#------------------------------------------------------------------------------ #$Date: 2023-07-29 04:02:20 +0200 (Sat, 29 Jul 2023) $ #$Revision: 285384 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/28/2022826.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022826 loop_ _publ_author_name 'Naeem, Marilyn' 'Le, Alexander N.' 'Bauer, Barbara E.' 'Chadeayne, Andrew R.' 'Golen, James A.' 'Manke, David R.' _publ_section_title ; N-Cyclohexyltryptamine: freebase, bromide and fumarate ; _journal_coeditor_code TX2070 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E Crystallographic Communications' _journal_page_first 752 _journal_page_last 756 _journal_paper_doi 10.1107/S2056989023006217 _journal_volume 79 _journal_year 2023 _chemical_formula_iupac 'C16 H22 N2' _chemical_formula_moiety 'C16 H22 N2' _chemical_formula_sum 'C16 H22 N2' _chemical_formula_weight 242.35 _chemical_name_common ; N-Cyclohexyltryptamine ; _chemical_name_systematic ; N-[2-(1H-Indol-3-yl)ethyl]cyclohexanamine ; _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_Hall 'P 2yb' _space_group_name_H-M_alt 'P 1 21 1' _atom_sites_solution_hydrogens mixed _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408) ; _cell_angle_alpha 90 _cell_angle_beta 116.784(2) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 8.5446(6) _cell_length_b 10.3990(7) _cell_length_c 8.6149(6) _cell_measurement_reflns_used 8705 _cell_measurement_temperature 297(2) _cell_measurement_theta_max 25.75 _cell_measurement_theta_min 2.65 _cell_volume 683.35(8) _computing_cell_refinement ; SAINT (Bruker, 2021) ; _computing_data_collection ; APEX4 (Bruker, 2021) ; _computing_data_reduction ; SAINT (Bruker, 2021) ; _computing_molecular_graphics ; OLEX2 (Dolomanov et al., 2009) ; _computing_publication_material ; publCIF (Westrip, 2010) ; _computing_structure_refinement ; SHELXL2018 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2014 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 297.15 _diffrn_measured_fraction_theta_full 0.995 _diffrn_measured_fraction_theta_max 0.991 _diffrn_measurement_device_type 'Bruker D8 Venture CMOS' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0341 _diffrn_reflns_av_unetI/netI 0.0215 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 10 _diffrn_reflns_limit_l_min -10 _diffrn_reflns_number 18695 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.821 _diffrn_reflns_theta_min 3.295 _diffrn_source_current 30.0 _diffrn_source_power 1.5 _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.069 _exptl_absorpt_correction_T_max 0.7453 _exptl_absorpt_correction_T_min 0.6447 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.178 _exptl_crystal_description block _exptl_crystal_F_000 264 _exptl_crystal_size_max 0.35 _exptl_crystal_size_mid 0.24 _exptl_crystal_size_min 0.2 _refine_diff_density_max 0.259 _refine_diff_density_min -0.156 _refine_ls_abs_structure_details ; Flack x determined using 1039 quotients [(I^+^)-(I^-^)]/[(I^+^)+(I^-^)] (Parsons et al., 2013) ; _refine_ls_abs_structure_Flack 0.5(7) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.040 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 171 _refine_ls_number_reflns 2621 _refine_ls_number_restraints 3 _refine_ls_restrained_S_all 1.040 _refine_ls_R_factor_all 0.0530 _refine_ls_R_factor_gt 0.0476 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0573P)^2^+0.1584P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1185 _refine_ls_wR_factor_ref 0.1237 _reflns_number_gt 2396 _reflns_number_total 2621 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file tx2070sup1.cif _cod_data_source_block I _cod_database_code 2022826 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.976 _shelx_estimated_absorpt_t_max 0.986 _shelx_hkl_file ; 1 0 0 0.00 0.30 -1 0 0 -0.10 0.30 2 0 0 9999.00 287.47 2 0 0 9778.42 286.77 -3 0 0 0.00 0.90 3 0 0 0.20 0.90 -3 0 0 0.50 1.00 -3 0 0 0.10 1.00 -3 0 0 1.20 1.10 3 0 0 0.60 0.90 -3 0 0 0.20 0.80 3 0 0 0.80 1.00 3 0 0 0.70 1.00 -3 0 0 0.20 0.80 -4 0 0 606.44 17.10 -4 0 0 593.94 17.50 4 0 0 586.44 17.20 4 0 0 573.54 17.20 -4 0 0 596.14 17.70 -4 0 0 580.84 17.20 -4 0 0 580.04 17.20 4 0 0 617.94 17.20 -4 0 0 599.44 17.20 4 0 0 588.44 17.60 -5 0 0 14.90 1.90 -5 0 0 16.90 1.70 5 0 0 13.50 1.90 -5 0 0 14.00 1.60 5 0 0 14.80 1.90 -5 0 0 14.80 1.90 5 0 0 14.20 1.60 -5 0 0 16.60 2.00 -5 0 0 12.00 1.80 5 0 0 14.90 1.90 -6 0 0 34.00 4.00 -6 0 0 31.30 3.20 -6 0 0 34.60 3.40 6 0 0 41.80 3.70 -6 0 0 36.80 2.70 6 0 0 33.60 2.90 -6 0 0 33.10 3.10 -6 0 0 33.50 2.70 6 0 0 35.00 3.50 6 0 0 28.40 3.70 -7 0 0 43.20 4.00 7 0 0 45.70 4.50 7 0 0 41.10 3.60 -7 0 0 39.10 3.00 7 0 0 36.50 3.10 -7 0 0 48.00 4.10 -7 0 0 38.90 3.10 -7 0 0 40.70 3.60 7 0 0 42.70 3.70 8 0 0 1.90 3.60 -8 0 0 0.50 1.70 -8 0 0 3.00 1.90 8 0 0 4.90 1.90 8 0 0 3.70 1.90 -8 0 0 3.30 2.00 8 0 0 3.40 2.20 -8 0 0 3.30 2.10 -8 0 0 4.00 1.90 -8 0 0 0.50 2.30 9 0 0 1.70 1.90 -9 0 0 2.10 2.10 9 0 0 2.20 1.90 -9 0 0 -3.20 5.00 9 0 0 -3.10 2.40 -9 0 0 0.90 1.90 9 0 0 -2.60 2.00 -9 0 0 0.60 2.10 -9 0 0 4.50 2.30 1 -1 0 318.17 9.80 -1 -1 0 353.46 9.80 -1 -1 0 339.67 9.80 1 -1 0 352.86 9.80 -1 -1 0 349.67 9.80 1 -1 0 347.07 9.80 1 -1 0 348.07 10.10 1 -1 0 338.27 9.90 -1 -1 0 368.96 9.90 1 1 0 350.36 9.80 -1 1 0 360.16 9.80 1 1 0 338.47 9.80 2 -1 0 4457.15 137.79 2 -1 0 4391.16 137.09 2 1 0 4521.55 136.79 3 -1 0 134.59 4.50 3 -1 0 135.59 4.60 -3 -1 0 134.49 4.50 3 -1 0 127.99 5.00 -3 -1 0 131.69 4.50 3 -1 0 139.19 4.40 -3 -1 0 133.49 4.70 -3 -1 0 137.89 4.50 -3 -1 0 136.29 4.50 3 -1 0 130.39 4.70 -3 1 0 130.69 5.00 3 1 0 141.79 4.50 -3 1 0 133.79 4.60 -3 1 0 141.69 4.30 3 1 0 130.99 4.60 3 1 0 132.49 4.50 -3 1 0 136.69 4.40 3 1 0 134.59 4.50 -3 1 0 132.49 4.60 -3 1 0 132.99 4.50 -4 -1 0 255.57 8.00 -4 -1 0 261.27 8.00 4 -1 0 255.87 8.00 4 -1 0 255.57 8.00 -4 -1 0 257.97 8.00 4 -1 0 251.77 8.60 -4 -1 0 257.87 8.00 -4 -1 0 250.87 8.20 4 -1 0 260.57 7.90 -4 -1 0 251.57 8.20 4 1 0 257.77 8.00 -4 1 0 264.77 7.90 -4 1 0 253.07 8.00 4 1 0 253.37 8.20 -4 1 0 254.17 8.10 -4 1 0 261.37 7.70 4 1 0 250.77 8.00 -4 1 0 256.77 8.20 4 1 0 248.58 8.00 -4 1 0 248.98 8.60 -5 -1 0 37.80 2.50 5 -1 0 35.00 2.40 5 -1 0 39.50 2.70 -5 -1 0 39.70 2.90 -5 -1 0 31.90 2.70 5 -1 0 36.80 3.30 -5 -1 0 35.70 2.70 -5 -1 0 36.20 2.80 5 -1 0 33.10 2.70 -5 -1 0 38.30 2.50 -5 1 0 35.70 2.70 -5 1 0 36.30 2.50 -5 1 0 33.70 3.20 -5 1 0 34.20 2.80 -5 1 0 35.90 2.20 5 1 0 35.20 2.60 5 1 0 36.00 2.60 5 1 0 38.00 3.00 -5 1 0 34.20 2.80 5 1 0 35.90 2.40 -6 -1 0 171.18 6.80 6 -1 0 170.68 6.50 -6 -1 0 172.78 6.30 -6 -1 0 175.88 6.90 6 -1 0 188.78 7.30 6 -1 0 174.88 6.40 6 -1 0 187.48 7.30 -6 -1 0 170.98 6.40 -6 -1 0 178.38 6.30 -6 -1 0 175.88 6.60 -6 1 0 177.78 6.30 -6 1 0 182.68 6.00 -6 1 0 174.78 6.60 6 1 0 178.28 6.90 6 1 0 177.38 6.30 6 1 0 176.48 6.40 -6 1 0 174.38 6.50 6 1 0 164.18 6.80 -6 1 0 162.48 8.00 -6 1 0 172.88 7.20 7 -1 0 118.39 6.20 7 -1 0 118.09 5.30 -7 -1 0 121.49 5.70 -7 -1 0 121.49 5.10 -7 -1 0 111.29 5.30 -7 -1 0 116.59 5.70 7 -1 0 120.49 5.10 7 -1 0 120.09 5.40 -7 -1 0 123.29 5.10 -7 1 0 109.99 5.00 -7 1 0 113.89 4.70 -7 1 0 120.59 5.40 7 1 0 113.59 5.20 7 1 0 114.89 5.30 -7 1 0 116.79 5.40 -7 1 0 126.89 5.70 7 1 0 131.69 6.20 8 -1 0 30.00 3.10 -8 -1 0 39.10 3.40 8 -1 0 40.10 3.10 -8 -1 0 40.50 4.10 8 -1 0 40.20 3.40 -8 -1 0 47.50 4.80 -8 -1 0 38.70 3.80 8 -1 0 36.60 4.70 -8 -1 0 34.70 5.30 8 -1 0 42.70 3.80 -8 -1 0 45.50 3.60 8 1 0 42.70 3.90 -8 1 0 41.30 4.60 8 1 0 38.40 4.70 -8 1 0 34.20 3.00 -8 1 0 45.70 3.50 8 1 0 41.00 3.70 -8 1 0 39.00 3.60 8 1 0 39.20 3.50 -8 1 0 46.00 3.90 -8 1 0 36.60 3.80 -9 -1 0 20.30 2.60 9 -1 0 21.30 2.80 -9 -1 0 31.90 3.70 -9 -1 0 25.00 3.60 -9 -1 0 19.70 2.80 -9 -1 0 24.30 3.20 9 -1 0 17.70 3.40 9 -1 0 22.80 2.80 9 -1 0 15.90 2.50 -9 -1 0 31.50 3.30 -9 1 0 19.80 3.10 -9 1 0 24.00 2.50 9 1 0 22.50 2.90 9 1 0 21.90 3.50 9 1 0 25.10 3.10 -9 1 0 30.10 3.70 -9 1 0 24.30 3.40 -9 1 0 24.40 3.20 9 1 0 25.30 3.30 -9 1 0 22.30 3.10 1 -2 0 1212.58 41.20 1 -2 0 1219.58 41.00 1 2 0 1208.78 39.10 1 2 0 1172.18 38.80 -2 -2 0 825.82 23.50 -2 -2 0 852.81 23.40 2 -2 0 788.12 23.80 2 -2 0 822.72 23.40 2 -2 0 864.51 23.50 -2 -2 0 924.21 24.30 -2 -2 0 797.32 23.40 -2 -2 0 835.42 23.40 2 -2 0 827.62 23.60 2 2 0 825.62 23.40 -2 2 0 829.62 23.50 2 2 0 814.42 23.40 -2 2 0 840.42 23.50 -2 2 0 832.22 24.00 2 2 0 817.02 23.40 -2 2 0 830.92 23.10 -3 -2 0 638.54 17.70 3 -2 0 602.34 18.20 3 -2 0 608.74 17.60 3 -2 0 611.84 17.70 -3 -2 0 613.54 17.60 -3 -2 0 621.44 17.50 3 -2 0 639.64 17.50 -3 -2 0 618.24 17.60 -3 -2 0 620.74 17.60 3 -2 0 597.84 17.60 3 2 0 607.64 17.60 -3 2 0 604.54 18.20 -3 2 0 619.34 17.50 -3 2 0 617.04 17.20 3 2 0 603.84 17.50 -3 2 0 612.64 17.70 3 2 0 567.54 17.50 3 2 0 593.54 17.50 -3 2 0 606.44 17.60 -3 2 0 646.74 18.00 -4 -2 0 13.80 1.40 4 -2 0 17.70 1.70 -4 -2 0 18.50 2.00 4 -2 0 13.80 1.50 -4 -2 0 15.60 1.50 4 -2 0 16.10 1.70 -4 -2 0 16.20 2.00 4 -2 0 15.10 1.90 -4 -2 0 17.50 1.90 -4 2 0 16.60 1.70 4 2 0 17.50 1.90 -4 2 0 13.70 1.60 -4 2 0 17.30 2.60 4 2 0 15.10 1.50 -4 2 0 17.60 1.30 -4 2 0 17.80 1.80 4 2 0 16.20 1.80 -4 2 0 20.90 1.80 -5 -2 0 5.70 1.40 -5 -2 0 5.60 1.40 5 -2 0 5.90 1.60 -5 -2 0 5.80 1.40 5 -2 0 6.90 1.60 -5 -2 0 8.10 1.80 -5 -2 0 3.60 1.30 -5 -2 0 8.90 1.70 5 -2 0 3.70 1.70 5 -2 0 7.50 1.30 5 2 0 5.70 1.30 -5 2 0 7.40 1.60 5 2 0 4.30 1.40 -5 2 0 4.90 1.50 5 2 0 7.40 1.60 -5 2 0 8.00 1.10 -5 2 0 5.10 1.40 -5 2 0 5.10 1.60 -5 2 0 4.60 1.40 5 2 0 5.70 1.30 -6 -2 0 115.39 5.00 -6 -2 0 108.19 5.20 -6 -2 0 120.09 5.00 6 -2 0 113.79 4.90 -6 -2 0 114.39 5.10 6 -2 0 114.49 5.90 6 -2 0 127.39 6.00 6 -2 0 115.59 5.00 -6 -2 0 111.29 4.80 -6 -2 0 112.19 4.80 -6 2 0 113.29 5.10 -6 2 0 117.09 6.10 6 2 0 113.29 4.80 -6 2 0 117.59 5.80 6 2 0 117.79 5.40 -6 2 0 108.89 4.20 6 2 0 117.89 4.70 6 2 0 111.19 4.80 -6 2 0 113.39 4.70 -6 2 0 120.59 5.00 7 -2 0 50.09 3.70 -7 -2 0 49.50 5.60 7 -2 0 50.99 3.90 7 -2 0 61.39 7.40 -7 -2 0 55.99 3.60 -7 -2 0 50.89 3.80 7 -2 0 52.99 3.50 -7 -2 0 53.39 3.60 7 -2 0 56.49 3.40 -7 -2 0 48.10 3.70 -7 2 0 54.69 4.30 7 2 0 57.49 3.70 -7 2 0 54.39 2.90 -7 2 0 53.19 4.60 -7 2 0 54.19 3.80 -7 2 0 51.79 3.90 -7 2 0 53.39 3.50 8 -2 0 1.30 1.80 -8 -2 0 -1.40 2.30 -8 -2 0 -3.00 2.00 -8 -2 0 -0.40 2.40 8 -2 0 -1.10 1.90 8 -2 0 -0.10 2.10 -8 -2 0 1.30 1.70 -8 -2 0 -1.20 1.70 8 -2 0 1.40 2.00 -8 -2 0 3.00 2.30 8 2 0 2.10 1.90 -8 2 0 -0.70 2.20 -8 2 0 3.40 2.10 8 2 0 1.90 2.20 -8 2 0 -0.40 2.10 8 2 0 0.60 2.00 -8 2 0 0.20 1.30 8 2 0 1.90 1.90 -8 2 0 1.90 2.20 -8 2 0 1.00 1.80 -9 -2 0 2.50 2.00 -9 -2 0 -0.50 2.80 -9 -2 0 -0.50 2.10 -9 -2 0 2.20 2.10 9 -2 0 2.50 2.30 -9 -2 0 0.60 1.90 9 -2 0 -1.10 2.00 9 -2 0 -3.60 2.50 9 -2 0 0.60 2.20 -9 -2 0 1.70 2.10 -9 2 0 2.70 2.40 -9 2 0 1.40 2.20 -9 2 0 0.50 1.50 9 2 0 -0.30 2.50 9 2 0 -1.10 2.30 -9 2 0 -0.80 3.00 -9 2 0 1.40 2.80 9 2 0 1.30 4.80 -9 2 0 3.60 2.40 9 2 0 0.50 1.90 0 -3 0 0.10 0.50 0 -3 0 0.00 0.80 0 -3 0 0.40 0.70 0 -3 0 -0.20 0.60 0 3 0 0.80 0.90 -1 -3 0 132.09 4.20 -1 -3 0 128.39 3.80 1 -3 0 131.39 4.80 1 -3 0 122.69 4.30 -1 -3 0 132.49 4.20 1 -3 0 128.39 3.90 1 -3 0 131.69 4.10 1 -3 0 127.49 3.70 -1 -3 0 128.49 3.80 1 -3 0 126.49 3.90 -1 3 0 126.69 4.40 -1 3 0 121.89 3.90 -1 3 0 129.39 3.90 -1 3 0 135.89 4.10 -1 3 0 125.69 4.70 1 3 0 129.19 4.20 2 -3 0 66.19 2.30 2 -3 0 64.39 2.70 2 -3 0 62.39 2.80 -2 -3 0 58.09 2.50 2 -3 0 62.69 2.50 2 -3 0 62.79 3.40 -2 -3 0 58.59 2.40 -2 -3 0 63.59 2.30 -2 -3 0 64.69 2.50 -2 -3 0 64.19 2.70 2 -3 0 62.19 2.50 2 3 0 62.69 2.30 -2 3 0 61.99 2.60 2 3 0 56.79 2.40 2 3 0 60.69 2.30 -2 3 0 60.39 2.40 -2 3 0 58.49 3.20 -2 3 0 65.09 2.50 -3 -3 0 294.27 8.80 -3 -3 0 297.07 9.10 -3 -3 0 307.87 8.80 -3 -3 0 299.77 8.80 3 -3 0 294.57 8.90 3 -3 0 295.57 8.90 3 -3 0 287.57 9.00 3 -3 0 306.37 8.80 3 -3 0 285.57 9.00 -3 -3 0 287.47 8.90 3 -3 0 298.87 9.80 -3 3 0 285.67 8.80 -3 3 0 286.17 8.30 -3 3 0 288.17 9.70 3 3 0 288.97 8.70 -3 3 0 298.87 8.90 3 3 0 280.87 8.70 -3 3 0 303.07 9.10 3 3 0 292.07 8.70 -4 -3 0 70.89 3.10 4 -3 0 72.79 2.90 4 -3 0 65.79 4.10 4 -3 0 73.09 3.50 -4 -3 0 66.59 3.10 4 -3 0 67.59 3.10 -4 -3 0 68.09 3.10 4 -3 0 65.99 3.20 4 -3 0 71.19 3.20 -4 -3 0 73.89 3.30 -4 -3 0 66.29 3.50 -4 3 0 70.09 4.00 4 3 0 67.69 3.00 -4 3 0 68.89 3.20 -4 3 0 68.69 3.30 4 3 0 69.99 3.10 4 3 0 66.89 3.10 -4 3 0 76.29 3.30 -4 3 0 66.39 2.40 5 -3 0 14.70 2.30 -5 -3 0 16.70 1.90 -5 -3 0 16.50 1.80 5 -3 0 18.10 2.20 5 -3 0 13.90 1.60 -5 -3 0 18.90 2.10 5 -3 0 14.70 1.90 -5 -3 0 15.60 1.80 -5 -3 0 14.20 2.20 5 -3 0 19.10 2.00 5 -3 0 19.10 2.20 -5 3 0 16.20 1.90 -5 3 0 17.40 1.90 -5 3 0 18.30 2.40 -5 3 0 16.00 2.00 5 3 0 13.50 1.60 5 3 0 18.10 1.90 5 3 0 14.70 1.70 5 3 0 15.70 1.80 -5 3 0 19.50 2.20 -6 -3 0 24.20 2.60 6 -3 0 19.40 2.80 6 -3 0 20.50 2.30 6 -3 0 21.20 2.30 -6 -3 0 23.00 2.70 6 -3 0 19.70 2.10 -6 -3 0 18.30 2.40 -6 -3 0 21.90 2.40 -6 -3 0 20.90 2.30 -6 -3 0 18.90 2.30 -6 3 0 17.80 2.20 6 3 0 24.10 2.60 -6 3 0 22.60 2.60 6 3 0 27.20 2.50 6 3 0 22.10 2.10 -6 3 0 20.20 1.80 -6 3 0 20.40 2.40 -6 3 0 18.10 3.10 7 -3 0 10.20 1.80 -7 -3 0 11.00 2.00 7 -3 0 8.00 2.30 7 -3 0 9.50 1.90 7 -3 0 14.00 2.50 7 -3 0 13.70 2.50 -7 -3 0 13.20 2.20 -7 -3 0 10.00 2.40 -7 -3 0 14.90 2.50 -7 -3 0 9.10 1.90 7 3 0 9.40 1.90 -7 3 0 6.90 1.60 -7 3 0 11.80 1.50 -7 3 0 11.60 2.50 7 3 0 16.00 2.40 -7 3 0 10.60 2.50 -7 3 0 14.60 2.40 -8 -3 0 16.60 3.10 -8 -3 0 10.10 2.40 -8 -3 0 15.00 2.50 8 -3 0 12.90 3.00 8 -3 0 10.90 2.50 -8 -3 0 19.80 3.10 8 -3 0 13.20 2.20 -8 -3 0 13.80 2.40 8 -3 0 13.00 2.20 -8 -3 0 15.80 2.30 8 3 0 19.30 2.70 8 3 0 16.60 2.60 -8 3 0 13.00 2.80 8 3 0 13.80 2.50 -8 3 0 13.80 2.40 -8 3 0 13.10 2.80 -8 3 0 14.10 2.30 8 3 0 14.90 2.60 -8 3 0 14.30 1.70 9 -3 0 4.50 2.90 9 -3 0 13.20 2.50 -9 -3 0 14.00 3.20 -9 -3 0 8.00 2.50 -9 -3 0 16.40 3.00 -9 -3 0 5.50 2.20 9 -3 0 7.00 2.20 -9 -3 0 9.50 2.50 9 -3 0 10.50 2.70 9 3 0 9.60 2.30 -9 3 0 8.90 3.50 9 3 0 9.40 2.80 -9 3 0 11.00 5.00 -9 3 0 7.70 1.60 -9 3 0 11.20 2.80 -9 3 0 11.00 2.60 0 -4 0 418.66 13.00 0 -4 0 432.36 12.50 0 -4 0 461.85 12.60 0 -4 0 438.06 12.80 0 4 0 428.76 12.80 1 -4 0 742.03 21.30 1 -4 0 763.92 21.40 -1 -4 0 745.13 21.70 1 -4 0 756.52 21.90 -1 -4 0 753.92 21.80 1 -4 0 783.22 21.70 1 -4 0 742.73 21.40 1 -4 0 782.62 22.40 -1 4 0 762.32 21.40 -1 4 0 767.42 22.00 -1 4 0 831.72 22.30 -1 4 0 772.52 22.30 1 4 0 735.63 21.80 2 -4 0 202.08 7.30 2 -4 0 196.78 6.60 -2 -4 0 213.08 6.60 -2 -4 0 204.48 6.40 2 -4 0 202.28 6.20 -2 -4 0 209.18 6.10 2 -4 0 206.28 6.50 2 -4 0 205.58 6.20 -2 -4 0 201.98 6.10 -2 4 0 202.88 7.20 -2 4 0 201.88 6.20 2 4 0 202.28 6.00 -2 4 0 205.78 6.40 2 4 0 204.38 6.40 2 4 0 206.08 6.10 -2 4 0 203.28 6.20 -3 -4 0 368.66 10.90 3 -4 0 367.26 11.00 -3 -4 0 348.37 10.60 3 -4 0 361.86 10.80 -3 -4 0 374.46 10.70 3 -4 0 351.16 11.10 -3 -4 0 372.46 11.10 3 -4 0 379.06 10.70 -3 -4 0 353.26 10.60 3 -4 0 369.76 11.90 3 4 0 364.56 10.60 3 4 0 360.26 10.60 -3 4 0 347.47 11.80 -3 4 0 366.76 10.80 3 4 0 354.26 10.70 -3 4 0 367.06 10.80 -3 4 0 362.26 11.00 4 -4 0 55.79 3.10 4 -4 0 61.29 2.70 4 -4 0 57.59 3.10 4 -4 0 58.49 4.10 -4 -4 0 56.99 2.90 4 -4 0 59.49 2.90 4 -4 0 55.19 3.00 -4 -4 0 56.09 3.10 -4 -4 0 56.49 2.80 -4 -4 0 57.99 2.70 -4 -4 0 58.39 2.90 4 4 0 56.59 2.60 -4 4 0 58.29 3.90 -4 4 0 59.49 3.00 -4 4 0 58.19 3.10 4 4 0 56.79 2.70 -4 4 0 55.39 1.80 -4 4 0 57.69 2.90 4 4 0 55.99 2.70 5 -4 0 11.30 2.40 5 -4 0 9.30 1.70 -5 -4 0 14.90 2.00 -5 -4 0 9.40 1.50 5 -4 0 10.10 2.00 5 -4 0 10.00 1.40 5 -4 0 17.40 2.10 -5 -4 0 11.90 1.80 -5 -4 0 13.50 2.00 -5 -4 0 11.50 1.50 5 -4 0 12.20 1.90 -5 4 0 7.90 1.60 -5 4 0 9.10 1.50 5 4 0 14.40 1.50 -5 4 0 10.40 2.10 -5 4 0 11.10 1.80 -5 4 0 11.90 1.10 5 4 0 11.80 1.60 5 4 0 11.60 1.70 6 -4 0 33.40 3.10 6 -4 0 34.70 4.30 -6 -4 0 38.10 3.20 -6 -4 0 38.00 2.80 -6 -4 0 33.90 3.40 6 -4 0 31.90 3.30 6 -4 0 36.80 3.00 -6 -4 0 30.50 3.00 6 -4 0 32.90 3.10 -6 -4 0 41.20 3.00 6 4 0 35.30 2.90 -6 4 0 31.10 3.20 6 4 0 34.40 3.20 -6 4 0 32.20 3.10 6 4 0 37.10 2.40 -6 4 0 34.80 4.20 -7 -4 0 17.30 2.70 -7 -4 0 16.80 2.50 7 -4 0 14.70 2.10 7 -4 0 18.50 2.60 -7 -4 0 14.90 2.60 -7 -4 0 12.20 2.10 7 -4 0 11.20 2.20 -7 -4 0 17.30 2.60 -7 -4 0 12.70 2.30 7 -4 0 12.50 2.90 -7 4 0 11.80 2.90 7 4 0 19.40 2.30 -7 4 0 14.10 1.70 7 4 0 16.20 2.20 -8 -4 0 4.10 1.70 -8 -4 0 -1.30 1.90 -8 -4 0 3.90 2.00 8 -4 0 0.40 2.40 8 -4 0 1.00 1.70 -8 -4 0 6.90 2.50 -8 -4 0 1.40 3.10 8 -4 0 2.50 2.00 8 -4 0 4.30 2.20 -8 -4 0 2.50 2.30 -8 4 0 3.30 2.10 -8 4 0 1.20 2.30 8 4 0 3.60 2.40 -8 4 0 3.40 1.90 8 4 0 4.50 3.20 -8 4 0 1.70 2.70 -8 4 0 3.00 1.20 0 -5 0 0.20 0.70 0 -5 0 -1.80 0.80 0 -5 0 -0.30 0.90 0 -5 0 0.90 1.10 0 5 0 -0.10 1.30 -1 -5 0 1234.08 35.00 1 -5 0 1210.58 35.00 -1 -5 0 1181.68 34.70 1 -5 0 1279.47 35.50 1 -5 0 1194.18 34.40 1 -5 0 1220.68 34.40 -1 -5 0 1234.88 34.90 1 -5 0 1255.97 34.30 1 -5 0 1231.18 34.70 1 5 0 1228.88 34.90 -1 5 0 1247.58 34.80 -1 5 0 1325.77 35.90 -1 5 0 1190.38 34.30 2 -5 0 300.17 9.70 -2 -5 0 312.97 9.50 -2 -5 0 297.57 8.90 2 -5 0 308.47 9.40 2 -5 0 325.57 10.50 2 -5 0 313.17 9.10 -2 -5 0 318.47 9.40 -2 -5 0 302.97 9.30 2 -5 0 308.57 9.10 -2 -5 0 312.17 8.90 -2 5 0 320.07 9.10 -2 5 0 303.47 9.00 -2 5 0 308.87 9.40 2 5 0 300.17 8.90 2 5 0 316.17 9.50 -2 5 0 292.07 10.20 3 -5 0 8.20 1.30 -3 -5 0 5.10 1.20 -3 -5 0 5.80 1.10 3 -5 0 4.60 1.70 -3 -5 0 5.90 1.10 3 -5 0 5.90 1.10 -3 -5 0 8.10 1.10 3 -5 0 9.10 1.60 -3 -5 0 6.90 1.60 3 -5 0 8.10 1.20 3 -5 0 7.40 1.40 -3 5 0 5.70 1.20 -3 5 0 7.00 1.80 3 5 0 7.10 1.00 3 5 0 5.80 1.00 -3 5 0 6.50 1.10 3 5 0 7.30 1.30 -3 5 0 6.80 1.20 4 -5 0 124.59 4.60 -4 -5 0 125.09 4.50 4 -5 0 120.59 6.00 -4 -5 0 123.99 4.70 -4 -5 0 117.89 4.30 4 -5 0 123.89 4.40 4 -5 0 116.29 4.90 -4 -5 0 123.19 4.40 4 -5 0 125.19 4.90 -4 -5 0 127.99 5.00 4 -5 0 122.49 4.70 -4 5 0 125.69 4.70 -4 5 0 121.59 5.80 4 5 0 121.89 4.40 -4 5 0 122.39 4.80 4 5 0 125.39 4.40 -4 5 0 119.79 4.60 4 5 0 120.59 4.40 -5 -5 0 99.19 4.30 5 -5 0 104.29 4.80 5 -5 0 104.89 4.40 5 -5 0 104.69 4.60 -5 -5 0 112.59 5.10 -5 -5 0 103.59 4.40 5 -5 0 100.49 4.60 -5 -5 0 104.19 4.50 5 -5 0 110.79 6.10 5 -5 0 104.39 4.20 5 5 0 105.19 4.20 -5 5 0 99.19 4.40 -5 5 0 105.89 5.90 5 5 0 102.99 4.10 -5 5 0 105.89 4.50 -5 5 0 105.19 4.70 5 5 0 107.09 4.50 6 -5 0 5.70 1.70 -6 -5 0 3.70 1.80 6 -5 0 4.30 1.80 6 -5 0 3.90 2.40 -6 -5 0 1.20 1.90 -6 -5 0 3.00 1.70 -6 -5 0 1.00 1.80 -6 -5 0 3.40 1.20 6 -5 0 1.70 2.30 6 -5 0 1.80 1.70 -6 5 0 0.10 1.60 -6 5 0 1.80 1.50 6 5 0 3.10 1.70 6 5 0 2.60 1.70 -6 5 0 3.60 2.20 6 5 0 2.80 1.30 -7 -5 0 17.60 2.70 -7 -5 0 21.40 2.70 7 -5 0 13.80 2.00 -7 -5 0 17.10 3.10 7 -5 0 18.90 2.70 -7 -5 0 20.10 2.50 -7 -5 0 17.80 2.50 -7 -5 0 21.00 2.80 7 -5 0 11.60 2.70 7 -5 0 14.50 2.50 -7 5 0 18.90 2.70 -7 5 0 17.50 1.30 -7 5 0 13.00 2.70 7 5 0 17.60 2.40 7 5 0 17.30 2.30 8 -5 0 8.60 2.10 -8 -5 0 4.00 2.20 -8 -5 0 4.00 1.50 8 -5 0 5.00 2.40 -8 -5 0 2.40 2.70 -8 -5 0 4.30 2.20 8 -5 0 4.00 2.80 -8 -5 0 4.00 2.60 -8 -5 0 1.90 3.10 -8 5 0 2.00 2.10 -8 5 0 2.10 2.70 8 5 0 8.10 2.30 8 5 0 7.40 2.30 8 5 0 7.20 2.10 -8 5 0 3.80 2.10 -8 5 0 7.30 2.60 0 -6 0 205.68 7.00 0 -6 0 213.08 7.40 0 -6 0 209.38 6.70 0 -6 0 205.68 6.50 0 6 0 212.68 7.10 1 -6 0 36.00 3.30 -1 -6 0 38.50 2.30 1 -6 0 38.90 2.70 -1 -6 0 34.00 2.50 -1 -6 0 40.20 2.80 1 -6 0 42.40 1.70 1 -6 0 36.80 2.20 -1 -6 0 36.50 2.20 -1 6 0 42.40 2.30 1 6 0 34.70 2.70 -1 6 0 35.20 3.00 2 -6 0 100.49 3.40 -2 -6 0 99.29 4.00 -2 -6 0 99.19 3.70 -2 -6 0 98.39 3.90 2 -6 0 96.89 3.80 2 -6 0 100.99 5.00 2 -6 0 96.19 3.30 -2 -6 0 88.79 4.30 2 -6 0 90.69 5.30 -2 6 0 99.19 3.80 -2 6 0 100.79 4.80 -2 6 0 98.09 3.40 2 6 0 94.69 4.10 -2 6 0 95.19 3.40 -3 -6 0 26.80 1.80 -3 -6 0 26.40 2.20 -3 -6 0 26.70 1.80 3 -6 0 24.40 2.30 -3 -6 0 27.40 2.40 3 -6 0 27.90 2.00 3 -6 0 27.80 2.20 3 -6 0 26.90 2.40 3 -6 0 24.30 1.90 -3 6 0 24.40 2.10 -3 6 0 26.20 2.30 3 6 0 23.00 1.70 3 6 0 22.40 1.60 -3 6 0 28.30 3.30 3 6 0 26.40 2.80 -3 6 0 25.00 2.00 4 -6 0 4.50 1.30 4 -6 0 5.80 1.60 4 -6 0 2.60 1.20 -4 -6 0 3.70 1.30 4 -6 0 3.10 1.30 -4 -6 0 3.70 1.40 -4 -6 0 5.50 1.70 -4 -6 0 3.60 1.30 -4 -6 0 4.00 1.10 4 -6 0 3.30 2.10 4 6 0 4.00 1.20 -4 6 0 4.50 1.60 -4 6 0 5.40 1.60 4 6 0 6.00 1.50 -4 6 0 0.30 3.10 -4 6 0 2.00 1.40 4 6 0 4.20 1.20 -5 -6 0 6.90 1.40 -5 -6 0 8.80 1.60 5 -6 0 9.10 2.10 5 -6 0 12.10 2.00 5 -6 0 7.10 2.40 -5 -6 0 6.30 1.80 5 -6 0 9.10 1.90 5 -6 0 10.50 1.70 -5 -6 0 9.50 1.70 -5 6 0 6.30 1.70 -5 6 0 13.70 2.00 5 6 0 9.10 1.70 -5 6 0 8.10 1.80 5 6 0 9.80 1.60 5 6 0 10.60 1.90 -6 -6 0 37.40 3.40 6 -6 0 43.30 3.30 6 -6 0 41.20 3.70 -6 -6 0 41.40 3.20 6 -6 0 41.70 3.90 -6 -6 0 43.00 3.40 6 -6 0 37.40 4.80 6 -6 0 41.60 3.00 -6 -6 0 39.80 3.50 6 6 0 43.00 3.10 6 6 0 44.40 2.90 -6 6 0 39.40 3.30 -6 6 0 41.10 4.70 -6 6 0 36.70 3.50 -7 -6 0 9.10 2.50 7 -6 0 10.10 2.40 -7 -6 0 7.80 2.10 -7 -6 0 5.10 2.10 7 -6 0 8.40 1.90 -7 -6 0 7.80 2.20 -7 -6 0 4.50 2.60 -7 -6 0 7.30 1.60 7 -6 0 10.10 2.60 7 -6 0 5.50 2.70 7 6 0 9.90 1.70 -7 6 0 4.60 2.20 7 6 0 7.80 2.20 -7 6 0 5.00 2.80 -7 6 0 6.10 2.20 7 6 0 6.30 1.90 8 -6 0 -0.10 2.50 -8 -6 0 -0.70 2.00 -8 -6 0 3.10 2.30 8 -6 0 1.30 2.00 8 -6 0 -0.60 2.00 -8 -6 0 1.50 2.10 -8 -6 0 -1.90 2.50 -8 -6 0 2.00 1.30 -8 -6 0 1.10 2.20 8 -6 0 2.10 2.40 -8 6 0 2.40 2.70 8 6 0 0.30 2.10 8 6 0 0.40 1.40 -8 6 0 -2.40 3.40 8 6 0 -0.40 1.80 -8 6 0 0.00 3.40 -8 6 0 1.10 2.30 0 -7 0 -0.70 1.20 0 -7 0 -0.10 1.70 0 -7 0 -0.10 1.00 0 -7 0 0.80 0.80 0 7 0 -2.90 1.30 -1 -7 0 74.19 3.30 1 -7 0 79.49 2.80 1 -7 0 77.99 3.30 -1 -7 0 74.79 3.30 1 -7 0 79.39 4.50 -1 -7 0 82.89 3.90 1 -7 0 75.19 3.80 -1 -7 0 75.59 3.70 -1 7 0 72.69 4.00 -1 7 0 75.89 3.30 1 7 0 75.69 3.80 2 -7 0 126.99 3.80 2 -7 0 132.69 6.20 -2 -7 0 132.69 5.00 -2 -7 0 129.79 4.90 -2 -7 0 126.99 5.00 2 -7 0 132.09 4.30 -2 -7 0 126.59 4.60 2 -7 0 128.79 4.80 2 -7 0 125.49 4.10 2 -7 0 119.29 5.10 -2 7 0 124.99 4.70 2 7 0 131.49 5.10 -2 7 0 129.29 4.20 -3 -7 0 21.20 2.30 3 -7 0 17.30 1.90 -3 -7 0 18.60 1.50 3 -7 0 20.30 1.70 3 -7 0 24.10 2.20 3 -7 0 18.70 2.00 -3 -7 0 17.70 2.00 3 -7 0 16.70 2.80 -3 7 0 18.30 2.00 -3 7 0 19.20 2.80 3 7 0 19.40 1.50 -3 7 0 19.80 2.30 3 7 0 18.40 2.00 -3 7 0 18.40 2.10 -4 -7 0 94.29 3.70 4 -7 0 94.49 4.40 -4 -7 0 87.79 4.10 -4 -7 0 91.79 4.80 4 -7 0 99.09 3.80 -4 -7 0 89.69 3.60 4 -7 0 94.49 3.90 4 -7 0 96.19 4.00 4 -7 0 84.19 5.70 -4 7 0 88.09 5.70 4 7 0 92.39 4.20 -4 7 0 95.29 5.70 -4 7 0 91.49 4.20 4 7 0 90.69 3.70 -4 7 0 77.69 5.60 4 7 0 91.99 3.50 5 -7 0 25.80 2.60 -5 -7 0 23.90 2.00 -5 -7 0 26.20 3.80 -5 -7 0 20.30 2.40 5 -7 0 28.00 2.90 5 -7 0 21.20 3.30 5 -7 0 28.60 2.60 5 -7 0 30.60 3.10 -5 -7 0 28.00 2.80 5 7 0 28.80 2.70 5 7 0 26.10 2.40 -5 7 0 29.00 2.70 5 7 0 28.00 2.90 -5 7 0 27.80 2.50 -5 7 0 22.60 3.90 6 -7 0 4.40 2.50 6 -7 0 6.40 1.80 6 -7 0 4.40 1.80 -6 -7 0 5.60 1.80 -6 -7 0 6.20 2.20 -6 -7 0 4.00 1.70 6 -7 0 5.20 2.00 6 -7 0 3.80 2.30 6 7 0 5.80 1.70 -6 7 0 3.70 2.00 6 7 0 6.40 1.70 -6 7 0 3.70 1.90 -6 7 0 2.90 2.70 -6 7 0 4.10 2.00 -7 -7 0 22.70 3.00 7 -7 0 21.40 4.50 7 -7 0 17.80 3.30 -7 -7 0 19.80 2.90 7 -7 0 21.00 2.40 -7 -7 0 24.20 2.60 -7 -7 0 19.40 2.60 7 -7 0 14.90 2.10 -7 7 0 28.30 3.30 7 7 0 29.00 2.80 -7 7 0 15.20 3.20 -7 7 0 20.70 2.70 7 7 0 22.60 2.20 -7 7 0 19.80 2.50 7 7 0 20.50 2.30 0 -8 0 17.50 2.30 0 -8 0 15.90 2.20 0 -8 0 15.10 1.70 0 -8 0 19.00 1.90 0 8 0 13.40 2.10 -1 -8 0 6.30 1.30 1 -8 0 5.40 1.00 -1 -8 0 7.40 1.50 1 -8 0 5.50 2.10 -1 -8 0 5.90 1.60 1 -8 0 5.40 1.40 -1 -8 0 6.10 1.70 1 8 0 8.10 2.00 -1 8 0 6.00 2.10 2 -8 0 50.49 2.30 -2 -8 0 46.00 3.20 -2 -8 0 53.19 2.90 2 -8 0 47.10 3.00 -2 -8 0 46.60 3.10 2 -8 0 47.20 4.50 -2 -8 0 48.00 3.00 -2 -8 0 49.20 3.30 2 -8 0 46.80 1.80 -2 8 0 49.30 3.00 2 8 0 52.59 3.70 -3 -8 0 46.20 3.30 3 -8 0 49.50 5.20 -3 -8 0 44.40 3.00 -3 -8 0 44.50 2.90 3 -8 0 43.40 2.50 3 -8 0 45.60 3.20 3 -8 0 46.30 2.70 3 8 0 44.00 3.50 -3 8 0 45.20 3.10 -3 8 0 42.80 2.50 -3 8 0 42.00 2.70 4 -8 0 81.89 4.20 -4 -8 0 77.89 3.20 4 -8 0 85.79 6.10 -4 -8 0 75.39 3.70 -4 -8 0 71.09 4.10 -4 -8 0 84.29 5.40 4 -8 0 79.69 3.60 -4 -8 0 80.29 4.40 -4 8 0 80.79 3.70 4 8 0 79.39 3.20 -4 8 0 76.49 4.10 -4 8 0 85.69 3.90 4 8 0 82.59 4.20 5 -8 0 11.20 2.90 5 -8 0 11.30 1.80 -5 -8 0 12.00 2.00 5 -8 0 15.70 3.80 -5 -8 0 11.60 1.60 -5 -8 0 7.60 2.10 5 -8 0 10.90 2.90 -5 -8 0 11.70 1.70 5 -8 0 11.40 2.00 -5 8 0 15.40 2.20 -5 8 0 17.50 2.20 5 8 0 14.90 1.70 5 8 0 13.70 1.80 5 8 0 12.40 2.00 -6 -8 0 7.90 1.70 6 -8 0 7.30 2.80 -6 -8 0 8.90 2.30 6 -8 0 7.30 1.80 6 -8 0 5.00 1.60 -6 -8 0 7.10 2.10 -6 -8 0 8.60 2.70 6 -8 0 6.30 2.00 6 -8 0 11.90 2.60 -6 8 0 5.20 1.80 -6 8 0 8.40 2.20 6 8 0 8.10 1.70 -6 8 0 5.80 3.50 6 8 0 9.30 2.00 -7 -8 0 -0.30 1.60 7 -8 0 1.30 2.00 7 -8 0 1.50 2.80 -7 -8 0 -1.00 1.90 7 -8 0 1.60 1.70 -7 -8 0 -0.20 2.70 -7 -8 0 1.20 1.90 7 -8 0 2.10 1.60 7 8 0 -4.10 4.80 -7 8 0 1.10 2.00 -7 8 0 1.00 2.10 7 8 0 0.60 1.70 7 8 0 -1.00 1.60 -7 8 0 2.00 1.90 0 -9 0 -0.40 1.30 0 -9 0 -1.10 1.70 0 -9 0 0.00 1.10 0 9 0 -3.30 1.70 -1 -9 0 112.79 4.50 1 -9 0 107.19 3.90 -1 -9 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52.79 3.10 -3 4 -4 54.89 3.60 3 4 4 46.80 3.50 3 4 4 50.39 3.50 -4 -4 -4 158.28 7.90 4 -4 4 141.39 5.90 -4 -4 -4 156.08 6.00 -4 -4 -4 157.28 6.20 -4 -4 -4 161.68 6.50 4 -4 4 158.28 7.00 4 -4 4 147.19 5.30 4 -4 4 147.29 8.00 -4 -4 -4 151.68 6.40 4 4 4 144.59 6.20 4 4 4 156.38 5.90 4 4 4 152.98 6.00 -4 4 -4 155.48 5.40 -4 4 -4 149.99 6.00 -4 4 -4 147.49 6.20 5 -4 4 29.50 3.20 -5 -4 -4 25.40 2.60 -5 -4 -4 24.60 3.00 -5 -4 -4 23.90 2.70 -5 -4 -4 21.40 3.50 -5 -4 -4 23.00 2.80 5 -4 4 22.30 2.50 5 -4 4 24.30 3.90 5 4 4 28.30 2.90 -5 4 -4 18.80 2.30 -5 4 -4 25.20 2.40 -5 4 -4 17.50 3.20 -5 4 -4 25.40 3.00 5 4 4 19.80 2.30 -5 4 -4 25.70 3.20 6 -4 4 16.50 2.80 6 -4 4 14.70 4.20 -6 -4 -4 19.90 4.90 6 -4 4 21.50 3.00 -6 -4 -4 15.80 3.30 -6 -4 -4 14.50 2.60 -6 -4 -4 16.20 2.70 -6 -4 -4 18.10 3.20 6 -4 4 13.40 2.30 6 4 4 11.40 2.20 -6 4 -4 15.70 1.90 -6 4 -4 23.50 3.40 -6 4 -4 19.30 2.90 -6 4 -4 16.20 3.50 6 4 4 21.90 3.10 6 4 4 11.20 2.20 -6 4 -4 12.90 2.80 9 -5 -4 18.50 4.60 -9 -5 4 21.50 2.90 9 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6.30 5 -5 -4 157.68 5.80 5 -5 -4 151.18 7.20 5 -5 -4 159.58 6.00 -5 -5 4 156.18 5.60 -5 -5 4 159.68 5.50 -5 -5 4 159.78 5.00 -5 -5 4 153.08 5.50 -5 5 4 157.78 5.70 -5 5 4 155.68 7.20 -5 5 4 158.48 5.30 -5 5 4 161.28 6.20 -5 5 4 155.88 6.40 5 5 -4 150.78 5.50 5 5 -4 171.78 5.80 -4 -5 4 56.79 2.80 -4 -5 4 59.19 2.90 4 -5 -4 55.29 2.70 -4 -5 4 56.59 2.60 -4 -5 4 54.59 2.60 4 -5 -4 53.39 3.70 4 -5 -4 57.29 3.10 4 -5 -4 59.59 3.40 4 -5 -4 61.19 3.20 -4 5 4 61.49 2.90 4 5 -4 55.29 3.00 4 5 -4 56.09 2.50 -4 5 4 58.39 3.60 -4 5 4 55.89 3.30 -4 5 4 63.49 2.70 4 5 -4 53.59 2.90 -4 5 4 56.69 3.00 3 -5 -4 216.88 6.90 -3 -5 4 216.58 6.30 3 -5 -4 212.08 6.90 3 -5 -4 212.48 6.80 -3 -5 4 217.28 6.70 -3 -5 4 210.98 6.80 3 -5 -4 203.38 7.50 -3 -5 4 196.48 6.80 -3 5 4 212.38 6.80 -3 5 4 213.78 7.10 3 5 -4 224.18 6.80 3 5 -4 217.78 6.80 3 5 -4 205.68 7.00 -3 5 4 221.08 7.50 -3 5 4 210.88 7.40 -3 5 4 216.08 6.80 2 -5 -4 279.37 8.90 2 -5 -4 273.57 9.30 -2 -5 4 290.17 8.70 -2 -5 4 287.27 9.30 -2 -5 4 278.37 8.60 2 -5 -4 284.57 8.70 2 -5 -4 252.57 9.10 -2 5 4 284.97 8.60 2 5 -4 288.67 8.70 -2 5 4 292.57 9.30 -2 5 4 292.57 8.70 2 5 -4 290.27 9.30 -2 5 4 293.27 8.90 2 5 -4 277.77 8.70 -1 -5 4 2.50 2.30 -1 -5 4 2.30 1.00 -1 -5 4 2.70 1.50 -1 -5 4 3.60 1.10 1 -5 -4 3.80 1.70 1 -5 -4 3.10 1.20 1 -5 -4 3.20 1.20 1 -5 -4 2.30 1.10 1 5 -4 2.50 1.20 -1 5 4 5.20 1.30 1 5 -4 2.30 1.20 1 5 -4 3.20 1.40 -1 5 4 3.20 1.10 -1 5 4 2.50 1.60 -1 5 4 2.40 1.20 0 -5 -4 364.66 11.90 0 -5 -4 396.56 12.00 0 -5 4 371.76 11.10 0 -5 -4 362.86 11.10 0 -5 4 371.66 11.20 0 -5 4 365.06 11.00 0 -5 -4 365.86 11.50 0 -5 4 384.36 12.30 0 5 -4 371.76 11.20 0 5 4 368.16 11.10 0 5 4 375.56 11.80 0 5 -4 370.26 12.30 0 5 4 354.66 11.40 0 5 -4 367.56 11.20 0 5 4 369.46 11.10 0 5 4 362.46 10.70 1 -5 4 17.70 2.50 -1 -5 -4 16.90 1.80 -1 -5 -4 16.90 1.80 -1 -5 -4 21.90 2.10 1 -5 4 19.10 1.70 1 -5 4 21.60 2.40 -1 -5 -4 23.10 2.60 1 -5 4 20.60 2.10 -1 -5 -4 15.60 2.10 1 5 4 16.90 1.70 -1 5 -4 22.00 2.40 1 5 4 12.70 2.00 -1 5 -4 18.80 1.40 1 5 4 17.90 2.00 -1 5 -4 18.10 2.60 -1 5 -4 19.00 2.00 1 5 4 21.30 2.30 1 5 4 17.70 1.70 2 -5 4 315.57 9.50 2 -5 4 284.87 13.20 -2 -5 -4 332.27 10.90 -2 -5 -4 310.27 9.90 2 -5 4 319.27 10.10 -2 -5 -4 292.37 11.20 2 -5 4 276.57 11.50 -2 -5 -4 330.67 10.00 -2 -5 -4 317.67 9.80 2 5 4 319.17 9.80 -2 5 -4 326.47 9.60 2 5 4 308.07 10.20 -2 5 -4 331.87 11.60 2 5 4 327.17 9.90 2 5 4 315.07 9.90 -2 5 -4 327.37 10.20 -2 5 -4 310.67 10.00 3 -5 4 113.89 4.10 -3 -5 -4 128.39 4.90 3 -5 4 116.29 5.10 -3 -5 -4 112.99 5.40 3 -5 4 120.69 5.00 -3 -5 -4 115.69 4.90 -3 -5 -4 123.19 5.10 3 -5 4 112.89 6.60 3 -5 4 115.39 5.20 -3 -5 -4 102.59 6.70 -3 5 -4 117.89 5.10 -3 5 -4 120.19 4.70 3 5 4 124.99 4.80 3 5 4 113.69 5.00 3 5 4 113.09 4.80 -4 -5 -4 71.19 4.00 -4 -5 -4 70.79 4.50 4 -5 4 69.09 4.00 4 -5 4 80.89 6.60 -4 -5 -4 66.19 3.80 4 -5 4 68.29 5.90 4 -5 4 63.29 4.00 4 -5 4 64.89 3.00 -4 -5 -4 77.29 4.50 -4 5 -4 65.69 4.10 4 5 4 69.89 3.90 4 5 4 60.69 4.00 4 5 4 73.19 3.80 -4 5 -4 66.09 3.80 -4 5 -4 64.09 3.00 4 5 4 64.59 5.80 -5 -5 -4 35.30 3.80 -5 -5 -4 40.80 3.50 -5 -5 -4 39.40 4.40 5 -5 4 26.30 4.00 -5 -5 -4 37.60 5.30 5 -5 4 36.30 3.40 -5 -5 -4 31.90 3.60 -5 5 -4 34.00 2.30 -5 5 -4 30.50 3.70 -5 5 -4 34.10 3.60 5 5 4 35.90 3.30 -5 5 -4 33.50 5.30 -5 5 -4 34.10 3.30 5 5 4 35.10 3.30 -6 -5 -4 17.30 3.50 6 -5 4 13.10 3.90 -6 -5 -4 21.80 3.30 6 -5 4 25.80 3.50 -6 -5 -4 24.40 3.20 6 -5 4 16.10 2.60 -6 -5 -4 28.90 3.80 6 5 4 12.60 2.40 -6 5 -4 17.90 1.70 -6 5 -4 23.10 3.20 -9 -6 4 24.40 3.20 9 -6 -4 25.60 3.50 -9 -6 4 21.20 3.00 9 -6 -4 14.90 3.00 9 -6 -4 17.10 2.60 9 -6 -4 22.10 4.90 -9 -6 4 19.90 2.90 -9 6 4 18.70 3.20 -9 6 4 20.50 2.10 -9 6 4 28.00 4.30 9 6 -4 19.40 2.60 9 6 -4 17.90 2.60 -8 -6 4 16.00 2.40 8 -6 -4 19.00 3.60 -8 -6 4 25.10 2.60 8 -6 -4 20.10 2.50 8 -6 -4 25.30 3.00 -8 -6 4 28.50 3.40 -8 -6 4 22.30 2.70 8 -6 -4 28.10 3.60 8 6 -4 22.00 2.70 -8 6 4 20.50 3.00 -8 6 4 28.70 3.90 -8 6 4 21.70 2.10 8 6 -4 24.80 2.80 -8 6 4 26.40 3.00 -7 -6 4 12.60 2.20 7 -6 -4 17.40 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3.60 -4 6 4 82.69 4.50 4 6 -4 82.19 3.10 -3 -6 4 35.50 2.50 -3 -6 4 36.80 2.30 -3 -6 4 35.30 2.20 3 -6 -4 36.50 2.60 3 -6 -4 33.40 3.10 3 -6 -4 31.70 2.30 -3 -6 4 34.50 1.60 3 -6 -4 34.20 3.30 -3 -6 4 36.30 2.60 -3 6 4 34.90 3.30 3 6 -4 34.40 2.40 3 6 -4 37.00 2.50 -3 6 4 37.30 3.00 -3 6 4 34.20 2.40 -3 6 4 36.30 2.30 -3 6 4 36.20 2.30 -2 -6 4 1.70 1.20 2 -6 -4 2.40 1.30 -2 -6 4 3.00 1.10 2 -6 -4 2.50 1.30 2 -6 -4 3.00 1.10 -2 -6 4 1.80 1.10 2 -6 -4 3.30 1.80 -2 -6 4 1.10 1.40 2 6 -4 3.30 1.40 2 6 -4 5.10 1.20 -2 6 4 1.80 1.10 2 6 -4 4.40 1.20 -2 6 4 3.60 1.20 -2 6 4 1.70 1.50 -2 6 4 1.90 1.20 -1 -6 4 10.50 1.90 -1 -6 4 15.80 1.50 1 -6 -4 18.50 1.60 1 -6 -4 15.30 2.30 -1 -6 4 14.90 1.50 -1 -6 4 15.80 1.60 1 -6 -4 13.20 1.50 1 -6 -4 11.80 1.70 -1 6 4 14.10 2.00 1 6 -4 14.70 1.50 1 6 -4 16.80 1.70 -1 6 4 12.70 1.70 -1 6 4 13.60 1.50 -1 6 4 14.60 1.50 0 -6 -4 448.66 13.30 0 -6 4 441.56 13.30 0 -6 -4 435.76 14.30 0 -6 -4 441.26 13.30 0 -6 4 467.25 14.70 0 -6 4 454.55 13.40 0 -6 -4 449.06 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2.70 -3 6 -4 38.90 3.30 3 6 4 40.20 4.00 3 6 4 29.30 3.90 3 6 4 41.00 3.00 -4 -6 -4 16.70 2.60 4 -6 4 5.80 3.00 -4 -6 -4 6.70 1.90 -4 -6 -4 10.90 2.20 4 -6 4 9.30 2.10 -4 -6 -4 3.20 2.10 -4 -6 -4 2.30 2.60 4 -6 4 6.50 1.80 -4 6 -4 7.30 1.90 -4 6 -4 10.70 2.40 4 6 4 8.20 2.40 -4 6 -4 7.90 2.70 4 6 4 9.20 2.10 4 6 4 8.00 2.00 4 6 4 8.30 1.80 -4 6 -4 9.70 1.90 5 -6 4 18.50 2.90 5 -6 4 6.00 5.00 -5 -6 -4 13.50 2.30 -5 -6 -4 24.60 3.20 5 -6 4 14.70 2.50 -5 -6 -4 19.70 2.60 -5 6 -4 16.80 3.20 5 6 4 17.90 2.90 -5 6 -4 14.90 2.70 5 6 4 22.70 2.60 -5 6 -4 13.10 2.20 5 6 4 20.50 2.70 -5 6 -4 21.80 2.60 8 -7 -4 6.00 2.40 8 -7 -4 9.40 2.90 8 -7 -4 9.20 2.50 -8 -7 4 8.20 2.20 8 -7 -4 4.60 2.90 -8 -7 4 4.70 2.00 -8 7 4 7.30 2.70 8 7 -4 10.40 3.30 8 7 -4 7.80 2.10 -8 7 4 6.80 1.10 -8 7 4 8.50 2.10 -7 -7 4 29.60 3.30 -7 -7 4 30.60 3.10 7 -7 -4 28.40 3.20 7 -7 -4 36.10 5.30 7 -7 -4 37.10 4.00 -7 -7 4 31.70 3.30 7 -7 -4 33.50 4.00 -7 -7 4 29.00 3.10 -7 7 4 33.60 3.40 7 7 -4 29.50 3.00 -7 7 4 29.80 2.10 -7 7 4 30.40 3.80 -7 7 4 29.20 3.40 -6 -7 4 29.30 2.80 6 -7 -4 27.70 3.80 6 -7 -4 34.10 3.10 6 -7 -4 34.00 3.60 -6 -7 4 31.40 3.00 6 -7 -4 29.30 3.50 -6 -7 4 32.90 3.00 -6 -7 4 31.30 3.10 6 7 -4 34.00 3.20 -6 7 4 34.90 3.30 6 7 -4 26.90 2.80 -6 7 4 25.70 2.90 -6 7 4 25.10 2.00 -5 -7 4 68.39 3.30 -5 -7 4 63.79 3.10 5 -7 -4 69.29 3.70 5 -7 -4 66.99 4.60 5 -7 -4 60.59 5.50 5 -7 -4 69.29 3.80 -5 -7 4 64.39 3.30 -5 -7 4 62.39 3.40 -5 7 4 65.59 3.50 -5 7 4 66.29 3.00 -5 7 4 61.49 4.10 5 7 -4 70.39 3.50 5 7 -4 67.29 3.40 -5 7 4 70.89 4.60 -5 7 4 63.69 3.50 4 -7 -4 82.19 4.80 4 -7 -4 83.19 3.80 -4 -7 4 85.79 3.30 -4 -7 4 86.09 3.50 4 -7 -4 89.49 5.90 -4 -7 4 86.89 3.60 -4 -7 4 80.89 3.70 4 -7 -4 91.39 3.90 4 -7 -4 86.39 3.60 -4 7 4 84.49 3.80 -4 7 4 82.69 4.50 -4 7 4 86.09 4.10 4 7 -4 90.49 3.80 -4 7 4 87.39 3.60 4 7 -4 85.39 3.70 -4 7 4 91.49 4.90 3 -7 -4 31.70 2.50 -3 -7 4 31.00 2.30 3 -7 -4 33.70 2.50 3 -7 -4 33.20 2.60 -3 -7 4 32.20 2.60 3 -7 -4 35.00 4.10 -3 -7 4 30.50 2.70 -3 -7 4 33.90 2.30 3 7 -4 34.60 2.30 -3 7 4 29.40 2.40 -3 7 4 30.80 2.50 3 7 -4 29.50 2.70 -3 7 4 31.20 3.10 -3 7 4 39.00 3.70 3 7 -4 35.90 2.60 -3 7 4 30.70 2.40 -2 -7 4 85.49 3.40 2 -7 -4 82.19 4.50 -2 -7 4 85.79 3.40 -2 -7 4 82.29 4.30 -2 -7 4 81.39 4.00 2 -7 -4 85.19 3.40 2 -7 -4 82.99 3.80 2 -7 -4 81.49 3.50 -2 7 4 86.69 3.40 2 7 -4 84.19 4.40 -2 7 4 86.79 4.80 -2 7 4 81.89 3.50 -2 7 4 83.49 3.70 2 7 -4 83.69 3.50 2 7 -4 91.79 3.60 1 -7 -4 7.50 1.40 -1 -7 4 8.80 1.30 1 -7 -4 7.00 1.40 -1 -7 4 7.00 1.40 1 -7 -4 9.30 2.30 1 -7 -4 7.30 1.70 -1 -7 4 6.70 1.40 1 7 -4 7.40 1.50 -1 7 4 8.80 1.70 1 7 -4 7.80 1.50 -1 7 4 7.60 1.30 -1 7 4 8.40 2.20 1 7 -4 6.70 1.90 -1 7 4 8.30 1.40 0 -7 4 397.76 13.40 0 -7 -4 394.86 13.00 0 -7 -4 393.36 12.40 0 -7 -4 384.86 11.60 0 -7 -4 397.36 11.80 0 -7 -4 400.26 11.80 0 -7 4 387.16 11.90 0 -7 4 389.96 11.80 0 -7 4 376.66 11.80 0 7 4 384.16 11.70 0 7 -4 416.86 12.00 0 7 4 409.56 13.00 0 7 -4 392.36 11.90 0 7 4 391.46 13.50 0 7 4 409.66 11.80 0 7 -4 395.56 13.40 -1 -7 -4 7.50 1.50 -1 -7 -4 5.50 2.00 -1 -7 -4 7.60 1.40 1 -7 4 6.50 1.60 1 -7 4 5.90 1.10 1 -7 4 0.60 3.30 -1 -7 -4 7.70 1.50 -1 -7 -4 9.40 2.20 1 7 4 5.30 2.10 1 7 4 5.60 1.50 -1 7 -4 4.10 2.00 -1 7 -4 7.00 1.70 1 7 4 4.70 1.80 -1 7 -4 8.00 1.80 -2 -7 -4 104.09 4.20 2 -7 4 107.29 3.70 -2 -7 -4 100.79 6.60 2 -7 4 116.59 4.70 -2 -7 -4 105.49 4.40 2 -7 4 100.09 4.40 -2 -7 -4 106.69 5.60 -2 -7 -4 112.19 4.50 2 -7 4 101.69 6.40 -2 -7 -4 114.39 5.30 -2 7 -4 108.69 4.60 2 7 4 116.79 5.70 -2 7 -4 99.69 3.80 2 7 4 108.69 4.50 -2 7 -4 105.39 4.90 2 7 4 97.19 4.50 -3 -7 -4 47.50 5.50 3 -7 4 56.89 5.80 -3 -7 -4 63.79 3.50 -3 -7 -4 64.79 3.80 -3 -7 -4 65.09 4.30 3 -7 4 61.89 3.60 3 -7 4 60.79 3.90 -3 -7 -4 62.89 3.60 3 7 4 59.89 3.90 3 7 4 68.49 4.80 -3 7 -4 58.09 3.80 -3 7 -4 71.69 4.70 -3 7 -4 66.59 5.40 3 7 4 57.39 3.40 -3 7 -4 62.59 3.10 -4 -7 -4 5.90 3.00 -4 -7 -4 3.10 1.80 4 -7 4 -1.00 1.80 -4 -7 -4 2.90 2.00 -4 -7 -4 1.70 1.60 4 -7 4 0.50 1.80 4 -7 4 0.10 2.60 -4 -7 -4 -0.30 2.00 4 7 4 0.20 1.60 -4 7 -4 2.80 1.50 -4 7 -4 2.90 3.10 -4 7 -4 1.70 2.90 4 7 4 -1.30 2.10 -4 7 -4 0.20 1.70 -5 -7 -4 1.90 2.30 -5 -7 -4 -2.60 2.60 -5 -7 -4 0.80 1.90 -5 -7 -4 6.20 2.60 -5 -7 -4 0.10 2.20 5 -7 4 0.60 1.90 5 -7 4 -1.30 2.90 5 -7 4 2.90 2.00 5 -7 4 5.30 2.50 -5 7 -4 -0.10 1.90 5 7 4 -0.10 1.70 5 7 4 6.60 2.70 5 7 4 5.30 2.50 -5 7 -4 4.00 1.80 -5 7 -4 1.10 2.60 -8 -8 4 2.00 2.00 -8 -8 4 4.50 2.10 8 -8 -4 10.30 3.00 -8 -8 4 3.60 2.00 8 -8 -4 2.20 4.10 8 -8 -4 2.20 2.70 -8 -8 4 3.40 2.00 8 -8 -4 1.40 1.80 -8 8 4 5.30 2.50 -8 8 4 5.10 2.00 8 8 -4 2.40 2.10 8 8 -4 1.90 1.90 -7 -8 4 6.50 1.80 7 -8 -4 4.50 1.90 7 -8 -4 6.60 2.20 -7 -8 4 3.50 2.20 7 -8 -4 5.30 3.00 7 -8 -4 6.60 2.60 -7 -8 4 6.20 2.00 -7 8 4 5.00 1.00 -7 8 4 6.80 2.00 -7 8 4 4.60 1.90 -7 8 4 4.30 2.30 7 8 -4 3.00 1.60 7 8 -4 7.30 2.00 -6 -8 4 32.80 3.20 6 -8 -4 32.10 4.10 -6 -8 4 32.90 3.00 -6 -8 4 36.10 2.90 6 -8 -4 36.00 5.40 6 -8 -4 27.10 3.00 6 -8 -4 35.00 3.60 -6 -8 4 36.10 3.00 -6 8 4 40.70 4.30 -6 8 4 28.60 3.10 6 8 -4 24.40 2.30 -6 8 4 38.90 3.90 6 8 -4 27.30 2.80 -6 8 4 32.10 3.80 -6 8 4 31.50 2.00 -5 -8 4 18.30 2.20 -5 -8 4 18.70 2.40 5 -8 -4 16.70 2.00 5 -8 -4 20.40 3.50 -5 -8 4 17.50 1.80 5 -8 -4 21.20 3.10 5 -8 -4 17.10 2.00 -5 -8 4 16.80 1.80 -5 8 4 19.70 2.10 5 8 -4 18.20 1.80 -5 8 4 18.20 2.80 -5 8 4 14.80 1.50 5 8 -4 18.70 2.00 -5 8 4 16.20 2.00 4 -8 -4 106.69 4.20 -4 -8 4 110.99 4.10 4 -8 -4 113.49 6.80 4 -8 -4 115.79 5.70 4 -8 -4 130.29 6.30 -4 -8 4 111.49 4.20 4 -8 -4 107.79 4.50 -4 -8 4 107.59 4.00 4 8 -4 109.99 4.20 -4 8 4 107.09 4.20 -4 8 4 111.89 4.40 -4 8 4 100.69 5.30 -4 8 4 110.69 4.40 -4 8 4 117.89 5.80 4 8 -4 113.49 4.40 3 -8 -4 89.39 3.70 3 -8 -4 89.69 6.00 -3 -8 4 83.39 3.50 3 -8 -4 87.59 3.70 -3 -8 4 81.49 4.10 -3 -8 4 90.29 3.50 3 -8 -4 85.79 5.00 3 -8 -4 84.49 3.80 -3 -8 4 84.49 4.20 -3 8 4 87.49 3.60 -3 8 4 88.99 4.70 3 8 -4 92.79 3.60 -3 8 4 90.69 3.80 -3 8 4 87.09 3.80 3 8 -4 87.39 4.10 -3 8 4 87.39 5.10 3 8 -4 90.39 3.60 2 -8 -4 24.70 2.30 2 -8 -4 22.10 2.00 -2 -8 4 23.50 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3.00 2 -4 -8 26.50 3.00 -2 -4 8 25.90 2.70 2 -4 -8 25.90 3.00 -2 4 8 29.70 3.10 2 4 -8 27.90 1.80 -2 4 8 21.70 2.00 2 4 -8 27.10 3.20 -2 4 8 20.20 2.50 -1 -4 8 1.70 2.30 1 -4 -8 1.80 1.90 1 -4 -8 -2.50 3.20 1 -4 -8 3.70 2.00 -1 -4 8 3.40 1.60 1 -4 -8 4.00 2.30 -1 -4 8 3.80 2.00 1 -4 -8 2.50 2.10 1 4 -8 2.30 1.10 1 4 -8 2.30 2.30 -1 4 8 3.80 1.80 1 4 -8 4.60 2.30 -1 4 8 3.20 2.10 -1 4 8 1.90 1.20 1 4 -8 3.40 2.60 0 -4 -8 0.50 1.70 0 -4 -8 4.20 2.30 0 -4 -8 1.50 2.40 0 -4 8 3.00 2.10 0 -4 -8 -5.00 4.70 0 -4 8 2.70 1.60 0 -4 8 1.50 1.50 0 -4 -8 2.40 1.90 0 4 -8 2.80 2.00 0 4 8 4.20 1.40 0 4 -8 0.60 2.80 0 4 8 3.60 2.50 0 4 8 0.50 2.60 0 4 8 3.30 2.20 0 4 -8 -0.40 2.20 0 4 -8 4.90 1.30 1 -4 8 3.40 5.60 1 -4 8 0.80 1.90 -1 -4 -8 3.60 2.90 1 -4 8 3.70 1.60 -1 -4 -8 -4.60 3.40 -1 -4 -8 1.40 1.70 -1 -4 -8 4.40 2.40 -1 -4 -8 0.30 2.20 1 -4 8 3.30 2.30 1 -4 8 0.80 1.80 -1 4 -8 6.60 2.70 1 4 8 1.60 1.20 -1 4 -8 0.20 1.30 -1 4 -8 2.40 1.60 -1 4 -8 2.70 2.40 1 4 8 0.20 1.70 1 4 8 1.70 1.90 1 4 8 1.30 2.10 -1 4 -8 0.10 1.90 -8 -5 8 0.20 1.80 -8 -5 8 -0.60 1.70 8 -5 -8 -4.40 2.10 -8 -5 8 -2.10 2.20 8 -5 -8 0.20 3.30 8 -5 -8 3.40 2.60 8 -5 -8 -2.60 2.70 -8 -5 8 1.10 2.00 -8 5 8 -2.30 1.80 8 5 -8 0.70 1.30 -8 5 8 -0.40 1.50 8 5 -8 2.30 2.20 -8 5 8 -0.90 2.10 -8 5 8 0.30 1.10 -8 5 8 -1.60 2.00 -8 5 8 0.40 2.30 8 5 -8 -2.90 2.00 -7 -5 8 2.90 1.80 7 -5 -8 4.10 2.40 -7 -5 8 4.10 1.70 7 -5 -8 6.40 2.60 7 -5 -8 5.40 2.80 -7 -5 8 3.30 2.10 -7 -5 8 2.10 2.00 -7 5 8 0.60 2.00 7 5 -8 1.80 2.20 -7 5 8 4.20 2.50 -7 5 8 3.70 2.10 -7 5 8 4.60 2.70 -7 5 8 3.50 2.20 7 5 -8 2.50 1.70 6 -5 -8 12.10 2.80 6 -5 -8 14.90 3.00 6 -5 -8 15.40 2.50 -6 -5 8 12.60 1.60 -6 -5 8 8.30 3.80 -6 -5 8 9.60 2.30 -6 5 8 10.60 2.50 -6 5 8 9.70 2.40 6 5 -8 10.30 2.50 -6 5 8 12.90 3.00 -6 5 8 9.70 2.50 6 5 -8 13.30 2.50 6 5 -8 9.80 2.30 5 -5 -8 27.50 3.40 -5 -5 8 19.70 2.20 -5 -5 8 21.80 2.40 5 -5 -8 24.70 2.80 -5 -5 8 22.00 2.60 5 -5 -8 28.50 3.30 5 -5 -8 22.50 2.70 5 5 -8 18.50 2.70 -5 5 8 16.10 2.60 -5 5 8 21.60 2.60 5 5 -8 24.90 2.90 -5 5 8 17.10 2.20 -5 5 8 20.20 2.60 5 5 -8 26.90 3.00 -4 -5 8 34.60 3.40 -4 -5 8 38.20 3.60 4 -5 -8 36.90 4.20 -4 -5 8 34.90 3.20 4 -5 -8 38.00 3.70 4 -5 -8 32.00 3.30 4 -5 -8 29.70 3.00 -4 5 8 35.70 3.40 4 5 -8 39.40 4.50 -4 5 8 32.30 3.60 -4 5 8 27.90 3.20 -4 5 8 37.10 4.10 4 5 -8 38.20 3.70 4 5 -8 38.60 3.90 3 -5 -8 12.10 2.50 3 -5 -8 14.30 2.30 3 -5 -8 17.40 2.60 -3 -5 8 13.90 2.10 -3 -5 8 17.10 2.50 3 -5 -8 10.60 2.40 -3 -5 8 15.00 2.10 -3 5 8 20.00 3.10 -3 5 8 15.70 1.40 3 5 -8 11.90 2.70 -3 5 8 14.20 2.20 3 5 -8 14.50 2.50 3 5 -8 14.40 2.20 -3 5 8 15.70 2.30 -2 -5 8 11.00 2.50 2 -5 -8 8.70 2.10 2 -5 -8 4.60 2.90 2 -5 -8 8.30 2.40 -2 -5 8 7.20 2.00 2 -5 -8 13.90 2.90 2 -5 -8 10.50 2.30 -2 -5 8 11.00 2.10 -2 5 8 5.20 1.70 -2 5 8 8.00 1.20 -2 5 8 11.20 2.70 2 5 -8 9.40 2.60 -2 5 8 7.40 2.20 2 5 -8 11.40 2.50 -2 5 8 7.20 2.00 1 -5 -8 12.60 2.40 1 -5 -8 14.40 2.60 -1 -5 8 13.40 2.10 -1 -5 8 15.70 2.10 -1 -5 8 14.60 2.50 1 -5 -8 11.20 2.30 1 -5 -8 12.40 2.40 -1 5 8 16.80 2.60 -1 5 8 17.70 1.60 -1 5 8 19.10 2.40 -1 5 8 14.70 2.80 1 5 -8 12.40 3.00 -1 5 8 19.70 3.10 1 5 -8 10.90 2.50 1 5 -8 26.40 4.80 0 -5 -8 32.30 3.80 0 -5 -8 27.80 3.20 0 -5 -8 23.80 4.70 0 -5 8 29.70 4.10 0 -5 -8 36.70 3.50 0 -5 8 31.50 3.00 0 -5 8 34.40 3.20 0 -5 8 25.40 3.00 0 -5 -8 36.20 4.80 0 5 -8 30.90 3.40 0 5 8 28.10 2.90 0 5 -8 28.10 2.90 0 5 8 29.50 2.40 0 5 8 31.20 3.10 0 5 8 34.10 3.80 -1 -5 -8 7.60 2.50 1 -5 8 14.80 3.80 1 -5 8 8.90 2.50 1 -5 8 16.20 2.90 -1 -5 -8 10.30 2.40 1 -5 8 14.30 2.60 -1 -5 -8 12.60 2.80 -1 -5 -8 17.50 3.00 1 -5 8 11.00 1.90 1 5 8 10.70 2.20 -1 5 -8 10.60 2.60 1 5 8 16.60 3.70 1 5 8 10.60 1.80 1 5 8 9.60 3.40 -1 5 -8 13.70 1.60 -1 5 -8 13.00 1.50 -1 5 -8 10.10 2.90 -7 -6 8 7.30 2.20 7 -6 -8 10.40 2.70 -7 -6 8 4.30 2.60 7 -6 -8 3.40 2.30 -7 -6 8 2.50 2.40 -7 -6 8 9.40 1.70 7 -6 -8 8.80 2.90 -7 -6 8 6.50 1.30 -7 6 8 7.70 2.40 -7 6 8 3.50 1.80 7 6 -8 4.80 1.50 -7 6 8 6.10 2.60 -7 6 8 4.50 2.10 -7 6 8 6.90 2.50 7 6 -8 3.40 2.20 7 6 -8 5.70 2.30 6 -6 -8 3.40 2.30 -6 -6 8 3.90 1.10 -6 -6 8 4.00 2.10 -6 -6 8 5.20 2.10 6 -6 -8 3.40 2.20 6 -6 -8 6.00 2.80 -6 -6 8 2.40 1.90 -6 6 8 3.80 2.40 -6 6 8 1.80 1.90 6 6 -8 2.20 2.10 -6 6 8 0.30 2.30 -6 6 8 1.30 1.90 6 6 -8 3.20 1.70 -6 6 8 0.30 1.70 6 6 -8 3.30 2.20 -5 -6 8 0.90 1.70 5 -6 -8 1.10 2.20 -5 -6 8 0.20 1.60 -5 -6 8 0.30 1.80 5 -6 -8 2.50 1.60 5 -6 -8 -1.20 2.50 5 -6 -8 2.10 2.00 -5 6 8 0.20 1.60 -5 6 8 -2.80 3.50 5 6 -8 0.40 1.70 5 6 -8 1.50 2.20 -5 6 8 0.70 2.40 -5 6 8 1.90 2.30 5 6 -8 0.90 2.20 -5 6 8 -2.80 1.60 4 -6 -8 2.20 2.20 -4 -6 8 5.80 2.20 -4 -6 8 3.80 1.80 4 -6 -8 -0.20 1.80 -4 -6 8 2.80 1.80 4 -6 -8 2.90 2.00 4 -6 -8 2.50 2.00 -4 6 8 1.90 2.20 -4 6 8 2.70 2.00 4 6 -8 3.80 2.00 4 6 -8 3.00 1.90 -4 6 8 3.10 1.70 -4 6 8 1.70 1.50 4 6 -8 6.10 2.00 -3 -6 8 9.70 1.80 3 -6 -8 15.80 2.60 3 -6 -8 15.70 3.00 -3 -6 8 11.70 2.30 3 -6 -8 12.30 2.40 -3 -6 8 11.60 2.10 3 -6 -8 14.10 2.40 3 6 -8 8.80 2.30 -3 6 8 9.70 2.60 -3 6 8 10.70 2.20 -3 6 8 11.30 2.10 -3 6 8 12.80 2.20 3 6 -8 13.30 2.40 3 6 -8 14.10 2.50 2 -6 -8 4.40 1.90 2 -6 -8 5.20 2.40 -2 -6 8 5.70 1.70 -2 -6 8 4.40 1.80 2 -6 -8 2.60 2.00 2 -6 -8 5.20 2.10 -2 6 8 7.20 3.30 2 6 -8 8.60 2.10 2 6 -8 2.80 3.30 -2 6 8 5.20 0.90 -2 6 8 3.30 1.70 -2 6 8 2.70 1.80 -2 6 8 4.40 2.60 1 -6 -8 0.20 2.00 1 -6 -8 2.60 2.10 -1 -6 8 1.10 2.70 1 -6 -8 -3.70 2.90 -1 -6 8 1.60 1.50 -1 -6 8 1.70 1.90 1 -6 -8 2.40 2.00 1 -6 -8 2.10 2.10 -1 -6 8 0.20 2.20 1 6 -8 -0.70 2.00 -1 6 8 -1.70 1.60 -1 6 8 1.10 2.50 -1 6 8 2.00 1.10 -1 6 8 2.80 1.70 1 6 -8 2.10 2.30 1 6 -8 3.80 2.90 -1 6 8 0.60 2.00 0 -6 -8 -5.30 3.20 0 -6 -8 3.00 2.20 0 -6 8 1.50 1.80 0 -6 8 2.70 3.10 0 -6 8 -1.70 2.20 0 -6 8 1.60 1.50 0 -6 -8 1.60 2.00 0 -6 -8 -2.20 2.00 0 -6 -8 -1.30 2.30 0 6 -8 -1.10 2.10 0 6 8 0.90 1.80 0 6 -8 0.40 2.10 0 6 8 2.50 1.20 0 6 8 -1.30 1.70 0 6 8 2.10 2.10 0 6 8 -0.20 2.40 0 6 -8 -0.20 2.30 6 -7 -8 2.80 2.60 6 -7 -8 1.30 2.10 -6 -7 8 1.60 1.90 6 -7 -8 2.80 2.50 -6 -7 8 3.60 2.10 -6 7 8 -0.20 2.20 -6 7 8 2.00 1.90 6 7 -8 5.60 2.20 6 7 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1.90 -2 7 8 -1.00 2.30 2 7 -8 5.40 2.10 1 -7 -8 3.70 2.50 1 -7 -8 1.80 2.40 1 -7 -8 3.30 2.10 -1 -7 8 1.70 1.50 -1 -7 8 3.30 3.00 -1 -7 8 1.90 2.30 1 -7 -8 5.40 2.50 1 -7 -8 -4.30 3.20 -1 -7 8 2.20 1.80 1 7 -8 2.80 2.30 1 7 -8 4.70 2.40 -1 7 8 2.80 2.10 -1 7 8 2.90 2.10 -1 7 8 5.90 2.00 1 7 -8 3.90 2.30 -1 7 8 3.40 2.70 5 -8 -8 9.90 2.40 -5 -8 8 7.50 2.40 5 -8 -8 6.90 2.20 -5 -8 8 9.00 2.00 -5 8 8 10.00 2.10 5 8 -8 8.10 2.00 -5 8 8 9.20 1.90 -5 8 8 6.60 2.50 5 8 -8 10.20 2.30 5 8 -8 6.40 2.50 -5 8 8 5.80 2.10 4 -8 -8 2.80 2.50 4 -8 -8 6.60 2.20 4 -8 -8 3.00 3.80 -4 -8 8 4.80 2.20 -4 -8 8 3.90 2.10 4 -8 -8 3.80 2.00 4 8 -8 4.30 2.30 4 8 -8 4.10 1.90 4 8 -8 5.00 2.00 -4 8 8 3.90 2.10 -4 8 8 3.40 2.70 -4 8 8 3.80 1.80 -4 8 8 5.10 2.00 -3 -8 8 2.80 1.80 -3 -8 8 5.30 1.90 3 -8 -8 5.70 3.60 3 -8 -8 0.80 2.10 3 -8 -8 5.70 2.20 -3 -8 8 3.90 3.30 3 -8 -8 3.80 2.30 -3 8 8 2.90 2.00 3 8 -8 3.60 2.40 3 8 -8 0.50 1.90 -3 8 8 3.80 1.70 -3 8 8 3.20 2.50 -3 8 8 2.40 1.70 2 -8 -8 -1.50 1.80 -2 -8 8 1.20 1.70 2 8 -8 -1.70 2.10 -2 8 8 -1.70 1.70 2 8 -8 1.10 2.00 -2 8 8 -1.50 2.30 8 0 -9 104.09 6.00 -8 0 9 108.09 5.90 -8 0 9 107.19 4.60 -8 0 9 97.39 8.40 8 0 -9 100.39 6.00 -8 0 9 90.99 5.20 8 0 -9 96.69 5.60 -8 0 9 97.29 5.40 -8 0 9 97.89 4.50 -7 0 9 -1.00 1.70 -7 0 9 2.30 2.40 7 0 -9 4.60 2.60 7 0 -9 1.00 2.00 7 0 -9 -2.00 2.30 -7 0 9 -0.20 1.80 7 0 -9 3.80 2.40 -7 0 9 2.20 3.40 -7 0 9 1.90 2.20 -6 0 9 8.60 2.20 6 0 -9 8.90 2.80 6 0 -9 7.60 2.50 -6 0 9 9.10 2.20 6 0 -9 10.20 2.30 -6 0 9 14.10 2.90 -6 0 9 12.40 2.80 5 0 -9 17.00 4.00 -5 0 9 20.40 3.30 -5 0 9 13.00 2.50 5 0 -9 10.80 2.00 5 0 -9 13.60 2.80 -5 0 9 11.00 1.80 4 0 -9 7.30 2.50 4 0 -9 10.20 2.00 4 0 -9 6.70 2.30 -4 0 9 8.40 2.40 -4 0 9 10.70 2.30 3 0 -9 5.00 2.30 3 0 -9 3.30 3.50 -3 0 9 4.90 1.90 3 0 -9 6.30 1.90 3 0 -9 5.50 2.10 -3 0 9 4.90 2.00 -3 0 9 2.30 2.10 -2 0 9 5.90 2.10 2 0 -9 3.80 2.50 2 0 -9 2.90 3.60 2 0 -9 9.60 2.80 -2 0 9 5.60 2.10 2 0 -9 8.90 2.30 -2 0 9 8.20 2.50 1 0 -9 0.60 2.00 -1 0 9 0.60 2.10 1 0 -9 0.30 1.60 1 0 -9 0.50 2.50 -1 0 9 -2.50 1.80 -1 0 9 0.40 1.70 1 0 -9 1.50 2.00 1 0 -9 11.00 6.00 0 0 -9 5.10 2.00 0 0 -9 1.60 4.10 0 0 9 2.40 1.90 0 0 9 5.00 1.90 0 0 9 5.40 2.50 0 0 -9 2.40 2.00 0 0 9 2.80 1.70 0 0 -9 1.20 1.70 0 0 -9 8.70 4.20 8 -1 -9 6.40 2.90 -8 -1 9 5.60 2.40 -8 -1 9 3.70 2.00 8 -1 -9 4.70 2.30 -8 -1 9 -0.90 2.40 8 -1 -9 -0.80 2.50 -8 -1 9 3.50 1.60 -8 -1 9 7.30 1.80 -8 1 9 4.20 2.50 8 1 -9 2.50 2.50 -8 1 9 4.90 2.50 -8 1 9 2.70 1.80 -8 1 9 2.40 2.40 -8 1 9 4.70 2.00 8 1 -9 1.40 2.60 8 1 -9 4.90 2.30 8 1 -9 3.20 2.10 -8 1 9 4.10 1.60 -7 -1 9 69.29 5.00 -7 -1 9 57.49 4.20 -7 -1 9 55.79 4.50 7 -1 -9 59.69 4.70 7 -1 -9 64.19 5.20 7 -1 -9 60.79 5.00 -7 -1 9 59.69 4.30 -7 -1 9 60.99 3.90 -7 1 9 60.99 4.50 7 1 -9 65.89 5.20 -7 1 9 55.19 4.90 -7 1 9 58.49 4.70 7 1 -9 58.69 7.00 7 1 -9 57.49 4.20 -7 1 9 57.99 6.50 -7 1 9 64.89 5.10 6 -1 -9 23.60 2.80 -6 -1 9 24.50 3.00 6 -1 -9 27.90 3.20 -6 -1 9 30.60 3.30 -6 -1 9 23.20 2.80 6 -1 -9 25.40 3.20 -6 -1 9 24.30 2.80 6 1 -9 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2 5 -9 2.30 2.50 2 5 -9 3.60 2.20 -2 5 9 4.50 2.00 -1 -5 9 6.60 2.80 1 -5 -9 7.90 3.10 -1 -5 9 4.50 1.80 1 -5 -9 2.30 2.50 -1 -5 9 5.80 2.10 1 -5 -9 4.70 2.40 1 -5 -9 3.00 2.10 -1 5 9 3.80 1.40 1 5 -9 4.20 2.70 -1 5 9 3.80 2.70 1 5 -9 2.20 2.50 -1 5 9 3.30 2.00 6 -6 -9 -0.70 2.20 6 -6 -9 4.40 2.50 -6 -6 9 2.60 1.80 -6 6 9 2.10 1.80 6 6 -9 0.00 2.30 6 6 -9 0.80 2.90 -6 6 9 2.40 2.30 -5 -6 9 1.70 1.90 5 -6 -9 5.80 2.90 5 -6 -9 2.90 2.60 5 -6 -9 2.80 1.90 5 -6 -9 -0.30 2.10 -5 -6 9 -1.50 2.30 -5 -6 9 2.70 1.70 5 6 -9 2.00 2.20 -5 6 9 1.20 2.30 -5 6 9 -0.80 1.70 5 6 -9 1.60 2.20 -5 6 9 3.10 2.60 -5 6 9 2.30 1.80 5 6 -9 0.90 1.90 4 -6 -9 1.00 2.00 -4 -6 9 4.40 2.40 4 -6 -9 -0.10 2.30 -4 -6 9 0.40 1.80 -4 -6 9 -0.40 1.60 4 -6 -9 1.80 2.60 4 -6 -9 0.90 2.90 -4 6 9 2.80 1.70 4 6 -9 1.50 2.10 -4 6 9 2.60 2.00 -4 6 9 0.70 1.70 4 6 -9 -1.80 2.10 -4 6 9 1.00 2.40 3 -6 -9 6.50 2.40 3 -6 -9 4.60 2.30 -3 -6 9 7.20 2.10 3 -6 -9 6.30 2.40 3 -6 -9 11.40 2.60 -3 -6 9 6.30 3.30 -3 6 9 4.30 2.00 3 6 -9 5.50 2.50 -3 6 9 3.50 2.10 -3 6 9 6.60 1.90 -3 6 9 5.20 2.70 3 6 -9 6.60 2.60 3 6 -9 8.20 2.60 2 -6 -9 50.29 4.80 -2 -6 9 35.00 3.30 -2 6 9 42.10 4.80 2 6 -9 31.50 6.40 -2 6 9 41.80 3.90 -7 0 10 4.70 2.90 -7 0 10 4.30 2.10 -7 0 10 1.50 2.30 -7 0 10 3.70 2.30 7 0 -10 1.40 4.30 7 0 -10 3.30 4.40 -7 0 10 -1.20 2.50 7 0 -10 0.70 2.50 7 0 -10 5.20 2.20 6 0 -10 -1.40 2.40 -6 0 10 -1.10 1.80 6 0 -10 -1.80 1.80 6 0 -10 -0.40 2.70 6 0 -10 -7.60 3.40 -6 0 10 0.00 2.20 -6 0 10 -1.40 2.30 -5 0 10 -0.60 1.50 -5 0 10 2.20 1.90 5 0 -10 -2.50 1.70 5 0 -10 -4.10 2.50 5 0 -10 -1.50 1.90 -5 0 10 -1.70 2.60 -4 0 10 -0.40 2.30 4 0 -10 -7.80 6.70 4 0 -10 -0.20 1.70 -4 0 10 -0.50 2.10 4 0 -10 -4.80 2.40 -4 0 10 -0.60 1.70 4 0 -10 0.10 2.50 -3 0 10 12.40 2.60 3 0 -10 11.80 3.10 -3 0 10 8.70 2.70 -3 0 10 7.90 2.40 3 0 -10 13.10 3.10 3 0 -10 11.30 2.20 2 0 -10 0.90 2.30 2 0 -10 -2.20 4.20 -2 0 10 3.60 2.60 2 0 -10 2.40 1.80 2 0 -10 -2.00 2.40 2 0 -10 -0.10 2.10 -2 0 10 4.60 2.30 -2 0 10 0.30 1.60 -2 0 10 0.70 2.20 -7 -1 10 9.60 2.50 7 -1 -10 12.80 3.40 7 -1 -10 13.90 2.70 -7 -1 10 15.20 2.40 -7 -1 10 8.70 2.70 7 -1 -10 10.70 5.10 7 -1 -10 8.40 2.80 -7 1 10 15.80 3.10 -7 1 10 6.80 2.80 7 1 -10 15.50 2.50 -7 1 10 12.40 4.30 -7 1 10 16.20 2.60 7 1 -10 9.20 3.20 -7 1 10 13.60 2.60 7 1 -10 17.90 4.70 7 1 -10 12.60 2.90 6 -1 -10 3.90 2.60 -6 -1 10 5.90 2.20 -6 -1 10 11.80 4.50 6 -1 -10 6.60 2.20 -6 -1 10 4.60 3.50 6 -1 -10 -0.40 4.20 6 -1 -10 5.90 4.50 -6 1 10 6.00 2.20 -6 1 10 5.60 2.20 6 1 -10 4.40 2.30 6 1 -10 10.20 2.20 6 1 -10 7.60 2.70 -6 1 10 11.20 2.50 -6 1 10 9.40 2.70 6 1 -10 2.40 3.90 5 -1 -10 3.40 2.00 -5 -1 10 4.90 3.50 5 -1 -10 0.90 5.70 -5 -1 10 1.20 1.80 5 -1 -10 -3.70 2.60 -5 -1 10 1.10 2.20 5 1 -10 -3.10 3.90 -5 1 10 0.10 1.80 -5 1 10 0.40 2.30 5 1 -10 -0.50 2.60 5 1 -10 -1.30 2.40 -5 1 10 -3.40 2.30 5 1 -10 0.00 1.70 4 -1 -10 -4.20 3.90 -4 -1 10 4.50 3.10 4 -1 -10 7.50 2.10 -4 -1 10 2.30 2.00 4 -1 -10 3.30 3.00 4 -1 -10 4.80 2.20 -4 -1 10 6.70 2.10 4 1 -10 3.60 2.70 4 1 -10 5.60 2.20 -4 1 10 4.30 2.00 4 1 -10 12.50 3.00 -4 1 10 5.10 2.60 -4 1 10 5.70 2.00 4 1 -10 -0.80 4.20 3 -1 -10 4.20 1.90 3 -1 -10 -0.40 3.60 3 -1 -10 0.00 2.00 3 -1 -10 -6.60 3.60 -3 -1 10 0.60 3.50 -3 -1 10 -0.40 2.90 -3 -1 10 0.60 1.70 3 1 -10 0.10 2.10 3 1 -10 -7.10 3.50 -3 1 10 0.90 1.80 3 1 -10 1.50 2.30 -3 1 10 2.20 2.00 -3 1 10 2.30 2.30 -2 -1 10 3.30 2.60 -2 -1 10 3.00 2.40 2 -1 -10 5.40 2.00 2 -1 -10 1.90 2.60 2 -1 -10 -5.70 5.80 -2 -1 10 1.90 2.00 2 -1 -10 4.50 2.60 2 -1 -10 0.90 2.20 -2 1 10 1.90 2.30 2 1 -10 0.60 3.20 2 1 -10 2.90 1.70 2 1 -10 5.10 2.60 -2 1 10 3.30 2.80 2 1 -10 4.30 4.40 -2 1 10 4.20 2.40 7 -2 -10 10.40 2.80 7 -2 -10 10.50 3.30 -7 -2 10 4.80 2.30 -7 2 10 5.60 2.20 7 2 -10 7.90 2.70 -7 2 10 10.80 2.40 6 -2 -10 5.10 2.70 -6 -2 10 5.60 2.90 6 -2 -10 0.80 2.20 6 -2 -10 -1.40 2.90 6 -2 -10 8.90 6.50 -6 -2 10 3.60 2.00 -6 -2 10 5.80 2.60 -6 2 10 3.60 2.30 6 2 -10 -0.80 3.90 6 2 -10 2.30 2.60 6 2 -10 5.80 1.90 -6 2 10 4.60 2.10 -6 2 10 1.30 2.00 6 2 -10 2.30 2.20 -6 2 10 2.10 2.30 -5 -2 10 6.50 2.50 5 -2 -10 1.10 3.30 -5 -2 10 9.80 2.50 5 -2 -10 4.00 3.10 5 -2 -10 9.00 3.20 5 -2 -10 6.50 2.40 -5 -2 10 6.70 2.90 -5 2 10 7.70 2.60 5 2 -10 -0.80 3.80 -5 2 10 9.30 2.60 5 2 -10 5.30 1.80 5 2 -10 7.00 2.60 -5 2 10 7.30 2.70 5 2 -10 8.10 2.90 -5 2 10 6.50 2.10 -4 -2 10 1.40 1.80 4 -2 -10 2.00 2.10 4 -2 -10 -2.50 2.60 -4 -2 10 1.90 2.20 -4 -2 10 -2.70 2.20 4 -2 -10 0.50 1.90 -4 2 10 2.40 2.50 -4 2 10 -0.70 1.70 -4 2 10 1.10 1.90 4 2 -10 -4.50 3.50 4 2 -10 2.00 1.60 4 2 -10 0.60 2.10 4 2 -10 0.10 2.50 -3 -2 10 1.90 1.80 -3 -2 10 3.90 2.00 3 -2 -10 8.60 3.10 3 -2 -10 4.60 2.10 3 -2 -10 4.70 2.10 3 -2 -10 0.00 2.10 -3 -2 10 5.50 3.80 3 2 -10 5.70 1.70 -3 2 10 5.70 2.40 3 2 -10 0.70 4.20 -3 2 10 2.20 2.00 -3 2 10 6.70 1.60 3 2 -10 4.30 2.40 -3 2 10 0.40 1.90 3 2 -10 3.80 2.20 2 -2 -10 6.80 2.20 2 -2 -10 4.50 3.70 -2 -2 10 4.50 2.60 -2 -2 10 3.30 1.80 -2 -2 10 3.80 2.20 2 -2 -10 4.70 2.50 2 2 -10 4.50 2.80 -2 2 10 3.80 2.40 2 2 -10 2.10 3.70 6 -3 -10 15.50 3.10 6 -3 -10 17.70 3.50 6 -3 -10 15.70 2.80 -6 -3 10 11.20 2.20 -6 -3 10 16.80 2.80 -6 3 10 11.20 2.70 6 3 -10 11.00 2.80 -6 3 10 15.70 3.00 6 3 -10 17.70 2.20 -6 3 10 12.00 2.30 5 -3 -10 2.80 2.20 5 -3 -10 -0.30 2.70 5 -3 -10 1.20 1.90 -5 -3 10 5.20 1.90 5 -3 -10 -2.00 3.10 -5 -3 10 5.60 2.20 -5 -3 10 3.60 2.40 5 3 -10 3.00 1.60 -5 3 10 1.00 2.50 5 3 -10 -1.20 2.60 5 3 -10 4.50 2.20 -5 3 10 4.90 2.00 5 3 -10 0.30 3.90 -5 3 10 1.00 2.20 -5 3 10 1.20 1.90 -4 -3 10 8.80 2.30 4 -3 -10 6.70 2.30 -4 -3 10 7.80 2.30 -4 -3 10 10.30 2.90 4 -3 -10 6.80 2.70 4 -3 -10 12.70 3.30 4 -3 -10 8.10 2.40 4 3 -10 12.70 1.80 -4 3 10 11.00 2.80 4 3 -10 7.90 2.60 4 3 -10 10.50 3.10 -4 3 10 8.60 1.50 -4 3 10 8.70 2.30 -4 3 10 10.90 2.80 -4 3 10 7.30 2.20 4 3 -10 8.80 4.30 3 -3 -10 1.50 2.10 -3 -3 10 -1.90 2.10 3 -3 -10 2.40 2.40 3 -3 -10 -0.70 2.10 -3 -3 10 -1.10 2.40 -3 -3 10 -1.00 1.70 3 -3 -10 -0.30 2.70 3 3 -10 -0.90 2.70 3 3 -10 3.00 3.40 3 3 -10 1.20 1.30 -3 3 10 1.90 2.20 -3 3 10 -0.30 1.30 -5 -4 10 1.60 1.60 -5 4 10 -0.30 2.30 -5 4 10 -1.20 2.40 -4 -4 10 12.40 2.70 -4 4 10 12.60 2.60 -4 4 10 9.30 2.30 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 43461 _shelx_res_file ; TITL umd2564i_a.res in P2(1) umd2564i_a.res created by SHELXL-2018/3 at 12:18:39 on 03-Mar-2022 REM Old TITL umd2564i in P2(1) REM SHELXT solution in P2(1): R1 0.158, Rweak 0.038, Alpha 0.014 REM 0.097 for 5 systematic absences, Orientation as input REM Flack x = 0.343 ( 0.978 ) from 1066 Parsons' quotients REM Formula found by SHELXT: C17 N CELL 0.71073 8.5446 10.399 8.6149 90 116.784 90 ZERR 2 0.0006 0.0007 0.0006 0 0.002 0 LATT -1 SYMM -X,0.5+Y,-Z SFAC C H N UNIT 32 44 4 EQIV $1 1-X,-0.5+Y,1-Z DFIX 0.87 0.01 N1 H1 DFIX 0.9 0.01 N2 H2 L.S. 10 PLAN 2 SIZE 0.2 0.24 0.35 TEMP 24 CONF HTAB N1 N2_$1 BOND $H LIST 6 htab 2 fmap 2 acta MORE -1 OMIT -1 5 1 OMIT -1 0 1 OMIT -1 1 1 OMIT 1 0 0 OMIT 0 0 1 REM REM REM WGHT 0.057300 0.158400 FVAR 1.69611 N1 3 0.684011 0.320120 0.768283 11.00000 0.06064 0.05976 = 0.04541 0.00395 0.01831 0.00752 N2 3 0.424179 0.581157 0.094277 11.00000 0.07085 0.06118 = 0.04450 0.00614 0.01456 -0.01033 C1 1 0.625665 0.338215 0.591814 11.00000 0.05406 0.09174 = 0.04303 -0.00693 0.01553 0.00346 AFIX 43 H1A 2 0.570884 0.275362 0.507790 11.00000 -1.20000 AFIX 0 C2 1 0.754920 0.434478 0.848660 11.00000 0.04544 0.05896 = 0.04703 0.00657 0.01880 0.01497 C3 1 0.832104 0.467226 1.023538 11.00000 0.06632 0.06387 = 0.05116 0.00085 0.02563 0.00554 AFIX 43 H3 2 0.840170 0.407744 1.107439 11.00000 -1.20000 AFIX 0 C4 1 0.896365 0.589957 1.069542 11.00000 0.06960 0.07443 = 0.06602 -0.01349 0.03262 -0.00216 AFIX 43 H4 2 0.950320 0.612645 1.186509 11.00000 -1.20000 AFIX 0 C5 1 0.882961 0.680503 0.946717 11.00000 0.06890 0.06558 = 0.08517 -0.00921 0.04085 -0.00049 AFIX 43 H5 2 0.926088 0.763121 0.981803 11.00000 -1.20000 AFIX 0 C6 1 0.806893 0.649519 0.774339 11.00000 0.05658 0.06101 = 0.09179 0.02452 0.04360 0.01390 AFIX 43 H6 2 0.797958 0.710952 0.692294 11.00000 -1.20000 AFIX 0 C7 1 0.741940 0.524413 0.720836 11.00000 0.04223 0.06773 = 0.05451 0.00976 0.02429 0.01479 C8 1 0.658860 0.459783 0.557345 11.00000 0.04749 0.08731 = 0.04903 0.01421 0.02001 0.01127 C9 1 0.623509 0.520388 0.386007 11.00000 0.06200 0.13557 = 0.05501 0.02718 0.02288 0.00795 AFIX 23 H9A 2 0.642061 0.612333 0.403785 11.00000 -1.20000 H9B 2 0.709578 0.488038 0.351364 11.00000 -1.20000 AFIX 0 C10 1 0.450419 0.499681 0.243124 11.00000 0.07866 0.07331 = 0.04635 0.01367 0.01233 -0.01463 AFIX 23 H10A 2 0.361947 0.519546 0.280822 11.00000 -1.20000 H10B 2 0.437557 0.410028 0.208452 11.00000 -1.20000 AFIX 0 C11 1 0.292023 0.538185 -0.076575 11.00000 0.04740 0.05226 = 0.04324 0.00287 0.01618 0.00201 AFIX 13 H11 2 0.177680 0.540657 -0.075896 11.00000 -1.20000 AFIX 0 C12 1 0.318074 0.403019 -0.129051 11.00000 0.06059 0.05397 = 0.06189 0.00532 0.02554 0.00510 AFIX 23 H12A 2 0.431796 0.397430 -0.128156 11.00000 -1.20000 H12B 2 0.315875 0.341579 -0.045337 11.00000 -1.20000 AFIX 0 C13 1 0.176166 0.369521 -0.308518 11.00000 0.08762 0.06450 = 0.06810 -0.01256 0.02905 -0.00632 AFIX 23 H13A 2 0.196778 0.283691 -0.339441 11.00000 -1.20000 H13B 2 0.063234 0.369608 -0.307234 11.00000 -1.20000 AFIX 0 C14 1 0.172337 0.463872 -0.443126 11.00000 0.08533 0.09669 = 0.05281 -0.00771 0.03019 0.00105 AFIX 23 H14A 2 0.281049 0.458099 -0.452537 11.00000 -1.20000 H14B 2 0.076703 0.442457 -0.555435 11.00000 -1.20000 AFIX 0 C15 1 0.148969 0.598223 -0.394632 11.00000 0.07082 0.08796 = 0.04768 0.01678 0.02237 0.01296 AFIX 23 H15A 2 0.033473 0.606436 -0.400188 11.00000 -1.20000 H15B 2 0.155915 0.657786 -0.477959 11.00000 -1.20000 AFIX 0 C16 1 0.286958 0.633726 -0.212937 11.00000 0.08438 0.05512 = 0.05105 0.00923 0.02473 0.00324 AFIX 23 H16A 2 0.262024 0.718893 -0.183813 11.00000 -1.20000 H16B 2 0.401106 0.636367 -0.211442 11.00000 -1.20000 AFIX 0 H2 2 0.524105 0.594422 0.083042 11.00000 0.09095 H1 2 0.671698 0.248909 0.813289 11.00000 0.06733 HKLF 4 REM umd2564i_a.res in P2(1) REM wR2 = 0.1237, GooF = S = 1.040, Restrained GooF = 1.040 for all data REM R1 = 0.0476 for 2396 Fo > 4sig(Fo) and 0.0530 for all 2621 data REM 171 parameters refined using 3 restraints END WGHT 0.0573 0.1586 REM Instructions for potential hydrogen bonds HTAB N1 N2_$1 REM Highest difference peak 0.259, deepest hole -0.156, 1-sigma level 0.031 Q1 1 0.5906 0.4339 0.3307 11.00000 0.05 0.26 Q2 1 0.7341 0.6006 0.6919 11.00000 0.05 0.19 ; _shelx_res_checksum 84132 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group N N1 0.6840(4) 0.3201(3) 0.7683(3) 0.0574(6) Uani d 1 . . N N2 0.4242(4) 0.5812(3) 0.0943(3) 0.0632(7) Uani d 1 . . C C1 0.6257(4) 0.3382(4) 0.5918(4) 0.0653(9) Uani d 1 . . H H1A 0.570884 0.275362 0.507790 0.078 Uiso calc 1 . . C C2 0.7549(4) 0.4345(3) 0.8487(4) 0.0512(7) Uani d 1 . . C C3 0.8321(4) 0.4672(3) 1.0235(4) 0.0608(8) Uani d 1 . . H H3 0.840170 0.407744 1.107439 0.073 Uiso calc 1 . . C C4 0.8964(5) 0.5900(4) 1.0695(5) 0.0692(9) Uani d 1 . . H H4 0.950320 0.612645 1.186509 0.083 Uiso calc 1 . . C C5 0.8830(5) 0.6805(4) 0.9467(5) 0.0709(9) Uani d 1 . . H H5 0.926088 0.763121 0.981803 0.085 Uiso calc 1 . . C C6 0.8069(4) 0.6495(3) 0.7743(5) 0.0660(9) Uani d 1 . . H H6 0.797958 0.710952 0.692294 0.079 Uiso calc 1 . . C C7 0.7419(4) 0.5244(3) 0.7208(4) 0.0539(7) Uani d 1 . . C C8 0.6589(4) 0.4598(4) 0.5573(4) 0.0619(8) Uani d 1 . . C C9 0.6235(5) 0.5204(5) 0.3860(4) 0.0855(13) Uani d 1 . . H H9A 0.642061 0.612333 0.403785 0.103 Uiso calc 1 . . H H9B 0.709578 0.488038 0.351364 0.103 Uiso calc 1 . . C C10 0.4504(5) 0.4997(4) 0.2431(4) 0.0721(11) Uani d 1 . . H H10A 0.361947 0.519546 0.280822 0.086 Uiso calc 1 . . H H10B 0.437557 0.410028 0.208452 0.086 Uiso calc 1 . . C C11 0.2920(4) 0.5382(3) -0.0766(3) 0.0492(6) Uani d 1 . . H H11 0.177680 0.540657 -0.075896 0.059 Uiso calc 1 . . C C12 0.3181(4) 0.4030(3) -0.1291(4) 0.0596(8) Uani d 1 . . H H12A 0.431796 0.397430 -0.128156 0.072 Uiso calc 1 . . H H12B 0.315875 0.341579 -0.045337 0.072 Uiso calc 1 . . C C13 0.1762(6) 0.3695(4) -0.3085(5) 0.0757(10) Uani d 1 . . H H13A 0.196778 0.283691 -0.339441 0.091 Uiso calc 1 . . H H13B 0.063234 0.369608 -0.307234 0.091 Uiso calc 1 . . C C14 0.1723(5) 0.4639(5) -0.4431(5) 0.0786(11) Uani d 1 . . H H14A 0.281049 0.458099 -0.452537 0.094 Uiso calc 1 . . H H14B 0.076703 0.442457 -0.555435 0.094 Uiso calc 1 . . C C15 0.1490(5) 0.5982(4) -0.3946(4) 0.0705(9) Uani d 1 . . H H15A 0.033473 0.606436 -0.400188 0.085 Uiso calc 1 . . H H15B 0.155915 0.657786 -0.477959 0.085 Uiso calc 1 . . C C16 0.2870(5) 0.6337(3) -0.2129(4) 0.0657(9) Uani d 1 . . H H16A 0.262024 0.718893 -0.183813 0.079 Uiso calc 1 . . H H16B 0.401106 0.636367 -0.211442 0.079 Uiso calc 1 . . H H2 0.524(3) 0.594(5) 0.083(5) 0.091(14) Uiso d 1 . . H H1 0.672(5) 0.249(2) 0.813(4) 0.067(11) Uiso d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 N1 0.0606(15) 0.0598(16) 0.0454(13) 0.0075(12) 0.0183(11) 0.0039(11) N2 0.0709(17) 0.0612(17) 0.0445(14) -0.0103(14) 0.0146(12) 0.0061(12) C1 0.0541(17) 0.092(3) 0.0430(16) 0.0035(17) 0.0155(13) -0.0069(17) C2 0.0454(14) 0.0590(19) 0.0470(15) 0.0150(12) 0.0188(12) 0.0066(12) C3 0.0663(19) 0.064(2) 0.0512(16) 0.0055(16) 0.0256(15) 0.0008(15) C4 0.070(2) 0.074(2) 0.066(2) -0.0022(18) 0.0326(17) -0.0135(19) C5 0.069(2) 0.066(2) 0.085(3) -0.0005(17) 0.041(2) -0.0092(19) C6 0.0566(17) 0.061(2) 0.092(3) 0.0139(15) 0.0436(18) 0.0245(18) C7 0.0422(14) 0.0677(19) 0.0545(16) 0.0148(14) 0.0243(13) 0.0098(15) C8 0.0475(16) 0.087(2) 0.0490(17) 0.0113(16) 0.0200(14) 0.0142(16) C9 0.062(2) 0.136(4) 0.0550(19) 0.008(2) 0.0229(16) 0.027(2) C10 0.079(2) 0.073(2) 0.0464(17) -0.0146(17) 0.0123(16) 0.0137(15) C11 0.0474(14) 0.0523(16) 0.0432(14) 0.0020(12) 0.0162(11) 0.0029(12) C12 0.0606(17) 0.0540(18) 0.0619(18) 0.0051(15) 0.0255(15) 0.0053(15) C13 0.088(3) 0.064(2) 0.068(2) -0.0063(18) 0.0290(19) -0.0126(17) C14 0.085(3) 0.097(3) 0.0528(19) 0.001(2) 0.0302(18) -0.0077(19) C15 0.071(2) 0.088(3) 0.0477(17) 0.0130(19) 0.0224(15) 0.0168(17) C16 0.084(2) 0.0551(19) 0.0510(18) 0.0032(16) 0.0247(17) 0.0092(14) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C1 N1 H1 . . 124(3) ? C2 N1 C1 . . 107.2(3) ? C2 N1 H1 . . 129(2) ? C10 N2 H2 . . 113(3) ? C11 N2 C10 . . 116.6(3) ? C11 N2 H2 . . 106(2) ? N1 C1 H1A . . 124.5 ? C8 C1 N1 . . 111.1(3) ? C8 C1 H1A . . 124.5 ? N1 C2 C3 . . 130.3(3) ? N1 C2 C7 . . 108.6(3) ? C3 C2 C7 . . 121.1(3) ? C2 C3 H3 . . 120.9 ? C4 C3 C2 . . 118.3(3) ? C4 C3 H3 . . 120.9 ? C3 C4 H4 . . 119.1 ? C3 C4 C5 . . 121.8(4) ? C5 C4 H4 . . 119.1 ? C4 C5 H5 . . 119.8 ? C6 C5 C4 . . 120.5(4) ? C6 C5 H5 . . 119.8 ? C5 C6 H6 . . 120.0 ? C5 C6 C7 . . 119.9(3) ? C7 C6 H6 . . 120.0 ? C2 C7 C8 . . 106.7(3) ? C6 C7 C2 . . 118.4(3) ? C6 C7 C8 . . 134.9(3) ? C1 C8 C7 . . 106.4(3) ? C1 C8 C9 . . 129.4(4) ? C7 C8 C9 . . 124.1(4) ? C8 C9 H9A . . 108.2 ? C8 C9 H9B . . 108.2 ? H9A C9 H9B . . 107.3 ? C10 C9 C8 . . 116.5(3) ? C10 C9 H9A . . 108.2 ? C10 C9 H9B . . 108.2 ? N2 C10 H10A . . 109.5 ? N2 C10 H10B . . 109.5 ? C9 C10 N2 . . 110.6(3) ? C9 C10 H10A . . 109.5 ? C9 C10 H10B . . 109.5 ? H10A C10 H10B . . 108.1 ? N2 C11 H11 . . 107.8 ? N2 C11 C12 . . 115.5(3) ? N2 C11 C16 . . 108.5(2) ? C12 C11 H11 . . 107.8 ? C12 C11 C16 . . 109.3(2) ? C16 C11 H11 . . 107.8 ? C11 C12 H12A . . 109.4 ? C11 C12 H12B . . 109.4 ? H12A C12 H12B . . 108.0 ? C13 C12 C11 . . 111.0(3) ? C13 C12 H12A . . 109.4 ? C13 C12 H12B . . 109.4 ? C12 C13 H13A . . 109.3 ? C12 C13 H13B . . 109.3 ? H13A C13 H13B . . 108.0 ? C14 C13 C12 . . 111.4(3) ? C14 C13 H13A . . 109.3 ? C14 C13 H13B . . 109.3 ? C13 C14 H14A . . 109.5 ? C13 C14 H14B . . 109.5 ? H14A C14 H14B . . 108.1 ? C15 C14 C13 . . 110.6(3) ? C15 C14 H14A . . 109.5 ? C15 C14 H14B . . 109.5 ? C14 C15 H15A . . 109.2 ? C14 C15 H15B . . 109.2 ? C14 C15 C16 . . 112.0(3) ? H15A C15 H15B . . 107.9 ? C16 C15 H15A . . 109.2 ? C16 C15 H15B . . 109.2 ? C11 C16 H16A . . 109.2 ? C11 C16 H16B . . 109.2 ? C15 C16 C11 . . 112.0(3) ? C15 C16 H16A . . 109.2 ? C15 C16 H16B . . 109.2 ? H16A C16 H16B . . 107.9 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag N1 C1 . 1.383(4) ? N1 C2 . 1.372(4) ? N1 H1 . 0.864(14) ? N2 C10 . 1.467(4) ? N2 C11 . 1.464(4) ? N2 H2 . 0.912(14) ? C1 H1A . 0.9300 ? C1 C8 . 1.357(5) ? C2 C3 . 1.388(4) ? C2 C7 . 1.410(4) ? C3 H3 . 0.9300 ? C3 C4 . 1.375(5) ? C4 H4 . 0.9300 ? C4 C5 . 1.382(5) ? C5 H5 . 0.9300 ? C5 C6 . 1.364(5) ? C6 H6 . 0.9300 ? C6 C7 . 1.408(5) ? C7 C8 . 1.428(5) ? C8 C9 . 1.505(4) ? C9 H9A . 0.9700 ? C9 H9B . 0.9700 ? C9 C10 . 1.452(5) ? C10 H10A . 0.9700 ? C10 H10B . 0.9700 ? C11 H11 . 0.9800 ? C11 C12 . 1.523(4) ? C11 C16 . 1.524(4) ? C12 H12A . 0.9700 ? C12 H12B . 0.9700 ? C12 C13 . 1.514(5) ? C13 H13A . 0.9700 ? C13 H13B . 0.9700 ? C13 C14 . 1.508(6) ? C14 H14A . 0.9700 ? C14 H14B . 0.9700 ? C14 C15 . 1.497(6) ? C15 H15A . 0.9700 ? C15 H15B . 0.9700 ? C15 C16 . 1.521(5) ? C16 H16A . 0.9700 ? C16 H16B . 0.9700 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag N1 H1 N2 2_646 0.864(14) 2.222(16) 3.069(4) 167(3) yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag N1 C1 C8 C7 . . . . -0.6(4) ? N1 C1 C8 C9 . . . . 178.0(3) ? N1 C2 C3 C4 . . . . 178.7(3) ? N1 C2 C7 C6 . . . . 179.9(3) ? N1 C2 C7 C8 . . . . 0.2(3) ? N2 C11 C12 C13 . . . . -179.1(3) ? N2 C11 C16 C15 . . . . -178.4(3) ? C1 N1 C2 C3 . . . . -179.5(3) ? C1 N1 C2 C7 . . . . -0.5(3) ? C1 C8 C9 C10 . . . . 47.2(6) ? C2 N1 C1 C8 . . . . 0.7(4) ? C2 C3 C4 C5 . . . . 1.2(5) ? C2 C7 C8 C1 . . . . 0.2(3) ? C2 C7 C8 C9 . . . . -178.4(3) ? C3 C2 C7 C6 . . . . -1.0(4) ? C3 C2 C7 C8 . . . . 179.3(3) ? C3 C4 C5 C6 . . . . -1.0(5) ? C4 C5 C6 C7 . . . . -0.2(5) ? C5 C6 C7 C2 . . . . 1.1(4) ? C5 C6 C7 C8 . . . . -179.2(3) ? C6 C7 C8 C1 . . . . -179.4(3) ? C6 C7 C8 C9 . . . . 1.9(5) ? C7 C2 C3 C4 . . . . -0.2(4) ? C7 C8 C9 C10 . . . . -134.5(4) ? C8 C9 C10 N2 . . . . 170.4(4) ? C10 N2 C11 C12 . . . . -56.0(4) ? C10 N2 C11 C16 . . . . -179.0(3) ? C11 N2 C10 C9 . . . . 156.9(4) ? C11 C12 C13 C14 . . . . 58.1(4) ? C12 C11 C16 C15 . . . . 54.9(4) ? C12 C13 C14 C15 . . . . -56.4(4) ? C13 C14 C15 C16 . . . . 54.5(4) ? C14 C15 C16 C11 . . . . -54.9(4) ? C16 C11 C12 C13 . . . . -56.5(4) ? _cod_database_fobs_code 2022826