#------------------------------------------------------------------------------ #$Date: 2023-07-22 03:59:02 +0200 (Sat, 22 Jul 2023) $ #$Revision: 285320 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/28/2022824.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022824 loop_ _publ_author_name 'Madhan, S.' 'NizamMohideen, M.' 'Pavunkumar, Vinayagam' 'MohanaKrishnan, Arasambattu K.' _publ_section_title ; Crystal-structure determination and Hirshfeld surface analysis of two new thiophene derivatives: (E)-N-{2-[2-(benzo[b]thiophen-2-yl)ethenyl]-5-fluorophenyl}benzenesulfonamide and (E)-N-{2-[2-(benzo[b]thiophen-2-yl)ethenyl]-5-fluorophenyl}-N-(but-2-yn-1-yl)benzenesulfonamide ; _journal_coeditor_code ZN2029 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E Crystallographic Communications' _journal_paper_doi 10.1107/S2056989023006096 _journal_volume 79 _journal_year 2023 _chemical_formula_iupac 'C26 H20 F N O2 S2' _chemical_formula_moiety 'C26 H20 F N O2 S2' _chemical_formula_sum 'C26 H20 F N O2 S2' _chemical_formula_weight 461.55 _chemical_name_systematic (E)-N-{2-[2-(Benzo[b]thiophen-2-yl)ethenyl]-5-fluorophenyl}-N-(but-2-yn-1-yl)benzenesulfonamide _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 115.179(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 9.3517(3) _cell_length_b 31.7075(11) _cell_length_c 8.6063(3) _cell_measurement_reflns_used 3616 _cell_measurement_temperature 297(2) _cell_measurement_theta_max 65.44 _cell_measurement_theta_min 2.79 _cell_volume 2309.45(14) _computing_cell_refinement ; SAINT (Bruker, 2016) ; _computing_data_collection ; APEX2 (Bruker, 2016) ; _computing_data_reduction ; SAINT (Bruker, 2016) ; _computing_molecular_graphics ; ORTEP-3 for Windows (Farrugia, 2012) and Mercury (Macrae et al., 2020) ; _computing_publication_material ; WinGX (Farrugia, 2012), publCIF (Westrip, 2010) and PLATON (Spek, 2020) ; _computing_structure_refinement ; SHELXL2018/3 (Sheldrick, 2015) ; _computing_structure_solution ; SHELXS2018/3 (Sheldrick, 2008) ; _diffrn_ambient_temperature 297(2) _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_device_type 'Bruker D8 Venture Diffractometer' _diffrn_measurement_method '\w and \f scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.1554 _diffrn_reflns_av_unetI/netI 0.0598 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 38 _diffrn_reflns_limit_k_min -37 _diffrn_reflns_limit_l_max 10 _diffrn_reflns_limit_l_min -10 _diffrn_reflns_number 39443 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 68.811 _diffrn_reflns_theta_min 5.226 _diffrn_source 'micro focus sealed tube' _exptl_absorpt_coefficient_mu 2.350 _exptl_absorpt_correction_T_max 0.7531 _exptl_absorpt_correction_T_min 0.6039 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Bruker, 2016) ; _exptl_crystal_colour White _exptl_crystal_density_diffrn 1.327 _exptl_crystal_description Solid _exptl_crystal_F_000 960 _exptl_crystal_size_max 0.112 _exptl_crystal_size_mid 0.072 _exptl_crystal_size_min 0.016 _refine_diff_density_max 0.334 _refine_diff_density_min -0.375 _refine_ls_extinction_coef 0.0040(6) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method ; SHELXL-2018/3 (Sheldrick 2015) ; _refine_ls_goodness_of_fit_ref 0.998 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 291 _refine_ls_number_reflns 4270 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.998 _refine_ls_R_factor_all 0.1353 _refine_ls_R_factor_gt 0.0659 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1325P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1661 _refine_ls_wR_factor_ref 0.2324 _reflns_number_gt 2098 _reflns_number_total 4270 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file zn2029sup1.cif _cod_data_source_block II _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 2022824 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.779 _shelx_estimated_absorpt_t_max 0.963 _shelx_hkl_file ; 0 0 -1 -1.50 1.10 0 0 -1 0.30 1.40 0 0 -2 4349.86 85.69 0 0 -2 4403.96 87.39 0 0 -3 -3.50 2.90 0 0 -3 0.50 2.60 0 0 -3 -1.90 2.70 0 0 -4 779.52 29.70 0 0 -4 794.42 34.00 0 0 -4 809.92 32.70 0 0 4 794.52 29.20 0 0 -4 769.82 28.00 0 0 5 -10.40 6.30 0 0 5 3.70 4.60 0 0 -5 -2.80 5.90 0 0 5 -5.70 6.90 0 0 -5 -3.10 4.20 0 0 -5 2.80 4.90 0 0 -5 -8.40 7.40 0 0 -5 -2.10 4.10 0 0 5 6.40 6.50 0 0 -5 -2.20 6.80 0 0 6 232.98 19.80 0 0 -6 212.08 20.90 0 0 -6 215.38 18.10 0 0 -6 194.68 19.60 0 0 -6 211.88 22.70 0 0 -6 173.48 25.30 0 0 6 219.08 19.50 0 0 6 202.78 20.40 0 0 -6 213.68 20.40 0 0 -7 2.00 6.00 0 0 -7 -12.90 10.60 0 0 7 8.20 7.00 0 0 -7 -9.30 5.90 0 0 -7 0.20 8.20 0 0 7 -11.00 5.90 0 0 -7 -7.00 26.00 0 0 -7 2.80 6.80 0 0 8 3.80 4.60 0 0 -8 12.00 7.80 0 0 -8 3.80 7.40 0 0 -8 3.10 6.50 0 0 8 8.90 6.60 0 0 9 -2.90 2.30 0 0 -9 4.30 5.90 0 0 -9 -2.50 8.60 0 0 9 10.30 6.70 0 1 -1 2475.35 47.80 0 1 -1 2435.16 47.00 0 -1 -1 2418.56 47.70 0 -1 -1 2393.76 46.80 0 1 -2 86.79 7.60 0 1 -2 90.29 7.20 0 -1 -2 74.09 6.60 0 -1 -2 86.69 7.80 0 1 -3 16.10 4.90 0 1 -3 13.10 5.50 0 -1 -3 27.30 6.20 0 -1 -3 27.00 6.30 0 1 -4 92.19 12.50 0 1 4 85.89 10.50 0 1 -4 91.99 11.40 0 1 -4 92.49 10.20 0 1 -4 80.49 9.60 0 -1 -4 90.09 12.20 0 -1 4 96.29 11.10 0 -1 -4 87.89 10.00 0 -1 -4 81.49 10.00 0 -1 -4 100.09 11.60 0 1 -5 68.59 13.90 0 1 -5 34.70 8.70 0 1 5 30.20 7.60 0 1 -5 38.30 8.60 0 1 5 67.39 13.30 0 1 -5 36.10 10.50 0 1 -5 27.80 7.40 0 1 -5 42.10 8.10 0 1 5 52.79 10.80 0 -1 -5 42.90 8.20 0 -1 -5 41.30 12.00 0 -1 -5 68.79 11.80 0 -1 5 14.90 7.70 0 -1 -5 44.30 10.70 0 -1 -5 50.49 11.50 0 -1 5 64.19 15.20 0 -1 5 54.39 10.10 0 -1 -5 41.40 8.80 0 -1 5 24.50 8.90 0 1 -6 48.10 13.40 0 1 -6 49.00 12.70 0 1 -6 91.49 15.00 0 1 -6 43.40 10.80 0 1 -6 49.70 9.40 0 1 -6 73.09 14.70 0 1 6 75.59 14.20 0 1 6 80.09 16.20 0 1 6 54.69 10.70 0 -1 6 92.99 14.10 0 -1 6 33.20 10.10 0 -1 -6 94.79 16.80 0 -1 -6 18.30 11.60 0 -1 -6 50.19 11.10 0 -1 6 76.89 13.80 0 -1 -6 52.89 12.30 0 1 -7 -6.70 20.20 0 1 7 -5.20 5.00 0 1 -7 6.30 7.60 0 1 -7 0.30 10.30 0 1 -7 4.20 7.20 0 1 -7 0.80 6.40 0 1 -7 -3.80 4.60 0 1 7 -0.50 5.90 0 -1 7 0.50 5.30 0 -1 -7 3.10 7.00 0 -1 -7 0.90 6.40 0 -1 -7 -19.70 8.90 0 -1 -7 -3.70 4.90 0 -1 -7 5.80 8.10 0 -1 7 -2.60 6.30 0 1 -8 3.60 7.40 0 1 -8 14.40 6.60 0 1 8 14.80 8.10 0 1 8 26.80 7.70 0 1 -8 7.40 6.40 0 -1 -8 32.50 8.40 0 -1 -8 36.60 10.10 0 -1 -8 16.70 9.30 0 -1 8 34.00 10.80 0 -1 8 21.00 7.40 0 1 -9 -9.30 7.60 0 1 9 5.00 3.60 0 1 -9 1.80 4.00 0 1 9 7.60 6.30 0 -1 9 4.30 4.50 0 -1 9 2.60 7.20 0 -1 -9 2.70 4.70 0 -1 -9 -1.30 8.70 0 2 -1 648.94 17.10 0 2 -1 689.33 17.70 0 -2 -1 658.43 17.70 0 -2 -1 666.43 16.90 0 2 -2 300.57 14.10 0 2 -2 318.97 13.60 0 -2 -2 303.07 13.10 0 -2 -2 304.37 13.00 0 -2 -2 304.87 14.30 0 2 -3 464.45 20.60 0 2 -3 444.06 21.40 0 -2 -3 457.25 21.50 0 -2 -3 427.26 19.50 0 2 -4 79.59 9.70 0 2 -4 58.69 11.00 0 2 -4 73.89 9.50 0 2 -4 82.79 11.10 0 2 4 95.19 10.50 0 2 4 93.89 9.70 0 -2 4 89.29 10.60 0 -2 -4 93.79 11.60 0 -2 -4 71.09 9.50 0 -2 -4 65.99 9.70 0 -2 -4 89.09 9.70 0 2 5 62.89 11.60 0 2 -5 37.70 8.80 0 2 -5 45.90 10.90 0 2 5 38.10 7.70 0 2 -5 38.90 8.70 0 2 5 63.89 12.60 0 2 -5 46.70 8.60 0 2 -5 39.60 11.20 0 2 -5 69.49 14.20 0 2 5 62.29 12.10 0 -2 5 47.30 10.40 0 -2 -5 80.29 13.80 0 -2 -5 40.10 9.40 0 -2 -5 44.40 8.90 0 -2 -5 55.59 9.40 0 -2 -5 69.49 14.20 0 -2 5 67.99 12.90 0 2 6 64.29 12.40 0 2 6 94.39 18.20 0 2 -6 95.79 13.10 0 2 -6 72.39 15.30 0 2 6 72.39 10.70 0 2 -6 66.59 16.60 0 2 -6 77.99 14.30 0 2 -6 91.79 14.50 0 2 -6 57.09 11.50 0 -2 -6 46.50 10.30 0 -2 -6 67.09 11.60 0 -2 -6 55.09 11.70 0 -2 6 87.89 13.30 0 -2 6 72.79 13.30 0 -2 6 80.29 12.20 0 -2 -6 27.70 13.70 0 -2 -6 89.19 16.60 0 -2 -6 55.59 12.90 0 2 -7 -7.90 10.70 0 2 7 -4.80 8.60 0 2 -7 -2.20 5.00 0 2 -7 -16.10 5.70 0 2 -7 -0.30 5.20 0 2 7 -0.50 6.50 0 2 -7 -1.10 7.70 0 2 -7 -14.00 19.70 0 -2 -7 4.40 6.40 0 -2 7 -2.30 6.70 0 -2 7 -2.60 5.70 0 -2 -7 5.20 7.40 0 -2 -7 3.00 10.10 0 -2 -7 18.80 8.10 0 -2 -7 4.00 8.10 0 2 8 -6.30 5.40 0 2 -8 0.00 6.70 0 2 8 7.70 4.70 0 2 -8 -1.70 4.90 0 2 -8 -4.80 5.60 0 -2 -8 -4.20 5.40 0 -2 8 -7.50 6.10 0 -2 8 -6.70 3.80 0 -2 -8 -0.90 6.70 0 -2 -8 -9.20 8.10 0 2 -9 9.10 5.00 0 2 -9 1.30 8.30 0 2 9 2.40 4.90 0 2 9 1.70 2.60 0 -2 9 8.10 10.40 0 -2 -9 -4.60 7.30 0 -2 9 0.60 3.40 0 -2 -9 3.80 5.00 0 3 0 0.80 1.00 0 3 0 0.10 1.00 0 -3 0 -1.30 1.00 0 -3 0 0.20 0.80 0 3 -1 588.94 16.60 0 3 -1 582.54 16.10 0 -3 -1 565.84 15.50 0 -3 -1 600.64 16.90 0 3 -2 2.20 2.50 0 3 -2 0.70 2.10 0 -3 -2 -0.30 2.30 0 -3 -2 -0.80 1.80 0 -3 -2 -0.90 2.70 0 3 -3 786.22 28.40 0 3 -3 826.72 30.10 0 -3 -3 808.82 29.80 0 -3 -3 808.32 27.90 0 3 4 128.89 11.20 0 3 -4 114.39 13.30 0 3 -4 111.59 12.40 0 3 4 114.69 11.00 0 3 -4 103.29 10.70 0 3 -4 109.29 10.70 0 -3 -4 132.39 13.20 0 -3 -4 117.59 11.10 0 -3 -4 127.79 11.90 0 -3 4 110.49 11.30 0 -3 -4 90.19 13.10 0 3 5 8.50 7.20 0 3 -5 16.90 7.80 0 3 -5 14.10 8.50 0 3 5 16.40 7.30 0 3 -5 27.90 9.80 0 3 5 27.40 10.20 0 3 -5 22.40 5.90 0 3 -5 17.70 6.90 0 3 5 20.50 7.00 0 3 -5 16.30 5.50 0 -3 -5 8.00 6.10 0 -3 -5 14.90 9.70 0 -3 -5 26.40 7.60 0 -3 -5 16.10 6.10 0 -3 -5 17.00 8.20 0 -3 5 6.10 7.10 0 -3 5 18.40 7.50 0 -3 -5 9.00 7.10 0 -3 5 18.80 6.50 0 3 6 31.90 9.00 0 3 6 88.79 15.40 0 3 -6 49.90 14.00 0 3 -6 43.50 10.70 0 3 6 63.39 13.50 0 3 -6 49.50 11.70 0 3 -6 38.30 11.30 0 3 -6 55.39 12.50 0 3 -6 34.80 8.90 0 -3 -6 28.10 8.20 0 -3 -6 40.30 9.50 0 -3 6 53.79 11.90 0 -3 6 49.30 10.60 0 -3 -6 86.49 17.00 0 -3 -6 34.60 13.00 0 -3 6 46.90 10.30 0 -3 -6 53.29 12.40 0 -3 -6 27.00 12.70 0 3 -7 142.69 24.00 0 3 -7 147.79 17.50 0 3 -7 111.69 16.80 0 3 7 118.59 16.30 0 3 -7 149.39 17.00 0 3 7 123.59 15.60 0 -3 -7 106.09 18.80 0 -3 -7 153.28 18.80 0 -3 -7 136.89 28.20 0 -3 -7 111.19 17.30 0 -3 7 138.69 17.30 0 -3 7 136.99 16.80 0 -3 -7 164.88 18.50 0 3 -8 13.70 7.70 0 3 -8 7.30 5.20 0 3 8 13.60 7.40 0 3 8 22.70 7.30 0 3 -8 12.60 11.60 0 3 -8 15.20 8.30 0 -3 -8 8.40 7.80 0 -3 -8 12.00 8.80 0 -3 8 22.00 8.70 0 -3 8 12.70 6.80 0 3 9 4.90 3.00 0 3 -9 7.90 4.40 0 3 9 5.40 5.40 0 3 -9 11.30 7.80 0 -3 -9 12.20 5.90 0 -3 9 17.50 11.90 0 -3 -9 12.20 8.30 0 -3 9 2.60 3.10 0 4 0 119.19 6.10 0 4 0 130.59 6.20 0 -4 0 125.19 5.60 0 -4 0 129.59 6.10 0 4 -1 524.35 16.00 0 -4 -1 531.45 16.10 0 -4 -1 529.55 15.10 0 -4 1 519.65 14.50 0 4 -2 49.70 6.50 0 4 -2 50.99 5.90 0 -4 -2 63.79 6.60 0 -4 -2 48.30 6.30 0 -4 -2 51.19 6.00 0 4 -3 807.42 28.70 0 4 -3 767.72 23.50 0 4 -3 804.02 30.10 0 -4 -3 809.62 28.20 0 -4 -3 851.51 30.80 0 4 4 36.20 6.50 0 4 -4 48.60 10.50 0 4 -4 54.49 9.40 0 4 -4 36.80 7.80 0 4 4 55.19 10.00 0 4 -4 42.40 7.20 0 -4 -4 41.50 8.70 0 -4 -4 49.90 9.20 0 -4 -4 61.69 9.50 0 4 -5 50.09 12.00 0 4 -5 65.99 15.20 0 4 5 71.99 10.30 0 4 -5 59.99 11.20 0 4 5 45.00 8.20 0 4 -5 47.80 8.30 0 4 5 47.10 9.30 0 4 -5 41.30 8.90 0 4 5 85.59 14.10 0 4 -5 51.39 10.80 0 -4 -5 53.39 10.90 0 -4 -5 29.40 11.50 0 -4 -5 58.69 11.10 0 -4 5 75.49 12.30 0 -4 -5 51.89 11.50 0 -4 5 57.19 10.40 0 -4 5 63.59 13.10 0 -4 -5 75.19 14.80 0 -4 -5 59.69 9.90 0 4 6 1.60 6.40 0 4 -6 -4.40 6.90 0 4 -6 -5.60 5.50 0 4 -6 13.10 11.00 0 4 6 -0.30 5.40 0 4 -6 2.40 4.90 0 4 6 -10.80 10.20 0 4 6 9.10 7.50 0 4 -6 -3.90 4.90 0 4 -6 4.70 8.10 0 -4 6 4.90 7.10 0 -4 -6 7.60 7.70 0 -4 -6 -15.80 16.60 0 -4 -6 4.80 6.50 0 -4 -6 5.70 7.40 0 -4 6 3.80 10.00 0 -4 -6 -0.60 5.90 0 -4 -6 4.60 5.50 0 -4 6 2.10 5.10 0 4 -7 -1.60 15.80 0 4 -7 1.30 7.10 0 4 7 2.90 6.00 0 4 7 -3.70 6.20 0 4 -7 -0.20 10.10 0 4 -7 6.60 5.80 0 4 -7 -5.10 5.60 0 -4 7 -1.80 8.00 0 -4 -7 9.10 10.60 0 -4 -7 -3.10 7.00 0 -4 7 -6.20 6.20 0 -4 -7 -13.10 7.00 0 -4 -7 -12.10 11.30 0 4 -8 1.10 10.10 0 4 -8 -1.50 4.00 0 4 -8 4.30 7.20 0 4 8 -1.90 5.20 0 4 8 3.80 6.30 0 4 -8 -1.40 5.40 0 -4 8 4.10 4.40 0 -4 -8 5.50 6.80 0 -4 8 -1.20 8.00 0 -4 -8 -2.00 7.10 0 4 9 -1.40 4.20 0 4 9 1.10 3.30 0 4 -9 -8.00 8.10 0 4 -9 -1.70 4.10 0 4 9 15.20 11.00 0 -4 -9 -9.50 7.80 0 -4 9 1.50 3.20 0 -4 -9 -8.40 3.90 0 5 0 0.90 1.60 0 5 0 -0.10 1.60 0 -5 0 -0.40 1.40 0 -5 0 1.30 1.90 0 5 -1 20.10 3.70 0 5 -1 19.30 3.70 0 5 1 30.20 4.30 0 -5 1 24.60 3.60 0 -5 -1 27.40 4.60 0 -5 1 24.80 3.40 0 -5 -1 23.40 3.80 0 5 -2 161.38 11.00 0 5 -2 180.78 10.70 0 -5 -2 167.08 11.30 0 -5 -2 178.28 10.60 0 -5 -2 163.98 10.10 0 5 -3 149.88 12.60 0 5 -3 128.49 8.40 0 -5 -3 131.19 11.00 0 -5 -3 134.49 12.00 0 5 -4 73.69 10.00 0 5 -4 67.49 9.20 0 5 4 56.59 8.80 0 5 -4 80.39 11.10 0 5 -4 86.99 10.10 0 5 4 71.99 10.00 0 5 -4 75.89 13.10 0 -5 -4 76.39 10.50 0 -5 -4 54.59 9.90 0 -5 -4 85.39 12.50 0 -5 4 69.99 9.80 0 -5 -4 69.59 9.90 0 5 -5 39.80 9.80 0 5 5 25.00 7.30 0 5 -5 37.30 8.80 0 5 -5 36.40 8.40 0 5 5 72.39 13.40 0 5 5 51.69 10.70 0 5 -5 29.40 11.00 0 5 -5 32.30 9.60 0 5 -5 41.30 9.90 0 5 5 32.70 8.40 0 -5 -5 44.30 10.00 0 -5 5 62.39 11.80 0 -5 -5 33.30 8.60 0 -5 5 48.70 11.60 0 -5 -5 26.50 11.60 0 -5 -5 51.89 9.80 0 -5 -5 67.69 13.70 0 -5 -5 38.20 10.30 0 5 6 2.00 8.50 0 5 -6 2.80 6.00 0 5 -6 -2.90 10.50 0 5 6 30.10 10.00 0 5 -6 4.60 8.50 0 5 -6 9.90 7.50 0 5 -6 18.50 10.60 0 5 6 1.70 4.80 0 5 -6 15.00 7.00 0 -5 6 15.10 13.30 0 -5 -6 12.20 7.40 0 -5 -6 12.50 11.00 0 -5 6 7.50 5.70 0 -5 6 7.60 8.90 0 -5 -6 -26.40 25.90 0 -5 -6 11.30 10.00 0 -5 -6 16.80 7.50 0 -5 -6 0.80 6.20 0 5 7 76.29 14.40 0 5 7 105.19 15.50 0 5 -7 104.99 16.20 0 5 -7 80.39 18.90 0 5 -7 120.29 25.60 0 5 -7 121.89 15.10 0 5 -7 61.99 13.10 0 -5 -7 88.69 19.50 0 -5 -7 86.39 13.70 0 -5 -7 106.99 15.80 0 -5 -7 99.79 16.90 0 -5 -7 115.59 22.20 0 -5 7 94.39 13.80 0 -5 7 111.99 17.70 0 5 -8 -25.60 9.00 0 5 8 -5.00 5.00 0 5 -8 -3.30 4.80 0 5 8 0.80 5.60 0 5 -8 -5.90 6.00 0 -5 -8 7.80 7.10 0 -5 8 -2.20 3.50 0 -5 8 13.90 8.50 0 -5 -8 6.90 6.80 0 5 9 -2.50 6.60 0 5 9 3.30 3.60 0 5 -9 0.80 3.70 0 5 9 0.90 2.50 0 5 -9 3.30 17.40 0 -5 9 3.20 3.60 0 -5 -9 3.20 5.70 0 -5 -9 -1.80 8.20 0 6 0 2166.68 44.30 0 6 0 2084.69 43.90 0 -6 0 2073.69 43.30 0 -6 0 2016.20 42.60 0 6 1 60.19 6.10 0 6 -1 59.09 5.70 0 6 -1 58.39 5.80 0 -6 1 65.49 5.30 0 -6 1 53.69 4.80 0 -6 -1 53.39 5.90 0 -6 -1 58.39 5.40 0 6 -2 49.90 6.80 0 -6 -2 50.49 6.40 0 -6 2 39.60 5.80 0 -6 -2 47.40 6.80 0 -6 -2 40.60 6.00 0 6 -3 -1.40 2.90 0 6 -3 -3.20 2.80 0 6 3 10.60 4.70 0 6 -3 2.00 3.30 0 -6 -3 1.40 3.30 0 -6 -3 -2.90 3.70 0 6 -4 40.80 7.50 0 6 4 49.80 8.70 0 6 -4 48.70 10.90 0 6 -4 66.49 9.00 0 6 -4 50.59 10.40 0 6 4 55.79 8.80 0 -6 4 45.50 8.10 0 -6 -4 62.69 11.80 0 -6 -4 48.10 9.60 0 -6 -4 32.30 7.80 0 -6 4 55.29 10.90 0 -6 -4 33.80 6.70 0 6 -5 35.70 11.40 0 6 5 30.50 7.60 0 6 5 44.90 11.80 0 6 5 32.80 8.70 0 6 -5 42.40 11.40 0 6 5 54.49 10.60 0 6 -5 34.00 8.40 0 6 -5 30.00 8.30 0 6 -5 33.70 7.70 0 6 -5 27.40 9.00 0 -6 -5 37.00 8.60 0 -6 5 30.10 8.50 0 -6 -5 45.90 10.20 0 -6 -5 49.20 11.50 0 -6 -5 32.30 11.30 0 -6 -5 32.30 8.00 0 -6 -5 44.00 12.20 0 -6 5 44.60 10.90 0 6 6 62.69 10.20 0 6 -6 50.09 11.50 0 6 -6 60.49 13.10 0 6 6 71.49 13.70 0 6 6 64.89 14.50 0 6 -6 43.70 9.50 0 6 6 81.89 13.50 0 6 -6 45.20 9.50 0 6 -6 63.89 14.80 0 6 -6 25.30 12.90 0 -6 -6 61.79 11.20 0 -6 -6 34.30 10.60 0 -6 6 67.29 13.90 0 -6 6 50.79 11.70 0 -6 -6 99.59 18.40 0 -6 -6 69.79 11.90 0 -6 -6 51.79 12.80 0 -6 6 41.00 10.10 0 6 -7 5.50 6.80 0 6 7 11.30 7.20 0 6 -7 15.30 7.60 0 6 -7 -17.60 17.20 0 6 7 10.50 7.70 0 6 -7 8.00 6.80 0 6 -7 17.10 9.30 0 6 -7 17.70 11.60 0 -6 -7 18.80 8.40 0 -6 -7 -3.80 7.90 0 -6 7 1.40 7.90 0 -6 -7 21.50 14.20 0 -6 7 11.00 7.40 0 -6 -7 1.20 8.90 0 6 -8 8.30 6.20 0 6 -8 17.00 10.70 0 6 8 16.50 6.70 0 6 8 12.90 5.90 0 6 8 11.60 5.40 0 6 -8 11.30 7.00 0 6 -8 13.80 5.50 0 -6 -8 3.70 6.90 0 -6 8 2.80 10.00 0 -6 8 5.70 5.10 0 -6 -8 23.50 9.10 0 6 9 -0.90 3.30 0 6 9 3.00 3.50 0 6 9 2.50 6.30 0 6 -9 -2.20 3.50 0 -6 9 3.10 3.40 0 -6 -9 -3.90 14.20 0 -6 -9 -3.10 4.70 0 7 0 3.00 2.50 0 7 0 1.70 2.20 0 -7 0 3.50 2.50 0 -7 0 0.50 1.90 0 7 -1 126.89 8.60 0 7 -1 138.49 8.90 0 7 1 130.59 8.70 0 -7 1 123.09 7.70 0 -7 -1 124.29 8.00 0 -7 -1 131.79 8.90 0 -7 1 138.19 7.50 0 7 -2 549.25 21.50 0 7 -2 535.55 20.80 0 -7 -2 519.25 19.80 0 -7 -2 530.55 20.90 0 -7 2 521.15 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6 40.20 11.30 0 -7 6 33.70 10.30 0 -7 6 41.70 10.50 0 -7 -6 51.59 12.40 0 -7 -6 42.80 11.20 0 -7 6 30.90 12.40 0 -7 6 31.50 13.10 0 7 7 -3.00 5.00 0 7 7 -4.20 5.70 0 7 -7 -7.90 11.00 0 7 -7 -6.80 5.90 0 7 -7 -5.20 5.90 0 7 -7 -3.40 5.30 0 7 -7 -2.30 7.10 0 7 -7 14.80 18.30 0 -7 -7 -1.40 7.60 0 -7 -7 -9.20 5.90 0 -7 7 -11.40 7.20 0 -7 -7 6.60 10.00 0 -7 -7 7.20 13.30 0 -7 7 -14.50 8.60 0 -7 7 -4.20 5.40 0 7 8 0.50 4.70 0 7 -8 9.00 6.60 0 7 -8 6.60 4.90 0 7 -8 6.10 7.60 0 7 8 6.70 5.40 0 7 -8 2.60 8.80 0 7 8 0.60 4.30 0 -7 -8 23.40 10.10 0 -7 -8 12.80 6.70 0 -7 8 7.20 5.60 0 -7 8 15.10 12.50 0 7 9 -0.70 5.50 0 7 9 7.00 4.10 0 7 -9 8.30 4.40 0 7 9 6.00 3.80 0 -7 -9 8.30 4.80 0 -7 9 6.00 2.90 0 8 0 9999.00 178.68 0 8 0 9969.00 178.88 0 -8 0 9926.91 177.18 0 -8 0 9767.82 177.48 0 8 1 408.86 16.60 0 8 -1 398.06 16.30 0 8 -1 405.46 16.50 0 -8 1 414.16 14.40 0 -8 -1 409.16 15.60 0 -8 -1 425.76 18.80 0 -8 -1 412.46 16.60 0 -8 1 421.46 15.50 0 8 -2 617.44 23.60 0 8 -2 629.14 23.20 0 8 -2 598.94 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5.20 0 -10 -2 26.80 5.90 0 -10 2 33.80 5.80 0 -10 -2 32.90 7.50 0 10 -3 162.08 14.30 0 10 -3 158.08 13.60 0 10 -3 151.78 12.00 0 10 -3 155.18 10.70 0 10 3 170.78 13.30 0 -10 3 164.58 13.60 0 -10 3 170.98 12.40 0 -10 -3 162.78 15.30 0 -10 -3 161.08 13.50 0 10 -4 61.29 9.70 0 10 4 66.69 9.70 0 10 -4 52.49 10.80 0 10 -4 50.59 10.30 0 10 4 62.99 10.40 0 10 -4 49.60 11.60 0 10 -4 72.29 8.80 0 10 -4 40.80 10.70 0 10 4 80.19 11.50 0 -10 -4 91.39 15.40 0 -10 -4 44.10 9.40 0 -10 -4 49.40 11.30 0 -10 -4 66.59 12.00 0 -10 4 55.99 13.50 0 -10 -4 59.99 9.80 0 -10 4 52.49 9.30 0 -10 4 80.49 11.90 0 10 5 298.37 21.00 0 10 -5 268.37 17.80 0 10 5 329.17 22.20 0 10 -5 285.17 22.50 0 10 5 287.47 23.30 0 10 -5 333.17 22.80 0 10 -5 318.77 26.40 0 10 -5 324.17 26.90 0 10 -5 304.47 21.00 0 10 -5 304.57 24.40 0 10 5 323.27 19.80 0 -10 -5 333.87 38.80 0 -10 5 321.27 20.80 0 -10 -5 287.97 24.00 0 -10 -5 281.47 23.10 0 -10 5 344.37 23.20 0 -10 -5 296.87 23.50 0 -10 -5 325.87 24.10 0 -10 5 273.67 20.00 0 -10 5 269.27 21.10 0 10 6 4.00 6.10 0 10 -6 -5.00 11.20 0 10 -6 -2.80 5.60 0 10 6 1.30 5.60 0 10 6 6.60 6.90 0 10 -6 8.90 7.80 0 10 -6 8.00 6.20 0 10 -6 1.50 8.10 0 10 -6 11.10 6.50 0 10 6 3.30 7.90 0 -10 -6 6.10 10.50 0 -10 -6 -3.10 10.10 0 -10 6 5.00 6.50 0 -10 6 -0.20 8.30 0 -10 -6 1.90 7.20 0 -10 6 -3.30 7.70 0 -10 -6 6.90 6.10 0 -10 6 -8.20 12.10 0 -10 6 -9.30 16.40 0 10 -7 4.80 6.00 0 10 -7 2.90 6.40 0 10 7 0.20 5.70 0 10 -7 -12.40 20.50 0 10 -7 -2.70 12.00 0 10 -7 1.90 7.90 0 10 7 9.60 7.90 0 10 7 1.50 7.50 0 10 -7 0.90 4.90 0 -10 7 7.60 11.60 0 -10 7 -0.80 8.00 0 -10 7 1.60 5.30 0 -10 -7 -1.50 7.20 0 -10 -7 -2.80 15.40 0 -10 -7 -6.90 6.10 0 10 -8 -9.40 4.20 0 10 -8 -4.40 7.90 0 10 -8 -9.80 6.30 0 10 -8 1.30 3.70 0 10 8 2.80 4.70 0 10 8 -2.90 3.90 0 10 8 0.10 4.10 0 -10 -8 5.90 5.90 0 -10 -8 9.60 9.10 0 -10 8 -1.60 3.30 0 10 -9 3.60 3.70 0 10 9 3.10 3.30 0 10 9 2.70 3.50 0 -10 -9 2.90 3.80 0 -10 9 0.70 1.90 0 -10 -9 -4.20 3.60 0 11 0 -1.80 2.70 0 11 0 0.20 3.00 0 -11 0 4.60 4.00 0 -11 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34.60 11.90 0 11 -5 18.80 7.90 0 -11 -5 15.60 9.10 0 -11 5 4.10 13.50 0 -11 5 21.40 7.90 0 -11 -5 15.70 10.50 0 -11 -5 -8.20 20.50 0 -11 5 14.50 9.90 0 -11 -5 20.40 9.00 0 -11 -5 19.80 11.40 0 -11 -5 8.20 7.90 0 -11 5 19.70 8.60 0 11 6 10.10 6.90 0 11 6 18.30 7.50 0 11 6 4.90 10.50 0 11 -6 12.50 11.10 0 11 6 3.80 8.80 0 11 -6 12.20 7.50 0 11 -6 5.20 6.70 0 11 -6 -20.30 12.80 0 11 -6 12.80 7.00 0 11 -6 6.40 7.90 0 -11 6 -16.80 8.50 0 -11 -6 12.30 8.30 0 -11 6 18.00 9.00 0 -11 -6 16.70 12.50 0 -11 -6 11.40 9.40 0 -11 -6 10.50 11.60 0 -11 6 7.20 8.70 0 11 -7 -2.60 5.70 0 11 7 11.50 6.90 0 11 -7 3.40 14.00 0 11 7 3.80 5.70 0 11 -7 12.70 6.60 0 11 -7 -23.40 23.00 0 11 -7 -9.10 6.40 0 11 7 0.90 6.00 0 11 -7 0.10 5.50 0 -11 7 13.30 8.10 0 -11 7 0.60 5.50 0 -11 -7 -7.80 17.80 0 -11 -7 4.00 6.90 0 -11 -7 8.10 7.00 0 -11 7 6.90 8.80 0 11 8 23.80 6.90 0 11 -8 8.00 4.30 0 11 8 10.20 4.80 0 11 -8 1.40 6.70 0 11 8 10.50 4.50 0 11 -8 4.20 8.10 0 -11 8 14.00 4.90 0 -11 -8 4.10 9.10 0 -11 -8 14.40 6.80 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5.90 0 -15 -3 -4.50 13.40 0 -15 3 -0.20 4.90 0 -15 -3 4.00 5.50 0 -15 3 -2.00 6.60 0 -15 -3 6.40 17.10 0 15 -4 0.20 6.10 0 15 -4 -8.40 9.20 0 15 4 -2.70 4.00 0 15 4 3.90 5.50 0 15 -4 1.30 8.20 0 15 -4 -2.90 7.40 0 15 -4 7.40 4.70 0 15 4 5.60 5.70 0 15 -4 1.10 6.50 0 15 4 -11.80 12.10 0 -15 -4 9.00 8.90 0 -15 4 1.30 6.30 0 -15 4 -2.70 5.70 0 -15 -4 4.00 7.40 0 -15 4 2.00 9.00 0 -15 -4 8.50 7.50 0 15 5 37.40 10.80 0 15 5 30.40 7.90 0 15 -5 27.60 11.00 0 15 -5 18.70 9.90 0 15 -5 47.10 13.80 0 15 -5 13.60 10.00 0 15 -5 24.80 8.60 0 15 -5 35.80 8.70 0 15 5 36.20 8.20 0 15 5 66.29 17.00 0 -15 -5 9.60 11.10 0 -15 5 36.10 7.90 0 -15 -5 30.50 10.00 0 -15 -5 32.80 11.40 0 -15 5 68.79 13.60 0 -15 5 30.90 10.80 0 15 -6 117.59 15.90 0 15 6 132.89 18.00 0 15 -6 74.29 15.00 0 15 6 87.29 15.40 0 15 -6 123.79 23.30 0 15 6 127.49 15.40 0 15 -6 104.89 18.90 0 15 -6 104.49 16.90 0 15 6 138.39 15.20 0 15 -6 120.39 24.80 0 15 6 124.29 14.60 0 -15 -6 121.99 16.60 0 -15 -6 115.49 24.30 0 -15 -6 76.69 22.80 0 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5.30 0 21 -7 5.50 7.90 0 21 7 4.10 5.00 0 21 7 3.00 7.90 0 21 -7 -1.10 5.20 0 -21 7 5.60 4.20 0 -21 7 1.80 5.60 0 -21 -7 -1.10 9.70 0 22 0 116.49 17.80 0 22 0 125.39 15.80 0 22 0 95.39 11.30 0 22 0 117.39 15.40 0 22 0 78.89 10.70 0 22 0 110.89 14.70 0 -22 0 99.79 14.70 0 -22 0 123.89 16.70 0 22 1 76.19 12.60 0 22 1 67.89 9.60 0 22 -1 75.39 13.10 0 22 1 75.79 14.70 0 22 -1 66.49 10.20 0 22 -1 82.39 14.80 0 22 -1 78.89 10.40 0 22 1 58.99 11.00 0 22 -1 67.39 12.00 0 22 1 82.99 10.10 0 22 -1 72.19 16.00 0 22 -1 53.39 12.60 0 -22 1 74.99 16.10 0 -22 -1 79.19 16.00 0 -22 1 89.09 14.40 0 -22 1 43.60 12.50 0 -22 -1 87.19 15.60 0 22 -2 116.49 17.70 0 22 2 116.99 15.90 0 22 -2 100.79 12.10 0 22 2 121.29 16.30 0 22 -2 114.89 17.30 0 22 2 129.79 13.10 0 22 -2 127.59 14.80 0 22 -2 145.39 18.50 0 22 -2 111.69 12.90 0 22 -2 122.89 17.40 0 -22 -2 125.59 17.20 0 -22 2 146.69 19.30 0 -22 2 109.89 15.20 0 -22 2 114.09 16.10 0 22 3 10.00 10.00 0 22 -3 21.60 8.70 0 22 -3 25.30 8.80 0 22 -3 26.10 11.70 0 22 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5.40 4.50 0 -22 -6 -1.00 9.20 0 22 7 -1.60 4.50 0 22 -7 -7.70 7.00 0 22 -7 3.40 4.50 0 22 -7 0.00 3.30 0 22 7 1.50 4.30 0 22 -7 -7.80 9.40 0 -22 -7 1.60 3.30 0 -22 7 0.90 3.50 0 -22 7 1.30 5.00 0 -22 -7 1.80 9.10 0 23 0 -0.40 6.40 0 23 0 0.10 3.80 0 23 0 -5.00 5.40 0 23 0 -0.70 8.60 0 23 0 -0.80 4.00 0 23 0 -2.20 5.40 0 -23 0 6.30 8.90 0 -23 0 -8.20 10.20 0 -23 0 -3.00 6.20 0 23 1 4.40 7.80 0 23 1 -4.00 3.40 0 23 -1 -2.60 5.20 0 23 1 6.20 4.40 0 23 -1 -0.30 3.70 0 23 -1 -2.00 4.60 0 23 1 7.80 6.80 0 23 -1 -5.10 5.20 0 23 -1 -8.50 9.80 0 23 -1 1.10 5.30 0 23 1 -1.10 5.90 0 23 -1 3.40 6.90 0 -23 1 -4.80 6.10 0 -23 1 -4.70 7.80 0 -23 1 -16.10 8.80 0 -23 -1 16.70 13.50 0 -23 -1 3.10 6.20 0 23 -2 137.59 14.10 0 23 -2 114.19 13.70 0 23 -2 143.69 19.00 0 23 -2 131.39 13.50 0 23 2 102.39 19.70 0 23 -2 114.69 16.90 0 23 2 114.49 12.30 0 23 2 108.39 18.90 0 23 2 135.19 13.10 0 23 -2 147.99 19.20 0 -23 2 77.49 16.70 0 -23 2 123.69 16.60 0 -23 -2 124.09 16.60 0 -23 2 101.19 18.00 0 23 3 54.59 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11.50 0 27 -2 43.70 9.90 0 27 -2 64.39 11.80 0 27 -2 41.00 14.30 0 27 2 30.00 6.20 0 27 2 70.39 14.50 0 -27 2 46.30 12.00 0 -27 2 39.60 11.20 0 -27 -2 76.79 14.20 0 -27 2 37.40 11.80 0 27 -3 8.00 11.10 0 27 -3 0.60 7.80 0 27 3 7.30 4.60 0 27 -3 -14.20 9.80 0 27 -3 8.30 8.10 0 27 -3 13.70 9.00 0 27 3 17.00 7.40 0 27 3 10.90 6.90 0 27 -3 15.30 7.80 0 27 3 14.30 7.40 0 27 -3 10.70 5.60 0 -27 3 6.50 8.40 0 -27 3 5.30 7.40 0 -27 -3 10.00 6.10 0 -27 3 15.30 11.90 0 27 -4 36.20 19.50 0 27 -4 36.40 8.30 0 27 -4 7.00 12.80 0 27 -4 52.99 11.00 0 27 4 50.49 11.00 0 27 -4 53.89 13.50 0 27 4 39.60 8.20 0 27 -4 60.89 11.70 0 27 4 55.59 10.90 0 27 -4 20.10 9.20 0 27 4 41.50 8.70 0 -27 4 33.30 7.40 0 -27 -4 49.40 10.90 0 -27 4 35.80 11.70 0 27 -5 2.40 4.40 0 27 5 31.60 10.00 0 27 5 9.00 6.50 0 27 5 14.80 4.90 0 27 -5 14.40 5.90 0 27 -5 14.00 6.50 0 -27 -5 4.90 4.30 0 -27 5 3.20 4.40 0 27 -6 2.80 5.30 0 27 -6 0.10 3.10 0 27 6 -4.20 3.60 0 27 -6 -3.60 8.20 0 27 6 6.60 5.50 0 27 -6 -5.80 4.80 0 -27 6 0.60 2.50 0 -27 6 2.70 4.20 0 -27 -6 0.20 4.10 0 28 0 1.10 4.30 0 28 0 3.90 7.40 0 28 0 -3.50 7.20 0 28 0 7.20 5.30 0 28 0 3.50 9.10 0 28 0 6.50 5.70 0 -28 0 -9.80 11.70 0 -28 0 14.20 9.90 0 -28 0 12.50 7.90 0 28 1 188.48 17.00 0 28 -1 190.78 18.00 0 28 -1 207.18 19.80 0 28 -1 185.58 23.70 0 28 1 208.28 20.00 0 28 -1 207.18 23.40 0 28 1 198.48 19.10 0 28 -1 209.58 21.20 0 28 -1 171.08 16.50 0 28 -1 203.08 18.10 0 -28 -1 155.98 18.10 0 -28 1 178.88 19.20 0 -28 -1 163.08 18.50 0 -28 1 162.58 20.20 0 -28 1 181.68 18.90 0 28 2 3.70 6.10 0 28 -2 7.80 10.20 0 28 -2 -4.70 10.90 0 28 -2 -2.80 7.70 0 28 2 22.00 8.40 0 28 -2 3.50 5.40 0 28 -2 8.30 7.00 0 28 2 8.00 4.40 0 28 -2 13.50 7.10 0 28 -2 2.80 6.60 0 28 2 6.10 5.50 0 -28 2 4.10 7.80 0 -28 2 2.20 10.00 0 -28 -2 12.50 7.70 0 -28 2 8.70 7.30 0 28 -3 12.10 7.60 0 28 3 5.40 7.40 0 28 3 12.10 5.50 0 28 3 20.10 6.70 0 28 -3 -16.10 13.40 0 28 -3 12.10 5.80 0 28 -3 -3.70 10.80 0 28 -3 7.90 6.90 0 28 -3 11.50 6.80 0 28 -3 10.00 7.30 0 28 3 6.40 5.70 0 -28 3 9.20 8.60 0 -28 3 10.50 6.70 0 -28 -3 11.60 7.50 0 -28 3 9.40 10.50 0 28 4 -0.90 6.00 0 28 -4 1.40 4.60 0 28 4 -7.00 5.00 0 28 -4 -1.70 6.10 0 28 -4 3.00 5.00 0 28 -4 6.50 9.50 0 28 -4 6.90 10.90 0 28 4 1.60 4.50 0 -28 4 2.20 4.20 0 -28 -4 -3.80 4.40 0 28 5 3.60 4.10 0 28 -5 3.80 5.20 0 28 5 28.70 9.50 0 28 -5 17.00 6.40 0 28 5 9.40 5.30 0 28 -5 8.40 5.50 0 28 5 1.00 7.80 0 28 5 10.80 4.40 0 -28 5 6.20 3.50 0 -28 -5 18.00 8.10 0 28 -6 -5.70 4.10 0 28 -6 0.20 3.50 0 28 6 -1.20 3.10 0 28 -6 -1.00 3.50 0 -28 -6 -1.10 2.30 0 -28 6 5.60 3.90 0 -28 6 -2.50 4.00 0 29 0 -23.70 9.10 0 29 0 -7.00 7.10 0 29 0 1.10 5.80 0 29 0 0.20 3.60 0 29 0 4.00 4.80 0 29 0 4.30 5.10 0 -29 0 -0.80 5.50 0 -29 0 -3.30 8.40 0 -29 0 -3.30 12.40 0 29 1 1.40 4.30 0 29 -1 0.10 4.20 0 29 -1 1.80 5.80 0 29 1 -2.00 7.90 0 29 -1 -3.30 9.90 0 29 -1 1.30 5.00 0 29 -1 0.40 7.70 0 29 1 7.80 6.30 0 29 1 -6.20 4.60 0 29 1 1.70 4.60 0 29 -1 4.30 5.90 0 -29 1 -10.50 8.90 0 -29 -1 11.90 7.20 0 -29 1 4.30 10.90 0 -29 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5 34.30 10.70 -4 4 -5 40.00 15.70 -4 4 -5 70.09 12.70 -4 4 -5 68.09 13.50 -4 4 -5 46.50 13.90 4 -4 5 60.99 10.00 -4 -4 -5 29.30 10.30 4 -4 5 39.50 8.40 4 -4 5 54.39 12.00 4 -4 5 38.40 12.40 -4 -4 -5 48.10 9.80 -4 -4 -5 50.99 16.50 -4 -4 -5 35.20 10.30 -4 -4 -5 49.60 10.40 -4 -4 -5 8.80 13.90 -4 4 -6 1.00 5.80 4 4 6 -6.70 5.60 -4 4 -6 -2.50 4.90 -4 4 -6 -7.10 6.10 -4 4 -6 0.60 5.00 4 -4 6 2.50 4.30 -4 -4 -6 29.80 10.10 -4 -4 -6 4.80 5.90 4 -4 6 -1.20 4.20 -4 -4 -6 1.00 4.80 -4 -4 -6 -1.60 4.80 -4 4 -7 0.10 2.60 -4 4 -7 1.80 3.90 -4 4 -7 4.60 5.40 -4 -4 -7 -1.00 3.70 -4 -4 -7 5.10 4.50 -4 5 10 0.30 2.70 -4 -5 10 3.70 7.10 -4 -5 10 7.20 4.90 -4 5 9 0.80 3.90 -4 5 9 -1.60 4.60 -4 5 9 -4.20 9.50 -4 5 9 -2.80 5.80 4 5 -9 0.40 6.50 -4 -5 9 -8.40 8.40 -4 -5 9 -8.60 5.30 -4 -5 9 3.10 6.30 4 -5 -9 25.30 18.10 4 5 -8 11.10 34.70 -4 5 8 1.20 4.90 -4 5 8 -0.30 4.40 4 5 -8 -5.50 7.70 4 5 -8 -16.50 15.30 -4 5 8 -2.80 13.50 -4 -5 8 0.00 7.60 -4 -5 8 1.20 7.70 -4 -5 8 0.40 5.90 4 -5 -8 13.20 14.00 -4 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8.50 7.00 5 12 0 -9.90 8.30 5 12 0 10.80 13.10 -5 -12 0 -4.50 4.70 5 -12 0 10.60 7.00 -5 -12 0 4.40 9.70 -5 -12 0 0.10 6.40 5 -12 0 1.40 6.30 -5 -12 0 -2.10 6.10 5 12 1 -6.40 11.00 -5 12 -1 3.30 4.50 -5 12 -1 -4.70 6.60 5 12 1 0.20 7.00 -5 -12 -1 4.40 13.60 -5 -12 -1 0.50 5.20 5 -12 1 -0.10 5.80 -5 -12 -1 -8.80 5.80 -5 -12 -1 9.60 8.90 -5 -12 -1 -13.80 7.90 5 -12 1 -1.70 6.50 -5 12 -2 5.80 6.20 -5 12 -2 -10.30 6.20 -5 12 -2 -15.90 9.20 5 12 2 4.10 8.10 5 12 2 -8.80 18.70 5 12 2 2.20 6.80 5 -12 2 -8.40 5.70 -5 -12 -2 -2.20 5.10 -5 -12 -2 7.30 10.90 5 -12 2 1.20 4.90 -5 -12 -2 3.50 9.70 -5 -12 -2 3.40 7.60 -5 -12 -2 -3.40 8.00 5 12 3 12.00 5.70 -5 12 -3 -6.60 12.70 -5 12 -3 0.70 7.10 -5 12 -3 8.70 5.90 -5 12 -3 -1.80 14.10 -5 12 -3 15.70 9.50 5 12 3 12.60 8.70 5 -12 3 6.00 5.30 5 -12 3 12.10 6.20 -5 -12 -3 0.30 11.40 -5 -12 -3 -6.90 22.00 -5 -12 -3 -5.90 5.20 -5 -12 -3 10.40 7.30 -5 -12 -3 15.00 11.40 -5 -12 -3 -13.20 7.80 -5 12 -4 26.90 9.50 -5 12 -4 48.90 16.40 5 12 4 18.20 7.80 -5 12 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30.30 8.60 5 13 -5 28.60 14.80 -5 13 5 19.50 6.40 5 13 -5 23.40 10.00 -5 -13 5 24.80 9.00 -5 -13 5 36.00 11.70 -5 -13 5 5.50 10.90 -5 -13 5 16.50 7.30 -5 -13 5 16.40 8.50 5 13 -4 97.19 16.60 5 13 -4 81.89 15.00 5 13 -4 57.99 13.60 5 13 -4 94.59 13.00 -5 13 4 80.79 11.40 -5 -13 4 57.59 11.80 -5 -13 4 63.79 13.10 -5 -13 4 87.59 14.60 -5 -13 4 102.29 20.90 -5 -13 4 77.99 13.70 5 -13 -4 86.99 16.10 5 13 -3 5.60 6.80 5 13 -3 2.10 6.30 5 13 -3 14.40 7.30 5 13 -3 7.80 9.70 5 13 -3 13.00 8.30 -5 -13 3 4.70 6.50 -5 -13 3 0.30 14.80 5 -13 -3 8.10 10.20 -5 -13 3 4.60 6.60 -5 -13 3 11.50 6.60 -5 -13 3 1.00 5.10 5 13 -2 22.30 7.00 5 13 -2 33.70 10.30 5 13 -2 27.20 6.30 5 13 -2 32.80 10.50 5 13 -2 49.60 12.50 -5 13 2 17.80 5.90 -5 -13 2 25.00 11.00 -5 -13 2 35.70 10.60 5 -13 -2 18.70 8.10 -5 -13 2 26.10 8.70 -5 -13 2 45.70 11.90 5 -13 -2 9.30 10.00 5 13 -1 30.80 15.30 5 13 -1 24.10 8.00 -5 13 1 23.40 4.30 5 13 -1 37.60 10.10 5 -13 -1 41.80 10.30 -5 -13 1 29.60 9.70 -5 -13 1 16.30 8.80 -5 -13 1 8.40 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57.99 10.00 5 14 -5 28.40 15.30 5 14 -5 50.19 13.00 -5 -14 5 43.20 13.20 -5 -14 5 37.60 12.00 -5 -14 5 29.20 9.30 -5 -14 5 22.70 12.10 -5 -14 5 48.70 12.90 5 14 -4 65.69 14.60 -5 14 4 71.89 10.30 5 14 -4 47.20 12.90 5 14 -4 45.00 11.30 5 14 -4 42.30 11.10 -5 -14 4 66.09 13.10 -5 -14 4 55.89 12.20 -5 -14 4 48.20 10.60 5 -14 -4 58.49 12.80 -5 -14 4 58.09 13.60 -5 -14 4 44.80 15.20 5 14 -3 2.50 6.60 5 14 -3 0.30 7.50 5 14 -3 3.00 5.60 5 14 -3 -3.90 9.70 5 14 -3 -4.70 4.60 -5 -14 3 -0.50 4.60 -5 -14 3 -0.30 6.70 -5 -14 3 -7.40 5.00 -5 -14 3 -8.80 6.70 5 -14 -3 -3.40 8.10 -5 -14 3 4.90 15.50 5 14 -2 96.29 16.60 5 14 -2 93.29 14.60 5 14 -2 69.89 13.30 5 14 -2 79.29 13.00 5 14 -2 92.49 12.20 -5 -14 2 85.29 13.80 5 -14 -2 76.49 13.80 -5 -14 2 75.49 14.80 -5 -14 2 68.39 11.80 -5 -14 2 71.89 22.90 -5 -14 2 76.09 15.60 5 -14 -2 81.29 13.60 5 14 -1 10.90 10.70 -5 14 1 14.70 4.20 5 14 -1 14.00 7.90 5 14 -1 10.80 7.20 5 14 -1 12.70 5.60 5 -14 -1 7.90 8.40 -5 -14 1 5.40 10.30 5 -14 -1 19.90 9.40 -5 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11 -3 -0.20 5.40 6 11 -3 3.60 5.10 6 11 -3 8.90 7.70 -6 -11 3 12.70 7.60 6 -11 -3 19.90 11.30 -6 -11 3 -2.50 5.20 -6 -11 3 4.10 7.50 -6 -11 3 -5.60 4.50 6 -11 -3 2.20 9.10 6 11 -2 218.08 19.50 6 11 -2 223.68 20.10 -6 11 2 221.78 8.60 6 11 -2 240.58 19.40 6 -11 -2 234.68 20.40 -6 -11 2 242.88 22.60 -6 -11 2 251.97 22.90 -6 -11 2 254.87 22.00 6 -11 -2 222.28 19.30 -6 -11 2 225.88 30.00 6 11 -1 27.50 10.50 6 11 -1 28.40 8.60 6 11 -1 13.00 6.90 6 -11 -1 22.40 7.90 -6 -11 1 11.10 8.50 -6 -11 1 13.20 7.90 -6 -11 1 16.20 7.20 6 -11 -1 18.80 9.20 -6 -11 1 15.30 12.90 -6 11 0 5.90 4.80 6 11 0 13.50 7.90 6 -11 0 15.00 7.20 -6 -11 0 6.90 7.00 -6 -11 0 17.50 11.60 6 -11 0 2.60 6.10 -6 -11 0 6.90 9.00 -6 -11 0 6.40 7.90 -6 11 -1 -4.20 5.50 -6 11 -1 -7.00 6.80 6 11 1 4.10 6.80 -6 -11 -1 7.00 9.50 -6 -11 -1 -3.10 9.10 -6 -11 -1 -2.00 9.20 6 -11 1 -3.00 5.40 -6 -11 -1 1.40 5.50 6 -11 1 -0.60 5.70 -6 11 -2 -3.00 6.30 6 11 2 2.80 6.50 -6 11 -2 15.00 9.20 -6 11 -2 1.20 7.50 -6 -11 -2 -5.30 12.50 -6 -11 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14.40 6 12 -6 115.89 20.70 6 12 -6 104.89 15.90 6 12 -6 89.59 16.70 -6 -12 6 49.20 16.50 -6 -12 6 108.69 16.40 -6 -12 6 108.79 19.00 -6 -12 6 61.99 13.40 6 -12 -6 73.79 14.50 6 12 -5 54.09 12.70 -6 12 5 78.39 12.30 6 12 -5 76.49 14.90 -6 -12 5 53.99 13.20 6 -12 -5 76.59 13.90 -6 -12 5 54.79 13.70 -6 -12 5 90.29 15.90 -6 -12 5 56.49 16.30 6 12 -4 13.10 7.80 6 12 -4 -14.30 10.00 6 12 -4 4.40 6.00 6 12 -4 10.20 7.40 -6 -12 4 15.70 8.60 6 -12 -4 13.30 10.10 -6 -12 4 -1.30 6.70 -6 -12 4 4.00 6.50 -6 -12 4 17.60 9.70 6 12 -3 16.20 7.50 6 12 -3 17.10 8.10 6 12 -3 23.10 6.90 6 12 -3 9.90 20.40 6 -12 -3 19.60 9.70 -6 -12 3 16.70 7.70 -6 -12 3 15.50 7.70 6 -12 -3 6.20 10.70 -6 -12 3 9.30 7.20 -6 -12 3 25.00 9.60 6 12 -2 24.50 9.40 6 12 -2 14.40 7.80 6 12 -2 25.50 7.50 -6 -12 2 17.30 7.00 6 -12 -2 18.80 10.10 -6 -12 2 24.90 7.50 -6 -12 2 11.40 8.40 -6 -12 2 11.20 6.90 6 -12 -2 21.70 9.60 6 12 -1 21.10 8.10 6 12 -1 11.80 11.40 6 12 -1 9.50 9.00 -6 -12 1 16.60 9.20 -6 -12 1 16.00 8.00 -6 -12 1 3.40 9.40 6 -12 -1 -3.00 7.20 -6 -12 1 36.20 13.10 6 -12 -1 2.80 6.60 6 12 0 280.57 22.30 -6 12 0 267.97 14.80 -6 -12 0 290.37 24.30 -6 -12 0 312.07 30.30 -6 -12 0 285.87 26.80 6 -12 0 256.07 20.00 -6 -12 0 242.08 24.30 6 -12 0 272.87 21.70 -6 12 -1 -1.90 8.10 6 12 1 14.90 7.50 -6 12 -1 -1.70 5.20 6 -12 1 -2.80 5.20 -6 -12 -1 -1.90 9.90 -6 -12 -1 -3.20 8.80 -6 -12 -1 1.70 5.70 6 -12 1 10.20 6.90 -6 -12 -1 -5.60 8.70 -6 12 -2 7.40 7.50 6 12 2 31.10 9.20 -6 12 -2 20.20 8.70 -6 12 -2 16.80 9.30 -6 -12 -2 16.60 15.40 -6 -12 -2 11.90 8.40 -6 -12 -2 15.80 12.70 -6 -12 -2 24.80 7.50 6 -12 2 24.00 9.60 6 -12 2 24.40 11.00 6 12 3 -15.50 6.70 -6 12 -3 -21.70 10.80 -6 12 -3 -1.90 4.40 -6 12 -3 -13.30 11.70 -6 -12 -3 1.40 6.10 -6 -12 -3 -2.90 5.90 6 -12 3 4.90 4.60 6 -12 3 -9.50 3.60 -6 12 -4 1.00 3.80 -6 12 -4 -3.40 7.20 -6 -12 -4 -3.90 6.10 -6 -12 -4 2.80 5.00 6 -12 4 4.40 3.40 -6 12 -5 5.70 5.10 -6 12 -5 -0.80 3.20 -6 -12 -5 1.10 4.30 6 -12 5 -2.60 2.60 6 -12 5 8.80 3.40 -6 13 9 7.80 4.30 -6 13 9 4.90 3.90 -6 13 9 10.00 4.70 -6 -13 9 11.00 7.90 -6 13 8 -4.60 4.10 6 13 -8 21.60 13.40 -6 13 8 -2.50 4.20 -6 -13 8 -1.40 10.00 -6 -13 8 -3.50 6.90 -6 -13 8 -8.90 9.00 6 13 -7 41.20 12.50 6 13 -7 24.70 11.60 -6 13 7 31.50 7.60 6 13 -7 36.10 12.60 -6 -13 7 40.50 15.10 -6 -13 7 36.90 9.30 -6 -13 7 -66.69 38.20 -6 -13 7 52.39 12.90 6 -13 -7 19.90 11.50 -6 -13 7 22.60 10.90 6 13 -6 -4.20 10.40 6 13 -6 1.20 5.30 -6 13 6 7.30 5.30 6 13 -6 -4.20 5.60 -6 13 6 -3.10 4.80 6 -13 -6 -18.70 11.50 -6 -13 6 10.60 7.50 -6 -13 6 -4.00 13.80 -6 -13 6 -2.20 5.50 -6 -13 6 -3.50 13.00 -6 -13 6 -6.40 8.90 6 13 -5 3.10 6.50 -6 13 5 6.90 6.40 6 13 -5 0.60 8.40 6 13 -5 -1.80 5.40 -6 -13 5 0.00 5.20 -6 -13 5 7.30 9.70 -6 -13 5 0.40 7.20 6 -13 -5 11.00 11.40 -6 -13 5 -10.50 14.20 -6 -13 5 -4.50 10.00 6 13 -4 6.30 6.70 6 13 -4 -25.10 16.80 6 13 -4 6.00 6.00 6 13 -4 -18.60 9.60 6 13 -4 -3.10 5.90 -6 -13 4 19.60 8.10 -6 -13 4 -1.10 8.50 -6 -13 4 -3.20 5.50 6 -13 -4 4.70 10.10 -6 -13 4 5.20 6.50 6 13 -3 14.00 7.20 6 13 -3 35.30 12.30 6 13 -3 45.30 10.60 6 13 -3 22.10 7.60 -6 -13 3 41.10 13.10 -6 -13 3 32.20 9.80 6 -13 -3 36.80 11.90 6 -13 -3 25.80 13.10 -6 -13 3 29.50 9.40 -6 -13 3 17.80 9.10 6 13 -2 5.20 10.60 6 13 -2 -1.00 5.90 6 13 -2 8.10 7.30 6 -13 -2 -12.40 7.80 6 -13 -2 3.30 7.60 -6 -13 2 -4.70 6.60 -6 -13 2 -13.10 5.90 -6 -13 2 1.40 5.10 -6 -13 2 14.10 7.00 6 13 -1 -3.50 7.80 6 13 -1 1.90 7.70 6 13 -1 0.70 6.20 -6 -13 1 -0.90 7.80 6 -13 -1 -8.70 8.20 -6 -13 1 -11.30 6.60 -6 -13 1 -14.30 10.00 -6 -13 1 -0.50 7.00 6 -13 -1 1.70 6.80 6 13 0 8.30 7.40 -6 13 0 1.40 4.60 -6 -13 0 23.10 12.20 -6 -13 0 2.80 9.30 6 -13 0 16.20 6.80 -6 -13 0 5.40 7.70 6 -13 0 9.00 7.90 6 13 1 60.29 11.80 -6 13 -1 28.70 10.90 -6 -13 -1 43.10 13.00 -6 -13 -1 42.70 10.60 6 -13 1 31.60 8.70 -6 -13 -1 54.79 13.00 6 -13 1 49.10 10.80 -6 -13 -1 44.20 20.00 -6 13 -2 -6.70 6.80 -6 13 -2 0.80 8.20 6 13 2 0.20 6.20 -6 13 -2 6.90 9.50 -6 -13 -2 11.10 11.20 -6 -13 -2 7.10 5.90 -6 -13 -2 3.00 15.50 6 -13 2 4.90 8.20 6 -13 2 6.10 6.40 -6 -13 -2 -15.00 10.90 6 13 3 23.30 9.10 -6 13 -3 11.70 4.60 -6 13 -3 39.20 11.60 -6 13 -3 3.40 11.50 -6 -13 -3 26.00 9.50 6 -13 3 12.90 5.60 -6 -13 -3 20.30 8.20 6 -13 3 14.00 5.30 -6 13 -4 12.00 3.80 -6 13 -4 24.70 9.20 -6 -13 -4 7.90 6.00 6 -13 4 23.40 6.60 6 -13 4 11.30 5.10 -6 14 9 2.20 3.80 -6 14 9 -0.30 3.20 -6 14 9 -4.20 5.00 -6 -14 9 -9.20 6.00 -6 14 8 -3.10 4.40 -6 14 8 -0.90 4.40 6 14 -8 -5.20 9.50 -6 -14 8 -1.40 7.70 -6 -14 8 7.20 7.30 6 14 -7 4.50 9.00 -6 14 7 2.60 6.10 -6 14 7 5.60 5.10 6 14 -7 1.90 6.20 6 14 -7 -1.50 7.00 -6 -14 7 0.20 9.00 6 -14 -7 -4.30 11.30 -6 -14 7 -9.10 15.20 -6 -14 7 0.10 9.50 6 14 -6 31.80 9.60 -6 14 6 29.50 7.60 -6 14 6 9.70 4.90 6 14 -6 18.00 8.10 -6 -14 6 42.50 14.80 -6 -14 6 17.60 10.20 -6 -14 6 36.60 12.40 6 -14 -6 11.50 10.70 -6 -14 6 39.60 16.30 -6 -14 6 22.80 8.30 6 14 -5 5.20 6.10 6 14 -5 8.00 6.70 6 14 -5 10.00 8.60 -6 -14 5 24.90 15.40 -6 -14 5 22.10 12.70 -6 -14 5 -1.20 6.90 6 -14 -5 -2.20 10.00 -6 -14 5 10.50 9.10 -6 -14 5 9.80 6.60 6 14 -4 -9.40 15.90 -6 14 4 26.90 9.10 6 14 -4 30.80 10.40 6 14 -4 27.90 9.00 6 14 -4 35.70 9.70 6 14 -4 20.00 17.80 -6 -14 4 0.10 16.70 -6 -14 4 32.50 11.60 6 -14 -4 43.20 12.80 -6 -14 4 39.80 10.70 -6 -14 4 30.40 10.50 -6 -14 4 18.60 10.40 6 14 -3 -35.50 20.40 6 14 -3 37.90 11.40 6 14 -3 30.10 7.90 6 14 -3 38.80 13.40 6 14 -3 27.20 8.50 6 -14 -3 40.00 13.90 -6 -14 3 48.80 13.40 6 -14 -3 49.00 13.50 -6 -14 3 34.10 11.00 -6 -14 3 21.80 9.00 -6 -14 3 27.00 10.70 6 14 -2 14.80 7.70 6 14 -2 15.00 6.90 6 14 -2 -2.20 12.50 -6 14 2 14.30 4.00 6 14 -2 15.20 7.80 6 -14 -2 18.80 10.50 -6 -14 2 9.90 7.60 -6 -14 2 11.90 6.30 -6 -14 2 11.20 10.30 -6 -14 2 9.20 9.20 6 14 -1 49.30 10.30 6 14 -1 59.59 12.10 6 14 -1 82.49 14.40 -6 -14 1 84.89 16.60 -6 -14 1 75.79 17.80 -6 -14 1 71.99 16.60 6 -14 -1 90.49 15.10 -6 -14 1 76.89 15.50 6 -14 -1 83.69 14.20 6 14 0 2.90 6.50 -6 14 0 4.10 4.40 -6 -14 0 3.40 9.50 -6 -14 0 -1.70 5.00 -6 -14 0 -9.10 6.90 6 -14 0 -5.10 5.10 -6 -14 0 -13.00 8.30 6 -14 0 0.20 5.60 6 14 1 14.20 8.00 -6 14 -1 20.50 6.90 -6 -14 -1 9.80 7.40 -6 -14 -1 18.70 14.10 6 -14 1 20.80 6.90 -6 -14 -1 6.20 10.50 -6 -14 -1 14.90 12.30 6 -14 1 27.80 8.60 -6 14 -2 -1.10 8.10 6 14 2 -4.50 5.50 -6 14 -2 6.40 10.30 -6 14 -2 -14.60 8.60 -6 -14 -2 6.00 8.20 -6 -14 -2 -7.30 4.80 6 -14 2 -2.50 5.10 6 -14 2 -9.60 4.50 -6 -14 -2 9.90 18.40 -6 -14 -2 -9.80 10.60 -6 14 -3 -2.80 9.60 -6 14 -3 15.40 17.50 -6 14 -3 0.50 3.90 -6 -14 -3 3.80 6.80 6 -14 3 0.60 4.70 -6 -14 -3 1.70 6.10 6 -14 3 -1.60 3.90 -6 14 -4 6.20 6.70 6 -14 4 -2.00 2.30 -6 -14 -4 0.60 5.40 -6 -14 -4 3.90 11.60 6 -14 4 0.90 3.30 -6 15 9 58.89 9.90 -6 15 9 31.10 6.60 -6 -15 9 14.00 6.70 6 15 -8 3.30 9.10 -6 15 8 8.10 4.50 -6 15 8 21.90 6.70 -6 -15 8 -7.00 10.20 -6 -15 8 26.80 9.30 6 15 -7 5.00 7.90 6 15 -7 1.70 8.40 -6 15 7 22.10 7.80 -6 15 7 10.00 7.90 -6 -15 7 25.90 15.40 6 -15 -7 -7.50 8.50 -6 -15 7 10.80 8.70 -6 -15 7 22.70 9.00 6 -15 -7 19.70 8.90 -6 -15 7 8.20 9.60 6 15 -6 -3.10 5.90 6 15 -6 1.70 7.00 6 15 -6 1.70 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-2.20 5.10 -10 -10 5 10.10 6.10 10 10 -4 3.00 4.70 -10 -10 4 -0.40 4.60 10 -10 -4 5.80 10.70 -10 -10 4 8.30 8.90 10 10 -3 16.00 6.90 -10 -10 3 5.00 5.10 10 -10 -3 2.50 5.80 -10 -10 3 15.50 8.30 10 10 -2 -4.80 2.60 -10 -10 2 1.60 4.60 10 -10 -2 6.20 5.40 -10 -10 2 -5.90 5.60 10 10 -1 -1.80 2.60 -10 -10 1 -10.50 5.00 -10 -10 1 -5.50 3.60 10 -10 -1 1.90 4.80 -10 -11 7 -5.00 4.40 -10 -11 6 3.90 6.80 -10 -11 5 0.30 4.60 10 11 -4 8.10 6.40 -10 -11 4 -10.80 7.50 -10 -11 4 1.40 4.80 10 11 -3 -1.80 3.90 -10 -11 3 0.90 4.70 10 -11 -3 4.30 6.30 -10 -11 3 -0.10 6.00 10 11 -2 4.50 3.10 -10 -11 2 15.10 6.50 -10 -11 2 -0.60 6.80 10 -11 -2 1.60 5.00 10 11 -1 -0.30 2.80 -10 -11 1 2.90 4.20 -10 -11 1 -0.50 6.10 10 -11 -1 -0.20 3.70 -10 -12 7 3.40 4.80 -10 -12 6 0.00 4.50 -10 -12 5 7.30 5.40 -10 -12 4 -2.70 4.10 -10 -12 4 6.20 7.40 10 12 -3 1.00 3.50 -10 -12 3 2.50 4.60 -10 -12 3 -4.30 6.40 10 -12 -3 -7.60 5.20 10 12 -2 3.60 3.60 -10 -12 2 1.80 5.90 10 -12 -2 -0.40 5.00 -10 -12 2 4.30 4.80 10 12 -1 -1.80 2.70 -10 -12 1 -5.40 4.10 -10 -12 1 -0.80 5.00 10 -12 -1 -4.40 3.10 -10 -13 6 0.80 5.60 -10 -13 5 -0.40 7.70 -10 -13 4 2.70 5.00 -10 -13 4 12.10 7.30 10 13 -3 8.40 4.30 -10 -13 3 2.80 5.90 10 -13 -3 -0.50 6.80 -10 -13 3 -3.40 5.90 10 13 -2 -0.20 2.70 -10 -13 2 1.30 4.90 -10 -13 2 27.60 8.20 10 -13 -2 -0.70 5.00 10 13 -1 -0.90 3.00 -10 -13 1 5.00 5.20 -10 -13 1 10.20 6.00 -10 -14 6 -8.00 4.80 -10 -14 5 15.80 6.60 -10 -14 4 10.00 9.00 -10 -14 4 19.20 8.00 -10 -14 3 4.90 5.20 10 -14 -3 -16.00 7.80 -10 -14 3 -3.60 5.60 10 14 -2 -1.80 1.80 10 -14 -2 4.80 5.80 -10 -14 2 -2.00 5.10 -10 -14 2 -1.10 5.20 -10 -15 6 0.20 5.50 -10 -15 5 3.20 5.70 -10 -15 4 -3.00 5.00 -10 -15 4 7.40 11.50 -10 -15 3 -1.50 5.60 -10 -15 3 -6.60 5.20 -10 -15 2 -8.30 4.50 -10 -15 2 -1.20 5.00 10 -15 -2 -10.10 5.10 -10 -16 5 -2.00 5.30 -10 -16 4 2.90 7.00 -10 -16 4 26.70 6.90 -10 -16 3 0.80 5.70 -10 -16 3 19.70 6.10 10 -16 -2 -16.50 6.50 -10 -17 5 -17.60 5.90 -10 -17 4 3.10 6.10 -10 -17 3 -4.50 5.70 -10 -17 3 -0.80 5.40 -11 0 6 -2.50 3.40 -11 0 5 -9.70 7.90 -11 0 4 1.60 5.20 11 0 -4 6.60 5.80 11 0 -3 -1.10 3.20 -11 1 6 0.50 3.80 -11 1 5 0.30 4.30 -11 -1 5 -5.40 4.30 11 1 -4 2.70 5.20 11 -1 -4 1.90 6.50 11 1 -3 0.90 2.80 11 -1 -3 4.60 3.80 -11 -2 6 2.20 4.00 -11 -2 5 1.30 4.20 11 2 -4 -1.90 4.00 -11 -2 4 -1.10 5.60 11 -2 -4 -1.20 4.40 11 2 -3 -5.60 3.10 11 -2 -3 -3.50 3.30 -11 -2 3 2.00 5.50 -11 -3 6 2.80 3.80 -11 -3 5 0.80 3.90 11 3 -4 -4.70 4.00 11 -3 -4 -7.10 4.80 -11 -3 4 2.50 4.10 11 3 -3 1.60 3.10 11 -3 -3 5.40 5.30 -11 -3 3 -0.50 4.20 -11 -4 6 -2.40 3.60 -11 -4 5 4.70 3.70 11 4 -4 -1.00 3.60 11 -4 -4 -8.80 5.20 -11 -4 4 -0.70 3.70 11 4 -3 -4.20 2.80 11 -4 -3 3.20 5.70 -11 -4 3 -9.30 6.10 -11 -5 6 -1.50 3.70 -11 -5 5 2.30 3.60 11 5 -4 4.40 3.80 -11 -5 4 2.70 3.80 11 -5 -4 5.30 7.40 11 5 -3 -2.70 3.00 -11 -5 3 2.90 9.00 11 -5 -3 -3.10 4.40 -11 -6 5 5.30 3.70 11 6 -4 -4.60 3.30 -11 -6 4 1.30 3.60 11 6 -3 0.70 3.00 -11 -6 3 -2.90 4.10 11 -6 -3 11.40 5.40 -11 -7 5 2.10 3.60 -11 -7 4 2.90 3.90 -11 -8 5 0.50 3.60 -11 -8 4 -1.20 3.60 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 98174 _shelx_res_file ; TITL SM14_a.res in P2(1)/c II.res created by SHELXL-2018/3 at 13:29:43 on 18-Feb-2023 CELL 1.54178 9.3517 31.7075 8.6063 90.000 115.179 90.000 ZERR 4.00 0.0003 0.0011 0.0003 0.000 0.002 0.000 LATT 1 SYMM - X, 1/2 + Y, 1/2 - Z SFAC C H N O S F UNIT 104 80 4 8 8 4 MERG 2 FMAP 2 PLAN 10 SIZE 0.016 0.072 0.112 ACTA EQIV $1 x, y, z-1 HTAB C2 O1_$1 EQIV $2 -1+X, Y, -2+Z HTAB C4 F1_$2 EQIV $3 x, y, z+1 HTAB C18 S1_$3 BOND $H CONF L.S. 10 TEMP 24.00 WGHT 0.132500 EXTI 0.003990 FVAR 0.43335 C1 1 0.254887 0.328084 -0.028452 11.00000 0.05998 0.07850 = 0.06254 -0.00453 0.02629 -0.00347 C2 1 0.236037 0.339337 -0.191803 11.00000 0.07335 0.09736 = 0.06611 -0.00043 0.03304 -0.00463 AFIX 43 H2 2 0.311900 0.355578 -0.207042 11.00000 -1.20000 AFIX 0 C3 1 0.102858 0.325996 -0.330910 11.00000 0.08039 0.10710 = 0.05928 -0.00293 0.02915 0.00498 AFIX 43 H3 2 0.089065 0.333320 -0.441041 11.00000 -1.20000 AFIX 0 C4 1 -0.010999 0.301842 -0.309635 11.00000 0.07397 0.08904 = 0.06169 -0.01318 0.02477 0.00084 AFIX 43 H4 2 -0.100010 0.293249 -0.405677 11.00000 -1.20000 AFIX 0 C5 1 0.005427 0.290444 -0.149754 11.00000 0.06302 0.07916 = 0.06588 -0.01316 0.01907 -0.00787 AFIX 43 H5 2 -0.071951 0.274308 -0.137015 11.00000 -1.20000 AFIX 0 C6 1 0.140820 0.303372 -0.004171 11.00000 0.05981 0.07135 = 0.05631 -0.00750 0.02432 -0.00130 C7 1 0.183594 0.295355 0.173174 11.00000 0.06540 0.07218 = 0.06497 -0.00504 0.02827 -0.01529 AFIX 43 H7 2 0.122120 0.279321 0.212083 11.00000 -1.20000 AFIX 0 C8 1 0.322691 0.313376 0.279783 11.00000 0.06282 0.06425 = 0.05740 -0.00322 0.02723 -0.00532 C9 1 0.396938 0.310337 0.464777 11.00000 0.06768 0.07130 = 0.06138 -0.00371 0.02343 -0.00675 AFIX 43 H9 2 0.350312 0.292242 0.514847 11.00000 -1.20000 AFIX 0 C10 1 0.526488 0.331066 0.571227 11.00000 0.06441 0.06495 = 0.05900 -0.00005 0.02485 -0.00063 AFIX 43 H10 2 0.571084 0.350331 0.523168 11.00000 -1.20000 AFIX 0 C11 1 0.602994 0.325550 0.758103 11.00000 0.05677 0.06133 = 0.05742 0.00045 0.02401 0.00011 C12 1 0.585241 0.287996 0.833629 11.00000 0.06818 0.06399 = 0.06624 0.00009 0.02918 -0.00291 AFIX 43 H12 2 0.521274 0.266825 0.763600 11.00000 -1.20000 AFIX 0 C13 1 0.659476 0.281373 1.008401 11.00000 0.07641 0.07041 = 0.06750 0.00697 0.03415 0.00013 AFIX 43 H13 2 0.646816 0.256223 1.056735 11.00000 -1.20000 AFIX 0 C14 1 0.752725 0.313216 1.108525 11.00000 0.07909 0.08092 = 0.04920 0.00923 0.02122 0.00665 C15 1 0.774266 0.350850 1.043491 11.00000 0.07005 0.07006 = 0.06007 -0.00072 0.02000 -0.00148 AFIX 43 H15 2 0.836300 0.371959 1.115842 11.00000 -1.20000 AFIX 0 C16 1 0.701610 0.356722 0.867722 11.00000 0.06244 0.05576 = 0.05668 0.00173 0.02472 0.00155 C17 1 0.652635 0.455428 0.982110 11.00000 0.07599 0.06310 = 0.06951 -0.00136 0.03307 0.00329 C18 1 0.581814 0.439301 1.078900 11.00000 0.10743 0.08510 = 0.08118 -0.01044 0.04397 -0.00922 AFIX 43 H18 2 0.505581 0.418355 1.033546 11.00000 -1.20000 AFIX 0 C19 1 0.622586 0.453891 1.244372 11.00000 0.13223 0.10640 = 0.09594 -0.00338 0.06311 0.00278 AFIX 43 H19 2 0.574503 0.442786 1.310278 11.00000 -1.20000 AFIX 0 C20 1 0.734420 0.484819 1.309250 11.00000 0.13389 0.11004 = 0.07917 -0.01870 0.04186 0.01599 AFIX 43 H20 2 0.762946 0.494415 1.420623 11.00000 -1.20000 AFIX 0 C21 1 0.804204 0.501693 1.215076 11.00000 0.11878 0.09562 = 0.09873 -0.03457 0.03393 -0.01860 AFIX 43 H21 2 0.878624 0.523052 1.260868 11.00000 -1.20000 AFIX 0 C22 1 0.764697 0.487097 1.049070 11.00000 0.09859 0.07244 = 0.08840 -0.01406 0.03765 -0.01605 AFIX 43 H22 2 0.812980 0.498474 0.983836 11.00000 -1.20000 AFIX 0 C23 1 0.887748 0.405043 0.814256 11.00000 0.07419 0.07635 = 0.08095 -0.00486 0.03540 -0.00898 AFIX 23 H23A 2 0.925473 0.380835 0.773623 11.00000 -1.20000 H23B 2 0.882648 0.428675 0.740500 11.00000 -1.20000 AFIX 0 C24 1 1.003928 0.414938 0.989083 11.00000 0.06827 0.06830 = 0.09015 -0.00549 0.03145 -0.00829 C25 1 1.095317 0.422023 1.132780 11.00000 0.08144 0.07480 = 0.10063 -0.00813 0.03009 -0.00842 C26 1 1.203077 0.430996 1.311427 11.00000 0.10166 0.12313 = 0.09310 -0.01523 0.01035 -0.01176 AFIX 137 H26A 2 1.143024 0.438114 1.374590 11.00000 -1.50000 H26B 2 1.270375 0.454214 1.315234 11.00000 -1.50000 H26C 2 1.266516 0.406545 1.361637 11.00000 -1.50000 AFIX 0 N1 3 0.725484 0.395833 0.794681 11.00000 0.06410 0.05553 = 0.06127 0.00215 0.02379 -0.00169 O1 4 0.450454 0.417326 0.715629 11.00000 0.06226 0.08426 = 0.08781 -0.00746 0.01168 0.00061 O2 4 0.639973 0.466814 0.679021 11.00000 0.13926 0.06804 = 0.07650 0.01737 0.04515 0.00004 S1 5 0.409231 0.340479 0.166272 11.00000 0.06548 0.09977 = 0.06558 -0.00556 0.02606 -0.01800 S2 5 0.605082 0.435350 0.776976 11.00000 0.08225 0.06163 = 0.06250 0.00296 0.02289 0.00198 F1 6 0.824454 0.307602 1.281697 11.00000 0.11393 0.10750 = 0.05521 0.01659 0.01872 -0.00633 HKLF 4 1.0 1.00 0.00 0.00 0.00 1.00 0.00 0.00 0.00 1.00 REM SM14_a.res in P2(1)/c REM wR2 = 0.2324, GooF = S = 0.998, Restrained GooF = 0.998 for all data REM R1 = 0.0659 for 2098 Fo > 4sig(Fo) and 0.1353 for all 4270 data REM 291 parameters refined using 0 restraints END WGHT 0.1320 0.0000 REM Highest difference peak 0.334, deepest hole -0.375, 1-sigma level 0.073 Q1 1 0.3798 0.3086 0.2731 11.00000 0.05 0.33 Q2 1 0.3027 0.3020 0.1504 11.00000 0.05 0.29 Q3 1 0.4638 0.4474 0.6046 11.00000 0.05 0.27 Q4 1 0.4608 0.3385 0.3465 11.00000 0.05 0.26 Q5 1 0.3961 0.3300 -0.0051 11.00000 0.05 0.25 Q6 1 0.5671 0.4736 0.8396 11.00000 0.05 0.23 Q7 1 0.4327 0.4594 0.7072 11.00000 0.05 0.23 Q8 1 0.4537 0.2986 0.6541 11.00000 0.05 0.22 Q9 1 1.3446 0.4394 1.5056 11.00000 0.05 0.22 Q10 1 0.8800 0.5425 0.9793 11.00000 0.05 0.22 ; _shelx_res_checksum 59705 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C C1 0.2549(6) 0.32808(15) -0.0285(6) 0.0669(12) Uani d 1 . . C C2 0.2360(6) 0.33934(17) -0.1918(6) 0.0778(14) Uani d 1 . . H H2 0.311900 0.355578 -0.207042 0.093 Uiso calc 1 . . C C3 0.1029(7) 0.32600(17) -0.3309(7) 0.0825(15) Uani d 1 . . H H3 0.089065 0.333320 -0.441041 0.099 Uiso calc 1 . . C C4 -0.0110(6) 0.30184(16) -0.3096(6) 0.0763(14) Uani d 1 . . H H4 -0.100010 0.293249 -0.405677 0.092 Uiso calc 1 . . C C5 0.0054(6) 0.29044(15) -0.1498(6) 0.0722(13) Uani d 1 . . H H5 -0.071951 0.274308 -0.137015 0.087 Uiso calc 1 . . C C6 0.1408(5) 0.30337(14) -0.0042(5) 0.0626(11) Uani d 1 . . C C7 0.1836(6) 0.29535(14) 0.1732(6) 0.0673(12) Uani d 1 . . H H7 0.122120 0.279321 0.212083 0.081 Uiso calc 1 . . C C8 0.3227(5) 0.31338(13) 0.2798(5) 0.0609(11) Uani d 1 . . C C9 0.3969(6) 0.31034(15) 0.4648(6) 0.0682(12) Uani d 1 . . H H9 0.350312 0.292242 0.514847 0.082 Uiso calc 1 . . C C10 0.5265(6) 0.33107(14) 0.5712(6) 0.0633(12) Uani d 1 . . H H10 0.571084 0.350331 0.523168 0.076 Uiso calc 1 . . C C11 0.6030(5) 0.32555(13) 0.7581(5) 0.0586(11) Uani d 1 . . C C12 0.5852(6) 0.28800(14) 0.8336(6) 0.0659(12) Uani d 1 . . H H12 0.521274 0.266825 0.763600 0.079 Uiso calc 1 . . C C13 0.6595(6) 0.28137(15) 1.0084(6) 0.0702(13) Uani d 1 . . H H13 0.646816 0.256223 1.056735 0.084 Uiso calc 1 . . C C14 0.7527(6) 0.31322(16) 1.1085(6) 0.0718(13) Uani d 1 . . C C15 0.7743(6) 0.35085(15) 1.0435(6) 0.0694(13) Uani d 1 . . H H15 0.836300 0.371959 1.115842 0.083 Uiso calc 1 . . C C16 0.7016(5) 0.35672(13) 0.8677(5) 0.0585(11) Uani d 1 . . C C17 0.6526(6) 0.45543(14) 0.9821(6) 0.0688(13) Uani d 1 . . C C18 0.5818(8) 0.43930(18) 1.0789(7) 0.0899(17) Uani d 1 . . H H18 0.505581 0.418355 1.033546 0.108 Uiso calc 1 . . C C19 0.6226(9) 0.4539(2) 1.2444(9) 0.106(2) Uani d 1 . . H H19 0.574503 0.442786 1.310278 0.128 Uiso calc 1 . . C C20 0.7344(9) 0.4848(2) 1.3093(9) 0.109(2) Uani d 1 . . H H20 0.762946 0.494415 1.420623 0.131 Uiso calc 1 . . C C21 0.8042(9) 0.5017(2) 1.2151(9) 0.109(2) Uani d 1 . . H H21 0.878624 0.523052 1.260868 0.130 Uiso calc 1 . . C C22 0.7647(7) 0.48710(16) 1.0491(7) 0.0872(16) Uani d 1 . . H H22 0.812980 0.498474 0.983836 0.105 Uiso calc 1 . . C C23 0.8877(6) 0.40504(16) 0.8143(7) 0.0763(14) Uani d 1 . . H H23A 0.925473 0.380835 0.773623 0.092 Uiso calc 1 . . H H23B 0.882648 0.428675 0.740500 0.092 Uiso calc 1 . . C C24 1.0039(6) 0.41494(15) 0.9891(7) 0.0764(14) Uani d 1 . . C C25 1.0953(7) 0.42202(17) 1.1328(8) 0.0886(17) Uani d 1 . . C C26 1.2031(8) 0.4310(2) 1.3114(8) 0.117(2) Uani d 1 . . H H26A 1.143024 0.438114 1.374590 0.175 Uiso calc 1 . . H H26B 1.270375 0.454214 1.315234 0.175 Uiso calc 1 . . H H26C 1.266516 0.406545 1.361637 0.175 Uiso calc 1 . . N N1 0.7255(4) 0.39583(10) 0.7947(5) 0.0613(10) Uani d 1 . . O O1 0.4505(4) 0.41733(11) 0.7156(4) 0.0851(11) Uani d 1 . . O O2 0.6400(5) 0.46681(11) 0.6790(5) 0.0949(12) Uani d 1 . . S S1 0.40923(16) 0.34048(5) 0.16627(16) 0.0776(5) Uani d 1 . . S S2 0.60508(16) 0.43535(4) 0.77698(15) 0.0715(4) Uani d 1 . . F F1 0.8245(4) 0.30760(10) 1.2817(3) 0.0982(10) Uani d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 C1 0.060(3) 0.078(3) 0.063(3) -0.003(2) 0.026(2) -0.005(2) C2 0.073(3) 0.097(4) 0.066(3) -0.005(3) 0.033(3) 0.000(3) C3 0.080(4) 0.107(4) 0.059(3) 0.005(3) 0.029(3) -0.003(3) C4 0.074(3) 0.089(3) 0.062(3) 0.001(3) 0.025(3) -0.013(2) C5 0.063(3) 0.079(3) 0.066(3) -0.008(2) 0.019(2) -0.013(2) C6 0.060(3) 0.071(3) 0.056(2) -0.001(2) 0.024(2) -0.008(2) C7 0.065(3) 0.072(3) 0.065(3) -0.015(2) 0.028(2) -0.005(2) C8 0.063(3) 0.064(2) 0.057(2) -0.005(2) 0.027(2) -0.003(2) C9 0.068(3) 0.071(3) 0.061(3) -0.007(2) 0.023(2) -0.004(2) C10 0.064(3) 0.065(3) 0.059(2) -0.001(2) 0.025(2) 0.000(2) C11 0.057(3) 0.061(2) 0.057(2) 0.000(2) 0.024(2) 0.0004(19) C12 0.068(3) 0.064(3) 0.066(3) -0.003(2) 0.029(2) 0.000(2) C13 0.076(3) 0.070(3) 0.067(3) 0.000(3) 0.034(3) 0.007(2) C14 0.079(3) 0.081(3) 0.049(2) 0.007(3) 0.021(2) 0.009(2) C15 0.070(3) 0.070(3) 0.060(3) -0.001(2) 0.020(2) -0.001(2) C16 0.062(3) 0.056(2) 0.057(2) 0.002(2) 0.025(2) 0.0017(18) C17 0.076(3) 0.063(3) 0.070(3) 0.003(2) 0.033(3) -0.001(2) C18 0.107(5) 0.085(3) 0.081(4) -0.009(3) 0.044(3) -0.010(3) C19 0.132(6) 0.106(4) 0.096(5) 0.003(4) 0.063(4) -0.003(4) C20 0.134(6) 0.110(5) 0.079(4) 0.016(5) 0.042(4) -0.019(4) C21 0.119(5) 0.096(4) 0.099(5) -0.019(4) 0.034(4) -0.035(4) C22 0.099(4) 0.072(3) 0.088(4) -0.016(3) 0.038(3) -0.014(3) C23 0.074(3) 0.076(3) 0.081(3) -0.009(3) 0.035(3) -0.005(2) C24 0.068(3) 0.068(3) 0.090(4) -0.008(3) 0.031(3) -0.005(3) C25 0.081(4) 0.075(3) 0.101(4) -0.008(3) 0.030(3) -0.008(3) C26 0.102(5) 0.123(5) 0.093(4) -0.012(4) 0.010(4) -0.015(4) N1 0.064(2) 0.0555(19) 0.061(2) -0.0017(17) 0.0238(18) 0.0022(16) O1 0.062(2) 0.084(2) 0.088(2) 0.0006(18) 0.0117(18) -0.0075(18) O2 0.139(3) 0.0680(19) 0.077(2) 0.000(2) 0.045(2) 0.0174(17) S1 0.0655(8) 0.0998(9) 0.0656(7) -0.0180(7) 0.0261(6) -0.0056(6) S2 0.0822(9) 0.0616(6) 0.0625(7) 0.0020(6) 0.0229(6) 0.0030(5) F1 0.114(2) 0.107(2) 0.0552(16) -0.0063(19) 0.0187(16) 0.0166(15) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C2 C1 C6 . . 121.0(4) ? C2 C1 S1 . . 128.2(4) ? C6 C1 S1 . . 110.8(3) ? C3 C2 C1 . . 118.7(5) ? C3 C2 H2 . . 120.6 ? C1 C2 H2 . . 120.6 ? C2 C3 C4 . . 121.1(5) ? C2 C3 H3 . . 119.4 ? C4 C3 H3 . . 119.4 ? C5 C4 C3 . . 121.0(5) ? C5 C4 H4 . . 119.5 ? C3 C4 H4 . . 119.5 ? C4 C5 C6 . . 119.4(5) ? C4 C5 H5 . . 120.3 ? C6 C5 H5 . . 120.3 ? C1 C6 C5 . . 118.7(4) ? C1 C6 C7 . . 111.9(4) ? C5 C6 C7 . . 129.5(5) ? C8 C7 C6 . . 113.6(4) ? C8 C7 H7 . . 123.2 ? C6 C7 H7 . . 123.2 ? C7 C8 C9 . . 126.1(4) ? C7 C8 S1 . . 111.7(3) ? C9 C8 S1 . . 122.2(3) ? C10 C9 C8 . . 126.3(5) ? C10 C9 H9 . . 116.9 ? C8 C9 H9 . . 116.9 ? C9 C10 C11 . . 124.7(5) ? C9 C10 H10 . . 117.7 ? C11 C10 H10 . . 117.7 ? C12 C11 C16 . . 117.4(4) ? C12 C11 C10 . . 120.8(4) ? C16 C11 C10 . . 121.8(4) ? C13 C12 C11 . . 122.1(4) ? C13 C12 H12 . . 118.9 ? C11 C12 H12 . . 118.9 ? C14 C13 C12 . . 117.6(4) ? C14 C13 H13 . . 121.2 ? C12 C13 H13 . . 121.2 ? F1 C14 C15 . . 118.2(4) ? F1 C14 C13 . . 118.5(4) ? C15 C14 C13 . . 123.3(4) ? C14 C15 C16 . . 118.4(4) ? C14 C15 H15 . . 120.8 ? C16 C15 H15 . . 120.8 ? C15 C16 C11 . . 121.1(4) ? C15 C16 N1 . . 119.7(4) ? C11 C16 N1 . . 119.2(4) ? C18 C17 C22 . . 119.6(5) ? C18 C17 S2 . . 119.9(4) ? C22 C17 S2 . . 120.4(4) ? C17 C18 C19 . . 120.6(6) ? C17 C18 H18 . . 119.7 ? C19 C18 H18 . . 119.7 ? C20 C19 C18 . . 119.1(7) ? C20 C19 H19 . . 120.4 ? C18 C19 H19 . . 120.4 ? C21 C20 C19 . . 121.4(6) ? C21 C20 H20 . . 119.3 ? C19 C20 H20 . . 119.3 ? C20 C21 C22 . . 119.9(6) ? C20 C21 H21 . . 120.0 ? C22 C21 H21 . . 120.0 ? C17 C22 C21 . . 119.3(6) ? C17 C22 H22 . . 120.3 ? C21 C22 H22 . . 120.3 ? C24 C23 N1 . . 115.7(4) ? C24 C23 H23A . . 108.3 ? N1 C23 H23A . . 108.3 ? C24 C23 H23B . . 108.3 ? N1 C23 H23B . . 108.3 ? H23A C23 H23B . . 107.4 ? C25 C24 C23 . . 177.7(6) ? C24 C25 C26 . . 177.9(7) ? C25 C26 H26A . . 109.5 ? C25 C26 H26B . . 109.5 ? H26A C26 H26B . . 109.5 ? C25 C26 H26C . . 109.5 ? H26A C26 H26C . . 109.5 ? H26B C26 H26C . . 109.5 ? C16 N1 C23 . . 117.3(4) ? C16 N1 S2 . . 117.7(3) ? C23 N1 S2 . . 119.1(3) ? C1 S1 C8 . . 92.1(2) ? O2 S2 O1 . . 120.6(2) ? O2 S2 N1 . . 105.5(2) ? O1 S2 N1 . . 105.9(2) ? O2 S2 C17 . . 108.5(2) ? O1 S2 C17 . . 107.5(2) ? N1 S2 C17 . . 108.3(2) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag C1 C2 . 1.387(7) ? C1 C6 . 1.409(7) ? C1 S1 . 1.729(5) ? C2 C3 . 1.376(7) ? C2 H2 . 0.9300 ? C3 C4 . 1.386(7) ? C3 H3 . 0.9300 ? C4 C5 . 1.367(7) ? C4 H4 . 0.9300 ? C5 C6 . 1.411(6) ? C5 H5 . 0.9300 ? C6 C7 . 1.426(6) ? C7 C8 . 1.358(6) ? C7 H7 . 0.9300 ? C8 C9 . 1.444(6) ? C8 S1 . 1.738(5) ? C9 C10 . 1.340(6) ? C9 H9 . 0.9300 ? C10 C11 . 1.466(6) ? C10 H10 . 0.9300 ? C11 C12 . 1.400(6) ? C11 C16 . 1.406(6) ? C12 C13 . 1.378(6) ? C12 H12 . 0.9300 ? C13 C14 . 1.372(7) ? C13 H13 . 0.9300 ? C14 F1 . 1.361(5) ? C14 C15 . 1.369(7) ? C15 C16 . 1.382(6) ? C15 H15 . 0.9300 ? C16 N1 . 1.450(5) ? C17 C18 . 1.365(7) ? C17 C22 . 1.387(7) ? C17 S2 . 1.747(5) ? C18 C19 . 1.388(8) ? C18 H18 . 0.9300 ? C19 C20 . 1.368(9) ? C19 H19 . 0.9300 ? C20 C21 . 1.349(9) ? C20 H20 . 0.9300 ? C21 C22 . 1.394(8) ? C21 H21 . 0.9300 ? C22 H22 . 0.9300 ? C23 C24 . 1.467(7) ? C23 N1 . 1.483(6) ? C23 H23A . 0.9700 ? C23 H23B . 0.9700 ? C24 C25 . 1.188(7) ? C25 C26 . 1.464(8) ? C26 H26A . 0.9600 ? C26 H26B . 0.9600 ? C26 H26C . 0.9600 ? N1 S2 . 1.648(4) ? O1 S2 . 1.431(4) ? O2 S2 . 1.431(4) ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C2 H2 O1 1_554 0.93 2.59 3.483(7) 162.0 yes C4 H4 F1 1_453 0.93 2.52 3.188(6) 129.5 yes C18 H18 S1 1_556 0.93 3.01 3.744(6) 136.5 yes C23 H23A Cg1 1_656 0.93 2.69 3.566(6) 151 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C6 C1 C2 C3 . . . . 0.2(8) ? S1 C1 C2 C3 . . . . 180.0(4) ? C1 C2 C3 C4 . . . . 0.1(8) ? C2 C3 C4 C5 . . . . -0.1(8) ? C3 C4 C5 C6 . . . . -0.2(8) ? C2 C1 C6 C5 . . . . -0.5(7) ? S1 C1 C6 C5 . . . . 179.7(4) ? C2 C1 C6 C7 . . . . 179.8(5) ? S1 C1 C6 C7 . . . . -0.1(5) ? C4 C5 C6 C1 . . . . 0.5(7) ? C4 C5 C6 C7 . . . . -179.8(5) ? C1 C6 C7 C8 . . . . 0.6(6) ? C5 C6 C7 C8 . . . . -179.0(5) ? C6 C7 C8 C9 . . . . -179.2(4) ? C6 C7 C8 S1 . . . . -0.9(5) ? C7 C8 C9 C10 . . . . -173.6(5) ? S1 C8 C9 C10 . . . . 8.3(7) ? C8 C9 C10 C11 . . . . -176.8(4) ? C9 C10 C11 C12 . . . . 24.6(7) ? C9 C10 C11 C16 . . . . -158.0(5) ? C16 C11 C12 C13 . . . . 0.5(7) ? C10 C11 C12 C13 . . . . 178.0(5) ? C11 C12 C13 C14 . . . . 0.2(7) ? C12 C13 C14 F1 . . . . 178.7(4) ? C12 C13 C14 C15 . . . . 0.4(8) ? F1 C14 C15 C16 . . . . -180.0(4) ? C13 C14 C15 C16 . . . . -1.6(8) ? C14 C15 C16 C11 . . . . 2.4(7) ? C14 C15 C16 N1 . . . . -178.4(4) ? C12 C11 C16 C15 . . . . -1.8(7) ? C10 C11 C16 C15 . . . . -179.3(4) ? C12 C11 C16 N1 . . . . 179.0(4) ? C10 C11 C16 N1 . . . . 1.5(7) ? C22 C17 C18 C19 . . . . -0.9(9) ? S2 C17 C18 C19 . . . . 177.7(5) ? C17 C18 C19 C20 . . . . 0.3(10) ? C18 C19 C20 C21 . . . . 0.8(11) ? C19 C20 C21 C22 . . . . -1.1(11) ? C18 C17 C22 C21 . . . . 0.6(9) ? S2 C17 C22 C21 . . . . -178.0(5) ? C20 C21 C22 C17 . . . . 0.5(10) ? C15 C16 N1 C23 . . . . 64.9(6) ? C11 C16 N1 C23 . . . . -115.9(5) ? C15 C16 N1 S2 . . . . -87.9(5) ? C11 C16 N1 S2 . . . . 91.3(5) ? C24 C23 N1 C16 . . . . -69.7(5) ? C24 C23 N1 S2 . . . . 82.7(5) ? C2 C1 S1 C8 . . . . 179.8(5) ? C6 C1 S1 C8 . . . . -0.4(4) ? C7 C8 S1 C1 . . . . 0.7(4) ? C9 C8 S1 C1 . . . . 179.1(4) ? C16 N1 S2 O2 . . . . -171.5(3) ? C23 N1 S2 O2 . . . . 36.2(4) ? C16 N1 S2 O1 . . . . -42.6(4) ? C23 N1 S2 O1 . . . . 165.2(3) ? C16 N1 S2 C17 . . . . 72.5(4) ? C23 N1 S2 C17 . . . . -79.8(4) ? C18 C17 S2 O2 . . . . 156.6(5) ? C22 C17 S2 O2 . . . . -24.9(5) ? C18 C17 S2 O1 . . . . 24.6(5) ? C22 C17 S2 O1 . . . . -156.9(4) ? C18 C17 S2 N1 . . . . -89.4(5) ? C22 C17 S2 N1 . . . . 89.1(4) ? _cod_database_fobs_code 2022824