25 21.30
10 3 3 523.15 21.60
10 3 3 577.54 33.00
10 3 3 557.34 22.70
-10 3 -3 578.14 32.00
10 3 3 542.25 21.30
-10 3 -3 512.35 21.40
10 3 3 514.75 21.90
-10 3 -3 511.55 21.90
10 3 3 558.74 21.70
-10 3 -3 505.55 21.50
-10 3 -3 538.05 21.20
10 -3 3 575.44 29.80
-10 -3 -3 567.84 30.30
-10 -3 -3 524.85 20.60
10 -3 3 509.65 20.30
-10 -3 -3 580.64 22.90
10 3 4 8.20 4.00
-10 3 -4 4.60 2.90
-10 3 -4 7.00 2.90
10 3 4 13.80 4.20
10 3 4 5.30 4.10
10 3 4 4.00 7.30
-10 3 -4 6.50 6.30
10 3 4 10.10 3.60
-10 3 -4 3.20 3.10
10 3 4 10.50 3.50
-10 3 -4 8.50 3.10
-10 3 -4 7.10 3.40
10 3 4 7.60 3.10
10 3 4 8.50 3.30
-10 3 -4 6.90 3.30
10 -3 4 5.70 5.60
-10 -3 -4 6.00 2.90
-10 -3 -4 9.40 4.10
10 -3 4 7.30 2.70
-10 -3 -4 14.70 7.50
-10 3 -5 53.19 6.20
-10 3 -5 61.29 6.40
10 3 5 55.49 6.20
10 3 5 52.99 6.20
10 3 5 61.09 6.60
10 3 5 38.40 5.40
-10 3 -5 47.80 5.50
-10 3 -5 50.29 6.20
-10 3 -5 51.19 6.20
-10 3 -5 49.40 11.70
-10 3 -5 51.99 6.30
10 -3 5 44.10 10.30
10 -3 5 50.49 5.00
10 -3 5 53.09 5.80
-10 -3 -5 52.49 4.70
-10 -3 -5 62.59 7.60
-10 -3 -5 49.40 6.30
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10 3 6 732.53 28.40
-10 3 -6 716.43 28.40
-10 3 -6 799.72 29.90
-10 3 -6 719.73 28.20
10 3 6 737.23 28.30
10 3 6 767.72 28.70
-10 3 -6 738.13 29.00
10 3 6 767.52 30.10
-10 3 -6 754.02 28.90
-10 3 -6 753.52 28.90
10 -3 6 751.02 27.70
-10 -3 -6 803.32 29.40
-10 -3 -6 717.43 26.30
10 -3 6 659.43 38.40
10 -3 6 717.83 28.10
-10 -3 -6 767.02 29.60
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-10 3 -7 2.90 2.10
-10 3 -7 1.90 3.10
-10 3 -7 -0.20 2.00
-10 3 -7 4.50 3.00
10 3 7 1.60 3.10
10 3 7 4.20 2.70
10 3 7 0.50 2.30
-10 3 -7 1.30 2.70
-10 -3 -7 -0.50 2.30
-10 -3 -7 2.60 3.70
10 -3 7 1.10 2.70
-10 -3 -7 -0.30 2.40
10 -3 7 -6.30 8.80
10 -3 7 1.10 2.20
-10 3 -8 -1.60 2.30
-10 3 -8 4.20 2.50
-10 3 -8 -0.50 2.50
-10 3 -8 6.00 2.80
10 3 8 0.10 2.30
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10 3 8 -3.10 1.40
-10 3 -8 -0.70 2.00
-10 -3 -8 -0.70 2.90
-10 -3 -8 -0.80 1.90
10 -3 8 -1.40 1.90
-10 -3 -8 -0.30 2.50
10 -3 8 -0.80 2.70
10 3 9 24.20 3.60
-10 3 -9 37.20 4.10
10 3 9 23.60 3.70
-10 3 -9 30.80 4.30
-10 3 -9 35.00 4.50
-10 3 -9 35.20 4.40
-10 3 -9 30.50 3.90
10 -3 9 29.20 3.30
-10 -3 -9 19.90 3.40
-10 -3 -9 28.20 3.90
-10 -3 -9 26.70 4.10
-10 3 -10 1.50 1.50
10 3 10 3.00 1.90
-10 3 -10 1.80 2.10
-10 3 -10 -0.50 1.40
-10 3 -10 1.80 1.70
-10 3 -10 -1.10 2.00
10 3 10 0.90 1.70
10 -3 10 -0.20 1.40
-10 -3 -10 3.60 2.60
10 -3 10 1.90 1.60
-10 -3 -10 2.10 1.50
10 3 11 47.80 3.40
10 3 11 43.00 3.50
-10 3 -11 47.70 3.50
-10 -3 -11 42.30 3.30
10 -3 11 39.80 3.30
10 4 -13 110.69 5.80
10 4 -13 115.99 6.00
10 4 -13 117.59 6.10
10 4 -13 111.29 5.30
-10 4 13 96.99 5.70
10 -4 -13 94.19 5.80
10 4 -12 229.78 10.50
10 4 -12 243.38 10.80
10 4 -12 260.47 11.40
-10 4 12 260.97 11.70
10 4 -12 272.77 11.70
-10 4 12 242.38 11.20
10 4 -12 251.27 11.50
10 -4 -12 273.67 11.90
10 -4 -12 256.17 11.10
10 4 -11 21.70 3.60
10 4 -11 28.20 3.50
10 4 -11 25.20 3.40
10 4 -11 23.40 3.60
-10 4 11 23.00 3.70
-10 4 11 24.70 4.00
10 4 -11 23.30 3.60
10 4 -11 22.70 3.50
10 -4 -11 24.50 3.70
10 -4 -11 19.50 3.50
10 -4 -11 25.80 4.10
10 4 -10 24.40 3.90
10 4 -10 24.70 4.20
10 4 -10 33.70 4.40
-10 4 10 40.80 5.00
10 4 -10 29.10 4.30
10 4 -10 33.20 4.30
-10 4 10 35.50 5.20
10 4 -10 32.80 4.80
10 -4 -10 31.10 4.70
10 -4 -10 27.70 4.50
10 -4 -10 29.80 4.50
10 4 -9 38.00 4.90
-10 4 9 47.70 3.80
10 4 -9 45.60 5.60
-10 4 9 50.09 5.80
-10 4 9 51.69 6.10
10 4 -9 35.50 4.70
10 4 -9 55.89 5.40
10 4 -9 42.50 4.70
-10 4 9 35.50 5.80
-10 -4 9 46.60 6.80
10 -4 -9 42.00 5.20
10 -4 -9 47.20 5.30
-10 4 8 589.24 20.50
10 4 -8 552.34 22.30
10 4 -8 565.54 23.20
-10 4 8 541.45 23.50
-10 4 8 589.74 23.40
10 4 -8 598.54 23.30
10 4 -8 567.24 22.70
-10 4 8 586.94 23.20
10 4 -8 572.34 22.90
10 4 -8 594.44 22.80
10 -4 -8 582.44 23.10
10 -4 -8 611.34 23.60
-10 -4 8 578.04 24.50
10 -4 -8 553.54 22.20
-10 4 7 152.48 9.30
10 4 -7 134.79 8.70
10 4 -7 141.69 9.30
-10 4 7 141.99 6.70
-10 4 7 161.58 9.20
10 4 -7 111.89 12.10
10 4 -7 145.89 8.80
10 4 -7 137.79 8.80
-10 4 7 120.99 10.30
10 4 -7 141.29 8.60
10 4 -7 146.59 8.60
10 -4 -7 119.49 9.80
10 -4 -7 145.19 8.50
-10 -4 7 149.99 9.30
10 -4 -7 160.28 9.30
10 -4 -7 149.09 8.90
10 4 -6 762.62 29.30
-10 4 6 805.32 26.90
10 4 -6 769.82 29.30
10 4 -6 745.33 28.80
-10 4 6 840.82 29.80
10 4 -6 781.82 29.30
10 4 -6 796.12 29.20
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-23 -3 3 62.19 3.60
23 3 -2 69.29 4.40
-23 3 2 76.09 4.70
23 3 -2 80.69 4.40
23 3 -2 61.89 4.10
23 3 -2 62.49 4.20
23 3 -2 73.29 4.30
23 -3 -2 82.49 4.40
-23 -3 2 57.39 4.60
23 -3 -2 63.99 4.10
-23 -3 2 76.39 4.00
23 3 -1 10.10 1.70
23 3 -1 11.50 2.00
-23 3 1 16.50 2.50
23 -3 -1 14.50 2.20
-23 -3 1 8.20 1.80
-23 -3 1 10.30 1.60
23 -3 -1 13.30 2.00
-23 3 0 1.10 1.20
23 3 0 4.10 1.40
23 3 0 2.50 1.30
-23 -3 0 1.90 1.50
-23 -3 0 2.20 1.50
23 -3 0 1.50 1.30
23 -3 0 2.50 1.70
-23 3 -1 -1.20 1.10
23 3 1 0.60 1.00
23 -3 1 0.50 0.90
-23 -3 -1 2.70 1.20
-23 -3 -1 -0.10 1.30
-23 4 6 57.29 3.40
23 4 -6 52.79 3.20
-23 4 6 50.39 3.40
23 4 -6 59.29 3.40
23 4 -6 52.99 3.30
23 4 -6 47.60 3.30
-23 -4 6 50.29 3.50
-23 -4 6 58.99 3.30
23 -4 -6 54.29 3.30
23 4 -5 10.70 1.80
-23 4 5 9.00 1.90
23 4 -5 12.30 2.00
23 4 -5 9.00 1.70
23 4 -5 10.20 1.80
-23 4 5 7.80 1.80
23 -4 -5 13.40 2.00
-23 -4 5 7.70 1.80
-23 -4 5 8.90 1.70
-23 4 4 1.70 2.20
-23 4 4 2.50 1.50
23 4 -4 3.30 1.30
23 4 -4 2.60 1.10
23 4 -4 0.90 1.20
23 4 -4 2.30 1.40
23 -4 -4 0.90 1.00
-23 -4 4 3.20 1.60
-23 -4 4 3.00 1.40
23 4 -3 4.30 1.50
23 4 -3 3.50 1.40
23 4 -3 4.70 1.60
-23 4 3 6.00 1.70
23 4 -3 4.40 1.40
-23 -4 3 4.20 1.30
-23 -4 3 0.80 1.50
23 -4 -3 8.00 1.60
23 4 -2 24.50 2.40
23 4 -2 28.50 2.60
23 4 -2 28.00 2.50
-23 4 2 31.00 2.80
23 4 -2 31.60 2.70
-23 -4 2 31.70 2.40
23 -4 -2 34.40 2.60
-23 4 1 1.70 1.20
23 4 -1 2.60 1.00
23 4 -1 0.40 1.10
-23 -4 1 -0.20 1.10
-23 -4 1 1.60 1.00
23 -4 -1 2.20 1.10
-24 0 9 -0.30 1.20
24 0 -9 -2.30 0.90
24 0 -8 35.10 2.90
-24 0 8 43.30 2.40
-24 0 8 44.20 3.40
24 0 -8 36.10 2.90
24 0 -7 2.00 1.30
-24 0 7 0.50 1.40
24 0 -7 -0.80 1.20
-24 0 7 2.40 1.10
24 0 -6 20.10 2.50
-24 0 6 25.10 2.20
-24 0 6 23.30 3.00
24 0 -6 24.70 2.90
-24 0 5 -1.50 1.10
-24 0 5 -2.70 1.30
-24 0 5 -0.60 1.50
24 0 -5 0.90 1.20
24 0 -5 -1.10 1.30
24 0 -4 178.58 7.70
-24 0 4 182.98 8.20
24 0 -4 181.88 8.20
-24 0 4 162.48 8.60
-24 0 3 1.30 1.50
24 0 -3 -0.60 1.10
-24 0 3 1.20 1.60
24 0 -3 0.10 1.40
-24 0 2 76.29 5.30
-24 0 2 82.19 4.90
24 0 -2 84.09 4.70
24 0 -2 84.49 4.80
24 0 -1 1.10 1.10
24 0 -1 1.00 1.20
-24 0 1 -0.80 1.70
-24 0 1 -0.60 1.30
24 0 0 18.10 2.10
24 0 0 19.90 2.40
-24 0 0 16.60 2.30
-24 0 -1 -0.60 1.10
24 0 1 -1.20 0.80
-24 1 8 10.60 1.90
24 1 -8 10.60 1.80
24 1 -8 11.00 1.80
24 1 -8 13.40 2.00
24 -1 -8 14.30 2.10
-24 -1 8 9.00 1.80
24 -1 -8 10.80 1.80
-24 -1 8 12.60 1.70
24 1 -7 1.30 1.20
-24 1 7 0.50 1.80
24 1 -7 -3.70 1.50
24 1 -7 0.10 1.20
24 1 -7 0.00 1.50
-24 1 7 -0.30 1.40
-24 -1 7 0.10 1.50
24 -1 -7 0.50 1.20
-24 -1 7 -0.20 1.10
24 -1 -7 1.20 1.40
-24 1 6 50.39 4.20
24 1 -6 56.19 3.70
24 1 -6 56.19 3.80
-24 1 6 62.49 4.20
24 1 -6 58.89 3.80
24 1 -6 52.99 3.90
-24 -1 6 57.29 4.00
24 -1 -6 59.89 3.90
-24 -1 6 56.69 3.30
24 -1 -6 58.69 3.80
24 1 -5 45.80 3.60
24 1 -5 45.80 3.50
-24 1 5 45.00 3.80
-24 1 5 44.50 4.10
24 1 -5 43.60 3.50
24 -1 -5 43.20 3.50
-24 -1 5 42.50 3.80
-24 -1 5 49.40 3.10
24 -1 -5 45.70 3.60
24 1 -4 -0.10 1.60
-24 1 4 2.00 1.50
24 1 -4 5.10 1.60
-24 1 4 -2.30 1.50
24 1 -4 -0.50 1.20
-24 -1 4 2.40 1.60
-24 -1 4 1.00 1.20
24 -1 -4 0.40 1.00
-24 -1 4 -1.30 1.70
24 -1 -4 1.10 2.00
24 1 -3 34.10 3.20
24 1 -3 39.10 3.60
-24 1 3 39.00 3.70
-24 1 3 37.50 3.80
24 1 -3 41.40 3.30
-24 -1 3 34.60 4.00
-24 -1 3 30.30 3.10
24 -1 -3 33.00 3.10
-24 -1 3 34.30 2.50
24 -1 -3 36.20 3.20
-24 1 2 72.79 4.80
-24 1 2 72.69 4.60
24 1 -2 71.49 4.30
24 1 -2 74.69 4.50
24 -1 -2 84.39 4.50
-24 -1 2 59.49 4.90
-24 -1 2 70.79 5.00
24 -1 -2 68.49 4.20
24 1 -1 0.50 1.30
-24 1 1 4.90 1.70
-24 1 1 1.90 1.40
24 1 -1 1.60 1.20
-24 -1 1 3.40 1.60
24 -1 -1 2.40 1.20
24 -1 -1 -1.60 1.10
24 1 0 74.49 3.80
-24 1 0 64.89 4.10
24 1 0 70.69 4.00
-24 1 0 60.99 4.10
-24 -1 0 70.09 4.50
24 -1 0 69.59 3.90
24 -1 0 65.39 3.70
24 1 1 32.00 2.50
-24 1 -1 26.90 2.70
-24 -1 -1 31.00 2.80
24 -1 1 29.60 2.40
24 2 -8 19.60 2.10
24 2 -8 24.90 2.30
24 2 -8 20.60 2.10
-24 -2 8 28.90 2.30
24 -2 -8 26.10 2.30
24 2 -7 157.78 6.70
24 2 -7 161.58 7.00
24 2 -7 160.38 6.70
24 2 -7 156.68 6.70
-24 2 7 160.58 7.20
24 -2 -7 160.18 6.80
24 -2 -7 157.18 6.70
-24 -2 7 175.78 6.60
24 2 -6 3.00 1.50
24 2 -6 0.40 1.20
24 2 -6 0.30 1.20
24 2 -6 1.00 1.20
-24 2 6 1.30 1.40
-24 -2 6 1.60 1.20
24 -2 -6 1.00 1.40
24 -2 -6 -0.20 1.10
24 2 -5 55.09 3.90
24 2 -5 75.39 4.30
24 2 -5 63.49 3.90
24 2 -5 61.59 3.90
-24 2 5 72.69 4.60
-24 -2 5 75.19 3.80
24 -2 -5 66.99 4.10
24 2 -4 2.90 1.50
-24 2 4 0.10 1.20
24 2 -4 -1.20 1.10
24 2 -4 0.60 1.30
24 2 -4 -5.40 2.00
24 -2 -4 0.40 1.10
-24 -2 4 1.80 1.40
-24 -2 4 0.40 1.20
24 2 -3 74.09 4.20
24 2 -3 76.49 4.30
-24 2 3 80.29 4.80
24 2 -3 74.79 4.30
24 2 -3 81.39 4.60
-24 -2 3 78.29 5.10
-24 -2 3 85.79 3.90
24 -2 -3 69.59 4.10
24 -2 -3 63.29 4.20
-24 2 2 5.60 1.80
24 2 -2 6.70 1.70
24 2 -2 7.60 1.70
-24 2 2 0.50 2.50
24 -2 -2 7.50 1.70
24 -2 -2 8.10 1.70
-24 -2 2 6.80 1.90
-24 2 1 134.99 6.30
24 2 -1 136.69 5.90
24 2 -1 132.99 6.00
-24 -2 1 117.19 5.80
24 -2 -1 132.79 5.90
24 -2 -1 125.39 5.70
-24 2 0 13.40 2.00
24 2 0 15.20 1.90
24 2 0 15.40 2.40
24 -2 0 13.20 1.80
-24 -2 0 10.10 1.80
24 3 -6 56.99 3.60
24 3 -6 68.69 3.60
24 3 -6 62.99 3.50
24 3 -6 63.39 3.50
-24 -3 6 68.69 3.50
24 -3 -6 64.49 3.60
24 3 -5 87.19 4.50
24 3 -5 85.89 4.50
-24 3 5 88.09 4.70
24 3 -5 82.99 4.30
24 3 -5 87.09 4.40
24 -3 -5 89.79 4.50
-24 -3 5 88.99 4.20
24 3 -4 29.30 2.70
24 3 -4 24.20 2.50
24 3 -4 31.60 2.70
-24 3 4 25.00 2.80
24 3 -4 33.70 2.60
24 -3 -4 31.60 2.60
-24 -3 4 37.80 2.60
-24 -3 4 30.60 3.10
-24 3 3 10.30 1.90
24 3 -3 14.30 2.00
24 3 -3 13.20 1.90
24 3 -3 8.40 1.80
-24 -3 3 9.50 1.80
24 -3 -3 10.90 1.70
-24 -3 3 10.80 1.50
24 3 -2 7.40 1.50
-24 3 2 3.00 1.40
24 3 -2 6.40 1.50
-24 -3 2 3.80 1.40
24 -3 -2 7.90 1.50
24 3 -1 15.00 1.70
-24 3 1 10.90 1.70
24 3 -1 20.10 2.00
-24 -3 1 12.50 1.80
24 -3 -1 13.90 2.00
-24 -3 1 9.90 1.70
-25 0 7 0.00 1.30
25 0 -7 1.40 1.10
-25 0 7 -1.50 1.20
25 0 -7 2.20 1.10
-25 0 6 38.20 3.30
-25 0 6 48.30 3.20
25 0 -6 46.80 3.10
25 0 -6 48.10 3.10
-25 0 5 -0.90 1.30
-25 0 5 0.60 1.40
25 0 -5 0.00 1.00
25 0 -5 0.70 1.60
-25 0 4 -1.20 1.30
25 0 -4 -1.70 0.90
-25 0 4 -1.10 1.30
-25 0 3 -2.70 1.10
25 0 -3 -0.50 1.10
-25 0 3 0.60 1.40
25 0 -2 98.49 4.60
25 0 -2 85.39 4.20
-25 0 2 87.59 4.90
-25 0 1 1.40 1.30
25 0 -1 -0.60 1.10
25 0 -1 1.70 1.20
25 1 -7 13.50 1.60
-25 1 7 13.20 1.80
25 1 -7 13.60 1.80
25 -1 -7 12.60 1.70
-25 1 6 1.90 1.20
25 1 -6 1.40 1.00
25 1 -6 -0.20 1.10
25 -1 -6 2.20 1.20
-25 -1 6 0.20 1.20
25 1 -5 26.90 2.50
-25 1 5 20.80 2.40
25 1 -5 22.00 2.30
25 -1 -5 26.40 2.50
-25 -1 5 22.20 2.60
-25 1 4 44.60 3.40
-25 1 4 42.30 3.50
25 1 -4 49.70 3.30
-25 -1 4 43.50 3.50
25 -1 -4 44.60 3.10
-25 1 3 14.50 2.00
-25 1 3 11.40 2.00
25 1 -3 12.00 1.80
25 -1 -3 13.10 1.80
-25 -1 3 15.80 2.30
-25 1 2 1.70 1.50
25 1 -2 1.00 1.10
-25 1 2 0.60 1.30
-25 -1 2 2.60 1.30
25 -1 -2 1.00 1.10
25 1 -1 28.70 2.90
25 1 -1 35.90 2.50
25 -1 -1 27.50 2.40
-25 -1 1 34.20 2.80
-25 2 5 59.09 3.60
25 2 -5 58.69 3.40
25 2 -5 51.09 3.20
-25 -2 5 58.89 3.80
25 -2 -5 59.39 3.30
-25 -2 5 59.39 2.80
25 2 -4 3.50 1.20
-25 2 4 1.30 1.20
-25 -2 4 0.90 1.20
25 -2 -4 2.10 1.00
25 2 -3 55.59 3.20
-25 2 3 54.59 3.40
25 -2 -3 53.19 3.10
-25 -2 3 46.00 3.40
0 0 0 0.00 0.00
_computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)'
;
_shelx_hkl_checksum 89457
_shelx_res_file
;
TITL jtm1769_a.res in P2(1)/c
jtm1769_a.res
created by SHELXL-2019/1 at 15:19:09 on 19-Apr-2023
REM Old TITL jtm1769 in P2(1)/c
REM SHELXT solution in P2(1)/c: R1 0.110, Rweak 0.005, Alpha 0.035
REM 0.510 for 308 systematic absences, Orientation as input
REM Formula found by SHELXT: C20 Br N O2
CELL 1.54178 20.5385 8.1977 12.3185 90.000 105.231 90.000
ZERR 4.000 0.0005 0.0002 0.0003 0.000 0.001 0.000
LATT 1
SYMM -X, 1/2+Y, 1/2-Z
SFAC C H BR N O
UNIT 80 112 4 4 8
TEMP -123
SIZE 0.048 0.068 0.228
L.S. 5
BOND $H
LIST 4
CONF
MPLA C1 > C8 N1
EQIV $1 x, -y+3/2, z-1/2
HTAB C2 O2_$1
HTAB C9 O2_$1
EQIV $2 -x+1, -y+2, -z+1
HTAB C20 O2_$2
ACTA 149.4
FMAP 2
PLAN 5
WGHT 0.045900 0.838700
FVAR 0.64039
BR1 3 0.235726 0.631036 -0.094157 11.00000 0.04657 0.04566 =
0.04404 -0.01268 0.01324 -0.00114
O1 5 0.942891 0.566542 1.233493 11.00000 0.04391 0.04419 =
0.02189 0.00267 0.00782 -0.00491
O2 5 0.858633 0.829346 1.104339 11.00000 0.05662 0.03204 =
0.03242 -0.00364 0.01924 0.00565
N1 4 0.864906 0.665698 0.954940 11.00000 0.03780 0.02679 =
0.02216 0.00204 0.01064 0.00722
C1 1 0.893660 0.512883 0.942147 11.00000 0.03374 0.02733 =
0.02486 0.00204 0.01165 0.00432
C2 1 0.890874 0.432600 0.842633 11.00000 0.04374 0.03503 =
0.02553 -0.00160 0.01201 0.00516
AFIX 43
H2 2 0.868176 0.478183 0.771913 11.00000 -1.20000
AFIX 0
C3 1 0.922918 0.281410 0.850630 11.00000 0.05443 0.03445 =
0.03811 -0.00665 0.02023 0.00536
AFIX 43
H3 2 0.921145 0.221844 0.783763 11.00000 -1.20000
AFIX 0
C4 1 0.957219 0.215682 0.953163 11.00000 0.05707 0.03193 =
0.04939 0.00365 0.02462 0.01380
AFIX 43
H4 2 0.978553 0.112444 0.955471 11.00000 -1.20000
AFIX 0
C5 1 0.960830 0.299563 1.053459 11.00000 0.04465 0.03648 =
0.03598 0.01097 0.01530 0.01096
AFIX 43
H5 2 0.984786 0.255493 1.123970 11.00000 -1.20000
AFIX 0
C6 1 0.928424 0.448796 1.046851 11.00000 0.03513 0.03033 =
0.02392 0.00408 0.01145 0.00343
C7 1 0.921527 0.567222 1.132430 11.00000 0.03457 0.03139 =
0.02428 0.00331 0.01093 -0.00120
C8 1 0.877630 0.707825 1.065271 11.00000 0.03742 0.02853 =
0.02285 0.00040 0.01238 0.00062
C9 1 0.823364 0.759125 0.861229 11.00000 0.03738 0.02966 =
0.02554 0.00675 0.01027 0.00563
AFIX 23
H9A 2 0.846127 0.762987 0.799706 11.00000 -1.20000
H9B 2 0.819151 0.872468 0.886282 11.00000 -1.20000
AFIX 0
C10 1 0.753170 0.686827 0.816303 11.00000 0.03685 0.03379 =
0.03017 0.00631 0.01132 0.00289
AFIX 23
H10A 2 0.727660 0.697533 0.873860 11.00000 -1.20000
H10B 2 0.756986 0.569283 0.800587 11.00000 -1.20000
AFIX 0
C11 1 0.715229 0.773750 0.708921 11.00000 0.03393 0.03832 =
0.03060 0.00706 0.00962 0.00280
AFIX 23
H11A 2 0.711684 0.890940 0.725920 11.00000 -1.20000
H11B 2 0.741989 0.765068 0.653024 11.00000 -1.20000
AFIX 0
C12 1 0.644803 0.708012 0.656499 11.00000 0.03531 0.03963 =
0.03646 0.00374 0.01135 0.00029
AFIX 23
H12A 2 0.616860 0.722365 0.710190 11.00000 -1.20000
H12B 2 0.647686 0.589718 0.642263 11.00000 -1.20000
AFIX 0
C13 1 0.610651 0.793676 0.546282 11.00000 0.03268 0.04680 =
0.03573 0.00314 0.00975 0.00067
AFIX 23
H13A 2 0.607081 0.911480 0.561449 11.00000 -1.20000
H13B 2 0.639655 0.782183 0.494000 11.00000 -1.20000
AFIX 0
C14 1 0.540779 0.728992 0.488919 11.00000 0.03653 0.04591 =
0.04133 0.00062 0.00789 -0.00218
AFIX 23
H14A 2 0.511876 0.738333 0.541513 11.00000 -1.20000
H14B 2 0.544331 0.611842 0.471812 11.00000 -1.20000
AFIX 0
C15 1 0.507062 0.818899 0.380387 11.00000 0.03332 0.05146 =
0.03790 0.00025 0.00932 -0.00053
AFIX 23
H15A 2 0.502037 0.935261 0.398112 11.00000 -1.20000
H15B 2 0.536913 0.813268 0.329128 11.00000 -1.20000
AFIX 0
C16 1 0.438163 0.751278 0.319761 11.00000 0.03893 0.05012 =
0.04010 -0.00026 0.00496 -0.00431
AFIX 23
H16A 2 0.409126 0.750231 0.372436 11.00000 -1.20000
H16B 2 0.443516 0.637118 0.297345 11.00000 -1.20000
AFIX 0
C17 1 0.402986 0.849405 0.215102 11.00000 0.03668 0.04680 =
0.03770 -0.00111 0.00838 -0.00049
AFIX 23
H17A 2 0.396679 0.962919 0.237824 11.00000 -1.20000
H17B 2 0.432541 0.852711 0.163291 11.00000 -1.20000
AFIX 0
C18 1 0.334621 0.779681 0.152554 11.00000 0.03840 0.04334 =
0.03675 -0.00105 0.00674 -0.00088
AFIX 23
H18A 2 0.341349 0.670770 0.122508 11.00000 -1.20000
H18B 2 0.306601 0.765498 0.206143 11.00000 -1.20000
AFIX 0
C19 1 0.297206 0.888125 0.056110 11.00000 0.04488 0.03351 =
0.04290 -0.00433 0.00616 0.00400
AFIX 23
H19A 2 0.292143 0.998012 0.086216 11.00000 -1.20000
H19B 2 0.324937 0.899538 0.001841 11.00000 -1.20000
AFIX 0
C20 1 0.228111 0.825585 -0.005923 11.00000 0.04397 0.03987 =
0.04424 -0.00839 0.00498 0.01158
AFIX 23
H20A 2 0.203421 0.911798 -0.056606 11.00000 -1.20000
H20B 2 0.202084 0.798731 0.048907 11.00000 -1.20000
AFIX 0
HKLF 4
REM jtm1769_a.res in P2(1)/c
REM wR2 = 0.0839, GooF = S = 1.060, Restrained GooF = 1.060 for all data
REM R1 = 0.0303 for 3810 Fo > 4sig(Fo) and 0.0323 for all 4091 data
REM 217 parameters refined using 0 restraints
END
WGHT 0.0459 0.8387
REM Highest difference peak 0.441, deepest hole -0.660, 1-sigma level 0.049
Q1 1 0.2589 0.6949 -0.1229 11.00000 0.05 0.44
Q2 1 0.2259 0.7177 -0.1410 11.00000 0.05 0.41
Q3 1 0.9122 0.4716 0.9932 11.00000 0.05 0.32
Q4 1 0.9497 0.2726 0.9030 11.00000 0.05 0.31
Q5 1 0.9021 0.6419 1.1029 11.00000 0.05 0.28
;
_shelx_res_checksum 75603
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Br Br1 0.23573(2) 0.63104(3) -0.09416(2) 0.04517(9) Uani d 1 . .
O O1 0.94289(6) 0.56654(16) 1.23349(9) 0.0368(3) Uani d 1 . .
O O2 0.85863(7) 0.82935(15) 1.10434(10) 0.0389(3) Uani d 1 . .
N N1 0.86491(7) 0.66570(16) 0.95494(10) 0.0284(3) Uani d 1 . .
C C1 0.89366(8) 0.51288(19) 0.94215(12) 0.0279(3) Uani d 1 . .
C C2 0.89087(9) 0.4326(2) 0.84263(13) 0.0342(3) Uani d 1 . .
H H2 0.868176 0.478183 0.771913 0.041 Uiso calc 1 . .
C C3 0.92292(10) 0.2814(2) 0.85063(15) 0.0408(4) Uani d 1 . .
H H3 0.921145 0.221844 0.783763 0.049 Uiso calc 1 . .
C C4 0.95722(11) 0.2157(2) 0.95316(17) 0.0441(4) Uani d 1 . .
H H4 0.978553 0.112444 0.955471 0.053 Uiso calc 1 . .
C C5 0.96083(9) 0.2996(2) 1.05346(15) 0.0381(4) Uani d 1 . .
H H5 0.984786 0.255493 1.123970 0.046 Uiso calc 1 . .
C C6 0.92842(8) 0.44880(19) 1.04685(12) 0.0291(3) Uani d 1 . .
C C7 0.92153(8) 0.5672(2) 1.13243(12) 0.0295(3) Uani d 1 . .
C C8 0.87763(8) 0.70783(19) 1.06527(12) 0.0288(3) Uani d 1 . .
C C9 0.82336(8) 0.75912(19) 0.86123(13) 0.0305(3) Uani d 1 . .
H H9A 0.846127 0.762987 0.799706 0.037 Uiso calc 1 . .
H H9B 0.819151 0.872468 0.886282 0.037 Uiso calc 1 . .
C C10 0.75317(8) 0.6868(2) 0.81630(13) 0.0331(3) Uani d 1 . .
H H10A 0.727660 0.697533 0.873860 0.040 Uiso calc 1 . .
H H10B 0.756986 0.569283 0.800587 0.040 Uiso calc 1 . .
C C11 0.71523(8) 0.7737(2) 0.70892(13) 0.0341(3) Uani d 1 . .
H H11A 0.711684 0.890940 0.725920 0.041 Uiso calc 1 . .
H H11B 0.741989 0.765068 0.653024 0.041 Uiso calc 1 . .
C C12 0.64480(9) 0.7080(2) 0.65650(15) 0.0368(4) Uani d 1 . .
H H12A 0.616860 0.722365 0.710190 0.044 Uiso calc 1 . .
H H12B 0.647686 0.589718 0.642263 0.044 Uiso calc 1 . .
C C13 0.61065(9) 0.7937(2) 0.54628(15) 0.0383(4) Uani d 1 . .
H H13A 0.607081 0.911480 0.561449 0.046 Uiso calc 1 . .
H H13B 0.639655 0.782183 0.494000 0.046 Uiso calc 1 . .
C C14 0.54078(9) 0.7290(2) 0.48892(16) 0.0417(4) Uani d 1 . .
H H14A 0.511876 0.738333 0.541513 0.050 Uiso calc 1 . .
H H14B 0.544331 0.611842 0.471812 0.050 Uiso calc 1 . .
C C15 0.50706(9) 0.8189(3) 0.38039(15) 0.0409(4) Uani d 1 . .
H H15A 0.502037 0.935261 0.398112 0.049 Uiso calc 1 . .
H H15B 0.536913 0.813268 0.329128 0.049 Uiso calc 1 . .
C C16 0.43816(10) 0.7513(3) 0.31976(16) 0.0441(4) Uani d 1 . .
H H16A 0.409126 0.750231 0.372436 0.053 Uiso calc 1 . .
H H16B 0.443516 0.637118 0.297345 0.053 Uiso calc 1 . .
C C17 0.40299(9) 0.8494(2) 0.21510(16) 0.0407(4) Uani d 1 . .
H H17A 0.396679 0.962919 0.237824 0.049 Uiso calc 1 . .
H H17B 0.432541 0.852711 0.163291 0.049 Uiso calc 1 . .
C C18 0.33462(9) 0.7797(2) 0.15255(15) 0.0401(4) Uani d 1 . .
H H18A 0.341349 0.670770 0.122508 0.048 Uiso calc 1 . .
H H18B 0.306601 0.765498 0.206143 0.048 Uiso calc 1 . .
C C19 0.29721(10) 0.8881(2) 0.05611(17) 0.0414(4) Uani d 1 . .
H H19A 0.292143 0.998012 0.086216 0.050 Uiso calc 1 . .
H H19B 0.324937 0.899538 0.001841 0.050 Uiso calc 1 . .
C C20 0.22811(10) 0.8256(2) -0.00592(17) 0.0439(4) Uani d 1 . .
H H20A 0.203421 0.911798 -0.056606 0.053 Uiso calc 1 . .
H H20B 0.202084 0.798731 0.048907 0.053 Uiso calc 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Br1 0.04657(13) 0.04566(14) 0.04404(13) -0.00114(8) 0.01324(9) -0.01268(8)
O1 0.0439(6) 0.0442(7) 0.0219(5) -0.0049(5) 0.0078(4) 0.0027(5)
O2 0.0566(7) 0.0320(6) 0.0324(6) 0.0056(5) 0.0192(5) -0.0036(5)
N1 0.0378(7) 0.0268(6) 0.0222(6) 0.0072(5) 0.0106(5) 0.0020(5)
C1 0.0337(7) 0.0273(7) 0.0249(7) 0.0043(6) 0.0116(6) 0.0020(6)
C2 0.0437(9) 0.0350(8) 0.0255(7) 0.0052(7) 0.0120(6) -0.0016(6)
C3 0.0544(10) 0.0344(9) 0.0381(9) 0.0054(8) 0.0202(8) -0.0067(7)
C4 0.0571(11) 0.0319(9) 0.0494(10) 0.0138(8) 0.0246(9) 0.0036(7)
C5 0.0446(9) 0.0365(9) 0.0360(8) 0.0110(7) 0.0153(7) 0.0110(7)
C6 0.0351(7) 0.0303(8) 0.0239(7) 0.0034(6) 0.0114(6) 0.0041(6)
C7 0.0346(7) 0.0314(8) 0.0243(7) -0.0012(6) 0.0109(6) 0.0033(6)
C8 0.0374(8) 0.0285(7) 0.0229(7) 0.0006(6) 0.0124(6) 0.0004(6)
C9 0.0374(8) 0.0297(7) 0.0255(7) 0.0056(6) 0.0103(6) 0.0067(6)
C10 0.0368(8) 0.0338(8) 0.0302(7) 0.0029(6) 0.0113(6) 0.0063(6)
C11 0.0339(8) 0.0383(8) 0.0306(8) 0.0028(6) 0.0096(6) 0.0071(6)
C12 0.0353(8) 0.0396(9) 0.0365(8) 0.0003(7) 0.0114(7) 0.0037(7)
C13 0.0327(8) 0.0468(10) 0.0357(8) 0.0007(7) 0.0098(7) 0.0031(7)
C14 0.0365(9) 0.0459(10) 0.0413(9) -0.0022(7) 0.0079(7) 0.0006(8)
C15 0.0333(8) 0.0515(10) 0.0379(9) -0.0005(8) 0.0093(7) 0.0002(8)
C16 0.0389(9) 0.0501(10) 0.0401(9) -0.0043(8) 0.0050(7) -0.0003(8)
C17 0.0367(9) 0.0468(10) 0.0377(9) -0.0005(7) 0.0084(7) -0.0011(7)
C18 0.0384(9) 0.0433(9) 0.0367(9) -0.0009(7) 0.0067(7) -0.0011(7)
C19 0.0449(10) 0.0335(8) 0.0429(9) 0.0040(7) 0.0062(8) -0.0043(7)
C20 0.0440(10) 0.0399(9) 0.0442(10) 0.0116(8) 0.0050(8) -0.0084(8)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Br Br -0.6763 1.2805 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
C8 N1 C1 . . 111.16(12) ?
C8 N1 C9 . . 125.20(13) ?
C1 N1 C9 . . 123.53(13) ?
C2 C1 C6 . . 122.08(14) ?
C2 C1 N1 . . 127.01(14) ?
C6 C1 N1 . . 110.90(13) ?
C1 C2 C3 . . 116.91(15) ?
C1 C2 H2 . . 121.5 ?
C3 C2 H2 . . 121.5 ?
C4 C3 C2 . . 121.89(16) ?
C4 C3 H3 . . 119.1 ?
C2 C3 H3 . . 119.1 ?
C3 C4 C5 . . 120.73(16) ?
C3 C4 H4 . . 119.6 ?
C5 C4 H4 . . 119.6 ?
C6 C5 C4 . . 117.98(16) ?
C6 C5 H5 . . 121.0 ?
C4 C5 H5 . . 121.0 ?
C5 C6 C1 . . 120.39(14) ?
C5 C6 C7 . . 132.69(15) ?
C1 C6 C7 . . 106.93(13) ?
O1 C7 C6 . . 131.37(15) ?
O1 C7 C8 . . 123.61(15) ?
C6 C7 C8 . . 105.03(12) ?
O2 C8 N1 . . 127.38(15) ?
O2 C8 C7 . . 126.65(14) ?
N1 C8 C7 . . 105.96(12) ?
N1 C9 C10 . . 112.60(13) ?
N1 C9 H9A . . 109.1 ?
C10 C9 H9A . . 109.1 ?
N1 C9 H9B . . 109.1 ?
C10 C9 H9B . . 109.1 ?
H9A C9 H9B . . 107.8 ?
C9 C10 C11 . . 110.67(13) ?
C9 C10 H10A . . 109.5 ?
C11 C10 H10A . . 109.5 ?
C9 C10 H10B . . 109.5 ?
C11 C10 H10B . . 109.5 ?
H10A C10 H10B . . 108.1 ?
C12 C11 C10 . . 114.56(14) ?
C12 C11 H11A . . 108.6 ?
C10 C11 H11A . . 108.6 ?
C12 C11 H11B . . 108.6 ?
C10 C11 H11B . . 108.6 ?
H11A C11 H11B . . 107.6 ?
C11 C12 C13 . . 112.25(14) ?
C11 C12 H12A . . 109.2 ?
C13 C12 H12A . . 109.2 ?
C11 C12 H12B . . 109.2 ?
C13 C12 H12B . . 109.2 ?
H12A C12 H12B . . 107.9 ?
C14 C13 C12 . . 114.24(15) ?
C14 C13 H13A . . 108.7 ?
C12 C13 H13A . . 108.7 ?
C14 C13 H13B . . 108.7 ?
C12 C13 H13B . . 108.7 ?
H13A C13 H13B . . 107.6 ?
C13 C14 C15 . . 113.28(16) ?
C13 C14 H14A . . 108.9 ?
C15 C14 H14A . . 108.9 ?
C13 C14 H14B . . 108.9 ?
C15 C14 H14B . . 108.9 ?
H14A C14 H14B . . 107.7 ?
C16 C15 C14 . . 113.84(16) ?
C16 C15 H15A . . 108.8 ?
C14 C15 H15A . . 108.8 ?
C16 C15 H15B . . 108.8 ?
C14 C15 H15B . . 108.8 ?
H15A C15 H15B . . 107.7 ?
C15 C16 C17 . . 113.24(16) ?
C15 C16 H16A . . 108.9 ?
C17 C16 H16A . . 108.9 ?
C15 C16 H16B . . 108.9 ?
C17 C16 H16B . . 108.9 ?
H16A C16 H16B . . 107.7 ?
C18 C17 C16 . . 113.39(16) ?
C18 C17 H17A . . 108.9 ?
C16 C17 H17A . . 108.9 ?
C18 C17 H17B . . 108.9 ?
C16 C17 H17B . . 108.9 ?
H17A C17 H17B . . 107.7 ?
C19 C18 C17 . . 112.64(16) ?
C19 C18 H18A . . 109.1 ?
C17 C18 H18A . . 109.1 ?
C19 C18 H18B . . 109.1 ?
C17 C18 H18B . . 109.1 ?
H18A C18 H18B . . 107.8 ?
C20 C19 C18 . . 114.25(16) ?
C20 C19 H19A . . 108.7 ?
C18 C19 H19A . . 108.7 ?
C20 C19 H19B . . 108.7 ?
C18 C19 H19B . . 108.7 ?
H19A C19 H19B . . 107.6 ?
C19 C20 Br1 . . 110.79(13) ?
C19 C20 H20A . . 109.5 ?
Br1 C20 H20A . . 109.5 ?
C19 C20 H20B . . 109.5 ?
Br1 C20 H20B . . 109.5 ?
H20A C20 H20B . . 108.1 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Br1 C20 . 1.9593(18) ?
O1 C7 . 1.2064(19) ?
O2 C8 . 1.214(2) ?
N1 C8 . 1.3595(19) ?
N1 C1 . 1.4113(19) ?
N1 C9 . 1.4593(19) ?
C1 C2 . 1.379(2) ?
C1 C6 . 1.402(2) ?
C2 C3 . 1.395(2) ?
C2 H2 . 0.9500 ?
C3 C4 . 1.384(3) ?
C3 H3 . 0.9500 ?
C4 C5 . 1.399(3) ?
C4 H4 . 0.9500 ?
C5 C6 . 1.385(2) ?
C5 H5 . 0.9500 ?
C6 C7 . 1.467(2) ?
C7 C8 . 1.560(2) ?
C9 C10 . 1.522(2) ?
C9 H9A . 0.9900 ?
C9 H9B . 0.9900 ?
C10 C11 . 1.524(2) ?
C10 H10A . 0.9900 ?
C10 H10B . 0.9900 ?
C11 C12 . 1.519(2) ?
C11 H11A . 0.9900 ?
C11 H11B . 0.9900 ?
C12 C13 . 1.526(2) ?
C12 H12A . 0.9900 ?
C12 H12B . 0.9900 ?
C13 C14 . 1.519(2) ?
C13 H13A . 0.9900 ?
C13 H13B . 0.9900 ?
C14 C15 . 1.524(3) ?
C14 H14A . 0.9900 ?
C14 H14B . 0.9900 ?
C15 C16 . 1.521(3) ?
C15 H15A . 0.9900 ?
C15 H15B . 0.9900 ?
C16 C17 . 1.530(3) ?
C16 H16A . 0.9900 ?
C16 H16B . 0.9900 ?
C17 C18 . 1.524(2) ?
C17 H17A . 0.9900 ?
C17 H17B . 0.9900 ?
C18 C19 . 1.521(3) ?
C18 H18A . 0.9900 ?
C18 H18B . 0.9900 ?
C19 C20 . 1.514(3) ?
C19 H19A . 0.9900 ?
C19 H19B . 0.9900 ?
C20 H20A . 0.9900 ?
C20 H20B . 0.9900 ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
C2 H2 O2 4_575 0.95 2.56 3.441(2) 154 yes
C3 H3 O1 4_565 0.95 2.51 3.271(2) 137 y
C5 H5 O1 2_747 0.95 2.51 3.424(2) 160 y
C9 H9A O2 4_575 0.99 2.60 3.503(2) 152 yes
C20 H20A O2 3_676 0.99 2.47 3.393(2) 156 yes
C20 H20B Cg2 3_666 0.99 2.96 3.756(2) 139 y
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
C8 N1 C1 C2 . . . . -179.95(16) ?
C9 N1 C1 C2 . . . . 3.8(3) ?
C8 N1 C1 C6 . . . . -1.14(19) ?
C9 N1 C1 C6 . . . . -177.41(14) ?
C6 C1 C2 C3 . . . . 1.6(3) ?
N1 C1 C2 C3 . . . . -179.68(16) ?
C1 C2 C3 C4 . . . . -1.3(3) ?
C2 C3 C4 C5 . . . . 0.1(3) ?
C3 C4 C5 C6 . . . . 0.8(3) ?
C4 C5 C6 C1 . . . . -0.5(3) ?
C4 C5 C6 C7 . . . . 179.77(18) ?
C2 C1 C6 C5 . . . . -0.8(3) ?
N1 C1 C6 C5 . . . . -179.66(15) ?
C2 C1 C6 C7 . . . . 179.05(15) ?
N1 C1 C6 C7 . . . . 0.16(18) ?
C5 C6 C7 O1 . . . . 0.3(3) ?
C1 C6 C7 O1 . . . . -179.48(17) ?
C5 C6 C7 C8 . . . . -179.49(18) ?
C1 C6 C7 C8 . . . . 0.71(16) ?
C1 N1 C8 O2 . . . . -178.14(16) ?
C9 N1 C8 O2 . . . . -1.9(3) ?
C1 N1 C8 C7 . . . . 1.52(17) ?
C9 N1 C8 C7 . . . . 177.72(14) ?
O1 C7 C8 O2 . . . . -1.5(3) ?
C6 C7 C8 O2 . . . . 178.29(16) ?
O1 C7 C8 N1 . . . . 178.80(15) ?
C6 C7 C8 N1 . . . . -1.37(16) ?
C8 N1 C9 C10 . . . . -101.92(18) ?
C1 N1 C9 C10 . . . . 73.83(19) ?
N1 C9 C10 C11 . . . . -172.10(13) ?
C9 C10 C11 C12 . . . . 179.03(14) ?
C10 C11 C12 C13 . . . . -177.09(15) ?
C11 C12 C13 C14 . . . . 178.41(15) ?
C12 C13 C14 C15 . . . . 178.72(16) ?
C13 C14 C15 C16 . . . . 177.83(17) ?
C14 C15 C16 C17 . . . . 176.30(16) ?
C15 C16 C17 C18 . . . . 178.65(16) ?
C16 C17 C18 C19 . . . . 174.02(16) ?
C17 C18 C19 C20 . . . . -178.23(16) ?
C18 C19 C20 Br1 . . . . -70.41(19) ?
_cod_database_fobs_code 2022919