#------------------------------------------------------------------------------ #$Date: 2023-04-05 18:09:22 +0200 (Wed, 05 Apr 2023) $ #$Revision: 282431 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/27/2022733.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022733 loop_ _publ_author_name 'N\"ather, Christian' 'Jess, Inke' _publ_section_title ; Synthesis, crystal structure and properties of bis(isoselenocyanato-\kN)tetrakis(4-methoxypyridine-\kN)cobalt(II) ; _journal_coeditor_code PK2678 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E Crystallographic Communications' _journal_page_first 216 _journal_page_last 220 _journal_paper_doi 10.1107/S2056989023001391 _journal_volume 79 _journal_year 2023 _chemical_formula_iupac '[Co (N C Se)2 (C6 H7 N1 O1)4]' _chemical_formula_moiety 'C26 H28 Co N6 O4 Se2' _chemical_formula_sum 'C26 H28 Co N6 O4 Se2' _chemical_formula_weight 705.39 _chemical_name_systematic ; Bis(isoselenocyanato-\kN)tetrakis(4-methoxypyridine-\kN)cobalt(II) ; _space_group_crystal_system orthorhombic _space_group_IT_number 61 _space_group_name_Hall '-P 2ac 2ab' _space_group_name_H-M_alt 'P b c a' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2016/6 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 10.0531(2) _cell_length_b 17.3479(4) _cell_length_c 34.3141(5) _cell_measurement_reflns_used 56525 _cell_measurement_temperature 200(2) _cell_measurement_theta_max 26.004 _cell_measurement_theta_min 1.187 _cell_volume 5984.4(2) _computing_cell_refinement ; X-Area (Stoe, 2008) ; _computing_data_collection ; X-Area (Stoe, 2008) ; _computing_data_reduction ; X-Area (Stoe, 2008) ; _computing_molecular_graphics ; DIAMOND (Brandenburg & Putz, 1999) ; _computing_publication_material ; Publcif (Westrip, 2010) ; _computing_structure_refinement ; SHELXL2016/6 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2014/5 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 200(2) _diffrn_measured_fraction_theta_full 0.994 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measurement_device_type 'Stoe IPDS-2' _diffrn_measurement_method 'Omega scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0345 _diffrn_reflns_av_unetI/netI 0.0146 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_l_max 42 _diffrn_reflns_limit_l_min -42 _diffrn_reflns_number 56525 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.004 _diffrn_reflns_theta_min 1.187 _exptl_absorpt_coefficient_mu 3.047 _exptl_absorpt_correction_T_max 0.738 _exptl_absorpt_correction_T_min 0.457 _exptl_absorpt_correction_type numerical _exptl_absorpt_process_details ; (X-Red and X-Shape; Stoe, 2008) ; _exptl_crystal_colour 'light pink' _exptl_crystal_density_diffrn 1.566 _exptl_crystal_description block _exptl_crystal_F_000 2824 _exptl_crystal_size_max 0.23 _exptl_crystal_size_mid 0.19 _exptl_crystal_size_min 0.17 _refine_diff_density_max 0.335 _refine_diff_density_min -0.475 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.073 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 356 _refine_ls_number_reflns 5862 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.073 _refine_ls_R_factor_all 0.0452 _refine_ls_R_factor_gt 0.0376 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0382P)^2^+4.2748P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0834 _refine_ls_wR_factor_ref 0.0871 _reflns_number_gt 5130 _reflns_number_total 5862 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file pk2678sup1.cif _cod_data_source_block I _cod_database_code 2022733 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_hkl_file ; -7 0 0 4.95 10.00 0 -8 0 0 21.13 9.84 0 -8 0 0 21.22 9.22 0 -9 0 0 -5.73 8.91 0 -9 0 0 -7.17 8.74 0 -9 0 0 7.88 6.85 0 -10 0 0 -5.30 8.14 0 -10 0 0 8.92 8.69 0 -10 0 0 -0.82 8.60 0 -11 0 0 7.58 8.61 0 -11 0 0 -0.26 8.36 0 -11 0 0 4.38 6.60 0 -12 0 0 358.65 10.12 0 -12 0 0 395.81 10.97 0 -12 0 0 349.47 11.59 0 -1 -1 0 2.10 15.53 0 -1 1 0 2.97 23.85 0 1 1 0 13.27 15.02 0 1 -1 0 -3.98 25.61 0 -3 1 0 1.32 14.02 0 -3 -1 0 2.06 13.53 0 -4 -1 0 797.09 11.76 0 -4 1 0 769.77 14.84 0 -5 -1 0 3.27 10.00 0 -5 1 0 -1.97 8.35 0 -6 1 0 217.74 11.97 0 -6 -1 0 211.28 11.04 0 -7 -1 0 -0.52 9.07 0 -7 1 0 8.68 10.56 0 -8 -1 0 26.68 6.81 0 -8 1 0 26.09 9.16 0 -8 1 0 34.09 10.08 0 -9 -1 0 -5.98 8.48 0 -9 1 0 3.87 9.20 0 -9 1 0 0.05 9.67 0 -9 -1 0 0.16 6.28 0 -9 1 0 1.60 8.58 0 -10 -1 0 157.71 9.33 0 -10 1 0 160.83 10.11 0 -10 -1 0 143.80 6.66 0 -10 1 0 142.13 11.34 0 -10 -1 0 136.06 9.77 0 -10 1 0 144.94 9.34 0 -11 1 0 3.74 6.56 0 -11 -1 0 10.71 9.32 0 -11 -1 0 11.52 8.54 0 -11 1 0 2.50 9.63 0 -11 -1 0 9.63 8.92 0 -11 1 0 11.64 10.83 0 -12 -1 0 -8.86 8.89 0 -12 1 0 -4.02 10.10 0 -12 -1 0 8.53 8.11 0 -12 1 0 -6.13 6.03 0 -12 -1 0 2.90 8.08 0 -12 1 0 -3.27 8.55 0 -12 1 0 14.72 9.21 0 0 -2 0 236.51 27.51 0 0 2 0 265.27 26.13 0 -1 -2 0 3.66 21.60 0 1 2 0 5.89 20.70 0 1 -2 0 -6.84 25.24 0 -1 2 0 5.50 17.17 0 -2 2 0 4.92 13.87 0 -2 -2 0 8.13 16.69 0 2 -2 0 3.82 13.64 0 2 2 0 3.58 16.13 0 -3 2 0 -7.43 15.16 0 -3 -2 0 -0.48 12.99 0 -4 -2 0 1382.79 13.85 0 -4 2 0 1389.32 15.01 0 -5 2 0 8.36 11.35 0 -5 -2 0 -3.47 9.65 0 -6 -2 0 143.61 10.88 0 -6 2 0 146.19 11.78 0 -6 2 0 148.80 13.00 0 -7 2 0 2.00 11.67 0 -7 2 0 -0.21 10.81 0 -7 -2 0 -2.05 6.54 0 -8 2 0 88.04 9.63 0 -8 -2 0 79.29 9.58 0 -8 2 0 70.45 10.52 0 -9 2 0 0.09 10.95 0 -9 -2 0 -0.87 8.74 0 -9 2 0 3.79 9.92 0 -10 -2 0 16.02 8.87 0 -10 2 0 9.94 11.21 0 -10 2 0 19.95 9.07 0 -10 2 0 19.33 8.56 0 -10 -2 0 7.21 8.59 0 -11 -2 0 4.01 10.24 0 -11 2 0 -0.19 9.34 0 -11 2 0 -0.46 10.37 0 -11 -2 0 10.67 8.43 0 -11 2 0 3.90 6.06 0 -11 -2 0 8.89 8.75 0 -11 2 0 2.89 10.67 0 -12 2 0 11.50 10.86 0 -12 2 0 9.33 9.48 0 -12 2 0 6.96 12.24 0 -12 -2 0 22.92 8.82 0 -12 -2 0 24.61 8.17 0 -12 2 0 18.81 8.80 0 -12 -2 0 17.96 8.42 0 0 3 0 3.97 22.20 0 0 -3 0 16.26 23.38 0 -1 3 0 10.40 22.03 0 1 -3 0 0.96 23.13 0 -1 -3 0 -0.44 13.27 0 1 3 0 2.64 18.55 0 2 -3 0 5280.66 35.97 0 2 3 0 5282.77 30.10 0 -2 3 0 5427.92 35.64 0 -2 -3 0 5363.74 30.33 0 -3 -3 0 6.56 11.97 0 3 -3 0 -2.04 14.67 0 3 3 0 -0.50 8.41 0 -3 3 0 1.05 14.74 0 -4 3 0 1391.25 17.49 0 -4 -3 0 1367.98 15.31 0 -4 3 0 1418.61 35.28 0 -5 -3 0 2.06 9.99 0 -5 3 0 3.99 13.59 0 -5 3 0 12.83 11.94 0 -6 3 0 157.04 9.32 0 -6 3 0 166.53 13.44 0 -6 -3 0 171.24 10.56 0 -7 -3 0 -3.01 9.20 0 -7 3 0 -9.11 10.88 0 -7 3 0 -0.60 13.59 0 -8 -3 0 5.79 9.65 0 -8 3 0 15.54 11.89 0 -8 3 0 6.65 10.51 0 -9 3 0 4.96 11.50 0 -9 -3 0 -5.71 8.76 0 -9 3 0 7.53 12.90 0 -9 3 0 3.42 10.18 0 -10 3 0 425.55 16.36 0 -10 -3 0 387.00 10.06 0 -10 3 0 400.51 16.30 0 -10 3 0 390.48 11.58 0 -11 3 0 4.89 13.02 0 -11 3 0 1.12 12.56 0 -11 3 0 -2.50 6.26 0 -11 3 0 -4.88 6.75 0 -11 -3 0 -5.85 8.64 0 -11 -3 0 2.92 7.95 0 -12 -3 0 19.61 8.24 0 -12 -3 0 21.00 8.55 0 -12 -3 0 12.12 8.76 0 -12 3 0 4.73 14.40 0 -12 3 0 5.15 14.53 0 -12 3 0 20.94 8.50 0 -12 3 0 16.20 9.30 0 -1 -4 0 2.73 17.10 0 -1 4 0 8.47 20.25 0 1 4 0 0.39 16.65 0 1 -4 0 0.71 21.38 0 -2 -4 0 22.14 13.86 0 2 4 0 18.59 13.48 0 2 -4 0 7.57 17.63 0 -2 4 0 29.70 17.01 0 3 -4 0 6.26 14.40 0 -3 4 0 9.73 15.58 0 -3 -4 0 2.24 12.03 0 3 4 0 -4.67 11.48 0 4 4 0 4713.67 21.97 0 4 -4 0 5010.00 25.90 0 -4 -4 0 4900.23 22.35 0 -4 4 0 4773.63 25.59 0 -5 4 0 -1.82 12.26 0 -5 -4 0 -4.68 9.42 0 -6 4 0 483.36 13.35 0 -6 4 0 465.34 28.62 0 -6 -4 0 460.74 8.87 0 -6 4 0 456.07 30.26 0 -7 -4 0 9.98 9.34 0 -7 4 0 1.99 16.60 0 -7 4 0 4.28 18.84 0 -7 4 0 6.16 10.47 0 -8 4 0 654.97 23.18 0 -8 4 0 649.01 12.28 0 -8 4 0 653.21 22.85 0 -8 -4 0 648.74 11.21 0 -9 4 0 4.57 10.10 0 -9 4 0 4.73 16.75 0 -9 4 0 0.59 16.02 0 -9 -4 0 8.78 8.86 0 -10 4 0 21.26 18.40 0 -10 -4 0 14.80 8.55 0 -10 4 0 23.43 9.74 0 -10 4 0 19.79 20.05 0 -11 -4 0 -6.76 8.74 0 -11 -4 0 -6.09 8.33 0 -11 4 0 6.56 9.24 0 -12 4 0 77.66 9.95 0 -12 4 0 51.31 9.02 0 -12 -4 0 79.68 6.48 0 -12 -4 0 80.44 8.66 0 0 5 0 6.73 16.02 0 0 -5 0 -1.37 12.10 0 -1 5 0 3.00 11.74 0 1 -5 0 7.48 17.80 0 -1 -5 0 2.89 14.46 0 1 5 0 1.22 9.85 0 3 -5 0 9.14 13.82 0 -3 -5 0 3.75 11.37 0 3 5 0 4.61 10.75 0 -3 5 0 5.76 13.04 0 4 -5 0 1001.60 16.50 0 -4 -5 0 1010.30 11.23 0 -4 5 0 976.95 13.48 0 4 5 0 995.22 13.53 0 -5 5 0 14.06 12.51 0 -5 -5 0 5.32 9.51 0 5 5 0 -0.19 6.72 0 5 -5 0 5.28 12.44 0 -6 -5 0 37.47 8.76 0 -6 5 0 34.92 12.06 0 -7 5 0 6.99 11.14 0 -7 -5 0 14.59 9.03 0 -8 5 0 244.56 11.55 0 -8 -5 0 272.39 10.04 0 -9 -5 0 0.93 8.62 0 -9 5 0 3.55 7.73 0 -10 -5 0 525.41 10.57 0 -10 5 0 519.62 11.93 0 -11 -5 0 4.50 8.03 0 -11 -5 0 4.61 6.00 0 -11 5 0 12.75 9.32 0 -12 -5 0 19.37 8.22 0 -12 5 0 8.22 9.37 0 0 6 0 9999.99 35.73 0 -1 6 0 -1.93 10.41 0 -1 -6 0 -9.05 8.94 0 1 -6 0 -0.18 15.43 0 1 6 0 2.26 12.10 0 2 6 0 91.59 11.99 0 2 -6 0 90.91 11.93 0 -2 -6 0 86.05 8.93 0 -2 6 0 83.89 13.57 0 3 -6 0 -5.56 14.76 0 -3 6 0 6.47 9.29 0 3 6 0 2.12 7.70 0 3 -6 0 3.66 15.08 0 -3 -6 0 -0.64 7.70 0 -4 -6 0 1116.11 13.69 0 4 -6 0 1157.05 17.05 0 -4 6 0 1171.09 17.01 0 4 6 0 1125.52 13.70 0 5 -6 0 8.13 12.98 0 5 6 0 -0.33 6.63 0 -5 6 0 -1.36 12.38 0 -5 -6 0 3.22 9.39 0 -6 -6 0 23.30 9.33 0 6 -6 0 10.94 11.65 0 -6 6 0 14.76 11.37 0 -7 6 0 2.29 8.03 0 -7 -6 0 4.60 6.63 0 -8 6 0 15.70 10.94 0 -8 -6 0 8.24 9.19 0 -9 6 0 -1.47 9.68 0 -9 -6 0 2.30 9.20 0 -10 -6 0 55.08 8.86 0 -10 6 0 74.44 10.24 0 -11 6 0 7.48 9.54 0 -11 -6 0 8.98 8.03 0 0 -7 0 23.03 13.74 0 0 7 0 13.48 12.48 0 -1 7 0 15.86 13.04 0 -1 -7 0 11.71 12.13 0 1 7 0 4.75 8.27 0 1 -7 0 16.20 13.54 0 -2 -7 0 71.08 11.77 0 2 -7 0 70.16 13.92 0 2 7 0 79.08 11.46 0 -2 7 0 75.09 9.20 0 3 7 0 1.94 7.47 0 3 -7 0 1.37 13.97 0 -3 7 0 -3.20 13.04 0 -3 -7 0 -5.05 10.50 0 -4 -7 0 58.53 7.13 0 -4 7 0 53.50 13.06 0 4 -7 0 55.83 13.67 0 4 7 0 66.16 10.54 0 5 7 0 -1.01 6.48 0 -5 7 0 -5.15 11.94 0 5 -7 0 -1.04 12.20 0 -5 -7 0 -2.64 6.52 0 -6 -7 0 10.22 9.18 0 6 7 0 14.38 9.12 0 -6 7 0 9.39 11.51 0 6 -7 0 4.43 11.55 0 -7 -7 0 7.91 9.29 0 -7 7 0 -1.65 8.21 0 -8 7 0 108.28 10.92 0 -8 -7 0 95.79 6.77 0 -9 7 0 1.77 9.59 0 -9 -7 0 -1.21 9.51 0 -10 7 0 382.27 11.63 0 -10 -7 0 355.39 10.09 0 -11 -7 0 -9.46 8.32 0 -11 7 0 -1.14 6.50 0 0 -8 0 9622.89 32.18 0 0 8 0 9734.60 30.58 0 -1 8 0 -1.53 12.20 0 1 8 0 7.70 11.43 0 -1 -8 0 3.38 11.83 0 1 -8 0 0.59 13.43 0 2 8 0 48.32 10.78 0 -2 -8 0 61.43 11.08 0 -2 8 0 69.12 12.56 0 2 -8 0 45.87 13.10 0 3 -8 0 5.69 12.78 0 -3 8 0 1.28 12.53 0 -3 -8 0 11.41 10.90 0 3 8 0 1.75 7.17 0 -4 8 0 248.07 13.49 0 4 -8 0 260.14 24.55 0 4 -8 0 258.83 10.49 0 4 -8 0 269.01 24.53 0 -4 -8 0 248.23 8.03 0 4 8 0 277.72 7.79 0 -5 8 0 0.88 11.70 0 5 8 0 11.37 9.28 0 -5 -8 0 3.48 7.10 0 5 -8 0 3.68 8.29 0 -6 8 0 20.42 11.76 0 -6 -8 0 14.20 9.39 0 6 -8 0 21.34 11.86 0 6 8 0 15.81 9.48 0 -7 -8 0 18.95 8.67 0 -7 8 0 13.29 11.11 0 7 -8 0 -7.95 11.94 0 -8 8 0 482.57 9.89 0 -8 -8 0 486.81 10.42 0 -9 8 0 13.58 7.48 0 -9 -8 0 3.75 9.07 0 -10 8 0 -5.51 10.21 0 -10 -8 0 6.79 8.63 0 -11 8 0 6.59 9.61 0 -11 -8 0 7.99 8.56 0 0 9 0 -6.56 8.02 0 0 -9 0 -6.51 12.14 0 -1 -9 0 7.44 8.04 0 -1 9 0 -1.07 11.38 0 1 -9 0 -6.19 12.23 0 1 9 0 13.65 10.96 0 2 -9 0 2202.35 17.14 0 2 9 0 2201.16 14.77 0 -2 9 0 2289.15 18.57 0 -2 -9 0 2199.05 14.81 0 -3 9 0 -3.04 12.66 0 3 9 0 -3.02 10.05 0 3 -9 0 8.47 13.40 0 -3 -9 0 -2.22 7.31 0 4 -9 0 1640.56 26.54 0 -4 9 0 1572.78 16.58 0 -4 -9 0 1551.28 11.97 0 4 -9 0 1582.32 17.92 0 4 9 0 1545.18 12.06 0 4 -9 0 1649.09 27.57 0 5 -9 0 2.83 8.95 0 5 9 0 6.69 6.51 0 -5 -9 0 9.54 6.79 0 -5 9 0 6.02 8.35 0 -6 -9 0 -0.41 6.91 0 6 9 0 17.02 9.22 0 6 -9 0 7.65 8.70 0 -6 9 0 12.93 7.78 0 7 -9 0 4.37 7.52 0 7 9 0 -4.88 6.14 0 -7 9 0 4.24 10.78 0 -7 -9 0 8.43 6.21 0 -8 -9 0 53.61 8.59 0 -8 9 0 36.80 10.26 0 -9 9 0 9.03 7.35 0 -9 -9 0 11.05 6.34 0 -10 -9 0 -3.69 8.66 0 -10 9 0 16.85 9.79 0 -11 9 0 11.59 9.59 0 -11 -9 0 -0.69 5.76 0 0 -10 0 273.78 8.95 0 0 10 0 282.50 11.43 0 -1 -10 0 -0.36 11.03 0 -1 10 0 2.90 10.51 0 1 -10 0 10.86 11.50 0 1 10 0 3.86 7.23 0 2 -10 0 58.69 12.62 0 -2 -10 0 61.73 10.38 0 2 10 0 66.57 9.98 0 -2 10 0 55.88 11.99 0 3 -10 0 8.58 9.04 0 -3 -10 0 17.02 9.76 0 3 10 0 1.60 9.62 0 -3 10 0 11.25 10.97 0 4 -10 0 2434.87 26.67 0 4 10 0 2413.41 15.90 0 -4 10 0 2368.64 17.33 0 4 -10 0 2452.56 27.06 0 4 -10 0 2371.37 18.67 0 -4 -10 0 2292.42 15.69 0 5 10 0 18.36 9.52 0 5 -10 0 -0.47 12.03 0 -5 -10 0 10.83 9.35 0 -5 10 0 -8.01 11.02 0 6 10 0 1477.96 12.81 0 -6 10 0 1601.81 15.75 0 -6 -10 0 1547.26 13.09 0 6 -10 0 1585.99 16.73 0 7 10 0 3.36 6.24 0 -7 10 0 3.49 10.89 0 7 -10 0 7.45 10.76 0 -7 -10 0 2.77 8.79 0 8 -10 0 16.20 11.19 0 -8 10 0 5.97 10.19 0 -8 -10 0 -0.99 8.56 0 -9 -10 0 4.49 6.17 0 -9 10 0 12.48 9.69 0 -10 10 0 49.23 7.66 0 -10 -10 0 65.36 8.45 0 0 11 0 -6.12 10.14 0 0 -11 0 -0.23 11.00 0 1 11 0 8.15 10.01 0 -1 -11 0 -2.61 10.63 0 1 -11 0 1.47 8.09 0 -1 11 0 -2.54 10.31 0 2 11 0 426.10 11.26 0 2 -11 0 428.12 13.46 0 -2 11 0 428.72 12.60 0 -2 -11 0 413.94 11.83 0 -3 11 0 1.32 10.87 0 3 -11 0 3.33 11.85 0 3 11 0 -5.15 9.94 0 -3 -11 0 13.50 9.73 0 -4 11 0 -3.29 7.67 0 4 11 0 14.63 9.83 0 4 -11 0 4.46 12.84 0 -4 -11 0 -2.05 10.01 0 4 -11 0 16.67 12.10 0 5 11 0 -3.30 6.20 0 5 -11 0 -10.80 12.07 0 -5 11 0 6.78 11.33 0 -5 -11 0 -8.64 8.99 0 6 -11 0 248.67 12.86 0 -6 11 0 242.78 11.73 0 -6 -11 0 232.67 9.50 0 6 11 0 226.36 7.16 0 7 11 0 20.37 8.57 0 -7 11 0 0.75 10.09 0 7 -11 0 7.37 11.18 0 -7 -11 0 14.56 8.96 0 -8 11 0 -7.85 10.45 0 8 11 0 -1.69 8.37 0 8 -11 0 1.60 10.86 0 -8 -11 0 8.84 6.12 0 -9 11 0 13.05 9.90 0 -9 -11 0 4.98 6.12 0 -10 -11 0 34.80 8.85 0 -10 11 0 49.44 9.95 0 0 -12 0 354.51 11.86 0 0 12 0 324.25 11.50 0 1 -12 0 7.08 10.71 0 -1 -12 0 -10.99 7.83 0 -1 12 0 -2.63 9.62 0 1 12 0 -4.50 7.21 0 -2 -12 0 140.28 10.69 0 2 -12 0 143.40 11.78 0 -2 12 0 135.25 7.85 0 2 12 0 131.00 10.51 0 -3 -12 0 -2.48 7.11 0 -3 12 0 -5.03 7.49 0 3 -12 0 7.27 8.39 0 3 12 0 9.82 6.90 0 -4 12 0 82.25 11.03 0 4 12 0 106.06 9.63 0 -4 -12 0 69.56 10.10 0 4 -12 0 85.04 12.11 0 4 -12 0 103.44 11.51 0 5 -12 0 -1.45 18.70 0 -5 12 0 9.11 10.94 0 5 12 0 11.56 8.73 0 5 -12 0 -4.97 8.29 0 -5 -12 0 11.53 9.15 0 5 -12 0 -0.26 17.99 0 6 12 0 482.69 9.90 0 -6 12 0 511.84 12.26 0 -6 -12 0 487.01 10.57 0 6 -12 0 480.09 12.99 0 -7 12 0 -5.11 9.75 0 7 -12 0 11.18 10.63 0 -7 -12 0 0.09 8.36 0 7 12 0 3.85 6.31 0 -8 12 0 50.59 10.82 0 8 -12 0 55.82 10.49 0 8 12 0 43.19 8.24 0 -8 -12 0 57.72 8.62 0 -9 12 0 -9.31 9.97 0 -9 -12 0 0.86 8.52 0 -10 12 0 39.62 9.70 0 -10 -12 0 35.09 8.09 0 0 13 0 -4.31 7.17 0 0 -13 0 16.00 11.03 0 1 13 0 8.41 9.94 0 -1 -13 0 10.71 7.40 0 -1 13 0 8.23 10.02 0 1 -13 0 -1.65 7.48 0 -2 -13 0 188.80 11.08 0 2 -13 0 181.01 12.54 0 -2 13 0 202.65 11.35 0 2 13 0 189.84 10.69 0 3 -13 0 13.64 12.09 0 3 13 0 13.62 9.43 0 -3 13 0 22.84 10.48 0 -3 -13 0 -2.52 9.83 0 4 13 0 2342.15 13.65 0 4 -13 0 2490.42 22.35 0 4 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139.13 9.07 0 -2 -6 -2 128.74 12.18 0 2 -6 2 131.35 15.16 0 3 -6 2 4671.78 25.51 0 -3 6 -2 4602.16 24.84 0 3 6 -2 4704.84 22.54 0 -3 6 2 4655.42 26.59 0 -3 -6 2 4591.22 20.97 0 3 6 2 4837.56 22.24 0 3 -6 -2 4713.28 27.89 0 -3 -6 -2 4626.96 21.78 0 -4 -6 -2 80.99 7.74 0 4 -6 2 93.29 12.62 0 -4 6 2 81.00 13.13 0 -4 6 -2 78.13 8.43 0 4 -6 -2 93.37 13.59 0 4 6 -2 93.66 10.46 0 -4 -6 2 73.11 7.16 0 4 6 2 83.68 10.21 0 -5 6 2 109.66 13.80 0 -5 -6 2 126.06 10.39 0 -5 6 -2 116.15 13.13 0 5 6 2 102.89 9.61 0 5 6 -2 129.52 10.35 0 5 -6 2 122.75 13.44 0 5 -6 -2 123.16 13.87 0 -5 -6 -2 110.84 9.89 0 6 6 -2 11.25 9.05 0 -6 -6 2 5.90 6.70 0 -6 6 -2 23.14 11.16 0 6 -6 2 0.73 11.32 0 -6 6 2 5.27 11.95 0 -6 -6 -2 13.19 9.70 0 -7 6 2 1988.68 17.23 0 -7 -6 -2 1986.41 14.20 0 -7 -6 2 2044.47 14.79 0 -7 6 -2 2003.96 16.75 0 -8 6 -2 -4.86 10.56 0 -8 -6 -2 8.86 8.72 0 -8 -6 2 27.80 9.00 0 -8 6 2 11.41 10.76 0 -9 -6 2 73.58 9.61 0 -9 -6 -2 74.14 9.53 0 -9 6 2 79.96 11.11 0 -9 6 -2 63.18 7.44 0 -10 -6 2 1.41 8.33 0 -10 6 2 20.75 10.04 0 -10 6 -2 12.88 6.92 0 -10 -6 2 10.13 8.81 0 -10 -6 -2 -0.02 6.15 0 -11 -6 2 10.61 8.50 0 -11 -6 -2 7.76 8.52 0 -11 6 -2 -2.45 9.71 0 -11 -6 2 27.08 8.16 0 -11 6 2 8.46 6.79 0 0 7 -2 1.94 12.94 0 0 -7 2 7.17 13.40 0 0 7 2 3.19 11.98 0 0 -7 -2 -2.84 14.13 0 1 7 2 9086.39 30.95 0 -1 -7 2 8813.38 30.94 0 1 7 -2 8923.03 29.75 0 1 -7 2 8958.41 32.36 0 -1 7 -2 9132.07 33.15 0 1 -7 -2 8881.24 34.85 0 -2 -7 2 637.20 13.28 0 -2 7 -2 671.37 11.84 0 -2 -7 -2 675.64 13.22 0 -2 7 2 675.27 15.31 0 2 -7 2 674.61 15.52 0 2 7 -2 684.45 13.38 0 2 7 2 681.36 13.09 0 2 -7 2 680.08 15.25 0 2 -7 -2 698.07 13.43 0 3 7 -2 153.18 11.28 0 -3 -7 2 160.95 11.39 0 3 -7 -2 161.37 13.83 0 -3 -7 -2 148.33 11.15 0 -3 7 -2 150.73 12.30 0 -3 7 2 158.10 13.42 0 3 7 2 159.65 10.88 0 3 -7 -2 160.81 14.78 0 3 -7 2 169.36 9.72 0 3 -7 2 164.79 15.48 0 4 -7 2 180.33 10.10 0 -4 7 2 182.59 13.34 0 4 7 -2 180.23 7.70 0 -4 -7 -2 168.25 8.06 0 4 7 2 178.49 10.49 0 -4 -7 2 156.97 10.46 0 -4 7 -2 177.88 13.42 0 4 -7 -2 188.64 13.88 0 -5 -7 2 1915.07 12.99 0 5 7 2 2021.01 14.50 0 5 -7 -2 2082.69 19.12 0 5 -7 2 2035.18 17.74 0 -5 7 -2 1935.18 17.13 0 -5 -7 -2 1904.31 14.28 0 -5 7 2 1951.36 15.94 0 5 7 -2 1948.42 14.91 0 6 7 -2 65.99 9.23 0 6 -7 2 73.68 8.21 0 -6 -7 -2 75.24 6.81 0 6 7 2 71.95 9.84 0 -6 7 2 70.18 8.95 0 6 -7 -2 79.44 8.80 0 -6 -7 2 77.08 6.61 0 -6 7 -2 81.17 11.29 0 -7 7 -2 527.87 9.97 0 -7 -7 2 506.31 10.75 0 -7 -7 -2 532.83 10.64 0 -7 7 2 513.17 12.76 0 -8 -7 2 2.47 6.28 0 -8 7 -2 16.85 10.47 0 -8 7 2 2.41 10.27 0 -8 -7 -2 7.17 6.05 0 -9 -7 -2 15.57 9.23 0 -9 7 2 -1.54 10.51 0 -9 -7 2 14.74 8.87 0 -9 7 -2 25.47 6.86 0 -10 7 -2 7.30 7.12 0 -10 7 2 16.91 9.61 0 -10 -7 -2 5.38 6.15 0 -10 -7 2 0.79 8.48 0 -11 -7 -2 93.97 8.86 0 -11 7 -2 74.80 9.64 0 -11 7 2 75.28 10.10 0 -11 -7 2 79.82 8.77 0 0 -8 -2 686.16 15.10 0 0 8 2 677.27 11.47 0 0 -8 2 695.25 11.71 0 0 8 -2 692.67 14.34 0 -1 -8 2 2365.92 18.32 0 -1 8 2 2322.67 17.18 0 1 8 -2 2358.77 16.22 0 1 -8 2 2327.80 20.23 0 1 8 2 2386.41 18.36 0 -1 8 -2 2307.12 19.47 0 1 -8 -2 2348.24 20.26 0 -1 -8 -2 2402.17 18.76 0 2 8 -2 883.94 13.91 0 2 8 2 883.46 13.19 0 -2 -8 -2 892.91 13.70 0 -2 -8 2 902.22 14.12 0 -2 8 -2 879.98 14.80 0 2 -8 2 889.28 15.75 0 2 -8 -2 901.82 17.26 0 -2 8 2 891.86 15.60 0 3 8 2 3386.69 18.55 0 -3 8 2 3306.86 21.76 0 -3 -8 2 3257.46 16.79 0 -3 -8 -2 3293.54 18.40 0 3 8 -2 3399.13 17.15 0 -3 8 -2 3364.01 21.21 0 3 -8 2 3431.04 28.36 0 3 -8 -2 3470.17 23.88 0 3 -8 -2 3447.10 28.82 0 3 -8 2 3355.68 20.04 0 -4 8 2 19.78 12.35 0 4 8 -2 1.80 9.57 0 4 -8 2 9.10 20.06 0 4 -8 -2 9.88 18.82 0 4 -8 -2 2.30 13.37 0 4 -8 2 15.48 13.06 0 4 8 2 4.34 6.87 0 -4 -8 -2 13.85 9.87 0 -4 8 -2 4.37 12.72 0 -4 -8 2 25.50 9.56 0 5 8 -2 111.76 6.99 0 -5 8 2 135.45 12.69 0 -5 -8 -2 114.14 9.82 0 -5 8 -2 111.20 11.57 0 5 -8 -2 116.80 9.62 0 -5 -8 2 115.05 6.94 0 5 8 2 126.88 10.02 0 5 -8 2 100.50 11.86 0 6 -8 2 23.58 11.63 0 -6 8 2 9.27 11.85 0 -6 8 -2 28.37 11.66 0 6 -8 -2 22.96 11.96 0 -6 -8 2 4.83 6.29 0 6 8 2 9.25 9.43 0 6 8 -2 12.30 8.80 0 -6 -8 -2 14.24 6.64 0 -7 8 -2 521.67 12.75 0 -7 8 2 514.44 12.52 0 -7 -8 2 511.65 11.10 0 7 8 -2 512.94 10.89 0 7 -8 2 564.57 13.44 0 -7 -8 -2 535.70 10.82 0 7 -8 -2 567.30 13.35 0 -8 8 2 5.88 11.02 0 -8 -8 -2 -5.06 8.40 0 -8 8 -2 -6.09 7.47 0 -8 -8 2 16.12 8.68 0 -9 8 -2 186.10 8.25 0 -9 8 2 195.50 8.43 0 -9 -8 2 197.70 7.45 0 -9 -8 -2 189.85 7.03 0 -10 8 -2 12.68 9.27 0 -10 8 2 8.95 9.85 0 -10 -8 2 8.99 8.22 0 -10 -8 -2 -5.86 6.16 0 -11 -8 -2 45.41 8.46 0 -11 8 -2 30.33 9.80 0 -11 -8 2 42.59 6.18 0 -11 8 2 54.59 10.00 0 0 -9 -2 -5.84 8.08 0 0 9 2 12.64 10.28 0 0 9 -2 -8.32 8.14 0 0 -9 2 1.54 12.15 0 -1 9 -2 18.15 11.65 0 1 -9 2 12.44 12.32 0 1 9 2 12.77 10.69 0 1 9 -2 7.64 11.18 0 -1 -9 2 11.09 11.65 0 -1 -9 -2 17.40 7.91 0 1 -9 -2 18.34 12.49 0 -1 9 2 2.64 7.38 0 2 9 -2 815.11 10.91 0 2 9 2 796.26 12.66 0 -2 9 -2 767.82 11.28 0 2 -9 2 785.61 11.79 0 -2 9 2 788.55 11.96 0 -2 -9 2 766.56 10.79 0 -2 -9 -2 778.92 10.37 0 2 -9 -2 791.57 16.08 0 3 -9 2 86.50 12.44 0 3 -9 -2 82.24 13.91 0 3 -9 2 84.96 9.83 0 -3 9 -2 76.16 12.13 0 -3 9 2 83.69 12.82 0 3 9 -2 85.59 10.53 0 -3 -9 2 86.65 10.34 0 3 9 2 76.06 10.20 0 -3 -9 -2 76.03 10.53 0 -4 9 -2 954.69 14.59 0 -4 -9 -2 1010.63 12.33 0 4 -9 2 1023.21 24.85 0 -4 9 2 1020.45 15.54 0 4 -9 2 1002.14 13.05 0 4 9 2 1021.85 12.47 0 4 9 -2 1012.34 12.80 0 -4 -9 2 985.02 12.24 0 4 -9 -2 1022.86 23.67 0 4 -9 -2 992.03 16.67 0 -5 9 -2 1244.96 14.73 0 5 9 2 1201.53 12.86 0 5 -9 -2 1213.78 16.41 0 -5 9 2 1208.11 15.81 0 5 9 -2 1188.20 11.07 0 -5 -9 -2 1182.38 12.86 0 -5 -9 2 1206.58 12.41 0 5 -9 2 1291.61 15.50 0 6 9 -2 425.89 10.98 0 6 -9 -2 449.35 13.07 0 -6 -9 2 428.80 10.86 0 -6 9 -2 424.57 12.69 0 6 -9 2 448.36 9.85 0 -6 9 2 430.09 12.68 0 -6 -9 -2 445.05 10.75 0 6 9 2 433.50 10.46 0 7 -9 2 3.77 10.79 0 -7 -9 -2 4.01 6.38 0 7 9 2 15.95 8.59 0 7 -9 -2 -2.85 10.77 0 -7 9 -2 11.52 7.55 0 -7 9 2 1.33 11.20 0 -7 -9 2 -4.26 9.56 0 7 9 -2 9.99 9.25 0 -8 9 2 23.29 11.02 0 -8 9 -2 36.20 10.07 0 -8 -9 -2 42.77 8.70 0 -8 -9 2 25.04 9.41 0 -9 9 -2 35.70 7.03 0 -9 9 2 49.15 10.39 0 -9 -9 -2 43.06 8.54 0 -9 -9 2 29.07 6.07 0 -10 -9 -2 49.95 6.51 0 -10 9 -2 55.10 10.02 0 -10 9 2 58.05 10.11 0 -10 -9 2 58.82 8.22 0 -11 -9 2 0.92 8.00 0 -11 -9 -2 0.66 8.22 0 -11 9 -2 8.29 9.34 0 -11 9 2 7.06 9.59 0 0 10 2 142.82 10.99 0 0 -10 -2 130.48 12.21 0 0 10 -2 136.43 11.56 0 0 -10 2 132.21 12.14 0 1 10 -2 472.22 9.63 0 1 10 2 491.06 11.44 0 1 -10 2 507.48 13.32 0 -1 -10 2 467.44 9.99 0 -1 10 2 492.25 10.55 0 -1 10 -2 489.92 9.64 0 1 -10 -2 482.18 14.62 0 -1 -10 -2 462.04 11.96 0 -2 -10 -2 310.90 8.43 0 -2 10 2 317.34 12.61 0 2 10 -2 327.41 11.47 0 2 -10 2 300.02 13.26 0 -2 -10 2 300.98 11.52 0 2 10 2 315.87 10.90 0 -2 10 -2 299.67 12.36 0 2 -10 -2 304.01 14.19 0 3 -10 2 5457.67 29.17 0 3 -10 -2 5461.09 26.34 0 -3 10 -2 5352.99 23.36 0 -3 -10 2 5262.65 21.16 0 3 10 2 5340.15 19.66 0 3 -10 2 5379.90 24.85 0 -3 -10 -2 5119.00 20.74 0 -3 10 2 5383.30 24.30 0 3 10 -2 5433.94 21.81 0 4 -10 -2 6.49 12.88 0 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13.00 0 5 11 -2 2118.43 13.11 0 5 -11 -2 2212.56 49.33 0 -5 -11 -2 2180.06 14.58 0 -5 11 -2 2213.10 16.79 0 -5 11 2 2216.10 16.92 0 5 -11 -2 2126.15 18.79 0 5 11 2 2125.28 12.86 0 5 -11 2 2250.14 17.96 0 -6 -11 2 90.80 9.28 0 -6 -11 -2 95.78 9.37 0 -6 11 2 86.66 10.96 0 6 -11 -2 93.32 11.53 0 6 11 -2 96.89 9.26 0 -6 11 -2 103.09 11.33 0 6 -11 2 90.91 11.78 0 6 11 2 94.60 8.90 0 7 11 2 847.91 9.14 0 7 -11 -2 971.14 14.71 0 7 -11 2 847.79 11.34 0 -7 -11 2 891.19 11.63 0 7 11 -2 833.34 9.78 0 -7 -11 -2 869.51 11.38 0 -7 11 2 849.66 11.38 0 -7 11 -2 834.25 10.52 0 -8 11 2 14.13 10.28 0 -8 -11 2 2.50 8.93 0 -8 11 -2 34.51 10.19 0 -8 -11 -2 19.35 6.09 0 8 -11 2 6.79 10.54 0 8 -11 -2 9.01 10.54 0 8 11 -2 29.32 8.83 0 -9 11 -2 2.90 9.77 0 -9 -11 2 19.15 8.70 0 -9 11 2 13.20 6.63 0 -9 -11 -2 26.00 8.43 0 -10 -11 2 21.94 8.04 0 -10 11 -2 14.13 9.15 0 -10 11 2 4.13 6.67 0 -10 -11 -2 -2.96 7.97 0 0 12 -2 4.56 10.40 0 0 -12 -2 13.76 10.39 0 0 -12 2 2.08 11.41 0 0 12 2 13.07 9.80 0 -1 12 -2 556.84 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24.19 10.97 0 -11 2 -3 16.49 11.02 0 -12 2 3 58.24 11.75 0 -12 -2 -3 44.31 6.76 0 -12 2 3 76.43 9.78 0 -12 2 -3 68.79 6.53 0 -12 2 -3 61.16 9.75 0 -12 2 3 54.81 10.83 0 -12 2 -3 83.51 13.07 0 -12 2 3 68.34 9.21 0 -12 -2 3 52.67 9.50 0 -12 -2 -3 63.71 6.36 0 -12 -2 3 66.14 8.72 0 -12 -2 3 69.66 8.57 0 -12 2 -3 57.38 11.48 0 0 -3 3 8.83 23.06 0 0 3 -3 14.79 22.80 0 0 -3 -3 8.80 19.61 0 0 3 3 3.63 17.93 0 0 -3 3 3.25 17.10 0 1 -3 -3 2016.88 32.58 0 -1 3 -3 2060.61 29.84 0 1 -3 3 2076.63 30.28 0 -1 -3 3 2082.03 26.62 0 -1 3 -3 2009.60 28.50 0 -1 3 3 2063.92 30.65 0 1 -3 -3 2024.53 29.53 0 -1 -3 -3 2037.76 24.98 0 1 3 3 2024.82 24.55 0 1 3 -3 1972.59 22.82 0 1 -3 3 2067.48 29.85 0 2 -3 -3 961.75 31.39 0 -2 -3 -3 963.05 14.82 0 -2 3 -3 973.73 27.73 0 2 -3 -3 998.15 25.51 0 -2 3 3 998.53 24.76 0 2 3 -3 964.86 15.18 0 2 3 3 991.53 17.71 0 2 -3 3 964.88 32.00 0 -2 -3 3 1019.25 18.32 0 -2 3 3 981.23 27.50 0 -2 3 -3 962.70 17.64 0 2 -3 3 990.40 21.89 0 3 3 -3 1799.05 19.44 0 -3 -3 -3 1769.58 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4 3 3672.87 26.68 0 1 -4 3 3488.59 30.39 0 -1 4 3 3594.71 31.33 0 -1 -4 -3 3588.08 27.29 0 -1 4 -3 3595.31 30.29 0 1 4 -3 3519.84 25.17 0 1 -4 3 3519.50 31.13 0 -1 -4 3 3564.66 28.14 0 2 -4 3 90.89 19.30 0 2 -4 -3 95.86 18.87 0 2 -4 -3 90.92 19.80 0 -2 4 -3 94.92 16.38 0 2 -4 3 100.23 12.09 0 2 4 -3 98.15 15.07 0 -2 -4 3 90.85 11.06 0 -2 -4 -3 91.21 9.66 0 2 4 3 91.33 9.16 0 -2 4 3 88.65 17.99 0 3 4 -3 356.98 12.81 0 3 -4 -3 376.62 16.91 0 3 -4 3 368.15 15.63 0 -3 4 -3 364.29 21.95 0 3 -4 -3 367.06 23.44 0 -3 -4 3 340.68 10.28 0 3 -4 3 367.46 25.63 0 3 4 3 375.51 12.57 0 -3 4 3 357.32 16.16 0 -3 -4 -3 356.08 9.69 0 -3 4 -3 350.95 11.65 0 -4 4 3 355.76 23.03 0 -4 4 -3 358.11 27.13 0 4 4 -3 348.23 9.26 0 -4 4 3 354.54 13.95 0 4 -4 3 366.40 13.40 0 -4 -4 -3 347.96 8.78 0 -4 -4 3 360.48 11.82 0 4 -4 -3 368.15 10.79 0 -4 4 -3 350.75 13.35 0 -5 4 -3 191.42 24.34 0 -5 -4 -3 187.53 7.95 0 -5 -4 3 223.88 11.18 0 -5 4 3 190.89 19.93 0 -5 4 3 194.08 13.14 0 -5 4 -3 195.37 12.26 0 5 4 -3 197.22 8.43 0 -6 -4 -3 1600.43 13.43 0 -6 -4 3 1639.34 14.76 0 -6 4 3 1621.93 30.52 0 -6 4 -3 1588.63 33.14 0 -6 4 3 1637.65 17.08 0 -6 4 -3 1566.01 13.45 0 -7 4 -3 73.24 18.93 0 -7 4 3 76.53 15.38 0 -7 4 -3 85.52 7.95 0 -7 -4 -3 56.27 6.56 0 -7 -4 3 86.03 9.85 0 -7 4 3 80.16 11.41 0 -7 4 -3 74.21 15.69 0 -8 4 -3 62.41 17.07 0 -8 4 3 58.51 17.65 0 -8 4 -3 59.58 15.85 0 -8 4 3 70.76 11.23 0 -8 4 -3 45.82 7.77 0 -8 -4 -3 62.67 9.20 0 -8 -4 3 51.28 9.76 0 -9 4 -3 77.46 15.40 0 -9 4 -3 97.65 10.02 0 -9 -4 3 78.00 9.12 0 -9 4 -3 83.36 17.85 0 -9 4 3 91.45 10.49 0 -9 -4 -3 71.27 9.21 0 -9 -4 3 85.91 9.33 0 -9 4 3 87.93 16.56 0 -10 4 3 16.13 16.05 0 -10 4 3 24.62 10.34 0 -10 -4 -3 19.69 8.99 0 -10 4 -3 18.71 18.87 0 -10 4 3 12.02 17.73 0 -10 -4 3 11.48 8.41 0 -10 4 -3 17.71 17.92 0 -10 -4 3 21.13 5.86 0 -10 4 -3 22.24 9.42 0 -11 -4 3 7.26 8.50 0 -11 4 3 15.43 8.73 0 -11 -4 -3 9.53 6.18 0 -11 4 -3 15.51 9.21 0 -11 -4 3 -2.11 8.91 0 -11 4 3 3.39 9.58 0 -12 -4 -3 12.75 8.18 0 -12 4 3 4.11 8.64 0 -12 4 -3 -1.74 9.08 0 -12 -4 -3 23.43 8.24 0 -12 4 3 13.32 6.61 0 -12 -4 -3 14.56 9.25 0 -12 4 -3 12.98 6.30 0 -12 -4 3 30.69 8.22 0 0 -5 3 5.07 12.06 0 0 5 3 0.90 14.37 0 0 5 -3 -2.92 16.03 0 0 -5 -3 4.96 15.98 0 1 -5 3 11.16 16.33 0 1 -5 -3 12.24 18.15 0 -1 -5 3 3.83 10.20 0 1 5 3 -1.60 13.42 0 -1 5 -3 7.03 15.99 0 -1 5 3 8.34 11.33 0 1 5 -3 9.68 10.05 0 1 -5 3 0.04 16.51 0 -1 -5 -3 8.72 13.75 0 -2 5 -3 5368.09 29.27 0 2 5 -3 5604.47 27.16 0 -2 -5 -3 5293.94 24.32 0 -2 -5 3 5313.56 25.04 0 2 5 3 5359.48 24.31 0 -2 5 3 5294.61 30.09 0 2 -5 3 5325.63 29.41 0 2 -5 -3 5443.47 34.50 0 3 -5 3 245.47 11.02 0 -3 5 3 236.99 11.48 0 -3 -5 -3 245.63 12.03 0 3 -5 -3 237.64 23.06 0 3 5 -3 241.78 9.36 0 -3 -5 3 235.40 12.42 0 3 -5 -3 250.33 15.96 0 -3 5 -3 263.25 14.56 0 3 -5 3 241.08 22.68 0 3 5 3 233.15 11.88 0 4 5 -3 2207.21 16.98 0 -4 -5 -3 2192.30 16.47 0 -4 5 3 2201.60 20.14 0 4 5 3 2325.41 16.84 0 -4 -5 3 2206.10 15.39 0 4 -5 -3 2241.93 18.40 0 -4 5 -3 2137.96 16.18 0 4 -5 3 2277.52 19.11 0 5 -5 -3 494.39 13.77 0 -5 5 3 475.13 13.78 0 -5 -5 -3 467.92 11.39 0 -5 5 -3 461.44 10.72 0 -5 -5 3 483.10 11.99 0 5 -5 3 477.24 10.50 0 5 5 -3 472.92 12.00 0 -6 -5 -3 9.95 6.55 0 -6 5 -3 12.78 10.84 0 -6 -5 3 8.52 9.79 0 -6 5 3 12.82 11.85 0 -7 5 3 40.90 11.59 0 -7 -5 3 49.41 9.68 0 -7 5 -3 54.41 7.94 0 -7 -5 -3 45.81 9.49 0 -8 -5 -3 211.15 9.93 0 -8 -5 3 211.73 7.68 0 -8 5 -3 207.66 11.62 0 -8 5 3 218.38 11.83 0 -9 5 -3 49.51 9.77 0 -9 5 3 45.08 10.46 0 -9 -5 3 49.50 8.91 0 -9 -5 -3 30.10 6.53 0 -9 -5 3 37.91 6.15 0 -10 -5 3 315.30 10.06 0 -10 -5 -3 319.00 7.71 0 -10 5 3 345.11 11.35 0 -10 -5 3 359.31 10.32 0 -10 5 -3 296.36 8.50 0 -11 -5 -3 -3.73 6.28 0 -11 5 3 27.51 9.73 0 -11 5 -3 1.78 6.89 0 -11 -5 3 11.93 8.42 0 -11 -5 3 3.00 8.52 0 -12 5 3 13.45 8.31 0 -12 5 3 14.20 9.27 0 -12 -5 3 12.00 7.82 0 -12 -5 3 -0.75 8.24 0 -12 5 -3 -7.01 6.59 0 -12 -5 -3 14.04 8.06 0 0 -6 3 3907.74 23.12 0 0 -6 -3 3954.39 26.10 0 0 6 3 3921.37 25.16 0 0 6 -3 3940.80 24.89 0 -1 6 -3 4829.71 27.28 0 1 -6 3 5102.92 29.23 0 1 6 3 4815.42 25.08 0 1 -6 3 4777.51 25.75 0 -1 -6 -3 4763.43 25.60 0 -1 -6 3 4858.48 26.06 0 1 -6 -3 4973.34 30.74 0 1 6 -3 4860.55 24.26 0 -1 6 3 4932.44 28.48 0 2 6 -3 11.72 11.73 0 -2 -6 -3 8.48 11.66 0 2 6 3 3.69 7.93 0 2 -6 -3 4.35 15.19 0 -2 6 3 0.76 13.49 0 -2 -6 3 8.11 8.39 0 2 -6 3 1.77 14.43 0 -2 6 -3 3.00 13.79 0 2 -6 3 10.95 14.82 0 3 -6 3 815.08 23.70 0 -3 6 -3 788.21 15.29 0 -3 -6 -3 762.82 13.00 0 3 -6 3 802.98 16.37 0 3 -6 -3 765.00 17.21 0 -3 -6 3 794.88 13.39 0 3 6 -3 828.36 13.67 0 3 -6 -3 820.56 22.38 0 -3 6 3 795.00 16.09 0 3 6 3 799.25 12.89 0 -4 6 3 608.86 15.50 0 4 6 3 646.21 12.20 0 4 -6 -3 625.39 33.35 0 -4 -6 -3 620.76 12.23 0 -4 -6 3 621.65 12.00 0 4 6 -3 589.00 12.08 0 -4 6 -3 632.88 14.34 0 4 -6 -3 654.84 16.02 0 4 -6 3 629.83 14.54 0 -5 6 3 2639.49 20.16 0 5 -6 -3 2799.75 20.65 0 -5 6 -3 2653.61 19.16 0 -5 -6 -3 2636.18 16.00 0 5 6 3 2700.66 15.99 0 5 -6 3 2717.82 19.37 0 5 6 -3 2654.41 17.25 0 -5 -6 3 2706.09 17.02 0 -6 -6 -3 7.31 9.42 0 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669.41 10.92 0 4 -13 -4 694.14 15.79 0 -4 -13 -4 637.47 11.19 0 -4 13 -4 639.95 10.05 0 4 -13 4 659.66 13.05 0 4 13 -4 668.42 11.13 0 4 -13 4 667.58 15.35 0 -4 13 4 648.55 12.04 0 -4 -13 4 651.10 11.33 0 4 -13 -4 661.56 14.33 0 5 13 4 417.37 7.94 0 5 -13 -4 447.88 19.14 0 5 -13 -4 432.88 15.86 0 -5 13 4 423.92 11.90 0 5 -13 -4 386.99 10.36 0 5 13 -4 417.32 10.42 0 -5 13 -4 395.26 8.88 0 -5 -13 4 430.74 10.59 0 -5 -13 -4 418.97 10.26 0 5 -13 4 429.75 18.43 0 5 -13 4 427.07 9.34 0 6 13 4 29.00 9.02 0 6 -13 -4 23.18 12.33 0 -6 -13 -4 28.24 6.53 0 -6 13 4 40.05 10.54 0 -6 13 -4 23.43 10.29 0 -6 -13 4 26.29 8.75 0 6 -13 4 44.09 11.17 0 6 13 -4 32.69 9.03 0 7 13 4 163.86 6.88 0 -7 13 -4 146.88 7.89 0 7 -13 -4 157.41 9.09 0 7 13 -4 158.81 7.39 0 -7 -13 4 149.12 9.78 0 -7 13 4 164.75 11.05 0 -7 -13 -4 148.34 6.70 0 7 -13 4 155.40 11.12 0 -8 -13 4 97.01 9.31 0 8 -13 -4 107.24 11.32 0 -8 13 4 104.41 10.35 0 8 13 4 89.23 8.79 0 -8 13 -4 99.15 10.50 0 8 -13 4 94.39 10.84 0 8 13 -4 91.71 9.43 0 -8 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6.24 0 -10 8 -5 4.98 6.45 0 -11 -8 -5 26.73 8.27 0 -11 -8 5 7.90 6.08 0 -11 -8 5 23.41 8.20 0 -11 8 5 22.30 9.98 0 -11 8 -5 29.92 6.72 0 0 -9 -5 -1.04 12.06 0 0 9 5 4.93 7.04 0 0 -9 5 3.09 10.29 0 0 -9 5 7.20 12.51 0 0 9 -5 1.06 12.13 0 1 9 -5 368.38 12.71 0 1 -9 5 384.06 11.87 0 -1 -9 -5 356.77 9.66 0 1 9 5 370.18 11.62 0 1 -9 -5 370.93 14.85 0 -1 -9 5 374.96 12.99 0 -1 9 5 383.99 13.11 0 -1 9 -5 384.83 13.58 0 1 -9 5 365.20 14.02 0 -2 9 5 1022.85 15.30 0 2 9 -5 990.85 14.05 0 2 -9 5 1035.87 14.63 0 2 -9 -5 989.44 17.11 0 -2 -9 5 988.26 11.31 0 2 -9 5 1028.84 15.43 0 -2 9 -5 1018.19 14.62 0 2 9 5 1042.05 12.68 0 -2 -9 -5 974.72 13.05 0 -3 9 -5 29.97 11.22 0 3 -9 5 44.86 11.59 0 3 -9 -5 49.17 13.20 0 -3 9 5 49.15 8.23 0 3 9 5 47.70 9.68 0 -3 -9 -5 38.29 9.57 0 3 -9 -5 50.59 13.51 0 3 -9 5 55.16 12.74 0 -3 -9 5 46.43 10.04 0 3 9 -5 50.69 7.39 0 4 -9 -5 1802.03 19.67 0 4 9 5 1804.35 12.54 0 -4 -9 5 1825.17 14.30 0 4 -9 5 1884.21 27.33 0 -4 -9 -5 1827.41 14.58 0 -4 9 5 1853.18 17.57 0 -4 9 -5 1820.72 13.88 0 4 -9 -5 1940.75 26.10 0 4 -9 5 1876.96 16.67 0 4 9 -5 1963.00 15.02 0 5 -9 -5 33.39 19.73 0 -5 -9 5 33.21 7.02 0 -5 9 5 30.82 11.97 0 5 9 -5 35.48 6.65 0 -5 9 -5 29.89 11.11 0 5 -9 -5 29.17 9.11 0 5 -9 5 31.52 11.42 0 -5 -9 -5 28.21 9.61 0 5 9 5 26.13 6.68 0 -6 9 5 -1.94 10.85 0 -6 9 -5 3.39 7.95 0 6 -9 5 0.88 11.19 0 -6 -9 5 17.31 9.18 0 6 9 5 3.20 9.01 0 6 9 -5 2.62 6.82 0 6 -9 -5 9.40 11.30 0 -6 -9 -5 -6.55 9.13 0 7 9 -5 37.51 9.12 0 -7 9 -5 28.69 10.86 0 7 -9 -5 46.49 11.46 0 -7 -9 5 33.40 6.33 0 -7 -9 -5 37.19 8.83 0 -7 9 5 23.39 10.66 0 7 -9 5 26.92 10.81 0 -8 9 -5 25.06 7.12 0 -8 9 5 30.02 10.42 0 -8 -9 5 24.01 9.20 0 -8 -9 -5 26.75 8.51 0 -9 9 5 52.33 10.33 0 -9 -9 -5 37.73 8.39 0 -9 -9 5 63.05 8.78 0 -9 -9 5 47.89 9.03 0 -9 9 -5 61.73 7.39 0 -10 -9 -5 44.23 6.47 0 -10 -9 5 30.87 8.36 0 -10 9 -5 53.11 9.96 0 -10 9 5 43.75 10.11 0 -11 -9 5 11.37 7.93 0 -11 -9 -5 6.05 8.33 0 -11 9 5 7.42 9.42 0 -11 -9 5 2.28 8.04 0 -11 9 -5 -3.49 9.63 0 0 10 5 -4.64 11.23 0 0 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124.71 11.85 0 5 11 -5 139.11 10.30 0 -6 11 -5 5.22 7.43 0 6 11 -5 -7.36 9.39 0 -6 -11 -5 3.15 6.52 0 -6 -11 5 7.10 9.08 0 6 -11 5 6.50 7.80 0 -6 11 5 8.22 10.63 0 6 -11 -5 6.51 11.48 0 6 11 5 16.43 9.02 0 -7 11 5 46.23 10.84 0 7 11 5 48.52 8.93 0 -7 -11 -5 37.87 6.46 0 -7 -11 5 55.35 6.32 0 7 -11 -5 61.94 11.45 0 7 11 -5 54.13 6.31 0 -7 11 -5 58.90 10.28 0 7 -11 5 54.88 10.80 0 -8 -11 -5 3.97 8.26 0 8 -11 5 25.20 10.81 0 8 -11 -5 30.80 10.64 0 8 11 -5 8.43 8.83 0 -8 -11 5 24.43 8.98 0 -8 11 5 20.53 9.93 0 -8 11 -5 30.02 10.39 0 -9 -11 5 22.98 6.44 0 -9 11 -5 26.90 9.92 0 -9 -11 5 36.93 8.09 0 -9 -11 -5 23.48 5.89 0 -9 11 5 18.10 10.31 0 -10 -11 -5 0.08 7.79 0 -10 -11 5 3.33 7.59 0 -10 11 5 4.04 10.23 0 -10 11 -5 8.86 9.69 0 -10 -11 5 -10.65 7.67 0 0 -12 5 2611.71 15.06 0 0 -12 -5 2623.30 17.84 0 0 12 -5 2600.12 15.29 0 0 12 5 2717.45 16.83 0 0 -12 5 2642.50 15.70 0 -1 12 -5 352.56 12.17 0 1 -12 -5 387.79 10.02 0 1 12 -5 397.83 11.60 0 -1 12 5 392.32 11.42 0 1 -12 5 380.58 12.91 0 -1 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5 9.74 10.42 0 6 13 5 7.60 6.20 0 -6 -13 -5 21.28 8.99 0 -7 13 5 52.81 10.17 0 7 -13 5 55.90 7.97 0 7 13 -5 49.11 9.39 0 -7 -13 -5 50.64 6.33 0 7 -13 -5 74.65 11.68 0 7 13 5 32.99 6.05 0 -7 13 -5 59.02 10.43 0 -7 -13 5 76.89 8.89 0 -8 -13 5 28.12 9.00 0 -8 13 5 34.18 9.92 0 -8 -13 -5 40.06 8.53 0 8 -13 -5 54.87 11.65 0 8 13 -5 33.80 6.71 0 8 -13 5 58.01 10.25 0 -8 -13 5 41.26 6.04 0 -8 13 -5 55.66 9.92 0 9 -13 5 73.67 10.64 0 -9 13 -5 43.84 7.31 0 -9 13 5 44.95 9.44 0 9 13 -5 29.86 8.88 0 -9 -13 5 28.64 5.98 0 -9 -13 -5 41.61 8.30 0 0 14 5 -2.70 10.06 0 0 -14 5 2.16 10.17 0 0 -14 -5 -2.85 7.87 0 0 14 -5 16.69 10.36 0 0 -14 5 -0.05 8.35 0 -1 14 -5 11.51 10.02 0 -1 14 5 9.26 10.22 0 1 14 5 4.05 9.51 0 1 -14 5 10.14 7.67 0 1 14 -5 2.52 10.12 0 1 -14 5 9.27 8.87 0 -1 -14 5 6.09 10.47 0 1 -14 -5 0.61 11.80 0 -1 -14 -5 16.74 10.72 0 -2 -14 -5 16.12 9.91 0 2 14 -5 10.11 10.00 0 2 -14 -5 -0.60 8.68 0 2 -14 5 13.38 9.37 0 -2 14 -5 -3.51 10.14 0 -2 14 5 15.70 7.24 0 2 -14 5 13.82 10.63 0 -2 -14 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10 28.32 12.10 0 3 -7 10 26.97 14.73 0 3 7 10 29.64 9.96 0 -3 7 -10 24.44 12.59 0 -3 -7 10 25.37 10.01 0 -3 7 -10 23.79 10.11 0 3 7 -10 23.88 11.62 0 -3 7 10 28.07 11.21 0 4 -7 10 521.26 10.16 0 4 -7 -10 544.55 15.35 0 -4 -7 10 521.35 12.70 0 -4 -7 -10 519.13 8.73 0 4 -7 10 532.08 15.61 0 -4 7 10 530.77 15.97 0 4 7 -10 554.05 13.17 0 4 7 10 534.86 8.62 0 -4 7 -10 498.98 9.91 0 4 -7 -10 536.47 17.98 0 -4 7 -10 532.71 14.83 0 -4 -7 10 505.51 10.53 0 -5 -7 10 1122.73 10.14 0 -5 -7 10 1075.70 11.31 0 -5 -7 -10 1163.22 12.34 0 5 -7 10 1206.47 21.07 0 5 -7 -10 1151.35 17.85 0 -5 7 10 1147.83 18.20 0 5 7 -10 1101.61 11.58 0 -5 7 -10 1110.38 14.56 0 -5 7 -10 1138.65 18.36 0 5 -7 -10 1200.25 16.46 0 5 -7 10 1178.02 11.96 0 -6 7 -10 12.98 10.67 0 -6 -7 10 -6.44 8.85 0 -6 -7 10 13.93 9.68 0 -6 7 10 7.15 11.48 0 6 -7 -10 -0.66 11.21 0 6 7 -10 -2.44 9.78 0 -6 7 -10 -1.33 12.77 0 6 -7 10 -4.07 8.02 0 -6 -7 -10 14.22 6.74 0 -7 -7 10 770.04 11.87 0 -7 7 -10 729.48 12.76 0 -7 -7 10 769.52 9.28 0 -7 7 -10 810.07 23.73 0 -7 7 10 803.85 14.23 0 7 7 -10 792.36 12.14 0 -7 -7 -10 742.82 10.97 0 -8 7 10 87.10 11.10 0 -8 -7 10 84.59 9.57 0 -8 -7 -10 77.11 6.57 0 -8 7 -10 75.18 11.08 0 -8 -7 10 80.05 6.50 0 -9 7 10 36.54 12.52 0 -9 -7 -10 17.88 8.43 0 -9 7 -10 20.18 10.25 0 -9 -7 10 29.09 9.21 0 -9 -7 10 18.53 8.30 0 -10 7 -10 -0.18 7.09 0 -10 -7 -10 -1.84 5.95 0 -10 -7 10 21.85 8.67 0 -10 -7 10 6.51 8.42 0 -10 7 10 -3.99 9.90 0 -11 -7 10 16.55 8.51 0 -11 7 -10 7.79 9.42 0 -11 -7 -10 7.51 5.88 0 -11 7 10 32.74 11.56 0 -11 -7 10 17.80 8.70 0 0 8 10 88.60 10.92 0 0 -8 -10 81.70 12.16 0 0 -8 -10 87.35 11.06 0 0 -8 10 74.42 12.34 0 0 -8 10 95.76 11.15 0 0 8 -10 70.06 12.06 0 -1 8 10 2090.21 18.08 0 1 -8 10 2041.55 15.28 0 -1 8 -10 2020.33 18.34 0 -1 -8 10 2047.50 15.51 0 1 -8 10 1996.27 17.33 0 -1 -8 10 2116.03 17.60 0 1 -8 -10 2047.00 17.58 0 1 8 -10 2018.35 17.42 0 1 8 10 2033.07 16.80 0 1 -8 -10 2040.39 20.10 0 -1 -8 -10 1989.50 15.45 0 2 8 10 41.14 7.42 0 2 -8 -10 31.88 11.03 0 2 8 -10 25.59 8.72 0 2 -8 10 37.65 10.93 0 -2 -8 -10 32.21 10.80 0 2 -8 -10 38.98 13.42 0 -2 8 -10 30.77 12.46 0 -2 8 10 43.43 10.84 0 -2 -8 10 43.74 9.53 0 -2 -8 10 32.93 8.16 0 2 -8 10 36.58 12.55 0 -3 -8 10 1899.92 14.11 0 3 -8 10 2052.26 20.11 0 -3 8 10 2009.65 18.55 0 3 -8 10 1986.85 14.31 0 -3 8 -10 1911.42 16.76 0 3 8 -10 2054.86 17.29 0 3 -8 -10 2022.04 20.02 0 3 8 10 2018.30 15.23 0 3 -8 -10 1870.10 21.47 0 -3 -8 -10 1944.34 13.79 0 -3 -8 10 1971.05 16.69 0 -4 -8 -10 1.46 9.05 0 4 -8 10 5.39 11.31 0 -4 -8 10 -2.85 7.76 0 4 8 -10 21.33 10.67 0 4 -8 -10 10.26 12.24 0 4 -8 -10 -7.78 14.60 0 -4 8 -10 0.49 11.67 0 4 -8 10 10.37 11.73 0 -4 -8 10 -15.92 8.91 0 -4 8 10 -8.70 10.39 0 4 8 10 -0.99 6.07 0 5 -8 10 579.51 17.85 0 -5 -8 10 568.52 11.53 0 -5 -8 10 537.23 7.99 0 -5 -8 -10 551.11 8.72 0 -5 8 10 551.63 13.56 0 5 -8 -10 545.12 16.70 0 5 -8 10 543.16 10.40 0 5 8 -10 573.45 11.94 0 -5 8 -10 560.19 13.20 0 5 -8 -10 572.41 14.32 0 -6 -8 10 23.12 9.82 0 6 8 -10 15.16 9.86 0 -6 -8 -10 11.13 6.88 0 -6 8 -10 14.97 10.64 0 6 -8 -10 19.50 14.22 0 -6 -8 10 16.91 8.77 0 6 -8 -10 15.92 10.48 0 6 -8 10 24.87 10.50 0 -6 8 10 24.81 11.41 0 -7 -8 10 401.06 10.88 0 -7 8 -10 384.18 11.65 0 7 8 -10 365.38 11.00 0 -7 -8 -10 392.00 7.94 0 -7 -8 10 394.34 7.76 0 7 -8 10 432.91 11.37 0 -7 8 10 378.27 12.23 0 -8 8 -10 32.65 10.21 0 -8 -8 10 23.76 8.62 0 -8 -8 -10 23.60 8.79 0 -8 8 10 31.46 12.90 0 -8 -8 10 17.18 6.15 0 -9 -8 -10 98.00 8.71 0 -9 -8 10 95.17 9.35 0 -9 8 -10 100.92 9.88 0 -9 8 10 100.92 10.68 0 -9 -8 10 106.01 8.87 0 -10 -8 -10 -0.98 5.80 0 -10 -8 10 5.14 8.71 0 -10 8 -10 16.08 9.55 0 -10 8 10 1.50 9.71 0 -10 -8 10 14.24 8.08 0 -11 8 -10 -2.04 9.98 0 -11 -8 10 17.47 8.27 0 -11 -8 -10 5.01 7.94 0 -11 8 10 2.61 9.70 0 -11 -8 10 20.89 8.26 0 0 -9 -10 -0.02 8.85 0 0 -9 10 1.48 10.25 0 0 -9 10 -1.32 11.47 0 0 -9 -10 6.44 10.49 0 0 9 -10 -8.69 11.49 0 0 9 10 8.44 10.46 0 -1 9 10 777.49 14.20 0 1 -9 -10 769.00 13.41 0 -1 -9 -10 751.38 11.18 0 1 -9 10 767.02 13.50 0 1 -9 10 778.46 13.80 0 1 9 -10 742.66 11.51 0 1 9 10 767.83 13.29 0 -1 -9 10 792.28 12.64 0 -1 -9 10 760.77 11.40 0 1 -9 -10 714.23 15.71 0 -1 9 -10 741.62 14.02 0 -2 -9 10 1518.64 15.56 0 2 -9 10 1548.18 15.69 0 -2 -9 10 1525.61 11.61 0 2 -9 10 1542.88 13.45 0 -2 -9 -10 1515.47 14.98 0 -2 9 10 1541.42 15.59 0 2 -9 -10 1534.60 15.45 0 2 9 -10 1586.05 16.04 0 2 -9 -10 1565.35 18.96 0 -2 9 -10 1520.43 13.47 0 2 9 10 1535.81 14.45 0 -3 9 10 581.12 12.88 0 3 -9 -10 579.82 15.10 0 3 9 10 594.81 10.86 0 3 -9 10 603.38 13.81 0 3 -9 -10 585.53 13.89 0 -3 9 -10 600.17 13.10 0 -3 -9 -10 576.05 11.47 0 -3 -9 10 585.85 10.84 0 3 -9 10 605.05 13.09 0 3 9 -10 605.48 13.03 0 -3 -9 10 582.30 12.41 0 4 -9 10 160.91 8.82 0 4 9 10 160.26 9.44 0 -4 -9 10 151.05 9.46 0 4 9 -10 148.72 10.85 0 4 -9 -10 156.15 13.51 0 -4 9 -10 159.22 11.95 0 4 -9 10 148.96 15.19 0 -4 -9 10 145.38 10.62 0 4 -9 -10 158.91 15.48 0 -4 -9 -10 147.29 6.92 0 -4 9 10 151.49 11.54 0 5 -9 -10 138.45 15.66 0 5 -9 10 134.22 11.43 0 -5 -9 -10 132.85 6.89 0 -5 -9 10 126.94 10.42 0 5 9 10 126.22 9.60 0 5 -9 -10 127.08 14.36 0 5 -9 10 127.52 16.69 0 -5 9 10 126.33 11.64 0 5 9 -10 129.70 7.93 0 -5 -9 10 122.31 6.82 0 -5 9 -10 127.84 11.44 0 6 9 -10 15.73 10.11 0 -6 -9 -10 10.01 6.24 0 -6 9 -10 20.98 10.61 0 -6 -9 10 15.60 9.92 0 -6 9 10 24.82 11.11 0 -6 -9 10 14.54 8.51 0 6 -9 -10 19.25 14.26 0 6 -9 -10 14.46 10.93 0 6 -9 10 46.09 10.32 0 -7 -9 -10 23.68 9.04 0 -7 -9 10 32.80 9.46 0 -7 9 -10 18.51 10.39 0 7 9 -10 31.78 9.13 0 -7 9 10 21.39 10.20 0 -7 -9 10 25.63 5.88 0 7 -9 10 44.99 9.88 0 -8 -9 -10 18.24 5.92 0 -8 9 -10 15.82 7.74 0 -8 -9 10 17.08 8.72 0 -8 9 10 33.07 10.03 0 8 9 -10 15.98 9.18 0 -8 -9 10 23.93 8.66 0 -9 -9 10 -2.36 8.57 0 -9 -9 10 -0.96 6.54 0 -9 9 -10 -5.03 9.26 0 -9 9 10 4.78 10.14 0 -9 -9 -10 19.79 8.37 0 -10 9 10 15.10 9.78 0 -10 -9 10 25.46 5.81 0 -10 9 -10 10.66 9.34 0 -10 -9 -10 27.60 5.71 0 -10 -9 10 13.45 8.09 0 0 -10 -10 32.46 9.99 0 0 10 -10 20.76 8.03 0 0 -10 10 29.70 8.05 0 0 -10 -10 24.95 12.22 0 0 -10 10 35.08 10.43 0 0 10 10 33.86 10.59 0 1 10 10 2902.99 18.19 0 1 -10 -10 2909.97 18.50 0 -1 10 10 2946.32 19.50 0 1 10 -10 2893.37 18.01 0 -1 -10 10 2970.38 16.56 0 1 -10 10 2890.88 18.52 0 -1 -10 10 2867.17 17.58 0 1 -10 10 2895.51 18.30 0 1 -10 -10 2905.22 21.34 0 -1 10 -10 2865.22 18.62 0 -1 -10 -10 2911.76 18.88 0 -2 10 -10 -5.37 11.05 0 -2 -10 -10 7.84 9.98 0 -2 10 10 10.95 10.11 0 2 -10 10 3.66 11.27 0 2 -10 -10 6.36 13.77 0 2 -10 10 -5.05 9.33 0 -2 -10 10 -1.52 8.62 0 2 -10 -10 1.12 9.71 0 -2 -10 10 20.02 10.30 0 2 10 -10 4.89 7.67 0 2 10 10 -0.06 9.18 0 -3 10 -10 1646.90 15.95 0 -3 10 10 1671.19 16.42 0 3 -10 -10 1563.69 18.74 0 3 -10 10 1670.50 13.44 0 3 -10 10 1719.16 17.31 0 3 10 -10 1666.61 15.01 0 3 -10 -10 1664.71 17.22 0 -3 -10 -10 1630.42 13.99 0 -3 -10 10 1654.89 13.21 0 -3 -10 10 1638.61 12.72 0 3 10 10 1679.50 13.70 0 -4 -10 10 1076.52 13.06 0 4 10 -10 1119.80 13.77 0 4 -10 10 1128.62 18.75 0 4 -10 10 1128.46 12.00 0 4 -10 -10 1110.45 17.00 0 -4 -10 -10 1090.77 12.58 0 -4 -10 10 1123.13 12.06 0 4 -10 -10 1157.95 17.23 0 -4 10 -10 1077.34 14.44 0 4 10 10 1095.78 12.42 0 -4 10 10 1087.15 14.51 0 5 -10 10 86.67 11.06 0 5 -10 -10 67.04 12.94 0 5 10 10 71.68 8.85 0 -5 10 -10 71.98 11.07 0 5 -10 10 66.19 14.83 0 -5 -10 10 60.37 8.92 0 5 -10 -10 62.80 14.33 0 5 10 -10 75.06 10.54 0 -5 -10 -10 62.12 6.49 0 -5 10 10 68.04 11.29 0 -5 -10 10 58.13 10.34 0 6 -10 -10 13.80 16.42 0 6 -10 10 17.69 16.35 0 -6 -10 10 10.87 6.41 0 6 -10 -10 26.37 11.04 0 -6 10 -10 22.90 10.75 0 -6 -10 10 17.28 5.94 0 -6 10 10 13.68 12.97 0 6 10 -10 17.61 9.35 0 -6 -10 -10 25.21 9.04 0 6 -10 10 19.57 10.26 0 7 10 -10 15.83 9.08 0 -7 10 -10 1.40 9.44 0 7 -10 10 2.60 10.32 0 -7 10 10 15.87 10.33 0 7 -10 -10 -4.56 10.00 0 -7 -10 10 18.57 8.66 0 -7 -10 10 21.06 9.02 0 -7 -10 -10 20.53 8.91 0 -8 -10 10 87.76 6.59 0 -8 10 -10 71.56 10.35 0 -8 -10 -10 85.47 8.75 0 -8 10 10 74.80 10.61 0 -8 -10 10 82.01 8.99 0 8 10 -10 73.07 9.36 0 8 -10 10 86.68 10.78 0 -9 -10 -10 72.32 6.23 0 -9 10 -10 78.58 9.94 0 -9 -10 10 80.34 8.04 0 -9 -10 10 77.00 9.59 0 -9 10 10 86.22 10.39 0 -10 -10 -10 32.31 5.77 0 -10 -10 10 45.34 8.37 0 -10 10 -10 25.89 6.54 0 -10 -10 10 27.26 5.96 0 -10 10 10 20.21 9.92 0 0 -11 -10 -2.71 11.74 0 0 11 -10 3.17 7.70 0 0 -11 10 1.83 7.88 0 0 -11 10 15.04 9.78 0 0 11 10 0.09 10.13 0 -1 -11 -10 2334.94 16.92 0 1 -11 -10 2265.88 18.25 0 1 -11 -10 2346.76 16.82 0 -1 -11 10 2378.69 14.30 0 1 -11 10 2386.15 17.45 0 1 11 10 2423.89 16.66 0 -1 11 10 2440.11 17.18 0 1 -11 10 2377.28 16.51 0 1 11 -10 2310.11 16.28 0 -1 -11 10 2377.41 13.49 0 -1 11 -10 2285.90 15.29 0 -2 -11 10 986.53 11.56 0 -2 -11 10 935.92 13.18 0 2 11 10 968.44 12.16 0 2 11 -10 969.72 13.00 0 -2 11 10 956.18 13.11 0 2 -11 10 1000.07 14.08 0 2 -11 -10 967.89 13.94 0 2 -11 -10 952.68 15.87 0 2 -11 10 952.69 13.57 0 -2 -11 -10 933.01 12.74 0 -2 11 -10 920.68 13.95 0 3 11 10 10.08 6.73 0 3 -11 -10 3.48 12.80 0 3 -11 10 15.81 11.51 0 -3 -11 -10 8.08 10.13 0 3 11 -10 17.27 10.28 0 3 -11 -10 17.45 12.42 0 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9.55 0 -6 -11 -22 27.02 6.11 0 -7 -11 -22 22.37 8.53 0 7 11 -22 -3.12 6.74 0 7 -11 22 0.15 12.83 0 -7 -11 -22 15.22 8.28 0 -7 11 -22 8.45 9.05 0 7 -11 -22 12.27 11.85 0 -7 -11 22 10.56 9.27 0 -7 11 22 11.60 12.27 0 -7 11 -22 11.19 8.36 0 7 -11 22 21.31 8.83 0 -8 -11 -22 5.28 5.76 0 8 11 -22 -9.85 9.55 0 -8 11 -22 2.84 9.15 0 -8 -11 22 -3.88 5.57 0 -8 11 22 5.93 13.28 0 8 -11 -22 8.77 11.21 0 -8 -11 22 17.92 9.11 0 0 12 -22 175.80 11.27 0 0 -12 -22 159.71 7.36 0 0 -12 22 171.82 10.58 0 0 12 22 169.32 10.13 0 0 -12 22 187.14 9.72 0 0 -12 -22 192.84 11.35 0 -1 -12 -22 61.53 10.20 0 1 12 -22 69.48 10.75 0 1 -12 22 100.90 9.85 0 1 12 22 78.07 8.80 0 -1 -12 22 57.65 10.03 0 1 -12 -22 66.29 9.71 0 1 -12 22 63.33 7.74 0 -1 -12 -22 61.61 8.78 0 -1 -12 22 60.13 9.17 0 -1 12 22 82.14 9.67 0 1 -12 -22 67.51 13.56 0 -1 12 -22 55.40 7.80 0 2 -12 22 17.64 9.39 0 -2 12 22 3.58 8.65 0 -2 -12 -22 3.85 8.76 0 2 -12 22 1.06 9.76 0 -2 -12 -22 7.09 9.13 0 2 12 -22 17.29 10.76 0 -2 -12 22 11.02 10.20 0 2 -12 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9.67 0 -6 -12 22 70.71 9.73 0 -6 -12 -22 75.50 9.06 0 6 -12 22 91.71 8.99 0 7 -12 22 1.93 12.34 0 -7 -12 -22 6.54 5.57 0 -7 12 -22 -1.55 9.41 0 -7 -12 22 14.41 5.51 0 7 -12 -22 -1.83 9.93 0 -7 -12 22 -0.60 9.09 0 -7 12 22 2.71 12.47 0 -7 -12 -22 9.22 5.81 0 7 -12 22 1.63 9.01 0 7 12 -22 0.87 9.56 0 0 13 -22 5.80 10.97 0 0 -13 -22 9.74 5.95 0 0 -13 22 -4.13 10.30 0 0 -13 22 16.93 8.95 0 0 -13 -22 8.33 9.95 0 0 13 22 4.56 8.56 0 -1 -13 -22 87.68 10.42 0 1 13 -22 61.04 11.00 0 1 -13 22 89.16 10.16 0 1 -13 -22 90.97 7.09 0 -1 -13 22 73.49 7.59 0 -1 13 22 99.74 9.07 0 1 -13 22 101.58 9.40 0 -1 -13 22 92.78 9.75 0 1 13 22 75.18 9.14 0 -1 -13 -22 79.56 9.24 0 1 -13 -22 91.79 13.50 0 -1 13 -22 84.21 11.07 0 -2 13 22 596.39 12.11 0 2 -13 22 646.17 11.71 0 -2 -13 -22 571.10 10.70 0 -2 -13 -22 536.77 12.08 0 2 -13 -22 613.36 12.50 0 2 13 -22 602.71 12.76 0 -2 -13 22 603.77 12.24 0 2 13 22 610.06 11.28 0 2 -13 22 628.70 12.05 0 2 -13 -22 621.73 15.11 0 -2 -13 22 627.73 10.98 0 -2 13 -22 592.24 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9.81 0 -2 -3 30 188.12 10.88 0 -3 -3 -30 8.15 9.43 0 3 3 30 12.82 7.01 0 3 -3 30 14.41 10.01 0 -3 3 30 -6.27 9.62 0 -3 3 -30 27.04 10.45 0 -3 -3 30 8.47 9.21 0 -3 -3 -30 30.03 9.30 0 -3 -3 -30 11.08 9.29 0 -3 3 -30 6.29 9.68 0 3 -3 -30 20.76 9.79 0 3 3 -30 9.17 6.76 0 3 3 -30 7.27 13.93 0 -3 -3 30 5.81 11.83 0 -4 -3 -30 40.64 9.58 0 4 -3 30 40.05 10.05 0 -4 3 -30 24.93 9.79 0 -4 3 30 47.87 9.81 0 -4 -3 -30 21.75 9.31 0 -4 -3 30 49.74 9.73 0 -4 3 -30 43.60 9.42 0 4 -3 -30 42.66 9.92 0 -4 -3 -30 44.03 9.46 0 4 3 -30 41.19 10.06 0 4 3 -30 38.77 13.31 0 -4 -3 30 47.10 14.03 0 -5 -3 30 118.83 17.10 0 -5 3 -30 100.47 9.88 0 -5 3 30 115.74 10.07 0 5 -3 30 119.46 7.97 0 -5 -3 -30 106.95 9.76 0 -5 -3 30 117.52 9.98 0 -5 3 -30 120.59 7.61 0 5 -3 -30 102.77 10.05 0 -5 -3 -30 114.11 9.53 0 5 3 -30 125.02 9.97 0 -5 -3 -30 127.17 9.71 0 -6 -3 30 25.01 18.37 0 6 -3 30 30.44 9.93 0 -6 3 -30 9.16 9.65 0 -6 3 30 38.78 9.19 0 -6 -3 -30 19.20 9.36 0 -6 -3 30 40.04 8.94 0 -6 3 -30 36.37 9.55 0 -6 -3 -30 28.54 9.15 0 6 -3 -30 23.83 10.18 0 6 3 -30 31.63 9.16 0 -6 -3 -30 24.87 9.12 0 -7 3 -30 38.26 6.55 0 -7 -3 30 48.84 21.69 0 -7 3 30 58.23 9.50 0 -7 -3 -30 40.90 8.86 0 -7 -3 -30 55.75 9.09 0 -7 -3 30 60.11 6.65 0 -7 3 -30 38.67 9.65 0 7 -3 -30 40.13 9.92 0 7 3 -30 44.88 9.14 0 -7 -3 -30 56.36 9.13 0 -8 -3 -30 11.92 6.39 0 -8 -3 30 15.18 20.74 0 -8 3 -30 3.00 9.11 0 -8 -3 -30 3.93 8.70 0 -8 -3 30 10.16 20.22 0 -8 3 30 7.02 9.46 0 -8 -3 -30 14.20 8.90 0 -8 -3 30 12.13 8.19 0 -8 3 -30 23.87 8.85 0 8 -3 -30 2.78 9.74 0 0 -4 -30 384.49 14.82 0 0 4 30 353.54 10.57 0 0 -4 -30 376.90 13.60 0 0 -4 30 375.62 10.49 0 0 -4 -30 357.29 10.55 0 0 4 -30 382.61 9.94 0 0 4 -30 388.27 15.76 0 0 -4 30 392.71 14.18 0 -1 -4 -30 134.16 12.26 0 1 4 30 125.26 7.52 0 -1 4 30 137.54 9.83 0 1 -4 30 150.49 10.12 0 -1 -4 30 152.86 9.77 0 -1 -4 -30 132.81 9.92 0 1 -4 -30 140.96 18.71 0 1 -4 -30 139.03 10.05 0 -1 4 -30 141.86 12.30 0 -1 4 -30 134.23 9.52 0 1 -4 -30 139.24 15.20 0 1 4 -30 117.25 7.18 0 -1 -4 -30 145.13 9.65 0 1 -4 30 132.87 10.30 0 1 4 -30 144.31 14.25 0 -1 -4 30 148.67 10.02 0 -2 -4 -30 16.49 9.75 0 2 4 30 7.85 6.75 0 2 4 -30 6.90 10.56 0 -2 4 30 9.79 10.21 0 2 -4 30 4.44 7.17 0 -2 -4 -30 11.91 11.07 0 -2 -4 30 11.09 9.71 0 -2 -4 -30 12.90 9.54 0 -2 4 -30 22.06 11.12 0 2 -4 -30 12.90 7.54 0 -2 4 -30 19.04 9.00 0 2 4 -30 5.50 9.48 0 -2 -4 30 8.73 11.85 0 -3 -4 30 492.15 14.80 0 3 4 30 500.61 8.27 0 -3 4 30 463.89 8.51 0 3 -4 30 476.80 11.62 0 -3 -4 -30 424.88 7.90 0 -3 4 -30 445.47 12.30 0 -3 -4 30 474.99 8.88 0 3 -4 -30 482.62 11.51 0 -3 -4 -30 499.96 11.42 0 -3 4 -30 510.03 11.15 0 3 4 -30 483.08 13.42 0 3 4 -30 479.33 11.39 0 -3 -4 -30 489.34 11.12 0 -4 -4 30 546.07 15.70 0 4 -4 30 539.91 12.28 0 -4 4 30 524.18 8.80 0 -4 4 -30 521.32 12.21 0 -4 -4 -30 477.69 8.86 0 4 4 -30 532.19 15.28 0 -4 -4 30 506.19 8.75 0 -4 4 -30 544.55 11.01 0 4 -4 -30 541.49 12.08 0 -4 -4 -30 511.04 11.23 0 4 4 -30 535.83 11.24 0 -4 -4 -30 494.30 9.15 0 -5 -4 30 182.66 15.46 0 5 -4 30 197.83 10.94 0 -5 4 30 174.36 10.17 0 -5 4 -30 185.83 10.71 0 -5 -4 -30 187.60 9.96 0 -5 -4 30 203.39 10.35 0 -5 4 -30 197.46 10.03 0 5 -4 -30 179.82 8.63 0 5 4 -30 169.94 7.71 0 -5 -4 -30 202.49 9.93 0 5 4 -30 167.02 12.98 0 -5 -4 -30 194.89 9.98 0 6 -4 30 11.82 9.62 0 -6 -4 30 18.47 13.72 0 -6 4 -30 5.75 9.30 0 -6 4 30 21.84 9.22 0 -6 -4 -30 23.30 8.54 0 -6 -4 30 26.66 9.26 0 -6 4 -30 21.46 9.23 0 6 -4 -30 22.92 10.33 0 6 4 -30 28.32 9.19 0 -6 -4 -30 14.29 8.75 0 -6 -4 -30 26.55 8.86 0 -7 4 -30 26.89 6.69 0 -7 4 30 38.31 9.56 0 -7 -4 30 29.26 14.20 0 -7 -4 -30 41.31 9.04 0 -7 -4 30 40.27 8.97 0 -7 4 -30 41.15 8.96 0 -7 -4 -30 24.99 8.69 0 7 -4 -30 29.02 10.29 0 -7 -4 -30 30.18 8.81 0 -8 4 -30 49.06 9.60 0 -8 4 30 64.63 9.65 0 -8 -4 -30 60.78 8.94 0 -8 -4 30 62.33 13.96 0 -8 -4 30 60.00 9.15 0 -8 4 -30 66.58 9.66 0 -8 -4 -30 68.62 6.58 0 8 -4 -30 73.32 10.63 0 -8 -4 -30 66.57 9.19 0 0 -5 -30 -1.26 12.24 0 0 5 30 -2.66 6.43 0 0 -5 30 -1.09 6.22 0 0 -5 -30 -10.73 9.14 0 0 5 -30 8.53 6.39 0 0 5 -30 1.97 11.29 0 0 -5 30 1.08 9.98 0 0 -5 -30 3.86 11.32 0 -1 -5 -30 206.50 10.62 0 1 5 30 191.62 9.97 0 -1 5 30 194.83 7.71 0 1 -5 -30 207.44 18.61 0 1 -5 30 201.01 7.73 0 1 -5 -30 202.02 17.67 0 -1 -5 30 200.03 9.76 0 -1 -5 -30 197.82 10.39 0 -1 -5 -30 189.89 10.20 0 1 -5 -30 193.74 7.74 0 -1 5 -30 199.78 12.09 0 -1 5 -30 192.12 7.45 0 1 5 -30 188.63 9.77 0 1 -5 30 215.96 10.68 0 1 5 -30 207.48 14.73 0 -1 -5 30 199.84 10.87 0 -2 -5 30 20.05 9.98 0 2 5 30 20.58 6.93 0 -2 5 30 27.07 9.88 0 2 5 -30 26.50 13.20 0 2 -5 30 23.99 9.93 0 -2 -5 -30 20.42 9.65 0 -2 -5 30 9.18 9.55 0 2 -5 -30 18.83 10.06 0 -2 5 -30 31.56 11.35 0 -2 5 -30 31.06 9.20 0 2 5 -30 26.40 6.82 0 -2 -5 -30 33.26 11.20 0 2 -5 30 38.46 10.02 0 -2 -5 -30 30.32 9.19 0 -3 -5 -30 49.90 8.94 0 -3 -5 30 49.02 12.38 0 -3 5 30 70.59 9.77 0 3 -5 30 48.87 9.73 0 -3 -5 -30 42.34 9.14 0 -3 5 -30 60.29 10.38 0 -3 -5 30 33.20 9.51 0 3 -5 -30 41.10 10.18 0 3 5 -30 43.56 10.67 0 -3 5 -30 40.16 9.09 0 3 5 -30 47.40 9.26 0 -3 -5 -30 58.05 9.50 0 -4 -5 30 71.34 10.21 0 4 5 -30 69.45 11.94 0 -4 -5 -30 76.10 9.38 0 4 -5 30 78.29 11.02 0 -4 5 30 93.24 9.46 0 -4 -5 -30 66.52 9.20 0 -4 5 -30 56.58 10.27 0 -4 -5 30 87.45 9.29 0 4 -5 -30 77.99 7.76 0 -4 5 -30 85.69 9.60 0 4 5 -30 59.89 9.13 0 -4 -5 -30 91.10 9.90 0 5 5 -30 35.83 11.36 0 5 -5 30 49.78 10.85 0 -5 5 30 30.81 9.87 0 -5 -5 30 39.61 12.26 0 -5 5 -30 28.24 9.96 0 -5 -5 -30 25.49 9.10 0 -5 -5 -30 36.67 6.35 0 -5 -5 30 31.49 8.88 0 -5 5 -30 42.98 9.42 0 5 -5 -30 46.74 10.61 0 5 5 -30 30.70 9.21 0 -5 -5 -30 43.13 9.55 0 6 -5 30 14.82 10.26 0 -6 5 30 18.89 9.26 0 6 5 -30 13.17 12.65 0 -6 5 -30 14.35 9.25 0 -6 -5 30 7.55 12.04 0 -6 -5 -30 18.42 6.53 0 -6 -5 -30 12.98 9.00 0 -6 -5 30 -5.30 6.61 0 -6 5 -30 22.07 9.61 0 6 -5 -30 16.15 10.04 0 6 5 -30 30.17 9.07 0 -6 -5 -30 21.71 8.04 0 -7 5 30 12.66 9.10 0 -7 5 -30 5.86 6.41 0 -7 -5 -30 -1.90 8.60 0 -7 -5 -30 13.02 8.47 0 -7 -5 30 0.81 13.49 0 -7 -5 30 7.81 8.61 0 -7 5 -30 13.04 8.92 0 7 -5 -30 11.44 10.01 0 -7 -5 -30 16.60 8.41 0 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427.06 11.65 0 -2 -6 -30 401.81 11.53 0 -3 -6 30 31.43 9.80 0 -3 6 30 18.96 9.54 0 3 -6 30 29.09 9.62 0 -3 -6 -30 33.19 8.96 0 -3 -6 30 14.22 9.43 0 -3 6 -30 42.51 10.67 0 3 -6 -30 32.94 9.69 0 3 6 -30 35.44 9.62 0 -3 6 -30 34.71 6.62 0 -3 -6 -30 33.43 9.10 0 3 6 -30 33.99 9.22 0 3 -6 30 46.35 9.74 0 -3 -6 -30 37.47 9.31 0 4 6 -30 41.70 11.78 0 -4 6 30 37.40 9.86 0 -4 -6 30 46.95 12.23 0 4 -6 30 58.84 10.42 0 -4 -6 -30 58.04 8.60 0 -4 6 -30 47.98 7.29 0 -4 -6 30 62.40 9.43 0 4 -6 -30 45.64 10.56 0 -4 6 -30 48.58 9.62 0 -4 -6 -30 48.72 9.58 0 4 6 -30 39.06 8.86 0 -4 -6 -30 35.86 9.46 0 5 -6 30 41.02 10.45 0 -5 6 30 69.13 9.31 0 -5 -6 30 68.17 12.47 0 -5 -6 -30 57.73 6.37 0 -5 6 -30 41.68 10.29 0 -5 -6 30 59.59 8.90 0 5 -6 -30 62.61 10.43 0 -5 6 -30 54.43 7.30 0 5 6 -30 54.49 11.72 0 5 6 -30 46.43 6.49 0 -5 -6 -30 48.74 9.41 0 -5 -6 -30 73.16 9.33 0 6 6 -30 22.80 10.90 0 6 -6 30 12.98 10.69 0 -6 6 30 34.68 9.67 0 -6 -6 -30 29.27 5.91 0 -6 6 -30 24.13 9.94 0 -6 -6 30 35.55 11.66 0 -6 -6 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30 5.12 9.60 0 -2 -7 -30 170.80 12.28 0 -2 -7 30 180.04 11.05 0 -2 7 30 180.13 9.63 0 2 7 -30 171.86 12.22 0 2 -7 30 166.72 10.31 0 -2 -7 -30 163.63 7.13 0 -2 -7 30 189.71 7.45 0 2 -7 -30 162.71 7.67 0 -2 7 -30 165.27 8.66 0 -2 7 -30 156.02 6.96 0 2 7 -30 177.29 7.32 0 -2 -7 -30 181.01 12.18 0 2 -7 30 170.53 10.51 0 -3 7 30 30.51 9.50 0 -3 -7 30 45.45 11.78 0 3 -7 30 34.32 10.08 0 -3 -7 -30 29.31 9.04 0 -3 -7 -30 33.13 8.91 0 -3 -7 30 33.39 9.11 0 3 -7 -30 38.67 7.37 0 -3 7 -30 20.31 7.35 0 3 7 -30 29.56 12.91 0 -3 7 -30 27.67 6.69 0 3 7 -30 29.79 8.89 0 -3 -7 -30 30.26 8.93 0 3 -7 30 37.92 9.68 0 -4 7 30 125.09 9.76 0 4 -7 30 117.93 10.62 0 -4 -7 30 95.22 12.34 0 -4 -7 -30 91.50 8.98 0 -4 7 -30 101.16 7.67 0 -4 -7 30 115.77 9.41 0 -4 -7 -30 104.78 9.66 0 4 -7 -30 113.54 10.78 0 -4 7 -30 97.25 9.54 0 4 7 -30 108.68 9.13 0 4 -7 30 96.45 7.37 0 4 7 -30 114.63 10.45 0 -5 7 30 -0.36 8.89 0 5 -7 30 28.79 10.24 0 -5 -7 -30 24.72 8.63 0 -5 -7 30 15.46 11.84 0 -5 7 -30 21.23 6.97 0 -5 -7 30 28.95 8.67 0 5 7 -30 11.51 9.66 0 5 -7 -30 19.50 10.32 0 -5 -7 -30 9.77 9.12 0 -5 7 -30 17.49 9.18 0 5 7 -30 14.00 8.63 0 -5 -7 -30 15.42 8.69 0 6 -7 30 22.02 10.05 0 -6 7 30 9.34 8.88 0 -6 -7 -30 -1.32 8.23 0 -6 7 -30 19.70 8.99 0 6 7 -30 6.93 8.76 0 -6 -7 30 4.35 9.39 0 -6 -7 30 16.58 8.88 0 -6 7 -30 -3.78 8.79 0 6 -7 -30 -16.32 10.36 0 -6 -7 -30 2.13 5.66 0 -6 -7 -30 -6.15 8.76 0 7 -7 30 23.93 10.06 0 -7 7 30 32.31 9.50 0 -7 -7 -30 10.87 8.55 0 -7 7 -30 16.30 9.48 0 -7 -7 30 11.19 9.58 0 -7 -7 30 11.67 8.99 0 7 7 -30 13.75 9.12 0 -7 7 -30 15.19 8.56 0 7 -7 -30 26.13 10.82 0 -7 -7 -30 14.07 8.40 0 -7 -7 -30 30.70 8.70 0 0 -8 30 468.42 11.45 0 0 -8 -30 466.10 14.34 0 0 -8 -30 452.52 11.14 0 0 -8 30 477.37 11.26 0 0 8 -30 482.52 10.88 0 0 8 -30 446.97 13.48 0 0 -8 -30 489.40 13.30 0 1 -8 30 16.20 10.06 0 1 8 -30 5.99 11.12 0 -1 -8 30 3.55 9.71 0 -1 8 30 11.05 9.03 0 -1 -8 -30 4.41 6.65 0 1 -8 30 0.61 9.82 0 1 -8 -30 5.14 9.74 0 -1 -8 30 13.40 9.50 0 -1 -8 -30 1.93 11.45 0 -1 8 -30 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8 -30 35.61 9.89 0 -5 8 -30 17.57 7.28 0 -5 -8 30 31.95 8.54 0 5 -8 -30 26.13 10.19 0 -5 8 -30 24.20 9.40 0 6 8 -30 4.18 8.96 0 -6 8 30 0.98 8.82 0 6 -8 30 -7.99 9.93 0 -6 -8 -30 3.09 8.26 0 -6 8 -30 4.08 9.41 0 -6 -8 30 4.15 11.43 0 -6 -8 -30 -1.79 8.41 0 -6 -8 30 10.26 8.19 0 6 -8 -30 10.75 10.28 0 -6 8 -30 -2.11 8.56 0 7 -8 30 9.80 10.14 0 -7 8 30 1.02 8.73 0 -7 -8 -30 2.50 6.12 0 -7 8 -30 2.90 9.27 0 -7 -8 -30 4.72 5.86 0 -7 -8 30 0.18 11.16 0 -7 -8 30 17.26 8.17 0 7 8 -30 -5.16 10.85 0 -7 8 -30 6.65 11.07 0 7 -8 -30 12.36 9.59 0 -7 -8 -30 -3.83 6.14 0 0 -9 30 14.63 9.88 0 0 -9 -30 -2.05 8.88 0 0 -9 -30 9.13 9.09 0 0 -9 30 22.56 9.71 0 0 9 -30 -7.88 9.22 0 0 9 -30 -7.24 11.60 0 1 -9 30 10.01 6.85 0 1 9 -30 21.80 11.14 0 -1 -9 30 28.45 10.10 0 -1 -9 -30 30.00 9.10 0 1 -9 30 19.23 9.45 0 1 -9 -30 34.80 9.29 0 -1 -9 30 18.65 8.97 0 -1 -9 -30 10.21 11.79 0 -1 9 -30 26.21 9.09 0 -1 9 -30 18.16 11.07 0 1 9 -30 18.92 8.45 0 1 -9 -30 23.06 15.84 0 2 -9 -30 64.86 21.60 0 -2 -9 30 57.25 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-41 5.24 11.99 0 -1 -2 -41 75.37 10.98 0 1 2 -41 77.11 12.80 0 1 2 41 80.22 6.63 0 -1 2 41 87.40 8.86 0 1 -2 41 69.93 8.68 0 -1 -2 41 87.83 8.82 0 -1 -2 -41 70.96 12.31 0 -1 -2 -41 67.18 8.90 0 1 -2 -41 52.70 8.93 0 -1 2 -41 53.32 6.51 0 1 2 -41 48.81 6.66 0 -1 2 -41 98.05 10.47 0 2 2 41 0.47 8.76 0 2 -2 41 8.10 8.50 0 -2 2 41 8.69 8.41 0 -2 -2 41 9.80 8.44 0 -2 -2 -41 5.90 8.59 0 -2 -2 -41 5.16 7.90 0 -2 -2 -41 0.27 8.61 0 -2 2 -41 -2.90 9.12 0 -2 2 -41 0.21 8.54 0 2 2 -41 4.65 13.35 0 2 -2 -41 10.58 8.55 0 2 2 -41 8.64 5.84 0 2 2 -41 2.57 16.09 0 0 -3 -41 -0.72 13.57 0 0 3 41 7.96 8.49 0 0 -3 41 -14.38 8.66 0 0 -3 -41 3.97 8.21 0 0 3 -41 -10.16 8.36 0 0 -3 -41 0.92 13.72 0 0 3 -41 5.10 12.00 0 1 3 -41 9.17 12.05 0 1 3 41 -1.12 8.67 0 -1 3 41 20.16 8.44 0 1 -3 41 20.35 8.48 0 -1 -3 41 18.59 8.51 0 -1 -3 -41 11.74 9.92 0 -1 -3 -41 3.09 8.67 0 1 -3 -41 1.59 8.43 0 -1 -3 -41 7.75 11.08 0 -1 3 -41 23.92 8.36 0 1 3 -41 24.89 8.46 0 -1 3 -41 1.02 11.79 0 2 3 41 47.86 8.57 0 -2 3 41 18.94 5.90 0 2 -3 41 15.93 8.64 0 -2 -3 41 34.88 8.35 0 -2 -3 -41 27.67 9.48 0 -2 -3 -41 30.78 8.54 0 -2 3 -41 25.38 9.57 0 2 -3 -41 19.36 8.81 0 -2 3 -41 26.86 8.42 0 2 3 -41 28.36 13.83 0 2 3 -41 38.36 8.41 0 -2 -3 -41 18.55 10.35 0 0 4 41 36.56 8.57 0 0 -4 41 41.60 8.51 0 0 -4 -41 32.78 8.75 0 0 -4 -41 35.60 15.80 0 0 4 -41 36.23 8.18 0 0 -4 -41 34.92 13.03 0 0 4 -41 24.98 12.26 0 1 4 -41 24.95 12.11 0 1 4 41 19.33 6.25 0 -1 4 41 27.79 8.46 0 -1 -4 -41 18.84 8.79 0 1 -4 41 8.76 8.54 0 -1 -4 41 17.72 8.46 0 -1 -4 -41 20.70 11.77 0 -1 -4 -41 11.08 8.45 0 1 -4 -41 27.72 8.61 0 -1 4 -41 16.31 6.20 0 1 4 -41 12.32 5.85 0 -1 4 -41 34.45 11.99 0 2 4 41 14.03 8.15 0 -2 4 41 3.27 8.55 0 2 -4 41 3.95 5.95 0 -2 -4 -41 0.53 9.34 0 -2 -4 41 -6.82 8.54 0 -2 -4 -41 9.89 8.18 0 -2 -4 -41 -7.32 8.84 0 2 4 -41 1.09 10.99 0 2 -4 -41 -0.93 8.40 0 -2 4 -41 15.18 9.53 0 -2 4 -41 15.93 5.87 0 2 4 -41 5.01 8.42 0 0 5 41 -5.03 8.10 0 0 -5 41 5.87 7.92 0 0 -5 -41 1.49 14.36 0 0 -5 -41 9.91 8.50 0 0 -5 -41 0.66 15.28 0 0 5 -41 -8.33 5.57 0 0 5 -41 8.22 9.47 0 1 5 -41 57.63 10.39 0 1 5 41 35.32 8.40 0 -1 5 41 36.70 8.92 0 1 -5 41 30.94 9.16 0 -1 -5 41 60.63 8.54 0 -1 -5 -41 35.10 12.19 0 -1 -5 -41 51.94 8.81 0 1 -5 -41 41.78 9.03 0 -1 5 -41 38.21 8.61 0 1 5 -41 39.66 8.59 0 -1 5 -41 48.64 9.89 0 -1 -5 -41 42.30 11.19 0 0 0 42 12.96 8.53 0 0 0 -42 26.36 8.56 0 0 0 -42 10.45 11.60 0 0 0 -42 5.44 10.21 0 1 0 42 -6.68 8.46 0 -1 0 42 29.70 8.28 0 1 0 -42 2.79 15.23 0 -1 0 -42 16.10 8.55 0 -1 0 -42 -3.61 11.78 0 1 0 -42 11.86 5.77 0 -1 0 -42 12.57 9.93 0 1 0 -42 9.05 15.09 0 0 1 42 -5.85 8.71 0 0 -1 42 -2.13 5.83 0 0 -1 -42 -2.57 6.04 0 0 1 -42 -3.46 8.34 0 0 1 -42 0.46 9.81 0 0 -1 -42 6.00 11.63 0 0 1 -42 6.16 11.86 0 0 -1 -42 2.48 11.77 0 -1 1 -42 7.73 8.44 0 1 1 -42 -3.61 13.38 0 1 1 42 3.47 8.60 0 1 -1 42 -0.20 6.11 0 -1 1 42 11.38 5.97 0 -1 -1 42 15.28 8.48 0 -1 -1 -42 21.92 8.40 0 -1 -1 -42 6.97 9.69 0 -1 -1 -42 1.89 10.04 0 -1 1 -42 -2.71 5.79 0 1 -1 -42 6.02 5.99 0 1 1 -42 -0.48 8.40 0 -1 1 -42 9.39 9.15 0 1 1 -42 6.21 11.60 0 0 2 42 -1.87 5.79 0 0 -2 42 7.50 6.11 0 0 -2 -42 2.66 11.98 0 0 -2 -42 7.44 5.82 0 0 2 -42 10.68 6.04 0 0 -2 -42 -3.22 13.69 0 0 2 -42 1.04 11.91 0 1 2 -42 11.49 11.74 0 1 2 42 2.50 8.49 0 -1 2 42 13.75 8.48 0 1 -2 42 4.01 6.20 0 -1 -2 42 4.55 8.44 0 -1 -2 -42 17.25 11.82 0 -1 -2 -42 -8.58 8.53 0 1 -2 -42 10.24 6.21 0 -1 2 -42 15.20 8.52 0 1 2 -42 7.55 8.58 0 -1 2 -42 28.20 11.58 0 -1 -2 -42 15.10 9.94 0 ; _shelx_hkl_checksum 13154 _shelx_res_file ; TITL Co(NCSe)2(4-Methoxypyridin)4 at 200K in Pbca aj1732.res created by SHELXL-2016/6 at 13:14:34 on 18-Jan-2023 CELL 0.71073 10.05310 17.34790 34.31410 90.0000 90.0000 90.0000 ZERR 8.00 0.0002 0.0004 0.0005 0.0000 0.0000 0.0000 LATT 1 SYMM 0.5-X, -Y, 0.5+Z SYMM -X, 0.5+Y, 0.5-Z SYMM 0.5+X, 0.5-Y, -Z SFAC C H N O CO SE UNIT 208 224 48 32 8 16 L.S. 10 TEMP -73 ACTA BOND $H HTAB EQIV $1 x+1/2, y, -z+3/2 HTAB C11 O11_$1 EQIV $2 x-1, y, z HTAB C15 O31_$2 EQIV $3 x-1/2, y, -z+3/2 HTAB C16 Se1_$3 EQIV $4 -x+3/2, y-1/2, z HTAB C22 Se1_$4 EQIV $5 -x+1, -y+1, -z+1 HTAB C26 Se1_$5 EQIV $6 x+1, y, z HTAB C36 Se2_$6 EQIV $7 x-1/2, -y+1/2, -z+1 HTAB C41 O21_$7 EQIV $8 -x+1/2, y+1/2, z HTAB C45 Se2_$8 HTAB C46 Se1_$2 WGHT 0.038200 4.274800 FVAR 0.36417 CO1 5 0.422962 0.389840 0.622074 11.00000 0.04374 0.04212 = 0.04252 0.00372 0.00192 -0.00171 N1 3 0.489840 0.500813 0.606511 11.00000 0.05533 0.04531 = 0.05218 0.00499 0.00561 -0.00253 C1 1 0.531999 0.562970 0.605943 11.00000 0.05081 0.05244 = 0.04048 0.00472 0.00429 0.00259 SE1 6 0.596338 0.658443 0.605352 11.00000 0.09470 0.05033 = 0.07579 0.00265 0.00388 -0.02052 N2 3 0.360087 0.278861 0.637258 11.00000 0.05182 0.04603 = 0.05324 0.00444 -0.00072 -0.00492 C2 1 0.346272 0.222627 0.655085 11.00000 0.04312 0.04629 = 0.04651 -0.00668 -0.00115 -0.00310 SE2 6 0.327693 0.137230 0.683055 11.00000 0.08200 0.04693 = 0.07415 0.01474 -0.00418 -0.00859 N11 3 0.356673 0.433411 0.677053 11.00000 0.03728 0.04700 = 0.04350 0.00196 0.00113 -0.00193 C11 1 0.429691 0.484094 0.696979 11.00000 0.03708 0.05126 = 0.04634 0.00470 0.00062 -0.00559 AFIX 43 H11 2 0.508929 0.502719 0.685193 11.00000 -1.20000 AFIX 0 C12 1 0.397795 0.511104 0.733417 11.00000 0.03927 0.04769 = 0.04357 0.00312 -0.00228 -0.00304 AFIX 43 H12 2 0.454554 0.546307 0.746578 11.00000 -1.20000 AFIX 0 C13 1 0.280943 0.485807 0.750516 11.00000 0.04311 0.04733 = 0.04258 0.00282 0.00295 0.00309 C14 1 0.203145 0.433195 0.729975 11.00000 0.03857 0.05385 = 0.05233 0.00343 0.00528 -0.00526 AFIX 43 H14 2 0.122509 0.414453 0.740865 11.00000 -1.20000 AFIX 0 C15 1 0.243589 0.408909 0.694222 11.00000 0.03774 0.04590 = 0.05111 0.00281 0.00135 -0.00424 AFIX 43 H15 2 0.189538 0.372893 0.680651 11.00000 -1.20000 AFIX 0 O11 4 0.236064 0.508329 0.785690 11.00000 0.05705 0.07595 = 0.05089 -0.01232 0.01269 -0.00919 C16 1 0.317738 0.560036 0.807673 11.00000 0.08201 0.08229 = 0.05853 -0.02274 0.01218 -0.01834 AFIX 137 H16A 2 0.402605 0.534966 0.813740 11.00000 -1.50000 H16B 2 0.272280 0.573788 0.831961 11.00000 -1.50000 H16C 2 0.334262 0.606763 0.792371 11.00000 -1.50000 AFIX 0 N21 3 0.504006 0.345616 0.567890 11.00000 0.05249 0.04584 = 0.04237 0.00247 0.00027 0.00297 C21 1 0.585598 0.284296 0.567900 11.00000 0.06084 0.04264 = 0.04520 0.00340 0.00021 0.00429 AFIX 43 H21 2 0.587114 0.252310 0.590368 11.00000 -1.20000 AFIX 0 C22 1 0.666576 0.265393 0.537352 11.00000 0.06168 0.04193 = 0.04988 -0.00012 -0.00034 0.00770 AFIX 43 H22 2 0.722378 0.221281 0.538708 11.00000 -1.20000 AFIX 0 C23 1 0.666073 0.311475 0.504411 11.00000 0.05344 0.04329 = 0.04568 -0.00524 0.00413 -0.00346 C24 1 0.577109 0.372433 0.502665 11.00000 0.06487 0.04830 = 0.04359 0.00437 -0.00029 0.00693 AFIX 43 H24 2 0.569119 0.403015 0.479818 11.00000 -1.20000 AFIX 0 C25 1 0.500710 0.387213 0.535115 11.00000 0.05684 0.05281 = 0.04340 0.00329 -0.00111 0.00980 AFIX 43 H25 2 0.441604 0.429897 0.534145 11.00000 -1.20000 AFIX 0 O21 4 0.753844 0.292861 0.476153 11.00000 0.07428 0.05038 = 0.05320 -0.00173 0.01715 0.00532 C26 1 0.767198 0.344882 0.444069 11.00000 0.10120 0.05966 = 0.06736 0.00683 0.03458 0.00584 AFIX 137 H26A 2 0.683599 0.346536 0.429403 11.00000 -1.50000 H26B 2 0.839033 0.327220 0.426951 11.00000 -1.50000 H26C 2 0.788117 0.396546 0.453862 11.00000 -1.50000 AFIX 0 N31 3 0.616481 0.364514 0.649363 11.00000 0.04195 0.04589 = 0.04451 0.00364 0.00221 -0.00111 C31 1 0.732763 0.387965 0.634226 11.00000 0.04805 0.05399 = 0.05200 0.01138 0.00441 -0.00621 AFIX 43 H31 2 0.730644 0.422024 0.612555 11.00000 -1.20000 AFIX 0 C32 1 0.854306 0.365552 0.648267 11.00000 0.04366 0.06170 = 0.06013 0.01043 0.00744 -0.00754 AFIX 43 H32 2 0.933751 0.384252 0.636632 11.00000 -1.20000 AFIX 0 C33 1 0.860169 0.315387 0.679575 11.00000 0.04044 0.04989 = 0.05014 -0.00167 -0.00296 -0.00306 C34 1 0.741799 0.291322 0.695865 11.00000 0.04721 0.05117 = 0.04501 0.00631 -0.00022 -0.00610 AFIX 43 H34 2 0.741410 0.257422 0.717608 11.00000 -1.20000 AFIX 0 C35 1 0.624586 0.317251 0.680085 11.00000 0.04151 0.05422 = 0.04324 0.00630 0.00347 -0.00508 AFIX 43 H35 2 0.543881 0.300535 0.691747 11.00000 -1.20000 AFIX 0 O31 4 0.982179 0.294254 0.691800 11.00000 0.04277 0.07121 = 0.06996 0.01158 -0.00636 -0.00440 C36 1 0.990733 0.231206 0.718563 11.00000 0.05770 0.08998 = 0.08384 0.02680 -0.01749 0.00436 AFIX 137 H36A 2 0.949864 0.245955 0.743396 11.00000 -1.50000 H36B 2 1.084362 0.217962 0.722851 11.00000 -1.50000 H36C 2 0.943834 0.186517 0.707773 11.00000 -1.50000 AFIX 0 N41 3 0.230045 0.412699 0.595905 11.00000 0.04959 0.04498 = 0.04660 0.00040 -0.00081 0.00125 C41 1 0.171972 0.360684 0.572404 11.00000 0.05581 0.05051 = 0.06230 -0.01211 -0.00918 0.00755 AFIX 43 H41 2 0.214155 0.312096 0.569187 11.00000 -1.20000 AFIX 0 C42 1 0.055733 0.373703 0.552876 11.00000 0.05689 0.05862 = 0.06198 -0.01280 -0.00827 0.00305 AFIX 43 H42 2 0.019107 0.335190 0.536376 11.00000 -1.20000 AFIX 0 C43 1 -0.007964 0.443966 0.557502 11.00000 0.04374 0.05865 = 0.05125 0.00660 0.00050 0.00131 C44 1 0.046740 0.496796 0.582948 11.00000 0.05023 0.04495 = 0.05631 0.00528 0.00642 0.00320 AFIX 43 H44 2 0.003580 0.544520 0.587894 11.00000 -1.20000 AFIX 0 C45 1 0.165244 0.478960 0.601048 11.00000 0.05245 0.04084 = 0.04941 0.00159 0.00186 -0.00017 AFIX 43 H45 2 0.202896 0.516039 0.618178 11.00000 -1.20000 AFIX 0 O41 4 -0.120765 0.454296 0.536666 11.00000 0.05314 0.07494 = 0.08069 0.00336 -0.01511 0.00819 C46 1 -0.185282 0.527646 0.539368 11.00000 0.06136 0.07576 = 0.10239 0.01734 -0.01296 0.01711 AFIX 137 H46A 2 -0.212437 0.536910 0.566395 11.00000 -1.50000 H46B 2 -0.263923 0.528030 0.522492 11.00000 -1.50000 H46C 2 -0.123661 0.568224 0.531068 11.00000 -1.50000 AFIX 0 HKLF 4 REM Co(NCSe)2(4-Methoxypyridin)4 at 200K in Pbca REM R1 = 0.0376 for 5130 Fo > 4sig(Fo) and 0.0452 for all 5862 data REM 356 parameters refined using 0 restraints END WGHT 0.0382 4.2747 REM Instructions for potential hydrogen bonds HTAB C11 O11_$1 HTAB C15 O31_$2 HTAB C16 Se1_$3 HTAB C22 Se1_$4 HTAB C26 Se1_$5 HTAB C36 Se2_$6 HTAB C41 O21_$7 HTAB C45 Se2_$8 HTAB C46 Se1_$2 REM Highest difference peak 0.335, deepest hole -0.475, 1-sigma level 0.047 Q1 1 0.2442 0.1482 0.6766 11.00000 0.05 0.34 Q2 1 0.6778 0.6315 0.6074 11.00000 0.05 0.29 Q3 1 0.3827 0.1418 0.6639 11.00000 0.05 0.28 Q4 1 0.3817 0.4119 0.6594 11.00000 0.05 0.26 Q5 1 0.3024 0.4048 0.6023 11.00000 0.05 0.25 Q6 1 0.5452 0.3860 0.6408 11.00000 0.05 0.24 Q7 1 0.4707 0.4606 0.6074 11.00000 0.05 0.23 Q8 1 0.4447 0.1584 0.7045 11.00000 0.05 0.22 Q9 1 0.4676 0.3512 0.5872 11.00000 0.05 0.22 Q10 1 0.4914 0.4448 0.6011 11.00000 0.05 0.22 Q11 1 0.4411 0.4608 0.6414 11.00000 0.05 0.22 Q12 1 0.3603 0.1526 0.7194 11.00000 0.05 0.21 Q13 1 0.3394 0.1685 0.7049 11.00000 0.05 0.21 Q14 1 0.5420 0.3406 0.6222 11.00000 0.05 0.21 Q15 1 0.3758 0.3189 0.6385 11.00000 0.05 0.20 Q16 1 0.4023 0.3617 0.6598 11.00000 0.05 0.19 Q17 1 0.2648 0.0732 0.6721 11.00000 0.05 0.19 Q18 1 0.5290 0.4478 0.6315 11.00000 0.05 0.19 Q19 1 0.2850 0.3916 0.6265 11.00000 0.05 0.19 Q20 1 0.4303 0.0897 0.6863 11.00000 0.05 0.18 ; _shelx_res_checksum 71124 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Co Co1 0.42296(4) 0.38984(2) 0.62207(2) 0.04280(10) Uani d 1 . . N N1 0.4898(3) 0.50081(14) 0.60651(7) 0.0509(5) Uani d 1 . . C C1 0.5320(3) 0.56297(17) 0.60594(8) 0.0479(6) Uani d 1 . . Se Se1 0.59634(4) 0.65844(2) 0.60535(2) 0.07361(13) Uani d 1 . . N N2 0.3601(2) 0.27886(13) 0.63726(7) 0.0504(5) Uani d 1 . . C C2 0.3463(3) 0.22263(16) 0.65509(8) 0.0453(6) Uani d 1 . . Se Se2 0.32769(4) 0.13723(2) 0.68306(2) 0.06769(12) Uani d 1 . . N N11 0.3567(2) 0.43341(13) 0.67705(6) 0.0426(5) Uani d 1 . . C C11 0.4297(3) 0.48409(16) 0.69698(8) 0.0449(6) Uani d 1 . . H H11 0.508929 0.502719 0.685193 0.054 Uiso calc 1 . . C C12 0.3978(3) 0.51110(16) 0.73342(7) 0.0435(6) Uani d 1 . . H H12 0.454554 0.546307 0.746578 0.052 Uiso calc 1 . . C C13 0.2809(3) 0.48581(15) 0.75052(8) 0.0443(6) Uani d 1 . . C C14 0.2031(3) 0.43319(16) 0.72997(8) 0.0482(6) Uani d 1 . . H H14 0.122509 0.414453 0.740865 0.058 Uiso calc 1 . . C C15 0.2436(3) 0.40891(15) 0.69422(8) 0.0449(6) Uani d 1 . . H H15 0.189538 0.372893 0.680651 0.054 Uiso calc 1 . . O O11 0.2361(2) 0.50833(14) 0.78569(6) 0.0613(5) Uani d 1 . . C C16 0.3177(4) 0.5600(2) 0.80767(10) 0.0743(10) Uani d 1 . . H H16A 0.402605 0.534966 0.813740 0.111 Uiso calc 1 . . H H16B 0.272280 0.573788 0.831961 0.111 Uiso calc 1 . . H H16C 0.334262 0.606763 0.792371 0.111 Uiso calc 1 . . N N21 0.5040(2) 0.34562(13) 0.56789(6) 0.0469(5) Uani d 1 . . C C21 0.5856(3) 0.28430(16) 0.56790(8) 0.0496(6) Uani d 1 . . H H21 0.587114 0.252310 0.590368 0.059 Uiso calc 1 . . C C22 0.6666(3) 0.26539(16) 0.53735(8) 0.0512(7) Uani d 1 . . H H22 0.722378 0.221281 0.538708 0.061 Uiso calc 1 . . C C23 0.6661(3) 0.31148(15) 0.50441(8) 0.0475(6) Uani d 1 . . C C24 0.5771(3) 0.37243(16) 0.50266(8) 0.0523(7) Uani d 1 . . H H24 0.569119 0.403015 0.479818 0.063 Uiso calc 1 . . C C25 0.5007(3) 0.38721(17) 0.53511(8) 0.0510(7) Uani d 1 . . H H25 0.441604 0.429897 0.534145 0.061 Uiso calc 1 . . O O21 0.7538(2) 0.29286(12) 0.47615(6) 0.0593(5) Uani d 1 . . C C26 0.7672(4) 0.3449(2) 0.44407(10) 0.0761(11) Uani d 1 . . H H26A 0.683599 0.346536 0.429403 0.114 Uiso calc 1 . . H H26B 0.839033 0.327220 0.426951 0.114 Uiso calc 1 . . H H26C 0.788117 0.396546 0.453862 0.114 Uiso calc 1 . . N N31 0.6165(2) 0.36451(13) 0.64936(6) 0.0441(5) Uani d 1 . . C C31 0.7328(3) 0.38797(17) 0.63423(8) 0.0513(7) Uani d 1 . . H H31 0.730644 0.422024 0.612555 0.062 Uiso calc 1 . . C C32 0.8543(3) 0.36555(18) 0.64827(9) 0.0552(7) Uani d 1 . . H H32 0.933751 0.384252 0.636632 0.066 Uiso calc 1 . . C C33 0.8602(3) 0.31539(17) 0.67957(8) 0.0468(6) Uani d 1 . . C C34 0.7418(3) 0.29132(16) 0.69587(8) 0.0478(6) Uani d 1 . . H H34 0.741410 0.257422 0.717608 0.057 Uiso calc 1 . . C C35 0.6246(3) 0.31725(17) 0.68008(7) 0.0463(6) Uani d 1 . . H H35 0.543881 0.300535 0.691747 0.056 Uiso calc 1 . . O O31 0.9822(2) 0.29425(13) 0.69180(6) 0.0613(5) Uani d 1 . . C C36 0.9907(4) 0.2312(2) 0.71856(11) 0.0772(10) Uani d 1 . . H H36A 0.949864 0.245955 0.743396 0.116 Uiso calc 1 . . H H36B 1.084362 0.217962 0.722851 0.116 Uiso calc 1 . . H H36C 0.943834 0.186517 0.707773 0.116 Uiso calc 1 . . N N41 0.2300(2) 0.41270(13) 0.59591(6) 0.0471(5) Uani d 1 . . C C41 0.1720(3) 0.36068(17) 0.57240(9) 0.0562(7) Uani d 1 . . H H41 0.214155 0.312096 0.569187 0.067 Uiso calc 1 . . C C42 0.0557(3) 0.37370(19) 0.55288(9) 0.0592(8) Uani d 1 . . H H42 0.019107 0.335190 0.536376 0.071 Uiso calc 1 . . C C43 -0.0080(3) 0.44397(18) 0.55750(8) 0.0512(6) Uani d 1 . . C C44 0.0467(3) 0.49680(16) 0.58295(8) 0.0505(7) Uani d 1 . . H H44 0.003580 0.544520 0.587894 0.061 Uiso calc 1 . . C C45 0.1652(3) 0.47896(15) 0.60105(8) 0.0476(6) Uani d 1 . . H H45 0.202896 0.516039 0.618178 0.057 Uiso calc 1 . . O O41 -0.1208(2) 0.45430(15) 0.53667(7) 0.0696(6) Uani d 1 . . C C46 -0.1853(4) 0.5276(2) 0.53937(13) 0.0798(11) Uani d 1 . . H H46A -0.212437 0.536910 0.566395 0.120 Uiso calc 1 . . H H46B -0.263923 0.528030 0.522492 0.120 Uiso calc 1 . . H H46C -0.123661 0.568224 0.531068 0.120 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Co1 0.04374(19) 0.04212(19) 0.04252(19) -0.00171(15) 0.00192(15) 0.00372(14) N1 0.0553(14) 0.0453(13) 0.0522(13) -0.0025(11) 0.0056(11) 0.0050(10) C1 0.0508(16) 0.0524(16) 0.0405(13) 0.0026(13) 0.0043(12) 0.0047(11) Se1 0.0947(3) 0.05033(18) 0.0758(2) -0.02052(18) 0.00388(19) 0.00265(15) N2 0.0518(14) 0.0460(13) 0.0532(13) -0.0049(11) -0.0007(11) 0.0044(11) C2 0.0431(14) 0.0463(15) 0.0465(14) -0.0031(12) -0.0012(11) -0.0067(12) Se2 0.0820(3) 0.04693(18) 0.0741(2) -0.00859(16) -0.00418(18) 0.01474(15) N11 0.0373(11) 0.0470(12) 0.0435(11) -0.0019(9) 0.0011(9) 0.0020(9) C11 0.0371(13) 0.0513(15) 0.0463(14) -0.0056(11) 0.0006(11) 0.0047(11) C12 0.0393(14) 0.0477(14) 0.0436(13) -0.0030(11) -0.0023(11) 0.0031(11) C13 0.0431(14) 0.0473(14) 0.0426(13) 0.0031(12) 0.0030(11) 0.0028(11) C14 0.0386(14) 0.0539(16) 0.0523(15) -0.0053(12) 0.0053(12) 0.0034(12) C15 0.0377(13) 0.0459(14) 0.0511(14) -0.0042(11) 0.0014(11) 0.0028(11) O11 0.0571(12) 0.0760(14) 0.0509(11) -0.0092(11) 0.0127(10) -0.0123(10) C16 0.082(2) 0.082(2) 0.0585(19) -0.018(2) 0.0122(17) -0.0227(17) N21 0.0525(14) 0.0458(12) 0.0424(11) 0.0030(10) 0.0003(10) 0.0025(9) C21 0.0608(17) 0.0426(14) 0.0452(14) 0.0043(13) 0.0002(12) 0.0034(11) C22 0.0617(18) 0.0419(14) 0.0499(15) 0.0077(13) -0.0003(13) -0.0001(12) C23 0.0534(16) 0.0433(14) 0.0457(14) -0.0035(12) 0.0041(12) -0.0052(11) C24 0.0649(18) 0.0483(15) 0.0436(14) 0.0069(13) -0.0003(13) 0.0044(12) C25 0.0568(17) 0.0528(16) 0.0434(14) 0.0098(13) -0.0011(13) 0.0033(12) O21 0.0743(14) 0.0504(11) 0.0532(11) 0.0053(10) 0.0172(10) -0.0017(9) C26 0.101(3) 0.0597(19) 0.067(2) 0.0058(19) 0.035(2) 0.0068(16) N31 0.0420(12) 0.0459(12) 0.0445(11) -0.0011(10) 0.0022(9) 0.0036(9) C31 0.0481(16) 0.0540(16) 0.0520(15) -0.0062(13) 0.0044(12) 0.0114(13) C32 0.0437(15) 0.0617(18) 0.0601(17) -0.0075(14) 0.0074(13) 0.0104(14) C33 0.0404(14) 0.0499(15) 0.0501(14) -0.0031(12) -0.0030(12) -0.0017(12) C34 0.0472(15) 0.0512(15) 0.0450(14) -0.0061(12) -0.0002(12) 0.0063(12) C35 0.0415(14) 0.0542(15) 0.0432(13) -0.0051(12) 0.0035(11) 0.0063(12) O31 0.0428(11) 0.0712(14) 0.0700(13) -0.0044(10) -0.0064(10) 0.0116(11) C36 0.058(2) 0.090(3) 0.084(2) 0.0044(19) -0.0175(18) 0.027(2) N41 0.0496(13) 0.0450(12) 0.0466(12) 0.0013(10) -0.0008(10) 0.0004(9) C41 0.0558(18) 0.0505(16) 0.0623(17) 0.0076(14) -0.0092(14) -0.0121(13) C42 0.0569(18) 0.0586(18) 0.0620(18) 0.0030(14) -0.0083(14) -0.0128(14) C43 0.0437(15) 0.0586(17) 0.0513(15) 0.0013(13) 0.0005(12) 0.0066(13) C44 0.0502(16) 0.0450(14) 0.0563(16) 0.0032(12) 0.0064(13) 0.0053(12) C45 0.0524(16) 0.0408(13) 0.0494(15) -0.0002(12) 0.0019(12) 0.0016(11) O41 0.0531(13) 0.0749(15) 0.0807(15) 0.0082(12) -0.0151(11) 0.0034(12) C46 0.061(2) 0.076(2) 0.102(3) 0.0171(18) -0.013(2) 0.017(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag N2 Co1 N1 . . 178.93(10) y N2 Co1 N11 . . 90.65(9) y N1 Co1 N11 . . 90.00(9) y N2 Co1 N21 . . 90.08(9) y N1 Co1 N21 . . 89.20(9) y N11 Co1 N21 . . 176.06(9) y N2 Co1 N41 . . 90.07(9) y N1 Co1 N41 . . 90.76(9) y N11 Co1 N41 . . 91.26(8) y N21 Co1 N41 . . 92.61(9) y N2 Co1 N31 . . 88.71(9) y N1 Co1 N31 . . 90.47(9) y N11 Co1 N31 . . 88.32(8) y N21 Co1 N31 . . 87.83(9) y N41 Co1 N31 . . 178.70(9) y C1 N1 Co1 . . 166.1(2) ? N1 C1 Se1 . . 179.7(3) ? C2 N2 Co1 . . 160.3(2) ? N2 C2 Se2 . . 178.8(3) ? C11 N11 C15 . . 116.6(2) ? C11 N11 Co1 . . 120.90(17) ? C15 N11 Co1 . . 122.44(18) ? N11 C11 C12 . . 124.3(2) ? N11 C11 H11 . . 117.9 ? C12 C11 H11 . . 117.9 ? C11 C12 C13 . . 118.4(2) ? C11 C12 H12 . . 120.8 ? C13 C12 H12 . . 120.8 ? O11 C13 C12 . . 124.9(3) ? O11 C13 C14 . . 117.1(2) ? C12 C13 C14 . . 118.0(2) ? C15 C14 C13 . . 119.4(2) ? C15 C14 H14 . . 120.3 ? C13 C14 H14 . . 120.3 ? N11 C15 C14 . . 123.3(3) ? N11 C15 H15 . . 118.4 ? C14 C15 H15 . . 118.4 ? C13 O11 C16 . . 117.5(2) ? O11 C16 H16A . . 109.5 ? O11 C16 H16B . . 109.5 ? H16A C16 H16B . . 109.5 ? O11 C16 H16C . . 109.5 ? H16A C16 H16C . . 109.5 ? H16B C16 H16C . . 109.5 ? C25 N21 C21 . . 116.3(2) ? C25 N21 Co1 . . 121.38(19) ? C21 N21 Co1 . . 120.60(18) ? N21 C21 C22 . . 123.6(3) ? N21 C21 H21 . . 118.2 ? C22 C21 H21 . . 118.2 ? C21 C22 C23 . . 119.0(3) ? C21 C22 H22 . . 120.5 ? C23 C22 H22 . . 120.5 ? O21 C23 C22 . . 116.5(3) ? O21 C23 C24 . . 125.0(3) ? C22 C23 C24 . . 118.6(3) ? C25 C24 C23 . . 117.8(3) ? C25 C24 H24 . . 121.1 ? C23 C24 H24 . . 121.1 ? N21 C25 C24 . . 124.5(3) ? N21 C25 H25 . . 117.8 ? C24 C25 H25 . . 117.8 ? C23 O21 C26 . . 117.6(2) ? O21 C26 H26A . . 109.5 ? O21 C26 H26B . . 109.5 ? H26A C26 H26B . . 109.5 ? O21 C26 H26C . . 109.5 ? H26A C26 H26C . . 109.5 ? H26B C26 H26C . . 109.5 ? C35 N31 C31 . . 115.9(2) ? C35 N31 Co1 . . 120.72(18) ? C31 N31 Co1 . . 122.96(18) ? N31 C31 C32 . . 123.7(3) ? N31 C31 H31 . . 118.2 ? C32 C31 H31 . . 118.2 ? C31 C32 C33 . . 119.3(3) ? C31 C32 H32 . . 120.3 ? C33 C32 H32 . . 120.3 ? O31 C33 C34 . . 125.2(3) ? O31 C33 C32 . . 116.9(3) ? C34 C33 C32 . . 117.9(3) ? C35 C34 C33 . . 118.8(2) ? C35 C34 H34 . . 120.6 ? C33 C34 H34 . . 120.6 ? N31 C35 C34 . . 124.3(3) ? N31 C35 H35 . . 117.8 ? C34 C35 H35 . . 117.8 ? C33 O31 C36 . . 117.6(2) ? O31 C36 H36A . . 109.5 ? O31 C36 H36B . . 109.5 ? H36A C36 H36B . . 109.5 ? O31 C36 H36C . . 109.5 ? H36A C36 H36C . . 109.5 ? H36B C36 H36C . . 109.5 ? C45 N41 C41 . . 116.5(2) ? C45 N41 Co1 . . 122.59(19) ? C41 N41 Co1 . . 120.87(19) ? N41 C41 C42 . . 123.7(3) ? N41 C41 H41 . . 118.1 ? C42 C41 H41 . . 118.1 ? C41 C42 C43 . . 119.0(3) ? C41 C42 H42 . . 120.5 ? C43 C42 H42 . . 120.5 ? O41 C43 C44 . . 125.5(3) ? O41 C43 C42 . . 116.3(3) ? C44 C43 C42 . . 118.2(3) ? C45 C44 C43 . . 118.7(3) ? C45 C44 H44 . . 120.6 ? C43 C44 H44 . . 120.6 ? N41 C45 C44 . . 123.8(3) ? N41 C45 H45 . . 118.1 ? C44 C45 H45 . . 118.1 ? C43 O41 C46 . . 117.6(3) ? O41 C46 H46A . . 109.5 ? O41 C46 H46B . . 109.5 ? H46A C46 H46B . . 109.5 ? O41 C46 H46C . . 109.5 ? H46A C46 H46C . . 109.5 ? H46B C46 H46C . . 109.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Co1 N2 . 2.092(2) y Co1 N1 . 2.108(2) y Co1 N11 . 2.139(2) y Co1 N21 . 2.170(2) y Co1 N41 . 2.174(2) y Co1 N31 . 2.203(2) y N1 C1 . 1.159(4) ? C1 Se1 . 1.778(3) ? N2 C2 . 1.160(3) ? C2 Se2 . 1.775(3) ? N11 C11 . 1.334(3) ? N11 C15 . 1.349(3) ? C11 C12 . 1.373(4) ? C11 H11 . 0.9500 ? C12 C13 . 1.384(4) ? C12 H12 . 0.9500 ? C13 O11 . 1.346(3) ? C13 C14 . 1.393(4) ? C14 C15 . 1.359(4) ? C14 H14 . 0.9500 ? C15 H15 . 0.9500 ? O11 C16 . 1.431(4) ? C16 H16A . 0.9800 ? C16 H16B . 0.9800 ? C16 H16C . 0.9800 ? N21 C25 . 1.337(3) ? N21 C21 . 1.343(3) ? C21 C22 . 1.367(4) ? C21 H21 . 0.9500 ? C22 C23 . 1.384(4) ? C22 H22 . 0.9500 ? C23 O21 . 1.350(3) ? C23 C24 . 1.386(4) ? C24 C25 . 1.377(4) ? C24 H24 . 0.9500 ? C25 H25 . 0.9500 ? O21 C26 . 1.430(4) ? C26 H26A . 0.9800 ? C26 H26B . 0.9800 ? C26 H26C . 0.9800 ? N31 C35 . 1.338(3) ? N31 C31 . 1.342(4) ? C31 C32 . 1.370(4) ? C31 H31 . 0.9500 ? C32 C33 . 1.384(4) ? C32 H32 . 0.9500 ? C33 O31 . 1.347(3) ? C33 C34 . 1.379(4) ? C34 C35 . 1.373(4) ? C34 H34 . 0.9500 ? C35 H35 . 0.9500 ? O31 C36 . 1.431(4) ? C36 H36A . 0.9800 ? C36 H36B . 0.9800 ? C36 H36C . 0.9800 ? N41 C45 . 1.333(3) ? N41 C41 . 1.344(4) ? C41 C42 . 1.366(4) ? C41 H41 . 0.9500 ? C42 C43 . 1.386(4) ? C42 H42 . 0.9500 ? C43 O41 . 1.353(3) ? C43 C44 . 1.380(4) ? C44 C45 . 1.379(4) ? C44 H44 . 0.9500 ? C45 H45 . 0.9500 ? O41 C46 . 1.431(4) ? C46 H46A . 0.9800 ? C46 H46B . 0.9800 ? C46 H46C . 0.9800 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA C11 H11 O11 6_657 0.95 2.49 3.165(3) 127.6 C15 H15 O31 1_455 0.95 2.52 3.297(3) 139.0 C16 H16B Se1 6_557 0.98 3.15 4.096(3) 163.1 C22 H22 Se1 8_755 0.95 3.12 3.817(3) 131.5 C26 H26A Se1 5_666 0.98 3.06 4.029(5) 171.4 C36 H36B Se2 1_655 0.98 3.13 3.952(4) 142.1 C41 H41 O21 4_456 0.95 2.43 3.248(4) 144.4 C45 H45 Se2 8_665 0.95 3.08 3.932(3) 150.5 C46 H46A Se1 1_455 0.98 3.15 3.885(4) 132.9 _cod_database_fobs_code 2022733