#------------------------------------------------------------------------------ #$Date: 2023-06-06 07:34:08 +0200 (Tue, 06 Jun 2023) $ #$Revision: 284383 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/27/2022752.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022752 loop_ _publ_author_name 'Karimli, Elvin G.' 'Khrustalev, Victor N.' 'Kurasova, Margarita N.' 'Akkurt, Mehmet' 'Khalilov, Ali N.' 'Bhattarai, Ajaya' 'Mamedov, İbrahim G' _publ_section_title ; Crystal structure and Hirshfeld surface analysis of (5aS,8aR)-3,5a-dimethyl-8-methyl-idene-2-oxododeca-hydro-oxireno[2',3':6,7]naphtho-[1,2-b]furan-6-yl (Z)-2-methyl-but-2-enoate extracted from Ferula persica. ; _journal_coeditor_code WM5679 _journal_issue 'Pt 5' _journal_name_full 'Acta crystallographica. Section E, Crystallographic communications' _journal_page_first 474 _journal_page_last 477 _journal_paper_doi 10.1107/S205698902300333X _journal_volume 79 _journal_year 2023 _chemical_absolute_configuration ad _chemical_formula_iupac 'C20 H26 O5' _chemical_formula_moiety 'C20 H26 O5' _chemical_formula_sum 'C20 H26 O5' _chemical_formula_weight 346.41 _chemical_name_systematic '(5aS,8aR)-3,5a-Dimethyl-8-methylidene-2-oxododecahydrooxireno[2',3':6,7]naphtho[1,2-b]furan-6-yl (Z)-2-methylbut-2-enoate' _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary difmap _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2013 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 7.11296(5) _cell_length_b 15.4597(10) _cell_length_c 16.0358(10) _cell_measurement_reflns_used 16716 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 77.339 _cell_measurement_theta_min 3.944 _cell_volume 1763.36(16) _computing_cell_refinement ; CrysAlis PRO (Rigaku OD, 2022) ; _computing_data_collection ; CrysAlis PRO (Rigaku OD, 2022) ; _computing_data_reduction ; CrysAlis PRO (Rigaku OD, 2022) ; _computing_molecular_graphics ; ORTEP-3 for Windows (Farrugia, 2012) ; _computing_publication_material ; PLATON (Spek, 2020) ; _computing_structure_refinement ; SHELXL (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, HyPix' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0243 _diffrn_reflns_av_unetI/netI 0.0173 _diffrn_reflns_limit_h_max 8 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 19755 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 77.817 _diffrn_reflns_theta_min 3.972 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_standards_decay_% 0 _diffrn_standards_interval_count 0 _diffrn_standards_interval_time 0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.757 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.674 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; (CrysAlis PRO; Rigaku OD, 2022) ; _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.305 _exptl_crystal_description prism _exptl_crystal_F_000 744 _exptl_crystal_size_max 0.21 _exptl_crystal_size_mid 0.18 _exptl_crystal_size_min 0.13 _refine_diff_density_max 0.561 _refine_diff_density_min -0.164 _refine_ls_abs_structure_details ; Flack x determined using 1576 quotients [(I^+^)-(I^-^)]/[(I^+^)+(I^-^)] (Parsons et al, 2013). ; _refine_ls_abs_structure_Flack 0.01(4) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.045 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 238 _refine_ls_number_reflns 3751 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.045 _refine_ls_R_factor_all 0.0315 _refine_ls_R_factor_gt 0.0313 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0444P)^2^+0.4585P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0819 _refine_ls_wR_factor_ref 0.0821 _reflns_number_gt 3717 _reflns_number_total 3751 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file wm5679sup1.cif _cod_data_source_block I _cod_depositor_comments 'Adding full bibliography for 2022752.cif.' _cod_database_code 2022752 _cod_database_fobs_code 2022752 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.857 _shelx_estimated_absorpt_t_max 0.908 _shelx_hkl_file ; 0 0 1 0.28 0.09 0 0 2 564.66 12.21 0 0 3 0.14 0.24 0 0 4 12.57 1.10 0 0 5 1.67 0.51 0 0 6 224.36 7.11 0 0 7 0.46 0.26 0 0 7 1.41 0.65 0 0 8 4662.14 95.56 0 0 8 4950.27 99.43 0 0 9 2.62 0.46 0 0 9 4.84 1.14 0 0 10 308.39 7.70 0 0 10 313.24 11.21 0 0 11 0.45 0.42 0 0 11 0.26 0.69 0 0 12 170.72 5.56 0 0 12 185.07 9.01 0 0 13 0.11 0.65 0 0 13 0.65 0.55 0 0 13 -0.33 0.96 0 0 14 21.17 1.77 0 0 14 21.94 2.01 0 0 14 23.51 1.77 0 0 14 17.90 3.03 0 0 15 0.86 0.75 0 0 15 0.09 0.54 0 0 15 -0.37 1.09 0 0 16 36.33 2.18 0 0 16 29.94 2.34 0 0 16 34.38 2.20 0 0 17 0.38 0.47 0 0 17 0.11 0.60 0 0 17 1.40 0.63 0 0 18 0.09 0.53 0 0 18 0.18 0.36 0 0 19 0.48 0.43 0 0 20 39.02 1.54 0 -1 0 0.21 0.09 0 -1 0 0.64 0.16 0 1 1 441.34 8.85 0 -1 -1 425.03 8.84 0 -1 1 428.12 9.29 0 -1 2 310.20 7.58 0 1 2 324.56 7.27 0 1 3 2865.59 58.66 0 1 3 2853.08 58.71 0 1 4 4.57 0.70 0 1 5 60.35 2.82 0 1 6 1621.08 35.66 0 1 7 179.53 4.41 0 -1 7 169.24 4.36 0 1 7 185.72 6.55 0 1 8 1447.53 30.26 0 1 8 1473.95 33.76 0 1 9 232.29 5.93 0 1 9 238.21 8.93 0 1 10 27.94 1.51 0 1 10 26.76 2.86 0 1 11 107.65 3.87 0 -1 11 108.76 3.96 0 1 11 113.72 6.50 0 -1 12 23.10 1.72 0 1 12 22.60 1.68 0 -1 12 22.57 1.87 0 1 12 27.45 3.27 0 -1 13 138.43 4.89 0 1 13 130.47 4.79 0 -1 13 138.21 4.95 0 -1 13 137.85 5.29 0 1 13 126.27 7.83 0 -1 14 6.86 1.04 0 1 14 8.60 1.17 0 -1 14 7.31 1.12 0 -1 14 4.89 1.11 0 1 14 7.10 2.00 0 1 15 46.54 2.48 0 -1 15 40.99 2.46 0 1 15 40.11 2.45 0 -1 15 42.25 2.55 0 -1 15 46.74 2.94 0 1 15 44.62 2.83 0 1 15 35.38 4.28 0 1 16 44.60 2.38 0 -1 16 45.51 2.50 0 1 16 47.83 2.89 0 -1 16 42.44 2.78 0 1 16 47.22 2.57 0 -1 16 44.72 2.54 0 1 17 9.77 1.05 0 -1 17 11.35 1.18 0 -1 17 11.95 1.41 0 1 17 10.68 1.32 0 -1 17 11.42 1.21 0 1 17 10.70 1.17 0 1 18 2.05 0.72 0 -1 18 1.99 0.69 0 -1 18 2.17 0.58 0 1 18 1.46 0.49 0 1 19 42.00 2.05 0 -1 19 39.80 1.96 0 -1 20 72.77 2.29 0 1 20 72.80 2.30 0 -2 0 5562.39 113.28 0 -2 0 5682.39 113.76 0 -2 1 2129.67 43.90 0 2 1 2135.34 42.84 0 -2 1 2097.76 42.85 0 -2 -1 2099.71 43.93 0 -2 2 1842.11 37.98 0 -2 2 1789.40 37.12 0 2 2 1800.92 37.11 0 -2 3 174.26 5.25 0 -2 3 169.04 4.72 0 2 3 170.45 4.69 0 -2 4 305.64 7.93 0 2 4 300.42 7.86 0 -2 5 5.16 0.83 0 2 5 2.02 0.56 0 -2 6 2340.95 49.58 0 2 6 2276.96 49.48 0 2 7 467.23 12.50 0 -2 7 477.21 12.70 0 -2 7 441.19 9.84 0 2 7 434.02 9.83 0 2 8 693.37 17.99 0 -2 8 689.58 18.02 0 -2 8 667.70 14.67 0 2 8 672.76 14.65 0 -2 9 12.01 1.79 0 2 9 10.87 1.69 0 2 9 10.87 0.86 0 -2 9 10.44 0.86 0 -2 10 6.10 0.91 0 -2 10 4.49 1.31 0 2 10 7.06 1.50 0 -2 11 158.75 5.13 0 -2 11 150.44 5.33 0 -2 11 159.72 7.97 0 2 11 162.77 7.95 0 -2 12 22.89 1.90 0 2 12 21.79 1.68 0 -2 12 22.69 1.74 0 -2 12 24.47 1.77 0 -2 12 25.96 3.20 0 2 12 21.95 2.99 0 -2 13 31.52 2.34 0 -2 13 27.97 2.06 0 2 13 28.48 2.00 0 -2 13 28.22 1.99 0 -2 13 29.98 3.70 0 2 13 27.11 3.48 0 -2 14 11.16 1.49 0 2 14 11.25 1.34 0 -2 14 11.84 1.36 0 -2 14 9.91 1.22 0 -2 14 11.89 2.46 0 2 14 13.74 2.58 0 -2 15 248.63 7.97 0 2 15 243.87 7.82 0 2 15 236.41 7.28 0 -2 15 246.68 7.49 0 2 15 241.96 7.07 0 -2 15 243.40 7.35 0 2 15 221.08 11.26 0 -2 15 252.81 12.01 0 2 16 9.58 1.30 0 -2 16 8.07 1.33 0 2 16 9.15 1.07 0 -2 16 8.79 1.15 0 2 16 10.38 1.22 0 -2 16 9.51 1.20 0 -2 17 87.24 3.85 0 2 17 90.00 3.84 0 -2 17 81.90 3.40 0 2 17 84.71 3.40 0 2 17 85.17 3.17 0 -2 17 85.09 3.43 0 -2 18 19.13 1.36 0 2 18 19.38 1.18 0 2 18 19.93 1.59 0 -2 18 18.29 1.51 0 2 19 12.01 1.08 0 -2 19 11.75 1.02 0 2 20 3.57 0.45 0 -2 20 2.38 0.39 0 -3 0 1.04 0.44 0 -3 -1 2640.18 55.34 0 -3 1 2699.85 55.32 0 3 1 2656.95 53.55 0 -3 1 2638.69 53.57 0 -3 2 3987.10 81.68 0 -3 2 3933.25 80.24 0 3 2 3943.63 80.22 0 -3 -2 4032.10 81.86 0 -3 3 5063.33 102.08 0 -3 3 4897.86 100.80 0 3 3 4959.80 100.78 0 -3 4 2799.45 60.23 0 -3 4 2897.59 59.25 0 3 4 2837.55 59.14 0 3 5 1013.79 23.16 0 -3 5 1044.51 23.30 0 3 6 39.77 2.50 0 -3 6 39.05 2.51 0 -3 7 446.13 9.98 0 3 7 444.61 9.95 0 3 7 474.15 12.73 0 -3 7 456.81 12.72 0 -3 8 165.13 4.36 0 3 8 159.60 4.31 0 3 8 156.02 6.56 0 -3 8 171.51 6.84 0 3 9 15.22 1.00 0 -3 9 14.59 1.98 0 -3 10 231.62 6.48 0 -3 10 217.45 6.70 0 -3 10 231.41 9.35 0 3 10 224.46 9.25 0 -3 -11 306.88 7.99 0 -3 11 321.21 9.05 0 -3 11 314.51 8.69 0 -3 11 334.75 8.72 0 -3 11 338.96 12.41 0 3 11 314.71 12.09 0 -3 -12 44.29 2.15 0 -3 12 53.58 4.67 0 3 12 51.91 4.57 0 -3 12 47.59 2.62 0 -3 12 45.01 2.51 0 -3 12 46.29 2.77 0 -3 13 0.33 0.74 0 3 13 1.31 1.08 0 -3 13 1.41 0.68 0 3 13 0.99 0.60 0 -3 13 0.68 0.55 0 -3 13 -0.12 0.65 0 -3 14 223.36 11.03 0 3 14 205.73 10.58 0 -3 14 219.87 7.04 0 3 14 224.12 6.87 0 -3 14 228.55 7.02 0 -3 14 227.29 7.53 0 -3 15 150.13 8.97 0 3 15 142.65 8.66 0 3 15 147.66 5.28 0 -3 15 151.44 5.46 0 -3 15 164.38 5.58 0 3 15 166.08 5.17 0 -3 15 157.66 5.96 0 3 16 16.46 1.51 0 -3 16 15.16 1.49 0 -3 16 17.96 1.58 0 3 16 15.05 1.29 0 3 16 18.58 1.77 0 -3 16 19.73 1.87 0 -3 17 10.66 1.31 0 3 17 7.70 1.00 0 -3 17 9.98 1.12 0 3 17 9.32 1.23 0 3 17 8.83 0.90 0 -3 17 11.29 1.19 0 3 18 185.26 5.71 0 -3 18 182.72 5.64 0 -3 18 185.31 5.35 0 3 19 25.45 1.51 0 -3 19 25.15 1.44 0 -3 20 52.40 1.73 0 -4 0 9.63 1.16 0 -4 1 48.53 2.63 0 -4 -1 48.56 2.68 0 -4 2 189.66 6.12 0 4 2 174.85 4.48 0 -4 2 178.70 4.52 0 -4 -2 196.94 6.33 0 -4 3 1256.33 27.68 0 -4 -3 1239.58 27.89 0 -4 3 1204.33 25.93 0 4 3 1201.73 25.86 0 -4 4 1024.76 23.64 0 -4 4 993.00 22.20 0 4 4 996.45 22.12 0 4 5 30.44 2.01 0 -4 5 30.75 2.04 0 4 6 2906.42 60.84 0 -4 6 2824.48 60.86 0 -4 7 727.35 15.49 0 4 7 774.77 18.55 0 -4 7 757.62 18.50 0 4 8 33.72 1.52 0 4 8 35.22 2.84 0 -4 8 35.37 2.90 0 -4 9 23.04 2.52 0 4 9 26.52 2.68 0 -4 10 58.70 2.74 0 -4 10 59.38 2.92 0 -4 -10 55.35 2.34 0 -4 10 56.05 2.65 0 -4 10 57.53 4.32 0 4 10 57.34 4.26 0 -4 11 163.53 5.31 0 -4 11 157.96 5.32 0 -4 11 154.35 5.55 0 -4 -11 157.34 4.79 0 -4 11 160.48 4.92 0 4 11 161.11 8.09 0 -4 11 168.95 8.25 0 -4 11 150.26 4.59 0 -4 -12 39.43 2.09 0 4 12 41.42 4.14 0 -4 12 44.82 4.30 0 -4 12 45.85 2.79 0 -4 12 39.74 1.96 0 -4 12 42.50 2.48 0 -4 12 45.57 2.58 0 -4 13 27.74 2.06 0 -4 13 28.64 2.12 0 -4 13 33.96 3.89 0 4 13 27.14 3.45 0 -4 13 32.87 2.45 0 -4 14 10.94 1.36 0 -4 14 13.20 1.47 0 4 14 14.36 1.43 0 4 14 15.88 2.78 0 -4 14 15.50 2.73 0 -4 14 11.76 1.56 0 4 15 7.54 1.11 0 -4 15 9.59 1.29 0 -4 15 9.51 1.28 0 4 15 9.00 2.10 0 -4 15 12.05 2.41 0 -4 16 13.84 1.39 0 4 16 13.94 1.34 0 -4 16 10.42 1.37 0 4 16 10.62 1.03 0 -4 16 12.30 1.32 0 4 17 63.97 3.06 0 4 17 57.07 2.64 0 -4 17 66.45 3.12 0 -4 17 62.84 2.86 0 4 18 31.95 1.90 0 -4 18 28.30 1.78 0 4 19 5.62 0.73 0 -4 19 7.07 0.74 0 -5 0 -0.12 0.42 0 -5 1 0.61 0.44 0 -5 -1 1.76 0.72 0 5 2 72.00 2.18 0 -5 2 76.30 2.26 0 -5 2 76.78 3.82 0 -5 -2 79.67 3.98 0 -5 3 142.23 4.15 0 5 3 141.82 4.10 0 -5 -3 136.71 5.82 0 -5 3 140.79 5.71 0 -5 -4 49.87 3.42 0 5 4 46.99 2.26 0 -5 4 43.44 2.24 0 -5 4 52.43 3.28 0 -5 5 145.01 5.06 0 -5 -5 137.91 6.34 0 5 5 144.85 5.01 0 -5 5 144.36 6.15 0 -5 6 274.50 8.38 0 5 6 269.81 8.28 0 -5 6 268.40 9.46 0 -5 7 57.07 3.49 0 5 7 62.70 3.56 0 -5 8 22.80 2.32 0 5 8 22.08 2.26 0 -5 -9 839.13 18.92 0 -5 9 865.53 19.93 0 5 9 879.63 22.82 0 -5 10 35.98 2.33 0 -5 10 37.26 2.19 0 -5 10 38.39 2.17 0 -5 10 35.10 1.93 0 -5 10 35.72 1.84 0 -5 10 36.59 3.40 0 5 10 35.93 3.38 0 -5 -10 36.24 1.89 0 -5 11 6.25 1.07 0 -5 -11 6.77 0.89 0 -5 11 6.62 0.98 0 -5 11 6.21 0.81 0 -5 11 5.30 0.92 0 5 11 7.22 1.67 0 -5 11 6.76 1.61 0 -5 12 236.39 7.63 0 -5 -12 238.22 6.70 0 -5 12 235.62 7.22 0 -5 12 228.44 6.45 0 -5 12 235.12 7.27 0 5 12 237.15 10.63 0 -5 12 236.49 10.61 0 -5 -13 44.63 2.31 0 5 13 38.94 4.12 0 -5 13 43.37 4.39 0 -5 13 44.99 2.68 0 -5 13 47.43 2.70 0 -5 13 42.35 2.11 0 -5 14 510.61 18.37 0 5 14 513.86 18.41 0 -5 14 555.97 13.83 0 -5 14 550.33 14.26 0 -5 14 546.19 13.82 0 5 14 535.33 13.45 0 -5 15 0.10 0.57 0 -5 15 0.23 0.69 0 -5 15 0.20 0.55 0 5 15 0.80 0.62 0 -5 16 28.07 1.99 0 -5 16 31.83 2.04 0 5 16 31.11 1.95 0 -5 16 29.00 2.13 0 -5 17 0.35 0.54 0 5 17 0.74 0.48 0 -5 17 0.46 0.50 0 5 17 0.78 0.63 0 5 18 30.61 1.80 0 -5 18 28.75 1.71 0 5 19 0.05 0.33 0 -5 19 -0.32 0.33 0 -5 19 0.25 0.31 0 -6 0 140.14 5.90 0 -6 1 602.67 16.50 0 -6 -1 648.96 16.81 0 -6 2 528.54 14.76 0 -6 -2 542.97 15.05 0 6 3 224.51 5.79 0 -6 3 233.19 5.89 0 -6 3 245.21 8.44 0 -6 -3 227.27 8.55 0 6 4 504.40 12.17 0 -6 4 520.16 12.26 0 -6 -4 523.67 15.25 0 -6 4 496.61 14.56 0 -6 5 2.15 0.59 0 6 5 3.28 0.67 0 -6 -5 1.27 0.90 0 -6 5 2.76 0.95 0 6 6 53.51 3.00 0 -6 -6 49.24 4.06 0 -6 6 56.93 3.12 0 -6 6 51.43 3.83 0 6 7 514.05 14.30 0 -6 -7 561.89 17.20 0 -6 7 527.30 14.48 0 6 8 635.11 17.45 0 -6 -8 670.09 20.41 0 -6 8 643.64 17.65 0 -6 9 635.80 15.29 0 -6 -9 632.49 14.63 0 -6 9 668.72 18.35 0 -6 -9 669.94 20.97 0 6 9 644.58 18.13 0 -6 9 643.07 15.52 0 -6 9 637.28 14.70 0 -6 10 67.66 3.18 0 -6 -10 71.53 2.88 0 6 10 71.89 4.85 0 -6 -10 69.16 5.83 0 -6 10 67.25 4.74 0 -6 10 66.05 3.28 0 -6 10 67.03 2.80 0 -6 11 47.42 2.68 0 -6 -11 45.05 2.32 0 6 11 52.52 4.35 0 -6 11 46.91 4.17 0 -6 -11 54.15 5.34 0 -6 11 44.68 2.28 0 -6 11 51.03 2.91 0 -6 12 221.25 7.25 0 -6 12 219.08 6.99 0 -6 -12 211.12 6.37 0 -6 12 219.23 10.11 0 6 12 203.50 9.81 0 -6 -12 221.02 11.70 0 -6 12 218.16 6.92 0 -6 12 213.42 6.22 0 -6 13 13.43 1.47 0 -6 -13 15.10 1.36 0 -6 13 15.57 1.72 0 -6 13 12.27 1.16 0 -6 13 15.15 1.57 0 6 13 12.87 2.36 0 -6 13 10.14 2.14 0 -6 -13 14.97 3.12 0 -6 14 0.84 0.72 0 -6 14 0.95 0.63 0 -6 14 1.16 0.62 0 -6 -14 1.76 1.37 0 -6 14 0.64 0.79 0 -6 15 10.18 1.25 0 6 15 14.37 1.38 0 -6 15 13.14 1.52 0 -6 15 11.60 1.36 0 -6 16 33.83 2.07 0 -6 16 34.42 2.27 0 6 16 34.01 1.99 0 -6 16 34.38 2.13 0 6 17 47.48 2.43 0 6 17 42.99 1.96 0 6 17 45.23 2.14 0 -6 18 6.59 0.81 0 -6 18 6.13 0.81 0 6 18 8.06 0.90 0 -6 19 31.99 1.35 0 6 19 37.06 1.54 0 -6 19 34.31 1.43 0 -7 0 -0.18 0.53 0 -7 1 610.78 16.79 0 -7 -1 583.50 16.92 0 -7 2 6.49 1.36 0 -7 -2 5.15 1.28 0 -7 3 106.35 5.51 0 -7 -3 99.66 5.64 0 -7 4 102.19 5.49 0 -7 -4 96.94 5.66 0 -7 4 90.40 3.24 0 -7 -5 27.35 3.06 0 -7 5 32.11 3.01 0 -7 5 28.51 1.89 0 7 5 25.01 1.75 0 -7 6 481.09 14.92 0 7 6 435.88 12.06 0 -7 6 465.68 12.31 0 -7 -6 459.25 15.44 0 7 7 24.74 2.19 0 -7 7 26.84 2.31 0 -7 -7 27.20 3.36 0 -7 -8 517.06 12.21 0 -7 8 527.00 13.09 0 -7 8 525.05 12.90 0 -7 8 529.55 12.41 0 -7 -8 529.33 18.08 0 7 8 511.55 14.82 0 -7 8 525.86 15.03 0 -7 8 519.36 12.70 0 -7 9 170.88 5.51 0 -7 -9 171.92 5.11 0 -7 9 178.21 5.88 0 -7 9 174.42 5.68 0 -7 9 167.22 5.18 0 -7 -9 171.75 9.52 0 7 9 156.07 7.14 0 -7 9 164.01 7.37 0 -7 -9 162.19 4.85 0 -7 9 170.03 5.15 0 -7 -10 106.24 3.88 0 -7 10 109.44 4.51 0 -7 10 110.82 4.39 0 -7 10 112.07 3.96 0 -7 -10 110.18 7.72 0 7 10 99.95 5.88 0 -7 10 119.49 6.39 0 -7 -11 42.72 2.26 0 -7 11 31.09 2.27 0 -7 11 37.59 2.52 0 -7 11 38.18 2.12 0 -7 -11 35.20 4.60 0 -7 11 30.10 3.30 0 7 11 30.03 3.26 0 -7 -12 10.48 1.18 0 -7 12 10.82 1.45 0 -7 -12 8.81 2.43 0 -7 12 11.14 2.12 0 -7 12 8.61 1.25 0 -7 12 10.25 1.15 0 -7 -13 6.60 0.99 0 -7 13 6.82 0.94 0 -7 13 6.95 1.14 0 -7 13 6.47 1.13 0 -7 13 5.67 1.14 0 -7 -13 6.72 2.21 0 -7 14 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15.65 1.49 -1 -13 4 7.67 2.17 1 -13 -4 10.79 2.66 -1 -13 5 51.60 2.74 1 -13 -5 55.66 2.68 -1 -13 5 49.70 2.27 1 -13 -5 57.11 2.80 -1 -13 5 53.36 2.70 1 -13 -5 52.05 2.59 1 -13 -5 55.17 5.70 -1 -13 5 50.83 5.16 1 -13 -5 51.15 2.88 -1 -13 5 55.68 2.64 -1 -13 5 55.06 2.87 1 -13 -5 51.53 2.69 1 -13 -6 242.35 7.14 -1 -13 6 243.35 7.20 1 -13 -6 245.18 6.84 1 -13 -6 210.53 11.99 -1 -13 6 233.83 11.67 -1 -13 6 240.11 7.25 1 -13 -6 250.41 6.96 -1 -13 6 228.52 7.35 1 -13 -6 244.04 7.37 -1 -13 6 241.44 6.81 1 -13 -6 240.13 7.11 -1 -13 6 248.61 7.38 -1 -13 7 18.18 1.61 1 -13 -7 14.48 3.00 -1 -13 7 19.51 1.76 -1 -13 7 19.07 1.62 1 -13 -7 20.10 1.66 1 -13 -7 16.44 1.33 -1 -13 7 16.79 1.54 1 -13 -7 19.06 1.58 -1 -13 7 18.97 1.75 -1 -13 8 29.05 2.15 1 -13 -8 27.79 1.88 -1 -13 8 27.69 1.99 -1 -13 8 28.16 1.98 1 -13 -8 26.38 1.82 -1 -13 8 26.59 2.02 -1 -13 8 26.06 1.84 -1 -13 9 43.48 2.58 1 -13 -9 42.63 2.23 -1 -13 9 46.72 2.52 -1 -13 9 45.08 2.48 1 -13 -9 43.95 2.27 1 -13 -9 41.40 1.98 -1 -13 9 41.32 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129.96 4.61 -1 -14 5 125.44 4.82 1 -14 -5 130.00 4.46 -1 -14 5 138.11 4.81 1 -14 -5 131.27 4.58 -1 -14 5 119.71 8.05 1 -14 -5 117.66 8.58 -1 -14 6 30.34 2.06 1 -14 -6 32.14 2.12 -1 -14 6 29.43 2.11 -1 -14 6 28.74 1.95 1 -14 -6 31.68 1.85 -1 -14 6 33.29 1.86 1 -14 -6 36.16 2.14 -1 -14 6 32.53 2.08 1 -14 -6 31.69 1.94 -1 -14 7 76.62 3.35 1 -14 -7 79.65 3.40 1 -14 -7 76.00 2.93 -1 -14 7 79.97 3.37 1 -14 -7 81.53 3.31 -1 -14 7 75.05 3.28 -1 -14 8 12.78 1.28 1 -14 -8 13.08 1.23 1 -14 -8 10.77 1.03 -1 -14 8 11.36 1.29 -1 -14 8 11.80 1.19 1 -14 -8 11.71 1.19 -1 -14 9 57.36 2.64 1 -14 -9 59.31 2.55 1 -14 -9 53.25 2.41 -1 -14 9 52.04 2.45 -1 -14 9 57.42 2.75 1 -14 -10 31.75 1.62 -1 -14 10 38.10 2.08 -1 -14 10 38.93 1.89 -1 -14 10 38.08 1.98 -1 -14 11 32.13 1.67 -1 -14 12 6.58 0.67 -1 -14 13 44.02 1.54 -1 -14 13 56.75 1.99 -1 -14 14 20.62 0.92 1 -15 12 27.83 1.30 -1 -15 -11 21.82 1.18 1 -15 11 23.40 1.28 1 -15 10 11.82 1.08 1 -15 10 13.09 1.06 -1 -15 -10 11.69 0.83 -1 -15 -10 12.73 1.02 1 -15 9 23.09 1.44 -1 -15 -9 23.52 1.54 1 -15 9 24.74 1.63 -1 -15 -9 20.71 1.36 -1 -15 -9 21.93 1.31 1 -15 9 19.82 1.43 1 -15 8 44.15 2.18 -1 -15 -8 40.36 2.23 -1 -15 -8 40.75 2.00 1 -15 8 46.38 2.39 1 -15 8 45.24 2.26 -1 -15 -8 43.94 2.06 -1 -15 -7 21.14 1.34 -1 -15 -7 25.42 1.67 1 -15 7 22.66 1.63 1 -15 7 24.16 1.77 -1 -15 -7 21.92 1.72 -1 -15 -7 21.87 1.46 -1 -15 -7 25.38 1.59 1 -15 7 22.13 1.64 -1 -15 -6 58.18 2.45 -1 -15 -6 56.48 2.64 -1 -15 -6 53.29 2.55 -1 -15 -6 53.90 2.80 -1 -15 -6 54.33 2.38 1 -15 6 54.58 2.70 -1 -15 -6 54.55 2.55 1 -15 6 53.91 2.80 1 -15 6 54.53 2.71 -1 -15 -5 20.25 1.56 1 -15 5 21.60 1.68 -1 -15 -5 20.19 1.58 1 -15 5 20.23 1.65 1 -15 5 19.52 1.70 -1 -15 -5 21.97 1.52 1 -15 5 19.57 1.42 -1 -15 -5 21.05 1.78 1 -15 4 3.06 0.85 -1 -15 -4 3.19 0.83 -1 -15 -4 3.62 0.77 1 -15 4 3.60 0.78 -1 -15 -4 4.41 0.85 1 -15 4 3.24 0.84 1 -15 4 3.16 0.81 1 -15 3 33.53 2.15 1 -15 3 33.29 2.14 -1 -15 -3 33.09 2.05 -1 -15 -3 32.28 2.01 -1 -15 -3 30.81 1.75 1 -15 3 31.45 2.07 -1 -15 -3 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46.03 2.03 -2 -12 14 38.62 1.74 -2 -12 15 58.18 1.94 -2 13 14 31.52 1.35 2 -13 14 32.93 1.37 -2 -13 -13 46.87 1.76 2 -13 13 52.77 2.11 2 -13 12 17.76 1.34 -2 -13 -12 16.70 1.19 -2 -13 -12 16.93 1.19 2 -13 11 5.79 0.90 -2 -13 -10 10.16 0.99 -2 -13 -10 7.74 0.77 2 -13 10 10.28 1.19 2 -13 9 6.30 1.06 -2 -13 -9 6.00 0.81 -2 -13 -9 6.93 0.94 -2 -13 -9 5.80 0.76 -2 -13 -9 5.69 0.88 2 -13 8 92.45 3.64 2 -13 8 89.17 3.87 -2 -13 -8 90.37 3.39 -2 -13 -8 93.11 3.50 2 -13 8 86.82 3.45 -2 -13 -8 89.40 3.43 -2 -13 -7 59.50 2.68 2 -13 7 56.16 2.79 2 -13 7 56.05 2.53 2 -13 7 58.58 3.07 -2 -13 -7 59.69 2.72 -2 -13 -7 58.73 2.52 -2 -13 -7 59.61 2.76 2 -13 7 62.26 2.87 -2 -13 -7 59.64 2.45 -2 -13 -6 14.84 1.30 -2 -13 -6 16.28 1.42 -2 -13 -6 15.42 2.91 2 -13 6 14.73 1.31 2 -13 6 15.89 1.58 -2 -13 -6 14.75 1.29 -2 -13 -6 16.11 1.44 2 -13 6 17.31 1.52 2 -13 6 12.63 1.32 -2 -13 -5 532.29 12.82 -2 -13 -5 533.84 12.99 -2 -13 -5 531.54 12.62 -2 -13 -5 500.27 19.33 2 -13 5 497.30 18.36 2 -13 5 532.29 13.60 -2 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3.11 -2 -13 -1 79.25 3.38 2 -13 1 76.11 3.39 -2 -13 -1 68.29 6.13 2 -13 1 79.08 6.38 2 -13 0 74.88 3.34 -2 -13 0 72.85 3.25 -2 -13 0 75.29 3.08 -2 -13 0 73.13 3.21 -2 -13 0 74.78 3.37 2 -13 0 70.06 2.98 2 -13 0 76.33 3.41 2 -13 0 72.41 3.23 -2 -13 0 70.34 3.21 2 -13 0 71.46 3.22 -2 -13 0 73.35 3.28 2 -13 0 72.29 3.17 -2 -13 0 67.99 3.10 -2 -13 0 74.01 6.22 2 -13 0 81.33 6.53 -2 -13 1 78.49 3.34 -2 -13 1 83.33 3.54 2 -13 -1 80.43 3.57 2 -13 -1 76.47 3.12 -2 -13 1 84.49 3.57 -2 -13 1 82.05 3.51 2 -13 -1 79.45 3.40 -2 -13 1 83.31 3.23 2 -13 -1 80.40 3.44 -2 -13 1 82.92 3.52 2 -13 -1 73.16 6.26 -2 -13 1 85.51 6.73 -2 -13 2 32.56 2.17 2 -13 -2 33.48 2.14 -2 -13 2 33.58 1.86 -2 -13 2 35.13 2.13 -2 -13 2 36.97 2.05 -2 -13 2 37.05 2.20 2 -13 -2 34.83 2.22 -2 -13 2 32.14 1.85 2 -13 -2 31.18 1.85 -2 -13 2 36.20 2.20 -2 -13 2 35.44 2.23 2 -13 -2 34.56 2.10 2 -13 -2 34.01 2.16 -2 -13 2 36.65 2.09 2 -13 -2 27.18 3.84 -2 -13 2 35.20 4.24 -2 -13 3 27.90 1.98 2 -13 -3 27.17 1.92 -2 -13 3 27.65 1.63 2 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1.37 -2 -13 6 14.59 1.54 -2 -13 6 12.80 1.19 2 -13 -6 9.70 2.37 -2 -13 7 59.34 2.84 -2 -13 7 56.91 2.48 -2 -13 7 60.85 3.09 -2 -13 7 59.74 2.75 2 -13 -7 59.55 2.57 2 -13 -7 58.02 2.73 2 -13 -7 63.22 2.94 2 -13 -7 55.41 2.70 -2 -13 8 94.96 3.68 2 -13 -8 88.07 3.35 -2 -13 8 89.43 3.46 -2 -13 8 91.50 3.86 -2 -13 8 88.11 3.68 -2 -13 9 5.57 0.92 2 -13 -9 4.55 0.70 -2 -13 9 4.56 0.76 -2 -13 9 4.87 0.90 -2 -13 9 4.61 0.93 -2 -13 9 6.73 1.05 -2 -13 10 9.86 1.16 -2 -13 10 9.95 0.97 -2 -13 10 10.03 1.12 -2 -13 10 9.46 1.15 -2 -13 10 8.92 1.05 2 -13 -11 5.74 0.64 -2 -13 11 7.83 0.90 -2 -13 11 7.35 0.94 -2 -13 11 6.24 0.70 -2 -13 12 17.79 1.17 2 13 12 17.86 1.23 2 13 13 41.35 1.60 -2 -13 14 30.66 1.24 -2 14 13 7.66 0.62 2 -14 13 7.44 0.62 2 -14 12 77.89 2.66 -2 -14 -12 74.54 2.43 2 -14 11 3.66 0.67 -2 -14 -11 3.72 0.63 -2 -14 -10 39.22 1.94 2 -14 10 44.67 2.20 -2 -14 -10 40.14 1.64 -2 -14 -10 42.44 2.10 2 -14 9 49.29 2.50 -2 -14 -9 45.14 2.02 -2 -14 -9 48.17 2.20 -2 -14 -9 47.44 2.03 -2 -14 -9 49.06 2.23 -2 -14 -8 17.03 1.30 -2 -14 -8 16.73 1.35 -2 -14 -8 17.21 1.29 2 -14 8 15.44 1.29 2 -14 8 14.25 1.39 -2 -14 -8 14.70 1.20 2 -14 8 16.18 1.30 -2 -14 -7 6.89 0.79 2 -14 7 7.40 1.09 2 -14 7 7.05 0.97 -2 -14 -7 6.07 0.87 2 -14 7 6.79 0.94 -2 -14 -7 6.69 0.93 -2 -14 -7 6.89 0.98 -2 -14 -6 15.28 1.35 -2 -14 -6 13.34 1.19 -2 -14 -6 14.70 1.36 2 -14 6 14.84 1.36 2 -14 6 14.44 1.26 2 -14 6 13.60 1.43 -2 -14 -6 14.18 1.21 2 -14 6 14.01 1.36 -2 -14 -6 15.25 1.19 -2 -14 -5 75.63 3.16 -2 -14 -5 66.67 2.88 -2 -14 -5 70.56 3.07 2 -14 5 75.54 3.13 2 -14 5 73.58 3.41 2 -14 5 69.46 3.10 -2 -14 -5 67.56 2.78 2 -14 5 68.95 3.15 -2 -14 -5 71.20 2.90 -2 -14 -4 51.31 2.29 2 -14 4 48.87 2.65 2 -14 4 45.96 2.68 2 -14 4 49.71 2.57 -2 -14 -4 51.00 2.52 -2 -14 -4 52.51 2.62 -2 -14 -4 49.48 2.48 2 -14 3 107.18 4.24 -2 -14 -3 113.38 4.10 -2 -14 -3 115.82 4.17 -2 -14 -3 103.40 3.58 2 -14 3 95.50 7.00 -2 -14 -3 98.84 7.45 2 -14 3 110.65 4.37 -2 -14 -3 113.02 4.09 2 -14 3 112.65 4.12 2 -14 3 111.77 4.19 -2 -14 -3 110.24 4.04 2 -14 3 109.52 4.15 -2 -14 -3 114.31 4.45 2 -14 2 32.10 1.86 -2 -14 -2 29.95 1.94 -2 -14 -2 27.33 1.55 2 -14 2 26.90 1.91 -2 -14 -2 34.63 2.05 2 -14 2 28.26 1.94 -2 -14 -2 29.82 1.91 2 -14 2 31.83 2.03 -2 -14 -2 28.24 3.86 2 -14 2 28.26 3.77 -2 -14 -2 33.66 2.21 2 -14 1 167.01 5.23 -2 -14 -1 164.73 5.36 -2 -14 -1 160.03 5.31 -2 -14 -1 161.85 5.62 2 -14 1 168.68 5.02 2 -14 1 162.36 5.38 -2 -14 -1 163.46 5.35 2 -14 1 167.51 5.44 -2 -14 -1 167.68 5.23 2 -14 1 166.10 5.48 -2 -14 -1 170.11 5.42 -2 -14 -1 157.46 5.00 -2 -14 -1 151.20 9.28 2 -14 1 154.80 9.22 2 -14 0 8.15 1.09 -2 -14 0 10.93 1.20 -2 -14 0 11.44 1.28 -2 -14 0 9.97 1.24 2 -14 0 10.24 1.00 -2 -14 0 10.36 1.22 -2 -14 0 10.73 1.20 2 -14 0 9.49 1.15 -2 -14 0 10.50 1.12 2 -14 0 9.99 1.21 -2 -14 0 8.72 1.12 2 -14 0 7.34 1.09 -2 -14 0 6.86 2.02 2 -14 0 7.93 2.13 -2 -14 1 162.54 5.20 -2 -14 1 156.63 5.37 2 -14 -1 167.45 5.52 2 -14 -1 155.42 4.78 2 -14 -1 161.31 5.29 -2 -14 1 160.57 5.33 -2 -14 1 167.81 5.47 -2 -14 1 158.58 4.98 -2 -14 1 171.46 5.50 2 -14 -1 158.80 5.31 2 -14 -1 160.71 9.47 -2 -14 1 147.80 9.06 -2 -14 2 33.40 2.09 -2 -14 2 32.49 1.94 -2 -14 2 30.95 1.99 2 -14 -2 36.83 2.27 -2 -14 2 31.66 2.08 2 -14 -2 32.44 2.01 -2 -14 2 32.33 2.11 -2 -14 2 30.51 1.78 -2 -14 2 33.93 2.15 2 -14 -2 30.85 2.08 2 -14 -2 33.41 2.11 2 -14 -2 29.99 4.08 -2 -14 2 29.68 3.86 -2 -14 3 114.64 3.94 -2 -14 3 116.29 4.20 -2 -14 3 110.77 4.05 2 -14 -3 119.60 4.34 -2 -14 3 108.50 3.86 -2 -14 3 119.80 4.42 -2 -14 3 112.76 3.73 2 -14 -3 110.49 4.24 -2 -14 3 98.79 7.14 2 -14 -3 106.10 7.70 -2 -14 3 112.01 4.24 -2 -14 3 115.49 4.34 2 -14 -3 112.02 4.09 -2 -14 4 49.01 2.47 -2 -14 4 48.67 2.25 -2 -14 4 46.56 2.35 2 -14 -4 52.40 2.63 2 -14 -4 51.32 2.51 -2 -14 4 47.00 2.60 -2 -14 4 47.96 2.61 2 -14 -5 71.38 3.04 -2 -14 5 73.67 3.27 2 -14 -5 70.24 3.06 -2 -14 5 67.77 2.96 -2 -14 5 68.38 2.93 2 -14 -5 68.24 3.17 -2 -14 5 67.94 3.16 -2 -14 6 16.80 1.51 2 -14 -6 17.09 1.41 -2 -14 6 17.62 1.46 -2 -14 6 17.16 1.33 2 -14 -6 17.31 1.37 -2 -14 6 15.62 1.33 2 -14 -6 18.59 1.50 2 -14 -6 15.56 1.45 -2 -14 7 5.67 0.97 -2 -14 7 7.25 1.01 2 -14 -7 5.39 0.75 -2 -14 7 5.94 0.85 2 -14 -7 5.81 0.96 2 -14 -7 3.95 0.76 -2 -14 8 16.86 1.50 -2 -14 8 14.98 1.37 -2 -14 8 15.29 1.39 -2 -14 8 15.80 1.35 -2 -14 8 14.69 1.18 2 -14 -8 16.65 1.24 -2 -14 9 44.82 2.34 -2 -14 9 43.97 2.21 -2 -14 9 43.75 2.25 -2 -14 9 43.90 2.18 -2 -14 9 44.99 1.97 2 -14 -9 43.86 1.85 -2 -14 10 37.70 1.97 -2 -14 10 38.89 1.67 -2 -14 10 41.48 2.02 -2 -14 10 42.99 2.00 2 -14 -11 3.07 0.42 -2 -14 11 3.86 0.60 -2 -14 11 2.79 0.56 2 14 12 73.21 2.41 -2 -14 12 80.68 2.59 -2 -14 13 6.88 0.55 2 -15 12 13.32 0.76 -2 15 12 12.52 0.73 2 -15 11 30.47 1.42 -2 -15 -11 27.45 1.30 -2 -15 -10 2.91 0.52 -2 -15 -10 2.13 0.35 2 -15 10 2.56 0.55 -2 -15 -10 3.78 0.60 -2 -15 -9 28.77 1.51 2 -15 9 30.75 1.72 -2 -15 -9 27.94 1.37 -2 -15 -9 31.30 1.73 -2 -15 -8 23.46 1.45 -2 -15 -8 22.11 1.35 -2 -15 -8 21.02 1.54 -2 -15 -8 20.78 1.33 -2 -15 -8 19.72 1.28 2 -15 8 21.85 1.53 -2 -15 -7 9.41 1.01 -2 -15 -7 8.10 0.92 -2 -15 -7 7.04 0.83 2 -15 7 10.48 1.04 -2 -15 -7 7.41 1.04 -2 -15 -7 8.97 0.92 -2 -15 -7 6.69 0.70 2 -15 7 6.98 1.00 2 -15 6 15.33 1.33 -2 -15 -6 13.41 1.08 -2 -15 -6 15.16 1.27 -2 -15 -6 15.63 1.34 -2 -15 -6 14.48 1.14 2 -15 6 15.85 1.32 2 -15 6 14.01 1.23 2 -15 6 14.65 1.39 2 -15 5 90.37 3.41 2 -15 5 95.75 3.78 2 -15 5 96.33 3.66 -2 -15 -5 88.06 3.32 -2 -15 -5 90.81 3.48 -2 -15 -5 98.85 3.37 -2 -15 -5 84.95 3.40 2 -15 5 93.46 3.54 2 -15 5 92.90 3.49 2 -15 4 117.81 4.17 2 -15 4 112.07 4.32 -2 -15 -4 117.61 4.43 -2 -15 -4 118.12 4.00 2 -15 4 124.06 4.37 -2 -15 -4 116.14 4.04 -2 -15 -4 112.78 4.11 2 -15 4 119.10 4.19 -2 -15 -4 118.38 4.04 2 -15 4 117.23 4.11 -2 -15 -3 16.61 1.53 -2 -15 -3 14.95 1.34 2 -15 3 17.56 1.53 -2 -15 -3 17.22 1.47 -2 -15 -3 15.57 1.36 -2 -15 -3 16.51 1.37 2 -15 3 16.57 1.41 2 -15 3 15.89 1.39 -2 -15 -2 29.48 1.89 -2 -15 -2 30.79 1.90 2 -15 2 33.38 1.99 2 -15 2 34.62 2.04 -2 -15 -2 33.52 2.01 -2 -15 -2 29.81 2.07 -2 -15 -1 38.11 2.21 -2 -15 -1 37.78 2.14 -2 -15 -1 34.45 2.20 -2 -15 -1 37.68 1.91 2 -15 1 37.03 2.25 -2 -15 -1 33.31 1.96 2 -15 1 37.49 2.05 -2 -15 -1 36.97 2.09 2 -15 1 35.66 2.11 -2 -15 0 8.31 1.10 -2 -15 0 8.99 1.10 -2 -15 0 7.92 1.10 -2 -15 0 8.92 0.99 2 -15 0 7.75 1.09 -2 -15 0 6.68 0.92 -2 -15 0 6.98 0.99 2 -15 0 7.83 1.01 -2 -15 0 8.92 1.08 2 -15 0 9.22 1.10 -2 -15 1 38.14 2.11 2 -15 -1 39.63 2.32 2 -15 -1 37.11 2.14 -2 -15 1 38.07 2.22 -2 -15 1 37.42 1.98 -2 -15 1 41.70 2.29 -2 -15 1 40.68 2.28 2 -15 -1 39.86 2.19 -2 -15 1 37.69 2.17 2 -15 -2 30.33 1.87 -2 -15 2 31.56 1.98 -2 -15 2 31.78 1.95 2 -15 -2 32.56 2.04 2 -15 -2 29.33 1.93 -2 -15 2 30.14 1.80 -2 -15 2 29.53 1.94 -2 -15 2 31.80 1.98 -2 -15 2 30.20 1.89 2 -15 -3 16.85 1.49 2 -15 -3 17.45 1.47 2 -15 -3 17.66 1.41 -2 -15 3 14.21 1.37 -2 -15 3 16.59 1.42 -2 -15 3 16.41 1.41 -2 -15 3 15.81 1.27 -2 -15 3 17.88 1.50 2 -15 -4 114.99 4.10 -2 -15 4 115.46 4.20 -2 -15 4 115.08 4.13 2 -15 -4 119.51 4.04 2 -15 -4 120.33 4.18 -2 -15 4 119.22 4.10 -2 -15 4 116.52 4.25 2 -15 -5 88.90 3.38 -2 -15 5 92.61 3.52 -2 -15 5 94.24 3.63 2 -15 -5 89.37 3.50 -2 -15 5 91.90 3.38 2 -15 -5 95.87 3.49 -2 -15 6 16.68 1.33 -2 -15 6 13.82 1.30 2 -15 -6 14.86 1.17 2 -15 -6 15.73 1.29 2 -15 -6 14.19 1.29 -2 -15 7 6.51 0.90 2 -15 -7 9.22 0.84 -2 -15 7 7.61 0.95 2 -15 -7 6.47 0.82 -2 -15 8 21.41 1.45 2 -15 -8 19.54 1.22 -2 -15 8 23.63 1.52 -2 -15 9 29.82 1.61 -2 -15 9 32.56 1.69 -2 -15 10 2.86 0.51 -2 -15 10 2.55 0.53 -2 -15 10 3.14 0.52 2 -15 -10 3.08 0.46 2 15 11 23.08 1.19 -2 -15 11 25.47 1.13 -2 -15 12 12.63 0.71 -2 -16 -10 5.57 0.56 -2 -16 -9 16.38 0.84 -2 -16 -9 17.59 1.12 -2 -16 -8 70.68 2.34 -2 -16 -8 69.18 2.64 -2 -16 -7 41.19 1.81 2 -16 7 41.34 1.86 -2 -16 -7 40.11 1.88 -2 -16 -7 37.43 1.97 2 -16 6 84.14 3.08 -2 -16 -6 91.85 3.07 -2 -16 -6 86.73 3.10 -2 -16 -6 85.77 3.04 -2 -16 -6 83.70 2.76 2 -16 6 85.36 3.04 2 -16 5 58.36 2.40 2 -16 5 58.02 2.54 -2 -16 -5 58.39 2.49 -2 -16 -5 58.37 2.30 2 -16 5 56.64 2.42 2 -16 4 37.11 1.97 2 -16 4 39.30 2.10 -2 -16 -4 39.69 1.92 2 -16 4 39.38 1.95 2 -16 4 35.82 1.92 -2 -16 -4 38.01 1.99 -2 -16 -4 39.29 2.03 -2 -16 -4 39.08 2.17 -2 -16 -3 25.11 1.61 -2 -16 -3 22.00 1.64 2 -16 3 25.48 1.60 -2 -16 -3 25.87 1.57 2 -16 3 24.34 1.63 -2 -16 -3 24.79 1.54 2 -16 3 23.91 1.56 -2 -16 -3 25.37 1.62 -2 -16 -2 7.10 0.95 -2 -16 -2 6.50 0.91 2 -16 2 7.83 1.04 -2 -16 -2 8.08 0.96 -2 -16 -2 8.54 0.96 2 -16 2 7.67 0.94 -2 -16 -2 9.96 1.05 -2 -16 -2 8.29 1.03 -2 -16 -1 31.80 1.90 -2 -16 -1 30.84 1.85 -2 -16 -1 30.27 1.56 2 -16 1 36.64 2.08 -2 -16 -1 33.04 1.99 -2 -16 -1 36.88 1.97 -2 -16 -1 33.75 1.83 -2 -16 -1 33.68 1.85 2 -16 1 31.50 1.84 2 -16 0 48.53 2.47 2 -16 0 50.18 2.48 -2 -16 0 47.54 2.12 -2 -16 0 51.65 2.49 -2 -16 0 51.29 2.26 -2 -16 0 50.56 2.36 -2 -16 0 50.04 2.43 -2 -16 0 48.71 2.30 2 -16 0 47.60 2.29 -2 -16 1 34.16 1.93 2 -16 -1 31.62 1.94 -2 -16 1 32.69 1.76 2 -16 -1 33.10 1.98 2 -16 -1 33.89 1.91 -2 -16 1 34.39 1.87 2 -16 -1 35.05 1.89 -2 -16 1 32.52 1.85 2 -16 -2 7.52 0.91 -2 -16 2 8.79 0.98 -2 -16 2 8.31 0.92 2 -16 -2 7.17 1.00 -2 -16 2 8.59 0.94 2 -16 -2 7.83 1.00 2 -16 -2 8.67 1.04 -2 -16 2 8.39 1.04 -2 -16 2 10.05 1.08 2 -16 -3 25.11 1.65 -2 -16 3 24.01 1.56 2 -16 -3 26.65 1.72 2 -16 -3 24.58 1.65 2 -16 -3 25.49 1.55 -2 -16 3 24.50 1.61 -2 -16 3 24.20 1.56 2 -16 -3 26.00 1.66 -2 -16 3 25.75 1.64 -2 -16 3 22.94 1.60 -2 -16 4 37.98 2.03 2 -16 -4 39.98 2.00 -2 -16 4 41.14 2.08 -2 -16 4 38.10 1.95 2 -16 -4 38.06 2.04 -2 -16 4 36.29 1.88 2 -16 -4 39.41 1.99 2 -16 -5 57.12 2.37 -2 -16 5 58.71 2.51 -2 -16 5 55.61 2.39 2 -16 -5 59.28 2.50 -2 -16 5 57.40 2.29 2 -16 -5 56.74 2.35 -2 -16 6 86.69 3.10 -2 -16 6 86.41 3.01 2 -16 -6 79.89 2.76 2 -16 -6 90.11 3.07 -2 -16 7 36.86 1.74 -2 -16 7 41.29 1.89 2 -16 -7 35.94 1.68 -2 -16 7 41.44 1.91 -2 -16 8 65.78 2.34 -2 -16 8 70.78 2.49 2 -16 -8 65.06 2.12 -2 -16 8 72.54 2.50 2 -16 -9 17.02 0.95 -2 -16 9 15.79 0.96 -2 -16 9 16.06 0.98 -2 -16 9 16.77 0.94 -2 -16 10 6.16 0.53 2 16 10 6.03 0.55 -2 -17 -8 24.87 1.03 -2 -17 -8 30.95 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12.59 1.88 -4 -7 0 12.58 1.87 -4 -7 0 16.80 1.29 4 -7 0 14.36 1.24 4 -7 0 13.98 1.29 4 -7 -1 590.93 14.44 4 -7 -1 617.84 14.57 4 -7 -1 627.03 18.61 4 -7 -1 624.96 14.08 4 -7 -1 596.96 14.46 4 7 1 630.00 14.52 -4 -7 1 594.49 14.15 -4 7 -1 621.17 17.89 -4 -7 1 586.50 16.98 -4 -7 1 613.70 13.90 4 -7 -1 597.84 14.26 4 -7 -2 19.58 1.55 -4 -7 2 18.16 1.37 4 7 2 17.55 1.41 4 -7 -2 18.29 2.56 4 -7 -2 17.53 1.29 4 -7 -2 19.75 1.52 -4 -7 2 17.52 2.11 -4 7 -2 19.00 2.45 4 -7 -2 18.27 1.43 -4 -7 2 17.24 1.22 4 -7 -3 127.98 4.44 -4 -7 3 121.01 5.92 -4 7 -3 126.11 6.79 4 -7 -3 128.18 4.56 4 -7 -3 134.43 4.61 4 7 3 132.24 4.48 -4 -7 3 128.20 4.29 4 -7 -3 135.81 7.05 4 -7 -3 135.67 4.22 4 -7 -3 134.01 4.50 -4 -7 3 132.64 4.44 4 7 3 129.00 4.40 -4 -7 3 133.74 4.08 -4 -7 4 116.49 4.10 -4 7 -4 116.20 6.63 -4 -7 4 115.82 5.71 4 -7 -4 114.49 4.24 4 -7 -4 116.93 4.22 -4 -7 4 105.97 3.88 4 -7 -4 110.90 6.36 4 -7 -4 120.10 3.83 4 -7 -4 115.24 4.11 4 7 4 122.66 4.18 -4 -7 4 116.41 3.68 -4 -7 5 19.41 1.52 -4 7 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9.30 1.24 -4 -7 10 11.17 1.37 4 7 10 12.37 1.23 -4 -7 10 9.17 0.87 4 7 10 11.81 1.49 4 7 11 66.14 3.39 4 7 11 63.53 2.86 -4 -7 11 67.19 3.33 -4 -7 11 66.91 3.22 4 7 12 137.26 5.10 -4 -7 12 134.22 4.80 -4 -7 12 131.11 4.92 4 7 12 138.68 4.52 -4 -7 13 150.09 5.05 4 7 13 154.76 5.27 -4 -7 13 159.96 5.29 -4 -7 14 9.76 1.04 -4 -7 14 8.97 0.88 -4 -7 14 9.71 1.10 4 7 14 8.70 1.05 4 7 15 11.96 1.02 -4 -7 15 14.19 1.07 -4 -7 16 24.24 1.16 4 7 16 24.58 1.16 4 8 -16 22.03 1.02 -4 8 15 16.03 1.00 -4 8 15 16.96 1.11 -4 -8 -14 46.70 1.79 -4 8 14 52.15 2.17 4 -8 13 3.43 0.76 -4 -8 -13 3.73 0.61 -4 8 13 3.83 0.72 4 -8 12 47.37 2.56 4 -8 12 47.76 2.11 -4 -8 -12 49.81 2.17 -4 8 12 50.60 2.42 4 -8 11 28.63 2.05 -4 8 11 26.80 1.77 4 -8 11 25.98 1.55 -4 -8 -11 28.33 1.64 -4 -8 -10 132.12 4.21 4 -8 10 124.05 4.85 4 -8 10 128.71 4.10 4 -8 10 127.97 4.58 -4 -8 -10 123.44 3.86 4 -8 9 37.43 1.92 -4 -8 -9 39.67 2.07 4 -8 8 7.02 0.85 4 -8 8 6.59 0.98 -4 -8 -7 122.58 3.82 4 -8 7 131.76 4.90 4 -8 7 124.13 4.42 4 -8 7 115.23 3.81 4 -8 7 124.54 3.81 4 -8 7 114.65 6.23 4 8 -7 114.02 6.93 -4 -8 -6 140.79 4.30 4 -8 6 144.58 5.21 4 -8 6 134.04 4.67 -4 -8 -6 139.58 4.37 4 -8 6 138.46 4.45 4 -8 6 145.78 4.87 4 -8 6 142.88 4.31 4 -8 6 129.56 6.92 4 8 -6 143.40 8.03 4 -8 5 38.04 2.08 4 -8 5 39.71 2.02 4 -8 5 39.50 2.14 4 -8 5 38.34 2.18 -4 -8 -5 43.12 2.09 4 -8 5 37.91 2.37 4 -8 5 39.03 2.09 4 -8 5 44.09 2.05 4 -8 5 37.46 3.61 -4 -8 -5 39.58 2.01 -4 -8 -5 40.86 1.99 4 -8 5 39.92 2.28 4 -8 4 50.64 2.41 4 -8 4 48.71 2.44 4 -8 4 48.22 2.35 4 -8 4 49.79 2.54 -4 -8 -4 50.55 2.35 4 -8 4 49.00 2.58 4 -8 4 46.17 2.26 4 -8 4 50.74 2.69 4 -8 4 52.93 2.33 4 -8 4 49.65 4.28 -4 -8 -4 49.14 2.26 -4 -8 -4 50.21 2.31 4 -8 3 206.65 5.79 4 -8 3 204.42 9.22 4 -8 3 199.26 6.16 4 -8 3 199.43 6.26 4 -8 3 193.47 5.83 4 -8 3 207.02 5.96 4 8 -3 204.94 6.46 4 -8 3 196.86 6.21 4 -8 3 199.80 6.09 4 -8 3 206.71 6.03 -4 -8 -3 209.18 5.90 -4 -8 -3 203.77 5.78 -4 -8 -3 204.98 5.75 4 -8 2 38.29 1.98 4 -8 2 37.81 3.72 4 -8 2 36.44 2.18 4 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207.90 9.22 4 -8 -3 197.59 6.14 -4 -8 3 201.76 5.99 4 -8 -3 204.84 6.21 -4 -8 3 205.76 5.69 -4 -8 3 201.96 5.77 4 -8 -4 53.59 2.74 -4 -8 4 53.54 2.48 4 8 4 50.96 2.50 -4 -8 4 51.09 2.56 4 -8 -4 47.50 2.51 4 -8 -4 53.89 2.72 4 -8 -4 53.03 2.33 4 -8 -4 56.96 4.46 -4 -8 4 50.77 2.23 -4 -8 4 49.74 2.29 4 -8 -5 37.19 2.25 -4 -8 5 40.64 2.12 4 8 5 39.80 2.16 -4 -8 5 39.33 2.26 4 -8 -5 39.48 2.19 4 -8 -5 41.79 2.38 4 -8 -5 38.34 1.94 4 -8 -5 35.59 3.53 -4 -8 5 38.87 1.87 -4 -8 5 39.91 1.99 4 -8 -6 132.90 6.97 4 -8 -6 141.30 4.32 4 -8 -6 140.08 4.85 -4 -8 6 141.88 4.55 4 8 6 136.25 7.87 4 -8 -6 143.36 4.92 -4 -8 6 146.15 4.99 -4 -8 6 135.87 4.15 -4 -8 6 137.55 4.33 4 8 6 144.84 4.75 4 -8 -6 147.45 4.70 -4 -8 7 117.67 3.83 -4 -8 7 122.56 4.09 4 8 7 108.30 6.84 4 -8 -7 125.15 3.83 4 -8 -7 116.74 6.26 -4 -8 7 120.18 4.53 4 -8 -7 119.18 4.32 4 -8 -7 125.00 4.44 4 8 7 129.40 4.38 -4 -8 8 5.75 0.69 -4 -8 8 5.74 1.02 4 8 8 7.26 0.97 -4 -8 8 6.74 0.84 4 -8 -8 7.92 1.00 4 -8 -8 5.51 0.92 -4 -8 8 7.59 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4 -9 6 83.79 3.77 4 -9 6 78.27 3.31 4 -9 6 82.68 3.31 4 -9 6 83.07 3.01 4 -9 6 78.56 5.26 4 -9 6 85.17 3.53 4 -9 6 77.41 3.06 4 9 -6 76.65 5.84 4 -9 5 107.61 3.99 4 -9 5 115.11 4.16 -4 -9 -5 113.58 3.89 4 -9 5 112.86 4.45 4 -9 5 112.74 3.98 4 -9 5 113.53 3.88 4 -9 5 112.18 6.57 4 -9 5 110.55 3.76 4 -9 5 112.07 3.87 4 -9 5 112.25 4.25 -4 -9 -5 109.11 3.76 4 -9 4 299.44 8.12 4 -9 4 319.17 8.65 -4 -9 -4 309.82 8.14 4 -9 4 317.31 8.11 4 9 -4 312.02 8.85 4 -9 4 308.59 8.74 -4 -9 -4 296.15 8.01 -4 -9 -4 302.05 7.98 4 -9 4 311.65 8.22 4 -9 4 308.33 8.32 4 -9 4 298.35 8.14 4 -9 4 303.49 8.45 4 -9 4 310.31 7.98 4 -9 4 313.59 12.00 4 -9 3 382.00 9.41 4 -9 3 366.17 13.55 4 -9 3 367.84 9.46 4 9 -3 370.18 10.13 4 -9 3 361.60 9.57 4 -9 3 380.11 10.03 -4 -9 -3 380.26 9.60 -4 -9 -3 382.97 9.46 -4 -9 -3 375.28 9.42 4 -9 3 367.57 9.89 4 -9 3 378.50 9.84 4 -9 3 368.11 9.67 4 -9 2 115.98 4.32 4 -9 2 115.72 4.26 4 9 -2 115.30 4.41 4 -9 2 115.41 4.34 4 -9 2 117.85 4.04 -4 -9 -2 117.68 4.13 4 -9 2 119.28 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9.95 1.14 4 -9 -8 8.96 1.07 -4 -9 9 73.93 3.40 4 -9 -9 71.78 2.94 4 9 9 77.11 3.13 -4 -9 9 78.54 3.06 -4 -9 10 10.28 1.00 -4 -9 10 9.85 1.22 4 9 10 9.43 1.05 -4 -9 11 11.85 1.24 4 9 11 9.79 1.02 4 9 11 11.21 1.36 4 9 12 10.70 1.25 -4 -9 12 9.38 1.08 -4 -9 13 11.91 1.04 4 9 13 11.60 1.16 -4 -9 13 14.96 1.19 -4 -9 14 42.78 1.74 4 9 14 40.94 1.88 -4 -9 14 40.12 1.81 4 9 15 8.95 0.67 -4 -9 15 10.55 0.74 -4 -9 15 9.91 0.69 -4 10 14 35.01 1.50 -4 10 14 31.19 1.27 4 10 -14 33.45 1.43 -4 10 13 71.10 2.49 -4 -10 -13 71.45 2.40 4 10 -13 74.01 2.67 -4 10 12 41.31 1.92 -4 -10 -12 42.21 1.86 -4 10 11 9.00 0.96 -4 -10 -11 9.01 0.92 -4 -10 -10 15.73 1.23 -4 -10 -10 16.37 1.13 4 -10 9 47.20 2.03 -4 -10 -9 47.32 2.30 -4 -10 -9 50.51 2.22 4 -10 8 13.83 1.32 -4 -10 -8 15.86 1.29 -4 -10 -8 16.93 1.36 4 -10 8 14.83 1.11 -4 -10 -7 182.80 5.22 4 -10 7 181.86 5.18 4 -10 7 197.91 6.32 4 -10 7 182.02 5.73 4 -10 6 59.92 2.83 4 -10 6 63.77 2.86 4 10 -6 62.47 3.14 4 10 -6 61.39 5.23 4 -10 6 68.37 3.08 4 -10 6 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0.19 0.62 -4 -10 4 1.05 0.59 -4 -10 4 0.74 0.60 -4 -10 4 1.91 0.65 4 -10 -4 0.61 0.60 4 -10 -5 519.79 13.11 4 10 5 564.55 13.04 4 -10 -5 544.33 13.45 -4 -10 5 535.83 13.10 4 -10 -5 540.57 13.44 -4 -10 5 534.99 12.73 -4 -10 5 522.92 13.25 -4 -10 6 61.52 2.99 -4 -10 6 61.43 2.86 4 10 6 63.46 5.30 4 -10 -6 63.76 2.84 4 10 6 67.59 2.87 4 -10 -6 65.99 3.09 -4 -10 6 62.42 2.61 4 -10 -6 59.30 2.97 -4 -10 7 187.00 5.70 -4 -10 7 185.56 5.26 -4 -10 7 187.97 6.01 4 -10 -7 178.70 5.77 4 -10 -7 187.94 5.86 4 10 7 188.15 5.63 -4 -10 8 15.34 1.47 -4 -10 8 17.84 1.39 4 -10 -8 17.78 1.46 4 -10 -8 17.19 1.42 4 10 8 16.34 1.36 -4 -10 9 46.03 2.53 -4 -10 9 47.68 2.23 4 -10 -9 46.84 2.24 4 10 9 49.81 2.33 4 10 10 14.68 1.22 -4 -10 10 17.82 1.49 4 10 11 9.54 0.94 4 10 11 8.72 1.13 -4 -10 11 7.54 1.00 -4 -10 11 7.76 0.97 4 10 12 45.46 2.29 -4 -10 12 41.70 2.08 4 10 13 79.34 2.91 -4 -10 13 75.09 2.65 -4 -10 13 75.05 2.71 4 10 14 33.70 1.52 -4 -10 14 33.89 1.45 -4 -10 14 33.55 1.47 -4 -10 14 35.51 1.43 -4 11 14 48.51 1.61 4 11 -13 24.40 1.18 -4 -11 -13 23.77 1.13 -4 11 12 5.11 0.61 -4 -11 -12 5.48 0.66 4 11 -12 5.47 0.69 -4 11 11 15.87 1.12 4 11 -11 17.66 1.29 -4 -11 -11 17.00 1.18 -4 -11 -10 41.53 1.95 4 11 -10 37.96 2.06 -4 -11 -10 34.91 1.67 -4 -11 -9 19.10 1.23 4 11 -9 20.57 1.58 -4 -11 -9 19.83 1.41 -4 -11 -9 20.97 1.35 4 11 -8 212.18 6.47 -4 -11 -8 213.04 6.04 -4 -11 -8 214.08 5.97 -4 -11 -7 77.85 2.86 4 11 -7 78.27 3.43 -4 -11 -7 81.36 3.15 -4 -11 -6 130.97 4.33 4 11 -6 136.07 4.81 -4 -11 -6 129.05 4.13 4 -11 6 126.41 4.42 4 -11 6 131.13 4.43 4 -11 5 123.55 4.20 4 11 -5 130.57 4.66 4 -11 5 120.19 4.14 4 -11 5 117.72 4.08 -4 -11 -5 128.31 4.14 4 -11 5 121.99 4.28 4 -11 5 122.76 4.39 4 -11 4 42.38 2.30 -4 -11 -4 46.64 2.36 4 11 -4 50.55 2.63 4 -11 4 44.21 2.30 4 -11 4 45.22 2.36 -4 -11 -4 44.04 2.23 4 -11 4 43.76 2.30 4 -11 4 44.92 2.50 4 -11 3 7.95 1.06 -4 -11 -3 7.45 1.03 4 11 -3 8.27 1.09 4 -11 3 7.95 1.08 4 -11 3 13.19 1.28 -4 -11 -3 8.99 1.06 4 -11 3 8.34 1.00 4 -11 3 14.54 1.49 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1.20 4 -11 -3 11.22 1.30 4 -11 -3 7.13 0.87 4 -11 -3 8.87 1.23 -4 -11 3 7.15 1.03 4 11 3 8.66 1.02 -4 -11 3 8.29 1.07 4 -11 -3 9.74 1.25 4 -11 -4 50.54 2.71 4 -11 -4 49.00 2.59 4 -11 -4 47.24 2.68 -4 -11 4 46.15 2.52 4 11 4 49.15 2.38 -4 -11 4 45.64 2.29 -4 -11 4 47.35 2.47 4 -11 -5 122.97 4.64 4 -11 -5 127.22 4.46 4 -11 -5 125.18 4.67 -4 -11 5 132.96 4.66 -4 -11 5 129.41 4.64 4 11 5 127.62 4.27 -4 -11 5 130.36 4.24 -4 -11 5 121.61 4.39 4 -11 -6 136.97 4.73 4 -11 -6 127.52 4.40 -4 -11 6 130.83 4.46 -4 -11 6 129.02 4.68 -4 -11 6 132.05 4.22 4 -11 -6 132.80 4.73 4 11 6 136.36 4.40 4 11 7 84.15 3.15 -4 -11 7 80.03 3.17 -4 -11 7 80.71 3.43 4 -11 -7 75.84 3.28 4 -11 -7 80.86 3.34 4 11 8 210.37 5.86 -4 -11 8 204.04 5.80 4 -11 -8 198.71 5.94 4 -11 -8 210.44 6.00 -4 -11 8 199.76 6.22 -4 -11 9 22.45 1.64 4 -11 -9 19.83 1.36 4 11 9 19.44 1.33 -4 -11 9 20.55 1.53 -4 -11 10 39.66 2.10 4 -11 -10 36.62 1.66 4 11 10 36.64 1.81 -4 -11 10 41.44 2.08 -4 -11 11 18.10 1.30 4 11 11 17.13 1.43 -4 -11 11 18.68 1.35 4 11 12 5.11 0.76 -4 -11 12 3.89 0.63 -4 -11 13 25.53 1.24 4 11 13 24.90 1.34 -4 -11 14 42.46 1.44 -4 -11 14 47.64 1.53 -4 -12 -13 12.99 0.69 -4 12 13 12.45 0.73 -4 -12 -12 3.18 0.49 4 12 -12 3.49 0.44 -4 12 12 2.98 0.39 -4 -12 -11 13.30 0.96 4 12 -11 13.43 0.96 -4 12 11 10.84 0.81 -4 -12 -10 64.32 2.41 4 12 -10 69.26 2.54 -4 12 10 56.82 2.21 -4 -12 -10 56.81 2.12 -4 -12 -9 7.48 0.75 4 12 -9 8.08 0.92 -4 -12 -9 8.29 0.89 -4 -12 -9 7.18 0.80 -4 -12 -8 66.25 2.50 4 12 -8 64.65 2.75 -4 -12 -8 58.10 2.48 -4 -12 -7 172.72 4.86 4 12 -7 168.56 5.36 -4 -12 -7 170.42 5.13 -4 -12 -7 186.34 5.25 -4 -12 -6 49.77 2.26 -4 -12 -6 54.64 2.48 -4 -12 -6 51.40 2.37 4 12 -6 57.06 2.66 -4 -12 -5 233.25 6.40 4 12 -5 227.72 6.69 4 -12 5 227.18 6.44 -4 -12 -5 229.41 6.36 4 -12 5 231.17 6.66 4 12 -4 15.31 1.37 4 -12 4 14.24 1.38 4 -12 4 14.03 1.30 4 -12 4 16.18 1.34 4 -12 4 13.69 1.27 -4 -12 -4 17.64 1.36 4 -12 4 14.44 1.40 4 12 -3 55.41 2.66 -4 -12 -3 52.73 2.58 4 -12 3 56.96 2.70 4 -12 3 53.71 2.75 4 -12 3 55.38 2.70 4 -12 3 55.25 2.66 -4 -12 -3 54.68 2.55 4 -12 3 51.95 2.76 4 12 -2 12.21 1.22 4 -12 2 12.89 1.31 4 -12 2 10.54 1.26 -4 -12 -2 9.69 1.16 4 -12 2 10.42 1.24 4 -12 2 12.51 1.32 -4 -12 -2 11.95 1.18 4 -12 2 10.05 1.28 4 12 -1 103.02 3.82 -4 -12 -1 103.62 3.88 -4 -12 -1 103.98 3.80 4 -12 1 101.52 4.04 4 -12 1 94.79 3.94 -4 -12 -1 96.28 3.52 4 -12 1 100.99 3.96 4 -12 1 100.97 4.04 4 -12 0 21.87 1.76 4 -12 0 22.89 1.78 -4 -12 0 22.22 1.69 4 -12 0 21.05 1.81 -4 -12 0 24.07 1.70 4 -12 0 21.15 1.78 4 -12 0 22.22 1.81 -4 -12 0 23.91 1.60 4 12 0 23.44 1.64 4 -12 -1 99.64 4.02 4 -12 -1 104.43 4.04 -4 -12 1 103.33 3.89 4 -12 -1 97.53 4.04 4 -12 -1 88.41 3.94 -4 -12 1 102.92 3.78 4 12 1 100.27 3.71 4 -12 -1 106.78 4.14 4 -12 -2 11.74 1.36 4 12 2 12.74 1.16 -4 -12 2 10.02 1.14 -4 -12 2 10.83 1.16 4 -12 -2 11.53 1.29 4 -12 -2 9.67 1.24 -4 -12 3 53.67 2.64 4 12 3 56.38 2.50 4 -12 -3 53.30 2.75 -4 -12 3 51.65 2.34 4 -12 -3 54.18 2.78 4 -12 -3 55.56 2.87 4 -12 -3 56.85 2.91 -4 -12 3 53.27 2.53 -4 -12 3 53.69 2.64 -4 -12 4 15.34 1.41 4 12 4 13.95 1.19 -4 -12 4 15.46 1.25 4 -12 -4 14.39 1.40 4 -12 -4 16.07 1.47 4 -12 -4 15.21 1.50 4 -12 -4 15.42 1.53 -4 -12 4 14.32 1.26 -4 -12 4 15.93 1.40 -4 -12 5 228.08 6.76 4 12 5 233.23 6.33 -4 -12 5 228.31 6.42 4 -12 -5 221.15 6.73 4 -12 -5 226.51 6.59 4 -12 -5 229.55 6.91 -4 -12 5 231.05 6.56 4 -12 -5 238.60 6.90 -4 -12 5 222.37 6.31 -4 -12 6 49.70 2.26 -4 -12 6 51.97 2.45 4 -12 -6 47.76 2.52 -4 -12 6 52.55 2.63 4 -12 -6 56.10 2.70 4 -12 -6 50.15 2.58 -4 -12 6 56.26 2.51 4 12 6 55.37 2.37 4 -12 -7 171.68 5.38 -4 -12 7 178.07 5.30 4 -12 -7 172.39 5.38 4 -12 -7 172.84 5.35 -4 -12 7 178.35 5.50 -4 -12 7 179.69 5.58 -4 -12 7 175.12 5.15 4 12 7 172.82 5.01 4 12 8 64.30 2.47 -4 -12 8 59.09 2.42 -4 -12 8 62.99 2.78 -4 -12 8 65.48 2.87 -4 -12 8 62.23 2.67 4 -12 -8 65.20 2.65 4 -12 -8 64.65 2.68 -4 -12 9 6.87 0.90 -4 -12 9 6.67 0.93 -4 -12 9 7.83 0.94 4 12 9 7.39 0.78 4 -12 -9 7.17 0.80 4 -12 -10 57.46 2.05 -4 -12 10 67.31 2.61 -4 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2 -3 74.98 6.07 -5 -2 3 78.43 5.57 5 -2 -3 82.83 5.53 5 2 3 74.70 5.57 5 2 4 2.72 0.73 -5 -2 4 2.57 1.09 -5 2 -4 1.50 1.24 5 2 4 0.59 1.02 5 -2 -4 1.60 0.88 -5 -2 4 2.50 0.61 -5 -2 4 3.06 0.71 5 -2 -4 1.54 0.64 5 2 4 2.66 0.59 5 2 4 2.23 0.52 5 -2 -4 2.38 0.62 5 2 5 25.57 1.97 5 -2 -5 27.33 2.02 5 2 5 25.39 1.65 -5 -2 5 27.16 3.27 5 -2 -5 23.13 2.91 5 2 5 27.89 3.27 5 -2 -5 24.50 1.59 -5 -2 5 28.93 1.90 -5 -2 5 28.47 1.86 5 2 6 36.29 2.40 5 2 6 37.17 1.99 -5 -2 6 37.80 3.86 5 -2 -6 33.28 3.42 5 2 6 39.71 3.82 5 -2 -6 40.25 1.97 -5 -2 6 38.85 2.27 -5 -2 6 41.39 2.34 5 2 7 111.69 3.84 -5 -2 7 106.30 6.63 5 2 7 112.79 4.59 5 2 7 106.04 3.51 5 -2 -7 99.60 5.91 5 2 7 100.51 6.09 -5 -2 7 108.08 4.23 5 2 8 63.86 2.59 5 2 8 67.94 3.49 -5 -2 8 70.74 3.31 -5 -2 8 68.52 5.22 5 2 8 67.49 2.86 -5 -2 9 67.34 5.28 5 2 9 75.95 2.85 5 2 9 78.12 3.86 -5 -2 9 77.60 3.59 5 2 9 76.80 3.13 -5 -2 9 84.34 3.55 5 2 10 38.72 1.88 -5 -2 10 35.35 2.39 -5 -2 10 37.23 2.21 -5 -2 10 45.35 4.19 5 2 10 36.50 2.06 -5 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174.56 8.54 5 -4 9 174.73 5.98 5 -4 9 176.85 5.34 5 -4 8 19.40 1.70 -5 4 8 20.00 2.74 5 -4 7 211.97 9.12 5 4 -7 220.85 9.88 -5 4 7 216.41 9.84 -5 -4 -7 237.77 6.17 5 -4 7 244.67 7.20 5 -4 6 196.21 6.10 -5 4 6 194.57 9.05 -5 -4 -6 187.72 5.36 5 -4 6 194.08 5.62 5 -4 6 185.73 8.54 5 4 -6 179.17 8.99 5 -4 6 201.42 5.95 5 4 -6 187.63 6.30 5 -4 5 142.61 4.89 -5 -4 -5 141.82 8.87 -5 4 5 151.81 7.86 5 4 -5 149.88 5.31 5 -4 5 150.58 4.74 5 -4 5 143.04 7.56 5 4 -5 148.65 8.19 -5 -4 -5 149.00 4.50 5 -4 5 156.68 5.02 -5 -4 -4 69.57 2.80 5 -4 4 72.78 3.09 -5 4 4 68.33 5.18 -5 -4 -4 73.45 6.11 5 4 -4 67.44 3.20 5 -4 4 71.03 2.95 5 -4 4 71.02 3.04 5 -4 4 67.98 2.91 5 -4 4 77.74 5.37 5 4 -4 71.07 5.65 5 -4 3 60.08 2.73 5 -4 3 54.40 2.67 -5 -4 -3 55.99 2.48 5 4 -3 56.28 2.81 5 4 -3 58.18 2.86 5 -4 3 52.81 2.55 5 -4 3 53.00 4.50 -5 -4 -3 54.70 5.10 -5 4 3 58.46 4.82 5 4 -3 63.23 5.31 -5 -4 -2 33.68 3.95 -5 4 2 32.49 3.62 5 -4 2 33.01 2.00 5 -4 2 29.83 1.95 5 4 -2 34.80 2.09 -5 -4 -2 31.07 1.79 5 -4 2 31.35 1.84 -5 -4 -2 31.93 1.70 5 -4 2 26.98 1.81 5 4 -2 31.86 3.84 5 -4 2 30.29 3.44 5 4 -2 32.82 2.04 5 4 -1 57.24 2.76 -5 -4 -1 58.03 2.61 5 4 -1 55.81 2.72 5 -4 1 64.69 2.96 5 4 -1 60.33 5.27 -5 -4 -1 64.62 5.27 -5 4 1 55.86 4.76 -5 -4 -1 59.20 2.51 -5 -4 0 30.87 1.78 5 -4 0 30.17 1.94 5 4 0 29.98 1.92 5 -4 0 33.67 2.02 5 4 0 26.69 3.56 -5 4 0 33.29 3.76 -5 -4 0 35.21 3.83 5 -4 0 33.56 3.58 -5 -4 0 33.01 1.90 5 4 0 31.04 1.94 -5 -4 1 55.62 2.59 5 4 1 57.31 2.68 5 -4 -1 54.82 2.70 5 -4 -1 55.30 2.67 -5 4 -1 65.01 5.36 -5 -4 1 49.60 4.47 5 -4 -1 51.04 4.48 -5 -4 1 55.65 2.54 5 4 2 30.68 1.89 -5 -4 2 32.20 1.91 5 4 2 32.24 1.94 5 4 2 29.29 1.86 5 -4 -2 31.99 2.04 5 4 2 30.60 3.77 -5 4 -2 36.20 4.06 -5 -4 2 33.27 3.56 5 -4 -2 31.91 3.50 5 -4 -2 36.24 2.09 5 -4 -3 57.81 2.74 5 4 3 60.71 2.75 5 -4 -3 57.81 2.89 5 4 3 64.23 5.40 5 4 3 56.27 2.78 -5 4 -3 65.84 5.59 -5 -4 3 50.12 4.41 5 -4 -3 59.04 4.71 -5 -4 3 62.84 2.80 5 -4 -4 69.98 3.04 5 -4 -4 67.21 3.21 5 4 4 66.77 2.96 5 4 4 83.14 6.10 -5 -4 4 74.05 3.15 5 -4 -4 77.68 5.39 -5 -4 4 67.73 5.07 -5 4 -4 65.95 5.80 5 4 4 73.27 3.30 -5 4 -5 138.67 8.78 -5 -4 5 138.22 7.51 5 4 5 150.37 5.34 5 -4 -5 148.64 4.86 -5 -4 5 155.64 5.11 5 -4 -5 137.87 7.49 5 4 5 164.05 8.61 5 -4 -5 158.37 5.40 5 4 5 146.07 4.89 -5 -4 6 196.17 9.08 5 4 6 192.02 6.42 5 -4 -6 189.94 5.65 -5 -4 6 195.40 6.06 5 4 6 189.67 5.84 5 -4 -6 189.13 6.30 5 -4 -6 183.90 8.55 5 4 6 185.77 9.16 5 4 7 241.74 7.54 5 -4 -7 231.38 6.42 5 -4 -7 240.27 7.40 5 4 7 231.25 6.66 -5 -4 7 229.41 10.08 5 -4 -7 221.82 9.36 5 4 7 225.90 9.96 5 4 8 21.13 1.59 -5 -4 8 18.82 2.68 5 4 8 19.41 1.86 -5 -4 8 18.55 1.62 5 4 9 177.98 5.44 -5 -4 9 165.31 5.51 5 4 9 181.38 6.27 -5 -4 9 176.84 5.66 5 4 10 54.80 2.58 -5 -4 10 49.62 2.63 -5 -4 10 51.16 2.60 -5 -4 11 6.75 0.98 -5 -4 11 4.07 0.81 -5 -4 11 4.89 0.71 5 4 11 5.05 0.87 -5 -4 12 55.73 2.69 -5 -4 12 54.15 2.49 5 4 12 65.90 3.21 -5 -4 12 62.36 2.43 -5 -4 12 58.82 2.55 -5 -4 13 137.30 3.99 5 4 13 142.67 4.84 -5 -4 13 135.88 4.40 5 -4 -14 0.43 0.43 -5 -4 14 0.08 0.27 5 4 14 0.50 0.52 -5 -4 14 0.22 0.32 -5 -4 14 0.40 0.39 -5 -4 15 11.10 0.84 5 4 15 12.34 1.01 5 4 16 15.65 0.87 5 4 16 18.15 0.96 -5 5 16 9.73 0.63 -5 5 15 3.04 0.52 5 5 -15 2.39 0.40 5 -5 15 2.57 0.51 -5 5 14 18.05 1.30 -5 5 14 16.66 1.03 5 5 -14 18.02 1.19 5 -5 14 19.23 1.34 -5 5 13 47.53 1.93 5 -5 13 49.17 2.46 -5 5 13 48.83 2.06 -5 5 13 49.75 2.37 5 5 -13 45.50 2.26 -5 -5 -12 92.49 2.91 -5 5 12 91.60 3.11 5 -5 12 93.49 3.74 5 -5 12 98.91 3.90 -5 5 12 88.17 3.24 -5 5 12 99.76 3.74 5 5 -12 93.50 3.67 5 -5 11 31.14 2.09 -5 5 11 31.84 1.65 -5 -5 -11 29.61 1.54 -5 5 11 31.43 2.06 -5 5 11 25.90 1.64 5 -5 10 3.44 0.88 -5 -5 -10 3.70 0.64 -5 5 10 3.67 0.64 5 -5 9 106.17 4.31 -5 5 9 105.67 6.36 5 -5 9 110.94 4.55 5 5 -8 7.56 1.13 -5 5 8 6.00 1.58 5 -5 8 4.70 1.03 -5 -5 -8 6.19 0.73 5 -5 8 5.90 1.07 5 -5 7 16.79 1.64 5 5 -7 18.78 1.66 5 -5 7 14.71 1.47 -5 5 7 18.57 2.60 -5 -5 -7 18.15 1.25 5 -5 7 13.54 2.09 5 -5 7 15.79 1.16 5 -5 6 70.85 3.41 5 5 -6 75.26 3.42 5 -5 6 78.68 3.10 5 -5 6 73.67 3.29 -5 -5 -6 69.28 6.03 -5 5 6 80.63 5.47 5 -5 6 75.91 5.14 5 -5 6 71.64 2.81 5 5 -6 72.59 5.60 -5 -5 -6 70.86 2.77 5 -5 5 81.15 5.42 -5 -5 -5 74.88 6.14 -5 5 5 68.22 5.04 -5 -5 -5 70.80 2.75 5 -5 5 67.99 3.24 5 5 -5 62.24 5.37 5 -5 5 68.94 2.96 5 -5 5 74.33 3.03 5 5 -5 68.02 3.23 5 -5 5 67.71 3.06 5 -5 4 64.40 4.97 -5 5 4 64.03 4.89 -5 -5 -4 70.30 5.80 5 -5 4 62.53 2.86 5 5 -4 63.78 5.48 5 5 -4 59.79 2.97 5 -5 4 61.05 2.94 5 -5 4 63.46 2.83 -5 -5 -4 64.59 2.62 5 -5 4 59.88 2.73 5 -5 3 7.03 1.02 5 5 -3 8.76 1.13 -5 -5 -3 6.69 0.89 5 5 -3 8.15 1.08 5 -5 3 6.79 0.97 5 5 -3 7.46 2.08 5 -5 3 5.00 1.54 -5 -5 -3 6.07 1.83 -5 5 3 5.70 1.56 5 -5 3 6.61 0.95 -5 -5 -3 6.97 0.82 5 -5 2 191.94 5.94 -5 -5 -2 188.74 5.48 -5 -5 -2 202.20 9.86 -5 5 2 189.13 9.07 5 -5 2 182.13 5.66 5 5 -2 193.90 5.98 5 -5 2 200.91 6.04 5 5 -2 190.16 6.08 -5 -5 -2 195.69 5.70 5 -5 2 192.35 9.26 5 5 -2 187.49 9.90 5 5 -1 388.94 10.03 -5 -5 -1 390.62 14.53 -5 5 1 389.81 14.25 5 5 -1 389.10 15.35 5 5 -1 381.30 10.19 -5 -5 -1 394.57 9.88 5 5 0 3.55 0.71 -5 -5 0 3.02 0.67 -5 5 0 2.39 1.19 -5 -5 0 3.20 1.28 5 -5 0 2.59 0.74 5 5 0 1.40 1.16 5 -5 0 1.71 1.18 -5 -5 0 2.73 0.70 5 5 0 2.34 0.67 5 -5 -1 381.69 10.04 -5 -5 1 400.44 10.02 -5 5 -1 389.94 14.73 -5 -5 1 373.55 14.01 5 -5 -1 390.09 14.32 5 -5 -1 409.38 10.34 5 5 1 388.35 10.18 -5 -5 1 397.84 10.05 -5 -5 2 193.06 5.96 5 5 2 194.94 6.04 5 5 2 202.40 6.09 5 -5 -2 201.64 6.11 -5 -5 2 196.92 5.95 -5 5 -2 202.10 10.07 -5 -5 2 199.62 9.18 5 -5 -2 204.18 9.43 5 -5 -2 200.92 6.15 5 5 2 200.02 10.23 -5 -5 3 6.87 0.98 -5 5 -3 5.43 1.68 -5 -5 3 8.69 1.79 5 -5 -3 6.26 0.98 5 5 3 10.66 2.31 5 -5 -3 8.63 1.84 5 -5 -3 7.73 1.01 5 5 3 8.79 1.04 -5 -5 4 59.54 2.87 5 -5 -4 65.29 3.08 5 -5 -4 70.61 5.16 5 5 4 74.46 5.83 5 -5 -4 65.55 2.99 -5 -5 4 65.16 2.99 -5 -5 4 67.88 4.94 -5 5 -4 65.10 5.61 -5 5 -5 65.11 5.74 -5 -5 5 64.57 4.87 5 5 5 74.51 3.45 5 -5 -5 67.26 5.01 5 5 5 67.15 5.52 5 -5 -5 70.58 3.26 -5 -5 5 71.17 3.20 5 -5 -5 69.59 3.05 5 -5 -6 73.02 3.08 5 -5 -6 73.78 3.41 -5 5 -6 75.61 6.23 -5 -5 6 73.61 5.16 5 -5 -6 83.39 5.40 5 5 6 64.68 5.29 5 5 6 74.62 3.59 5 5 7 18.71 1.81 5 -5 -7 18.56 1.66 5 5 7 20.28 1.54 5 -5 -7 17.35 1.36 -5 -5 7 17.94 1.20 -5 -5 7 19.18 2.59 5 5 7 14.33 2.38 5 -5 -7 19.22 2.49 5 -5 -7 18.20 1.25 -5 -5 8 5.75 0.98 5 5 8 7.71 1.29 -5 -5 8 5.48 0.69 5 -5 -8 7.18 1.09 5 5 8 6.21 0.94 5 -5 -9 111.88 4.46 5 5 9 122.23 4.21 -5 -5 9 104.44 4.16 5 5 9 120.57 4.84 -5 -5 9 111.89 6.51 -5 -5 9 120.93 4.33 5 -5 -10 4.45 0.90 5 5 10 4.40 0.81 -5 -5 10 2.98 0.73 -5 -5 10 5.07 0.80 -5 -5 10 3.54 0.63 -5 -5 10 3.98 0.73 -5 -5 10 2.76 0.71 -5 -5 11 30.79 1.63 5 5 11 27.80 1.78 5 -5 -11 30.21 2.00 -5 -5 11 26.84 1.85 -5 -5 11 32.88 1.89 -5 -5 11 29.62 1.79 5 -5 -12 89.67 3.55 -5 -5 12 92.05 3.55 -5 -5 12 95.31 3.12 -5 -5 12 90.58 3.32 -5 -5 12 92.40 3.28 5 5 12 95.95 3.95 -5 -5 13 48.82 2.28 5 5 13 52.74 2.60 -5 -5 13 45.29 2.03 -5 -5 14 17.70 1.17 5 5 14 19.10 1.39 -5 -5 14 16.53 1.01 5 5 15 3.36 0.57 5 5 16 8.22 0.59 5 6 -15 33.22 1.46 -5 6 15 36.15 1.51 -5 6 14 10.03 0.91 5 -6 14 9.62 0.93 5 6 -14 8.16 0.68 -5 6 13 10.38 0.77 5 6 -13 9.90 0.92 5 -6 13 11.26 1.13 -5 6 13 10.04 0.84 -5 6 13 10.47 1.05 5 6 -12 16.94 1.32 -5 6 12 18.39 1.49 -5 6 12 17.77 1.23 -5 -6 -12 18.78 1.13 -5 6 12 19.22 1.15 5 -6 12 20.54 1.34 5 -6 12 21.47 1.66 -5 6 11 16.97 1.46 5 6 -11 16.02 1.38 5 -6 11 15.21 1.19 -5 6 11 14.64 1.08 -5 -6 -11 15.32 1.11 5 -6 10 213.85 6.74 5 6 -10 222.44 6.65 5 -6 10 211.60 6.05 -5 6 10 217.18 5.84 -5 -6 -10 225.93 5.97 5 -6 9 5.18 1.05 5 6 -9 5.30 0.93 5 -6 9 4.32 0.77 5 -6 9 5.41 0.99 5 6 -8 51.35 2.74 -5 -6 -8 48.19 4.89 -5 6 8 57.07 4.36 5 -6 8 53.98 2.97 5 -6 8 51.09 2.44 5 -6 8 58.26 2.91 5 -6 7 140.57 5.29 5 6 -7 147.61 5.14 5 -6 7 147.58 4.36 5 -6 7 133.78 6.89 -5 -6 -7 139.05 8.59 -5 6 7 142.23 7.32 5 -6 7 148.88 5.13 -5 -6 -7 149.43 4.46 -5 -6 -7 147.49 4.33 -5 -6 -6 34.24 1.82 -5 -6 -6 35.58 1.80 5 -6 6 32.53 2.24 5 6 -6 33.15 2.13 5 -6 6 32.20 1.97 5 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377.05 9.37 5 -6 1 44.47 2.54 5 -6 1 47.59 2.51 5 -6 1 45.92 2.55 -5 -6 -1 48.71 2.40 5 6 -1 45.07 2.35 -5 -6 -1 46.31 2.26 -5 -6 -1 45.85 4.23 -5 6 1 41.11 3.98 5 6 -1 53.03 5.13 -5 -6 -1 49.44 2.29 -5 -6 0 256.43 7.06 5 6 0 269.52 12.29 -5 -6 0 250.35 6.91 5 -6 0 230.08 10.60 5 -6 0 241.50 7.31 5 -6 0 248.05 7.22 5 -6 0 237.85 7.20 -5 6 0 249.23 10.64 -5 -6 0 250.81 10.51 5 -6 -1 44.73 2.32 -5 -6 1 49.37 2.48 5 -6 -1 53.07 4.60 5 -6 -1 51.73 2.68 5 -6 -1 47.08 2.58 -5 6 -1 45.16 4.30 -5 -6 1 47.55 4.15 -5 6 -2 364.77 14.04 -5 -6 2 351.86 13.00 5 -6 -2 365.80 9.61 -5 -6 2 372.32 9.69 5 -6 -2 393.80 14.18 5 -6 -2 383.71 9.97 5 6 2 376.90 15.14 -5 -6 3 13.72 1.15 -5 -6 3 13.46 1.30 5 -6 -3 13.59 1.29 -5 -6 3 12.57 1.27 -5 -6 3 12.33 2.07 5 6 3 17.24 3.00 5 -6 -3 14.15 2.33 -5 6 -3 11.84 2.27 5 -6 -3 15.58 1.49 5 -6 -3 12.09 1.34 5 -6 -4 91.38 3.72 -5 -6 4 92.48 3.30 -5 -6 4 90.21 3.61 5 -6 -4 90.96 3.67 -5 -6 4 97.25 3.77 5 -6 -4 98.05 6.19 -5 -6 4 83.10 5.42 -5 6 -4 90.59 6.50 5 6 4 90.34 6.64 -5 -6 5 15.53 1.19 -5 -6 5 17.69 1.49 5 6 5 13.96 1.34 5 -6 -5 18.10 1.50 -5 -6 5 17.71 1.53 5 6 5 16.50 2.84 5 -6 -5 17.86 2.58 5 -6 -5 17.39 1.30 5 -6 -5 17.09 1.49 -5 -6 5 13.94 2.14 -5 6 -5 12.35 2.47 5 -6 -6 31.25 3.29 5 -6 -6 32.03 1.76 -5 -6 6 33.83 1.73 -5 -6 6 28.93 1.93 5 -6 -6 30.82 2.04 5 6 6 34.22 2.07 -5 6 -6 24.29 3.46 -5 -6 6 31.09 3.20 5 -6 -6 32.04 1.97 5 6 6 32.75 2.34 5 6 6 34.05 3.78 5 6 7 151.59 5.53 -5 -6 7 153.64 5.12 -5 -6 7 153.96 4.98 5 -6 -7 150.78 5.16 5 -6 -7 145.12 4.76 -5 -6 7 142.89 4.24 -5 -6 7 145.37 4.38 -5 -6 7 136.21 7.15 5 -6 -7 150.61 4.43 5 6 7 150.76 7.98 -5 6 -8 51.92 4.97 -5 -6 8 48.04 3.98 -5 -6 8 49.09 2.47 -5 -6 8 51.05 2.63 5 -6 -8 52.78 2.37 5 6 8 58.37 3.16 5 -6 -8 51.15 2.68 -5 -6 8 48.48 2.55 5 -6 -9 5.81 0.91 -5 -6 9 6.63 0.99 5 6 9 8.02 1.27 -5 -6 9 5.83 0.84 -5 -6 9 4.86 0.82 -5 -6 9 7.41 1.03 -5 -6 10 215.90 6.22 5 -6 -10 216.72 6.41 -5 -6 10 197.10 6.26 -5 -6 10 212.68 5.68 -5 -6 10 212.45 5.90 -5 -6 10 206.99 6.10 -5 -6 11 13.80 1.19 -5 -6 11 14.51 1.23 -5 -6 11 15.63 1.35 -5 -6 12 17.70 1.40 5 6 12 18.96 1.63 -5 -6 12 18.16 1.29 5 6 13 11.49 1.21 -5 -6 13 10.19 0.87 5 6 14 9.35 0.95 -5 -6 14 8.07 0.65 5 6 15 35.63 1.53 -5 7 15 10.66 0.69 -5 7 14 91.79 2.94 -5 7 13 21.37 1.36 -5 -7 -13 19.17 0.98 5 -7 13 23.45 1.50 5 7 -12 46.31 2.00 5 -7 12 51.13 2.10 -5 7 12 52.86 2.40 -5 -7 -12 50.57 1.96 5 -7 12 54.09 2.57 5 -7 11 65.43 2.48 -5 -7 -11 64.54 2.41 -5 -7 -10 27.52 1.56 5 -7 10 27.17 1.59 -5 7 10 25.53 1.36 5 7 -10 24.53 1.63 5 -7 9 28.91 2.12 5 -7 9 28.92 1.71 -5 7 9 29.74 1.52 5 7 -9 30.05 1.88 5 -7 8 282.64 7.55 5 -7 8 289.49 8.41 5 7 -8 282.35 7.87 5 7 -7 84.40 3.51 5 -7 7 87.60 3.07 5 -7 7 94.54 4.01 -5 -7 -7 92.50 3.11 -5 -7 -7 92.07 3.20 5 7 -6 2.72 0.69 5 -7 6 3.13 0.75 5 7 -6 2.56 1.27 5 -7 6 1.99 0.95 5 -7 6 3.05 0.60 5 -7 6 3.28 0.68 -5 -7 -6 3.60 0.66 -5 -7 -6 3.51 0.63 5 -7 6 3.01 0.84 5 -7 5 61.85 2.78 5 -7 5 63.16 2.88 5 -7 5 63.33 3.10 5 7 -5 62.84 5.42 5 -7 5 65.72 2.70 5 -7 5 64.74 4.88 5 -7 5 66.13 2.99 5 7 -5 59.59 2.83 -5 -7 -5 67.22 2.74 -5 -7 -5 65.08 2.64 -5 -7 -4 111.78 6.88 5 -7 4 112.19 6.81 5 -7 4 117.91 4.02 5 7 -4 124.72 4.28 5 -7 4 117.98 4.27 5 -7 4 115.01 4.24 5 -7 4 114.70 4.41 -5 -7 -4 122.03 3.95 5 -7 4 115.01 4.34 5 7 -4 121.21 7.84 -5 -7 -4 121.66 4.04 -5 -7 -4 125.16 4.04 -5 7 3 114.93 6.34 -5 -7 -3 113.41 6.82 5 -7 3 117.93 4.34 5 -7 3 117.31 4.30 5 -7 3 118.58 4.31 5 7 -3 118.51 7.82 5 -7 3 119.70 7.06 5 -7 3 113.96 4.02 -5 -7 -3 114.69 3.94 5 -7 3 117.57 4.39 5 7 -3 118.78 4.14 -5 -7 -3 122.94 4.04 -5 7 2 245.63 9.97 -5 -7 -2 239.07 10.35 5 -7 2 247.28 7.29 5 -7 2 253.54 7.22 5 -7 2 250.63 7.28 5 7 -2 253.00 12.07 5 -7 2 247.03 7.06 5 -7 2 238.03 10.81 5 -7 2 265.19 7.05 -5 -7 -2 242.07 6.86 5 -7 2 258.45 7.48 5 7 -2 241.06 6.91 -5 -7 -2 254.66 6.88 5 -7 1 139.43 4.94 5 -7 1 140.60 5.02 5 -7 1 142.39 5.00 -5 -7 -1 152.56 4.86 5 7 -1 140.96 8.79 -5 -7 -1 146.99 4.73 5 -7 1 147.30 5.20 -5 -7 -1 132.99 7.21 -5 7 1 143.98 7.33 -5 -7 -1 148.00 4.63 -5 -7 0 846.16 19.14 5 7 0 832.53 26.21 -5 -7 0 850.77 19.08 5 -7 0 802.21 24.17 5 -7 0 844.61 18.98 -5 7 0 824.21 23.40 -5 -7 0 807.42 23.04 5 -7 0 844.54 19.46 5 -7 0 829.12 19.47 -5 -7 1 144.92 4.84 5 -7 -1 137.87 7.86 5 -7 -1 150.93 4.80 -5 7 -1 139.55 7.45 -5 -7 1 145.82 7.24 5 -7 -1 147.31 5.11 5 -7 -1 148.91 5.14 -5 -7 1 139.89 4.57 -5 -7 2 242.52 6.70 5 7 2 251.97 7.21 5 -7 -2 250.41 10.84 5 -7 -2 253.33 6.87 5 7 2 229.85 7.07 -5 -7 2 234.16 9.59 -5 7 -2 226.97 10.17 5 7 2 245.68 11.89 5 -7 -2 249.00 7.32 -5 -7 3 123.02 4.01 -5 -7 3 114.15 4.21 5 -7 -3 119.54 4.11 5 7 3 117.76 4.31 5 -7 -3 108.94 6.81 5 -7 -3 117.89 4.08 -5 -7 3 117.61 6.26 -5 7 -3 111.06 6.86 5 7 3 127.94 8.21 5 -7 -3 123.12 4.52 5 -7 -3 118.84 4.51 -5 -7 4 116.75 3.88 -5 -7 4 112.83 4.17 5 7 4 113.65 4.23 5 -7 -4 113.18 4.08 -5 -7 4 117.36 4.34 5 -7 -4 120.88 7.03 5 -7 -4 120.89 4.04 5 -7 -4 122.91 4.52 5 -7 -4 118.56 4.40 -5 -7 4 112.26 6.09 5 7 4 129.01 8.13 5 7 5 61.75 5.42 -5 -7 5 62.99 2.58 -5 -7 5 67.14 2.72 -5 -7 5 63.53 2.91 5 -7 -5 61.13 2.94 5 7 5 67.53 3.00 5 -7 -5 60.17 2.79 5 -7 -5 62.96 4.89 5 -7 -5 65.00 2.72 5 -7 -6 2.63 0.73 -5 -7 6 2.46 0.58 -5 -7 6 2.52 0.67 5 7 6 2.57 1.23 5 -7 -6 1.51 0.83 5 -7 -6 2.85 0.59 -5 -7 6 2.88 0.59 5 -7 -6 2.86 0.70 5 7 6 2.78 0.71 -5 -7 7 93.06 3.18 -5 -7 7 89.60 3.48 5 -7 -7 89.76 3.49 5 -7 -7 89.23 3.13 5 7 7 94.93 4.17 5 7 7 95.50 3.62 5 -7 -7 88.96 3.54 -5 -7 7 91.30 3.68 -5 -7 8 289.27 8.03 5 -7 -8 285.46 7.60 5 7 8 295.16 8.71 -5 -7 8 287.91 7.73 5 7 8 293.29 7.93 -5 -7 9 31.17 1.75 5 7 9 29.94 1.86 -5 -7 9 30.05 1.84 5 7 10 27.03 1.72 -5 -7 10 25.65 1.63 5 7 11 62.67 2.64 -5 -7 11 63.55 2.54 -5 -7 11 64.20 2.62 5 7 12 55.83 2.70 -5 -7 12 49.71 2.14 5 7 13 24.96 1.59 -5 -7 13 20.82 1.16 5 7 14 95.01 3.06 -5 -7 14 85.76 2.64 5 7 15 10.30 0.71 5 8 -14 17.02 0.99 -5 8 14 15.74 0.93 -5 -8 -13 8.97 0.63 5 8 -13 11.06 0.97 -5 8 13 11.44 0.92 -5 -8 -12 18.82 1.11 5 -8 12 20.02 1.44 -5 8 12 18.63 1.29 5 -8 11 39.07 1.76 -5 -8 -11 36.15 1.72 5 -8 10 212.78 5.75 -5 -8 -10 216.18 5.81 5 -8 9 27.45 1.59 -5 -8 -9 29.81 1.68 5 -8 9 25.72 1.92 5 -8 8 47.27 2.69 5 -8 8 49.43 2.24 5 -8 7 37.35 2.35 5 8 -7 37.20 2.43 5 -8 7 32.65 1.66 -5 -8 -7 34.02 1.70 -5 -8 -6 34.83 1.81 -5 -8 -6 33.68 1.85 5 8 -6 38.40 2.45 5 8 -6 28.51 3.63 5 -8 6 36.01 1.92 5 -8 6 35.45 2.28 5 -8 6 36.26 2.11 5 -8 6 32.99 1.77 5 -8 6 34.27 3.43 -5 -8 -5 35.24 1.96 -5 -8 -5 37.24 1.94 5 8 -5 35.51 2.38 5 8 -5 31.37 3.96 -5 -8 -5 36.24 1.89 5 -8 5 40.58 2.17 5 -8 5 36.34 2.31 5 -8 5 41.90 2.34 5 -8 5 39.97 2.01 5 -8 5 38.78 3.78 5 -8 4 103.36 3.72 5 -8 4 114.35 6.78 5 -8 4 109.35 4.20 5 -8 4 112.19 4.07 5 -8 4 112.54 4.04 5 8 -4 113.49 4.47 5 -8 4 111.55 4.22 -5 -8 -4 105.74 3.73 -5 -8 -4 107.03 3.80 -5 -8 -4 105.39 3.72 5 8 -4 100.17 7.19 5 -8 3 1.93 0.65 5 -8 3 3.43 0.81 5 -8 3 1.94 0.74 -5 -8 -3 0.97 0.55 5 -8 3 1.72 0.64 -5 -8 -3 1.74 0.58 5 8 -3 1.12 0.63 5 8 -3 1.12 1.23 5 -8 3 1.44 1.01 5 -8 3 1.14 0.52 5 -8 3 2.30 0.71 -5 -8 -3 2.85 0.64 5 -8 2 166.41 5.53 5 8 -2 174.03 5.90 5 -8 2 173.52 5.82 -5 -8 -2 174.35 5.36 5 8 -2 166.51 9.74 5 -8 2 178.75 5.39 5 -8 2 183.21 9.04 5 -8 2 170.06 5.68 5 -8 2 175.28 5.60 -5 -8 -2 178.26 5.33 -5 -8 -2 177.74 5.35 5 -8 1 185.15 5.91 5 8 -1 185.29 6.08 5 -8 1 186.21 6.18 -5 -8 -1 189.38 5.72 5 8 -1 182.22 10.38 5 -8 1 169.47 8.89 -5 -8 -1 179.55 5.52 -5 -8 -1 198.42 5.68 5 -8 1 186.61 5.97 5 -8 1 190.29 6.06 5 -8 0 8.54 1.13 5 8 0 11.00 1.26 5 -8 0 9.81 1.27 -5 -8 0 9.99 1.16 5 -8 0 8.87 1.18 5 8 0 5.87 2.07 5 -8 0 7.40 1.02 5 -8 0 8.16 2.00 -5 -8 0 9.25 1.08 5 8 1 189.76 6.08 5 8 1 193.15 6.07 5 -8 -1 185.08 9.29 5 -8 -1 199.74 5.80 -5 -8 1 194.99 5.88 5 -8 -1 184.92 6.11 5 -8 -1 181.73 6.08 -5 -8 1 191.84 5.65 5 -8 -1 181.97 6.03 -5 -8 2 177.38 5.53 5 8 2 169.56 9.84 5 -8 -2 151.89 8.41 5 -8 -2 171.74 5.34 -5 -8 2 176.13 5.56 5 -8 -2 176.24 5.85 5 8 2 175.56 5.66 -5 -8 2 171.07 5.24 -5 -8 2 175.39 5.33 5 -8 -3 1.60 0.70 -5 -8 3 2.91 0.74 -5 -8 3 2.32 0.64 -5 -8 3 1.17 0.62 -5 -8 3 2.04 0.58 5 8 3 1.51 1.32 5 -8 -3 2.08 0.60 5 -8 -3 3.19 1.32 5 8 3 1.36 0.59 5 -8 -3 1.70 0.77 -5 -8 4 106.91 3.68 -5 -8 4 110.71 3.85 5 8 4 109.20 7.53 -5 -8 4 109.95 4.10 5 -8 -4 107.28 3.80 5 -8 -4 110.27 6.65 5 -8 -4 112.84 4.31 5 -8 -4 111.94 4.33 5 8 4 104.81 4.02 -5 -8 4 106.95 3.96 -5 -8 5 40.03 1.94 -5 -8 5 36.98 1.97 -5 -8 5 34.00 2.05 5 -8 -5 38.90 1.99 5 -8 -5 38.46 3.75 5 8 5 33.80 4.00 5 -8 -5 38.79 2.29 5 -8 -5 40.04 2.37 5 8 5 35.48 2.12 -5 -8 6 36.96 1.79 -5 -8 6 38.92 1.95 5 8 6 33.35 3.87 5 -8 -6 35.27 2.13 5 8 6 35.84 2.12 -5 -8 6 38.08 2.07 5 -8 -6 33.95 3.45 5 -8 -6 36.97 1.89 -5 -8 7 34.06 1.93 5 8 7 36.47 2.08 5 -8 -7 34.43 1.72 5 -8 -7 34.34 2.01 -5 -8 7 38.06 2.16 -5 -8 7 33.99 1.74 5 -8 -8 42.62 2.15 -5 -8 8 45.14 2.24 5 8 8 50.34 2.43 -5 -8 8 42.57 2.11 5 8 8 46.53 2.76 -5 -8 8 47.49 2.41 5 8 9 28.86 1.77 -5 -8 9 27.39 1.71 5 8 9 26.00 2.00 -5 -8 9 24.62 1.62 5 8 10 218.29 5.99 -5 -8 10 211.88 5.85 -5 -8 10 197.43 5.78 5 8 11 36.93 1.87 -5 -8 11 32.46 1.69 -5 -8 12 20.49 1.19 5 8 12 21.79 1.56 -5 -8 13 9.79 0.69 5 8 13 10.98 1.02 -5 -8 13 11.63 0.88 5 8 14 12.91 0.91 -5 -8 14 13.94 0.80 5 9 -14 22.92 0.99 5 9 -13 83.32 2.58 -5 9 13 82.46 2.45 -5 -9 -12 35.14 1.48 5 9 -12 36.38 1.81 -5 9 12 36.28 1.69 5 9 -11 14.58 1.25 -5 -9 -11 15.55 1.04 5 -9 11 13.26 0.97 5 9 -10 10.59 1.17 -5 -9 -10 10.20 0.94 5 -9 10 12.09 0.93 -5 -9 -10 10.00 0.78 5 -9 9 41.74 1.91 -5 -9 -9 43.74 1.89 5 -9 9 43.26 2.41 -5 -9 -9 44.05 2.05 5 9 -9 42.35 2.41 5 -9 8 50.91 2.68 5 -9 8 46.09 2.07 5 9 -8 43.29 2.53 -5 -9 -8 46.50 2.19 5 -9 7 57.31 2.93 5 9 -7 63.09 3.12 5 -9 7 58.64 2.42 -5 -9 -7 53.38 2.21 5 -9 6 6.67 1.00 5 -9 6 6.43 1.05 5 -9 6 5.23 0.72 5 9 -6 6.93 1.14 -5 -9 -6 5.03 0.73 5 -9 6 5.65 0.81 -5 -9 -5 89.43 3.26 5 9 -5 86.12 3.89 5 9 -5 82.99 6.37 5 -9 5 90.62 3.77 5 -9 5 97.29 3.77 5 -9 5 93.55 3.30 5 -9 5 90.24 5.83 -5 -9 -5 85.11 3.20 5 -9 5 91.61 3.46 5 -9 4 45.62 2.43 5 9 -4 54.12 2.90 5 -9 4 50.66 2.64 5 9 -4 41.51 4.58 5 -9 4 36.34 3.79 5 -9 4 50.35 2.34 -5 -9 -4 48.89 2.34 -5 -9 -4 50.57 2.34 5 -9 4 52.30 2.45 -5 -9 -4 45.78 2.26 5 -9 3 13.32 1.35 5 -9 3 10.16 1.19 5 -9 3 13.57 1.24 5 9 -3 10.51 1.30 5 -9 3 11.95 1.13 5 -9 3 12.53 1.35 5 9 -3 8.62 2.35 5 -9 3 9.52 2.00 5 -9 3 12.19 1.15 -5 -9 -3 12.35 1.17 -5 -9 -3 13.73 1.23 -5 -9 -3 11.66 1.14 5 -9 2 83.25 3.34 5 9 -2 87.96 3.71 5 -9 2 82.68 3.60 5 -9 2 78.00 3.16 5 9 -2 66.30 6.10 5 -9 2 79.18 3.18 5 -9 2 76.13 5.67 -5 -9 -2 74.32 3.10 -5 -9 -2 79.97 3.19 5 -9 2 77.78 3.46 5 -9 2 80.92 3.41 -5 -9 -2 82.12 3.26 5 -9 1 21.77 1.63 5 9 -1 24.78 1.87 5 -9 1 24.87 1.94 5 -9 1 22.75 1.66 5 -9 1 21.62 1.74 5 -9 1 22.15 1.80 5 -9 1 21.08 2.98 5 9 -1 23.57 3.65 -5 -9 -1 22.05 1.63 -5 -9 -1 23.59 1.63 5 -9 0 62.67 2.91 5 9 0 62.79 3.05 5 -9 0 66.67 3.25 5 9 0 63.07 5.95 -5 -9 0 57.35 2.68 -5 -9 0 64.70 2.81 5 -9 0 63.11 2.79 5 -9 0 64.19 5.18 -5 -9 0 61.86 2.83 5 -9 0 67.23 3.18 5 -9 -1 25.49 1.98 5 -9 -1 23.51 1.85 5 -9 -1 24.40 1.77 5 9 1 27.43 1.88 -5 -9 1 21.24 1.66 5 9 1 23.08 1.78 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-5 -9 8 40.57 2.14 5 9 8 46.28 2.23 5 9 8 42.62 2.57 -5 -9 8 40.68 2.07 5 -9 -8 43.99 2.12 -5 -9 9 39.54 2.00 5 9 9 45.78 2.14 5 9 9 43.13 2.48 5 -9 -9 37.15 1.75 -5 -9 9 34.57 1.86 5 9 10 10.86 1.02 -5 -9 10 10.43 0.95 -5 -9 10 11.56 0.99 5 9 11 13.20 1.05 -5 -9 11 13.69 0.97 5 9 12 32.42 1.77 -5 -9 12 29.05 1.30 5 9 13 77.37 2.67 -5 -9 13 77.57 2.44 -5 -9 14 24.60 1.02 5 10 -13 33.42 1.29 5 10 -12 1.62 0.42 -5 -10 -12 2.02 0.38 -5 10 12 1.93 0.42 5 10 -11 44.32 2.00 -5 -10 -11 43.06 1.75 -5 10 11 42.58 1.83 5 10 -10 79.40 3.01 -5 -10 -10 78.20 2.65 -5 -10 -9 52.64 2.03 -5 -10 -9 48.67 1.89 5 10 -9 47.12 2.42 -5 -10 -9 55.98 2.24 -5 -10 -8 119.57 3.70 -5 -10 -8 118.08 3.80 5 10 -8 110.23 4.18 5 -10 8 117.13 3.55 -5 -10 -7 6.25 0.72 5 10 -7 4.81 0.89 -5 -10 -7 5.68 0.86 5 -10 7 7.03 0.77 5 -10 6 104.49 3.47 -5 -10 -6 104.46 3.49 -5 -10 -5 20.23 1.39 5 -10 5 21.68 1.63 5 10 -5 18.63 1.63 5 -10 5 18.79 1.41 5 10 -4 30.21 2.09 5 -10 4 29.32 1.96 -5 -10 -4 28.52 1.71 5 -10 4 29.81 1.72 -5 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32.90 1.92 -5 -10 1 35.74 2.10 -5 -10 2 211.08 6.11 5 -10 -2 224.92 6.28 5 -10 -2 216.56 10.02 5 10 2 201.43 10.98 5 10 2 223.85 6.54 5 -10 -2 220.01 6.78 5 -10 -2 215.39 6.38 -5 -10 2 213.08 6.14 -5 -10 2 214.54 6.26 -5 -10 2 223.72 6.51 -5 -10 3 37.90 2.09 5 -10 -3 41.29 2.12 5 -10 -3 37.52 3.83 5 10 3 34.25 4.29 5 -10 -3 36.93 2.35 5 -10 -3 40.66 2.42 -5 -10 3 41.77 2.27 5 -10 -3 38.94 2.18 -5 -10 3 39.11 2.11 -5 -10 3 38.64 1.99 5 10 3 42.73 2.28 5 10 4 29.71 1.87 -5 -10 4 29.58 1.83 5 -10 -4 27.79 1.68 5 -10 -4 26.48 1.79 5 -10 -4 26.56 1.93 5 -10 -4 28.13 1.98 -5 -10 4 30.77 1.80 -5 -10 5 17.56 1.49 5 10 5 18.59 1.44 -5 -10 5 17.26 1.44 5 -10 -5 18.55 1.58 5 -10 -5 20.97 1.66 -5 -10 5 17.87 1.32 5 10 6 120.69 4.02 -5 -10 6 111.82 3.67 -5 -10 6 110.37 3.98 5 -10 -6 108.12 4.03 5 -10 -7 5.14 0.82 -5 -10 7 5.02 0.82 5 10 7 7.12 0.91 5 -10 -8 107.86 3.57 5 10 8 114.23 4.26 -5 -10 8 110.52 3.70 -5 -10 8 101.91 3.49 5 10 8 105.63 3.65 5 -10 -9 45.86 1.91 -5 -10 9 48.09 2.07 5 10 9 53.08 2.64 -5 -10 9 52.58 2.18 5 10 9 54.32 2.26 -5 -10 10 68.44 2.45 5 10 10 76.92 2.68 -5 -10 11 41.74 1.84 5 10 12 2.78 0.55 -5 -10 12 2.35 0.47 5 10 13 36.26 1.45 -5 -10 13 35.17 1.35 5 11 -12 9.09 0.62 -5 -11 -12 8.51 0.56 5 11 -11 18.33 1.06 -5 -11 -11 19.27 1.00 -5 11 11 16.25 0.91 5 11 -10 0.87 0.42 -5 11 10 0.66 0.35 -5 -11 -10 1.08 0.29 -5 -11 -10 1.26 0.42 -5 -11 -9 7.42 0.69 -5 -11 -9 6.12 0.58 5 11 -9 7.34 0.85 -5 -11 -9 7.64 0.79 -5 -11 -8 6.76 0.78 5 11 -8 6.98 0.91 -5 -11 -8 7.98 0.86 -5 -11 -7 14.49 1.15 5 11 -7 13.21 1.25 -5 -11 -7 12.54 0.92 5 11 -6 54.51 2.66 -5 -11 -6 58.86 2.31 5 11 -5 51.56 2.61 -5 -11 -5 48.66 2.19 -5 -11 -4 117.21 3.89 5 -11 4 114.85 4.00 5 11 -4 119.47 4.33 5 -11 4 120.39 4.28 5 -11 3 36.64 2.21 -5 -11 -3 39.54 2.04 5 -11 3 39.45 2.16 5 -11 3 36.05 2.04 5 11 -3 39.83 2.27 -5 -11 -3 34.35 1.95 5 -11 2 107.12 3.86 5 -11 2 117.97 4.31 5 -11 2 110.78 4.13 5 -11 2 109.14 4.07 5 11 -2 121.13 4.31 -5 -11 -2 110.67 3.94 -5 -11 -2 112.88 3.89 -5 -11 -1 53.53 2.49 5 11 -1 48.38 2.55 -5 -11 -1 54.82 2.57 5 -11 1 49.18 2.59 5 -11 1 51.37 2.66 5 11 -1 55.89 2.70 5 11 0 15.51 1.39 -5 -11 0 16.38 1.37 5 -11 0 15.82 1.51 5 -11 0 14.72 1.47 5 -11 0 15.18 1.29 -5 -11 0 14.74 1.35 -5 -11 1 52.82 2.58 5 11 1 55.78 2.65 5 -11 -1 52.64 2.74 5 -11 -1 54.22 2.48 5 -11 -2 112.39 4.28 -5 -11 2 111.80 4.03 5 -11 -2 108.57 4.28 -5 -11 2 108.16 3.71 5 11 2 113.17 4.02 -5 -11 2 110.02 3.92 5 -11 -3 40.21 2.38 5 -11 -3 40.89 2.36 -5 -11 3 37.25 2.12 -5 -11 3 39.63 2.05 5 -11 -3 40.21 2.40 5 11 3 41.41 2.16 -5 -11 3 39.07 2.06 5 -11 -4 117.75 4.30 5 -11 -4 122.65 4.38 5 -11 -4 119.53 4.43 -5 -11 4 113.03 3.95 5 11 4 110.29 3.92 -5 -11 4 115.84 3.88 5 -11 -5 46.79 2.42 5 -11 -5 46.83 2.45 -5 -11 5 46.28 2.32 5 -11 -5 43.04 2.44 -5 -11 5 44.53 2.24 5 11 5 46.18 2.22 -5 -11 5 48.98 2.17 -5 -11 6 61.47 2.61 5 -11 -6 60.20 2.85 5 -11 -6 56.15 2.60 -5 -11 6 53.69 2.53 5 11 6 58.97 2.50 -5 -11 7 14.61 1.18 5 -11 -7 13.61 1.31 5 -11 -7 13.92 1.17 5 11 7 13.05 1.10 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38.88 1.98 -5 -12 -2 39.01 2.02 5 12 -2 37.32 2.05 5 -12 2 37.36 2.09 5 -12 2 37.50 2.07 5 12 -1 57.45 2.61 5 -12 1 58.47 2.72 5 -12 1 60.63 2.79 -5 -12 -1 57.96 2.60 -5 -12 -1 57.08 2.54 5 -12 0 31.60 2.01 5 12 0 35.82 1.95 5 -12 0 34.47 2.08 5 -12 0 32.23 2.05 -5 -12 0 32.99 1.91 -5 -12 0 34.84 1.94 5 -12 -1 55.43 2.72 -5 -12 1 53.88 2.54 5 12 1 56.80 2.54 5 -12 -1 56.39 2.73 -5 -12 2 37.44 1.99 5 -12 -2 38.08 2.22 5 12 2 37.47 1.97 -5 -12 2 39.49 1.88 -5 -12 2 40.70 2.13 5 -12 -2 39.76 2.29 5 12 3 21.49 1.45 -5 -12 3 21.53 1.39 5 -12 -3 21.42 1.65 -5 -12 3 20.90 1.43 5 -12 -3 23.10 1.70 5 -12 -3 25.12 1.78 5 12 4 100.03 3.39 5 -12 -4 98.77 3.72 -5 -12 4 89.60 3.06 -5 -12 4 101.04 3.42 -5 -12 4 98.13 3.37 5 -12 -4 100.16 3.72 5 -12 -4 96.03 3.68 5 12 5 9.10 0.92 -5 -12 5 8.44 0.97 5 -12 -5 10.25 1.12 -5 -12 5 8.34 0.84 -5 -12 5 9.62 0.92 -5 -12 5 9.97 0.99 5 -12 -5 9.79 1.08 5 12 6 184.17 5.07 -5 -12 6 185.28 5.21 5 -12 -6 179.09 5.40 -5 -12 6 175.83 4.99 -5 -12 6 183.28 5.23 5 -12 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7 -7 -4 34.12 1.94 -7 -7 4 31.18 1.56 -7 -7 4 37.01 1.72 7 7 4 37.16 1.82 7 -7 -4 36.76 2.02 7 -7 -5 6.61 0.89 7 -7 -5 5.66 0.64 -7 -7 5 5.34 0.74 -7 -7 5 4.94 0.73 -7 -7 5 5.79 0.68 7 7 5 6.42 0.75 7 -7 -5 5.34 0.88 7 -7 -6 13.67 0.88 -7 -7 6 15.06 1.14 -7 -7 6 15.95 1.11 7 7 6 15.05 1.07 7 -7 -6 17.18 1.33 7 -7 -6 14.92 1.21 -7 -7 7 25.61 1.41 -7 -7 7 24.48 1.31 7 7 7 25.46 1.33 7 -7 -7 24.69 1.49 7 -7 -7 23.91 1.51 7 7 8 6.35 0.64 7 -7 -8 6.07 0.73 7 -7 -8 6.41 0.78 7 7 9 10.63 0.72 7 -7 -9 9.74 0.82 7 -7 -9 12.09 0.86 7 -7 -10 57.49 1.94 7 -7 -10 57.93 1.86 -7 -7 10 59.99 1.82 7 8 -9 25.75 1.11 7 -8 9 27.79 1.05 7 8 -8 28.93 1.28 7 8 -8 31.05 1.37 -7 -8 -8 30.27 1.18 -7 8 8 26.08 1.13 7 -8 8 29.48 1.20 7 8 -7 17.76 1.09 -7 -8 -7 21.64 1.07 7 8 -7 21.39 1.21 -7 8 7 16.20 0.92 7 -8 7 19.07 1.02 -7 8 6 54.16 1.89 -7 -8 -6 55.34 1.82 7 8 -6 56.99 2.21 7 -8 6 61.29 2.09 7 8 -6 58.01 2.27 -7 -8 -5 33.81 1.46 7 8 -5 31.45 1.64 7 -8 5 33.33 1.54 7 8 -5 34.89 1.75 -7 -8 -4 38.92 1.69 7 8 -4 41.26 1.98 7 8 -4 39.93 1.92 7 -8 4 38.31 1.68 7 -8 3 27.93 1.46 -7 -8 -3 25.75 1.42 -7 -8 -3 28.10 1.47 7 8 -3 27.35 1.59 7 -8 3 25.86 1.44 7 -8 2 20.11 1.31 -7 -8 -2 19.03 1.08 7 -8 2 17.56 1.21 -7 -8 -2 20.14 1.28 -7 -8 -2 22.05 1.31 7 8 -2 19.41 1.34 7 -8 2 21.20 1.36 7 -8 1 34.92 1.81 7 -8 1 32.78 1.70 -7 -8 -1 33.45 1.57 -7 -8 -1 37.37 1.77 -7 -8 -1 36.03 1.76 7 8 -1 36.03 1.87 7 -8 1 32.71 1.77 -7 -8 0 9.26 0.86 7 -8 0 9.97 1.01 -7 -8 0 9.78 0.95 7 8 0 9.58 0.98 7 -8 0 9.70 1.02 7 -8 -1 35.85 1.78 -7 -8 1 36.35 1.76 7 -8 -1 39.26 2.00 -7 -8 1 37.58 1.78 7 8 1 35.40 1.86 7 -8 -1 40.36 1.99 7 -8 -2 17.70 1.20 -7 -8 2 21.28 1.33 7 -8 -2 19.07 1.40 -7 -8 2 20.75 1.26 -7 -8 2 20.05 1.29 7 8 2 18.63 1.31 7 -8 -2 19.93 1.39 -7 -8 3 28.80 1.55 7 -8 -3 26.32 1.65 -7 -8 3 26.10 1.39 -7 -8 3 28.67 1.49 7 -8 -3 27.24 1.44 7 -8 -3 26.41 1.60 7 -8 -4 38.53 1.69 -7 -8 4 39.46 1.86 7 -8 -4 38.68 2.01 -7 -8 4 39.75 1.73 7 -8 -4 40.53 1.97 7 8 4 38.62 1.81 -7 -8 5 37.38 1.74 7 -8 -5 35.89 1.86 7 8 5 33.52 1.62 7 -8 -5 35.97 1.79 7 -8 -5 31.37 1.43 7 8 6 53.51 2.10 7 -8 -6 54.38 2.24 7 -8 -6 61.06 2.45 -7 -8 6 62.06 2.27 7 8 7 18.39 1.06 7 -8 -7 17.77 1.11 7 -8 -7 19.04 1.23 -7 -8 7 19.54 1.14 7 8 8 28.70 1.26 7 -8 -8 29.34 1.34 7 -8 -8 30.83 1.46 7 -8 -9 26.09 1.10 7 -8 -9 26.79 1.21 -7 -8 9 27.03 1.12 -7 -9 -8 40.51 1.29 7 9 -8 34.51 1.32 7 9 -7 92.84 2.72 7 -9 7 97.08 2.53 -7 -9 -7 95.27 2.59 7 9 -6 19.70 1.12 -7 -9 -6 19.29 1.02 7 -9 6 19.97 0.99 7 9 -5 9.35 0.84 7 -9 5 7.91 0.67 -7 -9 -5 9.05 0.69 7 9 -4 44.16 1.94 7 -9 4 47.47 1.79 -7 -9 -4 43.40 1.72 -7 -9 -3 2.59 0.51 7 9 -3 1.27 0.48 7 -9 3 1.88 0.42 -7 -9 -2 29.91 1.48 -7 -9 -2 26.91 1.23 7 -9 2 30.26 1.54 7 -9 2 27.13 1.41 7 -9 1 69.97 2.63 -7 -9 -1 73.58 2.56 7 -9 1 70.61 2.53 7 -9 1 69.46 2.54 -7 -9 -1 69.26 2.36 -7 -9 0 49.98 2.05 -7 -9 0 49.51 1.97 7 -9 0 50.01 2.17 7 -9 0 50.68 2.10 -7 -9 1 67.66 2.44 7 -9 -1 68.03 2.47 7 -9 -1 66.67 2.53 7 -9 -1 71.55 2.70 -7 -9 2 30.51 1.51 7 -9 -2 30.13 1.55 -7 -9 2 28.59 1.47 7 -9 -2 27.22 1.41 7 -9 -2 28.68 1.63 -7 -9 3 1.32 0.47 7 -9 -3 1.79 0.48 -7 -9 3 2.02 0.48 7 -9 -3 1.92 0.44 7 -9 -3 1.79 0.56 -7 -9 4 45.34 1.77 7 -9 -4 43.27 2.02 -7 -9 4 46.81 1.93 7 -9 -4 46.93 1.93 7 -9 -5 9.09 0.87 -7 -9 5 9.18 0.81 7 -9 -5 9.40 0.80 7 -9 -6 20.39 1.24 -7 -9 6 20.29 1.14 7 -9 -6 19.56 1.10 7 -9 -7 90.60 2.85 7 -9 -8 41.36 1.56 7 10 -7 11.68 0.67 -7 -10 -7 10.61 0.61 -7 -10 -6 12.96 0.74 -7 -10 -6 11.26 0.65 -7 -10 -5 27.13 1.06 -7 -10 -5 31.52 1.28 -7 -10 -4 46.19 1.63 -7 -10 -3 22.08 1.12 7 -10 2 38.10 1.66 -7 -10 -2 40.32 1.64 -7 -10 -1 80.63 2.52 7 -10 1 87.70 2.86 -7 -10 -1 90.27 2.78 -7 -10 0 4.67 0.57 7 10 0 4.32 0.63 7 -10 0 5.09 0.67 -7 -10 0 4.46 0.61 -7 -10 1 89.40 2.77 7 10 1 93.85 2.97 7 -10 -1 84.50 2.93 -7 -10 2 39.05 1.64 7 10 2 38.54 1.68 7 -10 -2 39.26 1.78 -7 -10 2 37.55 1.62 -7 -10 3 22.95 1.20 7 10 3 21.00 1.17 7 -10 -3 21.05 1.26 -7 -10 3 23.03 1.15 -7 -10 4 47.36 1.79 7 -10 -4 47.04 1.91 7 10 4 44.88 1.76 -7 -10 5 31.73 1.37 7 -10 -5 30.66 1.44 7 10 5 29.79 1.33 -7 -10 6 13.65 0.81 7 -10 -6 13.57 0.87 7 10 6 12.28 0.77 7 -10 -7 11.43 0.70 7 10 7 9.80 0.62 -7 -11 -5 1.35 0.28 7 11 -5 1.05 0.28 -7 -11 -4 87.95 2.40 -7 -11 -4 89.33 2.38 7 11 -4 92.77 2.52 -7 -11 -3 9.60 0.64 7 11 -3 9.73 0.73 -7 -11 -3 8.46 0.61 -7 -11 -2 38.32 1.43 7 11 -2 39.97 1.58 -7 -11 -2 40.91 1.51 7 11 -1 22.32 1.14 -7 -11 -1 20.51 1.06 7 -11 0 64.98 2.18 7 11 0 65.18 2.16 -7 -11 0 59.82 2.07 -7 -11 1 19.39 0.99 7 -11 -1 22.38 1.17 7 11 1 21.25 1.09 -7 -11 2 41.15 1.51 7 -11 -2 37.72 1.59 7 11 2 38.83 1.53 -7 -11 2 39.44 1.51 -7 -11 3 8.83 0.66 7 -11 -3 8.95 0.72 7 11 3 9.89 0.70 -7 -11 3 9.96 0.66 -7 -11 4 87.92 2.54 7 -11 -4 89.44 2.65 7 11 4 91.86 2.55 7 11 5 1.27 0.28 -7 -11 5 1.52 0.32 7 -11 -5 1.30 0.32 -7 -12 -3 18.04 0.78 7 12 -2 1.46 0.28 -7 -12 -2 1.55 0.27 -7 -12 -1 20.11 0.88 7 12 -1 19.72 0.88 -7 -12 -1 20.50 0.90 -7 -12 0 1.82 0.30 -7 -12 0 2.26 0.34 7 12 0 2.57 0.35 7 12 1 19.48 0.87 -7 -12 2 2.30 0.32 7 -12 -2 1.85 0.31 7 12 2 1.74 0.28 7 -12 -3 19.92 0.85 8 0 0 24.84 1.30 -8 0 0 23.82 1.18 8 0 -1 40.84 1.74 -8 0 1 42.15 1.71 8 0 -2 0.65 0.38 -8 0 2 2.31 0.47 8 0 -3 27.33 1.36 -8 0 -3 27.52 1.36 -8 0 3 26.28 1.38 8 0 4 8.51 0.64 8 0 -4 10.02 0.79 -8 0 -4 9.84 0.75 -8 0 4 9.54 0.83 8 0 5 8.05 0.59 8 0 -5 7.10 0.66 -8 0 5 7.80 0.75 -8 0 -5 8.15 0.62 -8 0 6 0.29 0.28 8 0 -6 0.28 0.27 8 0 6 0.33 0.21 -8 0 6 0.16 0.34 -8 0 7 0.10 0.25 8 0 -7 0.24 0.21 -8 0 7 0.55 0.33 -8 0 8 38.48 1.46 -8 0 9 0.98 0.25 -8 1 9 2.28 0.31 -8 1 8 3.43 0.40 -8 1 8 3.62 0.45 -8 1 7 10.21 0.71 -8 1 7 11.38 0.79 8 -1 7 9.83 0.58 -8 1 6 14.73 0.88 8 -1 6 14.78 0.78 -8 1 6 14.16 0.93 -8 -1 -6 13.41 0.74 -8 1 5 18.30 1.02 8 -1 5 19.53 0.98 -8 -1 -5 19.97 0.97 -8 1 5 18.34 1.11 8 -1 4 12.14 0.81 8 1 -4 10.59 0.73 -8 -1 -4 13.37 0.87 -8 1 4 11.93 0.90 8 1 -3 15.58 0.92 -8 -1 -3 17.88 1.08 -8 1 3 15.96 1.03 8 1 -2 16.13 0.96 -8 -1 -2 17.31 1.11 -8 1 2 16.78 1.03 8 -1 1 6.20 0.72 8 1 -1 5.96 0.60 -8 1 1 5.73 0.59 8 -1 0 226.26 5.87 8 -1 -1 6.47 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1.27 -8 -3 4 4.67 0.58 8 -3 -4 3.80 0.60 -8 -3 4 4.12 0.58 8 -3 -4 3.67 0.51 -8 -3 4 3.38 0.49 -8 -3 5 30.18 1.37 8 -3 -5 32.35 1.55 -8 -3 5 31.74 1.48 -8 -3 6 16.97 0.97 8 -3 -6 16.27 1.03 -8 -3 6 17.69 1.03 -8 -3 7 25.78 1.15 8 -3 -7 23.57 1.16 -8 -3 7 23.71 1.14 8 -3 -8 6.87 0.54 -8 -3 8 6.89 0.53 8 -4 8 59.56 1.66 -8 4 7 10.46 0.62 8 -4 7 13.30 0.70 -8 4 6 6.10 0.51 8 -4 6 7.04 0.58 -8 4 5 7.39 0.57 -8 -4 -5 8.34 0.60 -8 -4 -5 8.96 0.62 8 -4 5 9.62 0.71 -8 -4 -4 4.26 0.51 -8 -4 -4 3.41 0.47 -8 4 4 3.28 0.39 8 -4 3 12.71 0.92 -8 -4 -3 15.00 0.96 -8 -4 -3 15.48 0.97 8 -4 2 45.71 1.89 -8 -4 -2 48.26 1.89 8 -4 1 103.96 3.20 -8 -4 -1 100.18 3.04 8 -4 0 91.49 3.06 -8 -4 0 91.32 2.93 8 -4 -1 98.36 3.22 8 -4 -1 96.00 3.11 -8 -4 2 45.10 1.67 8 -4 -2 48.71 2.07 -8 -4 2 53.08 1.97 8 -4 -2 49.64 1.98 -8 -4 3 15.64 0.99 -8 -4 3 13.82 0.93 8 -4 -3 14.87 1.08 -8 -4 3 13.48 0.86 -8 -4 3 14.33 0.99 8 -4 -3 13.85 0.94 8 -4 -4 3.20 0.46 -8 -4 4 3.15 0.47 8 -4 -4 3.45 0.56 -8 -4 4 3.30 0.54 -8 -4 4 3.86 0.51 -8 -4 4 3.49 0.49 -8 -4 5 8.41 0.68 8 -4 -5 8.96 0.81 -8 -4 5 9.38 0.77 -8 -4 6 7.43 0.63 8 -4 -6 8.40 0.72 -8 -4 6 7.60 0.67 8 -4 -7 14.06 0.86 -8 -4 7 14.56 0.81 8 -4 -8 64.20 1.89 -8 -4 8 62.97 1.85 8 -5 7 1.70 0.29 -8 -5 -6 2.48 0.30 8 -5 6 2.61 0.38 -8 -5 -5 16.76 0.81 8 -5 5 18.97 0.97 -8 -5 -4 2.61 0.42 8 -5 4 3.49 0.47 -8 -5 -4 2.72 0.41 -8 -5 -3 20.28 1.08 -8 -5 -3 20.13 1.07 8 -5 2 11.90 0.87 -8 -5 -2 10.52 0.82 -8 -5 -2 12.51 0.89 8 -5 1 49.57 2.02 8 -5 1 48.63 1.95 -8 -5 -1 52.19 1.95 -8 -5 -1 51.74 1.97 8 -5 0 86.58 2.88 -8 -5 0 83.87 2.72 -8 -5 0 85.15 2.75 8 -5 -1 51.11 2.06 8 -5 -1 48.05 1.92 -8 -5 2 10.27 0.70 8 -5 -2 11.10 0.92 -8 -5 2 10.71 0.82 -8 -5 2 10.83 0.84 8 -5 -2 11.04 0.84 -8 -5 3 18.69 0.98 8 -5 -3 20.13 1.20 -8 -5 3 19.51 1.08 -8 -5 3 19.29 1.05 8 -5 -3 18.15 1.03 -8 -5 4 2.81 0.42 8 -5 -4 2.12 0.47 8 -5 -4 2.38 0.35 -8 -5 5 18.61 0.95 8 -5 -5 20.58 1.12 8 -5 -6 2.78 0.45 -8 -5 6 2.71 0.41 8 -5 -7 1.55 0.33 -8 -5 7 2.07 0.33 8 -6 7 7.08 0.45 8 -6 6 19.04 0.85 8 -6 5 41.87 1.48 8 -6 4 3.93 0.47 -8 -6 -4 3.91 0.43 -8 -6 -3 66.09 2.09 -8 -6 -3 63.71 2.07 -8 -6 -2 16.23 0.96 -8 -6 -2 17.07 0.97 8 -6 1 6.63 0.63 -8 -6 -1 5.17 0.60 -8 -6 -1 4.79 0.59 8 -6 0 137.16 3.86 -8 -6 0 132.07 3.70 8 -6 -1 6.16 0.68 8 -6 -1 5.60 0.59 8 -6 -2 17.02 1.07 -8 -6 2 13.35 0.77 8 -6 -2 13.28 0.75 -8 -6 2 18.51 1.00 -8 -6 2 16.72 0.97 8 -6 -3 65.57 2.20 -8 -6 3 57.69 1.83 -8 -6 3 61.79 1.93 -8 -6 3 62.83 1.99 -8 -6 4 4.23 0.47 8 -6 -4 2.90 0.37 8 -6 -4 4.75 0.57 8 -6 -5 39.36 1.53 -8 -6 5 35.96 1.36 8 -6 -6 17.18 0.89 -8 -6 6 15.53 0.78 8 -6 -7 8.14 0.53 -8 -7 -5 14.92 0.70 -8 -7 -4 28.12 1.03 -8 -7 -3 79.93 2.30 -8 -7 -2 11.91 0.76 -8 -7 -1 3.77 0.48 -8 -7 0 0.99 0.35 -8 -7 1 4.18 0.50 -8 -7 2 8.88 0.55 8 -7 -2 8.10 0.55 -8 -7 3 78.39 2.17 -8 -7 3 65.37 1.97 -8 -7 4 28.22 1.08 -8 -7 5 13.50 0.68 8 -8 4 13.16 0.62 -8 -8 -4 12.02 0.61 -8 -8 -3 2.22 0.29 8 -8 3 1.70 0.28 -8 -8 -2 29.96 1.14 8 -8 2 30.65 1.14 -8 -8 -1 3.80 0.44 -8 -8 0 17.36 0.89 -8 -8 2 29.08 1.13 -8 -8 3 2.66 0.33 8 -8 -3 2.33 0.34 8 -8 -4 12.80 0.65 -8 -9 0 0.02 0.17 -9 0 0 0.12 0.17 -9 0 1 1.41 0.23 -9 -1 0 10.81 0.56 0 0 0 0.00 0.00 TITL 22SAI_R130_gaus in P2(1)2(1)2(1) REM P2(1)2(1)2(1) (#19 in standard setting) CELL 1.54184 7.112961 15.459696 16.035794 90.0000 90.0000 90.0000 ZERR 4.00 0.000050 0.000093 0.000119 0.0000 0.0000 0.0000 LATT -1 SYMM -x+1/2,-y, z+1/2 SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y+1/2,-z SFAC C H O UNIT 80.00 104.00 20.00 REM CrysAlisPro recorded range (K): Min=99.9; max=100.1; aver:100.0 TEMP -173 SIZE 0.13 0.18 0.21 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 36468 _shelx_res_file ; TITL Sample2 in P2(1)2(1)2(1) CELL 1.54184 7.11296 15.45970 16.03579 90.0000 90.0000 90.0000 ZERR 4.00 0.00005 0.00009 0.00012 0.0000 0.0000 0.0000 LATT -1 SYMM 0.5-X, -Y, 0.5+Z SYMM -X, 0.5+Y, 0.5-Z SYMM 0.5+X, 0.5-Y, -Z SFAC C H O UNIT 80 104 20 TEMP -173.0 SIZE 0.13 0.18 0.21 L.S. 12 BOND $H ACTA CONF WGHT 0.044400 0.458500 FVAR 0.69069 O1 3 0.272141 0.555505 0.811836 11.00000 0.02479 0.03245 = 0.02026 -0.00126 0.00027 -0.00191 O2 3 0.170818 0.663968 0.891639 11.00000 0.03988 0.03415 = 0.02336 0.00215 0.00465 0.00691 O3 3 0.620777 0.618140 0.556787 11.00000 0.02682 0.01666 = 0.02175 0.00069 0.00516 0.00012 O4 3 0.713877 0.607600 0.423382 11.00000 0.04854 0.02163 = 0.02467 -0.00191 0.01064 -0.00131 C2 1 0.296892 0.616383 0.871074 11.00000 0.03474 0.02678 = 0.01563 0.00388 0.00193 -0.00247 C3 1 0.494881 0.611509 0.904311 11.00000 0.03554 0.02636 = 0.02139 0.00131 -0.00351 -0.00340 AFIX 13 H3 2 0.493644 0.569316 0.951575 11.00000 -1.20000 AFIX 0 C3A 1 0.604509 0.569142 0.832849 11.00000 0.02689 0.02237 = 0.02188 0.00249 -0.00535 -0.00201 AFIX 13 H3A 2 0.702609 0.530025 0.856790 11.00000 -1.20000 AFIX 0 C4 1 0.696525 0.629802 0.769976 11.00000 0.02728 0.02304 = 0.02748 0.00151 -0.00513 -0.00570 AFIX 23 H4A 2 0.789271 0.667453 0.798286 11.00000 -1.20000 H4B 2 0.600275 0.666977 0.743437 11.00000 -1.20000 AFIX 0 C5 1 0.794095 0.574224 0.704277 11.00000 0.02209 0.03044 = 0.02857 0.00252 -0.00325 -0.00433 AFIX 23 H5A 2 0.899388 0.542883 0.731056 11.00000 -1.20000 H5B 2 0.848286 0.612734 0.661204 11.00000 -1.20000 AFIX 0 C5A 1 0.663575 0.507245 0.660812 11.00000 0.02062 0.02045 = 0.02507 0.00149 -0.00034 0.00160 C6 1 0.654272 0.526139 0.566804 11.00000 0.02481 0.01685 = 0.02611 0.00123 0.00448 0.00219 AFIX 13 H6 2 0.779753 0.512375 0.542009 11.00000 -1.20000 AFIX 0 C7 1 0.506216 0.473850 0.520558 11.00000 0.03220 0.01727 = 0.02086 0.00015 0.00162 0.00299 AFIX 13 H7 2 0.547669 0.445362 0.467676 11.00000 -1.20000 AFIX 0 C8 1 0.355239 0.429867 0.567458 11.00000 0.02787 0.01703 = 0.02306 0.00041 -0.00175 0.00154 AFIX 13 H8 2 0.305476 0.375034 0.542819 11.00000 -1.20000 AFIX 0 C9 1 0.343079 0.438255 0.659314 11.00000 0.02157 0.02069 = 0.02295 -0.00005 -0.00126 0.00051 C9A 1 0.459782 0.510730 0.696074 11.00000 0.02105 0.01839 = 0.01884 0.00194 -0.00103 0.00012 AFIX 13 H9A 2 0.403300 0.566014 0.675569 11.00000 -1.20000 AFIX 0 C9B 1 0.451476 0.514038 0.791155 11.00000 0.02513 0.02062 = 0.01990 0.00265 -0.00188 -0.00180 AFIX 13 H9B 2 0.454260 0.453997 0.814323 11.00000 -1.20000 AFIX 0 O10 3 0.318726 0.508782 0.521073 11.00000 0.03079 0.01968 = 0.02582 0.00203 -0.00533 0.00077 C10 1 0.567973 0.696794 0.938853 11.00000 0.04626 0.03271 = 0.03480 -0.00972 0.00001 -0.00773 AFIX 137 H10A 2 0.562412 0.741174 0.895285 11.00000 -1.50000 H10B 2 0.698401 0.689501 0.957248 11.00000 -1.50000 H10C 2 0.490180 0.714631 0.986270 11.00000 -1.50000 AFIX 0 C11 1 0.747318 0.416118 0.671279 11.00000 0.02710 0.02610 = 0.03546 0.00619 -0.00234 0.00642 AFIX 137 H11A 2 0.745028 0.399893 0.730348 11.00000 -1.50000 H11B 2 0.877387 0.415852 0.651127 11.00000 -1.50000 H11C 2 0.672873 0.374571 0.639028 11.00000 -1.50000 AFIX 0 C12 1 0.667747 0.652059 0.482110 11.00000 0.02299 0.02040 = 0.02084 -0.00031 0.00218 -0.00172 C13 1 0.662231 0.748345 0.483492 11.00000 0.01834 0.01947 = 0.02250 -0.00037 0.00156 -0.00168 C14 1 0.663973 0.793392 0.411964 11.00000 0.01960 0.02003 = 0.02482 -0.00018 0.00039 -0.00111 AFIX 43 H14 2 0.665764 0.854553 0.417657 11.00000 -1.20000 AFIX 0 C15 1 0.661909 0.792866 0.567416 11.00000 0.02386 0.02028 = 0.02299 -0.00159 0.00103 -0.00129 AFIX 137 H15A 2 0.544096 0.779978 0.596562 11.00000 -1.50000 H15B 2 0.673203 0.855497 0.559424 11.00000 -1.50000 H15C 2 0.768221 0.771987 0.600671 11.00000 -1.50000 AFIX 0 C16 1 0.663466 0.759914 0.324426 11.00000 0.02614 0.02613 = 0.02125 0.00066 0.00109 0.00143 AFIX 137 H16A 2 0.615590 0.804769 0.286825 11.00000 -1.50000 H16B 2 0.582625 0.708704 0.321010 11.00000 -1.50000 H16C 2 0.791850 0.744338 0.308105 11.00000 -1.50000 AFIX 0 C17 1 0.236192 0.382173 0.701948 11.00000 0.02342 0.02581 = 0.02618 -0.00057 -0.00167 -0.00363 H17A 2 0.165226 0.338712 0.675219 11.00000 0.01784 H17B 2 0.217553 0.386951 0.761828 11.00000 0.02787 HKLF 4 REM Sample2 in P2(1)2(1)2(1) REM R1 = 0.0313 for 3717 Fo > 4sig(Fo) and 0.0315 for all 3751 data REM 238 parameters refined using 0 restraints END WGHT 0.0444 0.4585 REM Highest difference peak 0.561, deepest hole -0.164, 1-sigma level 0.038 Q1 1 0.4204 0.3478 0.7049 11.00000 0.05 0.56 Q2 1 0.5609 0.5118 0.6814 11.00000 0.05 0.19 Q3 1 0.4054 0.6213 0.8840 11.00000 0.05 0.18 Q4 1 0.5339 0.5409 0.8158 11.00000 0.05 0.16 Q5 1 0.6578 0.7022 0.4818 11.00000 0.05 0.16 Q6 1 0.7234 0.5391 0.6829 11.00000 0.05 0.15 Q7 1 0.4083 0.4698 0.6830 11.00000 0.05 0.14 Q8 1 0.6875 0.4613 0.6691 11.00000 0.05 0.13 Q9 1 0.6386 0.5971 0.8008 11.00000 0.05 0.13 Q10 1 0.0001 0.6455 0.8974 11.00000 0.05 0.13 Q11 1 0.5799 0.4968 0.5431 11.00000 0.05 0.12 Q12 1 0.4697 0.4349 0.5557 11.00000 0.05 0.12 Q13 1 0.6630 0.7399 0.8960 11.00000 0.05 0.12 Q14 1 0.5573 0.5954 0.8628 11.00000 0.05 0.12 Q15 1 0.5570 0.7736 0.4463 11.00000 0.05 0.11 Q16 1 0.5391 0.7811 1.0267 11.00000 0.05 0.11 Q17 1 0.0511 0.3558 0.7131 11.00000 0.05 0.11 Q18 1 0.4098 0.3627 0.8143 11.00000 0.05 0.11 Q19 1 0.6581 0.7678 0.5207 11.00000 0.05 0.11 Q20 1 0.9457 0.3396 0.6949 11.00000 0.05 0.10 ; _shelx_res_checksum 61594 _shelxl_version_number .2013 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O O1 0.27214(18) 0.55551(9) 0.81184(8) 0.0258(3) Uani d 1 . . O O2 0.1708(2) 0.66397(9) 0.89164(9) 0.0325(3) Uani d 1 . . O O3 0.62078(17) 0.61814(8) 0.55679(8) 0.0217(3) Uani d 1 . . O O4 0.7139(2) 0.60760(8) 0.42338(8) 0.0316(3) Uani d 1 . . C C2 0.2969(3) 0.61638(12) 0.87107(10) 0.0257(4) Uani d 1 . . C C3 0.4949(3) 0.61151(12) 0.90431(11) 0.0278(4) Uani d 1 . . H H3 0.4936 0.5693 0.9516 0.033 Uiso calc 1 . . C C3A 0.6045(3) 0.56914(11) 0.83285(11) 0.0237(4) Uani d 1 . . H H3A 0.7026 0.5300 0.8568 0.028 Uiso calc 1 . . C C4 0.6965(3) 0.62980(11) 0.76998(11) 0.0259(4) Uani d 1 . . H H4A 0.7893 0.6675 0.7983 0.031 Uiso calc 1 . . H H4B 0.6003 0.6670 0.7434 0.031 Uiso calc 1 . . C C5 0.7941(3) 0.57422(12) 0.70428(12) 0.0270(4) Uani d 1 . . H H5A 0.8994 0.5429 0.7311 0.032 Uiso calc 1 . . H H5B 0.8483 0.6127 0.6612 0.032 Uiso calc 1 . . C C5A 0.6636(2) 0.50725(11) 0.66081(11) 0.0220(3) Uani d 1 . . C C6 0.6543(3) 0.52614(11) 0.56680(11) 0.0226(3) Uani d 1 . . H H6 0.7798 0.5124 0.5420 0.027 Uiso calc 1 . . C C7 0.5062(3) 0.47385(11) 0.52056(11) 0.0234(4) Uani d 1 . . H H7 0.5477 0.4454 0.4677 0.028 Uiso calc 1 . . C C8 0.3552(3) 0.42987(11) 0.56746(11) 0.0227(3) Uani d 1 . . H H8 0.3055 0.3750 0.5428 0.027 Uiso calc 1 . . C C9 0.3431(2) 0.43826(11) 0.65931(11) 0.0217(3) Uani d 1 . . C C9A 0.4598(2) 0.51073(10) 0.69607(10) 0.0194(3) Uani d 1 . . H H9A 0.4033 0.5660 0.6756 0.023 Uiso calc 1 . . C C9B 0.4515(2) 0.51404(11) 0.79115(10) 0.0219(3) Uani d 1 . . H H9B 0.4543 0.4540 0.8143 0.026 Uiso calc 1 . . O O10 0.31873(19) 0.50878(8) 0.52107(8) 0.0254(3) Uani d 1 . . C C10 0.5680(4) 0.69679(14) 0.93885(14) 0.0379(5) Uani d 1 . . H H10A 0.5624 0.7412 0.8953 0.057 Uiso calc 1 . . H H10B 0.6984 0.6895 0.9572 0.057 Uiso calc 1 . . H H10C 0.4902 0.7146 0.9863 0.057 Uiso calc 1 . . C C11 0.7473(3) 0.41612(12) 0.67128(13) 0.0295(4) Uani d 1 . . H H11A 0.7450 0.3999 0.7303 0.044 Uiso calc 1 . . H H11B 0.8774 0.4159 0.6511 0.044 Uiso calc 1 . . H H11C 0.6729 0.3746 0.6390 0.044 Uiso calc 1 . . C C12 0.6677(3) 0.65206(11) 0.48211(11) 0.0214(3) Uani d 1 . . C C13 0.6622(2) 0.74835(11) 0.48349(10) 0.0201(3) Uani d 1 . . C C14 0.6640(2) 0.79339(11) 0.41196(11) 0.0215(3) Uani d 1 . . H H14 0.6658 0.8546 0.4177 0.026 Uiso calc 1 . . C C15 0.6619(3) 0.79287(11) 0.56742(11) 0.0224(3) Uani d 1 . . H H15A 0.5441 0.7800 0.5966 0.034 Uiso calc 1 . . H H15B 0.6732 0.8555 0.5594 0.034 Uiso calc 1 . . H H15C 0.7682 0.7720 0.6007 0.034 Uiso calc 1 . . C C16 0.6635(3) 0.75991(11) 0.32443(11) 0.0245(4) Uani d 1 . . H H16A 0.6156 0.8048 0.2868 0.037 Uiso calc 1 . . H H16B 0.5826 0.7087 0.3210 0.037 Uiso calc 1 . . H H16C 0.7918 0.7443 0.3081 0.037 Uiso calc 1 . . C C17 0.2362(3) 0.38217(12) 0.70195(12) 0.0251(4) Uani d 1 . . H H17A 0.165(3) 0.3387(14) 0.6752(13) 0.018(5) Uiso d 1 . . H H17B 0.218(3) 0.3870(14) 0.7618(15) 0.028(6) Uiso d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.0248(6) 0.0325(6) 0.0203(6) -0.0019(5) 0.0003(5) -0.0013(5) O2 0.0399(8) 0.0341(7) 0.0234(6) 0.0069(6) 0.0046(6) 0.0021(5) O3 0.0268(6) 0.0167(5) 0.0218(6) 0.0001(5) 0.0052(5) 0.0007(5) O4 0.0485(8) 0.0216(6) 0.0247(6) -0.0013(6) 0.0106(6) -0.0019(5) C2 0.0347(10) 0.0268(8) 0.0156(7) -0.0025(8) 0.0019(7) 0.0039(6) C3 0.0355(10) 0.0264(9) 0.0214(8) -0.0034(8) -0.0035(8) 0.0013(7) C3A 0.0269(9) 0.0224(8) 0.0219(8) -0.0020(7) -0.0054(7) 0.0025(7) C4 0.0273(9) 0.0230(8) 0.0275(9) -0.0057(7) -0.0051(7) 0.0015(7) C5 0.0221(8) 0.0304(9) 0.0286(9) -0.0043(7) -0.0033(7) 0.0025(7) C5A 0.0206(8) 0.0205(8) 0.0251(8) 0.0016(6) -0.0003(7) 0.0015(6) C6 0.0248(8) 0.0169(7) 0.0261(8) 0.0022(6) 0.0045(7) 0.0012(7) C7 0.0322(9) 0.0173(7) 0.0209(8) 0.0030(7) 0.0016(7) 0.0002(6) C8 0.0279(8) 0.0170(7) 0.0231(8) 0.0015(6) -0.0018(7) 0.0004(6) C9 0.0216(8) 0.0207(8) 0.0230(8) 0.0005(7) -0.0013(7) -0.0001(6) C9A 0.0211(8) 0.0184(7) 0.0188(7) 0.0001(6) -0.0010(6) 0.0019(6) C9B 0.0251(9) 0.0206(8) 0.0199(8) -0.0018(7) -0.0019(6) 0.0027(6) O10 0.0308(7) 0.0197(6) 0.0258(6) 0.0008(5) -0.0053(5) 0.0020(5) C10 0.0463(12) 0.0327(10) 0.0348(11) -0.0077(9) 0.0000(10) -0.0097(9) C11 0.0271(9) 0.0261(9) 0.0355(10) 0.0064(7) -0.0023(8) 0.0062(8) C12 0.0230(8) 0.0204(8) 0.0208(8) -0.0017(7) 0.0022(7) -0.0003(6) C13 0.0183(7) 0.0195(7) 0.0225(8) -0.0017(6) 0.0016(7) -0.0004(6) C14 0.0196(8) 0.0200(7) 0.0248(8) -0.0011(6) 0.0004(7) -0.0002(6) C15 0.0239(8) 0.0203(7) 0.0230(8) -0.0013(7) 0.0010(7) -0.0016(6) C16 0.0261(9) 0.0261(8) 0.0212(8) 0.0014(7) 0.0011(7) 0.0007(7) C17 0.0234(8) 0.0258(8) 0.0262(9) -0.0036(7) -0.0017(7) -0.0006(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 0 -1 0 0.1119 0 1 0 0.0701 0 -1 -1 0.0807 0 1 1 0.0867 1 0 0 0.1190 -1 0 0 0.0910 0 -1 1 0.1012 0 0 -1 0.0442 0 0 1 0.0816 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C2 O1 C9B . . 110.55(14) ? C12 O3 C6 . . 116.01(13) ? O2 C2 O1 . . 121.42(18) ? O2 C2 C3 . . 128.94(17) ? O1 C2 C3 . . 109.64(16) ? C2 C3 C10 . . 113.86(17) ? C2 C3 C3A . . 103.43(14) ? C10 C3 C3A . . 117.94(17) ? C2 C3 H3 . . 107.0 ? C10 C3 H3 . . 107.0 ? C3A C3 H3 . . 107.0 ? C4 C3A C3 . . 116.74(15) ? C4 C3A C9B . . 110.96(14) ? C3 C3A C9B . . 101.65(15) ? C4 C3A H3A . . 109.0 ? C3 C3A H3A . . 109.0 ? C9B C3A H3A . . 109.0 ? C3A C4 C5 . . 107.78(15) ? C3A C4 H4A . . 110.2 ? C5 C4 H4A . . 110.2 ? C3A C4 H4B . . 110.2 ? C5 C4 H4B . . 110.2 ? H4A C4 H4B . . 108.5 ? C4 C5 C5A . . 114.37(16) ? C4 C5 H5A . . 108.7 ? C5A C5 H5A . . 108.7 ? C4 C5 H5B . . 108.7 ? C5A C5 H5B . . 108.7 ? H5A C5 H5B . . 107.6 ? C6 C5A C11 . . 107.32(15) ? C6 C5A C5 . . 109.79(14) ? C11 C5A C5 . . 109.24(15) ? C6 C5A C9A . . 108.03(14) ? C11 C5A C9A . . 110.64(14) ? C5 C5A C9A . . 111.71(14) ? O3 C6 C7 . . 110.69(14) ? O3 C6 C5A . . 107.57(13) ? C7 C6 C5A . . 114.02(14) ? O3 C6 H6 . . 108.1 ? C7 C6 H6 . . 108.1 ? C5A C6 H6 . . 108.1 ? O10 C7 C8 . . 59.73(11) ? O10 C7 C6 . . 116.08(13) ? C8 C7 C6 . . 120.00(15) ? O10 C7 H7 . . 116.3 ? C8 C7 H7 . . 116.3 ? C6 C7 H7 . . 116.3 ? O10 C8 C7 . . 58.83(11) ? O10 C8 C9 . . 115.17(14) ? C7 C8 C9 . . 120.57(16) ? O10 C8 H8 . . 116.5 ? C7 C8 H8 . . 116.5 ? C9 C8 H8 . . 116.5 ? C17 C9 C8 . . 118.92(16) ? C17 C9 C9A . . 126.23(16) ? C8 C9 C9A . . 114.83(15) ? C9 C9A C9B . . 113.11(14) ? C9 C9A C5A . . 110.09(14) ? C9B C9A C5A . . 113.57(14) ? C9 C9A H9A . . 106.5 ? C9B C9A H9A . . 106.5 ? C5A C9A H9A . . 106.5 ? O1 C9B C9A . . 105.92(13) ? O1 C9B C3A . . 106.01(13) ? C9A C9B C3A . . 115.22(14) ? O1 C9B H9B . . 109.8 ? C9A C9B H9B . . 109.8 ? C3A C9B H9B . . 109.8 ? C7 O10 C8 . . 61.44(11) ? C3 C10 H10A . . 109.5 ? C3 C10 H10B . . 109.5 ? H10A C10 H10B . . 109.5 ? C3 C10 H10C . . 109.5 ? H10A C10 H10C . . 109.5 ? H10B C10 H10C . . 109.5 ? C5A C11 H11A . . 109.5 ? C5A C11 H11B . . 109.5 ? H11A C11 H11B . . 109.5 ? C5A C11 H11C . . 109.5 ? H11A C11 H11C . . 109.5 ? H11B C11 H11C . . 109.5 ? O4 C12 O3 . . 122.45(16) ? O4 C12 C13 . . 125.87(16) ? O3 C12 C13 . . 111.64(14) ? C14 C13 C12 . . 120.38(15) ? C14 C13 C15 . . 121.65(15) ? C12 C13 C15 . . 117.93(15) ? C13 C14 C16 . . 128.49(15) ? C13 C14 H14 . . 115.8 ? C16 C14 H14 . . 115.8 ? C13 C15 H15A . . 109.5 ? C13 C15 H15B . . 109.5 ? H15A C15 H15B . . 109.5 ? C13 C15 H15C . . 109.5 ? H15A C15 H15C . . 109.5 ? H15B C15 H15C . . 109.5 ? C14 C16 H16A . . 109.5 ? C14 C16 H16B . . 109.5 ? H16A C16 H16B . . 109.5 ? C14 C16 H16C . . 109.5 ? H16A C16 H16C . . 109.5 ? H16B C16 H16C . . 109.5 ? C9 C17 H17A . . 122.2(13) ? C9 C17 H17B . . 122.1(14) ? H17A C17 H17B . . 115.5(19) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag O1 C2 . 1.349(2) ? O1 C9B . 1.466(2) ? O2 C2 . 1.206(2) ? O3 C12 . 1.349(2) ? O3 C6 . 1.4510(19) ? O4 C12 . 1.211(2) ? C2 C3 . 1.508(3) ? C3 C10 . 1.522(3) ? C3 C3A . 1.533(3) ? C3 H3 . 1.0000 ? C3A C4 . 1.525(2) ? C3A C9B . 1.535(2) ? C3A H3A . 1.0000 ? C4 C5 . 1.526(3) ? C4 H4A . 0.9900 ? C4 H4B . 0.9900 ? C5 C5A . 1.556(2) ? C5 H5A . 0.9900 ? C5 H5B . 0.9900 ? C5A C6 . 1.537(2) ? C5A C11 . 1.539(2) ? C5A C9A . 1.557(2) ? C6 C7 . 1.521(3) ? C6 H6 . 1.0000 ? C7 O10 . 1.439(2) ? C7 C8 . 1.477(3) ? C7 H7 . 1.0000 ? C8 O10 . 1.452(2) ? C8 C9 . 1.481(2) ? C8 H8 . 1.0000 ? C9 C17 . 1.341(3) ? C9 C9A . 1.514(2) ? C9A C9B . 1.527(2) ? C9A H9A . 1.0000 ? C9B H9B . 1.0000 ? C10 H10A . 0.9800 ? C10 H10B . 0.9800 ? C10 H10C . 0.9800 ? C11 H11A . 0.9800 ? C11 H11B . 0.9800 ? C11 H11C . 0.9800 ? C12 C13 . 1.489(2) ? C13 C14 . 1.342(2) ? C13 C15 . 1.512(2) ? C14 C16 . 1.496(2) ? C14 H14 . 0.9500 ? C15 H15A . 0.9800 ? C15 H15B . 0.9800 ? C15 H15C . 0.9800 ? C16 H16A . 0.9800 ? C16 H16B . 0.9800 ? C16 H16C . 0.9800 ? C17 H17A . 0.94(2) ? C17 H17B . 0.97(2) ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C3A H3A O4 2_665 1.00 2.45 3.353(2) 149 yes C5 H5B O3 . 0.99 2.33 2.752(2) 105 no C8 H8 O2 2_564 1.00 2.50 3.176(2) 124 yes C9A H9A O3 . 1.00 2.58 3.010(2) 106 no C14 H14 O10 4_566 0.95 2.57 3.423(2) 149 yes C16 H16B O4 . 0.98 2.45 2.862(2) 105 no loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C9B O1 C2 O2 . . . . 172.91(16) ? C9B O1 C2 C3 . . . . -8.26(18) ? O2 C2 C3 C10 . . . . -28.0(3) ? O1 C2 C3 C10 . . . . 153.32(16) ? O2 C2 C3 C3A . . . . -157.18(18) ? O1 C2 C3 C3A . . . . 24.10(18) ? C2 C3 C3A C4 . . . . 92.11(18) ? C10 C3 C3A C4 . . . . -34.6(2) ? C2 C3 C3A C9B . . . . -28.74(17) ? C10 C3 C3A C9B . . . . -155.42(17) ? C3 C3A C4 C5 . . . . -179.07(15) ? C9B C3A C4 C5 . . . . -63.29(19) ? C3A C4 C5 C5A . . . . 55.2(2) ? C4 C5 C5A C6 . . . . 118.63(17) ? C4 C5 C5A C11 . . . . -123.94(17) ? C4 C5 C5A C9A . . . . -1.2(2) ? C12 O3 C6 C7 . . . . -75.56(18) ? C12 O3 C6 C5A . . . . 159.27(14) ? C11 C5A C6 O3 . . . . -166.03(14) ? C5 C5A C6 O3 . . . . -47.40(18) ? C9A C5A C6 O3 . . . . 74.64(17) ? C11 C5A C6 C7 . . . . 70.81(18) ? C5 C5A C6 C7 . . . . -170.56(14) ? C9A C5A C6 C7 . . . . -48.52(18) ? O3 C6 C7 O10 . . . . -36.6(2) ? C5A C6 C7 O10 . . . . 84.87(18) ? O3 C6 C7 C8 . . . . -105.14(17) ? C5A C6 C7 C8 . . . . 16.3(2) ? C6 C7 C8 O10 . . . . 104.52(16) ? O10 C7 C8 C9 . . . . -102.71(17) ? C6 C7 C8 C9 . . . . 1.8(2) ? O10 C8 C9 C17 . . . . 128.89(18) ? C7 C8 C9 C17 . . . . -163.85(17) ? O10 C8 C9 C9A . . . . -52.2(2) ? C7 C8 C9 C9A . . . . 15.0(2) ? C17 C9 C9A C9B . . . . 1.8(3) ? C8 C9 C9A C9B . . . . -176.92(15) ? C17 C9 C9A C5A . . . . 130.09(19) ? C8 C9 C9A C5A . . . . -48.67(19) ? C6 C5A C9A C9 . . . . 65.44(17) ? C11 C5A C9A C9 . . . . -51.76(19) ? C5 C5A C9A C9 . . . . -173.70(14) ? C6 C5A C9A C9B . . . . -166.57(14) ? C11 C5A C9A C9B . . . . 76.22(19) ? C5 C5A C9A C9B . . . . -45.71(19) ? C2 O1 C9B C9A . . . . -133.99(14) ? C2 O1 C9B C3A . . . . -11.12(17) ? C9 C9A C9B O1 . . . . -78.72(17) ? C5A C9A C9B O1 . . . . 154.87(13) ? C9 C9A C9B C3A . . . . 164.45(14) ? C5A C9A C9B C3A . . . . 38.0(2) ? C4 C3A C9B O1 . . . . -99.98(16) ? C3 C3A C9B O1 . . . . 24.83(16) ? C4 C3A C9B C9A . . . . 16.8(2) ? C3 C3A C9B C9A . . . . 141.61(15) ? C6 C7 O10 C8 . . . . -111.03(17) ? C9 C8 O10 C7 . . . . 111.87(18) ? C6 O3 C12 O4 . . . . 8.5(3) ? C6 O3 C12 C13 . . . . -169.25(15) ? O4 C12 C13 C14 . . . . 16.9(3) ? O3 C12 C13 C14 . . . . -165.42(16) ? O4 C12 C13 C15 . . . . -160.91(18) ? O3 C12 C13 C15 . . . . 16.8(2) ? C12 C13 C14 C16 . . . . 2.7(3) ? C15 C13 C14 C16 . . . . -179.63(18) ?