#------------------------------------------------------------------------------ #$Date: 2023-10-10 04:15:23 +0200 (Tue, 10 Oct 2023) $ #$Revision: 286863 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/28/2022875.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022875 loop_ _publ_author_name 'Poreba, Tomasz' 'Garbarino, Gaston' 'Comboni, Davide' 'Mezouar, Mohamed' _publ_section_title ; Deformation of polyiodides in Cs2I8 crystals at high pressure ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B Structural Science, Crystal Engineering and Materials' _journal_page_first 934 _journal_page_last 939 _journal_paper_doi 10.1107/S2052520621010192 _journal_volume 77 _journal_year 2021 _chemical_formula_moiety 'Cs I4' _chemical_formula_sum 'Cs I4' _chemical_formula_weight 640.51 _chemical_name_common 'Cesium Tetraiodide' _chemical_name_systematic 'dicesium octaiodide' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_primary dual _audit_creation_date 2021-07-19 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2021-07-20 deposited with the CCDC. 2021-07-23 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 114.957(9) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 10.1323(13) _cell_length_b 8.88899(15) _cell_length_c 11.0453(4) _cell_measurement_pressure 430000 _cell_measurement_reflns_used 1544 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 20.8080 _cell_measurement_theta_min 2.1480 _cell_volume 901.91(14) _computing_cell_refinement 'CrysAlisPro 1.171.40.67a (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.40.67a (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.40.67a (Rigaku OD, 2019)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT (Sheldrick, 2015)' _diffrn_ambient_environment Helium _diffrn_ambient_pressure 430000 _diffrn_ambient_temperature 296(2) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 13.3333 _diffrn_detector_type 'Eiger 9M CdTe' _diffrn_measured_fraction_theta_full 0.375 _diffrn_measured_fraction_theta_max 0.260 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -32.00 32.00 0.50 0.20 -- 0.00 0.00 0.00 128 ; _diffrn_measurement_device '1-circle goniometer' _diffrn_measurement_device_type 'esperanto-CrysAlisPro-abstract goniometer imported esperanto images' _diffrn_measurement_method 'phi scan' _diffrn_orient_matrix_UB_11 0.0423462000 _diffrn_orient_matrix_UB_12 -0.0107919000 _diffrn_orient_matrix_UB_13 0.0082439000 _diffrn_orient_matrix_UB_21 -0.0117356000 _diffrn_orient_matrix_UB_22 -0.0080106000 _diffrn_orient_matrix_UB_23 -0.0398509000 _diffrn_orient_matrix_UB_31 0.0082149000 _diffrn_orient_matrix_UB_32 0.0442220000 _diffrn_orient_matrix_UB_33 -0.0052027000 _diffrn_radiation_collimation '0.02 mm double pinhole' _diffrn_radiation_monochromator synchrotron _diffrn_radiation_probe x-ray _diffrn_radiation_type synchrotron _diffrn_radiation_wavelength 0.41077 _diffrn_reflns_av_R_equivalents 0.0188 _diffrn_reflns_av_unetI/netI 0.0233 _diffrn_reflns_Laue_measured_fraction_full 0.375 _diffrn_reflns_Laue_measured_fraction_max 0.260 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_h_min -6 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_number 2140 _diffrn_reflns_point_group_measured_fraction_full 0.375 _diffrn_reflns_point_group_measured_fraction_max 0.260 _diffrn_reflns_theta_full 14.268 _diffrn_reflns_theta_max 20.009 _diffrn_reflns_theta_min 2.151 _diffrn_source 'undulator, ID15B, ESRF' _exptl_absorpt_coefficient_mu 4.036 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.36211 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.67a (Rigaku Oxford Diffraction, 2019) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'dark red' _exptl_crystal_colour_modifier dark _exptl_crystal_colour_primary red _exptl_crystal_density_diffrn 4.717 _exptl_crystal_description plate _exptl_crystal_F_000 1068 _exptl_crystal_size_max 0.035 _exptl_crystal_size_mid 0.015 _exptl_crystal_size_min 0.01 _refine_diff_density_max 0.991 _refine_diff_density_min -0.766 _refine_diff_density_rms 0.207 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.040 _refine_ls_hydrogen_treatment undef _refine_ls_matrix_type full _refine_ls_number_parameters 46 _refine_ls_number_reflns 1137 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.040 _refine_ls_R_factor_all 0.0355 _refine_ls_R_factor_gt 0.0334 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0702P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0985 _refine_ls_wR_factor_ref 0.1000 _reflns_Friedel_coverage 0.000 _reflns_number_gt 1016 _reflns_number_total 1137 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file bm5146sup1.cif _cod_data_source_block CsI4_0p43GPa _cod_original_cell_volume 901.92(14) _cod_database_code 2022875 _shelx_shelxl_version_number 2017/1 _chemical_oxdiff_formula 'C11 H10 N O' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.961 _shelx_estimated_absorpt_t_min 0.872 _diffrn_measurement_specimen_suport 'diamond anvil cell' _reflns_odcompleteness_completeness 36.17 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 14.88 _olex2_refinement_description ; ; _shelx_res_file ; TITL csi4_0089_a.res in P2(1)/c csi4_0089.res created by SHELXL-2018/3 at 14:05:32 on 19-Jul-2021 REM Old TITL csi4_0089 in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.100, Rweak 0.002, Alpha 0.017 REM 0.436 for 33 systematic absences, Orientation as input REM Formula found by SHELXT: Cs2 I3 CELL 0.41077 10.1323 8.888988 11.045345 90 114.9566 90 ZERR 4 0.001308 0.000151 0.000376 0 0.0089 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC Cs I DISP Cs -1.803 0.7961 2042.8949 DISP I -2.2298 0.677 1764.6088 UNIT 4 16 L.S. 4 0 0 PLAN 10 SIZE 0.035 0.015 0.01 CONF list 4 MORE -1 fmap 2 53 acta SHEL 0.6 1000 REM REM REM WGHT 0.070200 FVAR 2.90030 I2 2 0.381619 0.709323 0.392699 11.00000 0.05804 0.03764 = 0.04074 -0.00185 0.02240 0.00439 CS1 1 0.776958 0.875453 0.695140 11.00000 0.06553 0.04869 = 0.04586 0.00552 0.02359 0.00659 I1 2 0.560568 0.902159 0.320202 11.00000 0.05841 0.05145 = 0.05098 0.00371 0.02802 -0.00152 I3 2 0.172465 0.511921 0.451007 11.00000 0.06364 0.03737 = 0.05944 0.00439 0.02993 -0.00135 I4 2 0.050667 0.856623 0.495632 11.00000 0.05937 0.04314 = 0.05025 -0.00236 0.02149 -0.00862 HKLF 4 REM csi4_0089_a.res in P2(1)/c REM wR2 = 0.1000, GooF = S = 1.040, Restrained GooF = 1.040 for all data REM R1 = 0.0334 for 1016 Fo > 4sig(Fo) and 0.0355 for all 1137 data REM 46 parameters refined using 0 restraints END WGHT 0.0702 0.0000 REM Highest difference peak 0.991, deepest hole -0.766, 1-sigma level 0.207 Q1 1 0.5966 0.8593 0.5976 11.00000 0.05 0.99 Q2 1 0.8397 0.9339 0.7376 11.00000 0.05 0.75 Q3 1 0.7068 0.8916 0.4177 11.00000 0.05 0.72 Q4 1 0.1478 1.0621 0.4982 11.00000 0.05 0.66 Q5 1 0.6172 1.1432 0.3184 11.00000 0.05 0.65 Q6 1 0.3306 0.5045 0.5399 11.00000 0.05 0.63 Q7 1 -0.0982 0.7789 0.4744 11.00000 0.05 0.63 Q8 1 0.4332 0.7396 0.1779 11.00000 0.05 0.63 Q9 1 0.6720 1.1193 0.3426 11.00000 0.05 0.61 Q10 1 0.1976 0.6750 0.2957 11.00000 0.05 0.57 ; _shelx_res_checksum 15905 _shelx_hkl_file ; 0 0 2 86591.2 1777.99 1 0 0 -2 81977.5 1780.53 1 0 0 -3 3.96151 12.9110 1 0 0 -4 24766.7 661.274 1 0 0 -5 6.81051 34.8600 1 0 0 6 168591. 3687.00 1 0 0 -6 170675. 3674.84 1 0 0 -7 219.502 70.1563 1 0 0 7 4.81964 50.0594 1 0 0 -8 26789.0 893.713 1 0 0 8 31449.2 927.313 1 0 0 9 61.2051 72.3904 1 0 0 -9 30.0993 68.7188 1 0 0 -10 97172.1 2404.49 1 0 0 10 92951.4 2413.67 1 0 0 11 32.3007 74.4394 1 0 0 12 202.723 106.594 1 0 0 -12 157.102 98.5989 1 0 0 13 39.2728 75.7249 1 0 0 -14 4691.37 410.108 1 0 1 -2 268402. 5442.32 1 0 1 2 267790. 5455.31 1 0 -1 2 268682. 5442.49 1 0 -1 -2 264699. 5459.59 1 0 1 -3 354705. 7206.49 1 0 -1 3 352341. 7210.77 1 0 1 3 352976. 7215.25 1 0 -1 4 83615.6 1908.49 1 0 1 4 84162.6 1924.80 1 0 1 -4 89084.7 1904.84 1 0 1 -5 551228. 11261.5 1 0 1 6 79170.9 1877.08 1 0 -1 6 79535.4 1869.28 1 0 1 7 15627.9 574.007 1 0 -1 7 16190.3 552.670 1 0 -1 -7 14377.6 554.924 1 0 -1 8 628.134 114.327 1 0 1 8 705.832 142.164 1 0 1 -8 598.936 119.230 1 0 -1 -8 579.684 113.844 1 0 1 9 6185.23 375.855 1 0 -1 -9 7178.07 408.524 1 0 -1 9 6856.49 397.978 1 0 1 -9 7037.44 394.470 1 0 1 -10 2630.64 244.535 1 0 1 10 2343.91 241.650 1 0 -1 10 3106.62 274.493 1 0 -1 11 50175.2 1487.22 1 0 1 -11 47714.6 1414.73 1 0 -1 -11 45773.1 1429.05 1 0 1 -12 6054.53 410.629 1 0 -1 -12 6043.27 436.919 1 0 -1 12 6335.06 439.278 1 0 -1 13 10.6533 82.1623 1 0 -1 -13 9.96153 106.031 1 0 1 -13 48.4976 92.3430 1 0 1 -14 1352.95 227.280 1 0 2 1 47729.1 1045.91 1 0 -2 -1 51109.5 1057.75 1 0 2 2 6253.69 211.875 1 0 -2 2 6001.32 189.803 1 0 -2 -2 6318.71 215.863 1 0 2 3 4879.02 205.401 1 0 -2 -3 5262.04 210.700 1 0 2 -3 4717.78 187.266 1 0 -2 3 4720.12 192.676 1 0 2 4 93708.1 2160.15 1 0 -2 4 97618.0 2150.16 1 0 -2 -4 97548.2 2162.33 1 0 -2 -5 7598.08 322.723 1 0 2 -5 7496.61 315.137 1 0 2 5 7976.21 331.732 1 0 -2 -6 8892.05 382.912 1 0 2 -6 8629.08 360.114 1 0 -2 6 7233.88 330.275 1 0 2 6 7596.90 353.184 1 0 -2 7 24953.9 771.606 1 0 2 -7 23812.5 754.862 1 0 2 7 23813.1 763.499 1 0 -2 -7 22824.2 767.183 1 0 -2 -8 97965.4 2408.84 1 0 2 -8 99359.0 2388.23 1 0 -2 8 106419. 2402.08 1 0 2 8 99778.3 2405.87 1 0 2 -9 12506.3 537.498 1 0 -2 9 11630.0 522.565 1 0 -2 -9 12034.6 542.733 1 0 2 9 11984.1 564.921 1 0 -2 10 41947.4 1275.29 1 0 2 10 40359.7 1270.27 1 0 -2 -10 42943.1 1298.99 1 0 2 -10 43509.1 1273.03 1 0 -2 -11 10584.2 547.590 1 0 2 11 10034.4 556.033 1 0 -2 11 11354.5 581.676 1 0 2 -12 979.520 174.993 1 0 -2 12 1194.85 196.749 1 0 -2 -12 800.258 168.837 1 0 2 12 460.995 135.499 1 0 2 13 1956.89 277.920 1 0 -2 13 1973.73 258.229 1 0 2 -13 2023.86 246.722 1 0 -3 -1 585237. 11781.0 1 0 3 1 584971. 11791.4 1 0 3 2 14474.0 404.269 1 0 -3 -2 15151.7 412.033 1 0 3 3 111576. 2382.65 1 0 -3 -3 113487. 2384.14 1 0 -3 3 107984. 2333.84 1 0 3 4 7203.06 308.093 1 0 -3 4 7299.17 278.749 1 0 -3 -4 6884.13 296.371 1 0 -3 -5 513326. 10686.2 1 0 3 5 526172. 10670.0 1 0 3 6 23352.8 748.005 1 0 3 -6 24666.6 719.503 1 0 -3 -6 24474.5 749.660 1 0 3 -7 888.163 122.323 1 0 3 7 696.605 113.384 1 0 -3 7 657.704 105.698 1 0 -3 -7 904.385 136.124 1 0 -3 -8 63730.0 1662.85 1 0 -3 8 67668.8 1674.12 1 0 3 -8 61730.5 1626.95 1 0 3 8 64827.5 1677.13 1 0 -3 9 13759.2 571.608 1 0 3 -9 12552.9 537.430 1 0 3 9 11925.3 552.476 1 0 -3 -9 12619.6 572.243 1 0 -3 -10 8710.13 482.136 1 0 3 10 8075.72 464.088 1 0 -3 10 8231.88 445.692 1 0 3 11 1360.93 208.656 1 0 -3 -11 1497.72 214.704 1 0 -3 11 1546.72 213.188 1 0 -3 12 1497.29 238.760 1 0 -3 -12 1451.30 219.096 1 0 3 12 1344.37 216.274 1 0 3 13 60.4234 86.4284 1 0 -4 -1 132607. 2747.38 1 0 -4 -2 193627. 4074.93 1 0 4 2 199348. 4063.01 1 0 4 3 20701.3 581.145 1 0 -4 -3 20908.9 582.593 1 0 -4 -4 112218. 2458.99 1 0 4 4 106656. 2452.15 1 0 -4 4 113612. 2405.23 1 0 -4 -5 55219.5 1342.92 1 0 4 6 315234. 6527.62 1 0 -4 6 311443. 6464.97 1 0 -4 -6 302226. 6524.63 1 0 -4 -7 11663.9 493.667 1 0 -4 7 11225.6 444.297 1 0 4 8 6528.89 373.538 1 0 -4 -8 6733.83 374.277 1 0 -4 8 6683.57 357.207 1 0 -4 -9 9386.96 484.642 1 0 4 9 9383.51 484.884 1 0 -4 -10 49688.8 1431.62 1 0 4 10 46711.6 1421.68 1 0 -4 11 2181.86 236.843 1 0 4 11 1790.86 225.792 1 0 -4 -11 2416.44 257.833 1 0 4 12 4900.05 394.808 1 0 -4 12 5111.36 392.826 1 0 -4 -12 5358.50 414.712 1 0 -4 -13 3168.93 330.730 1 0 -4 13 2817.04 300.868 1 0 4 13 2504.68 295.406 1 0 -5 -1 635629. 12817.2 1 0 -5 -2 83073.0 1813.91 1 0 -5 -3 103343. 2271.14 1 0 -5 -4 9354.50 362.280 1 0 -5 -5 20272.2 641.941 1 0 -5 5 20735.7 598.778 1 0 -5 6 8753.84 370.693 1 0 -5 -6 9863.90 423.259 1 0 -5 7 18776.7 641.386 1 0 -5 -7 17734.8 680.338 1 0 5 8 1588.49 186.859 1 0 -5 8 1480.84 160.467 1 0 -5 -8 1484.83 176.496 1 0 -5 9 91.8107 69.6571 1 0 -5 -9 70.6567 64.0567 1 0 5 10 936.050 167.482 1 0 -5 10 779.562 136.053 1 0 -5 -10 804.256 158.147 1 0 5 11 5326.01 405.776 1 0 -5 -11 6074.21 424.798 1 0 -5 11 5593.52 376.374 1 0 5 12 1267.29 219.978 1 0 -5 -12 1156.68 206.388 1 0 -5 -13 8243.10 541.648 1 0 -6 -1 5710.15 203.607 1 0 -6 -2 223413. 4635.96 1 0 -6 -3 152593. 3262.32 1 0 6 3 153415. 3251.36 1 0 6 5 1347.21 139.121 1 0 -6 5 1402.74 115.966 1 0 -6 6 1678.20 137.177 1 0 6 6 1769.61 172.383 1 0 -6 7 13145.1 490.678 1 0 6 7 14213.5 560.045 1 0 -6 8 3493.82 236.434 1 0 6 8 3811.17 294.153 1 0 6 9 6482.44 409.441 1 0 -6 9 5377.58 317.048 1 0 6 10 659.014 151.432 1 0 -6 10 573.746 113.819 1 0 6 11 1043.88 189.453 1 0 6 12 85.5100 89.9600 1 0 -7 0 1.37762 16.8788 1 0 -7 -1 39876.2 919.199 1 0 -7 -2 3226.20 163.879 1 0 -7 -3 1992.95 140.154 1 0 7 4 10490.5 389.404 1 0 -7 -5 2624.85 196.351 1 0 7 5 2831.14 195.439 1 0 -7 6 4107.40 218.320 1 0 -7 -6 4427.11 280.251 1 0 7 7 11732.4 506.494 1 0 -7 -7 12334.2 519.253 1 0 -7 7 11260.9 415.817 1 0 -7 8 2383.19 186.329 1 0 -7 -8 2672.89 234.386 1 0 7 8 2432.21 225.737 1 0 -7 -9 51001.7 1459.91 1 0 7 9 52064.3 1496.59 1 0 -7 -10 2036.97 233.717 1 0 7 10 1910.14 237.475 1 0 7 11 11920.1 631.814 1 0 -7 -11 12125.7 619.211 1 0 -7 -12 67.3752 95.8413 1 0 -8 0 121754. 2541.83 1 0 -8 -1 2166.40 118.821 1 0 -8 -2 2483.89 148.839 1 0 -8 -3 7430.34 302.668 1 0 -8 -4 37508.4 992.359 1 0 -8 -5 260.245 71.7873 1 0 8 5 291.450 74.4191 1 0 8 6 14823.5 567.107 1 0 -8 -6 16094.4 590.018 1 0 8 7 40989.4 1196.54 1 0 -8 -7 44116.4 1215.58 1 0 8 8 12698.4 555.570 1 0 -8 -8 12555.6 549.019 1 0 -8 -9 105.882 78.8733 1 0 8 9 237.274 92.2180 1 0 -8 -10 253.484 95.9838 1 0 8 10 207.484 102.387 1 0 8 11 2984.20 296.692 1 0 -8 -11 2601.83 269.155 1 0 8 12 297.249 121.528 1 0 -8 -12 269.652 121.417 1 0 -9 -1 25125.4 630.902 1 0 -9 -2 20220.0 563.180 1 0 -9 -3 30268.6 817.848 1 0 -9 -4 25718.7 725.132 1 0 -9 -5 29817.7 868.085 1 0 9 6 2183.55 191.586 1 0 -9 -6 2604.78 212.465 1 0 -9 -7 770.672 127.516 1 0 9 7 914.585 137.432 1 0 -9 -8 4530.16 311.160 1 0 -9 -9 1267.25 181.827 1 0 9 9 1055.88 166.447 1 0 -9 -10 1452.82 201.604 1 0 9 10 1572.94 215.053 1 0 9 11 848.083 169.701 1 0 -9 -11 887.033 177.686 1 0 -9 -12 1614.51 224.697 1 0 -10 0 28494.7 670.394 1 0 -10 1 22609.9 523.102 1 0 -10 -1 22319.9 589.006 1 0 10 8 4836.74 332.288 1 0 10 9 1014.12 163.506 1 0 10 10 39.5389 86.2525 1 0 10 11 602.901 148.962 1 0 -11 0 13.5197 21.1021 1 0 -11 -1 8471.67 278.128 1 0 -11 -2 10466.4 362.373 1 0 -11 -3 11462.7 418.038 1 0 -11 -4 10443.0 426.636 1 0 -11 -5 5327.29 300.865 1 0 -11 -6 515.531 110.436 1 0 -11 -7 38.6304 65.9147 1 0 -11 -8 28.1128 69.9787 1 0 -11 -9 59.5860 73.1013 1 0 11 10 96.1607 96.3239 1 0 -11 -10 60.6006 89.8280 1 0 11 11 16.4095 75.6317 1 0 -12 -3 1545.67 136.948 1 0 -12 -4 1585.00 155.177 1 0 -12 -5 4767.33 297.637 1 0 -12 -6 54.3056 63.4266 1 0 -12 -7 133.218 79.2018 1 0 -12 -8 739.754 150.150 1 0 -12 -9 474.355 125.838 1 0 -12 -10 2815.45 296.686 1 0 -12 -11 72.4360 85.3293 1 1 0 -14 30562.6 1146.40 1 -1 0 14 28270.1 1112.18 1 -1 0 13 9.75791 59.2113 1 -1 0 12 7149.46 473.953 1 1 0 -12 6783.73 450.595 1 -1 0 11 32.4557 79.6267 1 -1 0 10 11742.7 568.284 1 1 0 -10 14201.8 601.607 1 1 0 -9 6.08274 61.4241 1 -1 0 9 42.3318 63.5606 1 1 0 -8 72800.1 1827.86 1 1 0 -7 13.9449 33.1910 1 1 0 -6 20641.8 644.456 1 -1 0 6 21565.8 647.863 1 -1 0 5 21.9518 31.2247 1 1 0 -5 9.81452 21.3260 1 -1 0 4 387941. 7915.36 1 1 0 -4 385951. 7926.46 1 1 0 -3 5.66740 13.8589 1 1 0 -2 1149.72 69.4514 1 -1 0 -3 10.6148 19.8939 1 -1 0 -4 881943. 17892.9 1 -1 0 -5 18.8939 31.7999 1 -1 0 -6 170665. 3714.21 1 -1 0 -7 4.91441 50.3130 1 1 0 7 56.4103 45.6730 1 1 0 8 736.204 121.907 1 -1 0 -8 661.503 118.632 1 1 0 9 6.24059 37.8681 1 1 0 10 245.350 93.8479 1 -1 0 -10 408.281 132.125 1 -1 0 -11 24.7484 65.1213 1 -1 0 -12 6861.60 438.103 1 1 0 12 6798.93 448.955 1 1 0 13 9.97105 73.1464 1 1 1 -14 19.9609 87.2815 1 -1 1 14 42.7971 91.8181 1 -1 -1 14 42.7190 82.3687 1 1 -1 -13 2013.99 261.648 1 -1 -1 13 2103.79 271.996 1 -1 1 13 2092.14 270.192 1 1 1 -13 2283.63 270.526 1 -1 -1 12 4243.86 351.645 1 -1 1 12 4376.72 358.684 1 1 -1 -12 4742.14 371.750 1 1 1 -12 4770.71 364.311 1 1 -1 -11 1274.63 187.662 1 1 1 -11 1278.71 185.786 1 -1 -1 11 1444.39 195.758 1 1 1 -10 2901.59 258.761 1 1 -1 -10 2938.57 260.561 1 -1 -1 10 2738.21 251.771 1 1 1 -9 159698. 3569.03 1 -1 1 9 154215. 3610.31 1 1 -1 -9 156408. 3608.81 1 -1 -1 9 157439. 3562.06 1 -1 -1 8 195507. 4436.10 1 -1 1 8 196805. 4461.82 1 1 1 -8 202364. 4415.10 1 1 -1 -7 56537.1 1452.97 1 -1 -1 7 57625.3 1453.68 1 1 1 -7 58443.0 1451.73 1 -1 1 7 57097.4 1474.80 1 1 -1 -6 11537.7 441.143 1 -1 1 6 11714.6 439.083 1 -1 -1 6 12404.9 445.963 1 1 1 -5 42932.6 1048.70 1 -1 -1 5 41494.7 1059.82 1 1 -1 -5 43994.6 1104.25 1 -1 1 5 45356.7 1087.26 1 -1 1 4 39.0642 27.3877 1 -1 -1 4 41.5180 24.8622 1 1 1 -4 14.0118 18.0193 1 -1 -1 2 18.4805 10.0555 1 1 1 -2 17.4324 9.74276 1 1 1 2 853996. 17084.1 1 -1 -1 -2 843297. 17132.5 1 -1 -1 -3 13463.3 412.141 1 1 1 3 12960.4 394.673 1 1 1 4 96448.7 2122.49 1 -1 -1 -4 94122.7 2129.60 1 1 -1 5 44595.1 1143.31 1 1 1 5 49333.0 1179.27 1 1 1 6 71624.1 1739.12 1 -1 1 -6 73357.3 1733.52 1 1 -1 6 74146.5 1733.14 1 -1 1 -7 13457.1 528.411 1 1 1 7 14764.4 538.238 1 1 -1 8 18990.9 692.719 1 -1 -1 -8 21419.3 737.715 1 1 1 8 19975.7 713.980 1 -1 1 -8 21925.3 737.398 1 -1 1 -9 13783.4 570.548 1 -1 -1 -9 13273.6 577.587 1 1 1 9 13159.8 569.461 1 1 -1 9 13542.8 575.925 1 -1 -1 -10 543.109 126.930 1 1 -1 10 867.658 143.960 1 1 1 10 797.896 138.463 1 -1 1 -10 626.863 129.329 1 -1 -1 -11 7386.63 455.862 1 1 1 11 6206.42 411.178 1 1 -1 11 6393.89 412.615 1 -1 -1 -12 7456.12 489.177 1 -1 -1 -13 679.352 162.259 1 -1 -2 14 183.262 119.127 1 1 -2 -14 386.003 137.788 1 1 2 -13 11818.2 609.529 1 -1 2 13 10626.0 610.104 1 -1 -2 13 12177.0 642.749 1 -1 2 12 401.739 124.352 1 -1 -2 12 575.473 139.226 1 1 2 -12 596.774 135.661 1 1 2 -11 346.860 113.386 1 -1 2 11 366.566 114.108 1 -1 -2 11 375.494 111.142 1 -1 -2 10 309.553 101.767 1 -1 2 10 307.239 105.690 1 1 2 -10 265.892 90.9232 1 1 -2 -10 334.103 107.848 1 -1 2 9 24989.6 873.054 1 1 -2 -9 25757.6 875.228 1 -1 -2 9 26513.2 857.776 1 1 2 -9 28072.3 886.942 1 1 2 -8 17822.0 625.339 1 -1 -2 8 18013.6 615.595 1 1 -2 -8 17827.1 647.171 1 1 2 -7 1748.39 164.948 1 1 -2 -7 1986.67 188.370 1 -1 2 7 1937.69 173.789 1 -1 -2 7 2246.73 176.532 1 1 2 -6 415101. 8394.53 1 1 -2 -6 407390. 8450.85 1 -1 -2 6 404330. 8394.94 1 -1 2 6 401740. 8434.58 1 1 -2 -5 3739.09 224.014 1 -1 -2 5 3421.31 185.042 1 1 2 -5 3708.43 197.264 1 1 -2 -4 224443. 4667.73 1 1 2 -4 224471. 4611.99 1 -1 2 4 216552. 4666.70 1 -1 -2 4 225072. 4609.15 1 -1 2 3 987306. 11193.6 1 1 -2 -3 999999. 11194.4 1 1 2 -2 92402.7 1900.46 1 -1 -2 2 90963.0 1903.70 1 1 -2 -2 93351.2 1963.00 1 1 2 1 4385.26 156.619 1 -1 -2 -1 5148.18 166.827 1 -1 -2 -2 16011.2 467.293 1 1 2 2 17958.2 468.017 1 1 2 3 127567. 2741.44 1 -1 -2 -3 128633. 2746.87 1 1 2 4 264.439 56.1458 1 -1 -2 -4 257.169 58.7274 1 1 2 5 119462. 2580.18 1 -1 -2 -5 109873. 2551.67 1 -1 -2 -6 2374.47 188.663 1 1 2 6 2059.06 178.119 1 1 -2 7 204292. 4418.23 1 -1 -2 -7 196045. 4457.70 1 1 2 7 210396. 4452.60 1 1 -2 8 27058.0 857.431 1 1 2 8 26150.2 849.505 1 -1 -2 -8 27015.2 889.211 1 1 2 9 5513.03 353.471 1 1 -2 9 5891.95 346.356 1 -1 -2 -9 6457.28 385.699 1 -1 -2 -10 129.251 96.6368 1 1 2 10 121.463 79.8255 1 1 2 11 10621.6 563.962 1 -1 -2 -11 9851.55 538.788 1 -1 -2 -12 13154.6 663.620 1 1 2 12 10771.0 569.711 1 1 2 13 4735.54 389.110 1 -1 -2 -13 6174.74 461.412 1 1 3 -14 2931.58 334.173 1 1 -3 -13 2466.18 290.686 1 -1 3 13 2683.59 320.132 1 1 3 -13 2752.08 285.357 1 -1 -3 12 680.934 143.286 1 -1 3 12 740.456 170.790 1 1 3 -12 436.848 123.695 1 1 -3 -12 539.929 144.936 1 -1 -3 11 2612.49 256.626 1 1 -3 -11 2538.44 261.596 1 -1 3 11 2721.39 280.031 1 1 3 -11 2470.74 250.520 1 -1 3 10 231.318 102.228 1 -1 -3 10 128.009 70.7066 1 -1 -3 9 36491.7 1088.53 1 1 -3 -9 39811.1 1187.54 1 -1 3 9 39529.5 1174.78 1 1 -3 -8 379.045 96.5187 1 1 3 -8 357.473 92.9396 1 -1 3 8 481.290 108.897 1 -1 -3 8 477.141 99.7931 1 1 -3 -7 62661.0 1624.12 1 -1 3 7 64658.2 1621.15 1 -1 3 6 75483.6 1785.85 1 1 -3 -6 73431.6 1784.60 1 1 3 -6 72852.4 1716.50 1 -1 -3 5 41787.6 1037.43 1 1 3 -5 41054.5 1032.66 1 1 -3 -5 43994.5 1108.28 1 1 -3 -4 400772. 8658.41 1 -1 3 4 423686. 8637.00 1 -1 -3 4 426135. 8575.82 1 1 3 -4 428407. 8574.87 1 1 3 -3 164833. 3497.19 1 1 -3 -3 166767. 3590.92 1 -1 -3 3 172942. 3491.60 1 -1 3 3 174436. 3560.46 1 -1 -3 -1 673413. 13555.7 1 1 3 2 191407. 4029.44 1 -1 -3 -2 197123. 4026.80 1 -1 -3 -3 108190. 2365.30 1 1 3 3 111994. 2404.14 1 -1 -3 -4 55863.9 1296.88 1 1 3 4 52250.6 1311.96 1 -1 -3 -5 85791.2 1955.04 1 1 3 5 81572.0 1943.09 1 -1 -3 -6 17181.2 596.150 1 1 3 6 16586.9 602.718 1 1 3 7 161879. 3629.63 1 -1 -3 -7 162481. 3596.78 1 1 3 8 31886.9 997.095 1 -1 -3 -8 30065.1 968.357 1 -1 -3 -9 12340.4 574.699 1 1 3 9 12020.3 574.421 1 -1 -3 -10 61393.3 1648.42 1 1 3 10 52461.9 1555.21 1 1 3 11 1585.24 210.280 1 -1 -3 -11 1419.66 211.994 1 -1 -3 -12 511.980 142.976 1 1 3 12 394.471 126.374 1 -1 -3 -13 977.060 192.616 1 -1 -4 14 1933.99 257.564 1 -1 -4 13 4964.38 376.257 1 1 -4 -13 5294.99 415.409 1 1 4 -13 4576.87 358.018 1 -1 4 13 5554.89 453.832 1 -1 -4 12 265.808 101.216 1 1 4 -12 291.264 111.771 1 1 -4 -12 243.356 104.637 1 -1 4 12 352.452 138.833 1 -1 4 11 1022.39 180.599 1 -1 -4 11 1102.31 172.157 1 1 -4 -11 1138.50 180.338 1 1 4 -11 1171.97 188.808 1 1 -4 -10 31355.2 1030.50 1 1 4 -10 31874.9 981.895 1 -1 4 10 29376.3 1027.48 1 -1 -4 10 28471.3 939.869 1 1 -4 -9 24184.4 852.641 1 -1 4 9 22172.9 828.010 1 1 4 -9 22677.2 757.113 1 -1 4 8 168027. 3786.27 1 1 -4 -8 167116. 3780.92 1 1 4 -8 167423. 3683.50 1 -1 4 7 36.9065 57.5378 1 1 4 -7 109.745 56.0271 1 1 -4 -7 123.673 70.1235 1 -1 -4 7 103.028 51.0038 1 -1 -4 6 1125.47 112.446 1 1 -4 -6 1131.40 133.927 1 -1 4 6 1274.78 143.073 1 1 4 -6 1170.13 115.596 1 1 4 -5 29036.9 764.150 1 -1 4 5 30090.8 829.870 1 1 -4 -5 29326.7 837.486 1 -1 -4 5 31047.1 776.918 1 1 -4 -4 404252. 8275.47 1 -1 4 4 399759. 8266.47 1 -1 -4 4 401927. 8175.86 1 -1 -4 3 97443.8 2050.66 1 1 -4 -3 99457.1 2151.09 1 -1 -4 -1 110153. 2282.38 1 1 4 1 108815. 2286.75 1 -1 -4 -2 25152.0 650.418 1 1 4 2 27324.7 669.448 1 -1 -4 -3 3412.79 179.470 1 1 4 3 3495.95 185.862 1 -1 -4 -4 87432.2 1975.38 1 -1 -4 -5 85744.0 2049.66 1 1 4 5 93225.3 2088.64 1 -1 -4 -6 11852.8 470.854 1 1 4 6 12611.8 507.614 1 -1 -4 -7 150.048 70.0540 1 -1 -4 -8 28611.4 940.240 1 1 4 8 27699.2 922.665 1 1 4 9 1472.40 197.840 1 -1 -4 -9 1704.65 208.743 1 1 4 10 10389.7 541.656 1 -1 -4 -10 11065.5 562.577 1 1 4 11 3350.01 309.884 1 -1 -4 -11 3358.20 316.313 1 -1 -4 -12 3108.28 317.971 1 1 4 12 2780.61 295.226 1 -1 -5 14 2008.07 248.162 1 -1 -5 13 2849.32 276.738 1 -1 5 13 3207.16 338.858 1 1 -5 -13 3001.02 321.547 1 1 -5 -12 5799.04 417.804 1 -1 5 12 5876.34 440.000 1 -1 -5 12 5799.64 381.697 1 1 -5 -11 33689.5 1161.46 1 -1 5 11 34359.0 1174.45 1 -1 -5 11 34589.0 1098.28 1 -1 -5 10 28.8636 55.8112 1 1 -5 -10 7.35020 59.3261 1 1 -5 -9 174.989 89.3747 1 -1 5 9 109.490 91.9692 1 -1 -5 9 129.113 69.0422 1 1 -5 -8 20879.4 742.920 1 -1 -5 8 20069.7 664.843 1 -1 5 8 20402.4 743.885 1 1 -5 -7 1082.64 139.469 1 -1 5 7 965.019 131.332 1 -1 -5 7 947.998 114.112 1 -1 5 6 2775.29 213.079 1 -1 -5 6 2498.43 161.259 1 1 -5 -6 2426.66 203.151 1 1 -5 -5 10432.0 412.341 1 -1 -5 5 10385.4 340.071 1 -1 5 5 10189.1 407.727 1 1 -5 -4 6089.34 278.027 1 -1 5 4 6109.98 276.295 1 -1 -5 4 5767.34 211.428 1 1 -5 -3 23771.5 660.607 1 -1 -5 -1 48911.4 1081.52 1 1 5 1 49719.2 1087.80 1 1 5 2 9387.58 311.712 1 -1 -5 -2 8845.92 295.984 1 1 5 3 384177. 7896.06 1 -1 -5 -3 384135. 7872.56 1 1 5 4 1274.18 124.910 1 -1 -5 -4 1187.64 118.017 1 -1 -5 -5 51628.2 1294.56 1 -1 -5 -6 4555.81 275.248 1 -1 -5 -8 15381.1 626.444 1 -1 -5 -9 5485.80 363.826 1 -1 -5 -10 2191.78 245.143 1 1 5 11 9.85980 82.9685 1 1 5 12 357.188 123.930 1 -1 -5 -12 339.752 135.884 1 -1 -6 14 25.3977 74.0353 1 -1 6 13 125.367 115.306 1 -1 -6 13 36.8258 58.1609 1 1 -6 -13 146.134 103.940 1 -1 -6 12 841.502 141.402 1 1 -6 -12 862.582 167.915 1 -1 6 12 906.754 176.425 1 1 -6 -11 6299.76 433.588 1 -1 -6 11 6360.85 387.424 1 -1 6 11 5711.27 403.217 1 1 -6 -10 3324.79 282.406 1 -1 -6 10 3022.75 234.154 1 -1 6 10 3028.39 276.555 1 -1 -6 9 28098.0 873.273 1 1 -6 -9 31382.5 1019.69 1 1 -6 -8 14664.4 607.200 1 -1 6 8 14734.9 612.131 1 -1 -6 8 16075.8 580.919 1 1 -6 -7 37141.5 1066.28 1 -1 6 7 37901.2 1085.01 1 -1 -6 7 34747.2 953.593 1 -1 -6 6 1401.80 119.315 1 -1 6 6 1316.16 142.103 1 -1 6 5 23585.7 686.178 1 -1 -6 5 21459.8 596.042 1 -1 -6 4 4.85171 19.2459 1 -1 -6 3 47404.9 1018.12 1 -1 -6 0 206431. 4182.41 1 -1 -6 -1 169051. 3481.02 1 -1 -6 -2 74666.8 1670.22 1 1 6 2 78106.4 1681.13 1 -1 -6 -3 90316.3 2053.11 1 1 6 3 94102.0 2050.47 1 1 6 4 38164.2 1014.58 1 1 6 5 146649. 3240.10 1 -1 -6 -5 147902. 3237.27 1 -1 -6 -6 79533.1 1904.10 1 1 6 6 77454.0 1905.01 1 -1 -6 -7 427.202 98.8421 1 1 6 7 407.786 99.3686 1 1 6 8 1570.22 191.759 1 1 6 9 209.650 94.3914 1 1 6 10 8.33713 79.3718 1 1 6 11 92.8014 85.5640 1 1 6 12 817.667 180.078 1 1 -7 -13 41.6127 74.2854 1 -1 7 12 9.68302 90.7390 1 -1 -7 12 68.5395 62.9263 1 -1 7 11 275.782 111.649 1 -1 -7 11 231.955 80.3466 1 1 -7 -11 126.251 94.0620 1 -1 -7 10 5.07613 48.3268 1 1 -7 -10 14.7560 70.2409 1 -1 7 10 34.8052 89.0760 1 1 -7 -9 8079.29 452.382 1 -1 7 9 7266.93 440.894 1 -1 -7 9 7788.19 363.355 1 1 -7 -8 3318.34 265.835 1 -1 -7 8 3381.65 218.815 1 -1 7 8 3170.83 262.239 1 1 -7 -7 39843.7 1121.49 1 -1 -7 7 38413.6 996.508 1 -1 7 7 38114.4 1106.27 1 -1 7 6 25575.7 800.132 1 1 -7 -6 26018.2 817.601 1 -1 -7 6 28113.7 728.472 1 -1 -7 5 249603. 5123.01 1 1 -7 -5 246039. 5259.58 1 -1 -7 4 8722.11 269.217 1 -1 -7 3 28943.6 650.746 1 1 -7 -3 32708.5 819.734 1 -1 -7 0 109364. 2244.19 1 -1 -7 -1 40820.5 927.192 1 -1 -7 -2 28008.4 691.840 1 1 7 2 26155.8 676.008 1 1 7 3 2943.74 174.428 1 -1 -7 -3 2758.04 170.236 1 -1 -7 -4 21935.7 659.885 1 1 7 4 21388.6 646.036 1 -1 -7 -5 15075.0 529.376 1 1 7 5 15064.6 536.292 1 1 7 6 2462.50 211.031 1 -1 -7 -6 2441.24 202.676 1 -1 -7 -7 3264.06 255.301 1 1 7 7 3208.36 249.485 1 1 7 8 15704.7 654.692 1 -1 -7 -8 15240.7 632.663 1 1 7 9 4428.38 339.862 1 -1 -7 -9 4337.58 328.110 1 1 7 10 5648.59 407.629 1 -1 -7 -10 6039.07 409.760 1 -1 -7 -11 12204.9 626.313 1 1 7 11 12270.1 653.657 1 1 7 12 965.729 189.612 1 -1 -7 -12 978.941 195.349 1 -1 -8 12 17.4111 57.7861 1 -1 8 12 29.3536 90.1943 1 -1 8 11 267.731 111.804 1 1 -8 -11 313.643 119.508 1 -1 -8 11 306.406 86.8621 1 1 -8 -10 2347.82 246.996 1 -1 8 10 2722.28 276.759 1 1 -8 -9 3076.71 273.525 1 -1 8 9 3444.69 286.570 1 -1 -8 9 2845.84 204.555 1 1 -8 -8 42.8715 64.3747 1 -1 8 7 26397.3 860.427 1 -1 -8 7 27268.7 745.175 1 1 -8 -7 25891.1 847.152 1 1 -8 -6 30768.7 925.253 1 -1 -8 6 31840.4 813.915 1 -1 -8 5 6956.52 252.167 1 1 -8 -5 7443.76 358.502 1 1 -8 -4 8223.10 347.508 1 -1 -8 4 8165.51 246.227 1 1 -8 -3 65340.3 1536.36 1 1 -8 -2 2206.41 156.538 1 -1 -8 0 37367.1 799.657 1 -1 -8 -1 618.097 57.4878 1 -1 -8 -2 58279.6 1330.57 1 1 8 3 2137.33 140.591 1 -1 -8 -3 2713.16 167.588 1 1 8 4 84.9632 47.8964 1 -1 -8 -4 121.860 55.9744 1 -1 -8 -5 976.957 123.537 1 1 8 5 1079.43 131.056 1 1 8 6 30494.2 896.827 1 -1 -8 -6 30605.1 908.810 1 -1 -8 -7 7077.37 380.323 1 1 8 7 6608.01 379.863 1 -1 -8 -8 3309.13 262.455 1 1 8 8 2854.57 251.936 1 1 8 9 6872.44 412.572 1 -1 -8 -9 6590.97 411.572 1 -1 -8 -10 82.9378 88.2974 1 1 8 10 98.5431 85.2136 1 1 8 11 3274.20 315.099 1 -1 -8 -11 3318.35 314.013 1 -1 -8 -12 28.9534 70.8016 1 1 -9 -12 1121.71 197.339 1 -1 9 12 1075.74 195.598 1 -1 -9 11 197.684 70.9939 1 -1 9 11 212.080 97.6173 1 1 -9 -11 270.096 107.334 1 -1 -9 10 2512.18 198.451 1 1 -9 -10 3034.39 282.917 1 -1 9 10 2733.12 267.001 1 1 -9 -9 8034.04 442.412 1 -1 -9 9 7528.41 347.958 1 -1 9 9 8317.26 463.592 1 1 -9 -8 320.243 92.2981 1 -1 9 8 344.835 100.640 1 -1 -9 8 301.462 69.1835 1 -1 -9 7 389.625 70.7678 1 1 -9 -7 372.191 96.2014 1 -1 -9 6 1966.90 132.314 1 1 -9 -6 1816.95 177.010 1 1 -9 -5 3710.77 242.583 1 1 -9 -4 13372.8 476.163 1 1 -9 -3 19072.9 596.581 1 1 -9 -2 74390.5 1706.19 1 -1 -9 -1 2470.60 117.828 1 -1 -9 -2 64.7752 29.4503 1 -1 -9 -3 31568.4 828.138 1 -1 -9 -4 3999.06 224.024 1 1 9 5 19451.3 637.078 1 -1 -9 -5 21392.3 683.607 1 1 9 6 121.916 62.9032 1 -1 -9 -6 202.102 76.5410 1 1 9 7 295.969 94.3385 1 -1 -9 -7 221.995 84.7637 1 1 9 9 360.570 109.280 1 -1 -9 -9 645.747 141.961 1 -1 -9 -10 2347.70 254.802 1 -1 -9 -11 26.8224 70.5786 1 -1 10 11 92.8635 92.4783 1 1 -10 -10 7698.84 455.894 1 -1 10 10 8085.28 479.397 1 -1 -10 9 39.1916 47.5013 1 1 -10 -9 35.6148 73.9009 1 1 -10 -8 317.976 98.1268 1 -1 -10 8 289.747 69.9778 1 1 -10 -7 177.039 78.7532 1 -1 -10 7 180.200 58.4644 1 1 -10 -6 6030.48 332.071 1 -1 -10 6 6088.07 246.805 1 -1 -10 5 5112.16 190.286 1 1 -10 -5 5287.98 288.176 1 1 -10 -4 11689.8 475.383 1 -1 -10 -2 1830.51 114.093 1 -1 -10 -3 554.921 74.7230 1 -1 -10 -4 8265.63 340.666 1 -1 -10 -5 4.36143 48.1324 1 -1 -10 -6 4701.85 296.008 1 1 10 6 3485.37 237.344 1 1 10 7 6186.11 354.030 1 -1 -10 -7 6838.23 385.245 1 1 10 8 3247.55 261.068 1 -1 -10 -8 4236.28 318.770 1 1 10 9 7.12382 65.6671 1 -1 -10 -10 1484.33 213.288 1 1 10 10 1317.33 185.188 1 -1 -10 -11 189.551 104.213 1 1 10 11 192.792 97.9032 1 1 -11 -11 766.661 162.086 1 1 -11 -10 313.975 110.702 1 1 -11 -9 996.122 166.601 1 1 -11 -8 2996.00 261.781 1 1 -11 -7 2060.42 209.517 1 1 -11 -6 598.787 112.472 1 1 -11 -5 1181.35 141.203 1 1 -11 -4 265.672 72.9905 1 1 -11 -3 39.2722 46.2721 1 1 -11 -2 612.306 86.1372 1 -1 -11 -3 194.114 49.7832 1 -1 -11 -4 4467.80 243.737 1 -1 -11 -5 6527.91 336.117 1 -1 -11 -6 7788.98 399.700 1 1 11 7 6115.46 350.675 1 -1 -11 -7 7040.34 398.474 1 1 11 8 115.465 74.5117 1 -1 -11 -8 185.355 94.2484 1 -1 -11 -9 138.380 91.9399 1 1 11 9 139.894 82.4324 1 1 11 10 212.689 94.7830 1 -1 -11 -10 166.190 99.9148 1 1 11 11 116.859 90.9383 1 -1 -11 -11 355.169 127.277 1 1 -12 -10 61.6533 90.1724 1 1 -12 -9 76.6548 78.4868 1 1 -12 -8 308.709 106.953 1 1 -12 -7 577.091 123.518 1 1 -12 -6 4487.40 305.181 1 1 -12 -5 1209.32 146.872 1 1 -12 -4 9606.39 411.916 1 1 -12 -3 2482.04 182.601 1 -1 -12 -6 1028.47 142.592 1 -1 -12 -7 1431.12 182.196 1 -1 -12 -8 1654.44 211.421 1 -1 -12 -9 87.6786 88.5530 1 1 12 10 35.2625 70.2230 1 -1 -12 -10 49.3995 96.9572 1 2 0 -14 1920.92 255.782 1 -2 0 14 1778.59 254.580 1 2 0 -13 9.01862 85.8598 1 2 0 -12 44317.0 1369.24 1 -2 0 12 44926.0 1392.58 1 -2 0 11 15.2628 77.0613 1 2 0 -11 22.7589 55.6535 1 2 0 -10 49449.1 1412.29 1 -2 0 10 48280.2 1392.78 1 2 0 -8 322.246 84.6133 1 -2 0 8 362.337 90.3792 1 2 0 -7 18.3506 39.3698 1 -2 0 7 9.24036 45.3400 1 -2 0 6 169435. 3655.23 1 -2 0 5 18.9624 30.5576 1 2 0 -5 25.1461 31.2991 1 -2 0 4 125641. 2691.84 1 2 0 -4 126212. 2714.24 1 2 1 -15 160.345 116.634 1 2 1 -14 1166.25 201.603 1 2 -1 -14 1024.13 212.292 1 -2 -1 14 1208.26 209.278 1 -2 1 14 1143.91 211.420 1 2 1 -13 1315.31 198.339 1 2 -1 -13 1042.10 190.783 1 -2 1 13 1608.32 230.302 1 -2 -1 13 1371.92 213.319 1 2 1 -12 38150.1 1192.89 1 -2 -1 12 35380.4 1178.44 1 -2 1 12 34082.7 1190.18 1 2 -1 -12 38660.8 1235.16 1 2 -1 -11 3533.85 297.717 1 -2 -1 11 3205.38 278.509 1 -2 1 11 3260.64 290.063 1 2 1 -11 3432.35 287.126 1 2 1 -10 26056.9 861.486 1 2 -1 -10 24331.4 844.375 1 -2 -1 10 23049.2 819.454 1 2 1 -9 4273.03 290.449 1 -2 -1 9 3629.51 256.726 1 2 -1 -9 4143.56 297.009 1 2 1 -8 11044.9 460.055 1 -2 -1 8 10230.6 440.516 1 2 -1 -8 10719.6 477.209 1 2 1 -7 37248.2 1044.56 1 -2 -1 7 38115.4 1052.19 1 -2 1 7 41479.3 1084.24 1 2 -1 -7 41242.5 1114.41 1 -2 1 6 409795. 7923.12 1 2 1 -6 352806. 7943.97 1 -2 1 5 298695. 6108.80 1 2 1 -5 300689. 6085.89 1 2 -1 -5 289558. 6120.23 1 -2 -1 5 286083. 6087.91 1 2 -1 -4 8305.27 316.064 1 -2 -1 4 8385.14 303.923 1 -2 1 4 9173.78 323.429 1 2 1 -4 9613.39 317.988 1 2 1 -3 566043. 11472.1 1 2 2 -15 2042.15 270.967 1 -2 -2 14 346.154 128.321 1 2 -2 -14 139.015 123.483 1 -2 2 14 262.358 135.288 1 2 -2 -13 1491.97 226.464 1 -2 -2 13 1287.09 195.202 1 -2 2 13 1296.98 212.948 1 2 2 -13 1517.88 213.717 1 2 2 -12 1021.92 166.224 1 2 -2 -12 1012.07 172.950 1 -2 2 12 963.239 191.884 1 -2 -2 12 858.405 154.919 1 2 2 -11 55312.5 1521.32 1 -2 2 11 56157.1 1599.43 1 -2 2 10 69.8585 63.3196 1 2 2 -10 12.3141 64.7177 1 2 2 -9 9309.42 435.283 1 -2 -2 9 8616.85 409.081 1 -2 2 9 8482.84 435.149 1 2 2 -8 882.902 127.163 1 -2 -2 8 950.481 121.633 1 2 -2 -8 1006.71 143.454 1 -2 2 8 1141.73 150.123 1 2 -2 -7 377321. 7653.81 1 2 2 -7 361039. 7589.22 1 -2 -2 7 374957. 7582.30 1 -2 2 6 2022.31 166.803 1 2 -2 -6 2062.33 175.988 1 2 2 -6 1998.88 150.918 1 -2 -2 6 2030.51 153.881 1 -2 2 5 1789.41 147.894 1 2 -2 -5 1694.88 142.953 1 -2 -2 5 1846.15 132.903 1 2 2 -5 2063.13 140.427 1 2 -2 -4 239699. 5102.75 1 -2 -2 4 237899. 5053.27 1 -2 2 4 241313. 5146.37 1 2 2 -3 73293.4 1569.30 1 2 2 4 16180.3 474.207 1 2 2 5 13615.1 453.575 1 -2 -2 -6 3755.41 240.725 1 2 2 6 3546.15 216.073 1 2 2 7 16733.8 614.340 1 -2 -2 -7 20539.8 672.107 1 2 2 8 1866.20 176.058 1 -2 -2 -8 2053.13 198.598 1 2 2 9 34161.0 1050.20 1 -2 -2 -9 36384.4 1095.20 1 2 2 10 1315.40 168.203 1 -2 -3 15 1865.76 272.041 1 2 3 -15 1421.19 224.812 1 2 -3 -14 7176.36 502.219 1 -2 -3 14 8350.17 519.883 1 -2 3 14 8255.40 563.470 1 2 3 -14 8010.91 504.614 1 2 -3 -13 4609.41 394.280 1 -2 3 13 4457.80 397.617 1 2 3 -13 4134.07 341.663 1 2 3 -12 13869.4 631.370 1 -2 -3 12 13288.7 612.102 1 2 -3 -12 12981.4 639.776 1 -2 3 12 12823.9 666.966 1 2 -3 -11 257.066 104.994 1 -2 -3 11 270.190 89.5492 1 -2 3 11 202.380 98.4433 1 2 3 -11 240.105 91.5044 1 2 -3 -10 23.2394 68.9918 1 2 3 -10 87.5882 70.6379 1 -2 -3 10 29.0304 58.6362 1 -2 -3 9 28853.9 897.915 1 2 -3 -9 31958.8 1005.25 1 -2 3 9 30719.8 958.705 1 -2 -3 8 2972.28 208.088 1 2 -3 -8 2800.10 240.164 1 -2 3 8 2676.22 219.608 1 2 3 -7 51846.1 1281.12 1 -2 -3 7 50252.9 1271.66 1 2 -3 -6 97493.0 2266.36 1 -2 -3 6 94215.1 2178.39 1 -2 3 6 95756.2 2233.16 1 2 3 -5 11677.4 369.723 1 2 -3 -5 10029.1 415.650 1 -2 -3 5 12034.6 382.489 1 -2 3 5 10054.3 394.824 1 -2 -3 4 522300. 10553.8 1 2 -3 -4 522894. 10666.6 1 2 3 -4 519470. 10558.9 1 2 3 -3 17688.9 432.913 1 2 3 2 22579.0 573.844 1 2 3 3 342990. 7041.14 1 2 3 4 51241.9 1259.32 1 -2 -3 -4 53545.2 1276.78 1 -2 -3 -5 30924.2 837.616 1 2 3 5 24698.1 768.363 1 2 3 6 16562.7 597.198 1 -2 -3 -6 22191.2 693.119 1 2 3 7 58404.2 1581.35 1 -2 -3 -7 69080.2 1665.90 1 2 3 8 1099.31 148.067 1 -2 -3 -8 1551.52 186.754 1 -2 -3 -9 4383.85 324.331 1 2 3 9 4237.05 295.195 1 -2 -3 -10 12130.8 571.289 1 2 3 10 10085.9 504.195 1 2 3 11 7292.46 438.792 1 -2 -3 -11 8713.92 481.158 1 2 3 12 871.577 159.007 1 -2 -4 14 17.4334 77.6260 1 2 -4 -14 10.8912 75.5745 1 2 -4 -13 1582.40 235.410 1 -2 -4 13 1599.64 202.968 1 -2 4 13 1225.27 212.149 1 2 4 -13 1578.53 218.691 1 -2 -4 12 2632.78 251.331 1 2 -4 -12 3216.77 308.981 1 -2 4 12 2429.21 263.874 1 2 4 -12 2617.86 264.493 1 -2 4 11 136.574 86.7278 1 2 4 -11 302.713 98.1521 1 2 -4 -11 220.217 101.902 1 -2 -4 11 234.091 90.4656 1 -2 -4 10 2445.54 215.178 1 2 4 -10 3116.82 253.047 1 2 -4 -10 2768.80 264.526 1 -2 4 10 2730.79 253.663 1 -2 4 9 51635.6 1422.75 1 2 4 -9 50089.4 1338.20 1 2 -4 -9 51125.1 1424.52 1 2 4 -8 52630.9 1415.56 1 -2 4 8 57718.3 1543.10 1 2 4 -7 3528.36 214.333 1 -2 4 7 3158.60 227.512 1 2 -4 -7 3134.92 233.506 1 2 4 -6 68413.5 1594.46 1 2 -4 -6 70633.9 1696.24 1 -2 -4 6 70474.8 1601.41 1 -2 4 6 69150.9 1681.34 1 2 4 -5 41165.3 990.664 1 -2 -4 5 42214.6 995.969 1 2 -4 -5 40305.4 1088.35 1 -2 4 5 41138.0 1086.05 1 -2 -4 4 364695. 7371.60 1 2 4 -4 360848. 7372.77 1 2 4 0 74477.2 1562.74 1 2 4 1 248781. 5097.75 1 2 4 2 482785. 9823.06 1 2 4 3 18144.7 545.120 1 -2 -4 -3 16814.5 508.365 1 -2 -4 -4 21141.0 642.239 1 2 4 5 36612.8 1057.09 1 -2 -4 -5 40318.2 1063.21 1 2 4 6 203.195 67.9170 1 -2 -4 -6 260.553 78.4677 1 -2 -4 -7 5981.13 348.383 1 2 4 7 5727.46 335.873 1 -2 -4 -8 7.42072 74.9356 1 2 4 8 48.4699 57.6846 1 2 4 9 10032.2 503.572 1 -2 -4 -9 11414.4 544.580 1 -2 -4 -10 2705.57 271.143 1 2 4 10 2669.96 279.272 1 2 4 11 31.2260 60.2149 1 -2 -4 -11 85.0465 87.0687 1 -2 -4 -12 12094.7 607.356 1 2 4 12 10554.7 558.513 1 2 5 -15 93.1037 83.0803 1 -2 -5 15 95.0423 87.6296 1 2 5 -14 190.672 104.235 1 -2 5 13 3791.50 360.999 1 2 -5 -13 4275.54 376.104 1 -2 -5 13 3677.25 301.614 1 2 5 -13 4143.97 341.858 1 2 5 -12 7114.82 414.136 1 -2 5 12 8012.26 496.570 1 2 -5 -12 7435.08 482.254 1 -2 -5 12 7122.43 411.422 1 -2 5 11 22977.2 874.777 1 2 5 -11 22063.4 767.451 1 2 -5 -11 20525.6 820.082 1 -2 5 10 7269.43 451.637 1 2 -5 -10 7582.00 439.138 1 2 5 -10 7820.80 399.647 1 2 5 -9 1238.60 148.836 1 -2 -5 9 958.267 127.231 1 -2 5 9 1279.11 176.931 1 2 -5 -9 1134.68 161.857 1 -2 -5 8 32727.4 950.944 1 -2 5 8 34195.1 1053.84 1 2 -5 -8 37852.9 1116.09 1 2 5 -8 38315.0 999.649 1 -2 5 7 68304.2 1805.48 1 2 -5 -7 77129.0 1822.19 1 2 -5 -6 57148.2 1496.78 1 -2 -5 6 57666.1 1385.11 1 -2 5 6 60304.3 1508.77 1 2 -5 -5 22188.3 691.613 1 -2 -5 5 21142.5 580.318 1 2 5 -5 22596.3 582.182 1 -2 -5 4 2791.68 125.959 1 2 5 -4 2931.08 128.506 1 2 5 0 10953.4 299.274 1 2 5 1 5621.94 204.308 1 2 5 2 235.324 48.9975 1 -2 -5 -3 35948.5 906.694 1 2 5 3 34635.1 908.784 1 2 5 4 13823.7 490.341 1 -2 -5 -4 14156.3 484.395 1 2 5 5 8890.89 406.933 1 -2 -5 -5 9577.78 396.756 1 2 5 6 10022.1 447.605 1 -2 -5 -6 9262.19 413.379 1 2 5 7 174899. 3945.21 1 -2 -5 -7 174463. 3886.38 1 -2 -5 -8 13270.5 586.169 1 -2 -5 -9 168.425 107.054 1 -2 -5 -10 3212.36 294.995 1 -2 -5 -11 146.820 103.841 1 -2 -6 15 123.723 88.0242 1 -2 -6 14 2829.73 271.362 1 2 -6 -13 4649.31 394.729 1 -2 -6 13 3971.36 306.079 1 2 -6 -12 2635.66 288.681 1 -2 6 12 2610.55 295.497 1 -2 -6 12 2585.37 236.763 1 2 6 -12 2330.81 218.635 1 -2 -6 11 2114.41 206.201 1 2 -6 -11 2110.00 239.276 1 -2 6 11 2447.67 274.813 1 2 6 -11 2084.90 198.806 1 -2 6 10 189.400 99.6587 1 2 -6 -10 121.076 85.5213 1 2 6 -10 260.551 79.3665 1 -2 -6 10 165.532 67.5482 1 2 6 -9 61937.0 1550.20 1 -2 -6 9 60820.1 1559.06 1 2 -6 -9 64126.8 1689.74 1 -2 6 9 66751.2 1713.82 1 -2 6 8 17098.9 645.969 1 -2 -6 8 17553.3 581.276 1 2 6 -8 16906.7 565.327 1 -2 6 7 37728.3 1068.56 1 2 6 -7 36153.5 922.855 1 2 -6 -7 35386.0 1073.67 1 2 -6 -6 3498.57 241.499 1 -2 -6 6 3844.67 196.027 1 2 -6 -5 34940.5 1002.54 1 -2 -6 5 38801.5 891.376 1 -2 -6 4 29032.2 667.461 1 2 6 0 20543.9 476.049 1 2 6 1 74523.1 1610.85 1 2 6 2 10831.1 356.853 1 -2 -6 -3 125462. 2721.56 1 2 6 3 122320. 2720.51 1 -2 -6 -4 98423.1 2224.80 1 2 6 4 99416.5 2253.93 1 2 6 5 84823.6 1984.56 1 -2 -6 -5 82249.8 1943.42 1 2 6 6 3024.94 241.921 1 -2 -6 -6 3219.74 225.827 1 2 6 7 2338.39 228.311 1 -2 -6 -7 1865.07 187.164 1 -2 -6 -8 18349.5 716.543 1 2 6 8 20901.5 776.996 1 2 6 9 53.8906 78.8149 1 -2 -6 -9 22.6708 70.8147 1 2 6 10 5375.06 385.155 1 -2 -6 -10 5935.31 408.815 1 2 6 11 3125.27 304.729 1 -2 -6 -11 4040.89 346.689 1 -2 -6 -12 27.1140 71.3462 1 -2 -7 15 701.612 148.540 1 -2 -7 14 1968.84 227.669 1 2 -7 -13 2324.85 285.630 1 -2 7 13 2505.98 296.560 1 2 -7 -12 5072.80 399.890 1 -2 -7 12 5655.21 340.822 1 -2 7 12 5860.23 436.933 1 2 -7 -11 33.2499 75.3379 1 -2 -7 11 16.6380 51.9704 1 -2 7 11 44.0212 82.5002 1 -2 -7 10 5.07836 56.0444 1 -2 7 9 3144.86 271.855 1 -2 -7 9 3249.32 220.157 1 2 -7 -9 2853.06 254.540 1 -2 -7 8 257.484 65.4723 1 -2 7 8 219.563 93.1344 1 2 -7 -8 203.015 85.5045 1 -2 -7 7 924.253 104.202 1 2 -7 -7 914.750 139.887 1 2 -7 -6 40563.6 1169.55 1 -2 -7 6 41567.2 999.332 1 2 -7 -5 621.412 103.889 1 -2 -7 5 515.585 56.6557 1 2 7 1 384.924 47.6877 1 2 7 2 74620.6 1674.67 1 2 7 3 3034.99 181.495 1 -2 -7 -3 2749.31 167.348 1 2 7 4 2082.42 166.012 1 -2 -7 -4 1908.95 151.031 1 2 7 5 2365.10 193.515 1 -2 -7 -5 2358.51 181.294 1 2 7 6 12514.9 522.673 1 -2 -7 -6 10779.0 457.754 1 2 7 7 18329.8 702.899 1 -2 -7 -7 15825.8 612.074 1 2 7 8 45.6597 74.6840 1 2 7 9 2325.63 252.314 1 -2 -7 -9 2606.81 258.018 1 2 7 10 1551.30 214.768 1 -2 -7 -10 1968.10 238.085 1 -2 -7 -11 830.455 169.686 1 2 7 11 752.531 164.009 1 -2 -8 15 940.719 158.059 1 -2 -8 14 611.909 129.369 1 -2 -8 13 2237.66 226.534 1 -2 -8 12 131.109 76.5613 1 -2 8 12 203.684 108.000 1 2 -8 -12 173.172 94.6111 1 2 -8 -11 46.9445 79.0085 1 -2 8 11 8.88059 90.9134 1 -2 -8 11 38.8942 53.7218 1 2 -8 -10 23.9316 74.7498 1 -2 -8 10 5.02407 50.0234 1 -2 8 10 33.9613 78.2643 1 -2 8 9 3785.39 310.285 1 2 -8 -9 4129.25 311.338 1 -2 -8 8 22735.5 680.041 1 2 -8 -8 19688.5 764.606 1 -2 -8 7 883.691 103.784 1 2 -8 -7 955.552 137.181 1 2 -8 -6 2354.74 204.844 1 -2 -8 6 2393.16 141.369 1 2 -8 -5 45290.0 1152.49 1 -2 -8 5 39962.6 932.201 1 2 8 2 69067.3 1538.84 1 -2 -8 -3 4817.22 222.259 1 2 8 4 7219.79 333.682 1 -2 -8 -4 7745.45 340.389 1 2 8 5 1545.01 159.448 1 -2 -8 -5 1475.87 145.282 1 -2 -8 -6 6613.07 344.951 1 2 8 6 6073.39 340.893 1 2 8 7 3661.15 269.298 1 -2 -8 -7 3518.68 261.476 1 2 8 8 6725.74 400.359 1 -2 -8 -8 7167.92 409.691 1 -2 -8 -9 268.410 115.767 1 2 8 9 234.471 95.3878 1 -2 -8 -10 42.2595 82.9450 1 -2 -8 -11 96.0308 84.4315 1 2 8 11 135.183 104.079 1 -2 -9 13 796.796 134.214 1 -2 9 12 125.378 109.850 1 -2 -9 12 143.976 78.2584 1 2 -9 -12 163.094 94.0460 1 2 -9 -11 4015.32 350.973 1 -2 -9 11 4582.10 297.672 1 -2 9 11 4668.94 383.532 1 2 -9 -10 1079.32 175.099 1 -2 -9 10 1302.70 148.503 1 2 -9 -9 139.501 82.9550 1 -2 -9 9 177.475 68.1490 1 2 -9 -8 2654.76 247.750 1 -2 -9 8 2735.86 185.953 1 2 -9 -7 3061.39 266.923 1 -2 -9 7 3649.01 198.614 1 -2 -9 6 1348.15 99.9956 1 2 -9 -6 1292.42 159.592 1 2 -9 -5 6441.27 340.129 1 -2 -9 -4 3417.98 200.446 1 -2 -9 -5 14767.6 549.486 1 -2 -9 -6 2629.48 225.532 1 -2 -9 -7 2752.83 250.916 1 -2 -9 -8 6627.23 426.115 1 -2 -9 -9 5300.29 372.979 1 -2 -9 -10 315.144 116.363 1 -2 -9 -11 342.788 112.732 1 2 9 11 242.811 118.818 1 2 -10 -12 975.909 186.505 1 2 -10 -11 1998.57 243.979 1 -2 -10 11 2054.14 203.118 1 2 -10 -10 1336.52 195.421 1 -2 -10 10 1480.73 161.871 1 2 -10 -9 1445.08 196.185 1 -2 -10 9 1846.33 170.497 1 2 -10 -8 10093.5 503.697 1 2 -10 -7 12620.6 562.740 1 2 -10 -6 9077.60 439.602 1 2 10 4 8110.46 319.835 1 2 10 5 5166.41 277.138 1 -2 -10 -5 5184.91 266.309 1 2 10 6 6115.56 342.708 1 -2 -10 -6 6301.51 331.323 1 -2 -10 -7 575.972 117.749 1 2 10 7 446.986 97.0368 1 -2 -10 -8 39.7054 72.1848 1 2 10 8 64.9130 58.7652 1 -2 -10 -9 3280.62 280.181 1 2 10 9 2483.95 225.674 1 2 10 10 467.204 112.339 1 -2 -10 -10 467.371 121.930 1 2 -11 -11 114.951 88.0696 1 2 -11 -10 5034.99 386.092 1 2 -11 -9 1574.06 207.497 1 2 -11 -8 7105.94 420.881 1 2 -11 -7 4335.83 306.187 1 2 11 5 643.225 94.4604 1 2 11 6 4.71625 48.9287 1 2 11 7 1412.98 164.693 1 2 11 8 397.533 100.649 1 2 11 9 1397.37 180.238 1 2 11 10 665.042 126.954 1 2 12 7 441.796 96.5563 1 2 12 8 738.157 118.962 1 2 12 9 59.2435 57.2881 1 3 0 -15 21.1908 87.3578 1 3 0 -14 3248.24 331.710 1 -3 0 14 3121.91 325.538 1 3 0 -12 15487.1 678.546 1 -3 0 12 16004.5 706.452 1 3 0 -11 29.9854 78.7895 1 3 0 -10 3241.68 271.356 1 -3 0 10 3067.37 252.235 1 3 0 -9 18.4034 61.9454 1 -3 0 8 481174. 10030.5 1 3 0 -8 484526. 10037.6 1 3 0 -7 18.2773 44.1780 1 -3 0 7 25.8942 44.1822 1 -3 0 6 272323. 5708.37 1 3 1 -15 1826.81 257.711 1 3 -1 -15 2024.23 277.233 1 -3 -1 15 1709.78 257.802 1 -3 -1 14 110.298 104.090 1 -3 1 14 204.039 113.348 1 3 1 -14 159.383 98.9156 1 3 -1 -14 236.979 108.351 1 3 1 -13 4677.46 361.520 1 3 -1 -13 4797.31 389.363 1 -3 -1 13 4519.16 362.892 1 -3 1 13 3659.00 330.277 1 3 1 -12 3571.46 304.613 1 3 -1 -12 3908.26 337.235 1 -3 -1 12 3686.85 312.834 1 -3 1 12 3567.85 298.036 1 3 1 -11 4811.50 337.629 1 3 -1 -11 4937.46 352.577 1 -3 -1 11 4639.98 334.061 1 -3 1 11 4732.17 336.755 1 3 1 -10 117047. 2761.24 1 3 -1 -10 118970. 2820.27 1 -3 -1 10 119669. 2775.30 1 -3 1 10 112699. 2770.12 1 3 1 -9 100682. 2490.83 1 3 -1 -9 105488. 2510.71 1 -3 -1 9 108450. 2464.73 1 3 -1 -8 4854.27 300.385 1 -3 -1 8 5659.50 304.788 1 3 1 -8 5072.62 296.926 1 -3 -1 7 63793.2 1489.24 1 3 -1 -7 61423.9 1506.66 1 3 1 -6 11010.3 419.724 1 3 -1 -6 10830.5 438.857 1 3 1 -5 105034. 2342.28 1 3 2 -15 8858.94 550.558 1 -3 -2 15 9723.41 583.107 1 3 -2 -14 2001.62 260.748 1 -3 -2 14 1981.79 254.888 1 -3 2 14 2031.11 268.853 1 3 -2 -13 36.6249 68.9159 1 -3 2 13 18.7688 77.3745 1 3 2 -12 20533.2 791.066 1 -3 -2 12 19118.1 767.255 1 -3 2 12 19475.1 813.359 1 -3 2 11 3177.22 282.674 1 3 2 -11 3431.08 277.191 1 3 -2 -11 3651.71 309.012 1 -3 -2 11 3431.98 279.293 1 -3 2 10 1780.90 211.684 1 3 2 -10 1707.32 182.653 1 -3 -2 10 1815.52 195.945 1 -3 2 9 32034.1 997.640 1 -3 -2 9 32497.8 951.268 1 -3 -2 8 4.49246 40.7158 1 3 2 -8 18.6131 48.9068 1 3 2 -7 32919.8 922.615 1 -3 2 7 32310.0 946.803 1 3 -2 -6 247.875 73.5456 1 3 2 -6 307.933 61.6047 1 -3 2 6 289.563 68.5923 1 -3 -2 6 353.331 64.9872 1 -3 -2 5 382516. 7841.60 1 3 2 -5 380240. 7838.53 1 -3 -3 15 715.407 166.088 1 3 3 -15 637.507 153.350 1 3 3 -14 5359.91 385.563 1 -3 3 14 6809.77 497.251 1 3 -3 -14 6436.24 475.187 1 -3 -3 14 4780.32 381.506 1 3 3 -13 13842.0 655.423 1 3 -3 -13 13052.3 665.006 1 -3 -3 13 14792.6 664.951 1 3 3 -12 4599.71 326.564 1 -3 3 12 4587.72 381.060 1 3 -3 -12 4332.79 354.712 1 3 3 -11 24495.5 835.877 1 -3 3 11 22160.1 853.928 1 3 -3 -11 24246.9 890.391 1 -3 -3 11 23322.8 818.491 1 -3 -3 10 517.714 109.604 1 3 3 -10 559.757 112.830 1 3 -3 -10 802.319 160.900 1 -3 3 10 510.484 124.472 1 3 3 -9 1478.27 159.108 1 -3 3 9 1595.01 187.683 1 -3 -3 9 1605.61 167.721 1 3 -3 -9 1795.99 200.847 1 -3 -3 8 232.315 65.2034 1 -3 3 8 184.015 78.7312 1 3 -3 -8 179.169 72.5975 1 -3 3 7 105622. 2362.54 1 3 -3 -7 94624.2 2365.13 1 -3 -3 6 22922.0 635.268 1 3 3 -6 20236.9 609.028 1 3 3 -5 1722.04 116.865 1 3 3 -4 93607.1 2027.60 1 -3 -4 15 1199.07 201.566 1 3 4 -15 1487.57 223.185 1 3 4 -14 328.958 123.002 1 -3 4 14 400.056 157.646 1 3 -4 -14 226.154 127.892 1 -3 -4 14 533.409 140.550 1 3 4 -13 1859.09 224.801 1 -3 4 13 1722.97 249.308 1 3 -4 -13 1611.32 240.217 1 -3 -4 13 1534.79 202.785 1 3 4 -12 15681.3 662.643 1 -3 4 12 17009.4 759.256 1 3 -4 -12 16707.6 743.930 1 -3 -4 12 15909.3 665.907 1 -3 4 11 23.5524 60.5517 1 3 -4 -11 40.0926 78.6908 1 3 4 -11 56.1978 82.7488 1 -3 -4 11 18.8504 76.9890 1 3 4 -10 65287.1 1630.16 1 -3 4 10 63226.4 1729.49 1 -3 -4 10 63695.8 1618.48 1 3 4 -9 19740.0 668.166 1 -3 4 9 20017.4 741.550 1 -3 -4 9 20761.8 690.339 1 3 -4 -9 19049.8 725.487 1 -3 4 8 4161.89 282.323 1 3 -4 -8 3673.62 267.279 1 3 4 -8 3669.01 239.657 1 -3 -4 8 3211.11 210.015 1 3 4 -7 47079.1 1179.41 1 3 -4 -7 46237.8 1277.31 1 3 4 -6 12422.8 413.039 1 3 4 -5 97423.4 2106.87 1 3 4 -4 19821.5 505.810 1 -3 -5 15 1323.39 204.794 1 3 5 -15 1366.99 206.591 1 3 5 -14 176.371 102.038 1 3 -5 -14 294.851 136.382 1 -3 -5 14 258.902 105.580 1 -3 5 13 256.448 118.502 1 3 -5 -13 287.802 106.800 1 3 5 -13 340.643 115.167 1 -3 -5 13 298.531 111.797 1 3 5 -12 2871.25 251.712 1 3 -5 -12 2847.83 288.663 1 -3 5 12 2678.03 298.386 1 -3 -5 12 2973.47 255.958 1 3 -5 -11 180.606 93.8587 1 -3 5 11 134.024 81.0484 1 3 5 -11 151.889 81.1807 1 -3 -5 11 187.057 79.3812 1 3 5 -10 9804.17 446.953 1 -3 -5 10 10108.8 452.258 1 3 -5 -10 10206.9 544.037 1 -3 5 10 8418.42 468.800 1 3 5 -9 11328.4 454.089 1 -3 5 9 9367.71 489.384 1 -3 -5 9 10513.9 447.288 1 3 -5 -9 10235.9 501.176 1 3 5 -8 2334.33 179.743 1 3 -5 -8 2367.04 218.066 1 -3 5 8 2682.66 236.373 1 -3 -5 8 2236.20 173.039 1 3 5 -7 303807. 6342.88 1 3 -5 -7 306266. 6509.05 1 3 5 -6 198522. 4182.86 1 -3 -5 6 199644. 4170.23 1 3 5 -5 117010. 2482.22 1 3 5 -4 80592.1 1719.03 1 3 5 -3 93581.7 1935.94 1 3 5 1 112327. 2384.32 1 3 5 2 12.9217 24.6049 1 3 5 3 65968.3 1538.12 1 3 5 4 40340.0 1050.73 1 3 5 5 13650.3 488.408 1 3 5 6 4308.06 270.550 1 3 5 7 13229.1 537.260 1 3 5 8 1479.40 176.185 1 3 5 9 27378.8 904.868 1 -3 -6 14 47.1845 74.8740 1 -3 -6 13 214.425 94.7772 1 3 -6 -13 176.023 97.0830 1 3 6 -13 131.427 78.1669 1 3 -6 -12 500.749 139.119 1 3 6 -12 530.208 114.856 1 -3 -6 12 476.448 116.165 1 3 -6 -11 25759.1 974.967 1 -3 -6 11 25702.4 858.902 1 3 6 -11 26967.7 862.924 1 3 -6 -10 27089.4 975.272 1 -3 -6 10 26267.0 842.606 1 3 6 -10 25732.8 832.730 1 3 6 -9 15729.6 551.790 1 -3 -6 9 14710.6 535.671 1 3 -6 -9 15677.9 655.006 1 3 6 -8 2254.77 171.049 1 3 -6 -8 2361.41 221.497 1 -3 -6 8 2436.49 175.214 1 3 6 -7 11350.1 387.987 1 -3 -6 7 12211.2 408.359 1 -3 -6 6 8282.65 294.938 1 3 6 -6 7286.42 271.577 1 3 6 -5 2836.95 131.996 1 3 6 -4 23992.4 549.966 1 3 6 -1 185489. 3765.47 1 3 6 0 1861.66 97.6526 1 3 6 1 24438.1 620.019 1 3 6 2 2252.90 150.779 1 3 6 3 1602.67 141.909 1 3 6 4 11509.8 443.797 1 3 6 5 8737.52 403.567 1 3 6 6 17410.8 631.540 1 3 6 7 4812.19 318.112 1 3 6 8 4229.98 315.588 1 3 6 9 20249.1 834.030 1 3 6 10 1000.88 164.604 1 -3 -7 15 49.4056 70.6688 1 -3 -7 14 102.533 87.0658 1 -3 7 13 2215.70 282.064 1 3 -7 -13 2395.62 293.251 1 3 7 -13 1801.60 188.492 1 -3 7 12 2945.09 311.348 1 3 -7 -12 2769.79 299.869 1 -3 -7 12 2984.06 262.778 1 3 7 -12 3153.31 238.469 1 -3 7 11 1029.23 193.233 1 3 -7 -11 897.437 163.698 1 -3 -7 11 947.694 147.410 1 3 7 -11 743.070 118.009 1 3 -7 -10 1108.12 197.504 1 -3 -7 10 943.978 130.205 1 3 -7 -9 362.152 110.191 1 3 7 -9 236.802 66.0098 1 -3 -7 9 336.502 78.7278 1 3 -7 -8 615.975 130.576 1 3 7 -8 857.528 98.3752 1 -3 -7 7 17403.1 531.080 1 3 7 -7 18781.1 534.292 1 3 7 -6 3837.85 161.393 1 3 7 0 3384.93 139.406 1 3 7 1 135447. 2856.66 1 3 7 2 692.303 88.0351 1 3 7 3 99936.3 2287.71 1 3 7 5 1013.74 138.845 1 3 7 6 11200.1 493.280 1 3 7 7 2064.14 206.128 1 3 7 8 340.452 100.102 1 3 7 9 2380.34 249.837 1 3 7 10 109.350 81.3508 1 3 7 11 362.085 122.775 1 -3 -8 15 907.089 159.314 1 -3 -8 13 21.8101 67.0162 1 3 -8 -12 9072.05 565.324 1 -3 -8 12 9333.37 453.859 1 3 -8 -11 12028.1 619.768 1 -3 -8 11 13820.4 536.616 1 -3 -8 10 190.081 73.9635 1 3 -8 -10 170.696 96.4255 1 3 -8 -9 2758.42 260.941 1 -3 -8 7 11432.7 396.866 1 3 8 0 24773.0 564.200 1 3 8 1 14771.1 422.805 1 3 8 2 13274.2 420.059 1 3 8 3 25712.1 741.274 1 3 8 4 13515.4 485.711 1 3 8 5 877.169 116.998 1 3 8 6 42.4176 56.4429 1 3 8 7 966.409 149.795 1 3 8 8 9812.75 499.932 1 3 8 9 732.292 153.919 1 3 8 10 333.625 119.312 1 -3 -9 15 287.585 106.425 1 -3 -9 14 202.287 89.2502 1 -3 -9 13 1050.04 163.756 1 3 -9 -12 1172.61 206.433 1 -3 -9 12 1567.18 190.361 1 -3 -9 11 28.3877 60.4342 1 3 -9 -10 8.54138 68.9402 1 -3 -9 10 24.0937 56.7695 1 -3 -9 9 21813.0 668.880 1 3 -9 -9 20676.0 828.673 1 3 9 1 14207.9 379.602 1 3 9 2 662.610 75.1579 1 3 9 3 8768.03 351.909 1 3 9 4 38412.4 1026.94 1 3 9 5 610.304 99.2228 1 3 9 6 9413.35 418.030 1 3 9 7 341.858 89.2401 1 3 9 8 878.919 142.266 1 3 9 9 14.1837 63.1563 1 3 9 10 1032.60 177.033 1 -3 -10 12 107.888 81.0707 1 3 -10 -11 305.415 113.873 1 -3 -10 11 460.384 106.576 1 3 10 3 404.459 71.0580 1 3 10 4 625.319 91.5256 1 3 10 5 2492.34 194.202 1 3 10 6 7494.64 366.971 1 3 10 7 4041.46 276.400 1 3 10 9 242.387 90.4097 1 3 10 10 371.066 118.045 1 3 11 4 329.295 68.1783 1 3 11 5 641.487 100.432 1 3 11 6 4.83335 48.8061 1 3 11 7 1553.75 164.420 1 3 11 8 559.871 103.642 1 3 11 9 399.704 93.1733 1 3 11 10 36.8460 50.6366 1 4 0 -14 37.2035 78.2664 1 -4 0 14 9.24822 88.0466 1 4 0 -13 37.6390 97.6240 1 -4 0 12 1724.70 225.654 1 4 0 -12 1677.27 224.198 1 4 0 -11 218.793 96.7365 1 -4 0 10 26184.8 902.579 1 4 0 -10 27049.3 949.423 1 -4 0 9 17.5736 54.8912 1 -4 0 8 103749. 2501.34 1 4 0 -8 110690. 2570.16 1 -4 -1 15 3238.39 331.823 1 4 1 -15 2980.52 322.208 1 4 -1 -15 2927.66 335.185 1 -4 -1 14 2685.02 290.817 1 4 1 -14 2567.63 278.423 1 -4 1 14 2532.16 299.099 1 4 -1 -14 2645.90 304.027 1 -4 -1 13 9626.52 554.387 1 -4 1 13 10674.6 580.323 1 4 1 -13 10733.7 558.490 1 4 -1 -13 9996.06 569.706 1 -4 -1 12 4705.18 340.135 1 -4 1 12 4622.94 351.804 1 4 1 -12 4814.55 352.337 1 4 -1 -12 5500.98 402.315 1 -4 -1 11 10395.6 518.052 1 -4 1 11 10988.3 557.052 1 4 1 -11 11305.5 544.506 1 4 -1 -11 11498.6 564.742 1 4 -1 -10 18734.0 736.107 1 -4 -1 10 17706.0 679.198 1 -4 1 10 19088.0 728.193 1 4 1 -10 19154.0 714.526 1 4 1 -9 1651.88 181.811 1 4 -1 -9 1709.28 192.099 1 -4 -1 9 1747.34 182.363 1 -4 1 9 1625.95 186.329 1 -4 -1 8 24548.3 786.886 1 4 1 -8 23190.1 786.240 1 -4 1 8 26568.0 851.617 1 4 -1 -8 27201.3 864.198 1 4 1 -7 227066. 4931.59 1 -4 -2 15 1496.03 220.911 1 4 2 -15 1371.43 209.915 1 4 -2 -15 1663.74 248.462 1 -4 -2 14 6376.88 431.676 1 4 2 -14 6181.37 427.055 1 4 -2 -14 6838.09 500.744 1 4 -2 -13 78.4974 100.458 1 -4 -2 13 66.5503 87.4429 1 -4 -2 12 5146.48 368.854 1 -4 2 12 5543.26 400.907 1 4 -2 -12 5185.94 389.907 1 -4 -2 11 53090.1 1448.76 1 -4 2 11 49377.9 1472.98 1 4 -2 -11 52522.6 1494.57 1 4 -2 -10 46667.3 1371.13 1 -4 -2 10 46004.9 1300.05 1 4 2 -10 46948.9 1322.61 1 -4 2 10 46234.9 1329.86 1 -4 2 9 26240.5 879.610 1 4 -2 -9 23489.1 847.228 1 -4 -2 9 25309.1 800.190 1 4 2 -9 24629.0 795.347 1 -4 -2 8 73158.3 1751.50 1 4 2 -8 70487.4 1755.90 1 4 2 -7 27429.3 813.243 1 -4 -3 15 856.615 173.024 1 4 3 -15 1040.84 177.349 1 4 -3 -14 11.2523 96.5621 1 -4 3 14 32.4817 98.1289 1 4 3 -14 32.0418 75.0625 1 -4 -3 13 17698.3 728.979 1 4 3 -13 18342.8 734.009 1 4 -3 -13 17695.8 798.477 1 -4 3 13 18008.3 793.783 1 4 3 -12 8350.06 463.530 1 4 -3 -12 9758.09 551.120 1 -4 3 12 8485.76 509.202 1 4 3 -11 13419.4 572.524 1 -4 3 11 13506.1 610.906 1 4 -3 -11 12536.3 611.663 1 4 -3 -10 65410.9 1736.48 1 -4 3 10 62126.5 1685.24 1 -4 -3 10 61466.7 1592.23 1 4 3 -10 58224.7 1574.83 1 4 -3 -9 34767.0 1073.42 1 -4 -3 9 34896.8 995.512 1 -4 3 9 35530.2 1123.67 1 4 3 -9 33490.6 1000.99 1 -4 -3 8 42355.0 1132.28 1 4 3 -8 43052.9 1124.44 1 4 4 -16 2680.33 298.056 1 4 4 -15 17.0908 85.0830 1 -4 -4 14 1504.60 205.931 1 4 4 -14 1292.42 192.261 1 4 -4 -14 1380.84 231.064 1 -4 4 14 1632.18 255.351 1 -4 -4 13 6092.06 392.787 1 4 4 -13 6125.22 388.575 1 4 -4 -13 6178.52 447.197 1 -4 4 13 5584.33 424.884 1 -4 -4 12 3881.70 298.595 1 4 4 -12 2328.11 231.260 1 4 -4 -12 3663.47 360.743 1 -4 4 12 2824.80 288.264 1 -4 -4 11 10347.8 482.072 1 -4 4 11 11009.2 565.171 1 4 4 -11 10332.3 485.189 1 4 -4 -11 10598.2 567.305 1 4 -4 -10 28352.4 990.509 1 4 4 -10 27912.9 877.667 1 -4 -4 10 29228.8 902.965 1 -4 4 10 30780.5 1040.00 1 4 4 -9 20139.9 648.939 1 -4 -4 9 17902.7 629.205 1 -4 -4 8 68429.5 1710.98 1 4 4 -8 77231.2 1788.74 1 4 4 -7 12034.0 419.525 1 4 4 -6 10671.6 367.578 1 4 4 -5 20431.3 578.142 1 4 5 -16 46.6317 92.8626 1 4 5 -15 2141.84 238.345 1 -4 -5 15 2007.38 242.150 1 4 5 -14 1123.62 173.922 1 -4 -5 14 1283.00 188.493 1 4 -5 -14 993.929 204.006 1 4 5 -13 1859.08 214.608 1 -4 -5 13 1992.94 227.927 1 -4 5 13 2201.84 275.382 1 4 -5 -13 1662.57 235.501 1 -4 -5 12 7.22613 70.9154 1 4 -5 -12 87.0881 95.1998 1 4 5 -11 3085.33 247.620 1 -4 -5 11 3088.83 257.750 1 -4 5 11 2644.49 283.435 1 4 -5 -11 2957.09 294.047 1 4 -5 -10 28329.8 991.269 1 4 5 -10 28683.9 870.942 1 -4 -5 10 29104.6 881.383 1 4 5 -9 1030.12 126.511 1 -4 -5 9 1180.36 137.692 1 -4 -5 8 4890.76 269.462 1 4 5 -8 4900.08 253.445 1 4 5 -7 1447.85 127.396 1 4 5 -6 5197.23 220.825 1 4 5 -5 414568. 8437.65 1 4 6 -16 521.147 137.592 1 -4 -6 16 628.284 158.221 1 -4 -6 15 6159.73 428.556 1 4 6 -15 5891.88 411.589 1 4 6 -14 442.140 122.948 1 -4 -6 14 628.098 147.581 1 -4 -6 13 641.411 143.924 1 4 -6 -13 244.182 110.685 1 -4 6 13 556.974 162.605 1 4 6 -12 348.082 94.9480 1 4 -6 -12 419.524 144.073 1 -4 -6 12 281.612 96.5702 1 4 -6 -11 80.6741 78.4120 1 4 6 -11 107.469 70.6573 1 -4 -6 11 98.1916 72.1175 1 4 6 -10 2567.07 206.633 1 -4 -6 10 3506.35 247.716 1 4 6 -9 26354.3 771.859 1 -4 -6 9 24265.1 745.245 1 -4 -6 8 29586.6 837.726 1 4 6 -7 12440.0 413.388 1 4 6 -6 48630.3 1135.51 1 4 6 -5 144872. 3016.63 1 4 6 -4 95.3338 23.5142 1 4 7 -16 56.9088 77.4064 1 -4 -7 15 859.028 161.969 1 4 7 -15 770.709 152.271 1 4 7 -14 265.177 96.7516 1 -4 -7 14 229.730 102.413 1 -4 -7 13 2421.63 251.148 1 4 7 -13 2142.43 219.680 1 4 7 -12 318.283 92.2958 1 -4 -7 11 170.861 85.2693 1 4 7 -11 184.740 69.0347 1 4 7 -10 1252.24 130.427 1 -4 -7 10 1577.68 163.799 1 -4 -7 9 41221.7 1098.73 1 4 7 -8 18859.3 559.774 1 4 7 -7 5178.77 219.018 1 4 7 -6 3335.03 154.850 1 4 7 -5 4652.55 161.785 1 4 7 -1 5006.90 170.846 1 4 7 0 59166.8 1327.55 1 4 7 1 4958.32 219.456 1 4 7 2 7052.46 290.065 1 4 7 3 23777.9 707.095 1 4 7 4 5149.45 287.058 1 4 7 5 77060.5 1876.60 1 4 7 6 7300.32 386.633 1 -4 -8 16 9.11661 76.7147 1 -4 -8 15 1274.51 198.201 1 -4 -8 14 2373.34 250.213 1 4 8 -14 1488.95 162.354 1 -4 -8 13 35.1554 71.0017 1 -4 -8 12 332.779 105.177 1 4 8 -12 190.454 65.7248 1 -4 -8 11 7036.36 368.497 1 4 8 -11 5614.49 298.825 1 -4 -8 10 10177.0 418.794 1 4 8 -10 6584.78 293.025 1 4 8 -9 4225.95 205.317 1 4 8 -8 250.020 46.4383 1 4 8 -7 25416.6 642.815 1 4 8 -1 509.011 43.9956 1 4 8 0 20894.0 528.901 1 4 8 1 27260.2 702.384 1 4 8 2 14221.0 454.860 1 4 8 3 74991.1 1750.34 1 4 8 4 772.984 112.348 1 4 8 5 306.366 84.0449 1 4 8 6 1433.97 175.602 1 4 8 7 221.886 82.3096 1 4 8 8 14.2203 58.6223 1 -4 -9 15 350.841 125.043 1 -4 -9 14 2827.76 285.589 1 -4 -9 13 2334.35 244.711 1 -4 -9 12 1718.19 202.033 1 -4 -9 11 1618.30 180.716 1 4 9 0 62.8807 25.3707 1 4 9 1 19039.7 517.244 1 4 9 3 538.778 81.4802 1 4 9 4 3.87289 42.7409 1 4 9 5 53.9442 49.0418 1 4 9 6 7287.36 366.539 1 4 9 8 4114.94 304.242 1 4 10 1 8201.27 262.836 1 4 10 2 1845.27 136.085 1 4 10 3 2259.70 160.769 1 4 10 4 1523.40 141.667 1 4 10 5 320.086 74.0343 1 4 10 6 4.56661 43.4754 1 4 10 7 236.934 74.2147 1 4 10 8 157.276 76.0012 1 4 10 9 157.647 75.8531 1 4 11 3 477.082 78.9716 1 4 11 4 79.8420 44.1138 1 4 11 5 159.632 60.4890 1 4 11 6 4.37286 40.9752 1 4 11 7 500.294 96.5190 1 4 11 8 1127.50 145.157 1 5 0 -14 14176.0 716.249 1 -5 0 14 12645.5 663.676 1 5 0 -13 19.3936 86.3544 1 -5 0 13 16.4160 74.3902 1 -5 0 12 4763.10 357.950 1 5 0 -12 5849.33 406.823 1 5 0 -11 32.5223 69.7743 1 -5 0 11 23.5421 73.5343 1 5 0 -10 4952.75 353.689 1 5 1 -15 505.545 147.092 1 -5 -1 15 588.842 154.734 1 5 -1 -15 865.391 185.809 1 -5 1 15 1030.65 199.649 1 5 1 -14 19532.5 838.767 1 5 -1 -14 21148.1 898.948 1 -5 -1 14 18705.3 818.812 1 -5 1 14 18049.5 804.473 1 5 1 -13 3121.12 300.693 1 -5 -1 13 3168.81 300.133 1 -5 1 13 2659.45 289.588 1 -5 1 12 19795.2 814.166 1 5 1 -12 21568.8 860.530 1 -5 -1 12 18235.0 754.959 1 5 -1 -12 21005.8 893.953 1 5 -1 -11 2111.64 263.638 1 -5 -1 11 1517.72 195.503 1 -5 1 11 1906.37 230.161 1 5 1 -11 1624.35 206.089 1 -5 -1 10 47.9319 69.1524 1 5 1 -10 65.5102 71.4384 1 5 1 -9 2444.64 243.347 1 5 -2 -15 360.345 144.510 1 5 2 -15 294.179 130.108 1 5 2 -14 123.268 92.6387 1 -5 2 14 291.368 119.641 1 -5 -2 14 244.861 111.198 1 5 -2 -14 180.274 118.496 1 5 2 -13 15658.2 696.495 1 -5 -2 13 14860.5 681.828 1 -5 -2 12 3992.10 303.522 1 5 -2 -12 4448.15 362.064 1 -5 -2 11 33525.1 1062.83 1 5 -2 -11 32530.4 1114.44 1 5 2 -10 59113.5 1616.35 1 -5 -2 10 59612.6 1607.32 1 5 2 -9 188997. 4206.42 1 5 3 -16 347.478 123.638 1 -5 -3 15 339.321 125.477 1 5 3 -15 274.456 109.151 1 -5 3 14 4812.71 417.145 1 5 3 -14 4825.23 370.874 1 -5 -3 14 4427.97 357.127 1 5 3 -13 6833.86 419.325 1 -5 3 13 6581.02 479.311 1 -5 -3 13 6765.22 426.445 1 5 -3 -12 4002.90 345.736 1 5 3 -12 4648.54 324.387 1 -5 3 12 4670.70 378.192 1 -5 -3 12 4244.46 311.003 1 5 3 -11 27541.0 917.768 1 5 3 -10 1061.69 149.913 1 5 3 -9 16564.6 612.146 1 5 3 -8 373156. 7839.62 1 -5 -4 16 81.2686 87.1868 1 5 4 -16 60.7156 82.5876 1 -5 -4 15 235.986 114.610 1 5 4 -15 138.143 90.7826 1 5 4 -14 2785.81 265.290 1 -5 4 14 3174.40 359.572 1 -5 -4 14 3251.86 298.250 1 5 -4 -14 3186.90 348.792 1 5 4 -13 3889.96 295.140 1 -5 -4 13 4504.91 338.781 1 5 -4 -13 3669.17 340.393 1 5 4 -12 89.5035 68.9167 1 -5 -4 11 4598.59 312.567 1 5 4 -11 4328.82 285.851 1 5 4 -10 230.613 83.0556 1 -5 -4 10 122.267 84.3703 1 5 4 -9 18362.4 619.733 1 5 4 -8 11605.7 444.187 1 -5 -5 16 140.323 105.650 1 5 5 -15 3932.59 322.944 1 -5 -5 15 4792.81 372.216 1 5 5 -14 2448.84 239.868 1 -5 -5 14 2474.32 267.849 1 5 -5 -14 2299.58 296.405 1 5 5 -13 2740.91 246.990 1 -5 -5 13 2561.22 252.811 1 -5 -5 12 32.5454 66.6438 1 5 5 -12 82.3291 70.7080 1 5 5 -11 992.026 137.561 1 -5 -5 11 1105.73 158.890 1 5 5 -10 230.248 73.0542 1 5 5 -9 63.9108 52.9935 1 5 5 -8 38041.0 987.397 1 5 5 -7 516.690 74.9308 1 -5 -6 16 28.2819 77.7342 1 5 6 -16 83.6736 86.8142 1 5 6 -15 7.81981 65.8023 1 5 6 -14 375.994 110.699 1 -5 -6 14 535.760 140.129 1 -5 -6 13 25308.3 892.487 1 -5 -6 12 8912.96 466.309 1 5 6 -12 8439.80 427.990 1 5 6 -11 76.2758 61.7385 1 -5 -6 11 111.562 81.4874 1 5 6 -10 26.9218 50.0932 1 5 6 -9 15672.8 529.720 1 5 6 -8 3490.17 209.108 1 5 6 -7 1985.76 134.187 1 5 6 -6 1429.60 104.665 1 5 7 -16 468.091 121.570 1 -5 -7 16 724.796 161.167 1 5 7 -15 7.48067 66.6184 1 5 7 -14 636.699 127.734 1 -5 -7 14 895.609 165.804 1 -5 -7 13 1226.62 183.899 1 5 7 -12 1445.94 167.597 1 5 7 -11 8626.71 397.625 1 5 7 -10 6701.50 330.515 1 5 7 -7 52189.0 1220.86 1 5 7 -6 45100.0 1034.86 1 5 7 -5 20304.9 499.284 1 5 8 -16 93.5847 83.0428 1 -5 -8 16 153.966 97.1978 1 -5 -8 15 127.342 101.561 1 5 8 -15 86.3360 67.2902 1 -5 -8 14 16.8865 88.7398 1 -5 -8 13 842.905 162.946 1 5 8 -13 709.238 116.809 1 5 8 -12 5721.41 311.033 1 5 8 -11 6044.10 290.194 1 5 8 -10 569.027 86.3731 1 5 8 -9 4014.62 209.479 1 5 8 -8 2267.03 136.155 1 5 8 -7 7713.47 256.365 1 5 8 -6 8627.76 255.171 1 5 8 -5 26332.5 590.394 1 -5 -9 15 828.610 190.770 1 5 9 -13 801.061 98.1339 1 5 9 -12 72.7215 40.2004 1 5 9 -11 85.7059 43.4404 1 5 9 -1 6260.89 196.153 1 5 9 0 5994.94 220.601 1 5 9 1 684.428 73.4534 1 5 9 2 9587.43 345.649 1 5 9 3 383.029 70.6404 1 5 9 4 637.573 98.3295 1 5 10 0 11245.2 325.609 1 5 10 1 14028.2 413.040 1 5 10 2 3159.37 174.872 1 5 10 3 5172.14 244.019 1 5 10 4 394.308 73.0703 1 5 10 5 78.8239 48.3982 1 5 11 2 3810.10 190.991 1 5 11 3 51.2268 35.8744 1 5 11 4 2197.12 159.417 1 5 11 5 50.3887 41.9783 1 -6 0 15 56.2341 111.985 1 -6 0 14 6516.99 477.919 1 6 0 -14 7438.10 554.460 1 6 0 -13 42.8915 74.4111 1 6 -1 -15 51.0530 85.9262 1 -6 -1 14 7032.87 495.154 1 6 1 -14 8059.66 545.547 1 6 -1 -14 7671.87 541.712 1 6 1 -13 1715.60 244.755 1 6 1 -12 2687.10 298.127 1 6 2 -16 506.822 152.165 1 6 2 -15 298.845 119.873 1 6 2 -14 88.1985 96.1844 1 6 2 -13 6476.96 457.265 1 6 2 -12 265.881 107.180 1 -6 -3 16 648.014 165.497 1 6 3 -16 620.581 162.925 1 6 3 -15 1464.22 214.466 1 -6 -3 15 1247.46 213.885 1 6 3 -14 25.3101 76.4637 1 6 3 -13 7.93990 61.2350 1 6 3 -12 10708.2 540.913 1 6 3 -11 23258.2 858.132 1 6 4 -16 4092.78 342.287 1 -6 -4 16 5600.98 434.188 1 6 4 -15 531.809 136.682 1 -6 -4 15 537.585 153.803 1 6 4 -14 1775.10 214.010 1 -6 -4 14 2161.71 269.095 1 6 4 -13 8899.35 460.393 1 6 4 -12 1931.07 207.333 1 6 4 -11 2828.96 251.105 1 6 4 -10 12561.6 539.260 1 -6 -5 16 31.3029 97.7747 1 6 5 -15 3141.10 276.994 1 -6 -5 15 4275.25 373.068 1 6 5 -14 1529.84 195.978 1 -6 -5 14 1992.69 243.046 1 6 5 -13 1288.32 167.923 1 6 5 -12 10250.2 465.367 1 6 5 -11 66113.9 1675.66 1 6 5 -10 244.914 73.7928 1 6 5 -9 4536.97 265.721 1 -6 -6 16 32.0536 93.4409 1 6 6 -16 61.2186 78.3438 1 6 6 -15 1150.25 169.951 1 6 6 -14 1545.63 188.806 1 6 6 -13 892.687 142.804 1 6 6 -11 5069.17 294.773 1 6 6 -10 15624.8 548.910 1 6 7 -16 592.650 129.103 1 6 7 -15 26.9443 63.1215 1 6 7 -13 33.5661 59.5499 1 6 7 -12 1071.78 141.455 1 6 7 -11 8418.15 378.958 1 6 7 -10 304.688 72.2959 1 6 7 -9 1543.09 136.130 1 6 8 -16 575.030 124.209 1 6 8 -15 18.6593 55.3906 1 6 8 -14 524.583 109.404 1 6 8 -13 258.484 83.1569 1 6 8 -12 797.494 117.122 1 6 8 -11 4.09777 41.9491 1 6 8 -10 3142.61 210.434 1 6 8 -9 9789.09 365.577 1 6 8 -8 1716.47 124.899 1 6 8 -7 7734.63 277.686 1 6 8 -6 41255.5 944.332 1 6 9 -13 532.941 88.2359 1 6 9 -12 1038.09 115.846 1 6 9 -11 423.683 65.3726 1 6 9 -10 1620.33 118.766 1 6 9 -9 11856.4 364.500 1 6 9 -8 7880.69 250.467 1 6 9 -7 871.993 65.1104 1 6 9 -6 12364.4 306.385 1 6 10 -2 256.557 27.5683 1 6 10 -1 17.3918 20.6998 1 6 10 0 832.018 73.3209 1 7 2 -16 4163.10 408.556 1 7 2 -15 2306.48 311.074 1 7 3 -16 493.815 146.223 1 7 3 -15 1097.27 189.485 1 7 3 -14 3644.69 349.853 1 7 4 -16 552.031 140.023 1 7 4 -15 680.770 148.972 1 7 4 -14 12369.4 599.253 1 7 4 -13 3746.01 306.545 1 7 5 -16 503.628 125.891 1 7 5 -14 534.523 116.616 1 7 5 -13 9643.46 470.895 1 7 5 -12 5178.87 325.971 1 7 6 -15 409.771 103.593 1 7 6 -14 1436.80 174.278 1 7 6 -13 430.576 101.287 1 7 6 -12 3097.57 234.380 1 7 7 -17 1024.22 156.903 1 7 7 -15 1659.70 184.563 1 7 7 -13 138.266 60.6430 1 7 7 -12 6063.01 316.032 1 7 7 -11 521.237 91.7214 1 7 7 -10 3.59942 32.6217 1 7 8 -16 38.8712 55.6005 1 7 8 -15 1830.63 187.540 1 7 8 -14 299.033 85.3546 1 7 8 -13 304.612 84.3700 1 7 8 -12 126.547 59.9444 1 7 8 -11 648.055 98.6045 1 7 8 -10 3419.23 204.504 1 7 8 -9 53.4099 43.2254 1 7 9 -13 124.866 51.5351 1 7 9 -12 340.847 72.1947 1 7 9 -11 50.5312 43.9271 1 7 9 -10 3176.36 180.575 1 7 9 -9 119.550 41.7926 1 7 9 -8 1099.29 92.6532 1 7 9 -7 23887.0 597.875 1 0 0 0 0.00 0.00 0 TITL csi4_0089 in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 0.41077 10.132300 8.888988 11.045345 90.0000 114.9566 90.0000 ZERR 4.00 0.001308 0.000151 0.000376 0.0000 0.0089 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O UNIT 44.00 40.00 4.00 4.00 TREF HKLF 4 END ; _shelx_hkl_checksum 64089 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_diffrn_reflns_filtered 80 _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.659 _oxdiff_exptl_absorpt_empirical_full_min 0.655 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group I2 I 0.38162(11) 0.70932(5) 0.39270(4) 0.0449(5) Uani 1 1 d . . . . . Cs1 Cs 0.77696(13) 0.87545(5) 0.69514(4) 0.0533(6) Uani 1 1 d . . . . . I1 I 0.56057(15) 0.90216(6) 0.32020(5) 0.0519(6) Uani 1 1 d . . . . . I3 I 0.17247(13) 0.51192(5) 0.45101(5) 0.0521(5) Uani 1 1 d . . . . . I4 I 0.05067(13) 0.85662(6) 0.49563(5) 0.0515(5) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 I2 0.0580(14) 0.0376(3) 0.0407(2) -0.00185(12) 0.0224(4) 0.0044(3) Cs1 0.0655(17) 0.0487(3) 0.0459(3) 0.00552(13) 0.0236(5) 0.0066(3) I1 0.0584(18) 0.0514(3) 0.0510(3) 0.00371(16) 0.0280(5) -0.0015(4) I3 0.0636(15) 0.0374(3) 0.0594(3) 0.00439(15) 0.0299(5) -0.0014(3) I4 0.0594(17) 0.0431(3) 0.0502(3) -0.00236(14) 0.0215(5) -0.0086(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Cs Cs -1.8030 0.7961 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' I I -2.2298 0.6770 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Cs1 I2 Cs1 91.09(2) 3_676 . ? I1 I2 Cs1 60.73(2) . . ? I1 I2 Cs1 67.18(3) . 3_676 ? I1 I2 I3 175.73(4) . . ? I3 I2 Cs1 123.146(19) . . ? I3 I2 Cs1 110.07(3) . 3_676 ? I2 Cs1 I2 88.91(2) 3_676 . ? I2 Cs1 I4 101.340(19) 3_676 1_655 ? I2 Cs1 I4 62.88(2) 3_676 3_676 ? I1 Cs1 I2 116.21(3) 4_576 3_676 ? I1 Cs1 I2 42.360(18) 3_676 3_676 ? I1 Cs1 I2 40.92(2) . . ? I1 Cs1 I2 67.86(3) 3_676 . ? I1 Cs1 I2 64.96(2) 4_576 . ? I1 Cs1 I2 71.784(16) . 3_676 ? I1 Cs1 I1 80.09(3) . 3_676 ? I1 Cs1 I1 73.93(2) 3_676 4_576 ? I1 Cs1 I1 105.84(4) . 4_576 ? I1 Cs1 I3 117.30(2) 4_576 4_676 ? I1 Cs1 I3 77.42(2) 4_576 3_666 ? I1 Cs1 I3 133.80(4) 3_676 3_666 ? I1 Cs1 I3 135.50(3) . 4_676 ? I1 Cs1 I3 147.53(4) . 2_656 ? I1 Cs1 I3 120.79(2) 3_676 4_676 ? I1 Cs1 I3 73.818(17) . 3_666 ? I1 Cs1 I3 68.19(2) 3_676 2_656 ? I1 Cs1 I4 127.04(2) 3_676 4_676 ? I1 Cs1 I4 64.56(2) . 3_676 ? I1 Cs1 I4 170.35(3) 4_576 3_676 ? I1 Cs1 I4 139.300(16) 3_676 1_655 ? I1 Cs1 I4 138.530(18) 4_576 1_655 ? I1 Cs1 I4 147.10(2) . 4_676 ? I1 Cs1 I4 104.10(2) 3_676 3_676 ? I1 Cs1 I4 68.63(3) . 1_655 ? I3 Cs1 I2 79.936(16) 2_656 3_676 ? I3 Cs1 I2 171.24(3) 4_676 . ? I3 Cs1 I2 97.08(2) 4_676 3_676 ? I3 Cs1 I2 125.10(4) 2_656 . ? I3 Cs1 I2 145.329(16) 3_666 3_676 ? I3 Cs1 I2 67.40(2) 3_666 . ? I3 Cs1 I1 72.555(19) 2_656 4_576 ? I3 Cs1 I3 104.37(3) 3_666 4_676 ? I3 Cs1 I3 134.217(16) 2_656 3_666 ? I3 Cs1 I3 62.58(3) 2_656 4_676 ? I3 Cs1 I4 98.20(2) 3_666 3_676 ? I3 Cs1 I4 115.82(2) 2_656 3_676 ? I3 Cs1 I4 61.38(2) 3_666 1_655 ? I3 Cs1 I4 71.99(2) 4_676 3_676 ? I3 Cs1 I4 134.20(4) 2_656 1_655 ? I3 Cs1 I4 71.94(3) 4_676 1_655 ? I4 Cs1 I2 125.51(2) 4_676 . ? I4 Cs1 I2 100.668(19) 1_655 . ? I4 Cs1 I2 105.461(17) 3_676 . ? I4 Cs1 I2 140.137(18) 4_676 3_676 ? I4 Cs1 I1 70.70(3) 4_676 4_576 ? I4 Cs1 I3 64.369(18) 4_676 2_656 ? I4 Cs1 I3 73.539(18) 4_676 3_666 ? I4 Cs1 I3 51.70(2) 4_676 4_676 ? I4 Cs1 I4 116.61(3) 4_676 3_676 ? I4 Cs1 I4 39.11(2) 3_676 1_655 ? I4 Cs1 I4 92.03(3) 4_676 1_655 ? I2 I1 Cs1 78.36(2) . . ? I2 I1 Cs1 70.46(4) . 3_676 ? I2 I1 Cs1 103.75(2) . 4_575 ? Cs1 I1 Cs1 101.19(3) . 4_575 ? Cs1 I1 Cs1 99.91(3) . 3_676 ? Cs1 I1 Cs1 156.43(3) 3_676 4_575 ? I2 I3 Cs1 107.00(2) . 4_475 ? I2 I3 Cs1 125.77(3) . 2_646 ? I2 I3 Cs1 101.34(3) . 3_666 ? Cs1 I3 Cs1 117.42(3) 2_646 4_475 ? Cs1 I3 Cs1 101.41(3) 3_666 4_475 ? Cs1 I3 Cs1 98.852(12) 2_646 3_666 ? Cs1 I4 Cs1 94.45(4) 4_475 1_455 ? Cs1 I4 Cs1 140.89(2) 3_676 1_455 ? Cs1 I4 Cs1 100.194(19) 4_475 3_676 ? I4 I4 Cs1 66.97(4) 3_576 1_455 ? I4 I4 Cs1 112.11(5) 3_576 4_475 ? I4 I4 Cs1 73.91(3) 3_576 3_676 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag I2 Cs1 3.9787(8) 3_676 ? I2 Cs1 4.2537(14) . ? I2 I1 2.8447(13) . ? I2 I3 3.0227(12) . ? Cs1 I1 3.8914(17) 3_676 ? Cs1 I1 3.7884(9) . ? Cs1 I1 3.9192(13) 4_576 ? Cs1 I3 3.9272(8) 3_666 ? Cs1 I3 3.9359(16) 4_676 ? Cs1 I3 3.9140(7) 2_656 ? Cs1 I4 3.8981(10) 4_676 ? Cs1 I4 4.2110(14) 1_655 ? Cs1 I4 4.0334(11) 3_676 ? I4 I4 2.7648(14) 3_576 ? _cod_database_fobs_code 2022875