#------------------------------------------------------------------------------
#$Date: 2023-06-06 07:31:52 +0200 (Tue, 06 Jun 2023) $
#$Revision: 284374 $
#$URL: svn://www.crystallography.net/cod/cif/2/02/27/2022755.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2022755
loop_
_publ_author_name
'Mammadova, Gunay Z.'
'Annadurdyyeva, Selbi'
'Burkin, Gleb M.'
'Khrustalev, Victor N.'
'Akkurt, Mehmet'
'Yıldırım, Sema Öztürk'
'Bhattarai, Ajaya'
_publ_section_title
;
 Crystal structure and Hirshfeld surface analysis of
 <i>N</i>-[2-(5-methyl-furan-2-yl)phen-yl]-3-nitro-<i>N</i>-[(3-nitro-phen-yl)sulfon-yl]benzene-sulfonamide.
;
_journal_coeditor_code           TX2067
_journal_issue                   'Pt 5'
_journal_name_full
'Acta crystallographica. Section E, Crystallographic communications'
_journal_page_first              499
_journal_page_last               503
_journal_paper_doi               10.1107/S2056989023003523
_journal_volume                  79
_journal_year                    2023
_chemical_formula_iupac          'C23 H17 N3 O9 S2'
_chemical_formula_moiety         'C23 H17 N3 O9 S2'
_chemical_formula_sum            'C23 H17 N3 O9 S2'
_chemical_formula_weight         543.52
_chemical_name_systematic
<i>N</i>-[2-(5-Methylfuran-2-yl)phenyl]-3-nitro-<i>N</i>-[(3-nitrophenyl)sulfonyl]benzenesulfonamide
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     difmap
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-2013
_cell_angle_alpha                90
_cell_angle_beta                 90.8104(7)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   8.10683(6)
_cell_length_b                   19.20010(15)
_cell_length_c                   14.49754(10)
_cell_measurement_reflns_used    20996
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      77.68
_cell_measurement_theta_min      3.79
_cell_volume                     2256.34(3)
_computing_cell_refinement
;
CrysAlis PRO (Rigaku OD, 2021)
;
_computing_data_collection
;
CrysAlis PRO (Rigaku OD, 2021)
;
_computing_data_reduction
;
CrysAlis PRO (Rigaku OD, 2021)
;
_computing_molecular_graphics
;
ORTEP-3 for Windows (Farrugia, 2012)
;
_computing_publication_material
;
PLATON (Spek, 2020)
;
_computing_structure_refinement
;
SHELXL2016 (Sheldrick, 2015<i>b</i>)
;
_computing_structure_solution
;
SHELXL2016 (Sheldrick, 2015<i>a</i>)
;
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Rigaku XtaLAB Synergy Dualflex HyPix'
_diffrn_measurement_method       '\f and \w'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54184
_diffrn_reflns_av_R_equivalents  0.0551
_diffrn_reflns_av_unetI/netI     0.0324
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -8
_diffrn_reflns_limit_k_max       24
_diffrn_reflns_limit_k_min       -24
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            30531
_diffrn_reflns_theta_full        67.684
_diffrn_reflns_theta_max         77.837
_diffrn_reflns_theta_min         3.821
_diffrn_source                   'micro-focus sealed X-ray tube'
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    2.708
_exptl_absorpt_correction_T_max  0.725
_exptl_absorpt_correction_T_min  0.411
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
(CrysAlis PRO; Rigaku OD, 2021)
;
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.600
_exptl_crystal_description       'prismatic needle'
_exptl_crystal_F_000             1120
_exptl_crystal_size_max          0.33
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.11
_refine_diff_density_max         0.537
_refine_diff_density_min         -0.500
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.069
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     335
_refine_ls_number_reflns         4812
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.069
_refine_ls_R_factor_all          0.0376
_refine_ls_R_factor_gt           0.0363
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0588P)^2^+0.9267P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0991
_refine_ls_wR_factor_ref         0.1004
_reflns_number_gt                4547
_reflns_number_total             4812
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            tx2067sup1.cif
_cod_data_source_block           I
_cod_depositor_comments          'Adding full bibliography for 2022755.cif.'
_cod_original_cell_volume        2256.35(3)
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               2022755
_cod_database_fobs_code          2022755
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.469
_shelx_estimated_absorpt_t_max   0.755
_shelx_hkl_file
;
   0   0  -1 48.4150 13.5241   2
   0   0  -1 14.9686 5.91089  51
   0   0  -2 9829.90 496.109   2
   0   0  -2 9070.47 460.554  51
   0   0  -3 7.50931 26.4669   2
   0   0  -3 2.80450 14.5507  51
   0   0  -4 77300.3 3658.31   2
   0   0  -4 73542.4 3580.29  51
   0   0  -5-13.6670 36.7897   2
   0   0  -5 9.90081 15.9280  51
   0   0  -6 86022.6 3803.84   2
   0   0  -6 72336.8 3645.11  51
   0   0  -7 42.9411 48.8884   2
   0   0  -8 6089.48 498.575   4
   0   0  -8 6623.97 528.302   2
   0   0  -9 124.574 70.9862   2
   0   0  -9 53.4056 76.9664   4
   0   0 -10 1635.56 263.372   2
   0   0 -10 1186.80 127.959  20
   0   0 -10 1431.36 242.595   4
   0   0 -11 41.1722 72.5594   2
   0   0 -11 28.4508 37.3791  20
   0   0 -11-35.7914 63.0780   4
   0   0 -12 6464.03 429.622  20
   0   0  12 8111.16 465.493  14
   0   0 -12 6790.56 673.535   2
   0   0 -12 6188.60 628.098   4
   0   0 -13-10.6806 59.5221  20
   0   0  13-12.2163 41.2270  14
   0   0 -13-46.7591 67.2820   2
   0   0 -13 43.6834 99.3824   4
   0   0 -14 54153.9 3289.93   4
   0   0  14 64069.5 2997.69  14
   0   0 -14 59440.8 2949.01  19
   0   0 -14 59270.0 2971.46  20
   0   0  15 33.0150 51.3097  14
   0   0 -15-19.0745 58.2203  20
   0   0 -16 217.459 62.5311  20
   0   0 -16 237.393 51.1996  31
   0   0  16 326.024 81.0028   8
   0   0  16 278.688 69.2463  14
   0   0 -16 279.314 74.6784  48
   0   0  17 41.1644 41.0362   8
   0   0 -17-26.5250 40.2309   3
   0   0 -17-24.5815 36.4586  20
   0   0  17 20.8554 33.1759  14
   0   0  18 1262.65 102.813   8
   0   0 -18 1000.06 80.1889  10
   0   0  18 1200.85 103.977   5
   0  -1  -1 27770.0 1354.00   2
   0  -1  -2 221934. 10604.7   2
   0   1  -3 33304.0 1349.55  51
   0  -1  -3 32664.3 1396.24   2
   0   1  -4 84926.4 3399.92  51
   0   1  -4 77141.0 3460.04   2
   0  -1  -4 82395.2 3472.05   2
   0   1  -5 1876.09 143.858  51
   0   1  -5 1937.80 190.414   2
   0   1  -6 52753.9 2706.35  51
   0  -1  -6 57671.9 2835.20   2
   0   1  -6 59387.9 2822.31   2
   0  -1  -7 616.998 131.314   4
   0   1  -7 592.612 85.7351  51
   0  -1  -7 687.438 140.268   2
   0   1  -7 585.649 125.639   2
   0  -1  -8 230.672 88.7417   4
   0   1  -8 295.588 63.1080  51
   0  -1  -8 187.348 82.6882   2
   0   1  -8 407.149 116.490   2
   0  -1  -9 633.887 163.295   2
   0   1  -9 518.051 141.050   2
   0  -1  -9 508.292 135.829   4
   0  -1 -10 499.266 142.600   4
   0  -1 -10 331.584 135.803   2
   0   1 -10 250.597 110.074   2
   0   1 -10 290.526 65.8287  20
   0  -1 -10 313.350 64.6963  20
   0   1  10 220.613 53.6231  23
   0  -1 -11-35.8967 63.3029   4
   0  -1 -11 124.907 94.7519   2
   0   1 -11 122.199 109.672   2
   0  -1  11 63.8628 42.0092  14
   0  -1 -11 75.5261 41.9362  20
   0   1 -11 28.7877 44.8036  20
   0  -1 -12 80.5504 70.9743   4
   0   1 -12-44.6022 64.1762   2
   0  -1 -12-45.1399 45.9268   2
   0  -1  12 11.6196 40.9532  14
   0   1  12 70.7028 49.4328  14
   0  -1 -12-10.2057 57.8134  20
   0   1 -12 10.3667 54.8057  20
   0  -1 -13 1792.29 317.266   4
   0   1 -13 1908.84 335.972   2
   0  -1 -13 1495.77 305.527   2
   0   1  13 2450.55 210.438  14
   0  -1  13 2003.05 196.983  14
   0   1 -13 2249.35 195.758  20
   0  -1 -13 1987.36 184.900  20
   0   1  14 8192.92 474.338   8
   0   1  14 6541.27 596.041  49
   0   1 -14 6780.63 440.451  20
   0  -1 -14 6704.68 436.629  20
   0   1 -14 6785.44 422.017  19
   0  -1 -14 5158.36 619.891   4
   0  -1  14 7813.14 464.709  14
   0   1  14 7906.62 468.290  14
   0   1 -14 6320.07 663.943   2
   0   1  15 872.633 123.888   8
   0   1  15 948.240 122.231  14
   0  -1  15 824.346 116.641  14
   0   1 -15 793.276 97.2135  31
   0   1 -15 737.446 93.9872  19
   0   1 -15 798.951 108.341  20
   0  -1 -15 770.098 95.2332  19
   0  -1 -15 824.296 109.006  20
   0  -1 -16 8095.80 524.697  48
   0   1 -16 9049.54 507.457  20
   0  -1 -16 8708.00 504.002  20
   0  -1 -16 8744.71 494.600  31
   0   1  16 9096.32 520.230  14
   0  -1  16 8721.11 514.111  14
   0   1  16 9567.47 532.093   8
   0  -1 -17 17.3877 37.5476  48
   0   1 -17 12.2446 37.3940  20
   0  -1 -17-6.10841 35.7227  20
   0  -1 -17 24.1421 22.0800  31
   0   1  17 63.6869 43.6347   8
   0   1  17 63.4927 38.0005  14
   0  -1 -17 69.8037 43.5079   3
   0   1  18 3018.41 184.784   8
   0  -1 -18 2562.54 167.125  10
   0  -1  18 2982.65 188.927   5
   0   2   0 25758.2 1246.34  49
   0   2  -1 609.626 47.7407  50
   0  -2  -2 53566.5 2615.23   2
   0  -2  -3 73356.9 3799.42   2
   0   2  -3 81278.5 3773.59  51
   0  -2  -4 213457. 10638.6   2
   0   2  -4 226206. 10592.1  51
   0  -2  -5 123540. 6086.57   2
   0   2  -5 125332. 6012.53  51
   0  -2  -6 482.622 111.209   2
   0   2  -6 531.563 83.8527  51
   0  -2  -7 8193.23 626.914   2
   0   2  -7 8168.48 536.140  51
   0  -2  -7 11664.6 667.861   4
   0   2  -7 11056.6 659.961   4
   0  -2  -8 31036.8 1791.40   2
   0   2  -8 27266.4 1632.43  51
   0   2  -8 38813.7 1808.13   4
   0  -2  -8 39442.5 1815.69   4
   0  -2  -9 15437.0 963.612   4
   0   2  -9 15914.4 966.468   4
   0   2  10 7084.26 415.282  23
   0   2 -10 7106.04 595.868   4
   0  -2 -10 7075.97 593.633   4
   0   2 -10 6718.59 606.291   2
   0  -2 -10 6533.54 610.658   2
   0   2 -10 6425.50 413.317  20
   0  -2  10 7523.06 432.506  14
   0   2  11 7286.64 445.320  23
   0  -2 -11 7814.30 666.754   4
   0   2 -11 7627.55 652.885   4
   0  -2  11 8195.34 473.357  14
   0   2 -11 7223.12 452.804  20
   0  -2 -11 7507.51 453.497  20
   0   2 -11 7734.08 682.432   2
   0  -2 -11 6369.55 651.564   2
   0   2 -12 1465.99 160.943  20
   0  -2 -12 1844.35 171.079  20
   0  -2  12 2012.54 185.301  14
   0  -2 -12 1411.55 269.597   4
   0   2 -12 1238.12 267.239   4
   0   2  12 1955.04 167.972   6
   0  -2  12 2291.02 203.227   8
   0  -2 -12 1997.28 340.291   2
   0   2 -12 1112.61 265.665   2
   0   2 -13 3170.62 257.657  20
   0  -2 -13 3264.84 255.766  20
   0   2 -13 3113.86 241.806  19
   0   2  13 4077.74 289.414  14
   0  -2  13 3504.43 273.981  14
   0   2 -13 2987.41 419.028   4
   0  -2 -13 2922.86 419.396   4
   0   2 -13 3346.93 452.899   2
   0  -2  13 4101.51 295.668   8
   0  -2 -14 6505.88 426.290  20
   0   2 -14 6391.84 410.846  19
   0   2 -14 6477.72 431.004  20
   0   2  14 7657.69 457.071  14
   0  -2  14 7548.43 454.635  14
   0   2 -14 5280.89 613.645   4
   0  -2 -14 5976.57 642.042   4
   0  -2  14 8478.75 480.353   8
   0   2  14 7397.77 455.489   8
   0   2 -14 5616.09 634.578   2
   0   2  15 1172.06 139.236  14
   0  -2  15 1141.67 134.603  14
   0  -2 -15 995.879 121.808  20
   0   2 -15 1099.38 128.600  20
   0  -2 -15 1121.78 113.571  19
   0   2  15 1335.81 149.340   8
   0  -2  15 1111.77 146.652   8
   0  -2 -16-23.6161 46.7015  20
   0   2 -16-32.1728 49.7775  20
   0  -2  16 61.9602 44.1189  14
   0   2  16 9.28004 43.2677  14
   0  -2 -16 54.3879 46.9539  48
   0   2 -16 10.8233 39.7043  48
   0   2  16-9.69906 41.8669   8
   0  -2  16 10.7059 57.6376   8
   0   2 -17 3714.21 261.318  48
   0  -2 -17 3644.72 260.490  48
   0  -2 -17 4285.39 249.580  20
   0   2  17 4107.08 256.781  14
   0   2 -17 3840.62 265.683   3
   0  -2 -17 3700.11 261.183   3
   0  -2 -17 3483.73 227.915  31
   0   2 -17 3492.53 231.153  10
   0  -2  17 4346.36 271.576   8
   0   2  17 4468.97 265.549   8
   0  -2 -18 2150.07 134.332  20
   0  -2 -18 1801.21 128.980  10
   0  -2  18 2114.83 147.673   8
   0  -2  18 2098.20 145.221   5
   0   2  18 1881.28 140.536   5
   0   3   0 9.25434 13.3228  49
   0   3  -1 615.687 55.5761  50
   0   3   2 1563.52 93.0061  51
   0  -3  -3 24496.9 1353.72   2
   0   3  -3 28051.1 1343.33  51
   0  -3  -4 75180.3 3939.04   2
   0   3  -4 84090.1 3910.61  51
   0  -3  -5 108324. 5594.87   2
   0   3  -5 118305. 5541.40  51
   0  -3  -6 53109.2 2805.57   2
   0   3  -6 55832.6 2725.62  51
   0  -3  -7 9338.44 683.419   2
   0   3  -7 8866.05 591.370  51
   0   3  -7 12275.3 705.450   4
   0  -3  -7 11791.9 695.712   4
   0   3  -8 10150.8 667.303  51
   0   3  -8 12859.2 789.988   4
   0  -3  -8 13339.6 789.907   4
   0  -3  -8 10468.9 779.152   2
   0  -3  -9 1311.61 229.939   2
   0   3  -9 968.844 110.185  20
   0  -3  -9 1204.96 115.298  15
   0   3  -9 922.188 141.087  51
   0  -3  -9 1277.44 213.567   4
   0   3  -9 1646.69 235.778   4
   0  -3 -10 3065.98 361.400   4
   0   3 -10 3249.89 370.443   4
   0   3 -10 2736.87 219.619  20
   0   3  10 3167.43 223.398  23
   0   3 -10 2738.29 197.335  42
   0  -3 -10 2720.29 373.410   2
   0  -3  10 3368.43 237.972  14
   0  -3 -11 1389.00 256.859   4
   0   3 -11 1815.61 284.979   4
   0  -3  11 1726.06 162.455  14
   0   3 -11 1459.03 148.927  20
   0   3 -11 1472.36 141.998  19
   0   3  11 1392.53 143.480  23
   0   3 -12 1511.44 280.640   4
   0  -3 -12 1330.79 262.745   4
   0   3  12 1688.29 160.395   6
   0  -3  12 1696.62 176.565   8
   0  -3  12 1495.68 162.938  14
   0   3 -12 1497.30 157.365  20
   0  -3 -12 1549.46 153.960  20
   0   3 -12 1262.75 137.806  19
   0  -3  13 1555.58 175.340   8
   0   3 -13 1456.06 157.319  20
   0  -3 -13 1567.53 158.082  20
   0   3 -13 1513.35 145.331  19
   0   3  13 1002.04 220.917  49
   0  -3 -13 1320.41 274.298   4
   0   3 -13 1502.33 291.817   4
   0  -3  13 1409.72 161.070  14
   0   3  13 1853.80 178.578  14
   0   3  13 1499.06 149.296   6
   0  -3  14 785.021 114.676  14
   0   3  14 691.698 112.049  14
   0  -3  14 734.374 122.118   8
   0   3  14 675.079 110.227   8
   0   3  14 631.257 89.8720   6
   0  -3 -14 716.142 105.068  20
   0   3 -14 680.116 96.1519  19
   0   3 -14 656.183 105.514  20
   0   3  15 10183.0 580.108  14
   0  -3  15 9672.04 572.772  14
   0   3  15 10213.2 579.455   8
   0  -3  15 9934.68 593.180   8
   0   3 -15 9026.26 560.695  20
   0  -3 -15 9859.96 562.957  20
   0   3 -16 10.4178 35.4039  48
   0  -3 -16 104.853 55.5911  48
   0  -3 -16 123.709 46.0611  20
   0   3 -16 135.166 47.3559  20
   0   3  16 190.838 59.3509  14
   0  -3  16 84.7725 55.1336   8
   0   3  16 72.8649 47.4378   8
   0  -3  17 691.607 90.1931   8
   0   3 -17 554.201 62.1091  10
   0  -3 -17 636.848 87.1455  48
   0   3 -17 642.905 84.8575  48
   0  -3 -17 736.657 80.8352  20
   0  -3 -17 548.699 67.0689  31
   0  -3 -17 614.301 86.3187   3
   0   3 -17 501.929 78.9025   3
   0   3  17 654.218 82.3267  14
   0   3  17 635.915 81.5204   8
   0  -3  18 601.801 67.6999   8
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   2  -2  -4 33595.4 1764.88   4
   2   2  -3 108392. 5171.72   2
   2   2  -3 103938. 5234.68   4
   2  -2  -3 107244. 5236.36   4
   2  -2  -2 163761. 8086.89  27
   2   2  -2 174757. 8096.68  27
   2   2  -2 169353. 8031.69   2
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   2  -2   1 41456.5 2039.54   4
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   2   2   6 278.788 62.3977  50
   2   2   6 420.459 105.313  49
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   2   2   7 480.933 78.4348  50
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   2   2   8 9881.69 677.862  49
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   2   2   8 7823.08 521.436  50
   2  -2   8 7681.53 706.608  27
   2   2   8 9175.22 770.508  27
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   2   2   9 727.994 92.6500  14
   2   2   9 781.372 102.800   8
   2   2   9 740.418 97.3801   6
   2   2   9 1250.70 254.274  27
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   2   2   9 848.185 168.595  49
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   2   2  10 12169.5 663.418  14
   2   2  10 11036.9 660.700   8
   2   2  10 12872.7 672.517   6
   2  -2  10 11399.6 649.045   6
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   2  -5  17 2322.48 164.621   5
   2  -5  17 2747.82 183.764   8
   2  -6 -17 4231.07 220.602  31
   2  -6 -17 3416.08 210.311  10
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   2   6 -17 3624.89 213.189  43
   2  -6 -16 758.177 89.2775  31
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   2   6 -16 722.964 75.7026  10
   2  -6 -16 796.649 82.5154  20
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   2   6 -16 792.360 80.5310  40
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   2   6 -15 1171.78 134.612  48
   2  -6 -15 1587.55 134.907  20
   2   6 -15 1406.49 144.005   3
   2  -6 -15 1141.41 134.518   3
   2   6 -15 1485.76 135.054  40
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   2  -6 -14 1874.49 187.501   3
   2   6 -14 1963.14 189.503   3
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   2   6 -14 2102.57 180.629  10
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   2   6 -13 557.159 94.7689  10
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   2   6 -13 537.432 104.143  48
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   2   6 -11 7.14062 26.2013  41
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   2   6 -11 19.1158 33.6916  31
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   2   6  -8 18374.2 1119.95   2
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   2  -6  -8 14230.2 1106.72   4
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   2   6  -8 17255.1 904.797  41
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   2   6  -8 19601.9 965.341  48
   2  -6  -8 17997.2 887.948  34
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   2   6  -7 46.9649 53.5658   2
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   2   6  -7 191.159 102.579   4
   2  -6  -7 28.9148 58.9665   4
   2  -6  -7 92.9591 42.3024  48
   2   6  -7 101.244 46.0420  48
   2   6  -6 4178.89 351.112   2
   2   6  -6 3932.44 258.596   3
   2  -6  -6 3712.49 249.154   3
   2   6  -6 4087.00 392.240   4
   2  -6  -6 2884.02 333.688   4
   2  -6  -6 3716.24 248.085  48
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   2   6  -5 16073.7 893.779   2
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   2   6  -5 15747.4 796.151   3
   2  -6  -5 16262.6 794.569   3
   2  -6  -5 15296.9 936.650   4
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   2   6  -5 14326.6 787.516  48
   2   6  -4 945.642 127.308   2
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   2   6  -4 904.072 149.943   4
   2   6  -4 714.890 145.119  51
   2   6  -3 60.8971 43.8787   4
   2  -6  -3 82.4206 55.6775   4
   2   6  -3 18.6127 46.4500  51
   2   6  -2 205.583 60.8852   4
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   2   6   0 29.7891 24.7972   4
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   2   6   2 3743.60 299.116  27
   2  -6   2 3621.09 293.000  27
   2   6   3 1887.61 214.518  49
   2   6   3 1870.17 212.422  50
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   2   6   4 5496.88 419.443  49
   2   6   4 5098.27 396.135  50
   2   6   4 4833.05 402.847  27
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   2   6   5 35518.5 2020.82  49
   2   6   5 38363.9 1999.72  50
   2   6   5 39109.4 2044.73  27
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   2   6   6 3632.86 330.923  50
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   2   6   7 11715.5 758.819  50
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   2   6   7 12584.8 883.993  27
   2   6   8 2320.05 181.239  45
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   2   6   8 2638.10 192.734  17
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   2   6   9 19610.8 1239.49  49
   2   6   9 17099.5 1048.91  50
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   2   6   9 17373.4 1263.41  27
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   2   6   9 18362.5 951.580  17
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   2   6   9 18497.4 951.578  23
   2   6   9 18822.5 965.864   6
   2   6  10 2168.48 336.688  49
   2   6  10 2501.80 192.882  14
   2   6  10 2860.09 415.487  27
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   2   6  10 2296.51 193.419   8
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   2   6  10 2454.70 205.114   6
   2   6  10 2083.77 188.174  23
   2   6  11 3349.60 261.313   6
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   2   6  11 3322.93 246.511  14
   2   6  11 3795.65 501.322  27
   2  -6  11 2584.14 411.395  27
   2   6  11 3193.43 250.591  23
   2   6  11 3426.02 254.791   8
   2  -6  11 3297.74 282.220   8
   2   6  11 3242.81 243.634  17
   2   6  11 3576.95 436.892  49
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   2   6  12 1374.00 147.936  14
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   2   6  12 1339.68 148.707   8
   2  -6  12 1388.56 176.398   8
   2  -6  12 1096.48 262.855  27
   2   6  12 1365.97 296.087  27
   2   6  12 1717.65 171.467   6
   2   6  12 1578.48 281.815  49
   2  -6  13 10216.0 655.247   8
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   2   6  13 11231.7 654.229   5
   2  -6  13 11565.2 658.022   5
   2   6  13 10741.5 629.499   6
   2   6  13 10365.2 613.775  14
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   2   6  14 929.090 111.788  14
   2  -6  14 882.625 134.591   8
   2   6  14 988.273 119.324   6
   2   6  14 930.349 127.568   5
   2  -6  14 913.218 125.088   5
   2  -6  15 1992.71 187.660   8
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   2   6  15 1925.33 170.718   5
   2  -6  15 2126.93 184.570   5
   2   6  15 1901.07 160.461   6
   2   6  15 1513.01 132.916  38
   2   6  15 1944.03 160.310  14
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   2  -6  16 485.157 82.4988   8
   2  -6  16 386.183 67.6587   5
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   2  -6  17 119.637 36.5192   8
   2   7 -17 49.0093 18.9843  43
   2  -7 -17 65.9383 25.6766  31
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   2   7 -16 49.4180 34.4236  43
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   2  -7 -16-10.0363 27.0160  20
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   2  -7 -15 3238.16 224.302  31
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   2   7 -15 3182.87 210.938  40
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   2  -7 -15 2566.31 213.091  48
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   2  -7 -15 2933.57 205.567  20
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   2   7 -14 5931.14 347.429  40
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   2   7 -14 4645.30 341.887  48
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   2   7 -14 5236.34 334.533  10
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   2   7 -13 25.1322 38.3615   3
   2  -7 -13 12.7710 43.1001   3
   2  -7 -13 42.2544 31.2398  42
   2   7 -12 48.6959 85.9319   4
   2  -7 -12 97.7705 99.5763   4
   2   7 -12 67.7013 43.1917  10
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   2   7 -12 66.9884 52.9860  48
   2  -7 -12 68.5813 48.5530  48
   2  -7 -12 107.571 46.8858  13
   2   7 -12 81.0861 53.4440   3
   2  -7 -12 108.566 58.7526   3
   2   7 -12 116.307 88.3158   2
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   2   7 -11 810.994 94.9389  41
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   2   7 -11 875.247 240.855   4
   2  -7 -11 525.540 186.544   4
   2   7 -11 854.123 117.482  10
   2   7 -11 919.332 130.828   3
   2  -7 -11 726.476 120.247   3
   2   7 -11 1065.98 223.000   2
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   2  -7 -10 79.9429 31.8314  39
   2  -7 -10 27.3724 24.3306  34
   2   7 -10 10.4724 41.2969  20
   2  -7 -10-25.2553 42.6404  48
   2   7 -10 90.6382 49.3179  48
   2  -7 -10 9.34178 36.8453  15
   2   7 -10 46.1721 105.055   4
   2  -7 -10 88.3560 89.9092   4
   2   7 -10 76.6770 47.3097  10
   2   7 -10 26.3875 48.4257   3
   2  -7 -10-25.2621 36.3833   3
   2   7 -10 71.4210 62.9500   2
   2   7 -10 109.197 37.8000  41
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   2  -7  -9 1940.68 143.642  34
   2   7  -9 2035.78 182.450  20
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   2   7  -9 2202.00 198.477  48
   2  -7  -9 2158.16 175.595  15
   2   7  -9 2188.16 200.574   3
   2  -7  -9 1679.88 177.766   3
   2   7  -9 2392.76 362.689   4
   2  -7  -9 1462.43 275.013   4
   2   7  -9 1965.81 184.179  10
   2   7  -9 1828.63 282.213   2
   2  -7  -9 2324.46 163.021  39
   2   7  -9 1932.50 157.752  41
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   2   7  -8 5645.72 336.365  34
   2  -7  -8 5741.72 334.665  33
   2  -7  -8 6234.91 338.339  34
   2  -7  -8 5638.41 363.521  15
   2  -7  -8 5574.14 380.597  48
   2   7  -8 6735.23 402.096  48
   2   7  -8 6504.29 389.195  10
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   2   7  -8 6071.18 378.598  20
   2   7  -8 6279.99 525.746   2
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   2   7  -8 6229.13 399.003   3
   2  -7  -8 6231.10 390.475   3
   2  -7  -8 4645.07 511.156   4
   2   7  -8 6337.69 591.165   4
   2  -7  -8 6105.95 355.618  39
   2   7  -8 6234.60 359.242  41
   2   7  -7 3098.92 210.273  41
   2   7  -7 3077.06 215.807  42
   2   7  -7 3574.18 246.554   3
   2  -7  -7 3377.97 237.187   3
   2   7  -7 3350.79 386.203   4
   2  -7  -7 2450.83 326.710   4
   2  -7  -7 3472.59 230.872  21
   2   7  -7 2879.69 320.918   2
   2  -7  -7 3082.55 231.116  48
   2   7  -7 3658.66 245.747  48
   2   7  -6 822.901 99.8585   3
   2  -7  -6 924.931 100.502   3
   2  -7  -6 1019.09 181.439   4
   2   7  -6 694.504 157.825   4
   2   7  -6 1345.77 182.578   2
   2   7  -6 1188.36 206.443  51
   2  -7  -6 897.281 100.000  48
   2   7  -6 1073.60 107.492  48
   2   7  -5 419.278 110.610   4
   2  -7  -5 576.693 130.143   4
   2  -7  -5 512.661 70.6731   3
   2   7  -5 522.232 68.5403   3
   2   7  -5 570.112 112.133   2
   2   7  -5 448.918 128.534  51
   2  -7  -5 544.822 69.2475  48
   2   7  -5 593.423 72.2498  48
   2   7  -4 472.978 104.594   4
   2  -7  -4 463.738 109.155   4
   2   7  -4 216.136 99.3604  51
   2   7  -3 1626.48 183.616   4
   2  -7  -3 1471.61 183.191   4
   2   7  -3 1406.31 200.954  51
   2   7  -2 56545.5 2832.27   4
   2  -7  -2 57048.1 2843.40   4
   2  -7  -1 7336.32 458.552   4
   2   7  -1 7045.55 452.343   4
   2   7  -1 7505.85 508.396  51
   2   7  -1 7093.54 397.953   1
   2   7  -1 8270.47 448.574  27
   2   7   0 2496.45 235.590  50
   2   7   0 2382.42 161.788   1
   2   7   0 2669.38 202.012  27
   2  -7   0 2475.42 194.691  27
   2   7   1 2786.22 256.046  50
   2   7   1 2542.92 169.435   1
   2  -7   1 2694.85 218.451  27
   2   7   1 2609.96 216.461  27
   2   7   2 5523.54 399.397  49
   2   7   2 4875.31 352.066  27
   2  -7   2 4443.78 341.428  27
   2   7   3 865.465 135.085  27
   2  -7   3 736.024 125.397  27
   2   7   3 947.117 153.871  49
   2   7   3 1097.89 159.687  50
   2   7   4 5386.06 442.267  49
   2   7   4 5673.11 441.532  50
   2  -7   4 5178.07 420.615  27
   2   7   4 5413.55 425.535  27
   2   7   5 5675.80 487.403  49
   2   7   5 6224.23 479.364  50
   2   7   5 5820.02 475.045  27
   2  -7   5 5663.34 468.666  27
   2   7   6 3186.70 346.168  49
   2   7   6 2676.38 290.099  50
   2   7   6 2386.21 303.840  27
   2  -7   6 2686.49 316.700  27
   2   7   7 336.276 125.335  27
   2  -7   7 661.335 167.958  27
   2   7   7 446.074 65.9238  23
   2  -7   7 540.817 89.7652   8
  -2   7  -7 423.360 69.8702  19
   2   7   7 418.827 115.679  50
   2   7   7 517.272 72.6072  17
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   3   3 -17 84.2126 24.7999  43
   3  -3 -17 44.4117 21.9515  31
   3   3 -16 635.769 65.9447  31
   3  -3 -16 586.234 77.7177  31
   3   3 -16 734.824 84.4441  10
  -3  -3  16 761.072 86.9582   8
  -3   3  16 739.322 80.3056  14
   3   3 -16 494.268 76.4785   3
   3  -3 -16 629.168 83.5104   3
  -3   3  15 30.9193 35.3082  14
   3  -3 -15 133.575 49.7216  31
   3   3 -15 94.0228 42.3856  31
   3   3 -15 110.988 55.4072  48
   3  -3 -15 34.2240 43.5395  48
  -3  -3  15 87.5518 45.5268   8
   3   3 -15 72.2505 43.2105  10
   3  -3 -15 65.4028 43.0651   3
   3   3 -15 42.9268 37.9509   3
   3  -3 -15 54.4119 29.9738  42
   3   3 -14 1677.01 165.590  10
   3  -3 -14 1637.66 178.816  48
   3   3 -14 1432.44 171.163  48
   3  -3 -14 1310.91 165.566   3
   3   3 -14 1331.65 163.581   3
   3   3 -14 1603.17 154.037  31
   3  -3 -14 1805.92 168.545  31
   3   3 -14 1432.14 139.248  20
   3  -3 -14 1564.55 139.053  20
   3   3 -14 1504.31 119.404  41
   3  -3 -14 1763.34 142.210  42
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   3   3 -13 1664.59 198.588   3
   3  -3 -13 1768.89 202.106   3
   3   3 -13 1788.10 185.250  10
   3  -3 -13 1667.25 180.574  31
   3   3 -13 1864.86 178.989  31
   3   3 -13 2070.28 150.103  41
   3   3 -13 1822.58 158.004  42
   3  -3 -13 1993.71 143.497  41
   3  -3 -13 1738.90 155.750  42
   3  -3 -13 1798.79 204.869  48
   3   3 -13 2335.84 223.834  48
   3   3 -13 1646.96 161.194  20
   3  -3 -13 1806.92 161.055  20
   3   3 -12 1975.76 172.076  20
   3  -3 -12 1856.36 164.613  20
   3  -3 -12 1751.45 207.809  48
   3   3 -12 1868.71 210.557  48
   3   3 -12 2070.94 221.443   3
   3   3 -12 1278.80 327.816   4
   3  -3 -12 2047.40 392.493   4
   3  -3 -12 1582.11 197.369   3
   3  -3 -12 1679.29 168.707  13
   3   3 -12 2201.96 193.317  31
   3   3 -12 2092.80 169.208  42
   3   3 -12 1762.48 146.485  41
   3  -3 -12 1839.90 160.849  42
   3   3 -12 1672.62 145.381  34
   3  -3 -12 1913.06 153.367  34
   3   3 -11 201.073 50.0084  34
   3  -3 -11 162.619 49.9453  34
   3   3 -11 137.154 72.3514   3
   3  -3 -11 215.328 79.4380   3
   3   3 -11 244.803 197.063   4
   3  -3 -11 59.1089 190.339   4
   3  -3 -11 116.634 70.3411  48
   3   3 -11 153.816 70.0007  48
   3  -3 -11 132.671 51.4773  13
   3  -3 -11 130.275 40.8455  33
   3   3 -11 95.0667 51.8999  31
   3   3 -11 235.131 49.7980  41
   3   3 -11 230.918 58.3968  42
   3  -3 -11 148.651 47.7343  20
   3   3 -11 250.502 57.9591  20
   3  -3 -10 34335.9 1612.39  33
   3  -3 -10 34789.2 1614.75  34
   3   3 -10 35026.9 1615.07  34
   3   3 -10 33614.9 1612.21  33
   3   3 -10 32660.9 1664.01  31
   3  -3 -10 31645.8 1642.00  13
   3   3 -10 30575.9 1890.71   2
   3   3 -10 32137.6 1714.25   3
   3  -3 -10 28984.2 1686.22   3
   3   3 -10 30409.4 2071.27   4
   3  -3 -10 25402.5 1971.00   4
   3  -3 -10 29588.7 1691.67  48
   3   3 -10 33466.9 1718.10  48
   3  -3 -10 30127.0 1620.38  20
   3   3 -10 28744.5 1622.73  20
   3   3 -10 32851.1 1634.10  42
   3   3 -10 33452.1 1616.30  41
   3   3  -9 5.87953 23.1859  34
   3  -3  -9 5.86144 22.3321  34
  -3   3   9 37.8779 25.9575   7
   3   3  -9 10.7305 34.5358  31
   3   3  -9-5.92912 27.6590  33
   3  -3  -9 17.6282 27.4118  33
   3  -3  -9 18.2437 29.3624  13
   3   3  -9 149.569 62.7496   3
   3  -3  -9 41.3975 46.5728   3
   3   3  -9-32.9176 66.9882   2
   3   3  -9 52.6555 75.7687   4
   3  -3  -9-48.5605 69.8771   4
   3  -3  -9 27.7056 44.5789  48
   3   3  -9 14.8601 45.3659  48
   3  -3  -9 14.0717 21.4946  39
   3   3  -9 108.555 41.0025  20
   3   3  -9 80.0230 36.4222  42
   3  -3  -8 5208.83 335.737  13
   3   3  -8 4645.08 459.741   2
   3   3  -8 5165.15 374.221   3
   3  -3  -8 4921.77 361.216   3
   3   3  -8 4600.84 546.359   4
   3  -3  -8 3453.86 475.079   4
   3  -3  -8 4423.65 351.237  48
   3   3  -8 4855.28 366.681  48
   3   3  -8 5093.84 350.405  31
   3  -3  -8 6382.10 327.587  37
   3  -3  -8 5991.45 320.009  36
   3   3  -8 5652.19 311.158  33
   3   3  -8 5251.33 307.044  34
   3  -3  -8 5931.91 313.386  33
   3  -3  -8 5323.06 307.581  34
   3  -3  -8 5179.96 320.234  39
   3   3  -8 5156.60 327.779  42
   3   3  -7 63958.0 3407.89   2
   3  -3  -7 65795.5 3271.91  48
   3   3  -7 68142.7 3288.46  48
   3   3  -7 72450.8 3293.58   3
   3  -3  -7 63411.9 3267.66   3
   3  -3  -7 60983.7 3513.64   4
   3   3  -7 68395.7 3573.26   4
   3   3  -6 1517.63 198.028   2
   3  -3  -6 1510.52 143.257  48
   3   3  -6 1863.44 157.579  48
   3   3  -6 1550.74 149.495   3
   3  -3  -6 1684.86 148.867   3
   3   3  -6 1362.25 240.070   4
   3  -3  -6 1285.97 225.949   4
   3   3  -5 2968.52 273.222   2
   3  -3  -5 3248.64 230.012  48
   3   3  -5 3516.52 236.132  48
   3  -3  -5 3343.86 351.180   4
   3   3  -5 3309.89 351.152   4
   3  -3  -5 3502.74 234.737   3
   3   3  -5 3606.30 236.350   3
   3   3  -4 14466.8 835.810   2
   3  -3  -4 16479.7 804.773  48
   3   3  -4 15615.1 801.318  48
   3   3  -4 14625.3 946.795   4
   3   3  -4 15314.4 798.327   3
   3  -3  -4 14871.8 796.581   3
   3  -3  -4 14930.1 952.917   4
   3  -3  -3 48.6446 49.5212  27
   3   3  -3 32.4211 43.6695  27
   3  -3  -3 28.8071 25.6077   3
   3   3  -3 44.2006 28.7139   3
   3   3  -3 41.5422 42.3002   4
   3  -3  -3 21.6559 49.2970   4
   3   3  -2 188760. 9010.97  27
   3  -3  -2 189516. 9017.82  27
   3   3  -2 180671. 9041.20   4
   3  -3  -2 183454. 9054.32   4
   3   3  -1 72.7337 64.1860   4
   3  -3  -1 18.8315 81.3654   4
   3   3  -1 83.0318 56.1503  27
   3  -3  -1 148.669 65.1895  27
   3  -3   0 25055.0 1401.81  27
   3   3   0 26624.5 1408.80  27
   3   3   0 25104.7 1399.66   4
   3  -3   0 25844.5 1408.65   4
   3   3   1 50240.5 2624.30  27
   3  -3   1 48009.4 2613.18  27
   3  -3   1 52205.6 2620.98   4
   3   3   1 54093.4 2628.39   4
   3  -3   2 14648.4 894.616  27
   3   3   2 14511.3 891.540  27
  -3  -3  -3 2149.73 160.614   2
   3   3   3 2475.03 243.734  49
   3  -3   3 2337.07 265.556  27
   3   3   3 2587.84 273.686  27
   3  -3   4 304.245 104.293  27
   3   3   4 326.833 109.580  27
  -3  -3  -4 317.154 65.8933   2
   3   3   4 331.893 92.2827  49
   3   3   5 814.436 182.877  27
   3  -3   5 600.694 160.310  27
  -3  -3  -5 909.368 126.671   2
   3   3   5 775.422 151.517  49
   3  -3   6 70.7401 80.5502  27
   3   3   6 72.7767 64.2282  27
  -3  -3  -6 68.8477 46.4752   2
   3   3   6 105.829 71.3122  49
   3  -3   7 5645.30 589.653  27
   3   3   7 7054.15 659.237  27
   3   3   7 6269.57 545.631  49
  -3  -3  -7 6401.66 489.112   2
   3  -3   8 5267.44 332.211  38
   3  -3   8 5439.69 592.333  27
   3   3   8 6146.10 645.122  27
   3   3   8 4919.50 355.359   8
   3   3   8 5846.76 529.558  49
   3  -3   8 5394.78 355.775  14
   3   3   8 5149.57 337.738  14
  -3  -3  -8 5615.16 474.206   2
  -3   3  -8 6308.46 509.212   2
   3   3   8 5798.49 356.051   6
   3  -3   9 6338.43 375.639  38
   3   3   9 6380.52 682.733  27
   3  -3   9 5317.62 619.200  27
   3   3   9 6335.48 411.624   8
   3   3   9 6194.19 567.312  49
   3  -3   9 5403.13 392.168  14
   3   3   9 5784.40 379.497  14
   3   3   9 6132.89 394.392   6
  -3   3  -9 5977.00 371.042  20
  -3  -3  -9 6683.94 377.478  20
  -3  -3  -9 6343.02 541.081   2
  -3   3  -9 7063.68 570.656   2
   3   3  10 9741.72 939.141  27
   3  -3  10 10232.4 916.495  27
   3   3  10 10664.5 631.589   8
   3   3  10 11392.1 834.054  49
   3   3  10 9989.96 603.142  14
   3   3  10 10886.1 622.201   6
  -3   3 -10 9883.45 591.175  20
  -3  -3 -10 11468.8 600.757  20
  -3  -3 -10 10147.5 794.019   2
  -3   3 -10 12167.6 857.506   2
   3  -3  11 1351.27 302.386  27
   3   3  11 938.405 273.773  27
   3   3  11 1255.21 153.087   8
  -3   3 -11 1223.28 134.213  20
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  -3   3 -11 1328.75 255.725   2
   3   3  11 1497.79 179.954   5
   3  -3  11 1321.60 167.810   5
   3   3  11 1238.42 148.407   6
   3   3  11 1294.06 143.611  14
   3   3  11 1321.88 246.069  49
   3   3  12 23489.4 1323.82  14
  -3   3 -12 25461.9 1620.90   2
   3   3  12 25400.2 1350.91   8
  -3   3 -12 26687.7 1338.49  19
  -3   3 -12 24909.8 1319.24  20
  -3  -3 -12 26589.4 1318.99  20
   3   3  12 21256.1 1508.98  49
   3   3  12 24397.9 1740.59  27
   3  -3  12 22438.8 1674.81  27
   3   3  12 24250.8 1337.25   6
  -3   3 -12 34405.4 1730.46   4
  -3  -3 -12 35548.9 1731.18   4
   3   3  12 26705.0 1389.58   5
   3  -3  12 25759.8 1374.80   5
   3   3  13 10804.6 672.290   8
  -3   3 -13 12516.3 672.476  19
  -3   3 -13 12454.3 663.979  20
  -3  -3 -13 12902.6 660.550  20
   3   3  13 11568.1 704.781   5
   3  -3  13 12035.8 705.291   5
   3   3  13 11594.3 675.545   6
   3   3  13 11481.5 654.015  38
   3   3  13 10353.4 656.702  14
   3  -3  14 1657.43 185.281   8
   3   3  14 1618.68 166.837   8
  -3   3 -14 2178.28 171.562  20
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   3   3  14 1690.31 184.619   5
   3  -3  14 2241.82 203.909   5
   3   3  14 2016.18 175.015   6
   3   3  14 1835.12 152.173  38
   3   3  14 1477.26 159.291  14
  -3  -3 -15 4260.94 267.926  20
   3  -3  15 4184.21 305.337   5
   3   3  15 4519.41 308.191   5
   3  -3  15 4320.73 310.407   8
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  -3   3 -16 859.738 88.6701  19
   3   3  16 1132.10 113.217   5
   3  -3  16 938.813 108.271   5
   3  -3  16 1006.91 113.885   8
  -3  -3 -17 47.0273 22.7461  19
  -3   3 -17 49.0147 20.5783  19
   3   3  17 27.2235 22.6915   5
   3  -3  17 58.8707 26.4772   5
   3  -3  17 20.4048 24.4146   8
   3  -4 -17 486.057 56.2668  10
  -3  -4  17 564.431 56.1994   8
  -3   4  17 679.251 66.0572   8
  -3   4  17 519.253 52.6141  14
   3   4 -17 509.556 53.2831  40
   3  -4 -17 519.871 56.4143  31
  -3  -4  16 42.9070 32.4121   8
  -3   4  16 7.06427 33.7184   8
   3  -4 -16 39.0420 33.7641  31
   3   4 -16 18.3936 36.3799  10
   3  -4 -16 19.3266 31.4412  10
   3   4 -16-13.6228 24.9958   3
   3  -4 -16 41.2525 29.6858   3
  -3   4  16 5.74189 25.4733  14
   3   4 -16 11.8908 25.6725  40
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   3  -4 -15 50.8062 40.0792   3
   3   4 -15 39.9020 35.2029   3
   3   4 -15 37.6965 27.9195  31
   3  -4 -15 8.74605 35.6379  31
  -3   4  15 54.8147 38.2500  14
   3  -4 -15 36.3289 26.9825  42
   3   4 -15 34.4011 40.1373  10
   3   4 -14 3476.27 257.726  10
   3  -4 -14 3002.99 264.976  48
   3   4 -14 2944.70 262.376  48
   3   4 -14 3138.05 263.982   3
   3  -4 -14 2808.52 258.319   3
   3  -4 -14 3807.17 231.730  42
   3  -4 -14 3445.50 256.501  31
   3   4 -14 3170.50 236.056  31
   3  -4 -14 3322.57 228.875  20
   3  -4 -13 3564.92 264.627  31
   3   4 -13 3058.51 238.087  31
   3   4 -13 2790.35 261.612   3
   3  -4 -13 2841.56 263.790   3
   3   4 -13 3129.66 252.445  10
   3  -4 -13 2963.14 271.464  48
   3   4 -13 2913.11 267.176  48
   3  -4 -13 3445.74 241.927  13
   3  -4 -13 3119.87 220.755  42
   3   4 -13 2736.85 199.176  41
   3   4 -13 2899.15 226.209  20
   3  -4 -13 2998.85 220.669  20
   3   4 -12 16579.5 868.640  31
   3  -4 -12 15954.9 856.978  13
   3   4 -12 15305.3 905.852   3
   3   4 -12 14431.9 1228.64   4
   3  -4 -12 15857.9 909.461   3
   3  -4 -12 14949.5 1230.35   4
   3   4 -12 16026.0 878.620  10
   3  -4 -12 14852.6 814.617  34
   3   4 -12 14770.4 840.432  20
   3  -4 -12 16092.1 839.487  20
   3  -4 -12 16923.2 842.032  42
   3   4 -12 15352.8 817.180  41
   3   4 -12 16178.1 839.911  42
   3  -4 -12 14210.5 896.073  48
   3   4 -12 15369.0 908.559  48
   3  -4 -11 6582.41 415.723  13
   3  -4 -11 5809.57 449.641  48
   3   4 -11 7238.16 481.527  48
   3   4 -11 6371.93 465.849   3
   3  -4 -11 6294.33 457.216   3
   3  -4 -11 4372.78 632.385   4
   3   4 -11 5483.13 690.705   4
   3   4 -11 6200.34 404.921  20
   3  -4 -11 6590.32 402.361  20
   3   4 -11 7081.50 434.756  31
   3   4 -11 7095.91 411.292  42
   3   4 -11 6952.23 391.632  41
   3  -4 -11 6994.37 388.003  34
   3  -4 -11 6514.67 382.969  33
   3   4 -11 6339.23 381.369  34
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   3  -4 -10 2170.94 152.829  34
   3  -4 -10 1894.29 145.077  33
   3   4 -10 1795.83 143.211  34
   3   4 -10 1770.51 142.376  33
   3  -4 -10 1897.64 156.179  39
   3   4 -10 1879.04 151.126  41
   3   4 -10 1983.92 163.440  42
   3   4 -10 1496.33 152.361  20
   3  -4 -10 1730.36 154.596  20
   3  -4 -10 1659.17 162.258  13
   3   4 -10 1606.23 275.848   2
   3   4 -10 1691.34 201.722   3
   3  -4 -10 1546.59 186.168   3
   3   4 -10 1547.91 335.541   4
   3  -4 -10 1495.65 323.397   4
   3   4 -10 1630.86 175.557  31
   3  -4 -10 1875.08 200.050  48
   3   4 -10 1603.51 191.474  48
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   3   4  -9 7819.13 419.099  33
   3  -4  -9 7811.37 418.376  34
   3  -4  -9 7475.35 415.435  33
   3   4  -9 7804.21 417.818  34
  -3   4   9 7719.33 411.604   7
   3   4  -9 7689.10 464.200  31
   3  -4  -9 7189.11 447.021  13
   3  -4  -9 6376.91 467.938  48
   3   4  -9 8092.16 503.032  48
   3   4  -9 6503.03 427.840  20
   3   4  -9 7713.19 440.587  42
   3   4  -9 7077.31 423.568  41
   3  -4  -9 8197.20 435.776  39
   3   4  -9 7080.15 620.576   2
   3   4  -9 7066.85 490.169   3
   3  -4  -9 6928.47 475.612   3
   3  -4  -9 6141.33 674.894   4
   3   4  -9 6175.55 702.325   4
   3  -4  -8 2336.71 215.752  48
   3   4  -8 2615.80 232.126  48
   3  -4  -8 2407.54 183.816  39
   3   4  -8 2771.10 216.433  31
   3  -4  -8 3031.18 185.233  36
   3  -4  -8 2734.11 184.955  37
   3   4  -8 2425.30 308.380   2
   3   4  -8 2336.91 223.370   3
   3  -4  -8 2117.18 208.169   3
   3   4  -8 2054.67 350.628   4
   3  -4  -8 1809.25 325.652   4
   3   4  -8 2782.22 178.401  33
   3  -4  -8 2538.23 172.020  34
   3  -4  -8 2837.03 176.737  33
   3   4  -8 2459.49 171.732  34
   3  -4  -7 705.607 100.234   3
   3   4  -7 713.583 148.179   2
   3  -4  -7 868.356 110.380  48
   3   4  -7 754.584 110.026  48
   3   4  -7 994.974 122.765   3
   3   4  -7 1156.46 231.859   4
   3  -4  -7 630.427 171.446   4
   3   4  -6 31959.9 1818.04   2
   3  -4  -6 33815.5 1720.63  48
   3   4  -6 35370.4 1730.30  48
   3   4  -6 35788.6 1731.52   3
   3  -4  -6 34038.7 1719.97   3
   3  -4  -6 32243.1 1921.07   4
   3   4  -6 33830.1 1953.62   4
   3   4  -5 1183.47 156.507   2
   3  -4  -5 1423.69 128.668  48
   3   4  -5 1184.23 122.654  48
   3   4  -5 1308.22 216.801   4
   3  -4  -5 1488.23 223.610   4
   3  -4  -5 1360.26 125.342   3
   3   4  -5 1379.47 128.418   3
   3   4  -4 28478.4 1559.24   2
   3   4  -4 29785.8 1694.49   4
   3  -4  -4 30160.4 1702.28   4
   3   4  -4 30198.6 1524.51   3
   3  -4  -4 31280.3 1528.44   3
   3  -4  -4 31904.2 1531.57  48
   3   4  -4 30851.1 1528.56  48
   3   4  -3 49052.4 2185.30  27
   3   4  -3 37798.0 2031.93   3
   3  -4  -3 43016.7 2043.92   3
   3   4  -3 42278.7 2203.31   4
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   3   7   8 1480.67 170.635   5
   3  -7   8 1717.69 176.955   5
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   3   7   9 13954.0 1099.86  27
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   3   7   9 13644.5 746.650  23
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   3   7   9 12572.5 1028.27  49
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   3   7   9 14612.8 805.835   5
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   3   7  10 7371.42 766.970  27
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   3   7  10 7335.76 460.540  14
   3   7  10 8023.45 490.667   6
   3   7  10 8581.67 526.035   5
   3  -7  10 7803.95 506.582   5
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   3   7  11 1950.98 330.764  49
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   3   7  12 12304.4 705.439   6
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   3   7  14 2353.64 180.104  38
   3   7  14 2142.19 161.780  25
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   3   8 -11 962.257 282.922   4
   3   8 -11 1459.49 168.141   3
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   3  -8 -10 287.563 62.6585  15
   3   8 -10 334.964 78.9114  10
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   3   8  -9 232.933 67.0050  10
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   3   8  -8 404.378 67.2498  41
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   3   8  -8 605.481 94.4369   3
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   3   8  -8 434.917 56.8130  33
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   3  -8  -7 2328.87 184.749  15
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   3  -8  -7 2532.27 343.327   4
   3   8  -7 2472.98 207.075   3
   3  -8  -7 2651.19 209.211   3
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   3   8  -6 7337.60 422.831  31
   3   8  -6 6824.39 419.061   3
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   3  -8  -6 7652.44 416.724  47
   3   8  -6 7103.25 432.336  10
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   3   8   4 1324.12 222.891  49
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   3   8   7 26665.8 1258.18  30
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   3   8   7 24389.5 1286.23   6
   3   8   7 23385.7 1246.36  23
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   3   8   9 15150.1 810.005   5
   3  -8   9 12416.0 782.792   5
   3   8  10 2109.77 185.145  14
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   3   8  10 2519.94 400.346  27
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   3   8  11 251.367 164.865  27
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   3   8  11 620.473 113.687   5
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   3   8  11 804.159 97.7724  14
   3   8  11 773.109 209.368  49
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   3  -8  12 1178.97 163.360   8
   3   8  12 1523.34 157.289   6
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   3   9 -15 964.742 98.9682  43
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   3   9 -10 5445.51 349.414  10
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   3   9  -9 449.693 74.9695  41
   3   9  -9 527.187 99.4696  40
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   3   9  -9 661.769 102.559  10
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   3   9  -8 8249.53 518.260   3
   3  -9  -8 7600.36 509.337   3
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   3   9  -7 11223.0 623.998  29
   3   9  -7 9567.49 603.353   3
   3   9  -7 10267.5 819.799   4
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   3   9  -7 11027.2 632.185  10
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   3   9  -6 592.864 80.3639  31
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   3  -9  -4 4547.32 299.948  11
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   3   9  -1 24449.4 1231.58   1
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   3  -9   1 51948.3 2661.28  27
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   3   9   2 679.679 123.876  27
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   3   9   2 835.994 94.5503   1
   3   9   3 23673.1 1165.16   1
   3  -9   3 21541.3 1265.52  27
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   3   9   4 13415.9 915.098  27
   3   9   4 16372.8 791.355  28
   3   9   4 13913.2 782.956  17
   3   9   4 14546.8 788.615  45
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   4  -1  -7 33823.7 2227.42   4
   4  -1  -7 34870.3 1952.18   3
   4   1  -7 37816.2 1914.37   9
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   4   1  -7 36922.4 1950.47  10
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   4  -1  -7 41063.0 1898.73  33
   4   1  -7 39873.1 1914.48  39
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   4   1  -7 41213.0 1909.21  37
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   4   1  -6 41740.0 2026.16  37
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   4  -1  -6 41046.3 2015.86  33
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   4   1  -6 41753.9 2068.09  10
   4  -1  -6 36641.7 2308.19   4
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   4  -1  -5 18886.8 998.045   3
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   4  -2  -7 12.2691 22.5910  36
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   4  -2  -4 30826.6 1591.48   3
   4   2  -4 34822.4 1846.13   4
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   4   2  -3 38456.4 2001.45   3
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   4  -2  -2 4868.15 297.296   3
   4   2  -2 4197.12 414.041   4
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   4  -2  -1 22049.5 1146.23   3
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   4   2   0-25.0293 84.4644   4
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   4   8   8 32402.3 1760.62   6
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   4  -9 -12 6533.15 413.008  31
   4  -9 -11 9417.99 574.861  31
   4   9 -11 10234.9 549.394  31
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   4  -9 -11 9671.26 535.625   9
   4   9 -11 10228.1 584.159  40
   4   9 -11 10142.7 584.634  43
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   4  -9 -10 131.551 36.2167  34
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   4   9   3 7091.27 401.709   6
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   4   9   3 6811.23 393.503   1
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   4   9   7 640.411 84.8038  30
   4   9   7 525.020 170.981  27
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   4  10   3 16679.5 1024.16  17
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   4 -10   3 20607.2 1076.99  12
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   4 -10   4 13568.4 773.458  24
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   4  10   4 11632.5 738.077  17
   4 -10   4 13870.9 787.104  12
   4  10   5 11475.1 671.252   6
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   4 -10   5 11353.1 692.358  12
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   4  10   5 11213.8 655.272  17
   4 -10   6 2337.30 224.838  12
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   4  10   6 1844.31 196.399   6
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   4  10   6 2601.32 188.877  30
   4  10   6 2237.39 193.173  17
   4  10   6 2234.33 202.577   1
   4 -10   7 3545.70 300.509  12
   4  10   7 4122.44 286.867  45
   4 -10   7 3092.64 296.252   8
   4  10   7 3439.53 288.193   6
   4  10   7 4034.32 266.072  30
   4  10   7 3855.56 291.106   1
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   4  10   8 1105.26 133.892  17
   4  10   8 1081.71 144.318   6
   4 -10   8 1053.17 159.330   8
   4  10   8 1120.13 142.941   1
   4  10   8 1535.38 151.964  45
   4 -10   8 1229.98 157.616  12
   4  10   9 3957.16 280.234   1
   4 -10   9 2916.29 279.637   8
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   5  -5 -14 52.7565 19.6159  41
   5  -5 -14 35.5103 25.9215  42
   5   5 -14 28.9651 31.3525   3
   5  -5 -14 44.6454 30.3803   3
   5  -5 -14 49.5782 32.3184  31
   5   5 -14 74.2063 32.4486  31
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   5   5 -14 61.1125 28.3675  29
   5   5 -13 1018.05 126.058   3
   5   5 -13 1198.21 103.833  41
   5   5 -13 1307.62 128.482  40
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   5   5 -13 1360.83 136.673  10
   5   5 -12 1789.58 165.659  43
   5   5 -12 1793.77 171.404  40
   5   5 -12 1937.77 148.607  41
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   5  -5 -12 1962.34 187.511  31
   5   5 -12 1934.30 171.782  31
   5   5 -12 2036.53 189.450  10
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   5   5 -12 1463.28 170.982   3
   5  -5 -12 1325.24 166.168   3
   5  -5 -11 773.031 94.0445   9
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   5   5 -11 968.187 94.0616  33
   5   5 -11 939.675 92.0637  34
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   5   5 -10 6045.25 738.567   4
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   5  -5 -10 5481.75 454.559   3
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   5   5  -9 7097.04 821.500   4
   5  -5  -9 6181.91 762.988   4
   5   5  -9 8097.95 572.554   3
   5  -5  -9 11698.9 550.181  37
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   5   5  -9 9632.20 510.603  33
   5  -5  -9 10314.6 520.331  34
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   5   5  -9 10018.6 579.657  31
   5  -5  -8 2317.84 205.528  13
   5   5  -8 2610.26 241.286   3
   5  -5  -8 1780.44 202.640   3
   5   5  -8 2218.04 402.945   4
   5  -5  -8 2776.18 426.542   4
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   5  -5  -8 2608.47 204.601  39
   5   5  -8 2416.85 199.819  42
   5  -5  -8 2213.55 200.057   9
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   5   5  -8 2758.94 182.240  34
   5  -5  -8 2866.77 188.314  33
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   5  -5  -8 2543.98 231.761  31
   5  -5  -7 1470.37 148.895  13
   5   5  -7 1507.16 151.214  43
   5   5  -7 1514.93 139.952  41
   5   5  -7 1692.07 148.862  42
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   5  -5  -7 1310.17 155.134   3
   5   5  -7 1295.53 293.091   4
   5  -5  -7 1435.00 296.957   4
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   5  -5  -7 1539.30 126.783  34
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   5   5  -7 1492.91 170.872  10
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   5   5  -7 1634.58 146.436   9
   5   5  -7 1462.83 165.530  31
   5  -5  -7 1682.58 129.416  33
   5  -5  -7 1469.11 159.525  31
   5  -5  -6 231.428 59.8508  47
   5   5  -6 455.054 72.1180   9
   5   5  -6 518.476 95.1057  10
   5  -5  -6 334.221 63.0021  10
   5  -5  -6 369.374 73.9775   9
   5   5  -6 193.678 64.4587   3
   5  -5  -6 277.680 71.1424   3
   5   5  -6 292.205 69.8428  31
   5   5  -6 366.771 52.0520  33
   5  -5  -6 288.782 50.6731  33
   5  -5  -6 326.719 69.6514  31
   5  -5  -6 316.826 59.7396  36
   5   5  -6 286.042 53.0378  36
   5   5  -6 317.478 47.8085  34
   5  -5  -6 310.698 63.8740  37
   5   5  -6 233.179 134.988   4
   5  -5  -6 178.209 120.806   4
   5   5  -6 315.178 69.3712  40
   5   5  -6 229.149 56.4477  43
   5   5  -6 301.840 59.1401  42
   5   5  -5 1335.50 127.608  43
   5   5  -5 1252.86 134.660  40
   5   5  -5 1242.17 118.413  42
   5   5  -5 1607.96 140.085   9
   5   5  -5 1581.39 158.253  31
   5  -5  -5 1356.23 133.785  31
   5   5  -5 1142.31 101.533  33
   5  -5  -5 1118.89 104.864  33
   5   5  -5 1571.65 119.980  36
   5  -5  -5 1300.25 130.454  37
   5  -5  -5 1503.77 132.939  36
   5  -5  -5 1287.56 134.159  47
   5   5  -5 1430.21 152.325   3
   5  -5  -5 1611.22 156.649   3
   5   5  -5 969.904 235.652   4
   5  -5  -5 1300.57 270.601   4
   5   5  -4 1660.46 154.726  40
   5   5  -4 1672.75 139.710  42
   5   5  -4 1986.61 160.800   9
   5  -5  -4 1987.84 177.177   3
   5   5  -4 1968.49 311.407   4
   5  -5  -4 1875.01 305.281   4
   5   5  -4 1850.26 171.796   3
   5  -5  -4 1807.54 154.547  36
   5  -5  -4 1736.48 157.895  37
   5   5  -4 1894.49 138.865  36
   5   5  -4 2081.29 143.626  37
   5   5  -4 2279.74 187.508  31
   5  -5  -4 1792.94 140.524  32
   5  -5  -4 1632.01 149.751  31
   5  -5  -4 1571.18 157.405  47
   5   5  -3 1517.61 148.364  40
   5   5  -3 1761.46 155.992   9
   5   5  -3 1791.84 158.928  29
   5  -5  -3 2105.63 161.968  26
   5   5  -3 1816.52 154.219  26
   5  -5  -3 2182.63 181.951   3
   5   5  -3 2255.28 180.432   3
   5  -5  -3 1841.25 165.269  37
   5  -5  -3 1956.37 162.979  36
   5   5  -3 1867.73 139.790  36
   5  -5  -3 2103.54 164.781  35
   5  -5  -3 2198.43 178.301  46
   5  -5  -3 1953.71 145.214  32
   5   5  -3 2017.93 176.885  31
   5  -5  -3 2256.42 326.729   4
   5   5  -3 1690.26 283.962   4
   5  -5  -2 4009.72 278.324   3
   5   5  -2 4201.61 277.341   3
   5  -5  -2 3588.62 267.654  46
   5   5  -2 3702.10 254.184  29
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   5   5  -2 4599.64 425.229  27
   5  -5  -2 3519.27 258.445  36
   5   5  -2 3964.58 256.988  35
   5  -5  -2 4101.45 265.214  35
   5  -5  -2 3838.29 442.823   4
   5   5  -2 4120.84 444.450   4
   5  -5  -2 4082.62 258.132  26
   5   5  -2 3788.77 254.304  26
   5   5  -1 685.880 83.0914   9
   5  -5  -1 688.246 162.574  27
   5  -5  -1 511.887 79.1307  26
   5   5  -1 844.359 180.231  27
   5   5  -1 468.498 79.5645  26
   5  -5  -1 712.933 96.3364   3
   5   5  -1 718.654 93.6593   3
   5  -5  -1 809.630 82.3715  32
   5  -5  -1 636.535 89.5311  35
   5   5  -1 660.583 83.8997  28
   5   5  -1 547.868 74.7034  29
   5  -5  -1 524.302 86.0554  46
   5  -5  -1 905.211 196.302   4
   5   5  -1 684.967 171.831   4
   5   5   0 9426.68 536.279  25
   5  -5   0 9161.26 533.551  26
   5   5   0 9173.49 534.024  26
   5  -5   0 11098.7 558.910   3
   5   5   0 10482.7 549.179   3
   5  -5   0 8665.45 534.789  35
   5   5   0 9444.57 534.717  28
   5  -5   0 8468.12 704.677  27
   5   5   0 10000.5 732.749  27
   5  -5   0 8970.11 514.837  32
   5  -5   0 8890.59 542.604  46
   5   5   0 11163.7 536.657   9
   5   5   1 2684.16 192.006  28
   5  -5   1 2776.59 336.703  27
   5   5   1 2694.13 336.601  27
   5   5   1 2470.55 193.072  25
   5  -5   1 2543.23 191.599  26
   5   5   1 2221.82 184.576  26
   5  -5   1 2140.10 186.875  35
   5  -5   1 2379.00 172.895  32
   5   5   2 265.049 57.2720  38
   5   5   2 282.543 58.1223  35
   5  -5   2 401.887 73.4439  35
   5   5   2 492.220 73.0083  28
   5  -5   2 308.701 55.1108  32
   5   5   2 430.225 67.2389  45
   5  -5   2 477.279 139.729  27
   5   5   2 237.931 110.609  27
   5  -5   2 343.455 63.6583  26
   5   5   2 393.122 70.0715  26
   5   5   2 356.226 69.4514  25
   5   5   3 209.037 52.5015  38
   5   5   3 87.3231 38.9953  28
   5  -5   3 55.7060 33.6250  32
   5   5   3 113.927 39.9607  45
   5  -5   3 73.5771 74.9939  27
   5   5   3 36.3789 64.2655  27
   5   5   3 101.795 44.1701  25
   5   5   4 5723.12 339.589   1
   5   5   4 5809.82 335.026  30
   5  -5   4 5333.19 559.469  27
   5   5   4 6273.80 592.448  27
   5   5   4 5709.61 371.804  38
   5   5   4 5751.70 363.860  45
   5   5   5 54.0774 42.6836  38
   5  -5   5 147.632 47.0276  38
   5  -5   5-44.8521 64.5788  27
   5   5   5 178.458 111.212  27
   5   5   5 35.2834 37.9138   6
   5   5   5 48.8911 24.1978  30
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   5  -5   6 11604.5 629.693  38
   5  -5   6 9883.19 899.954  27
   5   5   6 9358.34 884.976  27
   5   5   6 9256.52 627.107   6
   5  -5   6 11855.4 673.162   5
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   5  -5   7 389.146 78.0872  38
   5  -5   7 265.217 143.984  27
   5   5   7 336.328 181.300  27
   5   5   7 515.908 104.738   5
   5  -5   7 384.778 95.7691   5
   5   5   7 327.591 86.3348   6
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   5  -5   8 479.576 81.6782  38
   5   5   8 315.405 74.4250  38
   5   5   8 586.686 121.882   5
   5  -5   8 398.770 98.9640   5
   5  -5   8 333.399 170.522  27
   5   5   8 241.748 151.652  27
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   5   5   9 11566.3 663.258  25
   5   5   9 11437.3 665.329  38
   5   5   9 10599.6 1025.92  27
   5  -5   9 9408.89 948.251  27
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   5   5   9 12659.6 733.922   5
   5  -5   9 10642.8 696.346   5
   5  -5  10-53.5064 76.9936  27
   5   5  10 61.0654 87.8691  27
   5   5  10-31.2808 46.2516  25
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   5  -5  10-15.1390 46.2182   5
   5   5  10-33.0261 46.1906  38
   5   5  11 55.8177 39.0357  25
   5   5  11 20.3100 40.0254  38
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   5   5  11 15.0234 59.2060   5
   5  -5  11-27.5548 39.6576   5
   5   5  12 6873.65 398.783  25
   5   5  12 6349.39 403.887  38
   5   5  12 7774.80 458.707   5
   5  -5  12 6931.72 438.614   5
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   5   5  13 106.724 39.8293  38
   5  -5  13 42.0041 50.2549   8
   5   5  13 88.9988 30.8312  25
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   5   6 -15 50.6520 18.1616  29
   5  -6 -15 46.2552 17.4179  42
   5  -6 -15 32.4831 22.7265  31
   5   6 -14 39.7772 24.2788  29
   5  -6 -14 17.8404 15.5860  41
   5  -6 -14-9.41136 26.6728  42
   5  -6 -14 38.8337 30.9005  31
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   5  -6 -13 1602.94 125.549  42
   5  -6 -13 1156.10 127.946  31
   5   6 -13 1489.32 125.546  31
   5   6 -13 1291.23 120.708  29
   5   6 -12 464.770 90.4653   3
   5  -6 -12 339.042 78.4237   3
   5   6 -12 533.431 93.1404  10
   5  -6 -12 473.037 92.7138  31
   5   6 -12 659.374 89.7631  31
   5   6 -12 562.423 89.6448  40
   5   6 -12 586.730 73.3352  41
   5   6 -12 474.023 81.7666  43
   5  -6 -12 552.163 78.6087  42
   5  -6 -12 470.055 62.8124  34
   5   6 -11 90.4107 52.9492   3
   5  -6 -11 98.6083 48.9876   3
   5   6 -11 100.905 56.2997  10
   5  -6 -11 136.274 54.7553  10
   5  -6 -11 88.9041 36.0479   9
   5   6 -11 173.456 39.8129  34
   5  -6 -11 146.139 41.1227  34
   5   6 -11 212.035 62.2910  31
   5  -6 -11 122.846 39.0957  33
   5  -6 -11 203.368 66.2483  31
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   5   6 -11 245.860 68.5187  40
   5   6 -11 115.124 54.6690  43
   5   6 -11 103.627 43.0766  41
   5  -6 -10 7493.30 465.019  13
   5   6 -10 6682.04 485.658   3
   5  -6 -10 5416.99 458.508   3
   5   6 -10 8288.74 453.015  41
   5   6 -10 7457.16 472.455  43
   5  -6 -10 8962.22 465.593  39
   5   6 -10 7238.00 476.410  40
   5  -6 -10 7577.64 446.159   9
   5   6 -10 7808.86 499.713  10
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   5  -6 -10 7126.16 488.627  31
   5   6 -10 8117.83 485.633  31
   5  -6 -10 7969.93 431.902  34
   5   6 -10 7750.80 422.241  34
   5   6 -10 7518.21 421.334  33
   5  -6 -10 8283.44 432.506  33
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   5   6  -9 24.7744 41.9725  31
   5   6  -9 76.2189 32.3483  33
   5  -6  -9 67.7573 51.7287  31
   5  -6  -9 121.570 40.3100  33
   5   6  -9 169.760 128.792   4
   5  -6  -9 51.4781 74.1671   4
   5   6  -9 43.0171 48.5353   3
   5  -6  -9 52.2222 51.5855   3
   5   6  -9 73.3034 48.2919  40
   5   6  -9 34.2793 40.4516  43
   5   6  -9 100.553 44.4626  41
   5   6  -9 81.9662 40.5688  42
   5  -6  -9 72.8829 43.8428  13
   5   6  -9 71.0378 59.7213  10
   5  -6  -9 53.5425 42.3679  10
   5  -6  -9 65.2964 40.4448   9
   5  -6  -9 129.348 40.2059  34
   5   6  -9 126.379 37.6167  34
   5  -6  -9 129.530 47.4689  37
   5  -6  -9 90.6086 42.4168  39
   5   6  -8 9401.99 611.202   3
   5  -6  -8 8191.38 587.535   3
   5   6  -8 7898.23 846.939   4
   5  -6  -8 7602.80 814.865   4
   5  -6  -8 12300.2 585.892  37
   5  -6  -8 12472.0 575.120  36
   5  -6  -8 9533.02 580.441   9
   5   6  -8 11199.2 637.640  10
   5  -6  -8 8363.50 567.597  10
   5   6  -8 9622.34 591.454  43
   5  -6  -8 10376.0 580.217  39
   5   6  -8 9728.19 571.827  42
   5   6  -8 9887.99 602.051  40
   5  -6  -8 9670.03 583.659  13
   5   6  -8 11162.6 620.652  31
   5  -6  -8 8465.32 591.384  31
   5  -6  -8 11574.6 556.118  33
   5   6  -8 10370.2 542.613  34
   5  -6  -8 10986.2 553.245  34
   5   6  -8 9932.66 542.018  33
   5   6  -7 39.0966 37.5123   3
   5  -6  -7 12.1596 30.3154   3
   5   6  -7-50.4084 72.5350   4
   5  -6  -7 140.995 106.925   4
   5   6  -7 53.7998 53.0056  10
   5  -6  -7 17.7006 28.4872  10
   5  -6  -7 50.8750 34.3450   9
   5   6  -7-11.4272 34.8891  40
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   5  -6  -7 105.750 35.3724  33
   5  -6  -7 11.3376 34.6155  31
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   5  -6  -7 24.9806 36.9380  37
   5  -6  -7 7.23328 24.4226  36
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   5  -6  -6 488.439 187.810   4
   5   6  -6 1264.37 147.239   3
   5  -6  -6 1120.95 114.984  36
   5  -6  -6 1256.10 123.752  37
   5   6  -6 1116.26 123.602  43
   5   6  -6 1020.31 129.932  40
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   5   6  -6 1016.90 109.707  42
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   5   6  -6 1011.27 94.1781  33
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   5   6  -6 1160.72 95.0161  34
   5   6  -5 4993.72 345.648   3
   5  -6  -5 5045.29 346.168   3
   5   6  -5 4679.78 532.256   4
   5  -6  -5 4714.20 531.944   4
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   5   7   0 737.943 93.0495  45
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   5  -7   0 1161.91 102.686  32
   5   7   1 5640.85 369.782  26
   5   7   1 6421.88 388.959  25
   5  -7   1 6516.11 378.373  26
   5   7   1 5999.36 365.911  38
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   5  -7   1 6381.26 361.433  32
   5   7   1 6775.77 390.155  28
   5   7   1 6043.75 535.189  27
   5  -7   1 6668.03 554.438  27
   5   7   1 6344.82 368.459  29
   5   7   1 5967.83 371.943  45
   5  -7   1 6320.15 395.927  46
   5  -7   1 5873.60 379.912  35
   5   7   1 6157.65 368.542  35
   5   7   2 3864.73 238.896  29
   5  -7   2 3731.03 409.108  27
   5   7   2 3576.56 397.566  27
   5   7   2 3920.35 258.922  28
   5   7   2 3447.97 224.916   1
   5  -7   2 3932.73 234.372  32
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   5   7   2 3095.63 238.549  26
   5   7   2 3592.50 262.118  25
   5   7   2 3719.62 249.919  45
   5   7   2 3307.73 243.599  38
   5   7   2 3026.48 233.020  35
   5  -7   2 3402.88 251.667  35
   5   7   3 2207.26 174.101  28
   5  -7   3 1691.23 165.786  24
   5  -7   3 1903.43 293.905  27
   5  -7   3 1963.73 168.991  26
   5   7   3 1772.22 161.883  26
   5   7   3 2020.59 299.793  27
   5  -7   3 1815.90 170.049  35
   5   7   3 1910.89 161.331  35
   5   7   3 1933.32 165.928  45
   5   7   3 1984.18 176.172  38
   5   7   3 1857.22 150.743   1
   5  -7   3 1722.96 143.617  32
   5  -7   4 3792.44 434.409  27
   5   7   4 2957.77 393.054  27
   5  -7   4 3490.60 250.395  24
   5   7   4 3172.61 225.374   1
   5   7   4 3008.60 231.427  35
   5   7   4 3045.27 247.630   6
   5   7   4 3152.87 218.249  30
   5  -7   4 3282.95 213.052  32
   5   7   4 3232.27 238.457  45
   5   7   5 1078.08 121.139   1
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   5   7   5 1088.41 111.122  30
   5  -7   5 1299.70 110.946  32
   5   7   5 1151.29 145.047   6
   5   7   5 1266.60 133.351  45
   5  -7   5 1378.90 267.940  27
   5   7   5 1347.10 262.968  27
   5   7   6 1701.77 160.577   1
   5   7   6 1753.30 145.802  30
   5  -7   6 1605.47 172.080  12
   5   7   6 1470.82 298.837  27
   5  -7   6 1583.84 305.144  27
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   5   7   6 1490.84 174.394   6
   5  -7   7 6689.98 700.482  27
   5   7   7 7287.73 735.706  27
   5   7   7 7195.99 491.398   6
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   6   2   3 36557.4 1944.60  35
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   6   2   3 36820.4 1945.20  26
   6   2   3 41630.7 1962.05  25
   6  -2   3 43429.7 2335.88  27
   6   2   3 40356.8 2303.17  27
   6   2   3 41434.8 1947.94  38
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   6   3  -4 353.440 56.4151  32
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   6  -3  -4 411.329 84.8028   3
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   7   2   2 17483.2 899.372  35
   7  -2   2 16686.1 901.141  35
   7   2   2 17632.6 889.179  38
   7   2   2 15444.2 847.812  37
   7  -2   2 14506.9 869.079  37
   7   2   2 15932.1 864.271  36
   7   2   2 16665.2 872.827  46
   7  -2   2 16230.8 892.543  46
   7  -2   2 14640.2 854.956  32
   7  -2   2 17203.7 901.226  26
   7   2   2 17019.6 897.889  26
   7   2   3 6279.07 402.700  36
   7   2   3 6343.95 426.711  35
   7  -2   3 7114.97 445.995  35
   7   2   3 7248.54 432.230  38
   7   2   3 6340.03 408.670  46
   7  -2   3 6568.78 433.594  46
   7  -2   3 5370.35 628.675  27
   7   2   3 6513.78 679.458  27
   7  -2   3 6855.01 438.467  26
   7   2   3 7044.34 440.758  26
   7   2   4 4117.29 297.376  36
   7   2   4 5214.45 346.796  35
   7  -2   4 4611.27 342.754  35
   7   2   4 4997.88 333.655  38
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   7  -2   4 4201.72 326.263  46
   7  -2   4 4666.09 570.271  27
   7   2   4 4603.52 566.702  27
   7  -2   4 4584.98 336.751  26
   7   2   4 4500.04 334.378  26
   7   2   5 3034.09 253.259  35
   7  -2   5 2807.50 253.554  35
   7   2   5 2463.03 206.607  36
   7   2   5 2647.86 231.125  38
   7   2   5 2793.01 231.231  46
   7  -2   5 2729.61 246.496  26
   7   2   5 3146.81 256.739  26
   7   2   5 3238.97 476.877  27
   7   2   5 2825.91 240.212  25
   7  -2   5 3375.88 482.873  27
   7   2   6 1355.26 149.992  38
   7   2   6 1152.59 152.402  26
   7  -2   6 686.732 224.135  27
   7   2   6 1350.35 320.441  27
   7  -2   6 958.839 138.866  26
   7   2   6 1107.43 137.153  25
   7   2   6 1230.00 155.331  35
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   7   2   7 987.059 138.359  26
   7   2   7 818.092 127.135  35
   7  -2   7 696.755 120.094  35
   7   2   8 537.684 91.5223  38
   7  -2   8 538.813 69.1358  32
   7  -2   8 351.942 89.5291  26
   7   2   8 381.501 93.4508  35
   7  -2   8 465.700 99.1918  35
   7  -2   9 1287.36 107.878  32
   7   2   9 1308.33 152.857  35
   7  -2   9 1194.55 145.574  35
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   7   2  11 601.516 58.0812  32
   7   2  11 789.579 90.8056  35
   7  -2  11 766.277 89.4717  35
   7  -2  11 658.467 83.1677  26
   7   2  11 785.080 92.1168  26
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   7  -2  13 149.095 26.5083  26
   7   2  13 213.102 30.4288  26
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   7   3 -12 1937.47 137.113  29
   7   3 -12 1823.65 124.277  41
   7  -3 -12 1916.39 125.361  41
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   7   3 -11 2853.76 172.774  34
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   7  -3 -11 2765.30 175.528  33
   7  -3 -11 2747.29 182.698  42
   7   3 -11 2877.21 197.858  29
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   7   3 -10 2239.48 151.069  34
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   7   3 -10 1982.65 196.842   3
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   7   3  -8 5593.82 362.549  29
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   7   3  -8 4862.60 381.713   3
   7  -3  -8 4680.31 357.325  31
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   7  -3  -7 28.4579 40.9627   9
   7   3  -7 53.1728 34.5816  41
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   7   3  -7 70.5462 53.7238   3
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   7  -3  -7 31.8396 32.4145  33
   7   3  -6 636.850 76.0387  33
   7  -3  -6 672.061 81.1528  33
   7  -3  -6 581.236 93.6494  31
   7   3  -6 545.983 88.2970   9
   7  -3  -6 612.271 98.5472   9
   7  -3  -6 524.909 78.7013  42
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   7  -3  -6 577.495 74.9871  34
   7  -3  -6 616.328 83.5964  39
   7   3  -6 758.004 86.6108  36
   7  -3  -6 684.609 88.0201  36
   7  -3  -6 499.233 185.290   4
   7   3  -6 371.509 164.422   4
   7   3  -6 489.175 85.3984  29
   7  -3  -6 553.985 102.892   3
   7   3  -6 479.166 99.5597   3
   7   3  -5 5231.04 317.501  33
   7  -3  -5 5029.48 318.503  33
   7   3  -5 5438.08 311.164  32
   7  -3  -5 5310.71 351.711  31
   7  -3  -5 5470.67 363.941   9
   7   3  -5 5677.41 356.827   9
   7  -3  -5 4853.03 332.029  39
   7   3  -5 4916.11 342.611  29
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   7  -3  -5 5341.33 338.279  36
   7   3  -5 6060.40 334.536  36
   7   3  -5 6265.60 336.787  37
   7  -3  -5 5494.26 377.410   3
   7   3  -5 5741.70 384.944   3
   7  -3  -5 5091.89 590.641   4
   7   3  -5 5095.00 599.064   4
   7  -3  -4 2263.50 374.793   4
   7   3  -4 2301.33 383.720   4
   7  -3  -4 2656.42 195.538  39
   7   3  -4 2111.06 174.779  28
   7   3  -4 2363.61 190.412  29
   7  -3  -4 2251.27 191.270  37
   7   3  -4 2762.98 186.461  36
   7   3  -4 2685.29 184.718  37
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   7  -3  -4 2935.59 188.727  32
   7   3  -4 2326.56 170.141  32
   7  -3  -4 2354.26 195.532  31
   7  -3  -4 2261.44 214.448   3
   7   3  -4 2576.25 224.065   3
   7  -3  -4 2811.76 206.887  47
   7  -3  -3 2484.17 183.226  32
   7   3  -3 2238.61 172.260  32
   7   3  -3 2402.05 187.142  29
   7   3  -3 1968.00 170.902  28
   7  -3  -3 2708.37 217.484   9
   7  -3  -3 2619.35 395.585   4
   7   3  -3 2463.09 381.645   4
   7  -3  -3 2252.22 186.348  39
   7  -3  -3 2442.77 197.545  37
   7   3  -3 2704.14 184.143  37
   7   3  -3 2566.08 184.373  36
   7  -3  -3 2291.15 194.432  47
   7  -3  -3 2733.80 225.653   3
   7   3  -3 2961.81 230.101   3
   7   3  -2 6909.00 425.415  29
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   7   3  -2 8865.45 722.460  27
   7   3  -2 7301.90 429.413  28
   7  -3  -2 8863.80 470.483  26
   7   3  -2 8040.89 463.539  26
   7  -3  -2 7800.07 467.185   9
   7   3  -2 8197.17 460.027   9
   7  -3  -2 7329.53 451.439  47
   7  -3  -2 8384.34 470.367  35
   7  -3  -2 6777.30 432.991  39
   7   3  -2 7774.75 434.220  36
   7  -3  -2 7524.01 452.379  37
   7   3  -2 7781.94 429.212  37
   7   3  -2 7016.81 414.852  41
   7  -3  -2 7683.62 435.929  32
   7   3  -2 6664.90 421.773  32
   7   3  -1 5639.63 328.347   9
   7  -3  -1 5004.22 326.305   9
   7   3  -1 5387.82 330.099  35
   7  -3  -1 4956.89 331.812  35
   7   3  -1 4416.80 290.062  37
   7  -3  -1 4477.25 316.921  37
   7  -3  -1 3894.69 307.608  36
   7   3  -1 4867.89 302.872  36
   7  -3  -1 5312.02 334.037  26
   7   3  -1 4888.97 325.689  26
   7  -3  -1 5174.91 542.220  27
   7   3  -1 4695.25 529.652  27
   7   3  -1 4599.80 298.098  28
   7  -3  -1 4514.78 316.707  47
   7  -3  -1 4964.41 332.305  46
   7   3   0 16337.8 837.443  28
   7  -3   0 17130.7 1161.27  27
   7   3   0 15947.7 1131.07  27
   7  -3   0 16206.3 850.555   9
   7  -3   0 14985.8 857.552  36
   7   3   0 16457.1 864.885  35
   7  -3   0 16774.6 874.334  35
   7   3   0 15544.7 823.370  37
   7   3   0 16478.6 840.300  36
   7  -3   0 14373.6 852.146  37
   7  -3   0 16897.7 869.062  26
   7   3   0 17057.1 870.686  26
   7  -3   0 15415.8 839.261  32
   7  -3   0 14339.0 848.620  47
   7  -3   0 15896.1 871.287  46
   7  -3   1 9232.68 766.511  27
   7   3   1 7333.23 704.543  27
   7  -3   1 8321.97 457.985   9
   7  -3   1 7666.43 479.258  36
   7   3   1 7999.95 481.364  35
   7  -3   1 8300.47 492.073  35
   7  -3   1 6374.06 460.529  37
   7   3   1 7723.21 454.643  36
   7  -3   1 8483.91 490.609  26
   7   3   1 8423.90 489.950  26
   7  -3   1 7278.35 453.698  32
   7   3   1 8171.30 460.163  46
   7  -3   1 8299.80 492.450  46
   7  -3   2 119.782 39.0028   9
   7   3   2 94.6809 37.7655  36
   7  -3   2 32.7496 43.1150  36
   7   3   2 32.5080 44.1956  35
   7  -3   2 11.7784 44.9335  35
   7   3   2 20.0947 35.5315  38
   7   3   2 118.045 41.2453  46
   7  -3   2 23.4258 43.0662  46
   7  -3   2 45.0305 91.6764  27
   7   3   2 133.480 90.5836  27
   7  -3   2 22.2886 42.5248  26
   7   3   2 99.2115 50.2423  26
   7  -3   2 91.1469 52.7289  32
   7   3   3 1935.18 185.572  35
   7  -3   3 2197.97 200.984  35
   7   3   3 1815.02 158.316  36
   7   3   3 1721.35 173.134  38
   7   3   3 1994.16 169.646  46
   7  -3   3 1877.34 187.792  46
   7  -3   3 1905.75 161.685  32
   7  -3   3 2017.90 189.922  26
   7   3   3 1799.97 183.194  26
   7  -3   3 2162.01 353.817  27
   7   3   3 1426.30 299.998  27
   7  -3   4 27295.1 1315.06  26
   7   3   4 24769.0 1301.78  26
   7   3   4 26823.0 1311.36  25
   7   3   4 22953.6 1246.39  36
   7   3   4 24954.9 1297.20  35
   7  -3   4 25875.1 1316.08  35
   7   3   4 25802.6 1294.99  38
   7   3   4 22978.1 1259.48  46
   7  -3   4 23432.1 1299.02  46
   7  -3   4 24863.7 1659.65  27
   7   3   4 25513.4 1665.55  27
   7  -3   4 23081.1 1246.69  32
   7   3   5 465.683 84.8663  46
   7   3   5 660.974 105.549  38
   7   3   5 671.497 110.458  35
   7  -3   5 659.167 119.064  35
   7  -3   5 751.131 227.061  27
   7   3   5 652.218 216.264  27
   7   3   5 657.870 111.288  25
   7  -3   5 479.278 101.395  26
   7   3   5 761.434 117.247  26
   7  -3   5 787.366 93.4627  32
   7   3   6 1907.06 176.685  46
   7   3   6 1997.86 188.384  38
   7   3   6 2004.33 198.702  35
   7  -3   6 1986.81 203.532  35
   7  -3   6 1718.15 153.001  32
   7  -3   6 1851.09 193.585  26
   7   3   6 2259.60 211.745  26
   7   3   6 1981.94 189.501  25
   7   3   7 4476.07 327.148  35
   7  -3   7 4251.12 327.762  35
   7  -3   7 4484.60 271.733  32
   7  -3   7 3931.79 313.193  26
   7   3   7 3909.62 319.586  26
   7   3   7 4427.31 308.443  25
   7   3   8 1682.85 172.243  35
   7  -3   8 1145.61 153.035  35
   7  -3   8 1148.52 147.433  26
   7   3   8 1136.40 153.715  26
   7   3   8 1679.12 153.240  25
   7  -3   8 1589.07 122.737  32
   7   3   9 310.054 66.5358  38
   7   3   9 351.652 77.9618  35
   7  -3   9 267.670 73.1654  35
   7  -3   9 165.754 59.4612  26
   7   3   9 378.295 83.6918  26
   7  -3   9 347.988 48.0564  32
   7  -3  10 34.1021 40.7153  26
   7   3  10 122.959 50.0282  26
   7   3  10 44.8821 40.8734  35
   7  -3  10-9.20718 37.5034  35
   7   3  10 29.8915 31.3878  38
   7  -3  11 171.297 46.8617  26
   7   3  11 208.518 50.9857  26
   7   3  11 147.362 44.5916  35
   7  -3  11 170.740 46.1242  35
   7   3  11 297.491 52.1788  38
   7  -3  12 3595.13 221.635  35
   7  -3  12 3438.14 218.274  46
   7  -3  12 3598.10 217.841  26
   7   3  12 3757.33 222.215  26
   7  -3  13 93.9842 22.7004  35
   7  -4 -13 3338.37 173.645  41
   7  -4 -13 3034.60 176.512  42
   7  -4 -12 7019.75 375.933  31
   7   4 -12 6601.52 354.262  41
   7  -4 -12 7183.49 356.100  41
   7  -4 -12 6459.26 356.605  42
   7  -4 -12 6244.59 348.361  34
   7   4 -11 843.425 89.7807  29
   7  -4 -11 808.873 73.2587  33
   7  -4 -11 836.129 75.4617  34
   7  -4 -11 783.629 78.0683  42
   7  -4 -11 778.042 70.8781   9
   7  -4 -11 609.007 89.5764   3
   7   4 -11 569.888 87.6902   3
   7  -4 -11 850.639 97.5084  31
   7   4 -10 2026.20 164.106  29
   7   4 -10 2011.31 135.884  34
   7  -4 -10 2200.46 144.071  33
   7  -4 -10 2175.46 144.102  34
   7   4 -10 1870.83 134.498  33
   7   4 -10 1902.46 145.050  41
   7  -4 -10 2079.49 152.184  42
   7  -4 -10 2011.94 145.927   9
   7   4 -10 1711.97 174.608   3
   7  -4 -10 1758.17 165.990  31
   7   4  -9 337.932 69.5505  29
   7   4  -9 280.979 55.1842  41
   7  -4  -9 283.363 55.4898  42
   7   4  -9 277.945 48.7574  34
   7  -4  -9 397.435 58.9225  34
   7  -4  -9 327.319 61.0321   9
   7  -4  -9 356.777 77.5850   3
   7   4  -9 299.864 76.9193   3
   7  -4  -9 397.282 77.8540  31
   7   4  -9 370.928 53.8352  33
   7  -4  -9 484.509 62.6154  33
   7   4  -8 89.1095 48.5357  29
   7   4  -8 85.2099 40.4941  41
   7  -4  -8 121.087 43.8057  42
   7  -4  -8 89.3536 39.8330  36
   7   4  -8 133.789 36.0074  34
   7  -4  -8 113.352 41.4311  34
   7  -4  -8 104.527 41.1723  39
   7  -4  -8 94.6079 40.1454  37
   7  -4  -8 25.1406 37.4565   9
   7  -4  -8 61.0368 46.7050   3
   7   4  -8 147.319 59.5772   3
   7  -4  -8 63.1646 40.3469  31
   7   4  -8 161.379 40.3054  33
   7  -4  -8 106.842 39.4147  33
   7   4  -7-30.5978 44.0278  29
   7   4  -7 22.2693 27.2341  41
   7  -4  -7-7.98530 29.2962  42
   7  -4  -7 36.2136 36.8470  36
   7   4  -7 16.6294 23.2571  34
   7  -4  -7 61.0641 35.1475  34
   7  -4  -7 7.87393 29.9779  39
   7  -4  -7 22.8756 36.3910  37
   7  -4  -7 66.9681 45.6563   9
   7  -4  -7-24.8487 43.7910   3
   7   4  -7 27.1134 43.6189   3
   7  -4  -7 10.3383 34.8882  31
   7   4  -7 5.77319 24.9240  33
   7  -4  -7 18.3887 31.8022  33
   7   4  -6-30.2039 48.0513  29
   7  -4  -6 32.0097 44.7656   9
   7   4  -6 44.9500 37.3483  41
   7  -4  -6 30.7206 36.6582  36
   7   4  -6 16.6841 25.9400  34
   7  -4  -6-6.09363 27.7363  34
   7  -4  -6 32.6776 34.2782  39
   7   4  -6 35.2195 24.6351  33
   7  -4  -6 18.7175 26.9420  33
   7  -4  -6 88.5246 43.6276  31
   7  -4  -6-12.4683 42.0797   3
   7   4  -6-13.3637 38.4639   3
   7   4  -5 7167.21 495.438  28
   7   4  -5 9315.73 529.912  29
   7  -4  -5 8970.34 819.710   4
   7   4  -5 8375.68 809.265   4
   7  -4  -5 8862.57 515.782  39
   7   4  -5 9325.40 507.880  41
   7  -4  -5 10345.6 537.932  47
   7   4  -5 8532.22 484.610  34
   7  -4  -5 9749.24 521.002  36
   7   4  -5 10468.9 509.950  36
   7   4  -5 8738.49 490.524  33
   7  -4  -5 9206.45 496.247  33
   7  -4  -5 8376.51 518.673  31
   7  -4  -5 9279.12 557.384   3
   7   4  -5 9605.66 564.559   3
   7   4  -4 198.717 45.2516  33
   7  -4  -4 275.315 55.0595  32
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   7  -8   2 562.299 81.5350  26
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   7  -8   5 79.5341 33.3226  32
   7  -8   6 436.088 69.9868  26
   7  -8   6 364.935 72.8619  35
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   8  -2  -9 8.68536 37.5760   3
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   8   2   9 27.9785 20.8890  32
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   8   2   9 49.0079 31.9475  26
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   8  -3   4 6551.68 424.620  37
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   8   3   5 358.907 80.4964  26
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   8   3   5 525.005 88.4843  35
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   8   3   7 10378.6 563.236  35
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   8   3  10 619.440 52.1891  32
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   8  -3  10 686.802 70.6789  35
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   8   4   0 11782.1 597.974  26
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   8  -4   0 9605.40 582.240  37
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   8  -4   1 4048.91 302.737  36
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   8  -4   2 8592.19 510.605  36
   8   4   2 8687.17 499.457  35
   8  -4   2 9099.17 516.754  35
   8  -4   2 8366.48 478.782  32
   8  -4   2 8100.23 497.186  26
   8   4   2 9345.00 510.462  26
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   8  -4   3 142.359 54.9848  47
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   8  -4   4 7302.68 453.952  46
   8  -4   4 7164.87 447.671  36
   8   4   4 7589.72 440.615  35
   8  -4   4 7395.56 452.433  35
   8  -4   4 6985.77 405.746  32
   8  -4   4 7143.97 440.372  26
   8   4   4 7351.41 444.445  26
   8  -4   4 6463.45 432.002  37
   8  -4   5 11.1294 42.3806  46
   8  -4   5 41.8064 46.3627  36
   8   4   5 9.31327 36.7132  35
   8  -4   5 32.0687 43.5155  35
   8  -4   5 5.80634 27.7280  32
   8  -4   5 48.1359 43.8164  26
   8   4   5 30.2841 41.0953  26
   8  -4   5 27.7995 34.0087  37
   8  -4   6 1163.90 96.3974  32
   8  -4   6 843.152 116.422  46
   8  -4   6 1031.92 115.360  26
   8   4   6 987.060 119.232  26
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   8   4   6 828.271 106.074  35
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   8  -4   7 1232.82 93.2955  32
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   8   4   7 1139.89 123.916  26
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   8   4   8 3538.47 235.691  26
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   8   4   9 87.7264 34.4822  26
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   8  -4  10 988.572 80.3512  26
   8  -4  10 1072.39 87.9069  35
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   8  -5  -9 776.534 75.7796   9
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   8   5   4 7869.92 444.746  35
   8  -5   4 7550.31 457.787  35
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   8  -5   8 979.231 98.9081  35
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   8   6   3 4294.32 275.429  26
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   8   6   6 149.434 50.0296  26
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   8  -7   1 55.1049 45.7988  36
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   8  -7   2 516.302 82.1508  35
   8  -7   2 653.478 77.0088  32
   8  -7   2 598.514 79.5158  26
   8   7   2 562.018 77.5972  26
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   8  -7   4 1079.35 116.068  35
   8  -7   4 1218.37 99.1242  32
   8  -7   4 974.253 103.765  26
   8  -7   4 947.642 118.136  37
   8  -7   5 28.2549 42.8556  46
   8  -7   5-15.3437 30.2334  35
   8  -7   5 55.6731 29.5546  32
   8  -7   5 9.03926 33.1619  37
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   8  -7   6 1543.03 138.423  46
   8  -7   6 1122.49 121.646  37
   8  -7   6 1276.98 119.804  35
   8  -7   7 1510.86 111.439  26
   8  -7   7 1438.41 130.487  46
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   8  -7   7 1405.42 126.954  36
   8  -7   7 1423.20 119.350  35
   8  -7   8 7879.57 420.085  36
   8  -7   8 7833.52 410.742  35
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   8  -7   8 8035.19 426.825  46
   8  -7   9 1664.72 117.351  46
   8  -7   9 1485.77 108.859  36
   8  -7   9 1422.10 101.494  35
   8  -7  10 5439.58 287.912  46
   8  -8 -10 729.001 53.3649  41
   8  -8  -9 3616.24 179.445   9
   8   8  -9 3326.03 181.093  29
   8  -8  -8 187.856 26.7511  33
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   8  -8  -8 247.753 32.2214  34
   8  -8  -8 206.975 39.0460   9
   8   8  -8 201.233 39.6933  29
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   8  -8  -7 1633.67 105.295  33
   8   8  -7 1314.55 118.883  29
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   8  -8  -6 17221.9 854.027  33
   8  -8  -6 17263.8 855.908  34
   8   8  -6 15018.8 874.008  29
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   8  -8  -6 18615.7 874.855  37
   8  -8  -6 17140.0 875.653  39
   8  -8  -5 2011.49 157.109  39
   8   8  -5 2135.59 161.727  29
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   8  -8  -5 2206.45 142.580  34
   8  -8  -5 2195.90 177.756   9
   8  -8  -5 2133.68 149.591  36
   8  -8  -5 2141.91 155.659  37
   8  -8  -4 2545.87 162.526  33
   8  -8  -4 2716.49 187.233  39
   8  -8  -4 2602.16 163.525  34
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   8  -8  -4 2476.74 174.159  36
   8  -8  -4 2370.65 195.402   9
   8  -8  -3 386.455 60.1063  36
   8  -8  -3 325.050 63.0218  39
   8  -8  -3 450.605 68.0436  37
   8  -8  -3 333.260 48.0099  33
   8  -8  -3 373.969 69.7376   9
   8  -8  -2 1071.05 114.362   9
   8   8  -2 1321.09 116.215  28
   8  -8  -2 1045.40 117.373  47
   8  -8  -2 1107.57 94.0441  33
   8  -8  -2 1083.15 112.543  39
   8  -8  -2 1227.04 118.512  37
   8  -8  -2 1261.05 116.057  36
   8  -8  -1 796.397 91.7347  36
   8  -8  -1 692.847 87.0044  39
   8  -8  -1 617.743 80.0477   9
   8  -8  -1 571.848 87.7820  47
   8  -8   0-35.9892 38.8455  47
   8  -8   0 8.12236 33.0651  36
   8  -8   1 930.817 109.873  36
   8  -8   1 786.931 106.656  47
   8  -8   2 14419.4 813.309  36
   8  -8   2 14183.9 817.017  37
   8  -8   2 14880.5 819.804  47
   8  -8   3 2272.12 197.948  37
   8  -8   3 2660.55 176.636  26
   8  -8   3 2158.84 192.675  47
   8  -8   3 2793.96 209.078  46
   8  -8   3 2139.99 191.611  36
   8  -8   3 2723.80 189.714  35
   8  -8   4 1876.46 169.809  37
   8  -8   4 1911.36 144.265  26
   8  -8   4 2215.60 179.286  46
   8  -8   4 1883.70 171.344  36
   8  -8   4 2024.29 158.736  35
   8  -8   5 3306.50 253.123  37
   8  -8   5 3823.98 229.748  26
   8  -8   5 4409.40 273.049  46
   8  -8   5 3432.32 256.374  36
   8  -8   5 4030.89 246.523  35
   8  -8   6 73.0402 38.8390  37
   8  -8   6 127.063 30.2500  26
   8  -8   6 45.8555 34.1497  46
   8  -8   6 89.3351 34.3390  35
   8  -8   7 160.176 35.9235  35
   8  -8   7 78.6287 34.4757  46
   8  -8   7 128.031 37.8863  37
   8  -8   8 243.605 46.8815  46
   8  -8   8 213.179 33.6807  35
   8  -8   9 183.818 33.2881  46
   8  -8   9 146.107 27.8906  36
   8   9  -9 201.178 31.5113  29
   8  -9  -9 322.628 34.9065   9
   8   9  -8 390.016 50.8783  29
   8  -9  -8 534.951 56.6543   9
   8  -9  -7 162.451 39.5929   9
   8   9  -7 141.706 34.8082  29
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   8  -9  -7 136.809 25.4086  34
   8  -9  -7 186.177 37.0068  39
   8  -9  -7 138.586 22.1962  33
   8  -9  -6 64.1720 25.3116  36
   8  -9  -6 45.3992 19.6396  34
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   9   3  -4 143.718 31.9222  33
   9  -3  -4 137.315 32.8508  33
   9  -3  -3 6474.25 341.174  36
   9  -3  -3 6184.81 338.357  37
   9   3  -3 5734.80 320.587  34
   9  -3  -3 6207.02 351.315   9
   9   3  -3 6031.19 324.553  33
   9  -3  -3 5513.18 325.254  33
   9  -3  -2 2812.29 178.795  36
   9  -3  -2 2877.04 179.212  37
   9  -3  -2 2572.73 179.257   9
   9   3  -2 2335.81 159.167  33
   9  -3  -2 2394.08 163.544  33
   9   3  -1 487.736 57.7803  33
   9  -3  -1 678.268 74.2532  32
   9   3  -1 548.444 63.0697  32
   9  -3  -1 588.735 72.2138  36
   9  -3  -1 572.681 70.7526  37
   9   3   0 1943.32 136.502  32
   9  -3   0 1600.60 134.998  37
   9  -3   0 1789.98 142.714  36
   9  -3   1 51.9312 33.7344  36
   9  -3   1 21.3237 28.2521  32
   9   3   1 61.0109 34.3824  32
   9  -3   2 6309.14 390.294  36
   9  -3   2 6654.11 380.175  32
   9   3   2 6552.98 384.325  32
   9  -3   2 7170.19 402.353  26
   9  -3   3 776.823 91.9716  36
   9  -3   3 1053.97 109.516  35
   9  -3   3 906.909 86.6084  32
   9  -3   3 912.710 100.802  26
   9   3   3 1182.15 110.836  26
   9  -3   4 289.993 54.7485  36
   9  -3   4 333.235 61.8433  35
   9  -3   4 320.574 47.3700  32
   9  -3   4 360.279 60.8590  26
   9   3   4 337.791 61.8898  26
   9   3   5 40.4213 26.3018  35
   9  -3   5-19.8591 28.5998  35
   9  -3   5 21.6847 20.8357  32
   9   3   5 37.1267 27.9599  32
   9  -3   5 64.7638 32.8318  26
   9   3   5 31.7108 31.6343  26
   9  -3   6 2126.55 157.003  35
   9  -3   6 2419.03 136.118  32
   9   3   6 2026.61 140.370  32
   9  -3   6 2114.03 151.622  26
   9   3   6 2303.52 160.059  26
   9  -3   7 1360.64 107.421  35
   9   3   7 1418.19 95.4592  32
   9  -3   7 1376.41 102.656  26
   9   3   7 1503.59 109.254  26
   9  -3   8 27.0090 15.8871  35
   9  -3   8 9.75314 11.9264  26
   9   3   8 21.9046 15.7807  26
   9  -4  -8 102.096 20.6475  34
   9  -4  -8 73.7881 16.9000  33
   9  -4  -7 557.926 50.9754  34
   9  -4  -7 543.584 50.2930  33
   9  -4  -6 2862.81 164.713  33
   9  -4  -6 2686.16 163.387  34
   9  -4  -5 808.961 76.0972  37
   9  -4  -5 921.837 73.3734  33
   9  -4  -5 781.530 69.2957  34
   9  -4  -5 737.554 85.5426   9
   9  -4  -4 10083.1 519.034  37
   9  -4  -4 9577.76 506.442  34
   9  -4  -4 9596.69 531.113   9
   9  -4  -4 10044.8 509.040  33
   9  -4  -3 558.424 65.2654  37
   9  -4  -3 510.516 69.8143   9
   9  -4  -3 480.226 56.3727  33
   9  -4  -2 8585.64 441.660  37
   9  -4  -2 8129.46 439.867   9
   9   4  -2 7859.84 418.683  33
   9  -4  -2 7594.78 422.906  33
   9  -4  -1 980.408 93.5527  37
   9  -4  -1 941.783 94.4313  36
   9   4  -1 773.144 74.3100  33
   9  -4   0 4243.63 245.342  37
   9  -4   0 3640.87 239.173  36
   9  -4   0 4168.20 235.586  32
   9   4   0 3844.34 227.839  32
   9  -4   1 3245.41 219.213  37
   9  -4   1 3328.01 224.450  36
   9  -4   1 3655.63 214.820  32
   9   4   1 3195.94 211.318  32
   9  -4   2 2414.21 179.493  36
   9  -4   2 2640.50 166.017  32
   9   4   2 2152.49 164.550  32
   9  -4   3 245.051 52.8655  36
   9  -4   3 129.248 36.3961  32
   9   4   3 211.028 45.9733  32
   9  -4   3 169.017 45.3654  26
   9   4   3 176.021 47.6462  26
   9  -4   4 36.5246 31.0451  36
   9  -4   4 107.022 38.5596  35
   9  -4   4 43.1407 25.6439  32
   9  -4   4 52.4818 27.9141  26
   9   4   4 18.7049 28.4541  26
   9  -4   5 1319.51 114.436  36
   9  -4   5 1373.55 113.983  26
   9   4   5 1736.54 126.217  26
   9  -4   5 1591.78 103.068  32
   9   4   5 1158.90 104.174  32
   9  -4   5 1556.17 124.843  35
   9  -4   6 10.1532 21.9317  35
   9  -4   6 20.5565 25.0917  46
   9  -4   6 35.4561 17.1979  32
   9   4   6 18.5088 20.9887  32
   9  -4   6 4.22874 18.7751  26
   9   4   6 19.1757 24.4036  26
   9  -4   7 371.924 48.1129  35
   9   4   7 476.922 45.0946  32
   9  -4   7 390.546 44.3792  26
   9  -4   8 2197.75 130.188  35
   9  -5  -8 57.6557 14.8936  34
   9  -5  -7 9662.51 488.042  33
   9  -5  -7 9836.91 489.571  34
   9  -5  -6 1501.40 101.988  33
   9  -5  -6 1658.48 104.854  34
   9  -5  -5 340.527 45.7788  37
   9  -5  -5 315.650 44.2267  36
   9  -5  -5 310.436 40.0468  34
   9  -5  -5 234.618 48.6269   9
   9  -5  -5 302.704 39.5368  33
   9  -5  -4 3290.19 193.561  36
   9  -5  -4 3510.93 198.605  37
   9  -5  -4 2865.72 181.668  34
   9  -5  -4 2688.54 198.011   9
   9  -5  -4 3215.92 184.645  33
   9  -5  -3 6371.70 332.034  37
   9  -5  -3 5553.98 313.393  34
   9  -5  -3 5548.78 331.819   9
   9  -5  -3 5804.63 315.473  33
   9  -5  -2 87.0239 28.7680  33
   9  -5  -2 91.1395 34.7539  37
   9  -5  -1 44.7316 24.2113  33
   9  -5  -1 40.5073 30.0904  37
   9  -5   0 5095.14 304.693  37
   9  -5   1 49.2629 32.1604  37
   9  -5   1 101.001 33.7514  32
   9   5   1 68.9849 31.9231  32
   9  -5   1 102.960 38.3554  36
   9  -5   2 2215.42 166.175  37
   9  -5   2 2497.99 177.034  36
   9  -5   2 2559.07 159.091  32
   9   5   2 2082.09 157.164  32
   9  -5   3 1896.99 152.898  36
   9  -5   3 2212.05 140.423  32
   9   5   3 1869.23 142.850  32
   9  -5   4 1218.01 115.303  36
   9  -5   4 1336.03 118.278  35
   9  -5   4 1587.82 106.077  32
   9   5   4 1198.44 108.057  32
   9  -5   4 1531.96 116.252  26
   9   5   4 1652.56 122.267  26
   9  -5   5 1458.25 122.337  36
   9  -5   5 1697.20 120.882  26
   9  -5   5 1784.05 129.882  35
   9  -5   6 93.8644 24.6933  26
   9   5   6 63.1587 24.0258  32
   9  -5   6 91.3460 26.4999  36
   9  -5   6 99.6775 29.5284  35
   9   5   7 3517.52 190.612  32
   9  -5   7 3326.69 195.503  35
   9  -6  -7 182.959 23.6428  33
   9  -6  -7 201.722 25.5535  34
   9  -6  -7 188.162 32.4379   9
   9  -6  -6 1717.86 107.325  34
   9  -6  -6 1685.23 105.469  33
   9  -6  -5 693.415 62.6696  36
   9  -6  -5 533.823 54.5734  34
   9  -6  -5 741.895 59.4664  33
   9  -6  -5 631.000 69.6427   9
   9  -6  -4 6426.91 327.258  36
   9  -6  -4 5992.89 327.207  37
   9  -6  -4 5911.54 315.089  33
   9  -6  -4 5843.97 315.478  34
   9  -6  -4 5387.02 332.614   9
   9  -6  -3 4191.43 231.423  36
   9  -6  -3 3911.00 230.800  37
   9  -6  -3 3820.86 215.930  33
   9  -6  -3 3480.62 213.672  34
   9  -6  -3 3701.09 231.858   9
   9  -6  -2 8214.35 443.101  33
   9  -6  -2 8619.17 459.342  36
   9  -6  -2 8966.47 464.588  37
   9  -6  -1 347.619 48.6577  33
   9  -6  -1 395.841 60.9881  36
   9  -6  -1 364.681 59.1571  37
   9  -6   0 947.363 95.0278  47
   9  -6   0 1010.83 97.4034  37
   9  -6   1 618.503 75.3445  37
   9  -6   2 78.6060 31.6819  37
   9   6   2 109.540 32.8073  32
   9   6   3-33.9487 29.6170  32
   9  -6   3-11.1424 24.0622  37
   9  -6   3-6.09294 26.3131  36
   9  -6   4 2313.60 163.541  36
   9   6   4 2325.25 156.262  32
   9  -6   5 576.848 64.7718  36
   9  -6   6 2975.23 178.735  36
   9   6   7 114.612 21.0391  32
   9  -7  -7 2307.10 138.602   9
   9  -7  -6 50.0810 14.3708  33
   9  -7  -6 71.8039 17.1864  34
   9  -7  -5 6403.13 310.086  36
   9  -7  -5 5601.13 299.051  34
   9  -7  -5 5363.67 296.127  33
   9  -7  -5 5885.48 320.836   9
   9  -7  -4 214.270 31.1084  33
   9  -7  -4 246.203 36.7896  36
   9  -7  -4 192.260 30.7213  34
   9  -7  -4 147.029 38.2796   9
   9  -7  -3 632.524 57.9230  33
   9  -7  -3 725.619 61.8356  34
   9  -7  -3 708.214 69.6422  36
   9  -7  -2 24.9255 21.2708  33
   9  -7  -2-4.48242 22.8082  36
   9  -7  -2 15.9000 19.1476  34
   9  -7  -2 4.87453 23.7901  37
   9  -7  -1 4642.93 268.583  33
   9  -7  -1 5694.24 300.451  47
   9  -7  -1 4847.84 290.441  37
   9  -7  -1 4970.07 287.550  36
   9  -7   0 838.094 74.3952  33
   9  -7   0 1056.08 95.7522  47
   9  -7   0 1064.38 95.7809  37
   9  -7   0 889.759 90.0811  36
   9  -7   1 325.878 54.0829  47
   9  -7   1 510.963 63.3787  37
   9  -7   1 443.339 61.8118  36
   9  -7   2 154.501 39.7385  37
   9  -7   3 6573.79 366.409  37
   9   7   3 6483.64 355.770  32
   9   7   4 4575.54 260.571  32
   9  -7   5 994.303 85.2147  36
   9   7   5 1023.04 81.3870  32
   9  -7   6 785.521 65.8695  36
   9  -8  -6 99.0585 24.0339   9
   9  -8  -5 1042.38 71.6641  34
   9  -8  -5 1024.28 87.2798   9
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   9  -8  -4 1592.53 104.799  37
   9  -8  -4 1170.40 83.9281  33
   9  -8  -4 1526.98 91.4174  34
   9  -8  -4 1304.84 102.413   9
   9  -8  -3 9786.61 496.761  34
   9  -8  -3 9670.01 493.725  33
   9  -8  -3 10290.0 509.392  36
   9  -8  -2 122.778 24.3182  33
   9  -8  -2 144.465 31.4502  36
   9  -8  -2 132.788 26.3196  34
   9  -8  -1 940.892 86.3571  47
   9  -8  -1 733.904 62.5991  33
   9  -8  -1 834.320 77.0060  36
   9  -8   0 605.101 67.4436  47
   9  -8   0 476.838 60.0559  37
   9  -8   0 514.912 60.7371  36
   9  -8   1 42.5717 24.8228  47
   9  -8   1-2.58885 17.2892  33
   9  -8   1 24.7674 26.1988  36
   9  -8   1 47.0769 27.6641  37
   9  -8   2 202.733 39.9260  47
   9  -8   2 142.797 25.1782  33
   9  -8   2 112.818 32.1215  37
   9  -8   2 184.067 39.5386  36
   9  -8   3 2224.80 152.846  37
   9  -8   3 2278.18 155.067  36
   9  -8   4 83.9414 24.8423  37
   9   8   4 115.876 27.6980  32
   9   8   5 1209.53 86.5332  32
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   9  -9  -3 2.93558 17.4242  36
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   9  -9  -2 4422.21 233.353  36
   9  -9  -2 4431.55 239.453  37
   9  -9  -2 3829.16 217.095  34
   9  -9  -1 1430.08 94.3041  33
   9  -9  -1 1699.76 100.581  34
   9  -9   0-21.1845 18.7525  33
   9  -9   0 11.8195 21.5865  36
   9  -9   0 2.15398 17.3950  34
   9  -9   0 43.3106 23.9863  47
   9  -9   1 154.141 22.7746  33
   9  -9   1 228.257 40.0437  36
   9  -9   1 204.489 40.4808  47
   9  -9   2 1980.46 141.076  37
   9  -9   2 2071.50 139.006  36
   9  -9   2 2174.39 143.893  47
   9  -9   3 8.18730 20.4100  37
   9  -9   3 3.91040 20.6789  36
   9  -9   3 19.5014 19.0373  47
   9  -9   4 5192.04 280.222  36
   9  -9   4 5049.35 278.502  37
   9  -9   5 1604.63 101.089  36
   9  -9   5 1506.73 96.5219  37
   9 -10  -4 7622.98 388.511  37
   9 -10  -3 379.848 37.8501  36
   9 -10  -3 484.862 46.0805  37
   9 -10  -2 1424.80 94.5502  36
   9 -10  -2 1474.07 100.756  37
   9 -10  -1 2109.17 129.472  36
   9 -10  -1 2103.10 135.662  37
   9 -10   0 670.084 64.4404  37
   9 -10   0 623.620 59.2326  36
   9 -10   0 803.832 71.3903  47
   9 -10   1 661.080 61.7902  36
   9 -10   1 789.132 69.9205  47
   9 -10   2 1244.76 93.2698  36
   9 -10   2 1447.55 100.551  47
   9 -10   3 371.856 42.3166  37
   9 -10   3 328.047 38.4649  36
   9 -10   3 312.368 39.4556  47
   9 -10   4 732.645 59.3892  37
   9 -10   4 810.802 60.3826  36
   9 -11  -3 1174.59 75.8700  37
   9 -11  -2 2312.36 135.278  37
   9 -11  -1 7865.48 403.128  37
   9 -11   0 370.423 35.9809  36
   9 -11   0 434.156 43.9321  37
   9 -11   1 480.477 47.5401  37
   9 -11   1 409.998 39.3503  36
   9 -11   2 1768.74 108.508  36
   9 -11   2 2010.49 118.450  47
  10   0  -4-1.90242 11.6137  33
  10   0  -3 2.20673 13.6600  33
  10   0  -3 10.3539 12.6446  34
  10   0  -2 4143.59 220.708  33
  10   0  -2 4028.16 218.605  34
  10   0  -1-21.3375 19.0202  34
  10   0   0 3152.96 175.409  33
  10   0   0 3055.03 172.627  34
  10   0   1-20.7714 21.6454  33
  10   0   2 2909.29 164.235  33
  10   0   3-2.10080 11.9006  33
  10   0   3 4.62007 13.7044  32
  10  -1  -4 784.492 55.5216  34
  10   1  -3 1630.83 101.410  33
  10  -1  -3 1765.86 103.744  34
  10   1  -2 684.548 56.6049  33
  10  -1  -2 746.300 57.2360  34
  10   1  -1 589.205 52.8901  33
  10  -1  -1 644.169 53.9297  34
  10   1   0 6268.54 325.027  33
  10   1   1 6252.98 348.515  33
  10   1   1 7517.10 355.819  32
  10   1   2 2.25751 14.7098  33
  10   1   2 10.5599 15.6644  32
  10   1   3 960.460 65.2684  33
  10  -2  -4 3666.14 194.384  33
  10  -2  -3 326.940 34.2146  33
  10  -2  -2 1646.54 103.154  33
  10  -2  -1 417.262 43.4418  33
  10  -2   0 2418.30 143.416  33
  10  -2   1 364.241 41.2600  33
  10   2   1 419.837 42.1102  32
  10  -2   2 7.10199 14.4964  33
  10   2   2 50.0937 17.5076  32
  10  -2   3 678.195 52.1366  33
  10  -3  -3 1790.29 107.823  33
  10  -3  -3 1861.19 108.394  34
  10  -3  -2 1201.41 83.1638  36
  10  -3  -2 1244.80 81.8940  33
  10  -3  -2 1293.78 82.8441  34
  10  -3  -1 9588.18 476.872  33
  10  -3  -1 9386.01 476.113  34
  10  -3   0 593.109 51.8974  33
  10  -3   0 587.228 51.2895  34
  10  -3   1 42.1419 19.7442  33
  10  -3   2-2.15397 12.9651  33
  10   3   2 4.50172 13.5483  32
  10  -3   3 116.822 19.1100  33
  10   3   3 145.585 22.0490  32
  10  -4  -3 2201.17 123.915  34
  10  -4  -2 925.989 62.9758  36
  10  -4  -2 762.898 56.6881  33
  10  -4  -2 754.969 57.7924  34
  10  -4  -1 4.13769 13.5064  33
  10  -4  -1 43.8635 15.3087  36
  10  -4  -1 12.7730 14.8747  34
  10  -4   0 597.135 49.6559  36
  10  -4   0 534.161 45.6999  33
  10  -4   0 549.019 46.4871  34
  10  -4   1 24.2091 13.6636  33
  10  -4   2 990.479 65.6420  33
  10  -5  -2 291.442 30.8914  36
  10  -5  -1 2622.76 144.268  36
  10  -5  -1 2450.69 138.971  34
  10  -5   0 1383.50 84.4931  36
  10  -5   0 1198.03 78.7810  34
  10  -5   1-13.5501 13.9083  34
   0   0   0    0.00    0.00   0
TITL 22VKh_R160_auto in P2(1)/n
REM P2(1)/n (#14 in standard setting)
CELL 1.54184   8.106830  19.200099  14.497544  90.0000  90.8104  90.0000
ZERR    5.00   0.000059   0.000146   0.000102   0.0000   0.0007   0.0000
LATT  1
SYMM -x+1/2, y+1/2,-z+1/2
SFAC C H N O S
UNIT 85.00 70.00 10.00 25.00 5.00
REM  CrysAlisPro recorded range (K): Min=99.9; max=100.0; aver:100.0
TEMP -173
TREF
HKLF 4
END
;
_shelx_hkl_checksum              37946
_shelx_res_file
;
TITL ZV2898 in P2(1)/n
CELL 1.54184   8.10683  19.20010  14.49754  90.0000  90.8104  90.0000
ZERR    4.00   0.00006   0.00015   0.00010   0.0000   0.0007   0.0000
LATT 1
SYMM 0.5-X, 0.5+Y, 0.5-Z
SFAC C H N O S
UNIT 92 68 12 36 8
TEMP -173.0
SIZE 0.11 0.12 0.33
L.S. 12
BOND $H
ACTA
CONF
WGHT    0.058800    0.926700
FVAR       2.82553
S1    5    0.741185    0.626431    0.561668    11.00000    0.01830    0.01684 =
         0.01676   -0.00100    0.00114    0.00090
S2    5    0.517388    0.680419    0.702674    11.00000    0.01788    0.01795 =
         0.01841    0.00124    0.00264    0.00142
O1    4    0.974305    0.864445    0.686650    11.00000    0.02795    0.01682 =
         0.02217   -0.00001    0.00303   -0.00192
O2    4    0.591241    0.631696    0.509394    11.00000    0.02244    0.02355 =
         0.02127   -0.00221   -0.00384    0.00365
O3    4    0.893533    0.650984    0.525725    11.00000    0.02434    0.01965 =
         0.02220   -0.00002    0.00549   -0.00060
O4    4    1.146294    0.366233    0.684995    11.00000    0.03613    0.03354 =
         0.03290    0.01169    0.00790    0.01696
O5    4    1.239880    0.466832    0.642602    11.00000    0.02089    0.03618 =
         0.04493    0.00155    0.00130    0.00404
O6    4    0.438246    0.614170    0.700083    11.00000    0.02310    0.01972 =
         0.02965    0.00427    0.00382   -0.00117
O7    4    0.546111    0.715705    0.788136    11.00000    0.02421    0.02803 =
         0.01954   -0.00114    0.00217    0.00487
O8    4    0.327878    0.963750    0.517938    11.00000    0.04309    0.02640 =
         0.04356    0.01281    0.00273    0.00813
O9    4    0.474629    0.948190    0.642509    11.00000    0.05189    0.02161 =
         0.03373   -0.00204    0.00183   -0.00100
N1    3    0.710513    0.672381    0.658140    11.00000    0.01701    0.01821 =
         0.01843   -0.00204    0.00103    0.00102
N2    3    1.127426    0.425809    0.656895    11.00000    0.02508    0.02843 =
         0.02066   -0.00015    0.00390    0.00819
N3    3    0.389515    0.926483    0.577899    11.00000    0.03241    0.02155 =
         0.02966    0.00320    0.00849    0.00503
C1    1    0.850719    0.681309    0.720305    11.00000    0.01608    0.01949 =
         0.01690   -0.00189    0.00161    0.00046
C2    1    0.943025    0.743182    0.718710    11.00000    0.01883    0.01898 =
         0.01811   -0.00084    0.00424    0.00016
C3    1    1.077892    0.747671    0.780220    11.00000    0.02058    0.02340 =
         0.02202   -0.00230    0.00155   -0.00327
AFIX  43
H3    2    1.141542    0.789205    0.782060    11.00000   -1.20000
AFIX   0
C4    1    1.120520    0.693107    0.838281    11.00000    0.02050    0.03039 =
         0.02068   -0.00049   -0.00088   -0.00028
AFIX  43
H4    2    1.214198    0.697244    0.878016    11.00000   -1.20000
AFIX   0
C5    1    1.027460    0.632378    0.838910    11.00000    0.02432    0.02452 =
         0.01838    0.00224   -0.00016    0.00349
AFIX  43
H5    2    1.056883    0.594927    0.878681    11.00000   -1.20000
AFIX   0
C6    1    0.890455    0.627233    0.780386    11.00000    0.02175    0.01890 =
         0.01944   -0.00032    0.00360   -0.00061
AFIX  43
H6    2    0.823756    0.586567    0.781497    11.00000   -1.20000
AFIX   0
C7    1    0.905652    0.802268    0.658347    11.00000    0.02051    0.01719 =
         0.02207   -0.00225    0.00487   -0.00105
C8    1    0.821976    0.812742    0.577400    11.00000    0.02431    0.01948 =
         0.02346    0.00160    0.00110   -0.00116
AFIX  43
H8    2    0.763839    0.778585    0.542429    11.00000   -1.20000
AFIX   0
C9    1    0.838252    0.884764    0.555125    11.00000    0.02646    0.02064 =
         0.02571    0.00407    0.00330    0.00068
AFIX  43
H9    2    0.792925    0.907700    0.502527    11.00000   -1.20000
AFIX   0
C10   1    0.930310    0.914128    0.623002    11.00000    0.02757    0.01851 =
         0.02567    0.00224    0.00825    0.00143
C11   1    0.984905    0.986411    0.643502    11.00000    0.03975    0.01987 =
         0.03147   -0.00038    0.00612   -0.00202
AFIX 137
H11A  2    0.924491    1.004277    0.696583    11.00000   -1.50000
H11B  2    0.962794    1.016082    0.589732    11.00000   -1.50000
H11C  2    1.103447    0.986561    0.657716    11.00000   -1.50000
AFIX   0
C12   1    0.772849    0.539250    0.594755    11.00000    0.01970    0.01734 =
         0.01786   -0.00190    0.00174    0.00132
C13   1    0.934484    0.517669    0.611634    11.00000    0.01864    0.02105 =
         0.01820   -0.00194    0.00233   -0.00066
AFIX  43
H13   2    1.024968    0.548663    0.605320    11.00000   -1.20000
AFIX   0
C14   1    0.957310    0.449133    0.637983    11.00000    0.02091    0.02214 =
         0.01717   -0.00207    0.00139    0.00442
C15   1    0.828550    0.402420    0.647287    11.00000    0.03120    0.01870 =
         0.01812   -0.00105    0.00094    0.00037
AFIX  43
H15   2    0.849099    0.355730    0.665845    11.00000   -1.20000
AFIX   0
C16   1    0.668623    0.425132    0.628958    11.00000    0.02663    0.02180 =
         0.01986   -0.00114    0.00006   -0.00596
AFIX  43
H16   2    0.578805    0.393662    0.634151    11.00000   -1.20000
AFIX   0
C17   1    0.639880    0.493870    0.603022    11.00000    0.01929    0.02252 =
         0.01905   -0.00203    0.00012   -0.00181
AFIX  43
H17   2    0.530627    0.509698    0.591068    11.00000   -1.20000
AFIX   0
C18   1    0.412015    0.737016    0.625937    11.00000    0.01672    0.01967 =
         0.02070    0.00050    0.00395    0.00302
C19   1    0.444626    0.807864    0.632079    11.00000    0.02049    0.02022 =
         0.02020   -0.00091    0.00421    0.00206
AFIX  43
H19   2    0.522517    0.825847    0.675475    11.00000   -1.20000
AFIX   0
C20   1    0.358447    0.851124    0.572072    11.00000    0.02287    0.01875 =
         0.02428    0.00190    0.00718    0.00391
C21   1    0.243702    0.826400    0.508376    11.00000    0.02166    0.02930 =
         0.02349    0.00483    0.00397    0.00715
AFIX  43
H21   2    0.188736    0.857452    0.467220    11.00000   -1.20000
AFIX   0
C22   1    0.210429    0.755670    0.505678    11.00000    0.01989    0.03115 =
         0.02501   -0.00112   -0.00059    0.00241
AFIX  43
H22   2    0.129816    0.738116    0.463544    11.00000   -1.20000
AFIX   0
C23   1    0.294622    0.710201    0.564449    11.00000    0.01818    0.02372 =
         0.02445   -0.00140    0.00206    0.00048
AFIX  43
H23   2    0.272388    0.661636    0.562664    11.00000   -1.20000
AFIX   0
HKLF 4
REM  ZV2898 in P2(1)/n
REM R1 =  0.0363 for    4547 Fo > 4sig(Fo)  and  0.0376 for all    4812 data
REM    335 parameters refined using      0 restraints
END
WGHT      0.0588      0.9267
REM Highest difference peak  0.537,  deepest hole -0.500,  1-sigma level  0.062
Q1    1   0.7492  0.5821  0.5949  11.00000  0.05    0.54
Q2    1   0.6225  0.6719  0.6779  11.00000  0.05    0.42
Q3    1   0.4847  0.7113  0.6565  11.00000  0.05    0.41
Q4    1   0.9443  0.4780  0.6079  11.00000  0.05    0.35
Q5    1   0.8227  0.8491  0.5584  11.00000  0.05    0.34
Q6    1   0.6997  0.5167  0.6008  11.00000  0.05    0.33
Q7    1   0.6578  0.4614  0.6109  11.00000  0.05    0.32
Q8    1   0.4377  0.7695  0.6207  11.00000  0.05    0.32
Q9    1   0.7238  0.6526  0.6284  11.00000  0.05    0.31
Q10   1   0.3777  0.8872  0.5789  11.00000  0.05    0.31
Q11   1   0.5318  0.6764  0.7748  11.00000  0.05    0.30
Q12   1   0.5139  0.7255  0.7434  11.00000  0.05    0.30
Q13   1   0.2168  0.7929  0.5237  11.00000  0.05    0.29
Q14   1   0.9055  0.7743  0.6959  11.00000  0.05    0.28
Q15   1   0.5003  0.6332  0.6998  11.00000  0.05    0.28
Q16   1   1.0459  0.6727  0.8473  11.00000  0.05    0.28
Q17   1   1.0981  0.7141  0.7995  11.00000  0.05    0.27
Q18   1   0.8784  0.6516  0.7451  11.00000  0.05    0.27
Q19   1   0.8856  0.7174  0.7211  11.00000  0.05    0.26
Q20   1   0.9383  0.9530  0.6314  11.00000  0.05    0.26
;
_shelx_res_checksum              61870
_shelxl_version_number           .2013
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
S S1 0.74119(4) 0.62643(2) 0.56167(2) 0.01729(11) Uani d 1 . .
S S2 0.51739(4) 0.68042(2) 0.70267(2) 0.01806(11) Uani d 1 . .
O O1 0.97431(14) 0.86445(5) 0.68665(7) 0.0223(2) Uani d 1 . .
O O2 0.59124(13) 0.63170(6) 0.50939(7) 0.0225(2) Uani d 1 . .
O O3 0.89353(13) 0.65098(5) 0.52573(7) 0.0220(2) Uani d 1 . .
O O4 1.14629(16) 0.36623(7) 0.68499(9) 0.0341(3) Uani d 1 . .
O O5 1.23988(15) 0.46683(7) 0.64260(9) 0.0340(3) Uani d 1 . .
O O6 0.43825(13) 0.61417(6) 0.70008(8) 0.0241(2) Uani d 1 . .
O O7 0.54611(13) 0.71571(6) 0.78814(7) 0.0239(2) Uani d 1 . .
O O8 0.32788(17) 0.96375(7) 0.51794(10) 0.0377(3) Uani d 1 . .
O O9 0.47463(18) 0.94819(6) 0.64251(9) 0.0357(3) Uani d 1 . .
N N1 0.71051(15) 0.67238(6) 0.65814(8) 0.0179(2) Uani d 1 . .
N N2 1.12743(17) 0.42581(7) 0.65689(9) 0.0247(3) Uani d 1 . .
N N3 0.38951(18) 0.92648(7) 0.57790(10) 0.0278(3) Uani d 1 . .
C C1 0.85072(17) 0.68131(7) 0.72031(10) 0.0175(3) Uani d 1 . .
C C2 0.94303(17) 0.74318(7) 0.71871(10) 0.0186(3) Uani d 1 . .
C C3 1.07789(18) 0.74767(8) 0.78022(10) 0.0220(3) Uani d 1 . .
H H3 1.1415 0.7892 0.7821 0.026 Uiso calc 1 . .
C C4 1.12052(19) 0.69311(9) 0.83828(11) 0.0239(3) Uani d 1 . .
H H4 1.2142 0.6972 0.8780 0.029 Uiso calc 1 . .
C C5 1.02746(19) 0.63238(8) 0.83891(10) 0.0224(3) Uani d 1 . .
H H5 1.0569 0.5949 0.8787 0.027 Uiso calc 1 . .
C C6 0.89046(18) 0.62723(7) 0.78039(10) 0.0200(3) Uani d 1 . .
H H6 0.8238 0.5866 0.7815 0.024 Uiso calc 1 . .
C C7 0.90565(18) 0.80227(8) 0.65835(10) 0.0199(3) Uani d 1 . .
C C8 0.82198(19) 0.81274(8) 0.57740(11) 0.0224(3) Uani d 1 . .
H H8 0.7638 0.7786 0.5424 0.027 Uiso calc 1 . .
C C9 0.8383(2) 0.88476(8) 0.55513(11) 0.0242(3) Uani d 1 . .
H H9 0.7929 0.9077 0.5025 0.029 Uiso calc 1 . .
C C10 0.9303(2) 0.91413(8) 0.62300(11) 0.0238(3) Uani d 1 . .
C C11 0.9849(2) 0.98641(8) 0.64350(12) 0.0303(4) Uani d 1 . .
H H11A 0.9245 1.0043 0.6966 0.045 Uiso calc 1 . .
H H11B 0.9628 1.0161 0.5897 0.045 Uiso calc 1 . .
H H11C 1.1034 0.9866 0.6577 0.045 Uiso calc 1 . .
C C12 0.77285(17) 0.53925(7) 0.59476(10) 0.0183(3) Uani d 1 . .
C C13 0.93448(18) 0.51767(8) 0.61163(10) 0.0193(3) Uani d 1 . .
H H13 1.0250 0.5487 0.6053 0.023 Uiso calc 1 . .
C C14 0.95731(18) 0.44913(8) 0.63798(10) 0.0201(3) Uani d 1 . .
C C15 0.8286(2) 0.40242(8) 0.64729(10) 0.0227(3) Uani d 1 . .
H H15 0.8491 0.3557 0.6658 0.027 Uiso calc 1 . .
C C16 0.66862(19) 0.42513(8) 0.62896(10) 0.0228(3) Uani d 1 . .
H H16 0.5788 0.3937 0.6342 0.027 Uiso calc 1 . .
C C17 0.63988(18) 0.49387(8) 0.60302(10) 0.0203(3) Uani d 1 . .
H H17 0.5306 0.5097 0.5911 0.024 Uiso calc 1 . .
C C18 0.41201(17) 0.73702(7) 0.62594(10) 0.0190(3) Uani d 1 . .
C C19 0.44463(18) 0.80786(8) 0.63208(10) 0.0203(3) Uani d 1 . .
H H19 0.5225 0.8258 0.6755 0.024 Uiso calc 1 . .
C C20 0.35845(18) 0.85112(8) 0.57207(11) 0.0219(3) Uani d 1 . .
C C21 0.24370(19) 0.82640(9) 0.50838(11) 0.0248(3) Uani d 1 . .
H H21 0.1887 0.8575 0.4672 0.030 Uiso calc 1 . .
C C22 0.21043(19) 0.75567(9) 0.50568(11) 0.0254(3) Uani d 1 . .
H H22 0.1298 0.7381 0.4635 0.030 Uiso calc 1 . .
C C23 0.29462(18) 0.71020(8) 0.56445(11) 0.0221(3) Uani d 1 . .
H H23 0.2724 0.6616 0.5627 0.027 Uiso calc 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
S1 0.01830(18) 0.01684(18) 0.01676(18) 0.00090(11) 0.00114(13) -0.00100(11)
S2 0.01788(18) 0.01795(18) 0.01841(18) 0.00142(12) 0.00264(12) 0.00124(12)
O1 0.0280(5) 0.0168(5) 0.0222(5) -0.0019(4) 0.0030(4) 0.0000(4)
O2 0.0224(5) 0.0235(5) 0.0213(5) 0.0036(4) -0.0038(4) -0.0022(4)
O3 0.0243(5) 0.0196(5) 0.0222(5) -0.0006(4) 0.0055(4) 0.0000(4)
O4 0.0361(7) 0.0335(6) 0.0329(6) 0.0170(5) 0.0079(5) 0.0117(5)
O5 0.0209(6) 0.0362(7) 0.0449(7) 0.0040(5) 0.0013(5) 0.0015(5)
O6 0.0231(5) 0.0197(5) 0.0296(6) -0.0012(4) 0.0038(4) 0.0043(4)
O7 0.0242(5) 0.0280(6) 0.0195(5) 0.0049(4) 0.0022(4) -0.0011(4)
O8 0.0431(7) 0.0264(6) 0.0436(7) 0.0081(5) 0.0027(6) 0.0128(5)
O9 0.0519(8) 0.0216(6) 0.0337(7) -0.0010(5) 0.0018(6) -0.0020(5)
N1 0.0170(6) 0.0182(6) 0.0184(6) 0.0010(4) 0.0010(4) -0.0020(4)
N2 0.0251(7) 0.0284(7) 0.0207(6) 0.0082(5) 0.0039(5) -0.0002(5)
N3 0.0324(7) 0.0216(7) 0.0297(7) 0.0050(5) 0.0085(6) 0.0032(5)
C1 0.0161(6) 0.0195(7) 0.0169(6) 0.0005(5) 0.0016(5) -0.0019(5)
C2 0.0188(6) 0.0190(7) 0.0181(6) 0.0002(5) 0.0042(5) -0.0008(5)
C3 0.0206(7) 0.0234(7) 0.0220(7) -0.0033(6) 0.0016(5) -0.0023(6)
C4 0.0205(7) 0.0304(8) 0.0207(7) -0.0003(6) -0.0009(5) -0.0005(6)
C5 0.0243(7) 0.0245(7) 0.0184(7) 0.0035(6) -0.0002(6) 0.0022(5)
C6 0.0217(7) 0.0189(7) 0.0194(7) -0.0006(5) 0.0036(5) -0.0003(5)
C7 0.0205(7) 0.0172(6) 0.0221(7) -0.0010(5) 0.0049(5) -0.0022(5)
C8 0.0243(7) 0.0195(7) 0.0235(7) -0.0012(5) 0.0011(6) 0.0016(5)
C9 0.0265(7) 0.0206(7) 0.0257(8) 0.0007(6) 0.0033(6) 0.0041(6)
C10 0.0276(7) 0.0185(7) 0.0257(7) 0.0014(6) 0.0083(6) 0.0022(6)
C11 0.0398(9) 0.0199(7) 0.0315(8) -0.0020(6) 0.0061(7) -0.0004(6)
C12 0.0197(7) 0.0173(6) 0.0179(6) 0.0013(5) 0.0017(5) -0.0019(5)
C13 0.0186(7) 0.0210(7) 0.0182(6) -0.0007(5) 0.0023(5) -0.0019(5)
C14 0.0209(7) 0.0221(7) 0.0172(6) 0.0044(5) 0.0014(5) -0.0021(5)
C15 0.0312(8) 0.0187(7) 0.0181(7) 0.0004(6) 0.0009(6) -0.0011(5)
C16 0.0266(7) 0.0218(7) 0.0199(7) -0.0060(6) 0.0001(6) -0.0011(5)
C17 0.0193(7) 0.0225(7) 0.0190(7) -0.0018(5) 0.0001(5) -0.0020(5)
C18 0.0167(6) 0.0197(7) 0.0207(7) 0.0030(5) 0.0040(5) 0.0005(5)
C19 0.0205(7) 0.0202(7) 0.0202(7) 0.0021(5) 0.0042(5) -0.0009(5)
C20 0.0229(7) 0.0187(7) 0.0243(7) 0.0039(5) 0.0072(6) 0.0019(6)
C21 0.0217(7) 0.0293(8) 0.0235(7) 0.0071(6) 0.0040(6) 0.0048(6)
C22 0.0199(7) 0.0312(8) 0.0250(7) 0.0024(6) -0.0006(6) -0.0011(6)
C23 0.0182(7) 0.0237(7) 0.0245(7) 0.0005(5) 0.0021(5) -0.0014(6)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
O2 S1 O3 . . 121.18(7) ?
O2 S1 N1 . . 105.71(6) ?
O3 S1 N1 . . 105.68(6) ?
O2 S1 C12 . . 109.40(7) ?
O3 S1 C12 . . 106.87(6) ?
N1 S1 C12 . . 107.24(6) ?
O6 S2 O7 . . 120.94(7) ?
O6 S2 N1 . . 108.91(6) ?
O7 S2 N1 . . 103.39(6) ?
O6 S2 C18 . . 108.60(7) ?
O7 S2 C18 . . 109.02(7) ?
N1 S2 C18 . . 104.78(6) ?
C10 O1 C7 . . 107.60(12) ?
C1 N1 S1 . . 117.17(9) ?
C1 N1 S2 . . 117.94(9) ?
S1 N1 S2 . . 120.70(7) ?
O4 N2 O5 . . 124.61(14) ?
O4 N2 C14 . . 117.32(13) ?
O5 N2 C14 . . 118.07(13) ?
O8 N3 O9 . . 124.14(15) ?
O8 N3 C20 . . 117.73(15) ?
O9 N3 C20 . . 118.13(13) ?
C6 C1 C2 . . 121.55(13) ?
C6 C1 N1 . . 118.27(12) ?
C2 C1 N1 . . 120.18(12) ?
C3 C2 C1 . . 116.87(13) ?
C3 C2 C7 . . 119.05(13) ?
C1 C2 C7 . . 124.08(13) ?
C4 C3 C2 . . 121.68(14) ?
C4 C3 H3 . . 119.2 ?
C2 C3 H3 . . 119.2 ?
C3 C4 C5 . . 120.55(14) ?
C3 C4 H4 . . 119.7 ?
C5 C4 H4 . . 119.7 ?
C4 C5 C6 . . 118.98(14) ?
C4 C5 H5 . . 120.5 ?
C6 C5 H5 . . 120.5 ?
C1 C6 C5 . . 120.32(13) ?
C1 C6 H6 . . 119.8 ?
C5 C6 H6 . . 119.8 ?
C8 C7 O1 . . 108.84(13) ?
C8 C7 C2 . . 136.62(14) ?
O1 C7 C2 . . 114.51(13) ?
C7 C8 C9 . . 106.95(14) ?
C7 C8 H8 . . 126.5 ?
C9 C8 H8 . . 126.5 ?
C10 C9 C8 . . 106.96(14) ?
C10 C9 H9 . . 126.5 ?
C8 C9 H9 . . 126.5 ?
C9 C10 O1 . . 109.63(13) ?
C9 C10 C11 . . 134.12(15) ?
O1 C10 C11 . . 116.20(14) ?
C10 C11 H11A . . 109.5 ?
C10 C11 H11B . . 109.5 ?
H11A C11 H11B . . 109.5 ?
C10 C11 H11C . . 109.5 ?
H11A C11 H11C . . 109.5 ?
H11B C11 H11C . . 109.5 ?
C17 C12 C13 . . 121.75(13) ?
C17 C12 S1 . . 120.58(11) ?
C13 C12 S1 . . 117.67(11) ?
C14 C13 C12 . . 116.99(13) ?
C14 C13 H13 . . 121.5 ?
C12 C13 H13 . . 121.5 ?
C13 C14 C15 . . 123.07(14) ?
C13 C14 N2 . . 117.55(13) ?
C15 C14 N2 . . 119.37(13) ?
C14 C15 C16 . . 118.73(14) ?
C14 C15 H15 . . 120.6 ?
C16 C15 H15 . . 120.6 ?
C15 C16 C17 . . 120.10(14) ?
C15 C16 H16 . . 119.9 ?
C17 C16 H16 . . 119.9 ?
C16 C17 C12 . . 119.34(14) ?
C16 C17 H17 . . 120.3 ?
C12 C17 H17 . . 120.3 ?
C19 C18 C23 . . 122.06(14) ?
C19 C18 S2 . . 118.18(12) ?
C23 C18 S2 . . 119.69(11) ?
C20 C19 C18 . . 116.97(14) ?
C20 C19 H19 . . 121.5 ?
C18 C19 H19 . . 121.5 ?
C19 C20 C21 . . 122.77(14) ?
C19 C20 N3 . . 118.00(14) ?
C21 C20 N3 . . 119.22(14) ?
C20 C21 C22 . . 118.91(15) ?
C20 C21 H21 . . 120.5 ?
C22 C21 H21 . . 120.5 ?
C21 C22 C23 . . 120.27(15) ?
C21 C22 H22 . . 119.9 ?
C23 C22 H22 . . 119.9 ?
C22 C23 C18 . . 118.97(14) ?
C22 C23 H23 . . 120.5 ?
C18 C23 H23 . . 120.5 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
S1 O2 . 1.4269(11) ?
S1 O3 . 1.4274(11) ?
S1 N1 . 1.6752(12) ?
S1 C12 . 1.7591(15) ?
S2 O6 . 1.4249(11) ?
S2 O7 . 1.4283(11) ?
S2 N1 . 1.7089(12) ?
S2 C18 . 1.7667(15) ?
O1 C10 . 1.3709(19) ?
O1 C7 . 1.3773(18) ?
O4 N2 . 1.2231(18) ?
O5 N2 . 1.2247(19) ?
O8 N3 . 1.227(2) ?
O9 N3 . 1.228(2) ?
N1 C1 . 1.4507(18) ?
N2 C14 . 1.4720(19) ?
N3 C20 . 1.471(2) ?
C1 C6 . 1.390(2) ?
C1 C2 . 1.404(2) ?
C2 C3 . 1.404(2) ?
C2 C7 . 1.462(2) ?
C3 C4 . 1.385(2) ?
C3 H3 . 0.9500 ?
C4 C5 . 1.389(2) ?
C4 H4 . 0.9500 ?
C5 C6 . 1.392(2) ?
C5 H5 . 0.9500 ?
C6 H6 . 0.9500 ?
C7 C8 . 1.362(2) ?
C8 C9 . 1.427(2) ?
C8 H8 . 0.9500 ?
C9 C10 . 1.350(2) ?
C9 H9 . 0.9500 ?
C10 C11 . 1.485(2) ?
C11 H11A . 0.9800 ?
C11 H11B . 0.9800 ?
C11 H11C . 0.9800 ?
C12 C17 . 1.393(2) ?
C12 C13 . 1.393(2) ?
C13 C14 . 1.382(2) ?
C13 H13 . 0.9500 ?
C14 C15 . 1.384(2) ?
C15 C16 . 1.390(2) ?
C15 H15 . 0.9500 ?
C16 C17 . 1.391(2) ?
C16 H16 . 0.9500 ?
C17 H17 . 0.9500 ?
C18 C19 . 1.388(2) ?
C18 C23 . 1.393(2) ?
C19 C20 . 1.385(2) ?
C19 H19 . 0.9500 ?
C20 C21 . 1.385(2) ?
C21 C22 . 1.385(2) ?
C21 H21 . 0.9500 ?
C22 C23 . 1.392(2) ?
C22 H22 . 0.9500 ?
C23 H23 . 0.9500 ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
C3 H3 O1 . 0.95 2.41 2.7460(18) 101 no
C3 H3 O4 2_756 0.95 2.31 3.226(2) 161 yes
C13 H13 O3 . 0.95 2.51 2.8637(18) 102 no
C16 H16 O2 3_666 0.95 2.53 3.0874(18) 118 yes
C19 H19 O4 2_656 0.95 2.58 2.981(2) 106 yes
C23 H23 O6 . 0.95 2.56 2.9252(19) 103 no
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
O2 S1 N1 C1 . . . . -174.19(10) ?
O3 S1 N1 C1 . . . . -44.58(11) ?
C12 S1 N1 C1 . . . . 69.16(11) ?
O2 S1 N1 S2 . . . . 29.26(10) ?
O3 S1 N1 S2 . . . . 158.87(8) ?
C12 S1 N1 S2 . . . . -87.39(9) ?
O6 S2 N1 C1 . . . . -112.41(11) ?
O7 S2 N1 C1 . . . . 17.40(12) ?
C18 S2 N1 C1 . . . . 131.55(11) ?
O6 S2 N1 S1 . . . . 43.96(10) ?
O7 S2 N1 S1 . . . . 173.77(8) ?
C18 S2 N1 S1 . . . . -72.08(9) ?
S1 N1 C1 C6 . . . . -81.02(15) ?
S2 N1 C1 C6 . . . . 76.19(15) ?
S1 N1 C1 C2 . . . . 98.73(14) ?
S2 N1 C1 C2 . . . . -104.06(13) ?
C6 C1 C2 C3 . . . . 0.4(2) ?
N1 C1 C2 C3 . . . . -179.36(12) ?
C6 C1 C2 C7 . . . . -178.88(13) ?
N1 C1 C2 C7 . . . . 1.4(2) ?
C1 C2 C3 C4 . . . . 1.5(2) ?
C7 C2 C3 C4 . . . . -179.21(14) ?
C2 C3 C4 C5 . . . . -1.6(2) ?
C3 C4 C5 C6 . . . . -0.1(2) ?
C2 C1 C6 C5 . . . . -2.1(2) ?
N1 C1 C6 C5 . . . . 177.64(13) ?
C4 C5 C6 C1 . . . . 1.9(2) ?
C10 O1 C7 C8 . . . . 0.89(16) ?
C10 O1 C7 C2 . . . . 179.24(12) ?
C3 C2 C7 C8 . . . . 158.66(17) ?
C1 C2 C7 C8 . . . . -22.1(3) ?
C3 C2 C7 O1 . . . . -19.06(19) ?
C1 C2 C7 O1 . . . . 160.19(13) ?
O1 C7 C8 C9 . . . . -0.59(17) ?
C2 C7 C8 C9 . . . . -178.40(16) ?
C7 C8 C9 C10 . . . . 0.06(18) ?
C8 C9 C10 O1 . . . . 0.49(17) ?
C8 C9 C10 C11 . . . . -176.60(17) ?
C7 O1 C10 C9 . . . . -0.86(16) ?
C7 O1 C10 C11 . . . . 176.82(13) ?
O2 S1 C12 C17 . . . . -25.39(14) ?
O3 S1 C12 C17 . . . . -158.26(11) ?
N1 S1 C12 C17 . . . . 88.80(13) ?
O2 S1 C12 C13 . . . . 154.26(11) ?
O3 S1 C12 C13 . . . . 21.39(13) ?
N1 S1 C12 C13 . . . . -91.55(12) ?
C17 C12 C13 C14 . . . . -0.6(2) ?
S1 C12 C13 C14 . . . . 179.70(10) ?
C12 C13 C14 C15 . . . . 0.4(2) ?
C12 C13 C14 N2 . . . . -179.44(12) ?
O4 N2 C14 C13 . . . . 176.14(13) ?
O5 N2 C14 C13 . . . . -4.6(2) ?
O4 N2 C14 C15 . . . . -3.7(2) ?
O5 N2 C14 C15 . . . . 175.51(14) ?
C13 C14 C15 C16 . . . . 0.3(2) ?
N2 C14 C15 C16 . . . . -179.83(13) ?
C14 C15 C16 C17 . . . . -0.9(2) ?
C15 C16 C17 C12 . . . . 0.7(2) ?
C13 C12 C17 C16 . . . . 0.1(2) ?
S1 C12 C17 C16 . . . . 179.75(11) ?
O6 S2 C18 C19 . . . . 166.10(11) ?
O7 S2 C18 C19 . . . . 32.49(13) ?
N1 S2 C18 C19 . . . . -77.64(12) ?
O6 S2 C18 C23 . . . . -11.09(14) ?
O7 S2 C18 C23 . . . . -144.70(12) ?
N1 S2 C18 C23 . . . . 105.16(12) ?
C23 C18 C19 C20 . . . . -1.9(2) ?
S2 C18 C19 C20 . . . . -179.03(10) ?
C18 C19 C20 C21 . . . . 0.3(2) ?
C18 C19 C20 N3 . . . . 179.36(12) ?
O8 N3 C20 C19 . . . . 171.70(14) ?
O9 N3 C20 C19 . . . . -8.6(2) ?
O8 N3 C20 C21 . . . . -9.2(2) ?
O9 N3 C20 C21 . . . . 170.48(14) ?
C19 C20 C21 C22 . . . . 1.5(2) ?
N3 C20 C21 C22 . . . . -177.54(13) ?
C20 C21 C22 C23 . . . . -1.8(2) ?
C21 C22 C23 C18 . . . . 0.2(2) ?
C19 C18 C23 C22 . . . . 1.7(2) ?
S2 C18 C23 C22 . . . . 178.77(11) ?