#------------------------------------------------------------------------------ #$Date: 2023-07-06 20:18:07 +0200 (Thu, 06 Jul 2023) $ #$Revision: 285051 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/27/2022768.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022768 loop_ _publ_author_name 'Radhakrishnan, Rengaraj' 'Mustaphi, Nour El Hoda' 'Sebbar, Nada Kheira' 'Mague, Joel T.' 'Thiruvalluvar, Aravazhi Amalan' _publ_section_title ; Synthesis, crystal structure and Hirshfeld surface analysis of (E)-benzo[d][1,3]dioxole-5-carbaldehyde oxime. ; _journal_coeditor_code HB8064 _journal_issue 'Pt 6' _journal_name_full 'Acta crystallographica. Section E, Crystallographic communications' _journal_page_first 545 _journal_page_last 548 _journal_paper_doi 10.1107/S2056989023004139 _journal_volume 79 _journal_year 2023 _chemical_formula_iupac 'C8 H7 N O3' _chemical_formula_moiety 'C8 H7 N O3' _chemical_formula_sum 'C8 H7 N O3' _chemical_formula_weight 165.15 _chemical_name_systematic ; (E)-Benzo[d][1,3]dioxole-5-carbaldehyde oxime ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 117.238(3) _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 6.8724(14) _cell_length_b 33.502(7) _cell_length_c 7.3449(15) _cell_measurement_reflns_used 6661 _cell_measurement_temperature 150(2) _cell_measurement_theta_max 28.126 _cell_measurement_theta_min 2.432 _cell_volume 1503.6(5) _computing_cell_refinement ; SAINT (Bruker, 2016) ; _computing_data_collection ; APEX3 (Bruker, 2016) ; _computing_data_reduction ; SAINT (Bruker, 2016) ; _computing_molecular_graphics ; DIAMOND (Brandenburg & Putz, 2012), PLATON (Spek, 2020) ; _computing_publication_material ; SHELXL2018/3 (Sheldrick, 2015b), PLATON (Spek, 2020) and publCIF (Westrip, 2010) ; _computing_structure_refinement ; SHELXL2018/3 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 150(2) _diffrn_detector_area_resol_mean 8.3333 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Bruker SMART APEX CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0479 _diffrn_reflns_av_unetI/netI 0.0473 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 43 _diffrn_reflns_limit_k_min -45 _diffrn_reflns_limit_l_max 9 _diffrn_reflns_limit_l_min -9 _diffrn_reflns_number 28032 _diffrn_reflns_theta_full 28.650 _diffrn_reflns_theta_max 28.677 _diffrn_reflns_theta_min 2.432 _diffrn_source 'fine-focus sealed tube' _exptl_absorpt_coefficient_mu 0.114 _exptl_absorpt_correction_T_max 0.99 _exptl_absorpt_correction_T_min 0.82 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.459 _exptl_crystal_density_method 'not measured' _exptl_crystal_description plate _exptl_crystal_F_000 688 _exptl_crystal_size_max 0.355 _exptl_crystal_size_mid 0.166 _exptl_crystal_size_min 0.097 _refine_diff_density_max 0.310 _refine_diff_density_min -0.193 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.047 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 217 _refine_ls_number_reflns 3858 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.047 _refine_ls_R_factor_all 0.0659 _refine_ls_R_factor_gt 0.0458 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0621P)^2^+0.2227P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1178 _refine_ls_wR_factor_ref 0.1265 _reflns_number_gt 2836 _reflns_number_total 3858 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file hb8064sup1.cif _cod_data_source_block I _cod_depositor_comments 'Adding full bibliography for 2022768.cif.' _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 2022768 _cod_database_fobs_code 2022768 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.961 _shelx_estimated_absorpt_t_max 0.989 _shelx_hkl_file ; 1 0 0 0.00 0.20 1 0 0 0.10 0.20 1 0 0 0.30 0.20 -1 0 0 -0.40 0.20 -1 0 0 0.00 0.20 1 0 0 0.10 0.20 -1 0 0 -0.10 0.20 2 0 0 20.90 2.30 -2 0 0 21.80 2.30 2 0 0 23.20 2.30 -2 0 0 19.90 2.30 2 0 0 21.20 2.30 -2 0 0 18.60 2.30 2 0 0 20.00 2.30 3 0 0 0.40 0.60 3 0 0 0.70 0.50 3 0 0 0.10 0.50 3 0 0 0.60 0.50 -3 0 0 -0.40 0.50 -3 0 0 -0.10 0.50 -3 0 0 0.30 0.60 4 0 0 23.60 3.00 4 0 0 26.10 3.00 -4 0 0 24.70 3.10 -4 0 0 24.10 3.00 4 0 0 33.10 3.10 4 0 0 26.80 3.10 -4 0 0 28.00 3.00 5 0 0 -1.20 1.00 -5 0 0 -0.80 1.10 -5 0 0 0.30 0.90 5 0 0 -0.60 0.90 5 0 0 -0.30 0.90 6 0 0 101.79 11.30 6 0 0 102.99 11.20 7 0 0 1.70 1.60 7 0 0 -0.90 1.70 8 0 0 1.70 2.90 8 0 0 2.70 2.20 -1 -1 0 175.78 18.70 1 -1 0 170.38 18.70 1 -1 0 175.68 18.70 1 -1 0 170.38 18.70 -1 -1 0 176.68 18.70 1 1 0 172.68 18.70 -1 1 0 173.58 18.70 1 1 0 178.28 18.70 -1 1 0 174.88 18.70 -1 1 0 180.98 18.70 1 1 0 161.58 18.70 2 -1 0 282.97 30.60 -2 -1 0 293.27 30.60 2 -1 0 286.97 30.60 -2 -1 0 285.57 30.60 -2 -1 0 297.07 30.60 2 -1 0 291.67 30.60 2 -1 0 271.87 30.60 -2 1 0 291.67 30.60 -2 1 0 289.47 30.60 2 1 0 280.27 30.60 2 1 0 266.37 30.60 -2 1 0 289.07 30.60 2 1 0 276.47 30.60 2 1 0 275.77 30.60 -3 -1 0 89.69 9.70 -3 -1 0 90.19 9.80 3 -1 0 89.09 9.70 3 -1 0 92.99 9.80 3 -1 0 86.99 9.70 3 -1 0 91.39 9.80 -3 -1 0 94.49 9.70 3 1 0 90.49 9.70 -3 1 0 87.19 9.80 3 1 0 91.19 9.80 -3 1 0 91.29 9.70 3 1 0 89.89 9.80 3 1 0 86.19 9.70 -3 1 0 88.99 9.70 -4 -1 0 71.59 7.50 4 -1 0 65.69 7.50 -4 -1 0 69.39 7.50 4 -1 0 75.29 7.60 -4 -1 0 69.39 7.60 4 -1 0 71.99 7.60 4 -1 0 64.19 7.50 4 1 0 63.39 7.60 4 1 0 66.09 7.50 4 1 0 63.09 7.50 4 1 0 70.09 7.60 -4 1 0 77.29 7.50 -4 1 0 67.39 7.60 -4 1 0 71.89 7.50 -5 -1 0 19.60 2.70 5 -1 0 19.00 2.50 -5 -1 0 24.80 2.60 5 -1 0 20.00 2.50 5 -1 0 21.60 2.70 5 1 0 20.60 2.50 5 1 0 22.30 2.70 -5 1 0 19.50 2.70 -5 1 0 22.70 2.60 5 1 0 17.60 2.50 6 -1 0 14.20 2.40 6 -1 0 19.60 2.60 6 1 0 15.50 2.40 6 1 0 20.20 2.70 6 1 0 19.80 2.70 7 -1 0 11.90 2.60 7 -1 0 14.90 2.20 7 1 0 7.50 2.10 7 1 0 14.40 2.40 8 -1 0 9.30 3.10 8 -1 0 11.40 2.70 8 1 0 10.10 2.50 8 1 0 13.10 3.30 1 -2 0 1.30 0.30 1 -2 0 0.80 0.20 -1 -2 0 0.80 0.20 1 -2 0 0.70 0.20 1 -2 0 1.40 0.20 -1 -2 0 1.10 0.20 1 2 0 1.10 0.20 1 2 0 1.20 0.30 -1 2 0 0.60 0.20 -1 2 0 0.20 0.20 -1 2 0 0.70 0.30 1 2 0 0.50 0.20 -2 -2 0 0.10 0.40 2 -2 0 -0.20 0.30 2 -2 0 -0.10 0.30 -2 -2 0 -0.40 0.30 2 -2 0 0.00 0.40 -2 -2 0 0.20 0.30 2 -2 0 0.10 0.40 2 2 0 0.20 0.30 2 2 0 1.50 0.40 -2 2 0 0.00 0.30 2 2 0 -0.10 0.30 -2 2 0 -0.20 0.30 2 2 0 0.30 0.30 -2 2 0 0.50 0.40 3 -2 0 91.89 9.30 3 -2 0 84.59 9.30 3 -2 0 84.19 9.30 3 -2 0 82.69 9.20 -3 -2 0 85.79 9.30 -3 -2 0 87.99 9.30 -3 -2 0 88.89 9.30 -3 2 0 91.39 9.30 3 2 0 83.49 9.30 3 2 0 80.59 9.20 3 2 0 84.99 9.30 -3 2 0 82.79 9.30 -3 2 0 86.79 9.30 3 2 0 81.79 9.30 -4 -2 0 0.30 0.70 4 -2 0 0.40 0.80 4 -2 0 -0.10 0.80 -4 -2 0 -0.20 0.70 4 -2 0 -0.20 0.70 4 -2 0 -0.30 0.60 -4 -2 0 -0.80 0.80 -4 2 0 0.30 0.70 -4 2 0 0.90 0.70 4 2 0 -0.80 0.80 -4 2 0 0.60 0.80 4 2 0 0.90 0.70 4 2 0 0.30 0.90 4 2 0 0.00 0.60 -5 -2 0 40.80 4.20 5 -2 0 36.20 3.90 5 -2 0 31.40 3.80 -5 -2 0 37.30 3.80 5 -2 0 32.30 3.70 -5 2 0 30.50 3.80 -5 2 0 30.30 3.90 5 2 0 34.30 3.80 5 2 0 27.70 3.80 5 2 0 30.60 3.70 6 -2 0 33.50 4.40 6 -2 0 33.50 4.40 6 2 0 38.00 4.40 6 2 0 44.30 4.50 6 2 0 37.90 4.60 7 -2 0 0.50 2.10 7 -2 0 3.80 1.70 7 2 0 2.40 1.60 7 2 0 2.00 2.00 8 -2 0 0.60 2.50 8 2 0 4.40 2.90 8 2 0 -1.20 2.00 0 -3 0 -0.10 0.10 0 -3 0 0.10 0.10 0 3 0 0.10 0.10 1 -3 0 198.08 20.50 1 -3 0 192.58 20.50 -1 -3 0 185.48 20.50 -1 -3 0 191.88 20.50 1 3 0 182.18 20.50 -1 3 0 194.58 20.50 1 3 0 189.08 20.50 -1 3 0 193.98 20.50 2 -3 0 622.84 66.89 2 -3 0 611.44 66.89 2 -3 0 638.74 66.89 -2 -3 0 614.14 66.89 -2 -3 0 663.63 66.89 2 -3 0 625.64 66.89 2 3 0 559.74 66.89 -2 3 0 644.24 66.89 -2 3 0 636.04 66.89 2 3 0 605.84 66.89 2 3 0 620.94 66.89 -2 3 0 630.94 66.89 2 3 0 608.74 66.89 3 -3 0 1.00 0.60 -3 -3 0 0.60 0.40 -3 -3 0 0.60 0.70 3 -3 0 -0.60 0.50 3 -3 0 0.50 0.60 -3 -3 0 0.40 0.50 3 -3 0 0.30 0.40 3 3 0 0.30 0.50 -3 3 0 0.70 0.50 3 3 0 0.90 0.60 -3 3 0 0.20 0.50 3 3 0 0.50 0.50 -3 3 0 0.50 0.60 3 3 0 -0.20 0.60 -4 -3 0 43.60 5.20 -4 -3 0 50.69 5.10 4 -3 0 46.30 5.10 -4 -3 0 45.90 5.10 4 -3 0 49.30 5.20 4 -3 0 49.10 5.10 4 -3 0 51.79 5.10 4 3 0 44.40 5.10 -4 3 0 40.00 5.10 4 3 0 43.30 5.10 -4 3 0 50.79 5.10 4 3 0 44.30 5.20 -4 3 0 41.50 5.10 4 3 0 42.30 5.10 5 -3 0 9.60 1.50 -5 -3 0 10.80 1.60 5 -3 0 11.90 1.80 5 -3 0 9.10 1.50 5 3 0 8.10 1.50 -5 3 0 7.00 1.60 -5 3 0 9.90 1.70 5 3 0 12.90 1.70 5 3 0 11.50 1.50 6 -3 0 304.97 30.80 6 -3 0 283.37 30.80 6 3 0 261.57 30.80 6 3 0 286.27 30.80 -6 3 0 295.77 30.80 6 3 0 277.97 30.70 7 -3 0 1.30 2.70 7 -3 0 -1.00 1.80 7 3 0 -1.40 2.00 7 3 0 0.30 1.50 8 -3 0 -0.60 2.90 8 3 0 -1.40 2.00 0 -4 0 194.88 21.60 0 4 0 199.98 21.60 0 4 0 210.28 21.70 0 4 0 201.08 21.60 -1 -4 0 412.16 44.70 1 -4 0 430.96 44.70 -1 -4 0 412.36 44.70 1 -4 0 435.36 44.70 -1 4 0 426.56 44.70 1 4 0 404.76 44.70 -1 4 0 398.96 44.70 1 4 0 400.36 44.70 1 4 0 415.76 44.70 -2 -4 0 387.36 42.80 -2 -4 0 414.26 42.80 2 -4 0 414.46 42.80 2 -4 0 389.66 42.80 2 -4 0 409.86 42.80 2 -4 0 405.06 42.80 2 4 0 360.56 42.80 -2 4 0 402.26 42.80 -2 4 0 401.26 42.80 -2 4 0 398.16 42.80 2 4 0 401.86 42.80 2 4 0 389.16 42.80 3 -4 0 7.00 1.00 -3 -4 0 4.90 1.00 3 -4 0 5.40 0.90 3 -4 0 6.50 1.00 -3 -4 0 8.80 1.00 3 -4 0 5.70 1.00 -3 -4 0 5.80 0.90 -3 4 0 5.60 1.00 3 4 0 7.50 0.90 -3 4 0 8.80 1.00 3 4 0 5.60 0.90 3 4 0 9.80 1.00 -3 4 0 5.60 1.00 3 4 0 6.80 1.00 4 -4 0 36.20 3.60 4 -4 0 28.80 3.50 4 -4 0 35.80 3.60 4 -4 0 26.20 3.60 -4 -4 0 27.50 3.60 -4 -4 0 27.10 3.50 -4 -4 0 34.20 3.60 -4 4 0 33.10 3.60 4 4 0 31.70 3.50 4 4 0 29.90 3.50 -4 4 0 37.50 3.60 -4 4 0 29.40 3.60 4 4 0 31.20 3.50 5 -4 0 33.40 3.60 5 -4 0 30.30 3.50 -5 -4 0 29.40 3.50 -5 4 0 28.90 3.50 5 4 0 28.00 3.50 -5 4 0 30.00 3.50 5 4 0 29.70 3.50 5 4 0 27.70 3.50 6 -4 0 0.90 1.30 6 -4 0 1.40 1.60 -6 4 0 1.70 1.60 6 4 0 0.00 1.30 6 4 0 1.70 1.20 6 4 0 2.20 1.60 7 -4 0 31.20 4.20 7 4 0 31.80 3.90 7 4 0 29.70 4.10 8 -4 0 3.50 2.60 8 4 0 -0.50 2.00 0 -5 0 0.50 0.20 0 -5 0 0.00 0.20 0 -5 0 0.10 0.10 0 5 0 0.30 0.20 0 5 0 0.10 0.10 0 5 0 0.00 0.10 0 5 0 -0.30 0.20 0 5 0 -0.20 0.10 1 -5 0 554.04 61.99 -1 -5 0 591.44 61.99 -1 -5 0 597.64 61.99 1 -5 0 592.44 61.99 1 5 0 577.94 61.99 -1 5 0 588.04 61.99 1 5 0 541.45 61.99 -1 5 0 581.64 61.99 1 5 0 564.54 61.99 -2 -5 0 340.57 36.30 -2 -5 0 338.37 36.40 2 -5 0 357.46 36.40 2 -5 0 350.26 36.40 2 -5 0 350.86 36.40 -2 -5 0 333.17 36.30 2 -5 0 346.77 36.30 2 5 0 326.47 36.30 2 5 0 334.47 36.30 -2 5 0 346.47 36.40 -2 5 0 337.07 36.30 -2 5 0 335.47 36.40 2 5 0 293.47 36.40 -3 -5 0 212.68 22.30 3 -5 0 206.08 22.30 3 -5 0 219.18 22.30 3 -5 0 216.08 22.30 -3 -5 0 198.58 22.30 3 -5 0 212.08 22.30 -3 -5 0 215.98 22.30 -3 5 0 208.48 22.30 3 5 0 196.18 22.30 3 5 0 186.98 22.30 -3 5 0 212.58 22.30 3 5 0 203.98 22.30 3 5 0 194.78 22.30 -3 5 0 215.48 22.30 4 -5 0 8.80 1.40 4 -5 0 6.90 1.30 -4 -5 0 11.40 1.30 -4 -5 0 9.60 1.30 4 -5 0 10.20 1.30 -4 -5 0 8.90 1.50 4 -5 0 12.20 1.50 4 5 0 9.80 1.40 4 5 0 9.10 1.30 4 5 0 6.00 1.20 -4 5 0 11.60 1.40 -4 5 0 10.20 1.30 -4 5 0 7.70 1.40 -5 -5 0 54.19 6.80 5 -5 0 75.29 6.90 5 -5 0 61.99 6.80 -5 5 0 58.29 6.80 5 5 0 62.79 6.80 5 5 0 64.29 6.80 5 5 0 58.39 6.80 -5 5 0 56.19 6.80 6 -5 0 11.90 1.90 6 -5 0 8.30 2.00 6 5 0 10.30 1.80 -6 5 0 6.40 1.90 6 5 0 10.40 1.60 6 5 0 12.10 2.00 7 -5 0 83.69 9.80 7 5 0 86.39 9.70 7 5 0 90.99 9.80 8 -5 0 -0.10 2.90 8 5 0 -1.70 1.90 0 -6 0 77.69 8.30 0 -6 0 72.99 8.30 0 -6 0 77.29 8.30 0 -6 0 77.49 8.30 0 6 0 82.19 8.40 0 6 0 79.59 8.30 0 6 0 78.49 8.30 0 6 0 75.29 8.30 1 -6 0 10.20 1.20 -1 -6 0 11.40 1.20 -1 -6 0 10.80 1.20 1 -6 0 11.30 1.20 1 6 0 11.70 1.20 1 6 0 10.00 1.20 -1 6 0 10.50 1.30 -1 6 0 10.40 1.20 1 6 0 10.60 1.20 -2 -6 0 174.68 19.20 2 -6 0 181.18 19.20 2 -6 0 171.68 19.30 2 -6 0 186.18 19.20 -2 -6 0 181.88 19.20 2 -6 0 187.58 19.20 -2 6 0 174.98 19.20 2 6 0 174.78 19.20 2 6 0 180.78 19.30 2 6 0 165.58 19.20 -2 6 0 183.68 19.30 -3 -6 0 245.98 25.60 3 -6 0 240.08 25.60 3 -6 0 241.88 25.60 -3 -6 0 247.18 25.60 3 -6 0 249.48 25.60 -3 -6 0 251.17 25.60 3 -6 0 242.78 25.60 3 6 0 235.08 25.60 -3 6 0 236.08 25.60 3 6 0 207.48 25.60 -3 6 0 245.48 25.60 3 6 0 230.78 25.60 -3 6 0 232.18 25.60 3 6 0 217.18 25.60 -4 -6 0 76.69 8.50 4 -6 0 81.19 8.40 -4 -6 0 72.49 8.50 4 -6 0 72.79 8.50 4 -6 0 84.89 8.50 4 -6 0 77.09 8.50 -4 -6 0 79.19 8.50 -4 6 0 72.39 8.50 4 6 0 74.79 8.40 -4 6 0 86.29 8.50 -4 6 0 75.19 8.50 4 6 0 83.59 8.50 4 6 0 74.09 8.50 5 -6 0 5.60 1.30 5 -6 0 8.60 1.80 5 -6 0 5.40 1.40 -5 -6 0 7.00 1.30 -5 6 0 5.50 1.30 5 6 0 7.20 1.20 -5 6 0 4.20 1.30 5 6 0 7.20 1.30 5 6 0 7.60 1.30 6 -6 0 22.20 3.00 -6 -6 0 17.70 2.70 6 6 0 25.70 2.90 6 6 0 19.50 2.70 -6 6 0 21.90 2.80 6 6 0 17.60 2.60 7 -6 0 -1.50 2.10 7 6 0 4.10 1.50 7 6 0 4.00 1.80 8 -6 0 1.30 3.00 8 6 0 -1.30 2.00 0 -7 0 -0.10 0.10 0 -7 0 -0.40 0.30 0 -7 0 -0.10 0.10 0 -7 0 0.70 0.20 0 7 0 0.20 0.10 0 7 0 0.00 0.20 0 7 0 0.00 0.10 0 7 0 0.10 0.30 -1 -7 0 20.40 2.20 1 -7 0 19.00 2.20 -1 -7 0 19.10 2.20 1 -7 0 21.30 2.20 1 7 0 22.40 2.20 1 7 0 19.50 2.20 -1 7 0 18.10 2.30 1 7 0 20.70 2.20 1 7 0 20.00 2.20 -1 7 0 21.10 2.20 2 -7 0 -0.30 0.40 -2 -7 0 -0.40 0.30 2 -7 0 0.30 0.40 2 -7 0 0.30 0.40 2 -7 0 0.00 0.20 -2 -7 0 0.10 0.40 -2 7 0 0.00 0.40 2 7 0 0.10 0.30 -2 7 0 0.60 0.50 -2 7 0 -0.10 0.40 2 7 0 0.10 0.40 2 7 0 0.50 0.40 3 -7 0 96.89 10.00 3 -7 0 98.79 10.00 3 -7 0 96.39 10.00 -3 -7 0 97.49 10.00 3 -7 0 96.09 9.90 -3 -7 0 90.89 10.00 -3 -7 0 91.99 10.00 3 7 0 84.69 9.90 -3 7 0 91.89 10.00 -3 7 0 95.39 10.00 3 7 0 87.69 10.00 3 7 0 82.99 10.00 -3 7 0 87.49 10.00 4 -7 0 40.40 4.90 4 -7 0 48.20 4.90 4 -7 0 47.60 4.80 -4 -7 0 45.40 4.80 -4 -7 0 42.60 4.80 4 -7 0 41.30 4.90 -4 7 0 49.40 4.90 4 7 0 40.30 4.80 4 7 0 44.50 4.90 -4 7 0 39.90 4.90 4 7 0 43.70 4.80 -4 7 0 40.10 4.90 -5 -7 0 1.90 1.00 5 -7 0 1.30 1.20 5 -7 0 3.70 1.30 5 -7 0 1.60 1.10 5 7 0 3.40 0.90 5 7 0 1.80 1.00 -5 7 0 2.70 1.10 5 7 0 1.10 1.10 -5 7 0 1.30 1.10 6 -7 0 69.19 6.90 -6 -7 0 62.69 6.90 6 7 0 55.49 6.70 6 7 0 54.99 6.80 6 7 0 61.39 6.90 -6 7 0 62.79 6.90 7 -7 0 4.50 2.00 7 7 0 3.90 1.90 7 7 0 2.60 1.50 -7 7 0 1.50 2.10 8 -7 0 4.00 3.10 8 7 0 0.90 2.00 0 -8 0 0.50 0.20 0 -8 0 0.50 0.30 0 -8 0 0.60 0.30 0 -8 0 0.60 0.20 0 8 0 0.70 0.10 0 8 0 0.70 0.30 0 8 0 0.50 0.10 0 8 0 0.60 0.20 1 -8 0 238.28 25.50 1 -8 0 224.88 25.50 -1 -8 0 234.78 25.50 -1 -8 0 229.98 25.50 1 8 0 243.68 25.50 -1 8 0 238.28 25.50 1 8 0 247.38 25.50 1 8 0 238.18 25.50 1 8 0 231.48 25.50 -1 8 0 237.18 25.50 2 -8 0 6.10 1.10 -2 -8 0 9.00 1.00 2 -8 0 8.30 1.10 -2 -8 0 8.60 1.10 2 -8 0 10.40 1.10 -2 8 0 9.90 1.10 2 8 0 8.10 1.00 2 8 0 9.80 1.00 -2 8 0 7.30 1.10 2 8 0 7.30 1.10 -3 -8 0 25.70 2.70 3 -8 0 25.30 2.70 -3 -8 0 21.00 2.70 3 -8 0 24.50 2.60 -3 -8 0 24.70 2.80 3 -8 0 23.70 2.70 3 -8 0 28.40 2.80 3 8 0 20.70 2.70 -3 8 0 23.50 2.70 -3 8 0 25.00 2.70 3 8 0 21.50 2.70 3 8 0 24.00 2.70 -3 8 0 22.00 2.70 4 -8 0 126.49 12.90 4 -8 0 126.69 13.00 4 -8 0 125.49 12.90 4 -8 0 126.19 12.90 -4 -8 0 118.09 12.90 -4 -8 0 131.39 12.90 -4 8 0 108.39 12.90 -4 8 0 119.79 12.90 4 8 0 117.39 12.90 4 8 0 106.19 12.90 4 8 0 108.39 12.90 5 -8 0 1.90 1.30 5 -8 0 0.30 1.40 -5 -8 0 1.90 1.00 5 8 0 0.10 1.10 5 8 0 1.40 1.00 5 8 0 0.10 0.80 -5 8 0 0.70 1.00 -5 8 0 1.40 1.20 -6 -8 0 7.50 1.60 6 -8 0 8.30 1.90 6 8 0 10.90 1.80 6 8 0 6.50 1.70 -6 8 0 9.80 1.80 6 8 0 5.90 1.40 7 -8 0 50.09 5.30 7 8 0 40.20 5.20 7 8 0 41.20 5.10 -7 8 0 42.30 5.30 8 -8 0 -3.10 2.70 8 8 0 0.00 1.90 0 -9 0 -0.10 0.30 0 -9 0 0.20 0.30 0 -9 0 0.30 0.20 0 -9 0 0.10 0.20 0 9 0 0.80 0.30 0 9 0 0.30 0.10 0 9 0 0.40 0.30 -1 -9 0 2.80 0.50 1 -9 0 1.20 0.40 -1 -9 0 2.50 0.40 1 -9 0 1.50 0.40 -1 -9 0 2.60 0.40 -1 9 0 2.00 0.40 -1 9 0 3.50 0.40 -1 9 0 1.30 0.50 1 9 0 1.90 0.30 1 9 0 2.50 0.30 1 9 0 2.40 0.40 2 -9 0 7.60 1.00 2 -9 0 8.00 1.00 2 -9 0 6.70 1.00 -2 -9 0 8.00 0.90 -2 -9 0 7.10 1.00 2 9 0 8.10 1.00 2 9 0 7.30 0.90 2 9 0 7.60 0.90 -2 9 0 5.80 1.00 2 9 0 8.60 0.90 -2 9 0 6.20 0.90 3 -9 0 22.00 2.20 -3 -9 0 18.80 2.30 3 -9 0 21.10 2.40 3 -9 0 20.10 2.40 -3 -9 0 22.20 2.30 -3 -9 0 20.40 2.40 3 -9 0 23.00 2.40 3 9 0 16.70 2.20 -3 9 0 18.60 2.30 -3 9 0 18.90 2.40 3 9 0 16.80 2.30 -3 9 0 20.30 2.30 3 9 0 19.90 2.30 -4 -9 0 38.70 4.40 4 -9 0 46.20 4.50 -4 -9 0 44.80 4.40 4 -9 0 44.60 4.50 4 -9 0 39.10 4.50 4 9 0 40.40 4.40 4 9 0 36.70 4.50 -4 9 0 38.00 4.50 4 9 0 36.30 4.40 -4 9 0 36.10 4.50 5 -9 0 18.60 2.50 5 -9 0 20.50 2.50 -5 -9 0 20.30 2.30 5 9 0 16.40 2.20 -5 9 0 21.80 2.40 5 9 0 17.70 2.30 -5 9 0 15.70 2.40 5 9 0 15.90 2.40 -6 -9 0 2.90 1.40 6 -9 0 0.30 1.50 -6 9 0 1.40 1.50 6 9 0 0.30 1.10 6 9 0 2.80 1.50 6 9 0 0.30 1.40 7 -9 0 11.60 2.60 -7 9 0 13.60 2.50 7 9 0 12.90 2.40 7 9 0 12.70 2.10 8 -9 0 -4.20 2.60 8 9 0 -0.40 1.90 0 -10 0 43.60 4.70 0 -10 0 43.90 4.60 0 -10 0 41.90 4.60 0 -10 0 39.70 4.60 0 10 0 46.80 4.70 0 10 0 42.50 4.70 1 -10 0 0.20 0.30 -1 -10 0 -0.30 0.40 1 -10 0 0.10 0.30 -1 -10 0 0.20 0.20 -1 -10 0 0.50 0.30 -1 10 0 0.10 0.20 1 10 0 0.60 0.20 1 10 0 0.20 0.30 -1 10 0 0.30 0.40 1 10 0 0.10 0.20 -1 10 0 -0.10 0.20 -2 -10 0 266.47 28.10 2 -10 0 269.27 28.10 2 -10 0 256.67 28.00 -2 -10 0 261.07 28.00 2 -10 0 269.07 28.00 -2 10 0 247.38 28.00 2 10 0 251.07 28.10 2 10 0 252.47 28.00 2 10 0 271.97 28.00 -2 10 0 258.17 28.10 2 10 0 260.17 28.00 3 -10 0 0.40 0.70 -3 -10 0 0.10 0.50 -3 -10 0 0.00 0.50 3 -10 0 0.30 0.40 3 -10 0 -0.20 0.60 3 -10 0 0.90 0.70 -3 -10 0 0.40 0.80 -3 10 0 0.00 0.70 -3 10 0 0.40 0.60 -3 10 0 -0.50 0.60 3 10 0 -0.70 0.50 3 10 0 0.00 0.40 3 10 0 0.80 0.70 4 -10 0 174.38 17.70 -4 -10 0 170.18 17.70 4 -10 0 171.38 17.70 -4 -10 0 167.68 17.70 4 -10 0 167.58 17.70 -4 10 0 161.78 17.70 4 10 0 157.88 17.70 4 10 0 151.58 17.70 4 10 0 157.48 17.70 -4 10 0 159.68 17.70 -5 -10 0 19.90 2.70 5 -10 0 20.60 2.90 5 -10 0 21.90 2.90 -5 10 0 29.50 2.90 5 10 0 23.00 2.90 -5 10 0 20.90 2.80 5 10 0 25.50 2.70 5 10 0 21.60 2.80 -6 -10 0 -0.10 1.30 6 -10 0 1.80 1.70 6 10 0 0.80 1.30 -6 10 0 0.40 1.40 6 10 0 0.80 1.10 7 -10 0 7.20 2.20 7 10 0 4.70 1.60 -7 10 0 6.50 2.10 7 10 0 7.00 2.10 8 -10 0 2.60 2.80 -8 10 0 -1.30 3.20 8 10 0 0.20 1.90 0 -11 0 0.20 0.20 0 -11 0 0.30 0.20 0 -11 0 0.10 0.30 0 -11 0 0.70 0.40 0 11 0 0.20 0.30 0 11 0 0.00 0.40 1 -11 0 41.30 4.60 1 -11 0 41.70 4.60 -1 -11 0 42.00 4.60 -1 -11 0 42.00 4.60 -1 -11 0 38.40 4.60 -1 11 0 47.70 4.60 -1 11 0 40.80 4.60 1 11 0 45.00 4.60 -1 11 0 40.50 4.50 1 11 0 45.30 4.60 1 11 0 41.60 4.50 -1 11 0 38.40 4.60 2 -11 0 56.49 6.50 -2 -11 0 61.89 6.50 2 -11 0 63.99 6.50 -2 -11 0 57.29 6.50 2 11 0 58.59 6.40 2 11 0 61.79 6.50 2 11 0 65.99 6.40 -2 11 0 56.99 6.50 -2 11 0 51.49 6.50 2 11 0 57.99 6.40 -3 -11 0 208.68 22.30 3 -11 0 232.28 22.40 3 -11 0 204.58 22.40 -3 -11 0 204.88 22.30 3 -11 0 200.88 22.30 -3 -11 0 198.08 22.50 3 11 0 204.48 22.30 -3 11 0 202.98 22.30 -3 11 0 204.78 22.40 3 11 0 196.48 22.30 3 11 0 203.78 22.40 3 11 0 221.58 22.30 4 -11 0 70.89 6.40 4 -11 0 56.99 6.40 -4 -11 0 64.89 6.30 -4 -11 0 58.59 6.40 4 11 0 49.90 6.40 4 11 0 51.29 6.30 -4 11 0 55.39 6.40 4 11 0 60.69 6.30 -4 11 0 56.29 6.40 5 -11 0 1.60 1.30 -5 -11 0 3.60 1.10 5 -11 0 5.80 1.40 5 11 0 3.40 1.20 -5 11 0 6.00 1.30 -5 11 0 4.40 1.20 5 11 0 4.20 1.20 5 11 0 3.40 0.90 6 -11 0 18.50 2.80 -6 -11 0 22.30 2.60 6 11 0 15.80 2.60 -6 11 0 21.70 2.70 6 11 0 17.80 2.40 7 -11 0 1.40 2.00 -7 11 0 0.60 2.00 7 11 0 1.00 1.80 7 11 0 0.00 1.40 0 -12 0 -0.30 0.20 0 -12 0 -0.20 0.30 0 -12 0 0.40 0.20 0 -12 0 0.00 0.40 0 12 0 0.30 0.30 0 12 0 -0.10 0.40 -1 -12 0 9.30 1.00 1 -12 0 7.00 1.00 -1 -12 0 6.90 1.10 1 -12 0 9.30 1.00 -1 -12 0 7.70 0.90 1 12 0 7.70 0.90 1 12 0 9.10 1.00 -1 12 0 7.90 0.90 -1 12 0 7.60 0.90 1 12 0 7.80 0.90 1 12 0 7.80 0.90 -1 12 0 7.90 0.90 -1 12 0 8.40 1.10 2 -12 0 283.87 31.10 -2 -12 0 297.87 31.10 2 -12 0 300.47 31.10 -2 -12 0 275.27 31.10 2 12 0 295.57 31.10 2 12 0 288.97 31.10 2 12 0 291.57 31.10 -2 12 0 284.27 31.10 -2 12 0 285.37 31.10 2 12 0 280.67 31.10 3 -12 0 -0.20 0.80 3 -12 0 0.30 0.70 -3 -12 0 0.30 0.60 -3 -12 0 0.40 0.50 3 -12 0 0.50 0.70 3 12 0 0.50 0.60 3 12 0 -0.10 0.40 -3 12 0 -0.20 0.60 -3 12 0 0.30 0.80 3 12 0 0.50 0.50 3 12 0 0.50 0.70 -4 -12 0 1.70 0.80 4 -12 0 1.50 1.10 4 -12 0 1.30 0.90 -4 -12 0 1.10 0.70 -4 12 0 0.80 0.90 -4 12 0 -0.10 1.00 4 12 0 0.90 0.80 4 12 0 1.90 0.70 4 12 0 1.30 0.80 -5 -12 0 11.60 1.70 5 -12 0 11.10 1.90 5 -12 0 13.30 2.00 5 12 0 11.10 1.70 5 12 0 8.80 1.70 -5 12 0 10.60 1.90 -5 12 0 12.00 1.80 5 12 0 13.20 1.60 -6 -12 0 57.79 7.00 6 -12 0 70.29 7.10 -6 12 0 62.09 7.10 6 12 0 57.09 7.00 6 12 0 62.99 6.90 7 -12 0 2.10 2.10 -7 12 0 -0.90 1.90 7 12 0 -0.20 1.90 7 12 0 1.20 1.40 0 -13 0 0.00 0.30 0 -13 0 -0.10 0.40 0 -13 0 0.30 0.30 0 -13 0 0.10 0.40 0 13 0 -0.10 0.50 0 13 0 -0.20 0.30 -1 -13 0 -0.10 0.40 -1 -13 0 0.00 0.30 1 -13 0 -0.20 0.30 1 -13 0 0.10 0.40 1 -13 0 -0.10 0.30 1 -13 0 0.20 0.50 -1 -13 0 -0.10 0.30 -1 13 0 0.20 0.20 1 13 0 0.10 0.30 -1 13 0 0.20 0.30 -1 13 0 0.20 0.30 1 13 0 0.00 0.40 -1 13 0 0.60 0.50 2 -13 0 22.90 2.80 2 -13 0 25.90 2.80 -2 -13 0 23.60 2.80 -2 -13 0 25.10 2.80 2 13 0 28.30 2.80 -2 13 0 24.10 2.80 2 13 0 24.10 2.70 -2 13 0 22.60 2.80 2 13 0 26.00 2.70 2 13 0 27.80 2.70 -2 13 0 21.10 2.90 -3 -13 0 3.70 0.70 -3 -13 0 3.20 0.80 3 -13 0 4.70 0.90 3 -13 0 2.80 0.90 3 -13 0 3.20 0.90 -3 13 0 2.90 0.70 3 13 0 4.10 0.70 3 13 0 4.90 0.60 3 13 0 3.10 0.70 -3 13 0 3.20 0.90 3 13 0 3.90 0.80 4 -13 0 2.60 1.00 4 -13 0 2.50 1.10 -4 -13 0 1.30 0.80 -4 -13 0 1.50 0.90 -4 13 0 1.00 0.80 -4 13 0 1.70 1.00 4 13 0 1.80 0.90 4 13 0 2.60 0.70 4 13 0 1.70 0.80 5 -13 0 0.30 1.30 -5 -13 0 0.60 1.00 5 -13 0 0.10 1.30 -5 13 0 0.00 1.30 -5 13 0 0.40 1.10 5 13 0 0.50 1.10 5 13 0 0.10 0.80 -6 -13 0 33.10 3.80 6 -13 0 29.30 4.00 -6 13 0 32.10 3.90 6 13 0 32.10 3.70 6 13 0 29.30 3.90 7 -13 0 8.90 2.70 7 13 0 10.70 2.30 7 13 0 7.60 1.70 -7 13 0 9.20 2.20 0 -14 0 19.80 2.10 0 -14 0 15.30 2.20 0 -14 0 20.60 2.10 0 -14 0 18.40 2.20 0 14 0 18.50 2.20 0 14 0 21.80 2.20 1 -14 0 10.40 1.30 1 -14 0 10.60 1.20 -1 -14 0 8.10 1.30 1 -14 0 10.20 1.40 1 -14 0 9.50 1.20 -1 -14 0 12.00 1.20 -1 -14 0 8.90 1.20 1 14 0 11.30 1.20 -1 14 0 9.10 1.40 -1 14 0 11.40 1.20 1 14 0 13.10 1.30 -1 14 0 9.90 1.20 -1 14 0 9.90 1.20 2 -14 0 100.49 10.90 2 -14 0 102.09 10.80 -2 -14 0 101.09 10.80 -2 -14 0 104.09 10.90 -2 -14 0 94.99 10.80 2 14 0 102.19 10.80 -2 14 0 97.49 10.80 2 14 0 102.19 10.90 2 14 0 100.99 10.80 2 14 0 104.59 10.80 -2 14 0 94.49 10.80 -2 14 0 91.89 10.90 3 -14 0 1.60 0.80 3 -14 0 1.60 0.80 -3 -14 0 0.40 0.70 -3 -14 0 1.40 0.50 -3 14 0 0.80 0.60 -3 14 0 0.80 0.90 3 14 0 1.80 0.60 3 14 0 1.50 0.80 3 14 0 1.30 0.60 3 14 0 0.70 0.40 -4 -14 0 12.80 1.50 4 -14 0 11.70 1.70 -4 -14 0 10.30 1.60 4 -14 0 10.70 1.60 4 14 0 10.40 1.50 4 14 0 10.30 1.40 -4 14 0 11.90 1.50 -4 14 0 6.80 1.70 4 14 0 10.00 1.60 5 -14 0 -0.30 1.30 -5 -14 0 0.30 1.00 5 -14 0 0.10 1.30 -5 14 0 0.60 1.20 5 14 0 0.40 0.80 -5 14 0 0.80 1.10 5 14 0 -0.70 1.10 -6 -14 0 1.70 1.40 6 -14 0 2.20 1.90 -6 14 0 0.10 1.40 6 14 0 2.90 1.50 6 14 0 1.40 1.10 7 -14 0 -0.20 2.20 7 14 0 0.10 1.30 -7 14 0 0.60 1.90 7 14 0 -1.60 1.80 0 -15 0 0.40 0.30 0 -15 0 0.70 0.60 0 -15 0 0.30 0.40 0 -15 0 0.80 0.30 0 15 0 0.60 0.40 0 15 0 0.30 0.60 -1 -15 0 0.60 0.50 1 -15 0 0.30 0.40 -1 -15 0 0.10 0.40 -1 -15 0 0.50 0.40 1 -15 0 0.00 0.40 -1 -15 0 0.30 0.30 1 -15 0 0.60 0.60 1 -15 0 0.10 0.50 -1 15 0 0.90 0.30 1 15 0 0.60 0.50 -1 15 0 0.40 0.30 1 15 0 0.10 0.40 -1 15 0 0.60 0.60 -1 15 0 0.70 0.30 -2 -15 0 37.40 4.20 -2 -15 0 36.90 4.30 2 -15 0 36.00 4.30 -2 -15 0 37.40 4.30 2 -15 0 37.60 4.20 2 15 0 40.80 4.20 2 15 0 37.80 4.20 -2 15 0 39.50 4.20 2 15 0 44.20 4.30 2 15 0 39.40 4.20 -2 15 0 30.70 4.30 -2 15 0 39.20 4.20 3 -15 0 47.40 6.00 3 -15 0 55.69 6.00 -3 -15 0 49.90 5.90 -3 -15 0 53.99 5.90 3 15 0 60.29 5.90 -3 15 0 53.99 6.00 3 15 0 52.59 5.90 3 15 0 57.29 5.90 -3 15 0 49.10 5.90 3 15 0 57.69 6.00 4 -15 0 -0.40 1.00 -4 -15 0 0.30 0.70 4 -15 0 0.70 1.10 -4 -15 0 0.50 1.10 -4 15 0 -0.40 1.10 4 15 0 0.50 0.90 4 15 0 0.00 0.60 -4 15 0 0.00 0.80 5 -15 0 7.50 1.60 -5 -15 0 8.00 1.30 5 -15 0 4.70 1.80 5 15 0 8.40 1.50 -5 15 0 6.20 1.70 5 15 0 6.50 1.10 -5 15 0 3.70 1.30 6 -15 0 44.20 5.20 -6 -15 0 48.80 5.30 6 15 0 44.70 5.20 6 15 0 39.80 5.00 -6 15 0 46.30 5.20 7 -15 0 -0.30 2.20 -7 -15 0 1.00 2.20 7 15 0 1.10 1.30 -7 15 0 0.70 1.90 7 15 0 -0.70 1.90 0 -16 0 1102.09 120.09 0 -16 0 1055.79 120.09 0 -16 0 1165.68 120.09 0 -16 0 1097.39 120.09 0 16 0 1165.38 120.09 0 16 0 1113.59 120.09 -1 -16 0 244.88 27.50 -1 -16 0 260.27 27.50 1 -16 0 239.78 27.50 1 -16 0 262.37 27.50 -1 -16 0 251.07 27.50 -1 -16 0 253.17 27.50 1 -16 0 234.58 27.50 -1 16 0 233.38 27.50 -1 16 0 266.37 27.50 1 16 0 266.87 27.50 -1 16 0 264.37 27.50 -1 16 0 264.87 27.50 1 16 0 260.67 27.50 2 -16 0 89.69 10.30 -2 -16 0 99.19 10.30 -2 -16 0 94.39 10.30 -2 -16 0 89.19 10.20 2 -16 0 89.09 10.30 -2 16 0 99.09 10.20 -2 16 0 85.89 10.30 2 16 0 95.09 10.30 2 16 0 96.39 10.20 2 16 0 97.99 10.20 -2 16 0 100.99 10.20 2 16 0 93.99 10.20 -3 -16 0 32.30 3.70 3 -16 0 29.50 3.70 3 -16 0 31.30 3.70 -3 -16 0 32.80 3.60 3 16 0 33.80 3.60 -3 16 0 34.50 3.60 3 16 0 33.80 3.60 3 16 0 29.70 3.50 -3 16 0 30.40 3.80 3 16 0 31.50 3.70 -4 -16 0 22.90 2.60 4 -16 0 21.10 2.70 4 -16 0 21.80 2.70 -4 16 0 23.70 2.60 4 16 0 23.30 2.70 -4 16 0 20.40 2.80 4 16 0 19.80 2.50 5 -16 0 1.50 1.40 5 -16 0 -0.80 1.40 -5 -16 0 0.30 1.00 -5 16 0 -0.60 1.10 -5 16 0 0.30 1.40 5 16 0 0.20 1.20 5 16 0 -0.20 0.80 6 -16 0 24.10 3.50 -6 -16 0 23.50 3.20 -6 16 0 28.90 3.20 6 16 0 25.50 3.20 6 16 0 21.30 2.90 7 -16 0 4.00 2.60 -7 -16 0 3.80 2.00 7 16 0 0.30 2.00 7 16 0 2.20 1.40 -7 16 0 2.40 1.90 1 -17 0 197.68 21.70 -1 -17 0 191.08 21.70 -1 -17 0 207.38 21.70 1 -17 0 200.48 21.70 -1 -17 0 201.78 21.70 1 -17 0 192.88 21.70 -1 -17 0 189.88 21.80 1 -17 0 204.78 21.80 1 17 0 206.48 21.80 -1 17 0 208.18 21.70 -1 17 0 211.08 21.70 -1 17 0 194.38 21.80 1 17 0 199.78 21.70 -1 17 0 207.78 21.70 -2 -17 0 18.50 2.40 2 -17 0 20.80 2.50 -2 -17 0 20.90 2.50 2 -17 0 21.20 2.50 -2 -17 0 20.00 2.50 -2 17 0 20.50 2.40 2 17 0 20.80 2.30 2 17 0 26.20 2.50 2 17 0 21.20 2.40 -2 17 0 22.30 2.60 -2 17 0 22.30 2.40 2 17 0 21.60 2.30 3 -17 0 18.80 2.70 3 -17 0 26.80 2.60 -3 -17 0 20.60 2.60 -3 -17 0 22.00 2.50 -3 17 0 20.30 2.50 -3 17 0 21.00 2.70 3 17 0 22.50 2.60 3 17 0 22.50 2.50 3 17 0 22.10 2.40 -4 -17 0 6.90 1.10 4 -17 0 7.30 1.40 4 -17 0 5.40 1.40 4 17 0 6.30 1.30 -4 17 0 4.60 1.40 4 17 0 7.20 0.90 -4 17 0 4.70 1.10 5 -17 0 40.40 4.60 -5 -17 0 38.00 4.40 5 -17 0 45.70 4.70 5 17 0 34.70 4.20 5 17 0 34.50 4.50 -5 17 0 41.40 4.60 -5 17 0 36.20 4.40 -6 -17 0 8.90 1.80 6 -17 0 9.10 2.10 6 17 0 13.80 2.00 6 17 0 6.40 1.40 -6 17 0 10.20 1.80 -7 -17 0 1.90 2.10 7 -17 0 1.40 2.40 -7 17 0 3.60 2.00 7 17 0 4.70 1.40 7 17 0 4.90 2.10 0 -18 0 654.53 67.59 0 -18 0 610.34 67.59 0 -18 0 588.64 67.69 0 -18 0 644.94 67.59 0 18 0 638.04 67.59 0 18 0 630.84 67.69 -1 -18 0 116.49 13.00 -1 -18 0 124.19 13.00 -1 -18 0 116.19 13.00 1 -18 0 115.29 13.00 1 -18 0 114.29 13.00 1 -18 0 108.09 13.00 -1 -18 0 116.99 13.00 1 -18 0 113.39 13.00 1 18 0 122.09 13.00 -1 18 0 115.69 12.90 -1 18 0 130.09 12.90 -1 18 0 129.19 13.00 -1 18 0 120.59 13.00 1 18 0 127.59 13.00 -2 -18 0 29.30 3.80 2 -18 0 30.10 3.90 2 -18 0 36.30 3.90 -2 -18 0 34.00 3.90 -2 18 0 37.20 3.80 2 18 0 36.60 3.80 -2 18 0 30.80 3.90 -2 18 0 37.90 3.80 2 18 0 34.30 3.70 2 18 0 36.60 3.90 -3 -18 0 10.70 1.50 -3 -18 0 10.00 1.30 3 -18 0 8.20 1.50 3 -18 0 10.60 1.50 -3 18 0 10.20 1.30 3 18 0 10.50 1.40 -3 18 0 8.50 1.60 3 18 0 10.80 1.20 3 18 0 9.30 1.20 4 -18 0 2.80 1.20 -4 -18 0 3.70 1.00 4 -18 0 5.40 1.40 -4 18 0 5.20 1.00 4 18 0 3.60 1.20 -4 18 0 2.70 1.30 4 18 0 5.50 0.80 5 -18 0 -0.30 1.40 5 -18 0 -0.40 1.40 -5 -18 0 -0.10 1.00 -5 18 0 0.20 1.60 -5 18 0 0.50 1.10 5 18 0 0.70 0.80 5 18 0 0.80 1.30 6 -18 0 25.30 3.30 -6 -18 0 22.60 2.80 6 18 0 22.70 2.60 6 18 0 16.10 2.80 -6 18 0 17.50 2.80 -7 -18 0 1.00 2.00 7 -18 0 -0.70 2.40 7 18 0 1.60 2.00 7 18 0 0.90 1.30 -7 18 0 4.00 2.00 0 19 0 6.80 1.20 1 -19 0 16.40 1.70 -1 -19 0 11.60 1.70 -1 -19 0 14.10 1.70 1 -19 0 12.10 1.90 -1 -19 0 16.20 1.90 -1 -19 0 13.40 1.70 1 -19 0 15.70 1.80 1 19 0 13.80 1.70 -1 19 0 13.90 1.90 -1 19 0 16.20 1.70 1 19 0 17.40 1.80 -1 19 0 15.70 1.60 -1 19 0 13.40 1.60 2 -19 0 0.70 0.60 -2 -19 0 -0.20 0.80 2 -19 0 0.70 0.90 2 -19 0 0.50 0.80 -2 -19 0 0.60 0.50 2 19 0 0.50 0.60 -2 19 0 0.80 0.40 -2 19 0 -0.60 0.80 -2 19 0 0.30 0.40 2 19 0 -0.20 0.70 -3 -19 0 164.48 18.20 3 -19 0 167.18 18.30 3 -19 0 173.98 18.30 -3 -19 0 163.78 18.30 3 19 0 166.98 18.20 3 19 0 169.18 18.20 -3 19 0 170.98 18.30 3 19 0 175.18 18.30 -3 19 0 170.08 18.20 4 -19 0 34.60 3.90 -4 -19 0 32.70 3.80 4 -19 0 33.70 4.00 -4 19 0 29.90 3.70 4 19 0 35.10 3.90 4 19 0 32.20 3.60 -4 19 0 33.40 4.00 5 -19 0 15.10 2.30 5 -19 0 12.80 2.30 -5 -19 0 13.20 2.00 5 19 0 16.30 1.80 5 19 0 19.00 2.30 -5 19 0 12.20 2.40 -5 19 0 11.10 2.00 6 -19 0 1.60 2.10 -6 -19 0 5.60 1.50 6 19 0 2.70 1.10 -6 19 0 1.60 1.50 6 19 0 1.40 1.60 7 -19 0 0.50 2.70 -7 -19 0 3.20 2.10 7 19 0 -0.30 2.20 -7 19 0 1.00 1.90 7 19 0 1.00 1.30 0 -20 0 39.70 4.10 0 -20 0 33.70 4.30 0 -20 0 35.20 4.20 0 -20 0 38.50 4.20 0 20 0 39.10 4.20 0 20 0 41.50 4.30 -1 -20 0 5.10 0.70 -1 -20 0 3.00 0.90 1 -20 0 3.00 0.80 1 -20 0 4.50 0.90 -1 -20 0 4.50 0.80 -1 -20 0 5.10 0.70 1 -20 0 5.60 1.10 1 -20 0 3.60 0.70 -1 20 0 5.70 0.70 -1 20 0 4.20 1.10 1 20 0 3.10 0.80 2 -20 0 67.59 7.80 -2 -20 0 62.89 7.60 2 -20 0 64.89 7.70 -2 -20 0 66.79 7.70 2 -20 0 74.39 7.70 -2 20 0 77.19 7.60 2 20 0 71.59 7.70 -2 20 0 68.69 7.80 -2 20 0 73.29 7.60 3 -20 0 1.40 1.10 -3 -20 0 1.30 0.70 -3 -20 0 1.50 1.00 3 -20 0 1.70 0.90 -3 20 0 0.70 1.10 -3 20 0 1.60 0.70 3 20 0 1.60 0.50 3 20 0 2.50 0.90 3 20 0 0.90 0.40 -4 -20 0 69.79 7.90 4 -20 0 75.19 8.00 4 -20 0 73.89 8.00 4 20 0 69.39 8.00 -4 20 0 63.29 7.90 4 20 0 77.19 7.80 -4 20 0 72.89 8.00 5 -20 0 7.50 1.90 -5 -20 0 10.90 1.60 5 -20 0 10.80 1.90 5 20 0 8.40 1.30 -5 20 0 9.60 1.50 5 20 0 8.90 1.80 -5 20 0 6.20 2.10 -6 -20 0 14.70 2.00 6 -20 0 12.60 2.40 6 20 0 10.80 2.20 -6 20 0 5.80 1.90 6 20 0 12.70 1.70 -6 20 0 13.80 4.20 -7 -20 0 2.50 2.10 7 -20 0 -0.80 2.90 7 20 0 -0.70 1.30 7 20 0 1.00 2.20 -7 20 0 1.70 1.90 0 -21 0 0.40 0.80 0 -21 0 0.20 0.40 0 -21 0 1.20 0.50 0 -21 0 0.40 0.60 0 21 0 0.00 0.60 0 21 0 0.80 0.80 -1 -21 0 87.79 10.20 -1 -21 0 90.59 10.30 1 -21 0 92.19 10.20 1 -21 0 86.69 10.20 -1 -21 0 91.99 10.20 -1 -21 0 92.39 10.20 1 -21 0 99.39 10.30 -1 21 0 96.19 10.30 1 21 0 103.39 10.20 -1 21 0 103.19 10.20 2 -21 0 32.00 4.00 2 -21 0 36.80 4.00 -2 -21 0 31.40 4.10 2 -21 0 37.40 4.10 -2 -21 0 34.80 3.90 -2 21 0 36.60 3.90 -2 21 0 34.60 4.10 2 21 0 34.50 4.00 -2 21 0 36.10 3.90 -3 -21 0 16.10 2.00 3 -21 0 19.10 2.40 3 -21 0 17.80 2.20 -3 -21 0 16.90 2.20 3 21 0 16.60 1.90 -3 21 0 16.70 2.00 -3 21 0 16.80 2.30 3 21 0 18.40 2.20 3 21 0 17.00 1.90 4 -21 0 67.79 7.80 4 -21 0 71.59 7.90 -4 -21 0 65.59 7.70 -4 21 0 72.49 7.70 4 21 0 71.69 7.60 -4 21 0 73.99 8.00 4 21 0 69.39 7.80 5 -21 0 5.70 1.70 5 -21 0 2.00 1.70 -5 -21 0 2.70 1.20 -5 21 0 3.50 1.60 5 21 0 1.40 0.80 5 21 0 4.20 1.40 -5 21 0 2.60 1.10 -6 -21 0 2.40 1.50 6 -21 0 -1.90 2.10 6 -21 0 2.80 2.00 6 21 0 1.30 1.60 -6 21 0 -0.40 2.20 -6 21 0 3.10 1.50 6 21 0 1.70 1.00 7 -21 0 1.80 2.60 -7 -21 0 -2.40 2.20 7 21 0 0.80 1.20 7 21 0 -0.40 2.20 -7 21 0 0.30 1.90 0 -22 0 56.39 6.70 0 -22 0 59.39 6.50 0 -22 0 60.29 6.60 0 -22 0 55.39 6.50 0 22 0 69.69 6.60 1 -22 0 67.29 7.00 1 -22 0 63.29 7.00 1 -22 0 53.39 7.10 -1 -22 0 59.79 6.90 -1 -22 0 58.79 7.10 -1 22 0 70.29 7.10 -1 22 0 68.79 6.90 1 22 0 67.69 7.00 2 -22 0 9.90 1.50 -2 -22 0 9.90 1.70 -2 -22 0 10.50 1.40 2 -22 0 12.70 1.70 2 -22 0 11.70 1.80 -2 22 0 13.50 1.40 -2 22 0 11.30 1.40 -2 22 0 9.60 1.70 2 22 0 16.00 1.70 3 -22 0 366.66 40.80 3 -22 0 409.96 40.90 3 -22 0 373.56 40.90 -3 -22 0 382.36 40.90 -3 -22 0 355.76 40.80 -3 22 0 373.56 40.80 3 22 0 385.86 40.90 -3 22 0 398.06 40.90 4 -22 0 2.70 1.30 4 -22 0 1.30 1.20 -4 -22 0 2.10 0.90 4 22 0 1.00 0.50 -4 22 0 0.50 1.40 -4 22 0 0.30 0.80 4 22 0 1.60 1.20 5 -22 0 1.40 1.60 -5 -22 0 0.30 1.10 5 -22 0 -0.40 1.60 5 22 0 -0.20 1.30 -5 22 0 0.70 1.80 5 22 0 0.10 0.70 -5 22 0 0.60 1.00 -6 -22 0 3.30 1.60 6 -22 0 5.90 2.20 6 -22 0 4.40 2.10 6 22 0 2.60 1.00 -6 22 0 0.50 1.40 6 22 0 4.60 1.80 -6 22 0 0.40 2.00 -7 -22 0 3.00 2.30 7 -22 0 3.90 2.70 -7 22 0 4.70 2.00 7 22 0 2.10 1.30 7 22 0 3.70 2.50 0 -23 0 0.60 0.90 0 -23 0 1.00 0.50 0 -23 0 0.90 0.70 0 23 0 1.00 0.70 1 -23 0 34.10 4.20 1 -23 0 35.40 4.40 -1 -23 0 35.80 4.20 1 -23 0 38.10 4.30 -1 -23 0 36.30 4.40 -1 23 0 42.50 4.40 1 23 0 40.80 4.30 -1 23 0 42.10 4.20 2 -23 0 11.50 1.40 -2 -23 0 9.10 1.60 2 -23 0 10.70 1.60 2 -23 0 10.60 1.70 -2 -23 0 9.00 1.30 -2 23 0 7.80 1.60 -2 23 0 11.50 1.20 2 23 0 11.20 1.50 -2 23 0 9.70 1.20 -3 -23 0 201.38 21.80 3 -23 0 193.98 21.80 3 -23 0 218.58 21.80 -3 -23 0 202.58 21.70 3 -23 0 199.08 21.90 -3 23 0 199.98 21.70 3 23 0 199.28 21.80 -3 23 0 197.68 21.90 4 -23 0 186.28 18.50 4 -23 0 164.58 18.40 -4 -23 0 173.38 18.30 4 -23 0 175.58 18.40 4 23 0 170.18 18.20 -4 23 0 176.48 18.50 -4 23 0 149.69 18.30 4 23 0 171.68 18.40 -5 -23 0 4.00 1.20 5 -23 0 1.90 1.70 5 -23 0 1.50 1.70 5 23 0 2.10 0.70 -5 23 0 -0.10 1.10 5 23 0 0.60 1.40 -5 23 0 0.20 1.90 6 -23 0 9.30 2.30 6 -23 0 6.40 2.60 -6 -23 0 4.50 1.80 6 -23 0 4.50 2.30 6 23 0 6.80 2.00 -6 23 0 7.80 1.60 -6 23 0 9.50 2.40 6 23 0 6.50 1.30 7 -23 0 5.50 2.90 -7 -23 0 7.30 2.40 7 23 0 5.30 1.50 7 23 0 4.80 2.60 -7 23 0 5.20 2.00 0 -24 0 8.70 1.20 0 -24 0 8.20 1.30 0 -24 0 8.10 1.50 0 24 0 10.70 1.30 1 -24 0 9.90 1.20 1 -24 0 7.50 1.30 -1 -24 0 6.10 1.00 1 -24 0 8.70 1.40 -1 -24 0 9.20 1.50 1 24 0 9.10 1.30 -1 24 0 4.60 1.40 2 -24 0 28.50 4.00 2 -24 0 32.10 3.90 2 -24 0 39.40 3.90 -2 -24 0 30.10 4.00 -2 -24 0 34.00 3.80 2 24 0 32.90 3.90 -2 24 0 33.60 3.70 -2 24 0 36.70 3.70 -2 24 0 33.30 4.00 -3 -24 0 2.00 0.80 3 -24 0 0.00 1.00 -3 -24 0 1.00 1.20 3 -24 0 3.10 1.30 3 -24 0 0.50 1.20 -3 24 0 2.30 0.60 -3 24 0 1.50 1.40 3 24 0 2.30 1.10 4 -24 0 156.88 17.00 4 -24 0 163.08 16.90 -4 -24 0 150.48 16.80 4 -24 0 160.38 16.90 -4 24 0 171.98 17.00 4 24 0 144.69 16.80 -4 24 0 147.89 16.70 5 -24 0 1.60 2.10 -5 -24 0 1.00 1.20 5 -24 0 -0.30 1.90 5 -24 0 0.90 1.60 5 24 0 1.00 1.50 5 24 0 0.40 0.70 -5 24 0 -0.10 1.90 -5 24 0 0.30 1.00 -6 -24 0 24.40 2.90 6 -24 0 21.00 3.70 6 -24 0 21.80 3.30 6 -24 0 16.50 3.30 -6 24 0 19.60 2.90 6 24 0 13.20 3.10 6 24 0 25.20 2.60 -6 24 0 19.40 3.40 0 -25 0 0.50 0.90 0 -25 0 0.20 1.10 0 -25 0 0.50 0.60 0 25 0 0.80 0.70 1 -25 0 26.80 3.50 1 -25 0 27.70 3.60 -1 -25 0 32.30 3.40 1 -25 0 31.70 3.40 -1 -25 0 29.30 3.60 1 25 0 29.60 3.40 -1 25 0 28.70 3.60 2 -25 0 36.20 4.80 -2 -25 0 40.70 4.90 2 -25 0 48.00 5.10 -2 -25 0 44.60 4.70 2 -25 0 45.00 4.80 -2 25 0 41.20 4.60 2 25 0 47.20 4.90 -2 25 0 46.20 5.00 -3 -25 0 3.30 1.40 -3 -25 0 3.50 0.90 3 -25 0 1.10 1.50 3 -25 0 2.70 1.10 3 -25 0 4.30 1.60 -3 25 0 2.60 0.70 -3 25 0 0.90 1.50 3 25 0 2.10 1.10 4 -25 0 0.80 1.50 4 -25 0 0.90 1.60 -4 -25 0 -0.30 0.90 4 -25 0 0.70 1.30 -4 25 0 -0.60 0.90 4 25 0 1.40 1.30 -4 25 0 -0.30 1.40 5 -25 0 16.90 3.00 -5 -25 0 13.00 2.30 5 -25 0 15.50 2.60 5 -25 0 21.80 3.00 5 25 0 22.80 2.70 -5 25 0 16.50 2.90 5 25 0 19.10 2.00 -5 25 0 12.70 2.20 6 -25 0 3.70 2.60 6 -25 0 8.30 2.70 6 -25 0 9.90 2.50 -6 -25 0 3.90 1.80 -6 25 0 5.70 1.70 -6 25 0 6.80 2.60 6 25 0 6.80 2.20 6 25 0 8.20 1.20 0 -26 0 188.08 20.70 0 -26 0 204.68 20.80 0 26 0 188.08 20.70 -1 -26 0 29.50 3.30 1 -26 0 25.10 3.40 1 -26 0 32.40 3.30 -1 -26 0 32.90 3.60 1 -26 0 23.90 3.50 -1 26 0 30.20 3.50 1 26 0 28.90 3.40 2 -26 0 302.67 31.90 -2 -26 0 290.27 32.00 2 -26 0 309.07 32.00 -2 -26 0 275.87 31.90 2 -26 0 297.57 31.90 -2 26 0 306.97 32.00 2 26 0 298.17 31.90 3 -26 0 98.59 11.50 3 -26 0 122.89 11.50 -3 -26 0 93.59 11.30 -3 -26 0 105.29 11.50 3 -26 0 105.09 11.40 -3 26 0 103.39 11.30 -3 26 0 106.89 11.50 3 26 0 108.69 11.50 4 -26 0 29.30 3.60 4 -26 0 30.30 3.70 -4 -26 0 29.60 3.40 4 -26 0 25.60 3.60 -4 26 0 26.10 3.70 -4 26 0 27.10 3.30 4 26 0 34.00 3.70 5 -26 0 0.10 1.80 5 -26 0 0.20 1.80 -5 -26 0 -0.20 1.20 5 -26 0 0.40 1.80 -5 26 0 -0.70 1.10 5 26 0 -0.90 1.50 -5 26 0 -0.80 1.70 6 -26 0 2.10 2.30 6 -26 0 5.40 2.70 -6 -26 0 3.70 1.70 6 -26 0 4.40 2.70 -6 26 0 2.90 2.60 6 26 0 4.80 2.10 6 26 0 6.20 1.00 -6 26 0 4.10 1.50 0 -27 0 3.70 1.30 0 -27 0 5.70 0.90 0 27 0 3.80 1.00 1 -27 0 41.50 4.90 1 -27 0 41.80 4.60 1 -27 0 35.70 4.60 -1 -27 0 43.10 4.50 -1 -27 0 48.80 4.90 -1 27 0 34.40 4.80 1 27 0 41.30 4.60 -2 -27 0 4.40 1.30 2 -27 0 4.50 1.40 2 -27 0 6.30 1.10 2 -27 0 4.00 1.60 -2 -27 0 5.50 1.00 -2 27 0 3.50 1.60 2 27 0 3.90 1.20 3 -27 0 65.09 7.00 -3 -27 0 61.89 6.90 3 -27 0 68.29 7.00 3 -27 0 67.69 7.20 -3 -27 0 70.09 7.10 -3 27 0 56.49 7.10 3 27 0 62.99 7.00 -3 27 0 57.99 6.80 4 -27 0 280.17 29.60 4 -27 0 307.77 29.70 4 27 0 270.17 29.60 -4 27 0 255.67 29.50 -4 27 0 269.77 29.70 5 -27 0 3.20 2.20 -5 -27 0 6.10 1.40 5 -27 0 0.90 1.90 5 -27 0 0.40 1.70 -5 27 0 1.70 1.20 -5 27 0 1.00 1.80 5 27 0 3.80 1.70 -6 -27 0 14.80 2.20 6 -27 0 12.70 2.60 6 -27 0 7.80 2.80 6 -27 0 12.90 3.20 6 27 0 7.80 2.50 -6 27 0 13.60 3.00 -6 27 0 8.40 1.80 0 -28 0 29.10 3.10 0 -28 0 22.00 2.60 0 28 0 20.30 2.70 1 -28 0 11.40 1.80 -1 -28 0 10.20 1.90 1 -28 0 11.90 1.60 -1 -28 0 12.80 1.60 1 -28 0 13.50 2.00 1 28 0 15.40 1.80 -1 28 0 9.70 2.00 2 -28 0 1.50 1.30 2 -28 0 0.30 1.50 -2 -28 0 0.30 1.20 -2 -28 0 0.70 0.80 2 -28 0 1.50 1.00 -2 28 0 -0.60 1.50 2 28 0 1.90 1.10 -3 -28 0 14.50 2.00 -3 -28 0 16.00 2.40 3 -28 0 14.70 2.30 3 -28 0 15.50 2.50 3 -28 0 19.30 2.30 -3 28 0 14.70 1.80 -3 28 0 13.40 2.40 3 28 0 20.10 2.30 -4 -28 0 23.90 3.40 4 -28 0 37.20 4.00 4 -28 0 29.80 4.00 4 -28 0 39.70 3.80 -4 28 0 36.90 4.00 -4 28 0 27.60 3.40 4 28 0 26.30 3.70 5 -28 0 6.60 2.10 5 -28 0 2.40 2.10 5 -28 0 1.70 1.80 -5 -28 0 2.10 1.40 -5 28 0 4.00 1.20 -5 28 0 2.40 2.00 5 28 0 2.10 1.70 6 -28 0 1.70 3.00 6 -28 0 1.00 2.70 6 -28 0 -0.90 2.50 -6 -28 0 1.60 1.80 -6 28 0 0.80 2.80 -6 28 0 1.00 1.50 6 28 0 -1.00 2.10 0 -29 0 0.20 0.80 0 -29 0 1.80 1.50 0 29 0 0.80 1.00 -1 -29 0 37.90 4.50 1 -29 0 37.30 4.20 -1 -29 0 35.00 4.20 1 -29 0 38.90 4.50 -1 29 0 39.00 4.50 1 29 0 39.30 4.30 2 -29 0 1.10 1.40 -2 -29 0 1.90 1.50 2 -29 0 0.90 1.60 2 -29 0 1.50 1.10 -2 -29 0 2.60 0.90 -2 29 0 3.20 1.60 2 29 0 2.20 1.20 3 -29 0 5.60 1.40 3 -29 0 4.80 1.70 -3 -29 0 2.20 1.70 -3 -29 0 1.60 1.00 3 -29 0 0.80 1.60 -3 29 0 2.00 0.60 3 29 0 2.50 1.30 -3 29 0 1.00 1.60 -4 -29 0 14.20 2.20 4 -29 0 20.50 3.00 4 -29 0 20.00 2.80 4 -29 0 21.80 2.60 -4 29 0 21.80 3.00 -4 29 0 16.00 2.10 4 29 0 15.60 2.50 5 -29 0 1.00 2.40 5 -29 0 0.10 2.40 -5 -29 0 3.00 1.40 5 -29 0 3.10 2.00 -5 29 0 1.80 2.10 5 29 0 0.50 1.70 -5 29 0 0.50 1.10 6 -29 0 -0.70 3.10 6 -29 0 0.70 3.00 -6 -29 0 1.80 1.80 6 -29 0 1.70 2.80 6 29 0 -1.90 2.20 -6 29 0 -1.50 1.50 -6 29 0 -0.30 2.90 0 -30 0 141.09 16.20 0 -30 0 166.98 16.40 1 -30 0 9.10 1.90 -1 -30 0 11.20 2.00 1 -30 0 7.70 1.30 -1 -30 0 6.80 1.20 -1 30 0 6.70 1.80 1 30 0 8.00 1.50 2 -30 0 12.40 2.00 2 -30 0 10.20 2.00 -2 -30 0 14.90 2.20 -2 -30 0 8.70 1.50 2 -30 0 10.40 1.60 2 30 0 12.50 1.80 -2 30 0 9.50 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5.70 -3 -25 -2 39.60 4.50 3 -25 2 38.10 4.50 -3 -25 -2 42.40 4.70 3 -25 2 32.40 4.60 3 25 2 41.00 4.60 -3 25 -2 38.50 4.70 3 25 2 36.90 4.30 4 -25 2 36.00 5.00 -4 -25 -2 42.10 4.90 4 -25 2 47.60 5.00 4 25 2 39.40 4.90 -4 25 -2 40.60 5.10 -4 25 -2 40.00 4.50 4 25 2 40.10 4.60 5 -25 2 4.00 2.20 5 -25 2 0.20 2.10 -5 -25 -2 2.20 1.90 -5 25 -2 -1.40 1.20 5 25 2 2.60 1.30 5 25 2 0.50 1.80 -5 25 -2 -0.60 2.40 7 -26 -2 7.70 3.20 -7 -26 2 2.50 2.00 -7 26 2 6.00 2.10 7 26 -2 4.40 2.30 6 -26 -2 22.90 3.00 -6 -26 2 15.00 2.40 6 -26 -2 20.10 3.30 -6 26 2 13.60 2.50 6 26 -2 21.80 2.90 -5 -26 2 5.80 1.20 5 -26 -2 10.50 1.90 5 -26 -2 5.50 2.20 5 -26 -2 7.10 2.20 5 26 -2 9.70 1.80 -5 26 2 4.10 1.40 -4 -26 2 219.58 24.00 4 -26 -2 231.48 24.20 4 -26 -2 231.58 24.10 4 -26 -2 230.68 24.10 4 26 -2 232.38 24.10 -4 26 2 200.38 24.00 3 -26 -2 7.00 1.90 3 -26 -2 8.90 1.40 3 -26 -2 4.60 1.50 -3 -26 2 6.00 1.60 -3 -26 2 6.10 1.00 -3 26 2 7.90 1.20 3 26 -2 12.70 1.50 -2 -26 2 45.60 6.30 -2 -26 2 57.79 6.40 2 -26 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99.59 10.80 -1 29 2 94.89 10.70 0 -29 -2 90.89 10.10 0 -29 -2 82.69 9.90 0 -29 2 91.09 10.00 0 -29 2 101.79 10.10 0 -29 2 94.89 9.80 0 29 -2 93.59 10.00 0 29 2 83.29 9.80 0 29 2 99.29 10.00 -1 -29 -2 9.70 2.20 1 -29 2 8.00 1.50 1 -29 2 9.30 2.00 -1 -29 -2 10.00 1.70 1 29 2 13.30 1.80 -1 29 -2 11.80 2.00 1 29 2 11.70 1.30 2 -29 2 -0.90 1.40 2 -29 2 0.60 1.10 -2 -29 -2 0.10 1.70 -2 -29 -2 0.10 1.10 -2 29 -2 0.70 1.70 2 29 2 0.00 0.60 2 29 2 -0.20 1.30 -3 -29 -2 10.70 2.00 3 -29 2 17.00 2.20 3 -29 2 12.40 2.50 -3 -29 -2 13.80 2.60 3 29 2 13.30 1.70 3 29 2 12.30 2.20 -3 29 -2 13.80 2.60 4 -29 2 58.69 6.80 4 -29 2 59.19 6.80 -4 29 -2 57.79 6.90 4 29 2 54.39 6.70 4 29 2 56.79 6.30 -5 -29 -2 5.40 2.20 5 -29 2 4.40 2.60 5 -29 2 3.90 2.90 -5 29 -2 6.60 1.30 5 29 2 5.80 2.30 -5 29 -2 5.80 3.10 5 29 2 5.90 1.40 6 -30 -2 5.90 2.60 6 -30 -2 5.10 2.90 -6 -30 2 6.40 1.70 6 -30 -2 5.50 2.90 6 30 -2 9.60 2.40 -6 30 2 5.30 1.60 -5 -30 2 8.40 1.60 5 -30 -2 8.00 2.60 5 -30 -2 11.90 2.30 5 -30 -2 13.80 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2.50 -1 10 3 23.50 2.50 1 10 -3 20.40 2.50 -1 10 3 25.00 2.50 -1 10 3 19.80 2.50 1 10 -3 25.30 2.60 0 -10 -3 117.29 11.90 0 -10 3 107.79 11.90 0 -10 -3 112.29 11.90 0 -10 -3 112.19 11.80 0 -10 3 104.89 11.90 0 -10 3 110.89 11.90 0 -10 -3 111.89 11.90 0 -10 3 99.69 11.80 0 10 3 111.99 11.90 0 10 3 106.49 11.90 0 10 -3 115.39 11.90 0 10 -3 108.29 11.80 0 10 -3 110.99 11.90 0 10 3 113.19 11.90 1 -10 3 71.39 7.70 -1 -10 -3 70.49 7.80 -1 -10 -3 80.49 7.80 1 -10 3 71.69 7.80 -1 -10 -3 67.99 7.80 1 -10 3 69.99 7.70 1 10 3 60.69 7.70 1 10 3 71.29 7.80 -1 10 -3 72.79 7.70 1 10 3 67.29 7.80 -1 10 -3 64.79 7.80 -1 10 -3 70.89 7.70 1 10 3 78.69 7.70 2 -10 3 0.00 0.70 2 -10 3 -0.40 0.70 2 -10 3 0.50 0.90 -2 -10 -3 0.40 0.90 -2 -10 -3 1.00 0.90 -2 -10 -3 0.40 0.70 2 10 3 0.10 0.70 -2 10 -3 -0.20 0.90 2 10 3 0.20 0.60 -2 10 -3 -0.10 0.70 2 10 3 0.70 0.70 3 -10 3 30.10 3.60 -3 -10 -3 30.40 3.60 3 -10 3 31.40 3.60 -3 -10 -3 32.50 3.70 -3 10 -3 30.30 3.60 3 10 3 31.40 3.60 3 10 3 29.10 3.60 -3 10 -3 27.80 3.70 4 -10 3 16.70 2.10 -4 -10 -3 12.30 2.20 4 -10 3 11.00 2.00 -4 10 -3 12.30 2.10 4 10 3 9.50 2.00 -4 10 -3 14.30 2.00 4 10 3 14.20 1.90 5 -10 3 10.00 2.00 5 10 3 9.40 1.80 5 10 3 4.70 1.80 -5 10 -3 4.00 1.70 -5 10 -3 8.30 2.20 6 -10 3 3.20 2.70 6 10 3 3.00 2.20 6 10 3 4.90 2.10 -6 10 -3 1.50 2.10 -8 -11 3 0.40 1.70 8 -11 -3 1.00 2.20 8 11 -3 0.20 1.20 8 11 -3 -0.20 1.90 8 11 -3 0.10 2.00 7 -11 -3 17.30 2.40 -7 -11 3 16.60 2.10 7 -11 -3 12.30 2.40 7 11 -3 13.20 2.40 7 11 -3 15.50 2.40 7 11 -3 13.00 1.80 -6 -11 3 4.60 1.20 6 -11 -3 7.70 1.50 6 -11 -3 7.50 1.60 -6 11 3 7.60 1.70 6 11 -3 6.80 1.50 6 11 -3 5.10 1.00 6 11 -3 6.20 1.50 -5 -11 3 13.60 1.40 5 -11 -3 7.90 1.50 5 -11 -3 10.10 1.60 5 -11 -3 11.90 1.70 -5 11 3 7.80 1.60 5 11 -3 10.90 1.60 5 11 -3 9.00 1.50 5 11 -3 10.90 1.30 4 -11 -3 29.50 3.90 -4 -11 3 30.70 3.90 4 -11 -3 36.30 4.00 4 -11 -3 34.60 4.00 4 -11 -3 32.40 3.90 4 11 -3 38.30 3.80 -4 11 3 31.40 4.00 -4 11 3 34.90 3.90 4 11 -3 37.50 3.90 -4 11 3 37.30 3.90 4 11 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22.10 2.90 8 12 -3 26.10 3.50 8 12 -3 17.80 3.40 7 -12 -3 -0.50 1.60 -7 -12 3 0.60 1.20 7 12 -3 -0.10 1.50 7 12 -3 -0.30 0.80 7 12 -3 2.20 1.60 6 -12 -3 0.40 1.40 6 -12 -3 -0.30 1.20 -6 -12 3 0.90 1.00 6 12 -3 1.40 1.30 6 12 -3 -0.70 0.60 -6 12 3 1.20 1.40 6 12 -3 3.20 1.20 -5 -12 3 33.90 4.10 5 -12 -3 34.70 4.20 5 -12 -3 40.60 4.30 5 -12 -3 32.60 4.20 5 12 -3 37.50 4.00 5 12 -3 37.40 4.20 -5 12 3 35.10 4.20 5 12 -3 36.80 4.20 4 -12 -3 0.70 0.80 -4 -12 3 1.00 0.50 4 -12 -3 1.30 0.90 4 -12 -3 0.90 1.00 4 -12 -3 0.10 0.90 -4 12 3 -0.10 0.60 4 12 -3 0.60 0.80 -4 12 3 -0.30 0.60 -4 12 3 0.30 0.80 4 12 -3 0.40 0.70 3 -12 -3 11.80 1.70 -3 -12 3 11.70 1.50 3 -12 -3 14.70 1.70 3 -12 -3 11.10 1.70 3 -12 -3 11.10 1.60 -3 -12 3 15.50 1.50 -3 12 3 15.00 1.60 3 12 -3 13.20 1.60 3 12 -3 9.30 1.60 -3 12 3 12.30 1.60 3 12 -3 13.70 1.60 -3 12 3 13.70 1.60 -2 -12 3 35.40 3.90 -2 -12 3 35.30 4.00 2 -12 -3 36.50 4.00 -2 -12 3 33.90 3.90 2 -12 -3 36.90 4.00 2 -12 -3 38.50 4.00 2 -12 -3 32.90 4.00 2 12 -3 33.50 4.00 -2 12 3 38.80 4.00 -2 12 3 35.80 4.00 2 12 -3 36.00 4.00 2 12 -3 37.40 4.00 -2 12 3 37.60 4.00 -1 -12 3 4.40 0.80 -1 -12 3 4.00 0.60 1 -12 -3 5.70 0.80 1 -12 -3 4.50 0.90 1 -12 -3 3.70 0.70 -1 -12 3 3.90 0.60 1 -12 -3 4.50 0.80 -1 12 3 5.50 0.80 -1 12 3 5.70 0.80 1 12 -3 3.70 0.80 -1 12 3 3.90 0.80 1 12 -3 5.90 0.90 0 -12 -3 0.80 0.60 0 -12 -3 0.40 0.80 0 -12 -3 0.80 0.60 0 -12 3 0.90 0.50 0 -12 3 0.90 0.80 0 -12 3 0.50 0.60 0 -12 -3 0.80 0.50 0 -12 3 0.40 0.40 0 12 3 0.80 0.70 0 12 3 0.90 0.60 0 12 3 1.30 0.70 0 12 -3 0.60 0.80 0 12 -3 0.50 0.70 -1 -12 -3 107.09 12.20 1 -12 3 113.09 12.10 1 -12 3 121.19 12.20 -1 -12 -3 112.39 12.20 1 -12 3 110.79 12.10 -1 -12 -3 109.09 12.10 1 12 3 114.39 12.20 1 12 3 121.29 12.10 1 12 3 105.69 12.10 -1 12 -3 108.19 12.20 -1 12 -3 100.19 12.10 -1 12 -3 118.59 12.10 1 12 3 112.79 12.10 -2 -12 -3 2.30 0.90 -2 -12 -3 0.80 1.10 2 -12 3 1.00 1.00 -2 -12 -3 1.10 1.10 2 -12 3 1.60 0.80 -2 12 -3 1.30 0.70 2 12 3 1.10 0.80 2 12 3 1.60 0.80 -2 12 -3 0.40 1.00 -3 -12 -3 5.10 1.50 3 -12 3 3.00 1.40 -3 -12 -3 4.90 1.20 3 -12 3 7.60 1.30 -3 12 -3 3.30 1.40 3 12 3 4.30 1.20 3 12 3 5.50 1.10 -3 12 -3 5.60 1.10 -4 -12 -3 0.30 1.60 4 -12 3 -0.10 1.30 4 -12 3 0.60 1.40 -4 12 -3 0.40 1.70 -4 12 -3 0.30 1.10 4 12 3 0.70 1.40 4 12 3 -0.50 1.10 5 -12 3 2.10 1.80 -5 12 -3 -0.60 1.40 -5 12 -3 0.00 2.00 5 12 3 1.00 1.60 5 12 3 2.90 1.40 6 -12 3 2.30 2.70 6 12 3 3.10 2.20 6 12 3 3.50 2.00 -6 12 -3 2.00 2.10 8 -13 -3 19.70 3.30 -8 -13 3 16.60 2.60 8 13 -3 14.40 2.10 8 13 -3 15.70 2.80 -7 -13 3 0.60 1.20 7 -13 -3 -0.30 1.70 7 13 -3 -0.10 1.50 7 13 -3 0.30 1.50 -7 13 3 -0.50 1.70 7 13 -3 0.60 0.80 6 -13 -3 118.39 13.00 6 -13 -3 118.89 13.00 -6 -13 3 116.19 12.90 6 13 -3 116.79 12.80 6 13 -3 126.49 13.00 6 13 -3 121.09 13.00 -6 13 3 114.59 13.00 5 -13 -3 18.90 2.70 5 -13 -3 26.30 2.80 5 -13 -3 21.80 2.70 -5 -13 3 21.70 2.60 5 -13 -3 22.20 2.80 5 13 -3 22.50 2.50 5 13 -3 20.40 2.40 -5 13 3 18.90 2.70 5 13 -3 24.10 2.80 5 13 -3 28.80 2.80 4 -13 -3 16.90 1.90 4 -13 -3 14.20 1.90 -4 -13 3 13.80 1.80 4 -13 -3 19.30 2.00 4 -13 -3 12.90 1.90 4 13 -3 16.20 2.00 4 13 -3 10.80 1.90 -4 13 3 17.70 1.80 -4 13 3 13.00 1.90 3 -13 -3 44.30 5.40 -3 -13 3 47.40 5.30 3 -13 -3 53.09 5.40 -3 -13 3 45.80 5.30 3 -13 -3 45.60 5.40 3 -13 -3 51.99 5.40 -3 13 3 50.19 5.40 -3 13 3 53.69 5.40 3 13 -3 51.59 5.40 3 13 -3 46.30 5.40 3 13 -3 52.19 5.40 -3 13 3 47.20 5.40 2 -13 -3 18.30 2.10 2 -13 -3 14.70 2.00 2 -13 -3 17.70 2.20 -2 -13 3 19.10 2.10 -2 -13 3 16.50 1.90 2 -13 -3 18.40 2.10 2 13 -3 17.50 2.10 2 13 -3 18.00 2.10 2 13 -3 17.00 2.10 -2 13 3 16.90 2.10 -2 13 3 17.80 2.10 -2 13 3 18.60 2.10 -1 -13 3 10.00 1.20 1 -13 -3 10.70 1.30 1 -13 -3 11.80 1.50 -1 -13 3 10.10 1.20 -1 -13 3 11.60 1.40 1 -13 -3 10.80 1.40 1 -13 -3 12.40 1.40 -1 13 3 9.00 1.40 1 13 -3 9.20 1.40 1 13 -3 10.30 1.40 -1 13 3 14.60 1.40 -1 13 3 13.00 1.50 1 13 -3 9.80 1.40 0 -13 -3 0.60 0.80 0 -13 3 1.70 0.60 0 -13 -3 2.80 0.70 0 -13 3 1.40 0.40 0 -13 -3 1.20 0.50 0 -13 3 1.30 0.80 0 -13 -3 0.80 0.70 0 -13 3 1.70 0.60 0 13 3 0.70 0.70 0 13 3 1.10 0.60 0 13 -3 0.80 0.70 0 13 3 0.80 0.70 0 13 -3 1.00 0.80 1 -13 3 79.09 8.80 1 -13 3 83.09 8.90 -1 -13 -3 85.49 8.80 1 -13 3 84.69 8.80 -1 -13 -3 75.89 8.90 -1 -13 -3 83.59 8.80 -1 13 -3 73.09 8.70 1 13 3 72.29 8.80 -1 13 -3 81.09 8.90 1 13 3 86.09 8.90 -1 13 -3 88.69 8.70 -2 -13 -3 11.60 1.50 -2 -13 -3 7.50 1.50 2 -13 3 9.30 1.50 2 -13 3 10.90 1.40 2 13 3 8.70 1.40 -2 13 -3 7.20 1.20 -2 13 -3 11.10 1.60 2 13 3 11.20 1.40 3 -13 3 32.50 4.30 -3 -13 -3 33.20 4.30 3 -13 3 36.20 4.20 -3 -13 -3 42.20 4.40 -3 13 -3 35.20 4.40 3 13 3 34.40 4.20 3 13 3 42.80 4.30 -4 -13 -3 0.50 1.70 4 -13 3 0.70 1.50 4 -13 3 -0.50 1.30 4 13 3 1.90 1.40 -4 13 -3 0.90 1.10 4 13 3 -0.70 1.10 -4 13 -3 0.60 1.50 5 -13 3 -0.90 2.00 5 13 3 -0.80 1.40 5 13 3 -0.30 1.60 -5 13 -3 0.80 2.00 -5 13 -3 -0.40 1.50 6 -13 3 -0.30 2.40 -6 13 -3 2.00 2.10 6 13 3 0.20 2.20 6 13 3 1.10 2.00 -8 -14 3 8.30 1.90 8 -14 -3 7.50 2.80 8 14 -3 4.50 1.30 8 14 -3 8.20 2.20 -7 -14 3 9.80 1.80 7 -14 -3 8.40 2.20 7 14 -3 11.90 2.10 -7 14 3 5.70 2.10 7 14 -3 10.60 1.40 7 14 -3 11.80 2.10 6 -14 -3 15.00 2.20 -6 -14 3 11.40 1.80 -6 14 3 12.50 2.10 6 14 -3 13.00 1.50 6 14 -3 9.00 2.00 6 14 -3 14.90 2.00 -5 -14 3 27.20 3.20 5 -14 -3 31.80 3.40 5 -14 -3 24.90 3.30 5 -14 -3 29.60 3.40 5 -14 -3 28.80 3.30 -5 14 3 23.10 3.30 5 14 -3 27.10 3.30 5 14 -3 28.40 3.30 4 -14 -3 86.49 9.40 -4 -14 3 85.19 9.30 4 -14 -3 87.99 9.40 4 -14 -3 84.59 9.40 4 -14 -3 90.19 9.40 -4 14 3 83.49 9.40 -4 14 3 81.89 9.30 4 14 -3 90.09 9.40 4 14 -3 87.49 9.40 3 -14 -3 11.10 1.60 -3 -14 3 12.90 1.40 3 -14 -3 11.70 1.50 -3 -14 3 9.00 1.30 3 -14 -3 12.60 1.50 3 -14 -3 9.40 1.50 3 14 -3 11.30 1.50 -3 14 3 11.60 1.40 -3 14 3 12.90 1.50 3 14 -3 11.30 1.40 3 14 -3 11.60 1.50 -3 14 3 10.00 1.50 2 -14 -3 111.09 11.60 2 -14 -3 105.99 11.70 2 -14 -3 110.89 11.60 -2 -14 3 102.09 11.60 2 -14 -3 108.99 11.60 -2 14 3 107.29 11.60 2 14 -3 104.39 11.60 -2 14 3 102.89 11.60 2 14 -3 105.59 11.60 2 14 -3 111.89 11.60 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3.70 3 -22 -3 34.70 3.70 3 22 -3 34.80 3.70 3 22 -3 31.20 3.70 3 22 -3 34.70 3.70 -3 22 3 35.00 3.60 2 -22 -3 24.00 2.70 2 -22 -3 23.10 2.60 -2 22 3 23.00 2.50 2 22 -3 15.70 2.50 2 22 -3 21.60 2.60 2 22 -3 21.70 2.60 -2 22 3 19.80 2.50 1 -22 -3 96.09 9.90 -1 -22 3 86.49 9.80 1 -22 -3 82.29 9.80 -1 -22 3 97.39 9.80 -1 22 3 92.79 9.70 1 22 -3 89.89 9.80 1 22 -3 86.19 9.80 -1 22 3 87.89 9.80 1 22 -3 86.69 9.80 0 -22 -3 3.70 1.10 0 -22 -3 2.40 1.20 0 -22 3 3.00 1.40 0 -22 3 2.40 0.60 0 22 3 1.70 0.90 0 22 -3 5.10 1.20 0 22 3 1.10 0.70 0 22 -3 2.90 1.20 -1 -22 -3 79.89 8.40 1 -22 3 76.69 8.30 -1 -22 -3 79.49 8.50 1 -22 3 81.29 8.50 1 22 3 69.89 8.30 1 22 3 76.29 8.50 -1 22 -3 76.19 8.50 2 -22 3 1.60 1.00 2 -22 3 0.70 1.30 -2 -22 -3 1.30 1.60 -2 -22 -3 1.80 1.10 2 22 3 1.70 1.20 2 22 3 1.50 0.90 -2 22 -3 1.00 1.50 -3 -22 -3 2.20 1.80 3 -22 3 1.40 1.40 3 -22 3 1.40 1.20 -3 -22 -3 0.90 1.30 3 22 3 0.20 1.00 -3 22 -3 0.00 0.70 -3 22 -3 0.00 1.50 3 22 3 -1.40 1.30 4 -22 3 30.60 4.30 4 -22 3 26.50 4.40 -4 -22 -3 49.30 4.80 -4 -22 -3 33.80 4.40 -4 22 -3 41.10 4.60 -4 22 -3 33.80 4.10 4 22 3 35.60 4.20 4 22 3 44.20 4.50 5 -22 3 2.40 2.50 5 -22 3 1.30 2.40 5 22 3 1.30 1.60 -5 22 -3 -0.40 1.30 -5 22 -3 -2.20 2.30 5 22 3 0.70 2.20 -7 -23 3 1.10 1.60 7 -23 -3 1.70 2.50 7 23 -3 0.10 1.90 -7 23 3 -1.10 1.70 -6 -23 3 3.00 1.20 6 -23 -3 0.50 1.80 6 23 -3 1.30 1.60 -6 23 3 2.60 1.40 5 -23 -3 2.00 1.60 5 -23 -3 3.60 1.80 5 -23 -3 1.70 1.70 -5 -23 3 3.50 1.00 5 23 -3 4.00 1.50 -5 23 3 1.50 1.20 4 -23 -3 0.20 1.40 4 -23 -3 1.90 1.20 4 -23 -3 -0.40 1.30 -4 -23 3 0.00 0.70 -4 23 3 0.00 1.00 4 23 -3 0.50 1.10 4 23 -3 -0.50 1.10 3 -23 -3 13.50 2.20 3 -23 -3 12.60 2.00 -3 -23 3 17.50 2.00 3 -23 -3 13.20 2.00 3 23 -3 11.30 1.90 3 23 -3 15.20 2.00 -3 23 3 14.60 1.90 3 23 -3 14.50 2.00 -2 -23 3 171.68 17.70 2 -23 -3 159.38 17.70 2 -23 -3 167.48 17.70 2 23 -3 152.28 17.70 -2 23 3 161.08 17.60 -2 23 3 163.58 17.60 2 23 -3 168.28 17.70 2 23 -3 162.78 17.70 1 -23 -3 3.90 1.20 1 -23 -3 6.10 1.10 -1 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2.10 7 24 -3 6.10 2.30 -6 -24 3 15.20 1.90 6 -24 -3 7.10 2.30 -6 24 3 9.50 2.00 6 24 -3 12.80 2.20 -5 -24 3 8.60 1.50 5 -24 -3 11.70 2.20 5 -24 -3 13.80 2.20 5 -24 -3 10.00 2.00 -5 24 3 9.10 1.70 5 24 -3 9.60 1.90 4 -24 -3 9.20 1.70 4 -24 -3 13.40 2.00 -4 -24 3 11.10 1.40 4 -24 -3 9.20 2.00 -4 24 3 7.30 1.60 4 24 -3 12.10 1.80 4 24 -3 8.90 1.70 3 -24 -3 189.58 20.90 3 -24 -3 210.08 21.00 -3 -24 3 184.68 20.90 3 -24 -3 192.98 20.90 -3 24 3 195.18 20.90 3 24 -3 192.58 20.90 3 24 -3 177.78 20.90 3 24 -3 207.28 20.90 2 -24 -3 36.10 3.70 -2 -24 3 24.70 3.50 2 -24 -3 34.70 3.50 2 24 -3 27.00 3.40 -2 24 3 30.10 3.40 2 24 -3 27.20 3.50 -2 24 3 29.40 3.40 2 24 -3 28.20 3.50 1 -24 -3 50.69 5.80 1 -24 -3 50.39 5.90 -1 -24 3 51.09 5.80 -1 -24 3 51.59 5.80 -1 24 3 50.89 5.80 1 24 -3 54.49 5.70 1 24 -3 58.69 5.90 -1 24 3 52.49 5.70 1 24 -3 45.10 5.70 0 -24 -3 7.10 1.70 0 -24 -3 7.30 1.30 0 -24 3 7.60 1.00 0 -24 3 5.80 1.70 0 24 3 7.20 1.10 0 24 -3 3.20 1.50 0 24 3 9.90 1.40 1 -24 3 16.90 2.20 -1 -24 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25 -3 23.30 3.60 4 -25 3 3.40 2.20 -4 -25 -3 2.90 1.80 4 -25 3 4.10 1.90 4 25 3 2.30 1.70 -4 25 -3 1.60 0.90 -4 25 -3 1.90 2.30 4 25 3 1.10 1.20 5 -25 3 0.70 2.70 5 -25 3 1.00 2.60 -5 25 -3 1.20 1.30 -5 25 -3 -0.90 2.90 5 25 3 -0.40 2.30 5 25 3 0.30 1.60 7 -26 -3 -1.20 2.80 -7 -26 3 2.40 1.70 7 26 -3 -0.60 2.10 -7 26 3 -1.10 1.90 6 -26 -3 6.80 2.30 -6 -26 3 8.70 1.70 6 26 -3 11.80 2.10 -6 26 3 6.80 1.80 5 -26 -3 7.10 2.10 -5 -26 3 4.50 1.10 5 -26 -3 4.60 1.70 5 -26 -3 4.70 2.00 5 26 -3 5.10 1.60 -5 26 3 5.50 1.30 -4 -26 3 8.70 1.40 4 -26 -3 8.80 2.00 4 -26 -3 10.60 2.10 4 -26 -3 12.00 1.90 -4 26 3 11.10 1.60 4 26 -3 12.50 1.80 3 -26 -3 8.80 1.60 3 -26 -3 7.90 1.70 3 26 -3 11.80 2.00 -3 26 3 8.60 1.40 3 26 -3 5.20 1.40 3 26 -3 7.10 1.50 2 -26 -3 190.78 19.90 -2 -26 3 176.88 19.80 2 -26 -3 182.68 19.80 -2 -26 3 189.48 19.90 -2 26 3 174.08 19.80 2 26 -3 183.88 19.80 2 26 -3 197.58 19.90 2 26 -3 171.78 19.80 -2 26 3 187.38 19.90 -1 -26 3 80.79 9.40 -1 -26 3 87.29 9.50 1 -26 -3 82.29 9.40 1 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2.10 -4 -27 3 8.10 1.20 4 -27 -3 9.70 1.70 4 27 -3 8.20 1.60 -4 27 3 5.70 1.40 3 -27 -3 93.89 9.80 3 -27 -3 92.99 9.70 -3 27 3 82.99 9.60 3 27 -3 90.79 9.70 3 27 -3 82.69 9.60 -2 -27 3 142.29 15.30 2 -27 -3 141.19 15.20 -2 -27 3 154.78 15.30 2 -27 -3 145.49 15.30 2 27 -3 132.19 15.20 2 27 -3 136.59 15.30 -2 27 3 129.59 15.20 2 27 -3 147.19 15.20 1 -27 -3 7.80 1.80 -1 -27 3 9.00 2.00 1 -27 -3 7.40 1.60 1 27 -3 8.60 1.70 -1 27 3 9.30 1.60 1 27 -3 9.40 1.70 1 27 -3 12.10 1.60 -1 27 3 10.80 1.40 0 -27 -3 3.30 1.50 0 -27 3 3.10 0.80 0 -27 3 3.60 1.50 0 -27 -3 1.70 1.20 0 27 3 2.10 1.20 0 27 -3 3.20 1.50 0 27 3 3.00 0.80 -1 -27 -3 19.20 2.70 1 -27 3 23.10 3.10 1 -27 3 21.90 2.60 -1 -27 -3 18.90 3.00 1 27 3 22.90 2.80 -1 27 -3 20.70 3.00 1 27 3 22.90 2.60 2 -27 3 10.40 2.10 2 -27 3 10.30 1.70 -2 -27 -3 10.30 1.90 -2 -27 -3 9.90 2.20 -2 27 -3 13.60 2.20 2 27 3 10.00 1.50 2 27 3 11.80 2.00 -3 -27 -3 37.10 4.30 3 -27 3 32.50 4.20 3 -27 3 27.70 4.40 -3 -27 -3 44.40 4.70 -3 27 -3 35.20 4.50 3 27 3 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1.20 7 5 -4 1.50 1.60 7 5 -4 1.50 1.70 7 5 -4 1.20 0.90 6 -5 -4 1.50 1.00 -6 -5 4 0.10 1.30 6 -5 -4 0.10 1.20 -6 -5 4 -0.50 0.90 6 5 -4 0.90 1.20 -6 5 4 1.50 1.10 -6 5 4 0.60 1.00 6 5 -4 -0.90 0.70 6 5 -4 0.80 1.20 5 -5 -4 322.47 33.20 -5 -5 4 313.67 33.20 5 -5 -4 288.57 33.10 -5 -5 4 296.67 33.10 5 5 -4 321.77 33.20 -5 5 4 302.47 33.10 5 5 -4 303.27 33.10 -5 5 4 312.37 33.10 5 5 -4 311.07 33.20 -4 -5 4 17.90 2.10 4 -5 -4 17.70 2.20 4 -5 -4 15.70 2.00 -4 -5 4 15.80 1.90 4 -5 -4 17.60 2.00 4 5 -4 18.80 2.10 4 5 -4 17.80 2.10 -4 5 4 11.60 2.00 4 5 -4 15.90 1.90 -4 5 4 16.50 2.10 -4 5 4 19.20 2.00 3 -5 -4 9.80 1.30 3 -5 -4 10.80 1.30 3 -5 -4 7.50 1.10 3 -5 -4 7.20 1.20 -3 -5 4 8.60 1.20 -3 -5 4 7.90 1.00 -3 5 4 9.60 1.30 -3 5 4 8.70 1.20 3 5 -4 8.50 1.00 3 5 -4 8.80 1.10 3 5 -4 9.70 1.20 3 5 -4 5.10 1.10 -3 5 4 9.10 1.10 -2 -5 4 1.40 0.40 2 -5 -4 0.10 0.60 -2 -5 4 0.60 0.60 2 -5 -4 0.40 0.50 2 -5 -4 1.70 0.70 2 -5 -4 0.60 0.60 -2 5 4 1.30 0.70 -2 5 4 1.20 0.50 -2 5 4 1.50 0.70 2 5 -4 0.70 0.40 2 5 -4 1.20 0.50 2 5 -4 0.90 0.60 2 5 -4 -1.30 0.70 -1 -5 4 12.70 1.60 -1 -5 4 11.30 1.40 1 -5 -4 13.10 1.60 1 -5 -4 10.80 1.50 1 -5 -4 12.30 1.60 1 -5 -4 12.80 1.50 1 5 -4 11.30 1.40 -1 5 4 11.50 1.60 1 5 -4 11.50 1.60 -1 5 4 13.40 1.60 1 5 -4 13.80 1.50 -1 5 4 14.30 1.50 1 5 -4 10.50 1.60 0 -5 -4 397.26 43.10 0 -5 4 395.36 43.00 0 -5 -4 384.66 43.10 0 -5 -4 416.06 43.10 0 -5 -4 417.06 43.10 0 -5 4 379.56 43.10 0 -5 4 411.26 43.10 0 5 4 399.36 43.10 0 5 4 396.46 43.10 0 5 -4 394.76 43.00 0 5 -4 393.86 43.10 0 5 4 409.46 43.10 0 5 4 405.66 43.10 0 5 -4 400.36 43.10 1 -5 4 3.20 1.00 -1 -5 -4 3.30 1.10 1 -5 4 5.00 0.90 1 -5 4 1.80 1.10 -1 -5 -4 4.80 1.00 1 5 4 4.50 1.00 1 5 4 5.50 1.10 1 5 4 5.20 1.00 1 5 4 2.70 1.00 -1 5 -4 3.40 0.80 -1 5 -4 2.70 1.00 -1 5 -4 3.60 1.10 2 -5 4 25.70 3.30 -2 -5 -4 25.80 3.30 2 -5 4 25.30 3.30 2 -5 4 27.00 3.30 -2 -5 -4 31.80 3.50 2 5 4 22.10 3.30 2 5 4 32.90 3.30 -2 5 -4 28.80 3.50 -2 5 -4 34.60 3.30 2 5 4 29.50 3.40 2 5 4 27.20 3.30 -3 -5 -4 0.50 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27.00 3.50 -4 -6 4 30.70 3.40 4 -6 -4 26.50 3.40 4 6 -4 30.90 3.40 4 6 -4 29.70 3.50 -4 6 4 31.90 3.40 -4 6 4 33.40 3.40 -4 6 4 31.90 3.50 4 6 -4 30.30 3.50 4 6 -4 31.50 3.30 3 -6 -4 126.09 14.70 -3 -6 4 124.59 14.70 3 -6 -4 140.49 14.70 3 -6 -4 138.69 14.70 3 -6 -4 135.79 14.60 -3 -6 4 138.09 14.60 -3 6 4 142.69 14.60 3 6 -4 129.79 14.70 3 6 -4 134.49 14.70 3 6 -4 141.29 14.60 3 6 -4 129.19 14.60 3 6 -4 142.19 14.60 -3 6 4 142.99 14.70 -3 6 4 126.99 14.70 2 -6 -4 248.28 25.60 2 -6 -4 227.98 25.60 2 -6 -4 241.38 25.60 -2 -6 4 232.08 25.60 2 -6 -4 228.78 25.60 -2 -6 4 231.78 25.60 -2 -6 4 231.48 25.50 2 6 -4 240.68 25.50 -2 6 4 244.88 25.60 2 6 -4 223.58 25.60 -2 6 4 247.08 25.60 -2 6 4 236.88 25.60 2 6 -4 252.17 25.60 -1 -6 4 29.50 3.40 1 -6 -4 29.90 3.40 1 -6 -4 28.50 3.30 1 -6 -4 31.00 3.40 -1 -6 4 31.70 3.30 1 -6 -4 25.20 3.30 1 6 -4 30.30 3.30 1 6 -4 26.50 3.40 1 6 -4 32.10 3.30 -1 6 4 26.30 3.40 -1 6 4 31.30 3.40 -1 6 4 32.20 3.40 1 6 -4 30.40 3.40 0 -6 -4 345.17 36.70 0 -6 -4 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9.00 2.30 9 -7 -4 0.50 2.20 9 -7 -4 -1.50 2.40 9 7 -4 1.30 1.50 9 7 -4 0.40 2.70 8 -7 -4 0.30 1.60 -8 -7 4 2.10 2.20 8 -7 -4 1.50 1.90 -8 -7 4 0.10 1.50 8 7 -4 1.90 2.10 8 7 -4 0.40 1.10 8 7 -4 -1.10 1.90 -7 -7 4 32.10 3.60 -7 -7 4 35.50 3.90 7 -7 -4 25.80 3.60 7 -7 -4 38.80 3.90 7 7 -4 30.70 3.80 7 7 -4 25.80 3.70 7 7 -4 25.90 3.40 -6 -7 4 0.20 1.40 6 -7 -4 -1.00 1.00 -6 -7 4 1.50 0.90 6 -7 -4 -0.70 1.20 6 7 -4 0.60 1.30 -6 7 4 1.00 1.00 6 7 -4 0.00 1.30 -6 7 4 1.10 1.10 6 7 -4 0.10 0.70 5 -7 -4 7.20 1.30 5 -7 -4 8.10 1.40 -5 -7 4 8.10 1.20 -5 -7 4 9.40 1.50 -5 7 4 8.10 1.50 -5 7 4 7.90 1.30 5 7 -4 8.70 1.50 5 7 -4 7.80 1.00 5 7 -4 6.40 1.40 -5 7 4 7.00 1.20 4 -7 -4 -0.50 0.70 4 -7 -4 0.30 0.70 -4 -7 4 -0.70 0.80 4 -7 -4 -0.30 0.80 4 7 -4 0.10 0.50 -4 7 4 -0.10 0.70 -4 7 4 -0.10 0.90 4 7 -4 0.00 0.70 4 7 -4 0.30 0.40 4 7 -4 0.00 0.80 -4 7 4 0.60 0.60 3 -7 -4 179.88 19.20 -3 -7 4 165.68 19.20 3 -7 -4 177.48 19.20 3 -7 -4 173.38 19.20 3 -7 -4 188.08 19.20 -3 -7 4 172.48 19.10 -3 7 4 172.58 19.20 -3 7 4 181.08 19.20 3 7 -4 183.58 19.20 3 7 -4 172.48 19.20 3 7 -4 181.08 19.10 3 7 -4 172.98 19.10 -3 7 4 187.98 19.20 3 7 -4 177.18 19.20 2 -7 -4 28.20 2.80 -2 -7 4 23.10 2.60 2 -7 -4 19.70 2.70 2 -7 -4 21.00 2.80 -2 -7 4 24.20 2.70 -2 -7 4 20.90 2.70 2 -7 -4 23.10 2.70 -2 7 4 27.40 2.70 -2 7 4 22.80 2.80 -2 7 4 26.90 2.80 2 7 -4 23.90 2.60 2 7 -4 25.50 2.60 2 7 -4 22.10 2.70 2 7 -4 21.50 2.80 -1 -7 4 79.99 8.50 1 -7 -4 73.89 8.50 -1 -7 4 79.59 8.50 1 -7 -4 73.39 8.50 1 -7 -4 77.19 8.60 -1 -7 4 71.79 8.50 1 -7 -4 80.19 8.50 -1 7 4 81.99 8.50 -1 7 4 78.59 8.60 1 7 -4 70.29 8.50 1 7 -4 74.89 8.60 1 7 -4 84.99 8.50 1 7 -4 81.49 8.50 -1 7 4 81.49 8.50 0 -7 4 146.49 16.00 0 -7 4 133.69 16.00 0 -7 4 151.68 16.10 0 -7 -4 153.68 16.00 0 -7 -4 135.89 16.00 0 -7 -4 152.08 16.00 0 -7 -4 150.08 16.10 0 7 4 147.99 16.00 0 7 4 156.48 16.00 0 7 4 154.18 16.00 0 7 4 139.09 16.00 0 7 -4 146.49 16.10 0 7 -4 149.59 16.00 0 7 -4 149.39 16.00 0 7 -4 152.98 16.00 1 -7 4 48.40 5.20 1 -7 4 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43.00 4.80 -5 24 4 34.40 4.50 5 24 -4 34.90 4.60 5 24 -4 39.10 4.60 -4 -24 4 36.20 4.00 4 -24 -4 31.30 4.30 4 -24 -4 40.20 4.20 4 24 -4 32.10 4.20 -4 24 4 35.50 4.20 4 24 -4 35.90 4.20 3 -24 -4 0.40 1.50 -3 -24 4 1.30 1.30 3 -24 -4 2.30 1.30 3 24 -4 -1.10 1.10 -3 24 4 1.40 1.10 3 24 -4 1.90 1.20 -2 -24 4 128.79 13.00 2 -24 -4 124.39 13.10 2 -24 -4 119.89 13.00 2 24 -4 120.19 13.10 2 24 -4 106.79 13.00 -2 24 4 122.49 13.00 -2 24 4 108.99 13.00 2 24 -4 124.59 13.00 -1 -24 4 1.50 1.40 -1 -24 4 1.60 1.10 1 -24 -4 1.70 1.30 -1 -24 4 1.00 0.60 1 -24 -4 2.60 1.20 1 24 -4 0.40 1.20 1 24 -4 0.80 1.10 -1 24 4 0.90 0.90 -1 24 4 0.30 1.10 0 -24 4 85.09 9.80 0 -24 4 82.79 9.50 0 -24 -4 87.39 9.70 0 -24 -4 90.09 9.80 0 24 -4 102.09 9.80 0 24 -4 82.89 9.80 0 24 4 96.89 9.70 0 24 4 84.49 9.60 1 -24 4 19.90 2.30 -1 -24 -4 19.60 2.80 1 -24 4 21.80 2.80 -1 -24 -4 15.30 2.50 1 24 4 14.40 2.30 -1 24 -4 18.70 2.70 1 24 4 22.00 2.60 2 -24 4 7.90 2.20 -2 -24 -4 18.00 2.60 2 -24 4 12.30 1.90 -2 -24 -4 11.30 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25 4 87.69 9.50 1 25 -4 88.29 9.70 1 25 -4 84.59 9.60 -1 25 4 80.49 9.60 0 -25 -4 41.00 4.70 0 -25 -4 39.10 4.80 0 -25 4 35.90 4.40 0 -25 4 40.00 4.80 0 25 4 41.10 4.50 0 25 4 41.80 4.60 0 25 -4 39.40 4.70 -1 -25 -4 0.60 1.30 -1 -25 -4 0.30 1.60 1 -25 4 0.70 1.90 1 -25 4 1.50 1.00 1 25 4 0.80 0.90 -1 25 -4 0.90 1.70 1 25 4 0.70 1.30 -2 -25 -4 10.60 2.00 -2 -25 -4 4.50 2.00 2 -25 4 9.40 1.60 2 -25 4 7.60 2.10 2 25 4 7.60 1.80 -2 25 -4 9.00 2.00 2 25 4 9.40 1.50 3 -25 4 4.20 1.70 -3 -25 -4 4.40 2.50 3 -25 4 1.00 2.20 3 25 4 4.10 1.40 3 25 4 4.60 1.90 -3 25 -4 5.00 2.30 4 -25 4 3.70 2.20 4 -25 4 -0.70 2.40 -4 25 -4 3.40 2.60 4 25 4 1.40 1.60 4 25 4 2.10 2.30 7 -26 -4 21.60 3.80 -7 -26 4 20.20 2.80 7 26 -4 21.60 3.20 -7 26 4 14.30 3.00 -6 -26 4 8.50 1.50 6 -26 -4 8.70 2.50 6 26 -4 7.10 2.00 -6 26 4 3.90 1.70 5 -26 -4 0.90 2.00 -5 -26 4 1.90 1.00 5 -26 -4 2.90 1.90 -5 26 4 3.00 1.40 5 26 -4 4.40 1.50 -4 -26 4 36.90 4.20 4 -26 -4 43.20 4.60 4 -26 -4 36.70 4.70 -4 26 4 36.30 4.50 4 26 -4 40.40 4.50 4 26 -4 37.80 4.60 -3 -26 4 52.29 5.60 3 -26 -4 47.20 5.60 3 -26 -4 41.50 5.70 -3 26 4 49.40 5.40 3 26 -4 47.10 5.50 3 26 -4 46.80 5.50 2 -26 -4 12.10 2.10 -2 -26 4 14.80 2.20 2 -26 -4 15.90 2.40 -2 -26 4 12.80 2.40 2 26 -4 14.00 2.10 -2 26 4 15.30 2.10 2 26 -4 16.60 2.30 2 26 -4 12.30 2.10 -2 26 4 14.60 1.90 -1 -26 4 0.20 0.60 1 -26 -4 1.20 1.30 -1 -26 4 0.90 1.50 1 -26 -4 1.10 1.40 -1 26 4 1.40 1.00 1 26 -4 0.30 1.40 -1 26 4 -0.50 1.10 1 26 -4 -0.30 1.30 0 -26 4 37.80 4.30 0 -26 4 40.50 4.70 0 -26 -4 38.80 4.60 0 -26 -4 41.20 4.70 0 26 4 34.00 4.40 0 26 -4 39.60 4.60 0 26 4 39.20 4.50 1 -26 4 7.10 2.00 -1 -26 -4 3.10 1.50 1 -26 4 6.30 1.20 -1 -26 -4 2.50 1.90 -1 26 -4 6.30 2.00 1 26 4 4.90 1.50 1 26 4 3.60 1.10 2 -26 4 48.60 5.00 -2 -26 -4 50.09 5.40 2 -26 4 29.50 5.10 -2 -26 -4 51.19 5.30 2 26 4 49.10 4.90 2 26 4 34.90 5.10 -2 26 -4 39.40 5.20 3 -26 4 6.20 1.90 -3 -26 -4 10.10 2.70 3 -26 4 2.60 2.10 3 26 4 9.00 2.30 -3 26 -4 9.30 2.70 3 26 4 6.70 1.60 4 -26 4 14.70 3.30 4 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1.10 2.30 9 -7 -5 -2.00 2.10 -9 -7 5 -0.50 2.70 9 -7 -5 0.90 2.90 9 7 -5 -0.90 2.40 9 7 -5 1.10 2.50 9 7 -5 1.80 1.40 8 -7 -5 33.50 3.50 8 -7 -5 26.90 3.70 -8 -7 5 29.00 3.70 8 7 -5 21.60 3.10 8 7 -5 22.90 3.60 8 7 -5 29.80 3.70 7 -7 -5 18.40 2.30 -7 -7 5 16.60 2.60 7 -7 -5 15.50 2.50 7 7 -5 15.40 2.00 7 7 -5 15.30 2.50 7 7 -5 17.90 2.60 6 -7 -5 115.39 12.00 -6 -7 5 115.69 11.90 6 -7 -5 104.59 11.90 -6 -7 5 108.49 12.00 6 7 -5 112.39 12.00 6 7 -5 104.59 12.00 -6 7 5 104.89 11.90 -6 7 5 118.79 12.00 6 7 -5 104.29 11.80 -5 -7 5 89.99 10.00 5 -7 -5 93.79 9.90 5 -7 -5 88.09 10.00 -5 -7 5 91.79 9.90 5 7 -5 84.79 10.00 -5 7 5 93.09 10.00 -5 7 5 89.69 10.00 5 7 -5 92.79 9.90 5 7 -5 93.69 10.00 -4 -7 5 10.30 1.20 4 -7 -5 7.30 1.40 4 -7 -5 8.20 1.30 4 -7 -5 8.20 1.50 -4 -7 5 6.40 1.40 -4 7 5 9.30 1.30 4 7 -5 10.50 1.10 -4 7 5 6.40 1.40 4 7 -5 11.40 1.60 -3 -7 5 4.80 1.10 3 -7 -5 4.70 1.00 3 -7 -5 3.70 0.90 3 -7 -5 5.00 1.10 -3 -7 5 4.40 0.80 3 7 -5 7.30 1.20 -3 7 5 6.30 1.10 -3 7 5 4.00 1.00 3 7 -5 4.00 1.10 3 7 -5 6.60 0.70 3 7 -5 6.50 0.80 -3 7 5 5.40 1.20 2 -7 -5 28.50 2.70 -2 -7 5 17.60 2.40 -2 -7 5 14.90 2.50 2 -7 -5 19.90 2.50 2 -7 -5 23.20 2.50 2 7 -5 21.10 2.30 -2 7 5 23.70 2.50 2 7 -5 20.00 2.30 -2 7 5 20.20 2.40 2 7 -5 22.10 2.60 -2 7 5 18.60 2.50 2 7 -5 23.30 2.60 -1 -7 5 11.50 1.70 -1 -7 5 16.10 1.70 1 -7 -5 15.10 1.80 1 -7 -5 9.40 1.60 1 -7 -5 11.80 1.90 -1 7 5 11.20 1.80 1 7 -5 12.80 1.80 1 7 -5 13.70 1.80 1 7 -5 13.60 1.60 -1 7 5 16.80 1.80 -1 7 5 12.00 1.80 0 -7 5 2.90 1.20 0 -7 5 0.90 0.80 0 -7 5 -0.50 0.90 0 -7 -5 1.60 1.00 0 -7 -5 1.30 0.90 0 -7 -5 1.80 1.10 0 7 -5 1.40 0.70 0 7 5 2.30 1.00 0 7 -5 0.40 1.00 0 7 5 1.70 1.10 0 7 -5 1.20 1.00 0 7 5 1.40 1.00 0 7 5 1.00 1.00 1 -7 5 205.08 24.00 1 -7 5 210.98 23.90 -1 -7 -5 234.58 23.90 1 -7 5 205.38 23.90 -1 -7 -5 222.78 24.00 -1 7 -5 240.78 24.00 1 7 5 232.68 24.00 1 7 5 221.88 23.90 -1 7 -5 221.48 23.90 -2 -7 -5 2.40 1.50 -2 -7 -5 3.60 1.50 2 -7 5 4.40 1.20 2 -7 5 2.20 1.40 2 -7 5 1.80 1.30 2 7 5 3.20 1.40 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5.80 1.10 -4 8 5 4.30 1.60 -4 8 5 5.10 1.10 4 8 -5 5.80 0.70 4 8 -5 4.80 0.70 4 8 -5 5.20 1.20 3 -8 -5 22.80 2.80 -3 -8 5 22.50 2.80 -3 -8 5 22.20 2.60 3 -8 -5 23.00 2.70 3 -8 -5 24.20 2.80 3 8 -5 23.00 2.80 -3 8 5 24.00 2.70 3 8 -5 21.80 2.50 3 8 -5 23.40 2.80 -3 8 5 23.10 2.80 -3 8 5 29.90 2.80 2 -8 -5 15.90 1.80 2 -8 -5 12.00 1.80 2 -8 -5 11.30 1.70 -2 -8 5 14.20 1.60 -2 -8 5 11.30 1.80 -2 8 5 10.60 1.80 -2 8 5 15.90 1.80 2 8 -5 13.80 1.90 2 8 -5 17.10 1.90 2 8 -5 10.90 1.50 -2 8 5 14.00 1.70 2 8 -5 14.10 1.50 -1 -8 5 5.50 1.20 1 -8 -5 4.30 1.00 -1 -8 5 6.90 1.00 1 -8 -5 5.90 1.30 1 -8 -5 5.30 1.10 -1 8 5 8.70 1.30 1 8 -5 4.70 1.20 1 8 -5 6.90 1.20 -1 8 5 2.70 1.10 -1 8 5 6.90 1.30 1 8 -5 6.30 0.80 0 -8 5 1.70 1.20 0 -8 -5 1.40 1.00 0 -8 -5 0.60 1.10 0 -8 5 2.50 0.90 0 -8 5 2.30 1.00 0 -8 -5 1.60 0.90 0 8 5 1.60 1.00 0 8 5 1.90 1.00 0 8 -5 0.80 1.00 0 8 -5 2.40 0.70 0 8 5 1.10 1.10 0 8 5 1.70 1.00 0 8 -5 1.80 1.20 1 -8 5 45.00 5.30 1 -8 5 39.60 5.30 -1 -8 -5 47.90 5.40 -1 8 -5 51.79 5.20 2 -8 5 7.70 1.60 -2 -8 -5 12.20 1.90 2 -8 5 9.30 1.90 -2 -8 -5 7.20 1.90 2 8 5 9.00 1.80 -2 8 -5 9.70 1.60 -2 8 -5 11.90 2.00 -3 -8 -5 0.50 1.90 3 -8 5 -1.10 1.60 3 -8 5 1.10 1.50 -3 -8 -5 0.90 1.80 -3 8 -5 2.90 2.00 3 8 5 1.20 1.50 -3 8 -5 0.60 1.30 4 -8 5 6.80 2.10 -4 -8 -5 5.90 2.30 -4 8 -5 5.40 2.50 4 8 5 4.10 2.00 -4 8 -5 6.00 1.90 9 -9 -5 16.90 3.20 -9 -9 5 15.80 3.20 9 -9 -5 12.90 2.70 9 9 -5 7.00 3.10 9 9 -5 10.90 1.90 9 9 -5 15.80 3.10 -8 -9 5 7.70 1.80 8 -9 -5 6.30 2.30 8 -9 -5 3.80 1.70 -8 -9 5 4.90 2.20 8 9 -5 3.50 1.10 8 9 -5 3.80 1.90 8 9 -5 3.40 2.00 -7 -9 5 -0.80 1.60 -7 -9 5 0.70 1.20 7 -9 -5 -0.50 1.30 7 -9 -5 0.50 1.60 7 9 -5 1.30 0.80 7 9 -5 0.10 1.50 7 9 -5 -0.20 1.50 -6 -9 5 8.10 1.70 6 -9 -5 5.20 1.30 6 -9 -5 5.20 1.70 6 9 -5 3.30 1.50 -6 9 5 2.70 1.40 6 9 -5 7.40 0.90 6 9 -5 5.10 1.60 5 -9 -5 52.09 5.60 -5 -9 5 45.20 5.60 5 -9 -5 48.40 5.50 -5 -9 5 49.40 5.40 5 9 -5 49.50 5.30 -5 9 5 45.80 5.50 5 9 -5 52.59 5.60 5 9 -5 47.90 5.50 -5 9 5 48.80 5.50 4 -9 -5 0.30 0.90 4 -9 -5 1.40 1.00 -4 -9 5 0.90 1.00 -4 -9 5 3.00 0.60 4 -9 -5 1.00 0.80 -4 9 5 0.80 0.90 4 9 -5 1.70 1.00 -4 9 5 0.00 1.10 4 9 -5 1.30 1.00 -4 9 5 1.60 0.80 -3 -9 5 1.60 0.60 3 -9 -5 1.10 0.80 3 -9 -5 1.70 0.90 3 -9 -5 0.10 0.90 -3 -9 5 1.70 0.90 -3 9 5 1.90 1.00 3 9 -5 1.30 0.90 3 9 -5 0.50 0.90 -3 9 5 1.20 0.90 -3 9 5 1.60 0.80 2 -9 -5 2.70 0.90 2 -9 -5 1.50 1.00 -2 -9 5 3.00 0.60 2 -9 -5 1.30 0.80 -2 -9 5 1.40 0.90 2 9 -5 3.00 1.00 2 9 -5 1.20 0.90 -2 9 5 2.00 0.90 -2 9 5 3.60 1.00 -2 9 5 1.90 0.80 -1 -9 5 13.60 1.80 1 -9 -5 18.90 2.10 -1 -9 5 10.90 1.90 1 -9 -5 13.30 1.90 1 -9 -5 18.70 2.00 1 9 -5 14.80 1.70 -1 9 5 15.40 1.90 1 9 -5 10.60 2.00 -1 9 5 18.30 2.10 1 9 -5 14.30 1.70 -1 9 5 13.00 2.00 1 9 -5 18.90 2.00 0 -9 -5 5.30 1.10 0 -9 5 6.20 1.00 0 -9 5 4.30 1.40 0 -9 -5 3.90 1.10 0 -9 5 3.20 1.10 0 -9 -5 3.80 1.30 0 9 -5 4.00 0.80 0 9 -5 4.20 1.20 0 9 5 3.90 1.20 0 9 -5 2.90 1.20 0 9 5 4.50 1.10 0 9 5 2.70 1.10 0 9 5 2.70 1.10 1 -9 5 275.27 30.50 -1 -9 -5 303.07 30.60 1 -9 5 256.67 30.60 -1 -9 -5 294.87 30.60 1 -9 5 286.77 30.60 -1 9 -5 296.27 30.60 1 9 5 276.17 30.60 -1 9 -5 279.47 30.50 1 9 5 287.97 30.60 2 -9 5 0.10 1.40 -2 -9 -5 0.80 1.50 -2 -9 -5 0.60 1.50 2 -9 5 0.60 1.20 -2 9 -5 -0.20 1.00 -2 9 -5 0.00 1.60 2 9 5 0.70 1.30 3 -9 5 2.40 1.70 -3 -9 -5 2.70 3.10 -3 -9 -5 2.10 2.00 3 -9 5 1.00 1.50 3 9 5 -0.10 1.50 -3 9 -5 1.90 1.30 -3 9 -5 0.20 1.70 4 -9 5 7.00 2.40 -4 -9 -5 12.00 2.80 4 9 5 4.30 2.00 -4 9 -5 7.80 1.90 -4 9 -5 6.00 2.30 -9 -10 5 7.80 3.10 -9 -10 5 8.50 2.50 9 -10 -5 10.40 2.60 9 10 -5 8.20 2.90 9 10 -5 6.50 1.50 8 -10 -5 41.70 4.90 8 -10 -5 36.60 4.50 -8 -10 5 43.80 4.80 -8 -10 5 36.60 4.40 8 10 -5 36.60 4.60 8 10 -5 31.00 4.10 8 10 -5 38.30 4.70 -7 -10 5 21.70 2.60 7 -10 -5 13.80 2.60 7 -10 -5 14.60 2.80 -7 -10 5 23.00 3.00 7 10 -5 19.90 2.30 7 10 -5 26.70 3.00 7 10 -5 20.00 2.90 6 -10 -5 0.30 1.20 6 -10 -5 -0.80 1.30 -6 -10 5 -0.50 1.40 6 10 -5 0.60 0.50 -6 10 5 1.10 1.30 6 10 -5 0.60 1.30 6 10 -5 -1.50 1.30 -5 -10 5 19.90 2.60 5 -10 -5 23.30 2.60 5 -10 -5 16.30 2.50 -5 -10 5 19.10 2.30 5 10 -5 24.30 2.60 -5 10 5 20.40 2.50 5 10 -5 17.20 2.60 -5 10 5 19.10 2.50 4 -10 -5 74.09 7.20 -4 -10 5 63.69 7.10 -4 -10 5 69.49 7.20 4 -10 -5 62.39 7.20 4 -10 -5 59.69 7.20 -4 10 5 61.39 7.20 -4 10 5 65.39 7.20 -4 10 5 59.79 7.20 4 10 -5 70.19 7.20 4 10 -5 66.19 7.20 3 -10 -5 36.10 3.90 -3 -10 5 36.40 3.90 -3 -10 5 33.40 3.70 3 -10 -5 30.20 3.80 3 -10 -5 33.30 3.80 3 10 -5 35.20 3.80 -3 10 5 36.70 3.90 3 10 -5 29.60 3.80 -3 10 5 33.00 3.90 -3 10 5 31.90 3.90 -2 -10 5 16.30 2.10 2 -10 -5 15.60 2.00 -2 -10 5 18.70 2.00 2 -10 -5 16.30 2.10 2 -10 -5 17.00 2.20 -2 10 5 16.90 2.10 -2 10 5 15.20 2.10 2 10 -5 14.60 2.20 -2 10 5 15.10 2.10 2 10 -5 16.20 2.10 -1 -10 5 3.50 0.90 1 -10 -5 4.10 1.20 1 -10 -5 6.20 1.10 -1 -10 5 6.20 1.20 1 -10 -5 8.20 1.50 1 10 -5 6.90 0.80 1 10 -5 7.20 1.40 1 10 -5 6.40 1.40 1 10 -5 6.80 0.80 -1 10 5 6.60 1.20 -1 10 5 4.30 1.20 -1 10 5 11.10 1.40 0 -10 5 12.90 1.90 0 -10 -5 10.70 1.80 0 -10 5 11.80 2.10 0 -10 5 11.80 1.80 0 -10 -5 13.70 2.10 0 10 5 15.10 2.00 0 10 5 20.00 2.30 0 10 -5 15.90 2.10 0 10 5 10.70 1.80 0 10 -5 14.60 2.00 0 10 -5 14.10 1.60 1 -10 5 15.20 2.50 1 -10 5 14.70 2.30 1 -10 5 13.40 2.10 -1 10 -5 21.50 2.60 -1 10 -5 21.40 2.20 -2 -10 -5 0.90 1.50 -2 -10 -5 1.00 1.60 2 -10 5 -1.60 1.40 2 -10 5 0.20 1.20 -2 10 -5 0.00 1.50 -2 10 -5 1.20 1.00 2 10 5 -0.20 1.20 2 10 5 0.40 1.30 3 -10 5 -0.50 1.50 -3 -10 -5 1.60 1.80 3 -10 5 2.30 1.60 -3 10 -5 1.20 1.70 -3 10 -5 2.40 1.30 3 10 5 2.70 1.50 4 -10 5 2.40 2.00 -4 -10 -5 0.70 2.20 4 10 5 3.50 1.90 -4 10 -5 1.60 1.70 -4 10 -5 -0.50 2.10 -8 -11 5 -1.70 2.10 8 -11 -5 -1.00 2.30 8 -11 -5 0.90 1.70 -8 -11 5 2.00 1.70 8 11 -5 1.40 0.90 8 11 -5 0.40 2.00 8 11 -5 3.10 2.10 7 -11 -5 4.10 1.80 -7 -11 5 4.30 1.40 7 -11 -5 8.00 1.70 -7 -11 5 3.20 1.90 7 11 -5 4.00 1.70 7 11 -5 5.20 1.70 7 11 -5 6.50 1.00 -6 -11 5 22.50 2.50 6 -11 -5 20.80 2.80 6 -11 -5 21.80 2.60 -6 -11 5 20.70 2.80 6 11 -5 19.10 2.70 6 11 -5 17.90 2.20 6 11 -5 26.50 2.90 5 -11 -5 51.29 5.90 5 -11 -5 46.60 5.90 -5 -11 5 59.39 6.00 -5 -11 5 51.79 5.80 -5 11 5 53.99 5.90 5 11 -5 53.29 6.00 5 11 -5 55.99 6.00 4 -11 -5 23.80 3.10 -4 -11 5 28.70 3.20 4 -11 -5 25.20 3.10 -4 -11 5 26.30 2.90 4 -11 -5 22.70 3.10 4 11 -5 25.80 3.20 -4 11 5 24.00 3.20 -4 11 5 28.60 3.10 -4 11 5 24.10 3.10 4 11 -5 31.70 3.20 -3 -11 5 5.60 1.20 3 -11 -5 5.20 1.10 -3 -11 5 4.30 0.80 3 -11 -5 4.00 1.10 3 -11 -5 4.10 1.10 -3 11 5 6.60 1.10 3 11 -5 4.40 1.10 -3 11 5 5.60 1.30 -3 11 5 6.10 1.20 3 11 -5 7.60 1.20 -2 -11 5 34.10 4.30 2 -11 -5 37.40 4.30 2 -11 -5 40.40 4.40 -2 -11 5 39.70 4.20 2 -11 -5 36.50 4.30 2 11 -5 33.10 4.30 -2 11 5 41.60 4.30 -2 11 5 39.50 4.30 -2 11 5 33.00 4.30 2 11 -5 42.50 4.30 -1 -11 5 5.00 0.90 -1 -11 5 7.20 1.20 1 -11 -5 4.90 1.10 1 -11 -5 4.90 1.20 1 -11 -5 7.60 1.40 -1 11 5 7.00 1.20 1 11 -5 5.80 1.20 -1 11 5 3.50 1.20 1 11 -5 6.40 1.30 -1 11 5 10.00 1.30 0 -11 -5 0.20 1.20 0 -11 5 1.10 0.80 0 -11 -5 0.80 0.90 0 -11 5 -0.20 0.90 0 -11 5 0.10 1.30 0 11 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-9 -9 11.60 2.10 5 -9 -9 11.70 2.70 -5 -9 9 9.10 1.90 -5 -9 9 8.10 2.50 -5 9 9 6.90 2.50 5 9 -9 9.80 2.60 -4 -9 9 3.00 1.70 4 -9 -9 4.20 1.70 -4 -9 9 3.70 2.30 4 9 -9 1.90 2.40 -4 9 9 2.10 2.40 -3 -9 9 -0.30 2.20 3 -9 -9 1.20 1.80 3 -9 -9 -0.10 2.20 -3 -9 9 2.20 1.90 -3 9 9 1.00 2.30 3 9 -9 -0.40 2.00 -2 -9 9 0.60 2.30 -2 -9 9 2.20 2.00 2 -9 -9 -0.70 1.90 2 -9 -9 1.60 2.80 -2 -9 9 -0.60 2.70 2 9 -9 -1.80 2.50 2 9 -9 1.40 2.40 -2 9 9 0.30 2.40 -1 -9 9 0.30 2.40 -1 -9 9 -4.00 3.70 -1 -9 9 0.00 2.70 1 -9 -9 1.40 3.10 1 -9 -9 -1.10 2.30 -1 9 9 0.70 2.50 1 9 -9 0.90 2.90 1 9 -9 2.20 1.40 1 9 -9 2.30 3.10 -6 -10 9 0.30 1.60 6 -10 -9 0.90 1.80 6 -10 -9 -1.40 2.30 -6 -10 9 0.90 2.50 6 10 -9 -0.40 2.50 -6 10 9 -2.40 2.30 5 -10 -9 3.30 1.70 -5 -10 9 6.90 2.30 -5 -10 9 4.70 1.60 -5 10 9 3.20 2.20 5 10 -9 3.70 2.70 4 -10 -9 2.50 1.70 -4 -10 9 1.90 1.60 -4 -10 9 -1.20 2.20 -4 10 9 0.90 2.30 4 10 -9 0.00 2.30 -3 -10 9 0.00 1.60 -3 -10 9 -0.40 2.20 3 -10 -9 0.30 2.70 3 -10 -9 2.20 1.90 -3 10 9 2.90 2.30 3 10 -9 1.60 2.40 2 -10 -9 0.10 2.00 -2 -10 9 -2.60 2.00 2 -10 -9 -0.70 2.80 -2 -10 9 1.20 2.30 -2 -10 9 1.50 2.80 -2 10 9 -1.50 2.40 2 10 -9 1.90 2.40 2 10 -9 -2.50 2.20 1 -10 -9 3.60 2.40 1 -10 -9 6.20 3.20 -1 -10 9 5.60 2.90 -1 -10 9 3.00 2.50 -1 -10 9 1.60 3.30 1 10 -9 6.00 3.00 6 -11 -9 7.50 2.20 -6 -11 9 6.40 2.00 -6 -11 9 7.20 2.60 6 -11 -9 13.00 3.00 6 11 -9 10.80 3.00 -6 11 9 7.70 2.70 5 -11 -9 15.30 2.30 -5 -11 9 13.50 2.70 -5 -11 9 9.70 2.10 5 11 -9 14.80 3.00 -5 11 9 11.20 2.70 -4 -11 9 1.90 1.70 4 -11 -9 -0.70 1.70 -4 -11 9 4.60 2.20 4 11 -9 2.30 2.20 -4 11 9 4.20 2.40 -3 -11 9 1.70 2.40 3 -11 -9 4.10 2.40 -3 -11 9 4.80 1.80 3 -11 -9 1.40 1.90 -3 11 9 2.80 2.30 3 11 -9 3.30 2.50 -2 -11 9 1.40 2.30 2 -11 -9 -2.10 2.50 -2 -11 9 3.80 2.10 -2 -11 9 1.40 3.20 2 -11 -9 0.10 2.10 -2 11 9 0.40 2.40 2 11 -9 2.00 2.50 2 11 -9 0.40 2.60 6 -12 -9 1.20 2.00 -6 -12 9 3.30 1.70 -6 -12 9 2.20 2.40 6 12 -9 3.50 2.60 -6 12 9 0.00 2.50 -5 -12 9 21.60 3.50 5 -12 -9 21.90 3.00 -5 -12 9 17.70 2.90 5 12 -9 25.60 3.80 -5 12 9 20.30 3.50 4 -12 -9 21.90 4.00 -4 -12 9 10.80 2.20 -4 -12 9 13.10 2.90 4 -12 -9 12.30 2.30 4 12 -9 7.70 2.90 -4 12 9 13.90 2.90 -3 -12 9 18.10 3.40 3 -12 -9 18.30 3.10 3 -12 -9 31.90 4.00 -3 -12 9 17.10 2.90 3 12 -9 26.00 3.70 -3 12 9 22.90 3.50 2 -12 -9 0.50 2.20 2 -12 -9 3.90 2.70 -2 -12 9 1.00 2.00 -2 -12 9 -0.10 2.40 -2 -12 9 7.40 3.40 2 12 -9 6.70 2.70 -2 12 9 5.00 2.60 2 12 -9 3.00 2.50 -6 -13 9 -1.10 2.50 -6 -13 9 0.60 1.60 6 -13 -9 0.50 2.00 6 13 -9 0.80 2.50 -6 13 9 1.20 2.40 5 -13 -9 3.60 1.90 -5 -13 9 3.10 1.60 -5 -13 9 7.30 2.60 -5 13 9 4.60 2.60 5 13 -9 5.60 2.70 4 -13 -9 4.10 2.70 -4 -13 9 3.30 1.70 -4 -13 9 7.40 2.50 4 -13 -9 4.50 2.00 4 13 -9 2.40 2.30 -4 13 9 2.30 2.50 -3 -13 9 6.10 2.00 3 -13 -9 7.10 2.10 -3 -13 9 8.50 2.60 3 -13 -9 13.60 3.20 3 13 -9 6.60 2.60 -3 13 9 9.10 2.70 2 -13 -9 0.40 3.00 -2 -13 9 0.70 3.40 -2 -13 9 2.50 2.50 2 -13 -9 2.50 2.20 -2 -13 9 0.30 2.00 2 13 -9 1.80 2.80 2 13 -9 2.00 2.60 -2 13 9 1.80 2.60 -6 -14 9 2.70 2.50 6 -14 -9 2.00 2.20 -6 -14 9 2.10 1.70 6 14 -9 0.60 3.10 -6 14 9 2.20 2.60 -5 -14 9 4.60 1.80 5 -14 -9 13.40 2.30 -5 -14 9 4.60 2.70 -5 14 9 9.20 2.90 5 14 -9 11.00 3.10 4 -14 -9 2.10 1.90 -4 -14 9 0.70 2.40 4 -14 -9 0.60 2.70 -4 -14 9 4.40 1.70 4 14 -9 5.40 2.30 -4 14 9 0.50 2.60 -3 -14 9 9.00 3.20 3 -14 -9 7.40 2.90 -3 -14 9 9.00 2.10 3 -14 -9 8.30 2.30 -3 -14 9 10.50 2.70 -3 14 9 10.80 2.80 3 14 -9 12.20 2.80 -2 -14 9 -0.50 2.50 2 -14 -9 -1.20 3.20 -2 -14 9 1.00 3.40 -2 -14 9 -0.60 2.00 2 -14 -9 -0.50 2.30 -2 14 9 -1.70 2.30 2 14 -9 1.50 2.40 2 14 -9 0.80 2.80 5 -15 -9 1.90 2.00 -5 -15 9 -1.30 2.60 -5 -15 9 -0.10 1.50 5 15 -9 0.00 2.50 -5 15 9 1.40 2.60 -4 -15 9 4.90 2.60 4 -15 -9 6.60 2.20 -4 -15 9 8.40 2.00 4 -15 -9 8.40 3.10 -4 15 9 10.90 2.70 4 15 -9 6.60 2.70 -3 -15 9 2.60 2.40 3 -15 -9 3.50 2.70 -3 -15 9 3.20 3.10 3 -15 -9 1.90 2.10 -3 -15 9 1.90 1.70 -3 15 9 2.20 2.50 3 15 -9 0.00 2.40 -2 -15 9 -2.70 3.30 2 -15 -9 -0.20 2.40 -2 -15 9 0.60 2.60 2 -15 -9 -1.20 3.10 -2 -15 9 0.20 2.00 2 15 -9 3.30 2.80 -2 15 9 0.80 2.50 2 15 -9 2.30 2.80 -5 -16 9 -1.00 2.60 5 -16 -9 0.10 2.20 -5 -16 9 1.70 1.60 5 16 -9 -1.80 2.40 -5 16 9 2.00 2.60 -4 -16 9 4.30 1.70 -4 -16 9 2.60 2.50 4 -16 -9 4.80 3.10 4 -16 -9 1.50 2.10 -4 16 9 3.10 2.60 4 16 -9 2.10 2.30 3 -16 -9 1.50 2.20 -3 -16 9 0.70 1.70 -3 -16 9 3.20 3.30 3 -16 -9 4.60 2.80 -3 -16 9 1.10 2.50 -3 16 9 3.20 2.60 3 16 -9 0.60 2.80 5 -17 -9 -1.60 2.20 -5 -17 9 1.60 2.60 -5 -17 9 1.50 1.60 5 17 -9 0.00 2.90 -5 17 9 2.20 2.90 4 -17 -9 -1.10 2.20 -4 -17 9 2.10 1.70 4 -17 -9 2.40 3.10 -4 -17 9 0.70 2.50 4 17 -9 -0.30 2.70 -4 17 9 1.50 2.60 3 -17 -9 -0.50 2.30 -3 -17 9 3.90 3.50 -3 -17 9 1.70 1.80 -3 -17 9 -0.60 2.60 3 -17 -9 1.10 2.80 3 17 -9 -1.90 2.60 -3 17 9 0.10 2.60 -4 -18 9 6.40 1.80 4 -18 -9 5.70 2.40 -4 -18 9 6.70 2.80 4 -18 -9 8.30 3.30 4 18 -9 2.70 2.50 -4 18 9 5.80 2.80 3 -18 -9 1.70 2.40 -3 -18 9 3.60 3.20 -3 -18 9 -0.20 2.90 -3 -18 9 -0.40 1.80 3 -18 -9 2.40 2.90 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 82462 _shelx_res_file ; TITL JTM1302_0m_a.res in P2(1)/n Z=8 shelx.res created by SHELXL-2018/3 at 10:54:18 on 05-Apr-2023 REM Old TITL JTM1302_0m in P2(1)/n REM SHELXT solution in P2(1)/n REM R1 0.150, Rweak 0.006, Alpha 0.019, Orientation as input REM Formula found by SHELXT: C16 N6 O2 CELL 0.71073 6.8724 33.5020 7.3449 90.000 117.238 90.000 ZERR 8.000 0.0014 0.0068 0.0015 0.000 0.003 0.000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z SFAC C H N O UNIT 64 56 8 24 TEMP -123 SIZE 0.097 0.166 0.355 L.S. 5 BOND $H LIST 4 FMAP 2 PLAN 5 HTAB O3 N2 EQIV $1 -x+3/2, y+1/2, -z+1/2 HTAB C7 O4_$1 EQIV $3 x-1, y, z HTAB C8 O6_$3 HTAB O6 N1 EQIV $4 -x+1/2, y-1/2, -z+1/2 HTAB C15 O1_$4 EQIV $5 x+1, y, z HTAB C16 O3_$5 CONF MPLA O1 O2 C1 > C7 MPLA O4 O5 C9 > C15 ACTA 57.3 WGHT 0.062100 0.222700 FVAR 0.41856 O1 4 0.210747 0.581097 0.128898 11.00000 0.03919 0.02851 = 0.05087 0.00553 0.02336 0.00735 O2 4 0.501311 0.544328 0.138790 11.00000 0.04001 0.02970 = 0.05599 0.00760 0.03279 0.00205 O3 4 0.409570 0.361281 0.455049 11.00000 0.03550 0.02432 = 0.05992 0.00507 0.02765 -0.00132 AFIX 3 H3A 2 0.516808 0.349351 0.445154 11.00000 -1.50000 AFIX 0 N1 3 0.431292 0.400309 0.392809 11.00000 0.02664 0.02306 = 0.03569 -0.00019 0.01375 -0.00338 C1 1 0.255124 0.464126 0.309147 11.00000 0.02035 0.02962 = 0.02447 -0.00419 0.00884 -0.00173 C2 1 0.081440 0.486678 0.302958 11.00000 0.02047 0.03579 = 0.03241 -0.00449 0.01365 -0.00297 AFIX 43 H2 2 -0.020388 0.474321 0.339202 11.00000 -1.20000 AFIX 0 C3 1 0.052432 0.526846 0.245181 11.00000 0.02231 0.03612 = 0.03735 -0.00468 0.01440 0.00483 AFIX 43 H3 2 -0.065828 0.542093 0.241589 11.00000 -1.20000 AFIX 0 C4 1 0.204270 0.543065 0.193887 11.00000 0.02698 0.02638 = 0.02822 -0.00109 0.01052 0.00337 C5 1 0.377489 0.520836 0.199389 11.00000 0.02400 0.03079 = 0.02572 -0.00230 0.01307 -0.00174 C6 1 0.408069 0.481721 0.255168 11.00000 0.02120 0.02805 = 0.02753 -0.00197 0.01215 0.00199 AFIX 43 H6 2 0.527136 0.466906 0.257669 11.00000 -1.20000 AFIX 0 C7 1 0.403130 0.583107 0.098956 11.00000 0.04632 0.03266 = 0.04137 0.00677 0.02593 0.00459 AFIX 23 H7A 2 0.363159 0.591287 -0.043339 11.00000 -1.20000 H7B 2 0.507199 0.602939 0.193416 11.00000 -1.20000 AFIX 0 C8 1 0.271150 0.422523 0.372246 11.00000 0.02285 0.02977 = 0.03433 -0.00345 0.01433 -0.00431 AFIX 43 H8 2 0.159251 0.411565 0.398925 11.00000 -1.20000 AFIX 0 O4 4 0.790287 0.155513 0.412591 11.00000 0.04230 0.02745 = 0.08254 -0.00556 0.03348 -0.00003 O5 4 0.544048 0.196649 0.455876 11.00000 0.03974 0.02787 = 0.09402 -0.00384 0.04387 -0.00665 O6 4 0.843243 0.383939 0.420288 11.00000 0.03471 0.02757 = 0.06120 0.00706 0.02695 -0.00209 AFIX 3 H6A 2 0.725059 0.395443 0.409864 11.00000 -1.50000 AFIX 0 N2 3 0.782974 0.343599 0.420834 11.00000 0.02725 0.02652 = 0.03595 0.00370 0.01451 -0.00259 C9 1 0.889377 0.276228 0.410334 11.00000 0.02082 0.03135 = 0.02766 0.00001 0.01102 -0.00046 C10 1 1.035980 0.251115 0.383784 11.00000 0.02137 0.04080 = 0.03542 -0.00018 0.01466 0.00047 AFIX 43 H10 2 1.152810 0.262583 0.366388 11.00000 -1.20000 AFIX 0 C11 1 1.016556 0.209667 0.381951 11.00000 0.02402 0.03993 = 0.04351 -0.00401 0.01647 0.00576 AFIX 43 H11 2 1.116764 0.192674 0.363450 11.00000 -1.20000 AFIX 0 C12 1 0.845219 0.194682 0.408249 11.00000 0.02649 0.02870 = 0.03771 -0.00261 0.01192 0.00254 C13 1 0.698622 0.219406 0.434700 11.00000 0.02112 0.03186 = 0.03796 -0.00169 0.01390 -0.00286 C14 1 0.714765 0.259901 0.437320 11.00000 0.02271 0.02964 = 0.03714 -0.00172 0.01545 0.00114 AFIX 43 H14 2 0.613289 0.276437 0.456418 11.00000 -1.20000 AFIX 0 C15 1 0.598875 0.156085 0.441957 11.00000 0.03581 0.02864 = 0.04415 0.00156 0.01637 -0.00167 AFIX 23 H15A 2 0.476274 0.142790 0.325521 11.00000 -1.20000 H15B 2 0.626735 0.141616 0.569104 11.00000 -1.20000 AFIX 0 C16 1 0.919676 0.319314 0.408302 11.00000 0.02368 0.03568 = 0.03306 0.00226 0.01525 -0.00293 AFIX 43 H16 2 1.043047 0.329466 0.397484 11.00000 -1.20000 AFIX 0 HKLF 4 REM JTM1302_0m_a.res in P2(1)/n Z=8 REM wR2 = 0.1265, GooF = S = 1.047, Restrained GooF = 1.047 for all data REM R1 = 0.0458 for 2836 Fo > 4sig(Fo) and 0.0659 for all 3858 data REM 217 parameters refined using 0 restraints END WGHT 0.0621 0.2226 REM Highest difference peak 0.310, deepest hole -0.193, 1-sigma level 0.053 Q1 1 0.3754 0.4960 0.1669 11.00000 0.05 0.31 Q2 1 0.2592 0.4412 0.3082 11.00000 0.05 0.30 Q3 1 0.8988 0.2968 0.4141 11.00000 0.05 0.29 Q4 1 1.0364 0.2301 0.4007 11.00000 0.05 0.26 Q5 1 0.1584 0.4723 0.2829 11.00000 0.05 0.26 ; _shelx_res_checksum 39507 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O O1 0.21075(18) 0.58110(3) 0.12890(17) 0.0385(3) Uani d 1 . . O O2 0.50131(18) 0.54433(3) 0.13879(17) 0.0377(3) Uani d 1 . . O O3 0.40957(17) 0.36128(3) 0.45505(17) 0.0377(3) Uani d 1 . . H H3A 0.516808 0.349351 0.445154 0.057 Uiso d 1 . . N N1 0.43129(18) 0.40031(3) 0.39281(18) 0.0287(3) Uani d 1 . . C C1 0.2551(2) 0.46413(4) 0.30915(19) 0.0254(3) Uani d 1 . . C C2 0.0814(2) 0.48668(4) 0.3030(2) 0.0290(3) Uani d 1 . . H H2 -0.020388 0.474321 0.339202 0.035 Uiso calc 1 . . C C3 0.0524(2) 0.52685(4) 0.2452(2) 0.0316(3) Uani d 1 . . H H3 -0.065828 0.542093 0.241589 0.038 Uiso calc 1 . . C C4 0.2043(2) 0.54306(4) 0.1939(2) 0.0280(3) Uani d 1 . . C C5 0.3775(2) 0.52084(4) 0.1994(2) 0.0262(3) Uani d 1 . . C C6 0.4081(2) 0.48172(4) 0.25517(19) 0.0252(3) Uani d 1 . . H H6 0.527136 0.466906 0.257669 0.030 Uiso calc 1 . . C C7 0.4031(3) 0.58311(4) 0.0990(3) 0.0379(4) Uani d 1 . . H H7A 0.363159 0.591287 -0.043339 0.045 Uiso calc 1 . . H H7B 0.507199 0.602939 0.193416 0.045 Uiso calc 1 . . C C8 0.2711(2) 0.42252(4) 0.3722(2) 0.0285(3) Uani d 1 . . H H8 0.159251 0.411565 0.398925 0.034 Uiso calc 1 . . O O4 0.79029(19) 0.15551(3) 0.4126(2) 0.0489(3) Uani d 1 . . O O5 0.54405(19) 0.19665(3) 0.4559(2) 0.0488(3) Uani d 1 . . O O6 0.84324(18) 0.38394(3) 0.42029(17) 0.0392(3) Uani d 1 . . H H6A 0.725059 0.395443 0.409864 0.059 Uiso d 1 . . N N2 0.78297(19) 0.34360(4) 0.42083(18) 0.0299(3) Uani d 1 . . C C9 0.8894(2) 0.27623(4) 0.4103(2) 0.0266(3) Uani d 1 . . C C10 1.0360(2) 0.25112(4) 0.3838(2) 0.0319(3) Uani d 1 . . H H10 1.152810 0.262583 0.366388 0.038 Uiso calc 1 . . C C11 1.0166(2) 0.20967(5) 0.3820(2) 0.0354(3) Uani d 1 . . H H11 1.116764 0.192674 0.363450 0.043 Uiso calc 1 . . C C12 0.8452(2) 0.19468(4) 0.4082(2) 0.0320(3) Uani d 1 . . C C13 0.6986(2) 0.21941(4) 0.4347(2) 0.0302(3) Uani d 1 . . C C14 0.7148(2) 0.25990(4) 0.4373(2) 0.0292(3) Uani d 1 . . H H14 0.613289 0.276437 0.456418 0.035 Uiso calc 1 . . C C15 0.5989(3) 0.15609(4) 0.4420(2) 0.0369(3) Uani d 1 . . H H15A 0.476274 0.142790 0.325521 0.044 Uiso calc 1 . . H H15B 0.626735 0.141616 0.569104 0.044 Uiso calc 1 . . C C16 0.9197(2) 0.31931(4) 0.4083(2) 0.0299(3) Uani d 1 . . H H16 1.043047 0.329466 0.397484 0.036 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.0392(6) 0.0285(6) 0.0509(7) 0.0074(4) 0.0234(5) 0.0055(5) O2 0.0400(6) 0.0297(6) 0.0560(7) 0.0021(4) 0.0328(5) 0.0076(5) O3 0.0355(6) 0.0243(5) 0.0599(7) -0.0013(4) 0.0277(5) 0.0051(5) N1 0.0266(6) 0.0231(6) 0.0357(6) -0.0034(4) 0.0137(5) -0.0002(5) C1 0.0204(6) 0.0296(7) 0.0245(6) -0.0017(5) 0.0088(5) -0.0042(5) C2 0.0205(7) 0.0358(8) 0.0324(7) -0.0030(5) 0.0137(6) -0.0045(6) C3 0.0223(7) 0.0361(8) 0.0373(8) 0.0048(6) 0.0144(6) -0.0047(6) C4 0.0270(7) 0.0264(7) 0.0282(7) 0.0034(5) 0.0105(6) -0.0011(5) C5 0.0240(7) 0.0308(7) 0.0257(6) -0.0017(5) 0.0131(5) -0.0023(5) C6 0.0212(6) 0.0281(7) 0.0275(7) 0.0020(5) 0.0121(5) -0.0020(5) C7 0.0463(9) 0.0327(8) 0.0414(9) 0.0046(7) 0.0259(7) 0.0068(6) C8 0.0229(7) 0.0298(7) 0.0343(7) -0.0043(5) 0.0143(6) -0.0035(6) O4 0.0423(7) 0.0275(6) 0.0825(9) 0.0000(5) 0.0335(7) -0.0056(5) O5 0.0397(6) 0.0279(6) 0.0940(10) -0.0066(5) 0.0439(7) -0.0038(6) O6 0.0347(6) 0.0276(6) 0.0612(7) -0.0021(4) 0.0269(5) 0.0071(5) N2 0.0272(6) 0.0265(6) 0.0360(6) -0.0026(5) 0.0145(5) 0.0037(5) C9 0.0208(6) 0.0313(7) 0.0277(7) -0.0005(5) 0.0110(5) 0.0000(5) C10 0.0214(7) 0.0408(9) 0.0354(8) 0.0005(6) 0.0147(6) -0.0002(6) C11 0.0240(7) 0.0399(9) 0.0435(8) 0.0058(6) 0.0165(6) -0.0040(6) C12 0.0265(7) 0.0287(8) 0.0377(8) 0.0025(5) 0.0119(6) -0.0026(6) C13 0.0211(7) 0.0319(8) 0.0380(8) -0.0029(5) 0.0139(6) -0.0017(6) C14 0.0227(7) 0.0296(7) 0.0371(8) 0.0011(5) 0.0154(6) -0.0017(6) C15 0.0358(8) 0.0286(8) 0.0441(9) -0.0017(6) 0.0164(7) 0.0016(6) C16 0.0237(7) 0.0357(8) 0.0331(7) -0.0029(6) 0.0153(6) 0.0023(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C4 O1 C7 . . 106.02(11) ? C5 O2 C7 . . 106.39(11) ? N1 O3 H3A . . 100.3 ? C8 N1 O3 . . 111.31(11) ? C2 C1 C6 . . 120.04(13) ? C2 C1 C8 . . 117.85(12) ? C6 C1 C8 . . 122.10(12) ? C1 C2 C3 . . 122.15(13) ? C1 C2 H2 . . 118.9 ? C3 C2 H2 . . 118.9 ? C4 C3 C2 . . 116.33(12) ? C4 C3 H3 . . 121.8 ? C2 C3 H3 . . 121.8 ? O1 C4 C3 . . 127.89(13) ? O1 C4 C5 . . 110.19(12) ? C3 C4 C5 . . 121.91(13) ? C6 C5 O2 . . 128.03(12) ? C6 C5 C4 . . 122.51(12) ? O2 C5 C4 . . 109.45(12) ? C5 C6 C1 . . 117.05(12) ? C5 C6 H6 . . 121.5 ? C1 C6 H6 . . 121.5 ? O2 C7 O1 . . 107.86(11) ? O2 C7 H7A . . 110.1 ? O1 C7 H7A . . 110.1 ? O2 C7 H7B . . 110.1 ? O1 C7 H7B . . 110.1 ? H7A C7 H7B . . 108.4 ? N1 C8 C1 . . 122.00(12) ? N1 C8 H8 . . 119.0 ? C1 C8 H8 . . 119.0 ? C12 O4 C15 . . 105.87(11) ? C13 O5 C15 . . 106.11(11) ? N2 O6 H6A . . 99.2 ? C16 N2 O6 . . 112.48(11) ? C10 C9 C14 . . 120.06(13) ? C10 C9 C16 . . 118.69(12) ? C14 C9 C16 . . 121.24(12) ? C9 C10 C11 . . 122.04(13) ? C9 C10 H10 . . 119.0 ? C11 C10 H10 . . 119.0 ? C12 C11 C10 . . 116.57(13) ? C12 C11 H11 . . 121.7 ? C10 C11 H11 . . 121.7 ? O4 C12 C11 . . 128.09(13) ? O4 C12 C13 . . 110.11(13) ? C11 C12 C13 . . 121.80(14) ? C14 C13 O5 . . 127.91(12) ? C14 C13 C12 . . 122.58(13) ? O5 C13 C12 . . 109.51(13) ? C13 C14 C9 . . 116.94(12) ? C13 C14 H14 . . 121.5 ? C9 C14 H14 . . 121.5 ? O5 C15 O4 . . 108.40(12) ? O5 C15 H15A . . 110.0 ? O4 C15 H15A . . 110.0 ? O5 C15 H15B . . 110.0 ? O4 C15 H15B . . 110.0 ? H15A C15 H15B . . 108.4 ? N2 C16 C9 . . 121.07(12) ? N2 C16 H16 . . 119.5 ? C9 C16 H16 . . 119.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag O1 C4 . 1.3685(17) ? O1 C7 . 1.4377(19) ? O2 C5 . 1.3742(16) ? O2 C7 . 1.4311(17) ? O3 N1 . 1.4154(15) ? O3 H3A . 0.8702 ? N1 C8 . 1.2790(18) ? C1 C2 . 1.3957(18) ? C1 C6 . 1.4110(18) ? C1 C8 . 1.4570(19) ? C2 C3 . 1.398(2) ? C2 H2 . 0.9500 ? C3 C4 . 1.373(2) ? C3 H3 . 0.9500 ? C4 C5 . 1.3890(19) ? C5 C6 . 1.3603(19) ? C6 H6 . 0.9500 ? C7 H7A . 0.9900 ? C7 H7B . 0.9900 ? C8 H8 . 0.9500 ? O4 C12 . 1.3699(18) ? O4 C15 . 1.427(2) ? O5 C13 . 1.3730(17) ? O5 C15 . 1.4264(18) ? O6 N2 . 1.4140(15) ? O6 H6A . 0.8701 ? N2 C16 . 1.2776(18) ? C9 C10 . 1.3931(19) ? C9 C14 . 1.4129(18) ? C9 C16 . 1.4595(19) ? C10 C11 . 1.394(2) ? C10 H10 . 0.9500 ? C11 C12 . 1.373(2) ? C11 H11 . 0.9500 ? C12 C13 . 1.3849(19) ? C13 C14 . 1.3606(19) ? C14 H14 . 0.9500 ? C15 H15A . 0.9900 ? C15 H15B . 0.9900 ? C16 H16 . 0.9500 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag O3 H3A N2 . 0.87 1.93 2.7549(16) 158 yes C7 H7B O4 2_655 0.99 2.58 3.239(2) 124 yes C8 H8 O6 1_455 0.95 2.43 3.3754(18) 173 yes O6 H6A N1 . 0.87 1.97 2.7989(17) 158 yes C15 H15A O1 2_545 0.99 2.54 3.1775(19) 122 yes C16 H16 O3 1_655 0.95 2.59 3.5173(18) 167 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C6 C1 C2 C3 . . . . -0.3(2) ? C8 C1 C2 C3 . . . . 179.76(13) ? C1 C2 C3 C4 . . . . 0.2(2) ? C7 O1 C4 C3 . . . . 179.08(14) ? C7 O1 C4 C5 . . . . -2.05(15) ? C2 C3 C4 O1 . . . . 178.64(13) ? C2 C3 C4 C5 . . . . -0.1(2) ? C7 O2 C5 C6 . . . . -179.40(14) ? C7 O2 C5 C4 . . . . 1.47(15) ? O1 C4 C5 C6 . . . . -178.80(12) ? C3 C4 C5 C6 . . . . 0.1(2) ? O1 C4 C5 O2 . . . . 0.38(16) ? C3 C4 C5 O2 . . . . 179.33(12) ? O2 C5 C6 C1 . . . . -179.25(13) ? C4 C5 C6 C1 . . . . -0.2(2) ? C2 C1 C6 C5 . . . . 0.29(19) ? C8 C1 C6 C5 . . . . -179.76(12) ? C5 O2 C7 O1 . . . . -2.71(15) ? C4 O1 C7 O2 . . . . 2.92(15) ? O3 N1 C8 C1 . . . . -179.96(11) ? C2 C1 C8 N1 . . . . -176.17(13) ? C6 C1 C8 N1 . . . . 3.9(2) ? C14 C9 C10 C11 . . . . 0.2(2) ? C16 C9 C10 C11 . . . . -179.38(13) ? C9 C10 C11 C12 . . . . -0.2(2) ? C15 O4 C12 C11 . . . . -179.48(15) ? C15 O4 C12 C13 . . . . 0.38(16) ? C10 C11 C12 O4 . . . . -179.98(14) ? C10 C11 C12 C13 . . . . 0.2(2) ? C15 O5 C13 C14 . . . . 179.94(14) ? C15 O5 C13 C12 . . . . 0.07(17) ? O4 C12 C13 C14 . . . . 179.83(13) ? C11 C12 C13 C14 . . . . -0.3(2) ? O4 C12 C13 O5 . . . . -0.29(17) ? C11 C12 C13 O5 . . . . 179.58(14) ? O5 C13 C14 C9 . . . . -179.49(14) ? C12 C13 C14 C9 . . . . 0.4(2) ? C10 C9 C14 C13 . . . . -0.3(2) ? C16 C9 C14 C13 . . . . 179.28(13) ? C13 O5 C15 O4 . . . . 0.16(17) ? C12 O4 C15 O5 . . . . -0.33(16) ? O6 N2 C16 C9 . . . . 178.85(11) ? C10 C9 C16 N2 . . . . 176.16(13) ? C14 C9 C16 N2 . . . . -3.5(2) ?