#------------------------------------------------------------------------------ #$Date: 2023-12-07 12:50:57 +0100 (Thu, 07 Dec 2023) $ #$Revision: 288144 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/29/2022909.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022909 loop_ _publ_author_name 'Gliese, Philipp J.' 'Appiarius, Yannik' 'Scheele, Tarek' 'Lork, Enno' 'Neudecker, Tim' 'Staubitz, Anne' _publ_section_title ; Synthesis and crystal structure of 2-(anthracen-9-yl)-1-(tert-butyl-dimethyl-sil-yl)-3,6-di-hydro-1λ4,2λ4-aza-borinine. ; _journal_coeditor_code VM2290 _journal_issue 'Pt 11' _journal_name_full 'Acta crystallographica. Section E, Crystallographic communications' _journal_page_first 1012 _journal_page_last 1016 _journal_paper_doi 10.1107/S2056989023008381 _journal_volume 79 _journal_year 2023 _chemical_formula_iupac 'C24 H30 B N Si' _chemical_formula_moiety 'C24 H30 B N Si' _chemical_formula_sum 'C24 H30 B N Si' _chemical_formula_weight 371.39 _chemical_name_systematic 2-(Anthracen-9-yl)-1-(tert-butyldimethylsilyl)-3,6-dihydro-1\l^4^,2\l^4^-azaborinine _space_group_crystal_system orthorhombic _space_group_IT_number 61 _space_group_name_Hall '-P 2ac 2ab' _space_group_name_H-M_alt 'P b c a' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_method ; Olex2 1.5 (compiled 2023.03.06 svn.rbb2c1857 for OlexSys, GUI svn.r6748) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 13.3292(6) _cell_length_b 11.1365(5) _cell_length_c 28.5973(12) _cell_measurement_reflns_used 9845 _cell_measurement_temperature 100.0 _cell_measurement_theta_max 30.46 _cell_measurement_theta_min 2.49 _cell_volume 4245.0(3) _computing_cell_refinement ; SAINT V8.40A (Bruker, 2019) ; _computing_data_collection ; PHOTON (Bruker, 2019) ; _computing_data_reduction ; SAINT V8.40A (Bruker, 2019) ; _computing_molecular_graphics ; Olex2 1.5 (Dolomanov et al., 2009) ORTEP-3 for Windows (Farrugia, 2012) ; _computing_publication_material ; Olex2 1.5 (Dolomanov et al., 2009), publCIF (Westrip, (2010) ; _computing_structure_refinement ; SHELXL Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2014/5 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 100.00 _diffrn_detector 'Bruker Photon 100 area detector' _diffrn_detector_area_resol_mean 7.9 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device 'three-circle diffractometer' _diffrn_measurement_device_type 'Bruker Photon 100' _diffrn_measurement_method '\w and \f scans' _diffrn_radiation_monochromator 'mirror optics' _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0486 _diffrn_reflns_av_unetI/netI 0.0227 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 38 _diffrn_reflns_limit_l_min -38 _diffrn_reflns_number 67479 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.281 _diffrn_reflns_theta_min 2.487 _diffrn_source 'microfocus sealed X-ray tube' _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.119 _exptl_absorpt_correction_T_max 0.7461 _exptl_absorpt_correction_T_min 0.7067 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.162 _exptl_crystal_description block _exptl_crystal_F_000 1600 _exptl_crystal_size_max 0.28 _exptl_crystal_size_mid 0.22 _exptl_crystal_size_min 0.2 _refine_diff_density_max 0.370 _refine_diff_density_min -0.285 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.068 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 249 _refine_ls_number_reflns 5264 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.068 _refine_ls_R_factor_all 0.0541 _refine_ls_R_factor_gt 0.0421 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0421P)^2^+2.6379P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0980 _refine_ls_wR_factor_ref 0.1033 _reflns_number_gt 4416 _reflns_number_total 5264 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file vm2290sup1.cif _cod_data_source_block I _cod_depositor_comments 'Adding full bibliography for 2022909.cif.' _cod_database_code 2022909 _cod_database_fobs_code 2022909 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.967 _shelx_estimated_absorpt_t_max 0.977 _shelx_hkl_file ; 0 -2 0 98.19 2.40 0 -2 0 94.09 2.70 0 2 0 98.39 2.40 0 2 0 97.79 2.70 0 -3 0 0.20 0.50 0 -3 0 0.50 0.40 0 3 0 0.00 0.40 0 3 0 -0.10 0.50 0 3 0 0.30 0.50 0 -3 0 0.20 0.40 0 4 0 -0.50 0.60 0 -4 0 0.50 0.70 0 4 0 -0.80 0.50 0 4 0 1.00 0.70 0 -4 0 0.90 0.60 0 -4 0 1.00 0.50 0 5 0 0.50 0.80 0 -5 0 1.00 0.70 0 -5 0 0.20 0.80 0 -5 0 -0.60 0.60 0 5 0 -0.20 0.90 0 5 0 1.10 0.70 0 6 0 825.22 18.60 0 -6 0 823.92 18.80 0 -6 0 793.82 17.70 0 -6 0 828.22 18.40 0 6 0 806.42 18.60 0 6 0 838.12 17.70 0 -7 0 0.10 1.00 0 7 0 -0.50 1.10 0 7 0 -0.20 1.00 0 -7 0 -0.50 0.90 0 7 0 -0.60 1.00 0 -7 0 0.60 1.40 0 -8 0 128.29 5.10 0 -8 0 140.39 5.80 0 -8 0 134.09 4.50 0 8 0 130.79 5.40 0 8 0 129.79 5.40 0 8 0 126.69 4.70 0 9 0 -3.50 1.50 0 9 0 -1.80 2.00 0 -9 0 3.00 2.30 0 9 0 -1.40 1.60 0 -9 0 -0.50 1.30 0 -9 0 -1.10 1.50 0 -10 0 91.49 4.30 0 10 0 95.59 5.30 0 10 0 94.59 5.60 0 10 0 92.19 4.80 0 -10 0 81.19 5.90 0 -10 0 95.29 5.00 0 11 0 0.30 2.50 0 11 0 3.60 3.30 0 11 0 6.10 2.60 0 -11 0 -2.00 1.90 0 12 0 25.60 5.10 0 -12 0 29.40 3.30 0 12 0 27.10 4.10 0 12 0 29.40 4.10 0 13 0 -0.60 3.30 0 13 0 -2.40 3.90 0 -13 0 -2.40 2.80 0 14 0 38.00 5.70 0 -14 0 35.80 4.20 1 1 0 -0.30 0.20 -1 1 0 -0.30 0.20 -1 1 0 -0.10 0.10 1 1 0 -0.10 0.20 1 -1 0 -0.10 0.20 1 -1 0 -0.20 0.20 -1 -1 0 0.00 0.10 -1 -1 0 0.00 0.20 -1 -1 0 0.30 0.20 -1 -2 0 0.40 0.30 -1 2 0 -0.10 0.40 1 -2 0 -0.10 0.40 1 -2 0 -0.30 0.40 -1 -2 0 0.90 0.40 -1 -2 0 -0.50 0.30 -1 2 0 0.20 0.40 1 2 0 -0.10 0.40 1 2 0 0.00 0.20 -1 2 0 0.20 0.40 1 2 0 -0.40 0.40 -1 3 0 -0.10 0.50 1 3 0 -0.30 0.40 1 3 0 0.40 0.60 -1 3 0 0.10 0.50 1 3 0 0.70 0.40 1 -3 0 -0.30 0.50 -1 3 0 -0.90 0.40 -1 -3 0 0.30 0.40 -1 -3 0 0.80 0.50 -1 -3 0 0.20 0.50 1 -3 0 -0.20 0.50 1 -4 0 0.20 0.70 1 4 0 -0.70 0.60 -1 4 0 0.60 0.60 -1 -4 0 -0.30 0.60 -1 -4 0 0.20 0.50 -1 4 0 0.50 0.70 -1 4 0 -0.30 0.70 1 4 0 -0.20 0.50 -1 -4 0 1.10 0.80 1 4 0 -0.50 0.60 1 5 0 -0.90 0.80 1 5 0 1.10 0.80 1 -5 0 0.50 0.60 1 5 0 0.40 0.60 1 -5 0 -0.60 0.90 -1 -5 0 0.10 0.70 -1 5 0 0.50 0.80 -1 5 0 1.10 0.80 -1 -5 0 -0.40 0.90 1 -5 0 -0.60 0.70 -1 5 0 -1.00 0.70 -1 -6 0 0.20 0.80 1 6 0 1.20 0.90 1 -6 0 0.10 1.00 1 -6 0 1.80 0.90 -1 -6 0 -0.20 0.80 1 6 0 0.50 1.10 1 6 0 0.00 0.80 -1 6 0 0.50 0.90 -1 6 0 0.70 1.00 -1 6 0 1.40 0.90 -1 -6 0 -0.30 1.20 -1 7 0 0.70 1.30 1 7 0 1.60 1.20 1 -7 0 -0.10 1.00 1 -7 0 0.20 1.60 -1 7 0 1.00 1.20 -1 7 0 0.00 1.20 1 7 0 1.80 1.00 -1 -7 0 -0.60 0.90 -1 -7 0 1.90 1.00 1 7 0 -1.10 1.20 -1 -7 0 0.40 1.50 1 8 0 0.90 1.20 -1 -8 0 0.40 1.60 1 -8 0 -1.60 1.20 -1 8 0 0.20 1.40 -1 -8 0 1.70 1.10 -1 8 0 -0.40 1.30 1 -8 0 1.40 1.70 -1 -8 0 -1.50 1.30 1 8 0 0.50 1.70 -1 8 0 -0.70 1.40 1 8 0 -2.20 1.20 1 -9 0 -1.60 1.30 -1 -9 0 2.20 1.70 -1 -9 0 -1.00 1.20 -1 9 0 -0.10 1.70 1 -9 0 1.60 2.10 -1 -9 0 1.60 2.20 -1 9 0 1.10 1.60 1 9 0 0.50 1.60 1 9 0 -1.70 1.50 -1 9 0 2.80 2.00 1 9 0 3.50 2.20 -1 -10 0 -1.40 2.90 -1 -10 0 -1.50 2.00 1 10 0 3.00 2.70 -1 -10 0 -3.60 1.50 -1 10 0 1.40 2.20 -1 10 0 0.70 2.40 -1 10 0 -0.10 1.90 1 -10 0 0.70 1.60 1 10 0 -1.70 1.90 1 -10 0 1.20 2.60 1 10 0 -0.90 2.00 -1 -11 0 -0.10 1.80 -1 11 0 1.00 2.70 -1 11 0 1.20 3.20 1 -11 0 1.40 2.10 -1 11 0 -0.10 2.30 1 11 0 -1.80 2.40 1 11 0 -1.50 2.20 1 11 0 -2.10 3.00 -1 -11 0 1.40 2.30 -1 12 0 0.80 2.80 -1 12 0 0.80 3.40 1 -12 0 1.20 2.60 -1 -12 0 0.10 2.70 1 12 0 2.60 3.00 1 12 0 -5.60 4.00 -1 12 0 0.80 3.60 -1 -12 0 0.40 2.30 1 12 0 1.90 2.90 -1 13 0 6.50 3.60 1 13 0 -6.60 3.70 1 13 0 9.50 3.70 1 -13 0 -1.20 2.80 -1 -13 0 -4.60 2.60 -1 13 0 -3.50 4.30 1 -14 0 -1.20 3.60 -1 -14 0 1.20 3.30 -1 14 0 6.80 4.20 1 14 0 4.30 4.20 -2 0 0 683.63 13.60 -2 0 0 692.33 13.70 2 0 0 668.03 13.70 2 0 0 582.94 13.60 2 0 0 683.83 13.20 2 1 0 27.50 1.00 -2 -1 0 26.50 1.00 -2 1 0 32.60 1.20 2 1 0 25.60 1.20 2 -1 0 26.60 1.20 -2 1 0 26.00 1.20 2 1 0 27.60 1.00 2 -1 0 27.90 0.90 -2 -1 0 25.10 1.20 -2 1 0 28.20 0.90 -2 -1 0 28.40 1.00 -2 2 0 128.29 3.30 2 2 0 127.79 3.50 -2 2 0 129.19 3.50 2 -2 0 132.39 3.40 2 -2 0 130.99 3.50 -2 -2 0 131.39 3.10 -2 -2 0 130.79 3.50 2 2 0 134.79 3.60 -2 -2 0 134.29 3.60 2 3 0 41.10 1.90 -2 -3 0 38.50 1.80 2 3 0 37.40 1.40 -2 3 0 39.10 1.80 2 -3 0 39.30 1.70 -2 3 0 40.40 1.70 -2 -3 0 39.50 1.80 -2 -3 0 38.70 1.30 2 4 0 58.69 2.60 -2 4 0 65.99 2.50 -2 4 0 61.29 2.50 -2 -4 0 65.09 2.00 2 4 0 66.29 2.10 -2 -4 0 69.09 2.70 2 -4 0 67.69 2.70 -2 4 0 69.09 2.70 2 -4 0 62.69 2.50 -2 -4 0 62.99 2.70 -2 -5 0 533.25 12.70 2 5 0 513.75 12.60 -2 5 0 524.55 12.40 -2 5 0 531.45 12.50 -2 -5 0 532.85 12.50 -2 -5 0 532.45 11.60 2 5 0 539.55 12.60 2 -5 0 524.05 12.20 2 5 0 540.55 11.60 -2 5 0 545.15 12.20 2 -5 0 549.95 12.60 -2 -6 0 295.77 7.20 2 6 0 308.67 8.40 2 -6 0 306.17 7.90 -2 -6 0 305.27 8.30 -2 6 0 305.97 7.80 2 -6 0 310.47 8.40 -2 6 0 296.17 8.20 2 6 0 292.37 8.30 -2 6 0 303.67 8.30 2 6 0 305.47 7.30 -2 -6 0 309.37 8.50 2 7 0 12.70 1.40 -2 -7 0 9.60 1.30 -2 7 0 12.30 1.90 2 7 0 10.90 1.70 -2 -7 0 12.10 1.80 -2 7 0 13.10 1.80 -2 -7 0 10.50 1.70 2 7 0 10.60 1.80 -2 7 0 12.30 1.60 2 -7 0 8.40 1.80 2 -7 0 11.60 1.70 -2 8 0 2.00 1.50 2 -8 0 2.30 1.30 2 8 0 0.30 1.20 2 -8 0 3.30 2.00 -2 8 0 3.40 1.70 -2 -8 0 0.00 1.80 -2 -8 0 3.20 1.10 2 8 0 1.50 1.60 -2 8 0 0.50 1.50 -2 -8 0 2.40 1.50 2 8 0 4.40 1.90 -2 9 0 13.40 2.70 -2 9 0 6.50 2.00 2 9 0 8.70 2.10 -2 -9 0 10.60 1.60 -2 -9 0 12.20 2.30 -2 9 0 10.10 2.30 -2 -9 0 11.20 2.70 2 -9 0 9.60 1.90 2 9 0 11.90 2.30 2 -9 0 9.50 2.60 -2 10 0 9.10 2.80 -2 10 0 11.40 2.70 2 10 0 9.40 2.20 2 10 0 10.50 2.90 -2 -10 0 13.20 2.70 2 -10 0 11.10 2.30 -2 -10 0 8.10 3.70 -2 -10 0 12.40 1.90 2 -10 0 9.10 3.50 2 10 0 12.40 2.50 -2 10 0 11.80 2.50 -2 11 0 31.00 4.30 2 11 0 30.40 3.80 2 11 0 26.60 3.10 -2 11 0 34.00 4.30 -2 -11 0 33.30 3.80 2 11 0 39.30 4.90 -2 11 0 27.70 3.70 2 -11 0 27.20 3.20 -2 -11 0 29.70 3.10 -2 -12 0 16.90 2.70 2 12 0 8.00 4.60 -2 12 0 11.40 3.80 -2 12 0 11.10 4.50 -2 -12 0 8.80 3.00 2 12 0 12.50 3.40 2 12 0 6.60 3.30 -2 12 0 15.20 3.50 2 -12 0 15.10 3.00 -2 -13 0 5.10 2.90 2 13 0 -1.00 3.40 -2 13 0 7.80 3.70 -2 -13 0 4.00 3.80 2 -13 0 8.70 3.30 2 14 0 30.20 5.00 -2 14 0 22.60 5.10 2 -14 0 31.40 4.40 -2 -14 0 35.30 4.00 -3 0 0 0.20 0.50 3 0 0 0.10 0.40 -3 0 0 -0.50 0.40 3 0 0 0.60 0.50 -3 1 0 0.50 0.50 3 1 0 -0.60 0.30 3 1 0 0.10 0.40 -3 1 0 1.30 0.50 -3 1 0 -0.10 0.30 3 -1 0 -0.30 0.40 3 -1 0 0.10 0.40 3 -1 0 -0.20 0.30 -3 -1 0 -0.10 0.30 3 1 0 -0.30 0.50 -3 -1 0 0.30 0.40 -3 -1 0 0.20 0.50 3 2 0 -0.20 0.40 -3 2 0 -0.10 0.50 -3 2 0 -0.10 0.40 -3 -2 0 0.20 0.50 3 2 0 -0.20 0.50 -3 -2 0 0.70 0.60 -3 -2 0 0.40 0.40 3 -2 0 0.20 0.40 3 -3 0 0.30 0.50 3 3 0 -0.80 0.60 3 -3 0 0.20 0.60 -3 3 0 0.50 0.60 3 3 0 0.10 0.60 -3 -3 0 0.50 0.40 -3 -3 0 0.30 0.60 -3 3 0 0.20 0.50 -3 -3 0 -0.10 0.60 -3 4 0 0.10 0.60 -3 -4 0 0.20 1.00 3 4 0 0.50 0.70 3 4 0 0.00 0.70 -3 -4 0 0.20 0.50 -3 -4 0 0.50 0.70 -3 4 0 0.40 0.80 3 -4 0 0.40 0.70 3 -4 0 0.50 0.70 -3 -5 0 -0.50 0.80 -3 5 0 -0.90 0.80 -3 -5 0 -0.70 0.90 3 -5 0 0.60 0.80 -3 -5 0 -0.20 0.50 3 5 0 -0.10 0.90 3 -5 0 -0.50 0.80 3 5 0 0.60 0.90 3 5 0 -0.80 0.60 -3 5 0 0.10 0.80 -3 5 0 0.60 0.90 -3 -6 0 0.50 1.10 -3 -6 0 0.50 0.70 3 -6 0 -0.30 1.00 -3 6 0 -0.50 1.00 3 6 0 0.60 1.20 -3 -6 0 -0.10 1.30 3 -6 0 0.00 1.10 3 6 0 0.60 1.00 -3 6 0 -1.90 0.90 3 6 0 0.10 0.80 -3 6 0 -0.80 1.10 3 7 0 0.20 1.20 -3 7 0 -1.30 1.30 -3 -7 0 0.00 1.30 3 -7 0 -0.60 1.40 3 7 0 0.30 1.40 -3 7 0 0.10 1.20 -3 -7 0 0.20 0.90 -3 7 0 0.60 1.30 3 7 0 0.70 1.00 -3 -7 0 -1.60 1.10 3 -7 0 -0.30 1.10 3 8 0 -1.50 1.40 -3 -8 0 0.50 1.40 3 8 0 1.20 1.90 3 8 0 -0.80 1.10 -3 8 0 -0.30 1.40 3 -8 0 -0.60 1.30 -3 8 0 -1.90 1.60 -3 8 0 1.40 1.70 -3 -8 0 -2.20 1.70 -3 -8 0 0.50 0.90 3 -8 0 -0.20 1.80 -3 9 0 -1.10 1.70 -3 9 0 -2.10 2.00 -3 9 0 1.40 1.90 3 9 0 0.10 1.40 3 -9 0 0.30 1.60 -3 -9 0 1.70 2.30 -3 -9 0 2.20 1.80 3 9 0 0.70 2.50 3 -9 0 -1.90 2.20 -3 -9 0 -0.20 1.30 3 9 0 0.90 1.90 3 10 0 -0.60 2.10 -3 -10 0 -4.20 2.10 3 10 0 1.00 1.90 -3 10 0 -1.40 2.10 -3 10 0 2.40 2.70 -3 -10 0 -1.80 1.40 3 -10 0 -0.70 2.90 3 -10 0 0.30 2.00 3 10 0 -3.70 2.80 -3 10 0 -0.70 2.50 -3 -11 0 0.90 1.70 -3 -11 0 -3.60 2.10 -3 11 0 2.00 3.20 3 11 0 2.40 2.40 -3 11 0 -0.50 2.30 3 -11 0 0.20 2.20 -3 11 0 1.30 3.20 3 11 0 -2.10 2.30 3 11 0 5.80 3.80 3 12 0 1.10 4.70 3 12 0 3.70 3.00 -3 -12 0 -0.70 2.10 -3 12 0 4.50 2.90 -3 12 0 -8.80 3.90 -3 -12 0 5.30 2.90 3 12 0 -4.30 2.80 -3 12 0 -3.50 4.40 3 -12 0 3.30 2.80 -3 -13 0 -1.80 4.20 -3 -13 0 -0.10 2.60 3 13 0 -2.10 3.40 -3 13 0 -4.00 3.50 3 -13 0 -4.00 3.10 3 -14 0 1.40 4.30 -3 -14 0 -0.30 3.30 -3 14 0 3.80 4.20 3 14 0 1.40 4.40 -4 0 0 117.29 3.40 -4 0 0 115.29 3.30 4 0 0 114.89 3.30 4 0 0 111.79 3.30 -4 1 0 68.19 2.40 4 1 0 68.19 2.00 4 -1 0 65.39 2.40 -4 -1 0 68.49 2.20 4 1 0 66.69 2.20 4 1 0 65.49 2.40 4 -1 0 64.29 2.30 4 -1 0 68.59 1.80 -4 -1 0 70.99 2.50 -4 2 0 500.15 11.10 -4 -2 0 497.55 11.20 -4 2 0 482.05 11.10 4 2 0 502.15 10.80 -4 -2 0 491.95 10.80 -4 2 0 490.25 10.40 4 -2 0 490.75 11.20 4 2 0 492.45 11.20 -4 -2 0 486.45 10.60 4 -2 0 490.25 10.50 -4 -3 0 20.40 1.20 -4 3 0 20.90 1.30 -4 -3 0 21.00 1.20 4 -3 0 19.60 1.60 4 -3 0 21.20 1.40 -4 3 0 23.20 1.70 -4 -3 0 20.00 1.50 4 3 0 20.00 1.70 -4 -3 0 19.40 1.60 4 3 0 22.90 1.50 -4 -4 0 44.80 1.70 4 -4 0 42.50 2.30 4 4 0 41.10 2.30 -4 -4 0 43.10 2.40 -4 4 0 43.20 2.10 -4 4 0 43.90 2.40 4 -4 0 42.20 2.20 -4 -4 0 43.40 2.40 4 4 0 40.20 2.40 4 5 0 149.39 5.10 -4 5 0 155.08 4.80 -4 5 0 158.48 5.00 4 -5 0 148.99 4.90 -4 -5 0 154.98 5.20 -4 -5 0 152.38 4.00 4 -5 0 152.78 4.80 4 5 0 152.98 5.00 -4 -6 0 189.38 5.00 -4 6 0 200.78 6.10 -4 6 0 187.28 6.10 4 6 0 188.68 6.30 -4 -6 0 190.88 6.20 4 -6 0 192.48 6.00 4 6 0 176.18 6.00 4 -6 0 187.28 5.90 -4 6 0 193.18 5.90 -4 -6 0 194.68 6.30 4 7 0 68.79 4.10 -4 -7 0 70.39 4.00 4 -7 0 71.19 3.60 4 7 0 70.69 3.80 -4 -7 0 68.39 3.80 -4 7 0 67.89 3.60 -4 7 0 62.49 3.80 -4 7 0 70.89 3.70 4 -7 0 71.49 3.90 -4 -7 0 71.39 2.70 4 -8 0 64.29 3.80 -4 8 0 66.69 4.10 -4 8 0 65.49 3.80 4 8 0 62.69 4.00 -4 8 0 62.49 4.20 4 8 0 58.39 3.00 -4 -8 0 54.99 4.20 -4 -8 0 67.49 4.20 4 8 0 61.49 4.40 -4 -8 0 67.69 2.80 4 -8 0 66.19 4.30 -4 -9 0 45.10 4.60 4 9 0 57.79 4.30 -4 -9 0 49.30 2.80 -4 9 0 53.49 4.20 -4 -9 0 56.79 4.20 -4 9 0 54.39 4.00 4 9 0 50.69 4.70 4 9 0 54.69 3.10 4 -9 0 63.89 4.90 -4 9 0 50.19 4.60 4 -9 0 46.40 3.80 -4 10 0 149.49 6.70 -4 -10 0 149.88 6.90 4 10 0 156.98 7.10 -4 10 0 159.28 6.70 4 -10 0 152.88 6.30 4 -10 0 145.59 7.50 4 10 0 149.39 7.60 -4 10 0 148.39 7.10 -4 -10 0 148.29 5.00 -4 -11 0 3.60 2.90 4 11 0 2.10 2.40 -4 11 0 3.10 2.60 -4 11 0 0.60 3.20 4 -11 0 2.40 2.40 4 11 0 -4.70 3.50 -4 -11 0 2.40 1.80 4 11 0 1.80 2.70 -4 11 0 4.90 3.50 -4 -12 0 163.28 5.70 -4 12 0 167.78 8.00 -4 -12 0 151.58 8.00 4 -12 0 169.08 7.50 4 12 0 144.89 9.50 4 12 0 139.89 6.40 -4 12 0 158.38 9.20 4 12 0 182.28 8.50 4 -13 0 85.19 7.00 4 13 0 65.29 6.80 -4 13 0 65.79 6.60 -4 -13 0 80.69 4.70 4 -14 0 159.28 8.40 -4 14 0 130.29 8.70 -4 -14 0 150.68 8.50 4 14 0 134.99 9.70 -5 0 0 0.30 0.70 5 0 0 1.00 0.70 5 0 0 0.90 0.70 -5 0 0 1.10 0.70 -5 1 0 1.40 0.80 5 -1 0 0.20 0.70 -5 -1 0 0.70 0.80 -5 1 0 0.20 0.30 5 1 0 0.00 0.70 5 1 0 0.50 0.60 -5 -1 0 -0.10 0.60 5 1 0 -0.20 0.40 -5 1 0 0.90 0.60 5 -1 0 0.00 0.60 -5 2 0 0.10 0.40 5 2 0 -0.30 0.80 -5 2 0 0.00 0.70 5 2 0 -0.30 0.60 -5 -2 0 -0.70 0.60 5 -2 0 0.10 0.50 5 -2 0 -1.10 0.70 -5 2 0 1.00 0.70 -5 -3 0 0.70 0.70 -5 -3 0 -0.70 0.60 5 -3 0 1.00 0.60 5 -3 0 -1.10 0.80 -5 -3 0 -0.60 0.70 5 3 0 -0.80 0.90 -5 3 0 0.00 0.80 5 3 0 -0.20 0.70 -5 3 0 -0.50 0.90 -5 3 0 0.60 0.60 -5 -4 0 -0.40 0.90 5 4 0 -0.10 0.80 -5 4 0 -0.10 0.70 -5 -4 0 0.40 0.70 -5 -4 0 0.60 0.90 5 -4 0 0.70 0.80 -5 4 0 -1.10 0.90 5 -4 0 0.80 0.90 5 4 0 -1.30 1.00 -5 -5 0 -0.50 0.70 -5 -5 0 -0.20 1.70 5 5 0 1.20 1.00 -5 -5 0 0.20 0.70 -5 -5 0 1.00 1.10 -5 5 0 -0.40 1.10 5 -5 0 0.60 1.00 -5 5 0 -0.20 0.90 5 -5 0 0.90 1.10 5 5 0 -0.20 1.30 5 -6 0 2.10 1.30 -5 6 0 0.90 1.40 -5 -6 0 0.60 0.80 5 6 0 -0.10 1.50 5 6 0 -0.30 1.20 5 -6 0 0.00 1.10 -5 -6 0 -1.60 1.20 -5 6 0 -1.50 1.00 -5 -7 0 -1.90 1.60 -5 7 0 -1.30 1.20 -5 7 0 0.30 1.70 5 -7 0 -0.40 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18.00 1.60 -6 0 0 12.70 1.50 6 1 0 1.60 0.90 6 -1 0 4.70 1.00 6 1 0 5.20 1.10 -6 1 0 1.10 0.90 -6 -1 0 2.20 0.90 6 1 0 2.20 0.60 6 1 0 2.00 0.60 -6 -1 0 4.30 1.00 6 -1 0 3.10 1.00 -6 1 0 3.20 1.00 6 2 0 817.02 18.00 -6 -2 0 811.82 18.10 -6 2 0 803.72 17.90 6 -2 0 799.22 17.80 6 -2 0 810.42 16.80 -6 2 0 813.32 16.70 6 2 0 813.72 17.50 -6 -2 0 819.62 17.50 6 -2 0 809.42 18.10 6 2 0 815.52 17.20 -6 -3 0 141.09 4.80 -6 3 0 138.39 4.80 -6 3 0 137.89 4.70 -6 -3 0 147.49 4.20 -6 3 0 148.59 3.90 6 -3 0 142.59 3.90 6 3 0 144.09 4.30 6 3 0 142.39 4.80 -6 -3 0 145.59 4.30 6 -3 0 142.29 4.80 6 -4 0 635.44 15.20 -6 4 0 642.44 15.00 -6 4 0 668.73 15.20 6 -4 0 641.94 14.30 -6 -4 0 642.84 14.20 -6 -4 0 651.63 15.40 -6 -4 0 648.74 14.70 -6 4 0 653.63 14.20 6 4 0 646.24 15.20 -6 -4 0 648.14 14.10 6 4 0 633.04 14.70 -6 -5 0 892.21 19.10 -6 -5 0 901.31 20.20 -6 -5 0 900.81 20.70 -6 5 0 922.21 19.60 -6 -5 0 883.91 19.10 6 5 0 895.81 20.10 6 5 0 892.31 20.50 -6 5 0 899.31 20.30 6 -5 0 917.31 19.80 6 -5 0 869.91 20.40 -6 5 0 914.61 20.50 6 -6 0 230.38 7.30 6 6 0 239.08 7.60 -6 -6 0 233.68 6.00 -6 6 0 224.18 6.60 -6 -6 0 229.08 7.50 -6 6 0 236.08 7.40 -6 -6 0 228.38 7.30 -6 -6 0 235.58 6.00 6 6 0 235.68 7.20 6 -6 0 235.18 7.00 -6 -7 0 -0.30 1.70 -6 -7 0 1.30 0.90 -6 7 0 -1.00 2.00 6 -7 0 1.80 1.60 6 7 0 0.40 1.40 6 7 0 -0.90 2.00 -6 -7 0 2.10 1.20 6 -7 0 0.60 1.80 -6 -7 0 2.30 1.60 -6 7 0 0.30 1.30 6 -8 0 146.09 6.10 6 8 0 153.98 6.20 -6 -8 0 146.29 4.70 -6 -8 0 149.69 6.40 -6 8 0 146.79 6.30 -6 -8 0 144.39 4.50 -6 8 0 156.58 6.50 6 -8 0 152.48 6.20 -6 8 0 152.58 5.80 -6 -8 0 146.59 6.40 6 9 0 -1.10 2.80 -6 9 0 -1.70 2.70 -6 -9 0 0.50 2.80 -6 -9 0 0.70 1.30 -6 -9 0 -0.50 2.20 6 -9 0 -2.80 2.60 -6 9 0 3.70 2.60 6 -9 0 -1.30 1.80 -6 9 0 0.70 1.90 6 9 0 3.30 2.20 6 10 0 7.10 3.50 6 -10 0 4.70 2.60 6 10 0 8.80 2.90 -6 10 0 5.00 2.40 -6 -10 0 6.80 2.80 -6 10 0 13.40 3.50 6 -10 0 2.40 3.20 -6 -11 0 262.47 7.30 6 11 0 234.48 13.40 -6 -11 0 267.17 10.40 6 11 0 243.28 11.20 6 -11 0 290.57 9.80 -6 11 0 284.47 9.70 -6 11 0 275.37 11.00 -6 12 0 -3.80 3.00 6 -12 0 2.80 3.30 -6 -12 0 -1.60 3.50 6 12 0 -0.20 3.40 -6 -12 0 1.90 2.10 6 -13 0 9.70 4.30 -6 -13 0 9.90 2.70 -6 13 0 17.20 4.40 6 13 0 17.20 4.50 7 0 0 0.60 1.00 -7 0 0 1.30 1.00 7 0 0 1.00 1.00 -7 0 0 1.90 1.00 7 1 0 -0.10 1.00 -7 1 0 -0.20 1.00 7 1 0 0.00 0.50 7 -1 0 -0.20 0.90 -7 -1 0 0.70 1.00 7 1 0 0.80 0.60 -7 1 0 -0.30 0.90 7 1 0 -0.80 0.90 -7 -1 0 0.50 0.90 7 2 0 0.10 0.70 -7 2 0 1.00 1.20 7 2 0 0.60 0.90 7 -2 0 0.20 1.00 -7 -2 0 0.10 1.00 7 2 0 1.10 1.10 -7 2 0 1.70 1.10 7 -2 0 0.90 0.60 7 -2 0 1.30 1.00 7 3 0 -0.50 0.80 7 -3 0 -1.30 0.70 7 -3 0 0.00 1.10 -7 -3 0 -0.90 0.90 -7 3 0 -1.00 1.20 -7 3 0 0.30 1.10 -7 3 0 -0.80 0.60 7 3 0 -1.70 1.20 -7 -3 0 -0.60 1.10 -7 4 0 -0.40 0.80 -7 -4 0 -1.20 1.00 7 -4 0 -1.60 1.00 -7 -4 0 -0.70 1.00 7 4 0 0.20 1.00 -7 4 0 0.30 1.40 -7 4 0 0.30 1.30 7 4 0 0.40 1.40 7 -4 0 -0.30 1.00 -7 -4 0 -0.10 1.00 -7 5 0 0.80 1.00 -7 -5 0 0.80 1.20 -7 5 0 2.00 1.60 -7 -5 0 1.40 0.90 7 5 0 -0.60 1.60 7 -5 0 2.70 1.10 7 5 0 -0.10 1.10 7 -5 0 -2.30 1.30 -7 -5 0 -0.70 1.20 -7 -5 0 0.00 1.00 -7 5 0 -0.30 1.40 7 -6 0 0.70 1.40 -7 6 0 2.40 1.70 -7 -6 0 -1.10 1.40 -7 -6 0 0.40 0.90 -7 -6 0 -0.60 1.10 7 -6 0 1.10 1.40 7 6 0 1.60 1.40 -7 -6 0 1.80 1.40 -7 6 0 1.20 1.20 -7 6 0 1.10 1.90 -7 -7 0 -0.10 1.80 -7 -7 0 1.50 1.80 -7 7 0 -0.70 1.50 7 -7 0 -1.40 1.70 -7 -7 0 -0.10 1.00 -7 -7 0 -0.20 1.20 7 -7 0 -0.10 1.70 -7 7 0 -0.60 2.10 7 7 0 0.60 2.10 7 7 0 1.50 1.60 7 -8 0 1.70 2.10 -7 8 0 2.50 2.10 -7 -8 0 -1.10 1.40 -7 -8 0 -1.10 1.10 -7 -8 0 -0.30 2.10 -7 8 0 0.60 2.60 7 8 0 -0.30 1.80 -7 -8 0 1.10 2.30 7 8 0 4.70 2.70 7 -8 0 -0.30 2.20 -7 8 0 0.90 1.60 -7 -9 0 2.10 2.30 7 -9 0 -0.10 2.70 -7 -9 0 -4.30 2.80 -7 9 0 -1.40 1.90 7 -9 0 5.40 2.40 7 9 0 -3.50 2.10 -7 9 0 -1.80 2.60 -7 -9 0 0.60 1.60 7 9 0 1.30 3.30 -7 -9 0 0.00 1.30 -7 -10 0 1.60 1.50 -7 -10 0 0.70 1.90 7 10 0 1.30 2.40 -7 -10 0 -2.20 2.50 7 -10 0 -3.20 3.50 7 -10 0 1.40 2.60 7 10 0 -8.10 3.80 -7 10 0 0.30 2.30 -7 10 0 -1.40 3.20 -7 11 0 -9.30 3.80 -7 -11 0 -0.10 3.20 7 11 0 0.80 4.90 -7 11 0 -0.80 2.90 7 11 0 1.30 3.00 -7 -11 0 -1.70 1.80 -7 -12 0 2.40 2.10 7 -12 0 0.50 3.40 -7 12 0 2.20 3.30 -7 -12 0 7.10 4.20 7 12 0 1.60 3.50 7 13 0 -1.70 4.20 7 -13 0 8.00 4.30 -7 13 0 -5.30 3.80 8 0 0 642.34 15.40 -8 0 0 673.93 15.60 8 0 0 661.13 15.40 -8 0 0 673.83 15.30 -8 -1 0 29.50 2.50 8 1 0 24.60 2.20 8 -1 0 24.20 2.30 8 1 0 23.60 2.30 -8 -1 0 28.20 2.30 -8 1 0 25.30 2.40 -8 1 0 24.80 2.30 8 -1 0 25.20 2.20 8 2 0 1.50 1.30 8 2 0 1.20 0.70 -8 2 0 1.80 1.30 8 -2 0 0.90 1.20 8 2 0 0.20 0.80 8 2 0 -0.80 1.00 -8 -2 0 0.40 1.20 8 -2 0 0.30 1.20 -8 2 0 2.90 1.40 8 -3 0 309.37 7.10 8 -3 0 299.97 8.60 8 3 0 300.07 8.60 -8 -3 0 297.47 8.70 -8 -3 0 311.77 7.90 -8 3 0 305.07 8.50 -8 3 0 306.57 7.00 -8 3 0 305.07 8.60 8 3 0 294.57 7.60 -8 4 0 2.50 1.70 8 4 0 3.90 1.80 8 -4 0 2.60 1.10 8 4 0 3.40 1.30 -8 4 0 1.70 0.90 -8 4 0 0.00 1.40 -8 -4 0 2.30 1.20 8 -4 0 3.60 1.50 -8 -4 0 2.10 1.50 -8 5 0 441.06 12.10 -8 5 0 468.45 10.80 -8 -5 0 459.15 10.90 8 -5 0 468.55 11.10 8 5 0 440.96 12.10 -8 5 0 460.45 12.00 8 5 0 454.05 11.50 -8 -5 0 470.45 12.50 -8 -5 0 473.05 10.90 8 -5 0 453.55 12.20 -8 -6 0 0.80 1.70 -8 -6 0 1.50 1.30 8 -6 0 -1.10 1.50 8 6 0 4.80 2.20 -8 6 0 -1.10 1.70 -8 6 0 0.40 1.20 -8 6 0 0.70 2.20 -8 -6 0 0.50 1.60 8 6 0 0.90 1.50 8 -6 0 0.50 1.70 -8 -6 0 1.20 1.10 -8 -7 0 570.44 14.70 8 7 0 571.84 15.40 8 -7 0 599.04 14.40 8 7 0 575.64 14.70 -8 7 0 579.04 15.00 -8 7 0 562.14 13.80 -8 -7 0 580.94 13.20 -8 -7 0 558.04 15.30 -8 7 0 571.84 15.20 -8 -7 0 574.94 13.20 8 -7 0 577.14 15.10 -8 -8 0 40.00 2.80 -8 -8 0 35.30 4.20 8 -8 0 41.00 4.20 -8 8 0 41.80 3.40 8 8 0 37.90 3.80 8 8 0 43.10 5.00 -8 8 0 36.10 4.10 -8 -8 0 37.30 2.50 -8 -8 0 33.10 3.60 8 -8 0 33.60 4.10 8 9 0 24.60 4.30 -8 -9 0 21.80 2.40 -8 -9 0 22.50 2.30 -8 -9 0 19.70 3.20 8 9 0 25.20 3.30 8 -9 0 20.00 3.50 -8 9 0 16.10 3.50 -8 9 0 23.80 3.00 8 -9 0 20.50 3.60 -8 -9 0 15.70 3.80 -8 -10 0 2.40 1.70 8 -10 0 -3.00 3.30 -8 -10 0 -2.20 2.70 8 10 0 -5.20 4.60 -8 -10 0 1.00 3.20 8 -10 0 -3.80 3.60 -8 10 0 7.70 3.80 8 10 0 0.90 2.60 -8 10 0 0.00 2.40 8 -11 0 133.39 7.30 8 11 0 124.59 7.30 -8 -11 0 132.59 8.00 -8 11 0 119.59 6.70 -8 -11 0 121.09 4.60 8 11 0 110.59 9.60 8 12 0 19.80 4.40 8 -12 0 17.10 4.30 -8 -12 0 16.20 2.50 -8 12 0 19.20 4.00 -8 -12 0 18.60 5.30 8 -13 0 56.99 6.30 -8 13 0 50.69 5.70 8 13 0 50.39 6.00 -9 0 0 -0.90 1.30 9 0 0 -0.80 1.10 9 0 0 -0.20 1.30 -9 0 0 -1.70 1.30 -9 1 0 -2.30 1.30 9 1 0 -1.90 1.10 9 -1 0 -0.10 1.30 -9 -1 0 1.30 1.30 9 1 0 -1.00 1.30 -9 1 0 0.40 1.20 -9 -1 0 1.60 1.30 9 -1 0 -0.80 1.20 9 2 0 0.00 1.10 -9 -2 0 -0.20 1.50 -9 -2 0 0.60 1.30 -9 2 0 -0.40 1.50 9 -2 0 1.20 1.30 9 2 0 -1.70 1.30 -9 2 0 -0.50 1.40 9 2 0 -0.30 0.70 9 -2 0 -0.50 1.30 -9 -3 0 1.60 1.30 9 3 0 0.20 1.20 -9 3 0 -0.30 1.50 -9 -3 0 0.10 1.40 9 3 0 -0.40 1.00 9 -3 0 0.00 0.80 9 3 0 0.00 1.70 9 -3 0 1.40 1.50 -9 3 0 -0.20 1.70 9 -4 0 1.20 1.00 9 4 0 -2.90 2.00 9 -4 0 -1.90 1.30 9 4 0 0.10 1.10 -9 4 0 -0.30 0.90 -9 4 0 1.90 1.90 -9 4 0 -1.00 1.50 -9 -4 0 0.10 1.30 -9 -4 0 0.20 1.40 -9 -5 0 0.90 1.40 9 -5 0 3.10 1.80 -9 5 0 0.30 2.10 -9 5 0 0.70 1.10 9 5 0 -1.30 1.30 9 -5 0 -2.30 1.20 9 5 0 2.30 2.10 -9 -5 0 0.50 1.50 -9 5 0 -0.20 1.70 -9 -5 0 -0.10 1.10 -9 6 0 1.90 2.50 9 6 0 -0.10 2.40 9 -6 0 -0.20 1.80 9 -6 0 0.10 1.60 9 6 0 -2.00 1.50 -9 -6 0 2.60 1.90 -9 6 0 0.60 2.00 -9 6 0 -0.20 1.30 -9 -6 0 2.30 1.20 -9 -6 0 0.30 1.90 -9 -7 0 0.60 1.20 9 -7 0 -1.30 1.90 9 -7 0 0.50 2.10 -9 7 0 0.80 2.20 -9 -7 0 -1.30 1.80 9 7 0 2.30 2.80 -9 -7 0 0.70 2.00 -9 7 0 -2.10 1.40 9 7 0 0.80 1.80 -9 8 0 0.40 1.80 -9 8 0 -4.90 2.40 9 8 0 -0.60 1.90 9 -8 0 -0.30 2.20 -9 -8 0 1.10 1.30 9 -8 0 2.10 2.50 -9 -8 0 2.10 2.20 9 8 0 -4.60 3.10 -9 -8 0 2.40 2.60 -9 -9 0 2.40 2.60 -9 9 0 -3.80 2.80 9 9 0 -6.80 4.00 9 9 0 -0.10 2.40 -9 9 0 -3.90 3.20 9 -9 0 -0.40 3.00 9 -9 0 -2.10 2.60 -9 -9 0 1.40 1.50 -9 9 0 -0.20 2.10 9 -10 0 -1.20 3.00 -9 10 0 -10.30 3.70 -9 -10 0 0.10 3.30 -9 10 0 -2.50 2.40 -9 -10 0 -1.20 1.80 9 10 0 -3.00 2.70 9 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4.70 -10 -5 0 60.29 3.60 -10 5 0 56.49 4.30 -10 -5 0 57.69 4.40 10 -5 0 58.19 4.30 10 5 0 58.19 3.40 10 5 0 59.89 4.80 -10 -6 0 10.10 2.10 10 6 0 7.10 1.90 -10 -6 0 6.90 2.30 -10 6 0 9.80 1.80 10 6 0 5.40 2.90 -10 -6 0 7.40 1.70 10 -6 0 9.40 2.00 -10 6 0 8.50 2.40 10 -6 0 9.90 2.50 10 7 0 10.70 2.30 -10 -7 0 14.70 3.10 10 -7 0 11.80 2.50 10 7 0 11.30 3.60 10 -7 0 15.10 3.10 -10 7 0 10.20 1.90 -10 -7 0 10.80 1.80 -10 7 0 12.60 2.90 -10 -7 0 11.10 2.20 10 8 0 51.59 5.20 -10 -8 0 45.30 3.60 -10 8 0 48.80 3.80 10 8 0 51.19 4.40 10 -8 0 57.59 5.30 10 -8 0 39.60 4.50 -10 8 0 44.00 5.10 -10 -8 0 55.29 5.10 -10 -8 0 49.70 3.10 10 9 0 3.80 4.50 -10 9 0 -0.50 2.30 -10 -9 0 4.60 2.30 10 9 0 4.10 2.70 10 -9 0 -7.60 3.20 -10 -9 0 -3.50 2.80 -10 -9 0 -0.40 1.70 10 -9 0 -0.50 3.10 10 10 0 26.90 4.40 10 -10 0 20.60 4.80 -10 10 0 38.70 4.50 -10 10 0 30.00 4.50 -10 -10 0 35.60 5.00 -10 -10 0 36.20 3.20 10 -10 0 40.80 4.90 -10 11 0 56.89 6.90 -10 -11 0 57.29 6.50 10 11 0 58.89 6.20 10 -11 0 58.79 6.80 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297.07 7.80 5 3 4 302.07 7.80 5 3 4 302.97 6.70 -5 3 -4 295.87 7.90 -5 -3 4 293.17 7.90 -5 -3 4 306.57 7.50 -5 3 4 293.57 7.30 -5 3 4 305.47 6.90 -5 -3 -4 294.17 6.60 5 3 -4 297.97 7.20 5 -3 4 301.37 7.80 5 -3 4 294.47 7.30 -5 3 4 275.07 8.20 -5 -3 -4 294.17 7.80 5 3 -4 302.67 7.80 -5 -4 4 129.19 4.70 5 -4 -4 128.39 4.00 5 4 4 127.49 4.50 -5 -4 4 129.59 4.10 -5 4 -4 139.09 4.70 -5 4 -4 131.79 4.60 5 -4 -4 134.49 4.60 -5 -4 4 126.79 4.30 -5 4 -4 130.59 4.10 5 4 4 129.69 4.50 -5 4 4 127.29 4.50 -5 4 4 129.49 3.90 5 4 -4 128.99 4.20 -5 -4 -4 136.89 4.60 5 -4 4 130.09 4.60 5 -4 4 134.69 4.20 5 4 -4 131.89 4.60 -5 -4 -4 131.69 3.20 -5 -4 -4 129.69 3.20 5 5 4 21.90 2.30 5 -5 -4 25.20 2.30 -5 -5 4 23.90 1.80 -5 -5 4 21.00 2.30 5 -5 -4 23.90 2.00 5 5 4 22.70 2.50 -5 -5 4 21.20 2.60 -5 5 -4 29.30 2.60 -5 5 -4 29.90 2.10 -5 -5 -4 23.50 1.20 -5 -5 -4 28.90 2.40 -5 5 4 24.80 2.00 -5 -5 -4 24.60 1.10 -5 -5 -4 22.50 2.20 5 -5 4 24.70 2.30 5 5 -4 26.60 2.50 5 5 -4 22.60 2.00 -5 5 4 26.80 2.40 5 6 4 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38.00 3.20 -9 -8 4 39.20 4.70 -9 -8 4 37.80 3.80 9 -8 4 41.10 4.60 -9 -8 -4 38.70 4.40 9 8 -4 46.80 5.10 9 8 -4 36.90 3.70 -9 8 4 41.20 3.50 -9 -8 -4 40.60 2.20 -9 8 4 44.10 4.30 9 -8 4 37.60 4.30 -9 -8 -4 37.60 2.20 -9 -9 4 97.39 5.20 9 9 4 113.39 7.60 -9 -9 4 94.19 4.60 -9 -9 4 83.39 6.60 -9 9 -4 106.29 5.40 -9 9 -4 96.29 6.50 9 9 4 108.69 6.10 9 -9 -4 103.99 6.30 9 -9 -4 103.29 6.20 -9 -9 4 104.59 6.60 -9 9 -4 94.69 7.40 9 -9 4 105.49 6.60 -9 9 4 100.09 5.20 -9 -9 -4 106.09 6.60 9 -9 4 71.09 9.20 9 9 -4 115.29 5.90 -9 9 4 99.59 6.60 9 9 -4 109.29 7.70 -9 -10 4 5.60 3.50 -9 10 -4 9.60 3.80 9 -10 -4 2.00 3.40 9 -10 -4 4.30 3.90 -9 10 -4 2.30 2.70 -9 10 -4 7.10 4.60 9 10 4 4.40 4.70 -9 -10 4 6.50 3.10 -9 -10 4 7.80 2.40 -9 10 4 9.30 3.40 -9 -10 -4 4.30 3.70 9 -10 4 2.40 3.20 9 10 -4 8.00 3.10 -9 10 4 -1.50 3.90 -9 10 4 8.90 2.80 9 10 -4 2.00 5.00 -9 -11 4 2.90 4.20 9 -11 -4 -6.10 3.80 -9 -11 4 1.40 2.50 9 11 4 0.80 3.50 -9 11 -4 0.00 4.10 9 -11 4 1.00 3.60 -9 11 4 1.70 3.60 9 11 -4 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12.60 4.90 10 -12 4 0.80 4.60 -10 12 4 10.40 4.60 -10 12 4 2.60 4.10 10 12 -4 5.60 4.20 11 0 -4 3.70 2.00 11 0 4 4.70 1.20 11 0 4 3.60 1.10 -11 0 4 5.80 1.90 -11 0 4 6.50 2.20 -11 0 -4 8.10 2.10 11 0 -4 4.10 1.80 11 0 4 4.70 2.20 11 0 4 5.50 1.90 -11 0 -4 7.40 2.20 11 1 4 175.98 4.90 11 -1 -4 175.68 6.40 -11 -1 4 179.18 6.70 -11 1 -4 178.38 6.80 -11 -1 4 181.68 6.80 -11 1 -4 167.98 6.60 11 1 4 184.88 7.20 11 -1 -4 180.78 6.90 11 1 4 178.18 5.20 11 1 4 177.08 6.30 -11 -1 -4 184.58 6.90 11 -1 4 173.68 6.60 -11 1 4 175.28 6.50 11 -1 4 180.78 7.00 -11 -1 -4 181.38 6.30 11 1 -4 181.28 6.70 -11 1 4 185.48 7.00 11 -1 4 180.38 4.80 11 1 -4 171.88 6.50 -11 2 -4 28.20 2.00 11 2 4 24.40 2.90 -11 2 -4 33.80 4.00 -11 2 -4 25.60 3.40 11 2 4 26.00 3.10 11 -2 -4 24.90 3.30 -11 -2 4 29.10 3.50 11 2 4 25.40 2.10 11 2 4 26.60 2.40 -11 -2 4 29.10 3.40 11 -2 -4 30.90 3.50 -11 -2 -4 29.00 3.10 -11 2 4 27.40 3.20 11 2 -4 25.50 3.20 -11 -2 -4 29.60 3.40 11 -2 4 26.20 3.40 11 -2 4 26.40 2.10 11 -2 4 29.90 3.50 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-6 4 20.50 2.50 -11 6 -4 11.80 2.90 -11 -6 4 14.80 2.80 11 6 4 19.60 2.80 11 6 4 18.60 2.70 -11 -6 4 15.40 2.90 11 6 4 16.10 3.80 -11 -6 -4 19.70 2.30 11 6 -4 18.80 2.40 11 6 -4 12.90 3.90 -11 6 4 16.50 1.80 11 -6 4 18.50 2.60 11 -6 4 16.20 3.10 -11 6 4 19.50 3.00 -11 -6 -4 13.30 3.20 -11 7 -4 74.19 5.90 -11 -7 4 72.69 5.70 11 7 4 76.49 6.80 11 7 4 74.99 5.00 11 -7 -4 76.59 4.20 -11 7 -4 73.89 4.20 -11 -7 4 71.39 4.90 -11 -7 4 76.39 4.30 11 -7 4 65.39 4.90 11 7 -4 70.19 4.30 -11 -7 -4 75.79 3.30 11 7 -4 74.79 6.90 -11 -7 -4 73.99 5.90 -11 -7 -4 73.19 3.70 -11 7 4 75.59 3.70 11 -7 4 66.79 7.50 -11 7 4 77.39 5.30 11 8 4 1.60 4.60 -11 -8 4 3.20 2.10 -11 8 -4 3.40 2.30 11 8 4 0.70 2.60 -11 -8 4 -0.10 3.00 11 -8 -4 0.10 2.50 -11 -8 4 1.00 2.80 -11 8 -4 0.90 3.20 -11 -8 4 2.00 3.20 11 -8 -4 2.30 3.10 -11 -8 -4 0.80 1.40 11 -8 4 2.20 3.00 -11 -8 -4 2.70 3.10 11 8 -4 3.10 2.30 -11 -8 -4 1.40 1.80 -11 8 4 -0.30 2.00 -11 8 4 -4.40 2.80 11 -8 4 0.40 2.70 11 -9 -4 47.00 5.90 11 -9 -4 43.10 4.60 11 9 4 42.60 5.20 -11 -9 4 49.00 5.50 -11 -9 4 38.30 3.90 -11 -9 4 48.00 6.20 -11 9 -4 48.20 4.60 -11 9 -4 43.80 5.70 11 9 4 41.70 6.20 11 9 -4 43.30 4.80 11 -9 4 40.90 4.80 -11 -9 -4 45.30 5.40 -11 9 4 41.60 4.20 -11 9 4 44.20 5.80 11 -9 4 36.70 4.70 11 10 4 56.19 6.20 -11 -10 4 64.19 7.50 -11 10 -4 56.69 7.20 11 -10 -4 70.29 7.20 -11 10 -4 67.89 5.70 -11 -10 4 62.09 4.60 11 10 -4 64.39 7.40 -11 10 4 65.99 6.70 -11 -10 -4 72.49 7.60 11 -10 4 63.29 6.90 -11 10 4 70.19 5.40 -11 -11 4 1.20 3.10 11 -11 -4 4.00 4.60 -11 11 -4 8.80 4.90 -11 11 -4 0.40 3.70 11 11 4 0.30 4.00 -11 -11 4 9.40 5.40 -11 11 4 9.80 3.80 11 11 -4 5.80 3.80 -11 11 4 -6.10 4.20 11 -11 4 2.90 4.10 -12 0 4 56.19 4.80 -12 0 -4 67.29 4.70 12 0 -4 56.49 4.40 12 0 4 58.39 4.90 -12 0 -4 64.09 4.50 -12 0 4 62.59 4.40 12 0 -4 50.49 4.50 12 0 4 64.59 4.20 12 -1 -4 33.20 4.00 -12 -1 4 38.40 3.80 -12 -1 4 34.50 3.80 12 1 4 38.40 4.20 12 1 4 35.50 2.30 12 1 4 36.80 2.50 -12 1 -4 31.10 3.40 12 1 4 35.80 3.40 -12 1 -4 37.30 4.30 12 -1 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3.50 7 -3 10 49.90 2.80 -7 4 -10 2.10 1.80 7 4 10 3.80 1.60 -7 4 -10 3.10 1.80 7 4 10 2.40 0.70 7 4 10 1.40 1.40 -7 -4 10 0.80 1.40 -7 -4 10 1.80 1.40 7 -4 -10 0.90 1.60 -7 -4 10 4.50 1.60 7 4 10 2.10 1.70 -7 4 -10 3.00 1.40 -7 -4 10 4.60 1.30 7 4 -10 2.70 1.70 -7 4 10 4.70 2.00 -7 4 10 2.00 1.10 7 -4 10 2.20 1.40 -7 4 10 1.70 1.10 -7 -4 -10 3.40 1.50 -7 4 10 2.60 1.10 7 4 -10 2.50 1.20 -7 -4 -10 3.60 0.70 7 -4 10 0.20 1.40 -7 -5 10 28.70 2.70 -7 -5 10 25.30 2.70 -7 5 -10 28.70 3.10 7 5 10 24.70 2.80 -7 -5 10 24.40 2.90 -7 -5 10 27.70 3.10 7 5 10 27.20 3.00 -7 5 -10 23.70 2.50 -7 5 -10 31.10 3.40 7 5 10 22.10 2.70 7 -5 -10 24.50 3.10 -7 -5 -10 27.40 2.90 7 -5 10 23.90 2.50 -7 5 10 27.10 2.30 7 5 -10 23.20 2.30 -7 5 10 27.00 2.30 7 5 -10 22.00 2.60 7 -5 10 24.50 2.90 -7 5 10 25.20 3.00 -7 -6 10 15.50 2.70 -7 -6 10 13.00 2.10 7 6 10 14.10 2.40 7 -6 -10 13.40 2.40 -7 6 -10 12.60 2.10 -7 6 -10 14.70 2.70 7 6 10 18.10 2.70 -7 6 -10 16.00 2.90 -7 -6 10 13.70 2.50 -7 6 10 13.80 2.00 7 6 -10 10.80 2.00 7 6 -10 16.00 2.60 -7 -6 -10 11.20 2.20 7 -6 10 11.70 2.50 -7 6 10 11.10 1.90 7 -6 10 11.00 2.20 -7 6 10 14.10 2.70 7 7 10 164.08 6.70 -7 7 -10 146.99 7.10 -7 -7 10 175.28 6.30 -7 -7 10 166.88 6.70 -7 -7 10 176.28 7.10 -7 7 -10 176.98 7.30 7 -7 -10 178.78 6.70 -7 7 -10 171.18 6.40 -7 7 -10 163.88 7.60 7 7 10 179.98 7.20 7 -7 10 165.28 6.80 7 -7 10 179.98 7.00 7 7 -10 169.38 6.20 -7 7 10 165.18 6.80 7 7 -10 153.28 7.10 -7 7 10 166.48 6.00 -7 8 -10 36.20 4.10 -7 -8 10 33.60 4.40 7 8 10 40.60 4.70 7 -8 -10 36.80 4.10 -7 8 -10 40.20 4.80 7 8 10 39.60 4.50 -7 8 -10 41.70 3.90 -7 -8 10 41.80 4.70 -7 -8 10 37.30 3.50 -7 8 10 41.00 3.70 -7 8 10 38.40 5.40 7 -8 10 38.50 4.20 7 8 -10 34.10 4.20 7 8 -10 37.70 3.70 -7 8 10 39.70 4.30 7 -8 10 44.30 4.90 -7 -9 10 73.09 5.80 -7 -9 10 71.09 7.40 7 9 10 74.19 5.60 -7 -9 10 70.69 4.60 7 9 10 77.59 6.40 -7 9 -10 78.49 5.10 -7 9 -10 74.39 7.10 -7 9 -10 88.19 6.30 7 -9 -10 70.49 5.20 -7 -9 -10 77.79 5.80 7 -9 10 83.89 5.80 7 9 -10 71.79 4.90 7 9 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2.40 8 9 -10 -3.00 2.20 -8 9 10 0.00 2.20 8 -9 10 -5.00 2.70 -8 10 -10 94.79 9.10 8 -10 -10 111.29 7.60 -8 -10 10 101.59 7.50 -8 10 -10 111.89 6.60 8 10 10 102.69 8.00 -8 -10 10 115.49 5.90 -8 10 -10 115.29 7.90 -8 -10 10 87.79 6.90 8 10 10 105.39 7.20 8 10 -10 107.59 6.20 -8 10 10 119.79 6.20 8 -10 10 106.79 7.20 -8 -11 10 1.00 3.00 -8 11 -10 4.40 4.70 8 11 10 -0.50 3.60 8 -11 -10 -0.70 3.70 -8 -11 10 5.10 3.90 -8 11 -10 2.20 3.50 8 11 -10 3.60 3.20 -8 11 10 5.30 3.40 8 -11 10 2.00 3.80 -8 12 -10 13.50 4.30 -8 -12 10 2.80 5.10 8 12 10 9.50 4.60 -8 12 -10 -1.00 5.20 8 -12 -10 5.10 4.50 -8 -12 10 4.20 3.60 8 -12 10 10.40 4.70 -8 12 10 2.70 3.90 8 12 -10 6.00 3.80 -9 0 10 502.95 12.50 9 0 10 501.65 13.60 -9 0 -10 500.35 13.10 -9 0 -10 507.45 12.40 9 0 10 517.25 12.10 9 0 -10 507.25 13.20 -9 0 10 504.35 13.20 9 0 10 511.75 12.50 -9 0 -10 505.65 12.10 9 0 -10 494.15 11.90 -9 1 -10 15.50 2.30 9 1 10 13.20 1.90 -9 -1 10 16.70 2.50 9 -1 -10 11.80 1.60 -9 -1 10 13.60 2.00 9 -1 -10 13.10 2.40 9 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9.00 -9 6 10 262.07 8.00 9 6 -10 268.07 7.70 9 -6 10 255.97 8.40 9 6 -10 250.77 9.10 -9 -7 10 7.90 2.10 9 7 10 9.00 2.90 -9 -7 10 15.10 3.10 -9 -7 10 12.10 2.90 9 7 10 9.70 3.40 9 -7 -10 5.60 2.60 -9 -7 10 11.90 3.00 -9 7 -10 6.60 3.20 -9 7 -10 14.20 2.50 9 7 10 8.20 3.00 -9 7 10 12.40 2.40 -9 -7 -10 10.90 2.70 9 7 -10 12.60 2.20 9 -7 10 10.10 2.70 9 -7 10 8.80 2.70 9 7 -10 5.50 3.50 -9 7 10 12.10 2.10 -9 -8 10 29.60 3.90 -9 -8 10 40.90 4.90 -9 8 -10 28.60 3.40 9 -8 -10 32.60 4.10 9 8 10 22.70 4.10 9 8 10 22.80 3.60 -9 -8 10 22.70 3.60 -9 8 -10 24.80 4.20 -9 -8 10 24.60 3.20 -9 8 -10 21.60 3.90 -9 -8 -10 21.80 3.50 9 8 -10 23.00 3.00 9 -8 10 21.50 3.90 -9 8 10 26.20 2.90 -9 8 10 26.50 4.70 -9 -9 10 13.00 3.80 -9 9 -10 10.60 5.40 -9 9 -10 10.00 3.00 -9 9 -10 12.90 3.90 -9 -9 10 10.20 2.80 9 9 10 12.10 4.40 9 9 10 7.80 3.60 -9 -9 10 6.90 3.30 -9 -9 -10 7.00 3.10 9 9 -10 10.90 2.80 -9 9 10 12.50 3.00 -9 9 10 14.30 2.80 9 -9 10 8.80 3.20 9 -10 -10 162.28 8.20 -9 -10 10 161.68 7.10 -9 10 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52.69 2.70 -1 -3 21 56.39 3.70 -1 3 -21 59.09 3.30 -1 3 -21 48.10 3.50 1 3 21 51.49 3.00 1 3 -21 50.49 3.50 1 -3 21 50.49 3.60 -1 3 21 52.69 2.20 -1 3 21 49.99 3.20 -1 3 21 54.29 3.40 1 3 -21 57.69 4.20 1 3 -21 52.19 3.00 1 3 -21 44.60 3.10 1 -3 21 55.49 3.90 -1 3 21 51.69 3.80 -1 4 -21 21.50 3.00 -1 4 -21 20.20 2.60 -1 -4 21 19.60 2.80 1 4 21 22.20 2.10 -1 4 -21 18.60 2.50 -1 4 -21 22.00 2.60 1 4 21 17.00 2.60 1 4 21 19.00 2.20 -1 -4 21 20.70 2.70 -1 -4 21 21.40 2.60 1 -4 21 21.10 2.80 1 4 -21 18.80 2.40 1 -4 21 22.80 3.00 1 4 -21 18.10 2.40 1 4 -21 18.60 3.10 -1 4 21 21.90 2.50 -1 4 21 21.00 2.60 -1 4 21 19.20 1.50 -1 4 21 19.40 2.60 -1 -5 21 -0.10 1.70 -1 5 -21 -0.10 1.70 -1 5 -21 -4.00 2.00 1 5 21 1.30 1.30 1 5 21 3.40 2.10 1 5 21 3.00 2.30 1 5 21 2.60 1.60 -1 5 -21 0.60 2.80 1 5 21 2.40 1.40 -1 -5 21 3.10 2.30 -1 -5 21 0.20 1.90 1 5 -21 1.60 2.60 -1 5 21 -1.80 2.40 -1 5 21 1.60 1.90 -1 5 21 2.30 1.90 1 -5 21 -0.20 2.20 -1 5 21 4.10 1.60 1 5 -21 1.10 1.80 1 -5 21 5.40 2.10 -1 5 21 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4.30 -1 9 21 54.69 6.30 1 9 -21 69.59 5.60 -1 9 21 67.09 4.20 1 -9 21 73.59 5.90 1 10 21 3.00 3.20 -1 -10 21 5.10 3.40 -1 10 -21 4.20 3.30 1 10 21 1.50 3.50 -1 10 21 -6.60 3.50 -1 10 21 -1.20 2.30 1 10 -21 0.80 3.50 1 -10 21 -2.70 3.40 -1 10 21 -0.30 2.70 1 11 21 37.70 5.70 1 11 21 33.90 4.80 -1 -11 21 40.50 5.10 -1 11 -21 31.60 4.90 1 11 -21 40.50 5.40 -1 11 21 27.70 4.10 -1 11 21 35.00 4.40 -1 11 21 31.30 5.50 1 -11 21 36.90 5.30 1 12 21 -4.30 4.80 -1 -12 21 3.50 4.50 -1 12 -21 5.00 4.60 1 -12 21 8.30 4.50 -1 12 21 -5.60 4.60 1 12 -21 2.50 4.60 -2 0 21 -1.10 1.30 -2 0 -21 0.70 1.10 2 0 21 0.40 1.60 -2 0 -21 -0.50 1.10 -2 0 21 -0.50 1.50 -2 0 21 -0.40 0.90 2 0 -21 -0.50 1.20 2 0 21 1.60 1.40 -2 0 -21 -0.90 1.30 -2 0 -21 2.40 1.80 -2 1 -21 507.85 13.20 2 1 21 506.85 12.60 -2 -1 21 504.95 13.20 2 1 21 503.35 13.20 -2 1 -21 522.25 13.10 -2 1 -21 514.15 11.90 -2 -1 21 532.65 13.10 2 -1 -21 526.75 13.00 -2 -1 21 519.65 12.40 -2 1 -21 492.15 12.10 2 1 21 507.15 12.30 -2 1 21 528.75 11.60 -2 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8.20 -12 -1 27 72.79 5.90 -12 1 27 60.69 5.30 -12 1 27 92.59 8.20 12 -1 27 79.79 7.20 -12 2 -27 0.50 4.30 12 2 27 1.20 3.50 -12 -2 27 4.50 3.10 -12 -2 27 8.70 4.80 -12 2 27 1.40 2.70 12 -2 27 4.90 4.00 -12 2 27 2.70 4.80 -12 -3 27 5.10 3.50 -12 -3 27 7.60 4.60 -12 3 -27 0.30 4.40 -12 3 27 8.00 5.10 12 -3 27 -2.00 4.20 -12 3 27 6.50 2.70 0 0 -28 41.50 4.30 0 0 28 33.70 4.00 0 1 28 -1.40 2.10 0 -1 28 0.40 2.20 0 1 -28 1.20 2.20 0 -1 -28 0.90 2.30 0 2 28 3.20 2.10 0 2 -28 -0.50 2.10 0 2 -28 2.40 1.70 0 -2 28 2.20 2.50 0 -3 28 3.00 2.70 0 3 -28 2.20 2.20 0 3 -28 -4.10 2.40 0 3 28 0.00 3.10 0 3 28 0.00 2.10 0 4 28 14.10 2.60 0 4 28 13.90 2.00 0 4 -28 8.00 3.50 0 4 28 11.50 3.40 0 4 -28 12.20 3.10 0 -4 28 19.20 3.50 0 5 28 0.90 3.40 0 -5 28 -4.70 2.70 0 5 -28 -0.60 3.10 0 5 28 1.90 2.20 0 5 -28 -3.80 2.70 0 5 28 -3.20 1.80 0 6 -28 8.40 3.20 0 6 28 5.70 3.50 0 -6 28 3.10 3.00 0 6 28 3.40 2.50 0 6 -28 5.80 3.70 0 6 28 2.60 1.90 0 6 28 1.90 3.50 0 7 28 0.10 2.10 0 7 28 1.20 2.40 0 -7 28 -5.40 3.30 0 7 -28 -1.60 3.10 0 7 28 2.00 3.50 0 8 -28 28.40 4.30 0 8 28 24.40 5.00 0 8 28 26.00 3.20 0 -8 28 24.60 4.60 0 8 28 32.20 3.90 0 9 -28 9.70 4.40 0 -9 28 -5.40 4.20 0 9 28 4.60 4.30 0 9 28 1.00 3.00 0 10 28 27.00 6.00 0 -10 28 30.00 5.90 0 10 -28 15.30 5.30 0 10 28 23.70 4.10 1 0 -28 8.50 2.60 -1 0 28 9.10 2.50 -1 0 -28 4.30 2.40 1 0 28 5.00 2.30 -1 1 -28 2.90 2.40 1 -1 -28 -0.70 2.20 -1 1 -28 0.20 1.40 -1 -1 28 1.70 2.20 1 1 28 1.90 2.10 -1 -1 -28 -2.30 2.10 1 -1 28 1.00 2.20 1 1 -28 0.70 2.20 -1 1 28 -0.10 2.10 1 2 28 71.99 4.60 -1 2 -28 77.49 5.20 -1 2 -28 69.29 3.60 -1 -2 28 63.99 5.10 1 2 -28 62.89 2.60 1 2 -28 70.59 4.90 1 -2 28 66.79 5.00 -1 2 28 64.49 4.60 -1 2 28 74.09 5.60 1 3 28 4.80 2.30 -1 3 -28 6.70 2.90 1 3 28 9.20 2.20 -1 3 -28 7.40 2.70 -1 -3 28 6.40 2.90 1 3 28 10.00 3.20 -1 3 28 9.10 3.40 1 -3 28 9.10 2.90 1 3 -28 10.70 2.80 -1 3 28 8.70 2.60 1 3 -28 7.50 2.20 1 4 28 21.10 2.80 -1 4 -28 17.10 3.10 1 4 28 16.50 3.50 1 4 28 14.60 2.40 -1 -4 28 19.30 5.20 -1 4 28 12.50 2.90 1 -4 28 18.40 3.60 1 4 -28 17.70 2.90 -1 4 28 6.50 3.70 1 4 -28 16.50 3.40 -1 5 -28 130.49 6.90 -1 -5 28 133.19 7.00 1 5 28 129.89 5.70 1 5 28 129.49 6.30 1 5 28 130.79 5.10 -1 5 -28 118.69 6.40 1 5 -28 126.29 7.60 1 5 -28 138.49 6.40 -1 5 28 135.79 6.70 1 -5 28 118.29 6.90 -1 5 28 135.49 4.30 -1 5 28 137.79 6.20 1 6 28 1.70 3.00 1 6 28 5.10 2.20 -1 -6 28 4.00 3.20 1 6 28 4.20 3.50 -1 6 -28 -0.20 3.80 1 6 28 4.10 2.20 -1 6 -28 2.80 2.90 -1 6 28 7.10 1.80 1 6 -28 0.70 3.60 1 6 -28 3.60 2.80 -1 6 28 3.00 2.60 -1 6 28 2.00 3.30 -1 6 28 -1.60 3.60 1 -6 28 4.80 3.10 -1 -7 28 15.00 4.00 1 7 28 11.70 2.50 1 7 28 13.40 2.70 1 7 28 12.50 4.10 -1 7 -28 20.20 8.00 -1 7 -28 11.40 3.60 -1 7 28 13.60 4.00 -1 7 28 9.50 4.50 1 -7 28 17.40 4.00 -1 7 28 10.60 3.00 -1 7 28 11.50 2.10 1 7 -28 12.40 3.50 1 8 28 0.60 2.80 -1 -8 28 7.20 3.90 1 8 28 1.40 2.30 -1 8 -28 4.60 3.90 1 8 28 -1.70 4.20 -1 8 28 12.80 4.30 1 8 -28 3.30 3.50 1 -8 28 6.60 4.20 -1 8 28 1.20 2.20 -1 8 28 2.30 3.10 1 9 28 45.70 6.10 -1 -9 28 55.99 7.10 -1 9 -28 57.99 7.10 1 9 28 58.99 5.60 1 9 -28 52.09 5.70 -1 9 28 64.39 4.40 1 -9 28 57.29 7.30 -1 9 28 57.29 5.30 -1 9 28 60.79 6.80 1 10 28 -2.20 4.90 -1 10 -28 4.70 4.60 -1 -10 28 0.40 4.90 -1 10 28 1.70 3.30 1 10 -28 -1.10 4.80 -1 10 28 8.20 5.00 1 -10 28 -6.90 4.70 -2 0 -28 107.19 6.10 2 0 -28 98.89 5.60 -2 0 28 110.89 5.80 2 0 28 109.19 5.70 -2 1 -28 29.20 3.70 -2 -1 28 33.60 3.80 -2 1 -28 29.00 2.70 2 -1 -28 25.40 3.20 -2 1 -28 23.50 4.00 2 1 28 31.20 3.70 -2 -1 -28 28.50 3.70 -2 1 28 23.50 3.90 2 1 -28 31.90 3.80 -2 1 28 32.30 4.10 2 -1 28 25.60 3.40 2 2 28 179.98 6.80 -2 2 -28 175.28 7.50 -2 -2 28 188.58 7.90 -2 2 -28 189.88 5.90 -2 2 28 187.28 7.30 -2 2 28 161.18 7.80 2 2 -28 187.58 7.30 2 -2 28 182.88 7.60 2 3 28 19.10 2.60 -2 3 -28 20.10 3.30 -2 -3 28 19.10 3.20 2 3 28 18.80 2.70 -2 3 -28 22.00 3.00 -2 3 28 12.70 3.80 2 3 -28 16.80 2.30 2 -3 28 14.50 3.20 -2 3 28 17.80 3.00 2 3 -28 18.50 3.30 2 4 28 1.10 2.90 2 4 28 4.60 2.10 -2 4 -28 2.60 3.10 -2 4 -28 2.00 2.90 2 4 28 0.40 2.20 -2 4 28 4.60 2.60 2 4 -28 2.50 2.80 2 -4 28 5.10 2.90 2 4 -28 8.00 2.60 -2 4 28 5.40 3.60 -2 5 -28 21.20 3.70 -2 5 -28 23.20 3.50 -2 -5 28 23.90 3.90 2 5 28 21.70 3.40 2 5 28 21.20 2.80 2 5 28 23.20 2.90 -2 5 28 28.40 4.40 -2 5 28 24.90 4.20 2 -5 28 16.70 3.50 -2 5 28 20.60 3.20 2 5 -28 22.90 5.40 2 6 28 41.30 5.10 -2 -6 28 49.60 5.70 2 6 28 40.30 3.60 -2 6 -28 42.30 5.10 2 6 28 41.50 4.10 -2 6 -28 53.69 6.10 2 6 28 50.69 4.40 -2 6 28 56.89 5.90 2 6 -28 45.40 4.80 -2 6 28 46.80 4.80 -2 6 28 46.20 5.30 2 6 -28 46.90 5.40 2 -6 28 51.99 5.40 2 7 28 382.16 10.90 -2 7 -28 426.26 13.50 2 7 28 407.66 14.20 2 7 28 382.86 10.00 -2 -7 28 375.36 13.40 -2 7 28 395.86 11.70 2 -7 28 381.66 13.40 2 7 -28 404.86 13.00 -2 7 28 419.86 13.90 -2 7 28 394.56 12.10 -2 7 28 390.16 9.10 2 8 28 4.20 4.30 2 8 28 -0.70 3.10 -2 8 -28 4.80 3.90 -2 -8 28 -3.60 3.80 2 -8 28 4.50 3.70 -2 8 28 3.10 3.00 2 8 -28 -2.90 3.60 -2 8 28 0.80 4.00 -2 8 28 -0.90 1.90 -2 9 -28 48.60 5.60 2 9 28 39.10 6.00 2 9 28 48.00 6.00 -2 -9 28 64.79 7.40 2 -9 28 42.20 5.60 2 9 -28 57.49 6.20 -2 9 28 55.39 6.40 -2 9 28 50.79 5.80 -2 9 28 50.59 3.80 -3 0 28 70.29 5.80 -3 0 -28 64.89 3.30 3 0 -28 70.29 4.90 3 0 28 73.19 4.80 -3 0 -28 77.09 5.40 -3 0 -28 58.79 5.70 -3 0 28 69.39 5.20 -3 1 -28 -2.20 2.20 -3 1 -28 -0.50 3.50 3 -1 -28 0.30 2.10 -3 -1 28 0.20 1.60 -3 -1 28 -0.50 2.50 3 1 28 0.20 2.10 -3 1 -28 0.80 2.10 3 1 -28 0.80 2.30 3 -1 28 2.60 2.20 -3 -1 -28 -2.20 2.30 -3 1 28 5.70 3.30 -3 1 28 3.60 2.50 -3 -2 28 -1.20 2.50 3 2 28 0.50 2.00 -3 2 -28 0.00 3.80 -3 -2 28 -2.60 1.70 3 2 28 2.20 2.40 -3 2 -28 -1.20 2.30 3 2 -28 1.40 2.30 -3 2 28 -1.10 2.20 3 -2 28 4.00 2.60 -3 -3 28 -0.10 2.80 3 3 28 0.20 2.10 3 3 28 1.30 2.30 -3 3 -28 0.90 2.80 -3 3 28 5.20 4.00 3 -3 28 -0.70 2.60 3 3 -28 2.80 1.80 3 3 -28 -2.40 2.30 -3 3 28 -3.90 2.30 3 4 28 0.00 2.90 3 4 28 3.10 2.50 3 4 28 5.90 2.20 -3 4 -28 1.00 3.10 -3 4 -28 4.00 2.90 -3 -4 28 3.60 2.80 -3 -4 28 9.00 2.60 3 4 -28 7.10 2.80 3 -4 28 8.20 3.40 3 4 -28 3.70 2.40 -3 4 28 1.10 4.00 -3 4 28 3.50 2.60 -3 -5 28 3.50 2.60 -3 5 -28 6.20 3.00 -3 -5 28 12.00 3.40 3 5 28 1.40 2.70 3 5 28 4.30 2.70 3 5 28 4.80 2.10 -3 5 -28 2.10 3.40 3 5 -28 1.10 2.90 -3 5 28 6.60 4.20 3 -5 28 1.60 3.00 -3 5 28 7.60 2.90 3 5 -28 7.50 3.40 -3 5 28 8.70 3.10 3 6 28 3.10 2.00 3 6 28 0.90 3.40 -3 6 -28 5.10 4.10 3 6 28 2.00 2.80 -3 6 -28 2.90 3.40 -3 -6 28 3.70 3.00 -3 -6 28 7.40 3.30 3 6 -28 9.80 3.80 -3 6 28 3.70 2.90 3 6 -28 3.40 3.10 -3 6 28 1.10 4.50 3 -6 28 2.90 3.20 -3 -7 28 1.30 3.10 -3 -7 28 5.80 3.70 -3 7 -28 3.20 3.50 3 7 28 2.20 3.10 3 7 28 4.40 3.90 -3 7 28 7.70 3.30 -3 7 28 -4.80 3.70 -3 7 28 5.70 4.70 3 7 -28 3.90 3.50 3 -7 28 -2.50 3.30 -3 8 -28 6.10 3.90 3 8 28 3.50 3.40 -3 -8 28 3.20 4.00 3 8 28 -3.10 4.60 -3 -8 28 5.70 3.70 -3 8 28 2.30 4.20 3 -8 28 -0.90 4.00 3 8 -28 8.90 4.00 -3 8 28 -1.30 3.30 -3 -9 28 10.10 4.40 -3 -9 28 -4.20 4.40 -3 9 -28 7.80 4.40 3 9 28 7.30 5.20 -3 9 28 7.50 4.00 -3 9 28 7.00 3.20 -3 9 28 9.70 4.90 3 -9 28 2.80 4.40 3 9 -28 3.30 4.20 4 0 28 3.90 2.40 -4 0 28 9.00 2.80 -4 0 -28 6.80 2.70 -4 0 28 6.00 3.30 -4 0 -28 8.70 2.20 4 0 -28 10.70 2.60 -4 0 28 4.10 1.70 -4 0 -28 10.60 3.30 -4 -1 28 3.80 3.20 4 -1 -28 2.70 2.30 -4 1 -28 4.50 3.60 4 1 28 0.80 2.10 -4 1 -28 5.30 2.90 -4 -1 28 1.10 2.50 -4 -1 28 3.10 1.80 4 -1 28 -0.70 2.40 -4 1 28 0.60 1.40 4 1 -28 2.90 2.30 -4 1 28 -2.50 2.30 -4 -1 -28 0.90 1.80 -4 1 28 -1.40 3.10 -4 -1 -28 1.70 2.90 -4 -1 -28 2.10 3.10 -4 -2 28 35.60 4.20 -4 2 -28 40.40 4.00 4 2 28 35.70 3.80 -4 2 28 39.10 4.50 -4 2 28 30.80 4.00 4 2 -28 44.10 4.30 4 -2 28 39.20 4.50 4 3 28 1.80 2.70 -4 -3 28 3.20 3.00 4 3 28 0.90 2.10 -4 3 -28 2.00 2.90 -4 3 -28 4.20 3.10 -4 -3 28 2.50 2.20 4 -3 28 2.60 2.70 4 3 -28 1.70 1.60 4 3 -28 -1.60 2.40 -4 3 28 1.80 2.50 4 4 28 10.10 2.30 -4 4 -28 13.40 3.50 -4 4 -28 16.10 3.70 -4 -4 28 17.40 3.10 4 4 28 14.30 3.00 4 4 28 11.90 3.00 -4 -4 28 15.20 3.50 4 4 -28 12.60 2.90 4 4 -28 7.10 2.60 -4 4 28 13.70 3.20 4 5 28 6.80 2.10 -4 5 -28 8.30 3.90 4 5 28 5.00 3.00 4 5 28 4.20 2.60 -4 -5 28 5.30 3.00 -4 5 -28 8.10 3.00 -4 -5 28 7.00 3.30 4 5 -28 6.50 3.20 4 -5 28 0.30 2.90 -4 5 28 7.60 3.20 4 5 -28 4.10 3.00 -4 5 28 6.70 3.50 -4 6 -28 -0.20 3.00 -4 -6 28 -4.00 3.20 4 6 28 0.10 1.80 4 6 28 1.00 3.10 -4 -6 28 3.30 3.10 -4 6 -28 1.80 4.20 4 6 28 -3.00 3.60 -4 6 28 -1.60 3.00 4 -6 28 -1.50 3.30 -4 6 28 -0.40 3.50 4 6 -28 1.70 2.90 -4 7 -28 4.20 3.60 4 7 28 4.10 4.10 -4 -7 28 3.20 3.60 4 7 28 -0.40 3.50 -4 -7 28 -1.40 3.40 -4 7 28 -1.10 3.20 4 -7 28 6.40 3.70 4 7 -28 1.40 3.10 -4 7 28 -5.40 3.50 -4 8 -28 -3.70 3.80 4 8 28 5.00 5.00 -4 -8 28 -2.10 3.80 -4 -8 28 2.90 4.20 4 8 28 10.10 4.60 4 -8 28 -9.10 3.70 -4 8 28 -0.40 4.10 -4 8 28 5.80 3.70 4 8 -28 0.30 3.50 4 9 28 9.30 5.20 -4 -9 28 22.90 4.90 -4 -9 28 9.20 4.80 -4 9 -28 14.90 4.80 -4 9 28 20.60 4.60 -4 9 28 14.90 5.20 4 9 -28 15.40 4.60 4 -9 28 21.00 4.80 -5 0 -28 110.89 6.70 -5 0 28 133.29 6.80 -5 0 -28 100.09 8.00 5 0 -28 122.49 5.90 -5 0 -28 121.09 5.30 5 0 28 133.79 6.10 -5 0 28 116.09 6.60 5 1 28 4.70 2.30 -5 -1 28 0.10 3.00 -5 1 -28 -2.10 2.50 -5 1 -28 -0.40 2.70 -5 -1 28 1.60 2.00 -5 -1 28 -3.20 3.10 -5 1 -28 -0.10 3.90 5 -1 28 2.50 2.50 -5 -1 -28 3.40 2.20 5 1 -28 2.50 2.30 -5 1 28 3.70 2.60 -5 1 28 -0.30 1.50 -5 -1 -28 8.20 3.30 -5 1 28 0.10 3.20 -5 -1 -28 1.20 2.70 5 2 28 11.60 3.20 -5 -2 28 16.30 3.40 5 2 28 13.00 2.60 -5 -2 28 15.70 4.00 -5 2 -28 12.50 3.10 -5 -2 28 12.00 2.50 -5 2 -28 14.10 3.20 5 2 -28 9.40 2.70 -5 2 28 11.80 1.70 -5 2 28 15.90 3.60 -5 2 28 13.50 3.30 -5 -2 -28 13.60 2.30 5 -2 28 11.60 3.00 5 3 28 13.20 3.30 -5 -3 28 13.10 2.60 -5 -3 28 10.30 3.30 5 3 28 12.00 2.40 -5 3 -28 4.90 3.30 -5 3 -28 11.40 3.20 -5 3 28 11.80 3.20 -5 -3 -28 10.20 1.70 5 3 -28 14.40 2.90 5 -3 28 14.10 3.40 -5 3 28 8.80 3.60 5 4 28 -2.50 1.90 5 4 28 -3.60 3.00 -5 4 -28 7.50 3.70 -5 -4 28 3.40 2.40 -5 -4 28 1.40 2.90 -5 4 -28 2.00 2.80 5 4 -28 2.30 2.60 -5 4 28 3.60 3.10 5 4 -28 1.20 2.50 5 -4 28 1.50 3.00 5 5 28 -0.20 1.90 -5 5 -28 -2.10 3.10 -5 5 -28 -1.30 4.00 -5 -5 28 -2.10 2.50 -5 -5 28 2.10 3.20 5 5 28 -2.50 3.20 5 5 28 -3.30 3.20 -5 5 28 -2.90 3.00 5 -5 28 5.80 3.40 -5 5 28 -0.50 3.10 5 5 -28 -4.90 2.60 5 6 28 12.90 4.00 -5 6 -28 16.00 4.00 5 6 28 16.20 3.90 -5 -6 28 17.80 3.80 -5 -6 28 19.40 4.10 -5 6 28 21.90 4.20 5 6 -28 19.00 3.70 -5 6 28 18.70 3.90 5 -6 28 14.50 4.20 5 7 28 5.50 4.20 -5 -7 28 -3.40 3.50 -5 7 -28 5.50 3.50 5 7 28 8.50 4.40 -5 -7 28 2.40 3.90 -5 7 28 10.70 4.10 -5 7 28 -1.20 3.50 5 -7 28 3.10 3.50 5 7 -28 6.30 3.40 -5 8 -28 0.60 4.10 5 8 28 -8.80 4.30 -5 -8 28 -5.80 4.10 -5 -8 28 0.70 4.10 5 8 -28 -0.30 3.60 5 -8 28 3.70 4.10 -5 8 28 6.40 4.40 -5 8 28 -2.30 4.00 -5 -9 28 7.20 5.00 -5 -9 28 -5.50 4.50 -5 9 -28 14.30 5.10 5 9 28 1.20 5.10 -5 9 28 -2.30 4.70 5 9 -28 -1.40 4.40 5 -9 28 13.90 4.80 -6 0 -28 372.46 12.00 -6 0 28 367.16 9.90 6 0 -28 370.56 10.90 -6 0 -28 382.06 13.80 6 0 28 371.76 11.20 -6 0 28 375.06 13.50 -6 0 28 341.67 11.10 -6 0 -28 364.16 11.30 -6 -1 28 12.70 2.30 -6 1 -28 7.90 3.00 -6 -1 28 11.30 3.20 6 1 28 5.90 2.60 6 1 28 8.60 3.30 -6 1 -28 9.90 2.90 -6 -1 28 7.90 3.70 -6 1 28 3.80 3.40 -6 1 28 10.10 2.00 -6 -1 -28 14.00 3.40 -6 -1 -28 8.40 2.80 -6 -1 -28 4.70 2.90 6 -1 28 10.40 3.00 6 1 -28 7.70 2.60 -6 2 -28 -0.40 2.60 6 2 28 3.20 2.30 -6 2 -28 -0.80 3.00 -6 -2 28 2.30 2.10 6 2 28 -1.70 3.10 -6 -2 28 2.50 2.90 -6 -2 28 7.60 3.70 -6 -2 -28 -0.20 3.10 -6 -2 -28 -0.20 2.50 6 -2 28 -0.60 2.60 -6 2 28 -0.70 3.30 6 2 -28 5.90 2.50 6 3 28 26.90 4.10 6 3 28 23.00 2.80 -6 3 -28 23.90 3.80 -6 3 -28 27.20 4.10 -6 -3 28 31.20 4.10 -6 -3 28 26.70 3.30 -6 3 28 22.40 6.30 6 3 -28 24.30 3.40 -6 3 28 15.30 3.90 6 -3 28 27.80 3.90 -6 -3 -28 24.50 2.80 -6 4 -28 74.19 6.50 -6 -4 28 66.89 5.20 -6 4 -28 69.79 6.00 6 4 28 62.09 5.80 -6 -4 28 75.39 6.40 6 4 28 76.29 4.20 6 4 -28 68.79 4.10 6 4 -28 80.99 5.50 6 -4 28 67.79 5.90 -6 -4 -28 63.79 3.90 -6 4 28 78.39 5.80 -6 -5 28 59.49 5.60 6 5 28 70.39 3.70 6 5 28 61.09 6.60 -6 5 -28 83.39 7.80 -6 -5 28 65.29 6.30 -6 5 -28 76.19 6.20 6 -5 28 74.19 6.30 -6 5 28 69.19 6.10 6 5 -28 79.09 5.70 -6 -6 28 40.40 4.90 -6 -6 28 37.60 5.10 6 6 28 40.40 5.90 -6 6 -28 38.20 4.80 6 6 28 36.70 5.30 6 -6 28 34.60 5.00 -6 6 28 44.50 5.20 -6 6 28 35.80 5.40 6 6 -28 36.70 4.30 -6 -7 28 63.39 6.80 -6 7 -28 61.09 6.70 6 7 28 63.89 8.00 -6 -7 28 57.19 6.70 -6 7 28 72.49 7.00 -6 7 28 58.69 6.90 6 -7 28 48.30 5.60 6 7 -28 59.99 6.20 -6 -8 28 27.50 5.10 -6 8 -28 24.00 5.30 6 8 28 34.70 6.00 -6 -8 28 26.60 5.20 6 8 -28 21.60 4.40 -6 8 28 29.80 5.20 6 -8 28 20.60 4.80 -6 8 28 17.10 4.90 -7 0 -28 6.10 3.20 -7 0 28 6.00 3.30 -7 0 -28 5.90 3.90 7 0 28 3.60 2.60 -7 0 28 5.60 1.90 7 0 -28 7.30 2.60 -7 0 28 -0.30 3.40 -7 0 -28 6.40 3.10 -7 -1 28 -1.40 3.50 7 1 28 -0.40 2.40 -7 -1 28 -1.20 1.80 -7 1 -28 -1.70 3.30 -7 1 -28 2.10 3.00 -7 -1 28 -1.30 3.00 7 1 28 0.90 3.70 7 1 -28 -1.90 2.50 7 -1 28 3.20 2.70 -7 -1 -28 -1.00 2.90 -7 -1 -28 -7.30 3.30 -7 1 28 0.20 1.70 -7 1 28 -0.20 3.20 -7 -1 -28 1.40 3.90 -7 1 28 1.70 3.10 7 2 28 0.40 2.30 7 2 28 0.40 3.40 -7 2 -28 1.20 3.00 -7 -2 28 3.00 3.30 -7 -2 28 4.70 3.70 -7 2 -28 -5.60 3.40 -7 -2 28 -3.30 2.00 -7 -2 -28 -2.70 3.20 -7 -2 -28 5.00 3.00 7 2 -28 -1.20 2.40 -7 2 28 -1.40 1.40 -7 2 28 1.70 3.60 -7 2 28 -0.50 3.10 7 -2 28 1.90 2.80 -7 -3 28 66.69 8.40 -7 3 -28 55.69 5.90 -7 3 -28 59.19 5.90 -7 -3 28 59.29 5.90 7 3 28 56.09 4.30 7 3 28 53.89 6.00 -7 -3 28 58.69 4.80 -7 3 28 52.39 2.70 -7 3 28 61.69 5.90 -7 -3 -28 47.10 4.90 -7 3 28 64.69 6.00 7 3 -28 57.79 5.00 -7 4 -28 21.70 4.20 7 4 28 17.10 2.50 7 4 28 8.40 3.90 -7 -4 28 15.60 4.10 -7 -4 28 15.60 3.40 -7 4 -28 19.60 5.80 -7 4 28 16.70 4.30 -7 -4 -28 14.00 3.10 7 4 -28 13.30 3.20 -7 4 28 18.10 4.00 -7 4 28 15.20 3.50 7 -4 28 15.80 3.70 7 4 -28 10.50 2.80 7 5 28 7.70 1.90 -7 -5 28 4.40 3.70 -7 5 -28 8.20 3.90 -7 -5 28 4.80 3.20 -7 5 28 -1.00 3.60 -7 5 28 13.60 3.70 -7 -5 -28 4.50 3.00 7 -5 28 0.00 3.30 7 5 -28 0.60 3.10 -7 -6 28 6.10 3.30 7 6 28 -2.40 4.00 -7 6 -28 6.00 3.60 -7 -6 28 -1.70 3.90 -7 6 28 -4.00 3.40 7 -6 28 7.60 3.70 7 6 -28 1.90 3.30 -7 6 28 3.50 4.00 7 7 28 2.20 4.70 -7 -7 28 2.00 4.40 -7 7 -28 3.00 4.20 -7 -7 28 2.60 3.80 7 -7 28 5.10 4.00 7 7 -28 -1.60 3.60 -7 7 28 -4.10 4.10 -7 8 -28 -2.50 4.50 -7 -8 28 9.00 4.10 7 8 28 5.10 5.40 -7 -8 28 3.60 4.60 7 -8 28 2.10 4.70 -7 8 28 -1.00 4.60 -7 8 28 3.60 4.80 7 8 -28 1.00 4.20 -8 0 -28 0.50 2.90 -8 0 -28 6.40 4.70 -8 0 28 0.40 1.80 8 0 28 -2.00 2.60 -8 0 28 4.70 3.50 -8 0 -28 3.90 3.80 -8 0 28 3.00 3.10 -8 1 -28 11.40 3.50 -8 1 -28 13.70 4.30 8 1 28 11.60 2.90 -8 -1 28 7.80 3.40 8 1 28 5.80 4.20 -8 -1 28 9.20 3.50 -8 -1 28 9.20 2.30 8 1 -28 8.70 2.70 -8 -1 -28 3.00 3.70 -8 -1 -28 13.90 4.20 -8 1 28 9.50 3.70 -8 1 28 7.30 2.00 8 -1 28 7.20 3.00 -8 1 28 12.10 4.10 8 2 28 26.70 7.00 -8 -2 28 21.00 4.10 8 2 28 34.60 4.20 -8 2 -28 25.80 4.10 -8 -2 28 24.00 3.30 -8 -2 28 37.10 4.70 -8 2 28 14.80 4.10 -8 2 28 29.10 4.10 8 -2 28 31.80 4.20 -8 2 28 25.80 2.90 -8 -2 -28 29.10 4.10 8 2 -28 30.70 3.50 -8 -3 28 -2.00 2.30 -8 -3 28 2.80 4.00 -8 -3 28 -1.00 3.20 -8 3 -28 1.80 3.40 8 3 28 -3.60 2.40 -8 3 28 3.80 3.10 8 -3 28 6.20 3.30 -8 3 28 4.00 3.50 -8 3 28 2.60 1.60 8 3 -28 5.50 2.80 -8 3 28 -0.90 3.60 8 4 28 25.50 2.90 -8 -4 28 30.70 4.80 -8 -4 28 31.20 4.10 -8 4 -28 28.50 4.50 8 -4 28 26.10 4.50 -8 4 28 31.20 4.80 -8 4 28 29.00 4.20 8 4 -28 27.30 3.70 -8 5 -28 18.50 4.10 -8 -5 28 12.00 4.40 -8 -5 28 15.70 3.60 8 5 28 10.00 4.30 -8 5 28 9.30 3.70 -8 5 28 9.10 4.20 8 5 -28 14.80 3.50 8 -5 28 16.70 4.20 8 6 28 12.60 4.60 -8 6 -28 15.70 4.40 -8 -6 28 10.00 4.60 -8 -6 28 6.70 4.00 -8 6 28 10.70 4.50 8 -6 28 4.20 3.70 -8 6 28 15.00 4.30 8 6 -28 13.40 3.90 -8 -7 28 18.90 5.10 8 7 28 16.10 5.20 -8 7 -28 23.30 5.00 -8 -7 28 23.10 4.80 -8 7 28 24.60 5.00 8 -7 28 8.20 4.30 8 7 -28 20.00 4.20 -9 0 -28 3.40 3.10 -9 0 28 12.80 3.90 9 0 28 4.10 3.00 -9 0 28 5.10 2.30 -9 -1 28 4.30 2.30 9 1 28 2.60 2.80 -9 1 -28 3.70 3.30 -9 -1 28 5.10 3.80 -9 1 28 2.40 2.00 -9 1 28 6.30 3.80 9 1 -28 -1.60 2.70 9 -1 28 2.40 2.90 -9 -1 -28 1.30 4.30 -9 -2 28 1.80 3.80 9 2 28 3.30 2.80 -9 -2 28 5.00 2.60 -9 2 -28 8.40 3.80 9 -2 28 3.80 4.00 9 2 -28 5.90 2.90 -9 2 28 6.70 1.90 -9 2 28 6.20 3.70 9 3 28 4.10 2.70 -9 3 -28 5.50 3.60 -9 -3 28 3.30 2.70 -9 -3 28 8.40 4.00 9 3 -28 4.80 2.90 -9 3 28 3.90 3.20 -9 3 28 3.50 1.80 -9 3 28 -2.70 3.70 9 -3 28 7.20 3.60 -9 -4 28 2.30 3.90 -9 4 -28 -0.50 3.60 9 4 28 5.10 3.30 -9 -4 28 2.10 3.10 9 4 -28 3.80 3.00 9 -4 28 -2.40 3.70 -9 4 28 0.10 1.60 -9 4 28 1.60 4.10 -9 4 28 -1.70 3.30 -9 -5 28 3.70 3.40 9 5 28 7.00 4.30 -9 -5 28 4.20 4.00 -9 5 -28 4.60 3.80 -9 5 28 0.30 4.10 -9 5 28 -2.80 3.60 -9 5 28 -0.20 1.50 9 5 -28 -1.10 3.40 9 -5 28 -5.10 3.80 -9 6 -28 -0.90 4.10 -9 -6 28 2.40 3.70 -9 -6 28 -3.10 4.40 9 6 28 6.70 4.90 9 -6 28 -2.80 4.00 -9 6 28 -2.50 4.00 -10 0 28 75.69 7.40 10 0 28 63.39 5.80 -10 0 28 70.79 4.70 -10 -1 28 15.30 4.20 10 1 28 6.60 3.50 -10 1 -28 12.60 3.80 -10 -1 28 11.10 2.80 10 -1 28 6.80 3.70 -10 1 28 10.50 4.30 -10 1 28 13.80 2.60 -10 -2 28 71.39 5.40 10 2 28 76.19 5.60 -10 2 -28 64.09 7.00 -10 -2 28 75.39 7.30 10 -2 28 68.59 6.30 -10 2 28 92.39 7.60 -10 2 28 65.99 4.20 10 2 -28 67.19 5.20 -10 2 28 72.99 5.50 -10 -3 28 -2.90 2.70 -10 3 -28 3.70 3.80 10 3 28 3.20 2.90 -10 -3 28 7.60 4.20 10 -3 28 1.50 3.60 -10 3 28 0.90 2.00 10 3 -28 -6.50 2.90 -10 3 28 0.00 3.30 -10 3 28 -1.60 4.10 -10 -4 28 15.40 3.80 -10 4 -28 25.20 4.80 -10 -4 28 27.90 5.20 10 4 -28 18.50 3.60 -10 4 28 9.20 4.80 -10 4 28 18.30 2.40 -10 4 28 23.50 3.90 10 -4 28 16.90 4.40 -10 -5 28 6.30 4.70 -10 -5 28 0.50 3.80 -10 5 -28 -0.40 4.10 10 5 28 2.30 4.90 -10 5 28 3.60 2.00 10 5 -28 2.90 3.60 10 -5 28 3.60 4.10 -10 5 28 8.00 4.20 -11 0 28 3.00 2.60 -11 0 28 3.60 4.50 11 0 28 -2.40 3.40 11 1 28 7.00 3.60 -11 -1 28 2.30 2.90 -11 1 -28 -1.70 3.80 -11 -1 28 -1.20 4.20 -11 1 28 -4.20 4.10 -11 1 28 0.30 2.40 11 -1 28 4.20 3.90 -11 -2 28 11.50 3.20 -11 2 -28 14.50 4.30 -11 -2 28 14.40 4.90 11 2 28 12.60 3.50 -11 2 28 8.20 2.70 -11 2 28 14.20 4.80 11 -2 28 8.30 4.10 -11 -3 28 5.10 3.10 -11 3 -28 9.50 4.70 -11 -3 28 3.00 4.80 -11 3 28 4.90 4.90 11 3 -28 -4.40 3.20 -11 3 28 1.50 2.30 11 -3 28 3.80 4.00 -11 -4 28 9.20 3.90 11 4 28 18.80 5.20 -11 4 -28 22.90 4.80 -11 -4 28 10.60 4.90 -11 4 28 10.10 2.60 11 -4 28 13.80 4.80 11 4 -28 14.00 3.80 -11 4 28 17.10 5.20 -12 0 28 128.29 9.40 -12 0 28 127.09 6.90 -12 -1 28 -4.60 3.00 -12 -1 28 2.40 4.80 12 1 28 3.60 3.90 -12 1 28 18.30 4.80 -12 1 28 0.80 2.80 12 -1 28 4.00 4.30 0 0 29 -1.20 2.30 0 0 -29 -1.50 2.50 0 1 29 -0.50 2.20 0 1 -29 -1.10 2.30 0 -1 29 2.30 2.40 0 -1 -29 1.70 2.50 0 2 -29 59.69 3.00 0 2 29 59.79 4.70 0 -2 29 65.79 5.20 0 2 -29 65.09 5.10 0 2 29 49.00 5.40 0 3 -29 0.60 2.70 0 3 29 -3.80 3.40 0 -3 29 1.70 2.60 0 3 -29 4.60 2.40 0 3 29 4.10 2.40 0 4 29 163.08 6.50 0 -4 29 153.38 7.60 0 4 29 147.19 7.20 0 4 29 142.19 5.20 0 4 -29 151.38 7.40 0 4 -29 160.78 6.30 0 5 29 -0.60 1.90 0 5 -29 -2.50 3.20 0 5 29 0.00 2.30 0 5 -29 -4.60 2.80 0 -5 29 -0.50 3.20 0 5 29 -0.70 3.50 0 6 -29 16.30 3.50 0 6 29 15.20 4.00 0 6 -29 16.40 4.70 0 6 29 20.90 4.10 0 6 29 21.50 2.50 0 6 29 18.10 3.00 0 -6 29 11.40 3.80 0 7 29 -1.10 3.90 0 7 29 0.00 2.20 0 -7 29 1.80 3.50 0 7 29 0.30 2.60 0 7 -29 -7.80 3.20 0 -8 29 124.49 8.30 0 8 29 122.39 5.40 0 8 -29 122.69 8.00 0 8 29 116.09 5.80 0 8 29 113.69 8.60 0 9 29 -2.70 4.50 0 9 29 -4.20 3.10 0 -9 29 1.70 4.50 0 9 -29 0.10 4.20 -1 0 29 0.20 2.40 -1 0 -29 6.70 2.70 1 0 29 1.20 2.30 1 0 -29 1.80 2.50 -1 1 -29 3.40 2.70 -1 -1 29 11.90 3.20 1 -1 -29 3.50 2.50 1 1 29 6.70 2.60 -1 1 29 5.80 2.50 -1 -1 -29 7.50 2.60 1 1 -29 9.10 2.80 1 -1 29 10.80 2.80 -1 2 -29 41.80 4.70 -1 2 -29 40.70 3.10 -1 -2 29 44.10 4.70 1 2 29 38.40 4.20 1 2 -29 37.30 4.40 1 -2 29 39.90 4.60 -1 2 29 42.20 4.50 -1 2 29 42.50 4.70 -1 -3 29 3.10 3.00 -1 3 -29 5.60 2.60 1 3 29 2.70 2.30 1 3 29 4.40 3.30 1 -3 29 0.90 2.70 -1 3 29 2.20 3.60 1 3 -29 -1.70 2.50 -1 3 29 4.40 2.60 1 3 -29 3.30 2.30 1 4 29 113.49 6.20 1 4 29 101.19 4.60 -1 4 -29 98.19 6.70 -1 -4 29 103.39 6.40 1 4 29 106.69 5.40 -1 4 -29 100.09 6.30 -1 4 29 99.19 6.50 -1 4 29 106.99 5.70 1 4 -29 83.29 9.00 1 4 -29 102.89 5.20 1 -4 29 98.19 7.50 -1 5 -29 43.10 4.50 -1 5 -29 41.70 5.10 -1 -5 29 49.80 5.30 1 5 29 40.90 5.10 1 5 29 40.20 3.70 1 5 29 40.50 4.10 -1 5 29 43.20 2.80 -1 5 29 45.10 5.60 1 5 -29 43.30 5.10 -1 5 29 36.30 4.40 1 -5 29 42.00 4.70 1 6 29 0.90 2.40 1 6 29 3.80 2.30 1 6 29 0.40 3.30 -1 6 -29 -1.50 4.30 1 6 29 4.40 3.30 -1 -6 29 0.30 3.40 -1 6 -29 -0.30 3.00 -1 6 29 4.50 2.80 -1 6 29 4.10 3.60 -1 6 29 3.50 4.00 1 6 -29 2.60 3.10 1 6 -29 0.30 4.40 1 -6 29 2.30 3.20 -1 6 29 -0.20 1.70 1 7 29 6.60 3.90 1 7 29 5.60 2.70 -1 -7 29 7.00 4.00 -1 7 -29 5.40 3.60 1 7 29 6.60 2.50 -1 7 29 13.10 4.30 1 7 -29 4.40 3.70 1 -7 29 7.60 3.80 -1 7 29 5.80 1.90 -1 7 29 2.80 3.00 1 8 29 46.90 4.70 -1 -8 29 54.49 6.10 -1 8 -29 52.09 6.60 1 8 29 43.10 5.00 1 8 29 39.10 5.90 1 -8 29 48.70 5.90 -1 8 29 58.69 6.40 -1 8 29 47.60 3.80 1 8 -29 46.70 5.50 -1 8 29 44.30 5.30 -1 9 -29 25.00 5.00 1 9 29 17.10 5.70 -1 -9 29 22.40 5.30 1 9 29 22.40 3.90 -1 9 29 15.70 3.10 -1 9 29 7.70 5.00 1 9 -29 15.60 4.80 1 -9 29 19.90 5.10 -2 0 -29 2.20 2.50 2 0 -29 4.40 2.40 -2 0 29 -1.30 2.40 2 0 29 2.70 2.30 -2 1 -29 4.30 2.50 -2 1 -29 1.30 1.80 -2 -1 29 -1.80 2.40 2 -1 -29 2.50 2.50 2 1 29 0.40 2.30 -2 1 29 1.00 2.40 -2 -1 -29 2.10 2.80 2 -1 29 -3.30 2.30 2 1 -29 0.00 2.30 -2 -2 29 1.50 2.50 -2 2 -29 1.70 4.00 -2 2 -29 4.00 2.30 2 2 29 3.00 2.30 -2 2 29 -0.20 4.00 2 2 -29 0.80 2.40 -2 2 29 1.10 2.40 2 -2 29 3.40 2.70 2 3 29 3.70 2.20 2 3 29 4.20 2.30 -2 3 -29 2.00 2.80 2 3 29 5.30 3.30 -2 3 -29 2.30 3.10 -2 3 29 7.70 4.00 2 3 -29 2.10 2.00 2 -3 29 3.60 2.60 -2 3 29 -2.00 2.50 2 3 -29 3.50 2.70 -2 -4 29 10.60 3.10 2 4 29 16.60 3.40 -2 4 -29 6.40 3.10 2 4 29 14.20 2.60 -2 4 -29 6.80 3.00 2 4 29 9.40 2.60 2 4 -29 7.90 4.20 -2 4 29 10.10 2.90 -2 4 29 7.10 4.10 2 -4 29 4.60 2.90 2 4 -29 11.00 2.80 -2 5 -29 0.70 2.90 2 5 29 1.40 2.50 -2 -5 29 6.00 3.10 2 5 29 8.90 3.30 -2 5 -29 -0.10 3.60 2 5 29 -3.30 2.10 2 5 -29 -1.30 2.80 2 -5 29 4.40 3.30 -2 5 29 -1.70 4.10 2 5 -29 -1.80 3.30 -2 5 29 2.30 2.70 -2 -6 29 43.10 5.30 2 6 29 38.10 5.20 -2 6 -29 49.80 7.20 2 6 29 37.80 4.20 2 6 29 40.10 3.80 -2 6 -29 46.50 5.40 -2 6 29 40.40 5.10 -2 6 29 47.10 5.20 2 6 -29 53.79 5.50 2 -6 29 62.79 6.10 -2 6 29 60.29 5.20 2 7 29 4.70 2.30 -2 7 -29 11.20 3.60 2 7 29 3.40 4.10 2 7 29 0.80 2.90 -2 -7 29 3.50 3.70 -2 7 29 4.90 3.10 2 -7 29 0.70 4.00 2 7 -29 5.00 3.40 -2 7 29 2.30 4.00 -2 -8 29 -4.20 3.90 -2 8 -29 -2.90 3.70 2 8 29 1.30 3.40 2 8 29 2.60 4.40 2 8 -29 5.30 3.80 -2 8 29 8.10 3.60 2 -8 29 -1.90 3.90 -2 8 29 5.40 4.50 -2 8 29 4.50 1.90 -2 -9 29 4.70 4.50 -2 9 -29 -3.70 4.20 2 9 29 3.60 5.10 2 9 29 0.30 4.70 2 9 -29 1.90 4.20 2 -9 29 3.00 4.20 -2 9 29 2.30 2.80 -2 9 29 1.10 3.60 -2 9 29 1.00 4.80 3 0 29 3.40 2.40 -3 0 -29 5.30 3.60 3 0 -29 4.00 2.70 -3 0 -29 -1.10 1.70 -3 0 29 2.80 2.70 3 1 29 112.79 5.70 -3 -1 29 115.59 6.40 -3 1 -29 107.29 4.60 3 -1 -29 104.49 6.00 -3 1 29 116.59 6.30 3 -1 29 102.49 6.00 3 1 -29 114.99 6.10 -3 -2 29 30.90 4.40 -3 2 -29 37.30 4.20 -3 2 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55.19 6.80 -6 -2 35 57.99 5.50 6 2 35 39.70 4.90 6 2 -35 42.50 5.30 6 -2 35 51.39 5.90 -6 2 35 49.20 6.20 6 3 35 2.20 3.90 -6 -3 35 2.10 3.60 -6 3 -35 8.90 5.10 -6 -3 35 -1.70 5.00 6 3 -35 11.40 4.40 6 -3 35 3.80 4.60 -6 3 35 4.40 4.80 -7 0 35 2.10 2.80 7 0 35 -5.70 3.90 -7 0 35 -3.30 4.80 -7 0 -35 3.90 4.60 0 0 -36 94.59 7.50 0 0 36 89.79 7.50 0 1 -36 5.80 4.20 0 1 36 -9.70 3.60 0 -1 36 -0.60 4.00 0 -2 36 12.20 4.30 0 2 36 3.20 3.90 0 2 -36 7.50 4.50 0 3 -36 -1.90 3.90 0 -3 36 -7.00 4.30 0 3 36 4.20 4.00 0 4 -36 47.00 5.70 0 -4 36 65.69 7.70 0 4 36 39.60 6.70 1 0 36 24.90 4.80 -1 0 -36 33.20 4.80 1 0 -36 31.50 5.00 -1 0 36 30.10 5.10 -1 -1 36 24.50 4.90 -1 1 -36 19.80 4.80 1 1 36 23.30 4.60 -1 1 36 21.70 4.80 1 -1 36 20.10 4.90 1 1 -36 18.20 4.50 1 2 36 12.80 4.30 -1 2 -36 5.40 4.10 -1 -2 36 9.10 4.50 1 2 -36 17.60 4.50 1 -2 36 8.50 4.50 -1 2 36 15.90 4.60 -1 -3 36 2.90 4.30 1 3 36 6.90 4.70 -1 3 -36 12.30 4.60 1 -3 36 0.00 4.40 1 3 -36 5.90 4.20 -1 3 36 6.40 4.40 -1 4 -36 17.70 5.20 1 4 36 15.20 4.40 -1 -4 36 11.20 5.10 1 4 -36 10.20 4.50 -1 4 36 23.40 4.80 1 -4 36 12.40 4.70 2 0 36 72.29 7.00 -2 0 -36 75.89 7.40 2 0 -36 63.49 7.10 -2 0 36 60.79 7.40 2 1 36 5.60 3.80 -2 1 -36 3.00 4.20 -2 -1 36 2.10 4.30 2 -1 36 -4.00 3.80 2 1 -36 4.40 4.10 -2 1 36 11.10 4.40 -2 -2 36 -4.50 4.20 -2 2 -36 2.30 4.20 -2 2 36 1.60 4.20 2 2 -36 3.20 4.20 2 -2 36 -0.70 3.90 -2 3 -36 -1.30 3.90 2 3 36 -2.20 3.70 -2 -3 36 4.50 4.60 2 3 -36 2.80 4.20 2 -3 36 -2.60 4.20 -2 3 36 2.40 4.20 2 4 36 1.60 4.10 -2 4 -36 3.30 4.80 -2 -4 36 11.30 5.10 2 4 -36 5.90 4.50 -2 4 36 6.00 4.40 2 -4 36 0.50 4.60 -3 0 -36 38.30 5.30 -3 0 36 36.20 5.60 3 0 36 38.70 5.20 3 0 -36 36.00 5.00 -3 -1 36 1.20 4.20 3 1 36 3.40 4.00 -3 1 -36 9.80 4.30 -3 1 36 1.00 4.30 3 1 -36 -0.20 4.00 3 -1 36 7.10 4.30 -3 -2 36 29.20 5.20 -3 2 -36 29.00 5.30 3 2 36 28.50 5.50 3 2 -36 27.60 4.80 3 -2 36 33.30 5.10 -3 2 36 27.70 5.00 -3 3 -36 6.60 4.40 3 3 36 -4.40 3.80 -3 -3 36 2.70 4.70 3 3 -36 0.30 4.10 -3 3 36 -2.40 4.20 3 -3 36 3.10 4.50 -3 4 -36 34.70 6.10 3 4 36 34.70 4.60 -3 -4 36 31.50 5.70 3 4 -36 25.50 5.10 3 -4 36 26.90 5.40 -3 4 36 27.10 5.10 -4 0 36 65.59 7.90 4 0 -36 95.39 7.50 -4 0 -36 78.49 7.70 4 0 36 71.39 7.10 4 1 36 12.90 4.20 -4 1 -36 8.10 4.40 -4 -1 36 5.20 4.80 4 -1 36 20.10 4.50 4 1 -36 8.80 4.40 -4 1 36 17.00 5.00 -4 -2 36 75.19 8.10 -4 2 -36 90.89 8.50 4 2 36 72.69 6.70 4 -2 36 67.29 7.50 4 2 -36 59.29 7.40 -4 2 36 64.89 7.70 -4 -3 36 0.60 4.90 4 3 36 8.40 4.00 -4 3 -36 6.50 5.00 4 -3 36 9.50 4.70 4 3 -36 3.00 4.40 -4 3 36 9.20 4.90 -5 0 -36 4.10 4.50 5 0 36 9.00 4.30 -5 0 36 16.20 5.00 5 1 36 5.00 4.10 -5 -1 36 -1.70 4.60 -5 1 -36 5.20 4.90 -5 1 36 3.70 4.70 5 1 -36 -4.60 4.10 5 -1 36 1.90 4.10 -5 -2 36 -7.00 4.90 5 2 36 1.30 4.00 -5 2 -36 10.20 5.00 5 2 -36 0.20 4.30 -5 2 36 -1.10 4.60 5 -2 36 1.60 4.40 0 0 -37 6.30 4.30 0 0 37 1.70 4.30 0 1 37 1.80 4.20 0 -1 37 5.10 4.40 0 1 -37 -7.10 4.40 0 -2 37 11.40 4.80 0 2 37 -1.70 4.20 0 2 -37 5.30 4.60 0 3 -37 -4.70 4.40 0 3 37 7.30 4.30 0 -3 37 3.10 4.70 1 0 -37 2.60 4.30 -1 0 37 -6.30 4.30 -1 0 -37 1.00 4.70 1 0 37 -0.90 4.40 -1 -1 37 31.40 5.40 1 1 37 23.10 4.90 -1 1 -37 19.50 5.30 1 -1 37 18.20 5.10 -1 1 37 22.30 4.70 1 1 -37 20.40 4.80 1 2 37 -0.10 4.10 -1 -2 37 12.20 4.90 -1 2 -37 7.70 4.70 -1 2 37 19.30 4.60 1 -2 37 9.70 4.70 1 2 -37 1.80 4.40 1 3 37 7.10 4.50 -1 3 -37 17.30 5.10 -1 -3 37 6.40 4.80 1 3 -37 7.80 4.90 1 -3 37 9.70 4.80 -1 3 37 12.80 4.70 2 0 37 0.20 4.20 -2 0 37 0.00 4.50 2 0 -37 -1.50 4.30 -2 0 -37 3.20 4.40 2 1 37 6.50 4.20 -2 -1 37 13.90 4.80 -2 1 -37 5.70 4.50 -2 1 37 4.80 4.50 2 1 -37 -0.70 4.30 2 -1 37 2.00 4.30 -2 -2 37 -4.00 4.40 2 2 37 -2.20 4.00 -2 2 -37 0.70 4.70 2 -2 37 -1.20 4.50 2 2 -37 -0.30 4.40 -2 2 37 -2.40 4.60 -2 -3 37 19.40 5.20 -2 3 -37 20.60 5.40 2 -3 37 19.10 5.00 -2 3 37 18.10 5.10 2 3 -37 21.50 5.10 -3 0 37 -2.10 4.50 3 0 37 2.30 4.20 3 0 -37 3.40 4.30 -3 0 -37 0.60 4.60 3 1 37 98.39 7.90 -3 -1 37 97.19 8.80 -3 1 -37 105.49 8.70 -3 1 37 106.19 9.00 3 1 -37 102.09 8.10 3 -1 37 99.79 8.30 3 2 37 60.49 7.20 -3 2 -37 63.19 6.80 -3 -2 37 74.79 8.30 3 -2 37 66.99 8.00 -3 2 37 80.69 8.20 3 2 -37 66.19 7.90 4 0 37 2.70 4.10 -4 0 -37 1.40 4.80 -4 0 37 12.80 5.10 -4 -1 37 0.60 5.00 4 1 37 7.20 4.50 -4 1 -37 7.10 4.60 4 -1 37 -1.00 4.30 -4 1 37 15.90 5.00 4 1 -37 -5.00 4.30 0 0 -38 14.90 5.10 0 0 38 6.10 4.70 0 -1 38 -0.20 4.80 0 1 -38 13.60 5.00 0 1 38 7.30 4.60 1 0 38 68.79 8.30 1 0 -38 56.79 6.30 -1 0 -38 66.39 8.00 -1 0 38 66.89 8.20 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 65165 _shelx_res_file ; TITL gliesep200207_0ma_a.res in Pbca gliesep200207_0ma.res created by SHELXL-2019/1 at 18:28:59 on 25-May-2023 REM Old TITL GlieseP200207_0ma in Pbca REM SHELXT solution in Pbca REM R1 0.126, Rweak 0.004, Alpha 0.026, Orientation as input REM Formula found by SHELXT: C25 N Si CELL 0.71073 13.3292 11.1365 28.5973 90 90 90 ZERR 8 0.0006 0.0005 0.0012 0 0 0 LATT 1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H B N Si UNIT 192 240 8 8 8 L.S. 10 PLAN 5 SIZE 0.28 0.22 0.2 TEMP -173.15 CONF BOND $H list 4 MORE -1 fmap 2 acta OMIT 1 0 2 REM REM REM WGHT 0.042100 2.637900 FVAR 0.26657 SI1 5 0.644138 0.535257 0.676761 11.00000 0.01541 0.01078 = 0.01295 -0.00092 -0.00323 -0.00045 N1 4 0.596215 0.462294 0.626649 11.00000 0.01504 0.00869 = 0.01267 -0.00034 -0.00054 0.00044 C11 1 0.521255 0.647512 0.580876 11.00000 0.01377 0.01149 = 0.01053 -0.00006 -0.00333 -0.00094 C19 1 0.417259 0.831444 0.586330 11.00000 0.01563 0.01364 = 0.01543 -0.00101 -0.00496 0.00205 C12 1 0.593918 0.714747 0.556103 11.00000 0.01493 0.01153 = 0.01141 0.00035 -0.00371 -0.00085 C24 1 0.432273 0.705650 0.595060 11.00000 0.01360 0.01295 = 0.01258 -0.00048 -0.00361 0.00006 C17 1 0.578253 0.840293 0.546603 11.00000 0.01726 0.01221 = 0.01439 0.00087 -0.00538 -0.00277 C18 1 0.491125 0.896066 0.562574 11.00000 0.02039 0.01121 = 0.01866 0.00090 -0.00549 0.00109 AFIX 43 H18 2 0.481850 0.979511 0.557198 11.00000 -1.20000 AFIX 0 C13 1 0.685301 0.661953 0.539871 11.00000 0.01770 0.01320 = 0.01496 -0.00116 -0.00049 -0.00050 AFIX 43 H13 2 0.698476 0.579903 0.546572 11.00000 -1.20000 AFIX 0 C16 1 0.652392 0.904627 0.520649 11.00000 0.02123 0.01334 = 0.01929 0.00461 -0.00525 -0.00482 AFIX 43 H16 2 0.642415 0.987500 0.514292 11.00000 -1.20000 AFIX 0 C23 1 0.354839 0.642562 0.619565 11.00000 0.01773 0.01590 = 0.01620 0.00076 -0.00131 -0.00137 AFIX 43 H23 2 0.363308 0.559548 0.626116 11.00000 -1.20000 AFIX 0 C14 1 0.754057 0.726475 0.514997 11.00000 0.01803 0.01947 = 0.01715 -0.00269 0.00199 -0.00192 AFIX 43 H14 2 0.813807 0.688816 0.504372 11.00000 -1.20000 AFIX 0 C2 1 0.480115 0.291425 0.572709 11.00000 0.01999 0.01275 = 0.02241 -0.00272 -0.00226 -0.00417 AFIX 43 H2 2 0.429913 0.239109 0.560836 11.00000 -1.20000 AFIX 0 C1 1 0.488844 0.416128 0.553818 11.00000 0.02036 0.01359 = 0.01519 0.00087 -0.00341 -0.00054 AFIX 23 H1A 2 0.421131 0.445468 0.545345 11.00000 -1.20000 H1B 2 0.529719 0.414180 0.524923 11.00000 -1.20000 AFIX 0 C3 1 0.541882 0.253110 0.605929 11.00000 0.02494 0.00880 = 0.02214 0.00072 -0.00136 -0.00186 AFIX 43 H3 2 0.534485 0.173818 0.617685 11.00000 -1.20000 AFIX 0 C15 1 0.736751 0.849789 0.504893 11.00000 0.02099 0.02104 = 0.01639 0.00295 0.00007 -0.00920 AFIX 43 H15 2 0.784345 0.893832 0.487081 11.00000 -1.20000 AFIX 0 C20 1 0.326579 0.887218 0.601943 11.00000 0.02093 0.01726 = 0.02188 -0.00196 -0.00351 0.00606 AFIX 43 H20 2 0.316206 0.970332 0.596236 11.00000 -1.20000 AFIX 0 C7 1 0.587073 0.465276 0.731835 11.00000 0.03023 0.01958 = 0.01254 0.00052 0.00000 0.00111 C5 1 0.615174 0.698694 0.676834 11.00000 0.02620 0.01305 = 0.01899 -0.00362 -0.00633 -0.00011 AFIX 137 H5A 2 0.639979 0.735062 0.647849 11.00000 -1.50000 H5B 2 0.647856 0.736898 0.703685 11.00000 -1.50000 H5C 2 0.542432 0.710205 0.679006 11.00000 -1.50000 AFIX 0 C4 1 0.622998 0.331860 0.625346 11.00000 0.02042 0.00974 = 0.01639 -0.00089 -0.00474 0.00313 AFIX 23 H4A 2 0.638945 0.304962 0.657494 11.00000 -1.20000 H4B 2 0.684208 0.321657 0.606145 11.00000 -1.20000 AFIX 0 C22 1 0.269361 0.698767 0.633694 11.00000 0.01598 0.02586 = 0.02025 -0.00026 0.00143 -0.00209 AFIX 43 H22 2 0.218894 0.654525 0.649613 11.00000 -1.20000 AFIX 0 C21 1 0.255081 0.823145 0.624804 11.00000 0.01679 0.02565 = 0.02382 -0.00424 0.00020 0.00592 AFIX 43 H21 2 0.195274 0.861639 0.634892 11.00000 -1.20000 AFIX 0 C6 1 0.783520 0.520134 0.676160 11.00000 0.01742 0.01850 = 0.03490 0.00054 -0.00764 -0.00126 AFIX 137 H6A 2 0.801667 0.434860 0.675946 11.00000 -1.50000 H6B 2 0.811589 0.558499 0.704089 11.00000 -1.50000 H6C 2 0.810525 0.559100 0.648130 11.00000 -1.50000 AFIX 0 C8 1 0.476693 0.433012 0.723045 11.00000 0.02645 0.04118 = 0.02557 0.00846 0.00921 -0.00161 AFIX 137 H8A 2 0.440495 0.504437 0.712272 11.00000 -1.50000 H8B 2 0.446415 0.403817 0.752130 11.00000 -1.50000 H8C 2 0.472708 0.370187 0.699121 11.00000 -1.50000 AFIX 0 B1 3 0.538203 0.507548 0.589596 11.00000 0.01162 0.01161 = 0.01244 0.00052 0.00156 -0.00027 C9 1 0.642709 0.353585 0.749918 11.00000 0.04468 0.03503 = 0.02376 0.01445 0.00276 0.00811 AFIX 137 H9A 2 0.635604 0.288080 0.727276 11.00000 -1.50000 H9B 2 0.614021 0.328939 0.779975 11.00000 -1.50000 H9C 2 0.713960 0.372554 0.754027 11.00000 -1.50000 AFIX 0 C10 1 0.591408 0.559227 0.771239 11.00000 0.08168 0.03630 = 0.01651 -0.00641 0.00586 -0.00839 AFIX 137 H10A 2 0.660967 0.585254 0.775764 11.00000 -1.50000 H10B 2 0.566082 0.523710 0.800285 11.00000 -1.50000 H10C 2 0.549936 0.628553 0.762762 11.00000 -1.50000 AFIX 0 HKLF 4 REM gliesep200207_0ma_a.res in Pbca REM wR2 = 0.1033, GooF = S = 1.068, Restrained GooF = 1.068 for all data REM R1 = 0.0421 for 4416 Fo > 4sig(Fo) and 0.0541 for all 5264 data REM 249 parameters refined using 0 restraints END WGHT 0.0414 2.6480 REM Highest difference peak 0.370, deepest hole -0.285, 1-sigma level 0.050 Q1 1 0.5293 0.5805 0.5849 11.00000 0.05 0.37 Q2 1 0.5847 0.7807 0.5510 11.00000 0.05 0.35 Q3 1 0.5147 0.4604 0.5704 11.00000 0.05 0.34 Q4 1 0.6309 0.6190 0.6760 11.00000 0.05 0.34 Q5 1 0.6149 0.4970 0.7068 11.00000 0.05 0.33 ; _shelx_res_checksum 35317 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Si Si1 0.64414(3) 0.53526(3) 0.67676(2) 0.01305(9) Uani d 1 . . N N1 0.59622(8) 0.46229(9) 0.62665(4) 0.0121(2) Uani d 1 . . C C11 0.52126(9) 0.64751(11) 0.58088(4) 0.0119(2) Uani d 1 . . C C19 0.41726(10) 0.83144(12) 0.58633(5) 0.0149(3) Uani d 1 . . C C12 0.59392(9) 0.71475(11) 0.55610(4) 0.0126(2) Uani d 1 . . C C24 0.43227(9) 0.70565(11) 0.59506(4) 0.0130(2) Uani d 1 . . C C17 0.57825(10) 0.84029(12) 0.54660(5) 0.0146(3) Uani d 1 . . C C18 0.49112(10) 0.89607(12) 0.56257(5) 0.0168(3) Uani d 1 . . H H18 0.481850 0.979511 0.557198 0.020 Uiso calc 1 . . C C13 0.68530(10) 0.66195(12) 0.53987(4) 0.0153(3) Uani d 1 . . H H13 0.698476 0.579903 0.546572 0.018 Uiso calc 1 . . C C16 0.65239(10) 0.90463(12) 0.52065(5) 0.0180(3) Uani d 1 . . H H16 0.642415 0.987500 0.514292 0.022 Uiso calc 1 . . C C23 0.35484(10) 0.64256(12) 0.61956(5) 0.0166(3) Uani d 1 . . H H23 0.363308 0.559548 0.626116 0.020 Uiso calc 1 . . C C14 0.75406(10) 0.72648(12) 0.51500(5) 0.0182(3) Uani d 1 . . H H14 0.813807 0.688816 0.504372 0.022 Uiso calc 1 . . C C2 0.48012(10) 0.29143(12) 0.57271(5) 0.0184(3) Uani d 1 . . H H2 0.429913 0.239109 0.560836 0.022 Uiso calc 1 . . C C1 0.48884(10) 0.41613(12) 0.55382(5) 0.0164(3) Uani d 1 . . H H1A 0.421131 0.445468 0.545345 0.020 Uiso calc 1 . . H H1B 0.529719 0.414180 0.524923 0.020 Uiso calc 1 . . C C3 0.54188(11) 0.25311(12) 0.60593(5) 0.0186(3) Uani d 1 . . H H3 0.534485 0.173818 0.617685 0.022 Uiso calc 1 . . C C15 0.73675(11) 0.84979(13) 0.50489(5) 0.0195(3) Uani d 1 . . H H15 0.784345 0.893832 0.487081 0.023 Uiso calc 1 . . C C20 0.32658(11) 0.88722(13) 0.60194(5) 0.0200(3) Uani d 1 . . H H20 0.316206 0.970332 0.596236 0.024 Uiso calc 1 . . C C7 0.58707(11) 0.46528(13) 0.73184(5) 0.0208(3) Uani d 1 . . C C5 0.61517(11) 0.69869(12) 0.67683(5) 0.0194(3) Uani d 1 . . H H5A 0.639979 0.735062 0.647849 0.029 Uiso calc 1 . . H H5B 0.647856 0.736898 0.703685 0.029 Uiso calc 1 . . H H5C 0.542432 0.710205 0.679006 0.029 Uiso calc 1 . . C C4 0.62300(10) 0.33186(11) 0.62535(5) 0.0155(3) Uani d 1 . . H H4A 0.638945 0.304962 0.657494 0.019 Uiso calc 1 . . H H4B 0.684208 0.321657 0.606145 0.019 Uiso calc 1 . . C C22 0.26936(10) 0.69877(14) 0.63369(5) 0.0207(3) Uani d 1 . . H H22 0.218894 0.654525 0.649613 0.025 Uiso calc 1 . . C C21 0.25508(11) 0.82314(14) 0.62480(5) 0.0221(3) Uani d 1 . . H H21 0.195274 0.861639 0.634892 0.027 Uiso calc 1 . . C C6 0.78352(10) 0.52013(13) 0.67616(6) 0.0236(3) Uani d 1 . . H H6A 0.801667 0.434860 0.675946 0.035 Uiso calc 1 . . H H6B 0.811589 0.558499 0.704089 0.035 Uiso calc 1 . . H H6C 0.810525 0.559100 0.648130 0.035 Uiso calc 1 . . C C8 0.47669(12) 0.43301(16) 0.72304(6) 0.0311(4) Uani d 1 . . H H8A 0.440495 0.504437 0.712272 0.047 Uiso calc 1 . . H H8B 0.446415 0.403817 0.752130 0.047 Uiso calc 1 . . H H8C 0.472708 0.370187 0.699121 0.047 Uiso calc 1 . . B B1 0.53820(10) 0.50755(13) 0.58960(5) 0.0119(3) Uani d 1 . . C C9 0.64271(14) 0.35359(15) 0.74992(6) 0.0345(4) Uani d 1 . . H H9A 0.635604 0.288080 0.727276 0.052 Uiso calc 1 . . H H9B 0.614021 0.328939 0.779975 0.052 Uiso calc 1 . . H H9C 0.713960 0.372554 0.754027 0.052 Uiso calc 1 . . C C10 0.59141(18) 0.55923(17) 0.77124(6) 0.0448(5) Uani d 1 . . H H10A 0.660967 0.585254 0.775764 0.067 Uiso calc 1 . . H H10B 0.566082 0.523710 0.800285 0.067 Uiso calc 1 . . H H10C 0.549936 0.628553 0.762762 0.067 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Si1 0.01541(18) 0.01078(17) 0.01295(17) -0.00045(13) -0.00323(13) -0.00092(13) N1 0.0150(5) 0.0087(5) 0.0127(5) 0.0004(4) -0.0005(4) -0.0003(4) C11 0.0138(6) 0.0115(6) 0.0105(6) -0.0009(5) -0.0033(4) -0.0001(5) C19 0.0156(6) 0.0136(6) 0.0154(6) 0.0021(5) -0.0050(5) -0.0010(5) C12 0.0149(6) 0.0115(6) 0.0114(6) -0.0008(5) -0.0037(5) 0.0004(5) C24 0.0136(6) 0.0130(6) 0.0126(6) 0.0001(5) -0.0036(5) -0.0005(5) C17 0.0173(6) 0.0122(6) 0.0144(6) -0.0028(5) -0.0054(5) 0.0009(5) C18 0.0204(7) 0.0112(6) 0.0187(7) 0.0011(5) -0.0055(5) 0.0009(5) C13 0.0177(6) 0.0132(6) 0.0150(6) -0.0005(5) -0.0005(5) -0.0012(5) C16 0.0212(7) 0.0133(6) 0.0193(7) -0.0048(5) -0.0053(5) 0.0046(5) C23 0.0177(6) 0.0159(6) 0.0162(6) -0.0014(5) -0.0013(5) 0.0008(5) C14 0.0180(6) 0.0195(7) 0.0171(6) -0.0019(5) 0.0020(5) -0.0027(5) C2 0.0200(7) 0.0127(6) 0.0224(7) -0.0042(5) -0.0023(5) -0.0027(5) C1 0.0204(7) 0.0136(6) 0.0152(6) -0.0005(5) -0.0034(5) 0.0009(5) C3 0.0249(7) 0.0088(6) 0.0221(7) -0.0019(5) -0.0014(5) 0.0007(5) C15 0.0210(7) 0.0210(7) 0.0164(6) -0.0092(6) 0.0001(5) 0.0030(5) C20 0.0209(7) 0.0173(7) 0.0219(7) 0.0061(5) -0.0035(5) -0.0020(5) C7 0.0302(8) 0.0196(7) 0.0125(6) 0.0011(6) 0.0000(5) 0.0005(5) C5 0.0262(7) 0.0131(6) 0.0190(7) -0.0001(5) -0.0063(6) -0.0036(5) C4 0.0204(7) 0.0097(6) 0.0164(6) 0.0031(5) -0.0047(5) -0.0009(5) C22 0.0160(7) 0.0259(7) 0.0202(7) -0.0021(6) 0.0014(5) -0.0003(6) C21 0.0168(7) 0.0256(7) 0.0238(7) 0.0059(6) 0.0002(6) -0.0042(6) C6 0.0174(7) 0.0185(7) 0.0349(8) -0.0013(5) -0.0076(6) 0.0005(6) C8 0.0264(8) 0.0412(10) 0.0256(8) -0.0016(7) 0.0092(6) 0.0085(7) B1 0.0116(6) 0.0116(6) 0.0124(6) -0.0003(5) 0.0016(5) 0.0005(5) C9 0.0447(10) 0.0350(9) 0.0238(8) 0.0081(8) 0.0028(7) 0.0144(7) C10 0.0817(15) 0.0363(10) 0.0165(8) -0.0084(10) 0.0059(9) -0.0064(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag N1 Si1 C7 . . 109.65(6) ? N1 Si1 C5 . . 112.07(6) ? N1 Si1 C6 . . 108.12(6) ? C5 Si1 C7 . . 108.35(7) ? C5 Si1 C6 . . 107.16(7) ? C6 Si1 C7 . . 111.50(7) ? C4 N1 Si1 . . 112.36(8) ? B1 N1 Si1 . . 130.21(9) ? B1 N1 C4 . . 117.43(10) ? C12 C11 B1 . . 119.92(11) ? C24 C11 C12 . . 118.47(11) ? C24 C11 B1 . . 121.51(11) ? C18 C19 C24 . . 119.27(12) ? C18 C19 C20 . . 121.60(12) ? C20 C19 C24 . . 119.13(12) ? C11 C12 C17 . . 120.62(12) ? C11 C12 C13 . . 121.88(11) ? C13 C12 C17 . . 117.49(12) ? C11 C24 C19 . . 120.97(12) ? C11 C24 C23 . . 121.44(12) ? C23 C24 C19 . . 117.58(12) ? C18 C17 C12 . . 119.46(12) ? C18 C17 C16 . . 121.54(12) ? C16 C17 C12 . . 119.00(12) ? C19 C18 H18 . . 119.4 ? C17 C18 C19 . . 121.15(12) ? C17 C18 H18 . . 119.4 ? C12 C13 H13 . . 119.2 ? C14 C13 C12 . . 121.65(12) ? C14 C13 H13 . . 119.2 ? C17 C16 H16 . . 119.3 ? C15 C16 C17 . . 121.34(12) ? C15 C16 H16 . . 119.3 ? C24 C23 H23 . . 119.2 ? C22 C23 C24 . . 121.53(13) ? C22 C23 H23 . . 119.2 ? C13 C14 H14 . . 119.8 ? C13 C14 C15 . . 120.36(13) ? C15 C14 H14 . . 119.8 ? C1 C2 H2 . . 119.7 ? C3 C2 H2 . . 119.7 ? C3 C2 C1 . . 120.60(12) ? C2 C1 H1A . . 108.9 ? C2 C1 H1B . . 108.9 ? C2 C1 B1 . . 113.30(11) ? H1A C1 H1B . . 107.7 ? B1 C1 H1A . . 108.9 ? B1 C1 H1B . . 108.9 ? C2 C3 H3 . . 119.2 ? C2 C3 C4 . . 121.63(12) ? C4 C3 H3 . . 119.2 ? C16 C15 C14 . . 120.11(13) ? C16 C15 H15 . . 119.9 ? C14 C15 H15 . . 119.9 ? C19 C20 H20 . . 119.5 ? C21 C20 C19 . . 121.00(13) ? C21 C20 H20 . . 119.5 ? C8 C7 Si1 . . 109.95(10) ? C8 C7 C9 . . 109.14(13) ? C8 C7 C10 . . 108.36(14) ? C9 C7 Si1 . . 114.47(11) ? C9 C7 C10 . . 106.60(14) ? C10 C7 Si1 . . 108.10(11) ? Si1 C5 H5A . . 109.5 ? Si1 C5 H5B . . 109.5 ? Si1 C5 H5C . . 109.5 ? H5A C5 H5B . . 109.5 ? H5A C5 H5C . . 109.5 ? H5B C5 H5C . . 109.5 ? N1 C4 C3 . . 113.90(11) ? N1 C4 H4A . . 108.8 ? N1 C4 H4B . . 108.8 ? C3 C4 H4A . . 108.8 ? C3 C4 H4B . . 108.8 ? H4A C4 H4B . . 107.7 ? C23 C22 H22 . . 119.8 ? C23 C22 C21 . . 120.48(13) ? C21 C22 H22 . . 119.8 ? C20 C21 C22 . . 120.28(13) ? C20 C21 H21 . . 119.9 ? C22 C21 H21 . . 119.9 ? Si1 C6 H6A . . 109.5 ? Si1 C6 H6B . . 109.5 ? Si1 C6 H6C . . 109.5 ? H6A C6 H6B . . 109.5 ? H6A C6 H6C . . 109.5 ? H6B C6 H6C . . 109.5 ? C7 C8 H8A . . 109.5 ? C7 C8 H8B . . 109.5 ? C7 C8 H8C . . 109.5 ? H8A C8 H8B . . 109.5 ? H8A C8 H8C . . 109.5 ? H8B C8 H8C . . 109.5 ? N1 B1 C11 . . 123.12(11) ? N1 B1 C1 . . 118.97(11) ? C1 B1 C11 . . 117.89(11) ? C7 C9 H9A . . 109.5 ? C7 C9 H9B . . 109.5 ? C7 C9 H9C . . 109.5 ? H9A C9 H9B . . 109.5 ? H9A C9 H9C . . 109.5 ? H9B C9 H9C . . 109.5 ? C7 C10 H10A . . 109.5 ? C7 C10 H10B . . 109.5 ? C7 C10 H10C . . 109.5 ? H10A C10 H10B . . 109.5 ? H10A C10 H10C . . 109.5 ? H10B C10 H10C . . 109.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Si1 N1 . 1.7669(11) ? Si1 C7 . 1.9148(14) ? Si1 C5 . 1.8606(14) ? Si1 C6 . 1.8655(15) ? N1 C4 . 1.4963(16) ? N1 B1 . 1.4052(17) ? C11 C12 . 1.4144(17) ? C11 C24 . 1.4108(18) ? C11 B1 . 1.5946(18) ? C19 C24 . 1.4370(18) ? C19 C18 . 1.3960(19) ? C19 C20 . 1.4304(19) ? C12 C17 . 1.4395(18) ? C12 C13 . 1.4300(18) ? C24 C23 . 1.4318(18) ? C17 C18 . 1.3940(19) ? C17 C16 . 1.4286(19) ? C18 H18 . 0.9500 ? C13 H13 . 0.9500 ? C13 C14 . 1.3646(19) ? C16 H16 . 0.9500 ? C16 C15 . 1.357(2) ? C23 H23 . 0.9500 ? C23 C22 . 1.3613(19) ? C14 H14 . 0.9500 ? C14 C15 . 1.422(2) ? C2 H2 . 0.9500 ? C2 C1 . 1.4947(18) ? C2 C3 . 1.3276(19) ? C1 H1A . 0.9900 ? C1 H1B . 0.9900 ? C1 B1 . 1.5863(19) ? C3 H3 . 0.9500 ? C3 C4 . 1.4988(18) ? C15 H15 . 0.9500 ? C20 H20 . 0.9500 ? C20 C21 . 1.358(2) ? C7 C8 . 1.535(2) ? C7 C9 . 1.538(2) ? C7 C10 . 1.539(2) ? C5 H5A . 0.9800 ? C5 H5B . 0.9800 ? C5 H5C . 0.9800 ? C4 H4A . 0.9900 ? C4 H4B . 0.9900 ? C22 H22 . 0.9500 ? C22 C21 . 1.421(2) ? C21 H21 . 0.9500 ? C6 H6A . 0.9800 ? C6 H6B . 0.9800 ? C6 H6C . 0.9800 ? C8 H8A . 0.9800 ? C8 H8B . 0.9800 ? C8 H8C . 0.9800 ? C9 H9A . 0.9800 ? C9 H9B . 0.9800 ? C9 H9C . 0.9800 ? C10 H10A . 0.9800 ? C10 H10B . 0.9800 ? C10 H10C . 0.9800 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_D _geom_hbond_site_symmetry_H _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C5 H5A Cg2 1_555 1_555 1_555 0.98 2.86 3.4529(15) 120 y C5 H5A Cg5 1_555 1_555 1_555 0.98 2.91 3.7305(15) 142 y C5 H5A Cg7 1_555 1_555 1_555 0.98 2.88 3.4772(15) 120 y C2 H2 Cg3 1_555 1_555 5_666 0.95 2.92 3.6380(15) 133 y C4 H4B Cg3 1_555 1_555 8_755 0.99 2.97 3.9373(15) 167 y loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag Si1 N1 C4 C3 . . . . 143.11(10) ? Si1 N1 B1 C11 . . . . 12.58(19) ? Si1 N1 B1 C1 . . . . -168.86(9) ? C11 C12 C17 C18 . . . . 0.84(18) ? C11 C12 C17 C16 . . . . -178.72(12) ? C11 C12 C13 C14 . . . . 178.38(12) ? C11 C24 C23 C22 . . . . 179.33(13) ? C19 C24 C23 C22 . . . . 0.77(19) ? C19 C20 C21 C22 . . . . 0.1(2) ? C12 C11 C24 C19 . . . . -2.54(18) ? C12 C11 C24 C23 . . . . 178.94(12) ? C12 C11 B1 N1 . . . . 83.53(16) ? C12 C11 B1 C1 . . . . -95.05(14) ? C12 C17 C18 C19 . . . . -2.07(19) ? C12 C17 C16 C15 . . . . 0.0(2) ? C12 C13 C14 C15 . . . . 0.7(2) ? C24 C11 C12 C17 . . . . 1.44(18) ? C24 C11 C12 C13 . . . . -178.99(11) ? C24 C11 B1 N1 . . . . -100.06(15) ? C24 C11 B1 C1 . . . . 81.36(15) ? C24 C19 C18 C17 . . . . 0.99(19) ? C24 C19 C20 C21 . . . . 0.1(2) ? C24 C23 C22 C21 . . . . -0.6(2) ? C17 C12 C13 C14 . . . . -2.04(19) ? C17 C16 C15 C14 . . . . -1.4(2) ? C18 C19 C24 C11 . . . . 1.37(19) ? C18 C19 C24 C23 . . . . 179.94(12) ? C18 C19 C20 C21 . . . . 179.65(13) ? C18 C17 C16 C15 . . . . -179.54(13) ? C13 C12 C17 C18 . . . . -178.75(12) ? C13 C12 C17 C16 . . . . 1.69(18) ? C13 C14 C15 C16 . . . . 1.1(2) ? C16 C17 C18 C19 . . . . 177.47(12) ? C23 C22 C21 C20 . . . . 0.2(2) ? C2 C1 B1 N1 . . . . 20.11(17) ? C2 C1 B1 C11 . . . . -161.25(12) ? C2 C3 C4 N1 . . . . 32.76(19) ? C1 C2 C3 C4 . . . . -0.7(2) ? C3 C2 C1 B1 . . . . -25.46(19) ? C20 C19 C24 C11 . . . . -179.05(12) ? C20 C19 C24 C23 . . . . -0.48(18) ? C20 C19 C18 C17 . . . . -178.58(13) ? C7 Si1 N1 C4 . . . . -62.08(10) ? C7 Si1 N1 B1 . . . . 117.35(12) ? C5 Si1 N1 C4 . . . . 177.55(9) ? C5 Si1 N1 B1 . . . . -3.01(14) ? C4 N1 B1 C11 . . . . -168.01(11) ? C4 N1 B1 C1 . . . . 10.55(17) ? C6 Si1 N1 C4 . . . . 59.67(10) ? C6 Si1 N1 B1 . . . . -120.89(12) ? B1 N1 C4 C3 . . . . -36.40(16) ? B1 C11 C12 C17 . . . . 177.96(11) ? B1 C11 C12 C13 . . . . -2.47(18) ? B1 C11 C24 C19 . . . . -179.00(11) ? B1 C11 C24 C23 . . . . 2.49(18) ?