#------------------------------------------------------------------------------
#$Date: 2023-04-05 13:23:00 +0200 (Wed, 05 Apr 2023) $
#$Revision: 282408 $
#$URL: svn://www.crystallography.net/cod/cif/2/02/27/2022727.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2022727
loop_
_publ_author_name
'Akiyama, Yukihito'
'Suzuki, Soma'
'Suda, Shintaro'
'Takiguchi, Yuji'
'Nakane, Daisuke'
'Akitsu, Takashiro'
_publ_section_title
;
Crystal structure and Hirshfeld surface analysis of
mono/bis(aqua-\kO)[N-(2-oxidobenzylidene)valinato-\k3
O,N,O′]copper(II): dimeric Schiff base copper(II) complexes having
different numbers of coordinated water molecules
;
_journal_coeditor_code EX2068
_journal_issue 4
_journal_name_full
'Acta Crystallographica Section E Crystallographic Communications'
_journal_page_first 361
_journal_page_last 366
_journal_paper_doi 10.1107/S2056989023002487
_journal_volume 79
_journal_year 2023
_chemical_absolute_configuration syn
_chemical_formula_iupac
'[Cu (C12 H13 N2 O3) (H2 O1)2], [Cu (C12 H13 N2 O3) (H2 O1)]'
_chemical_formula_moiety 'C12 H17 Cu1 N2 O5, C12 H15 Cu1 N2 O4'
_chemical_formula_sum 'C24 H32 Cu2 N4 O9'
_chemical_formula_weight 619.59
_chemical_name_systematic
Bis(aqua-\kO)[N-(2-oxidobenzylidene)valinato-\k^3^O,N,O']copper(II)--(aqua-\kO)[N-(2-oxidobenzylidene)valinato-\k^3^O,N,O']copper(II)
_space_group_crystal_system orthorhombic
_space_group_IT_number 19
_space_group_name_Hall 'P 2ac 2ab'
_space_group_name_H-M_alt 'P 21 21 21'
_atom_sites_solution_hydrogens mixed
_cell_angle_alpha 90
_cell_angle_beta 90
_cell_angle_gamma 90
_cell_formula_units_Z 4
_cell_length_a 5.2966(3)
_cell_length_b 15.8698(10)
_cell_length_c 29.5216(16)
_cell_measurement_reflns_used 9895
_cell_measurement_temperature 173.(2)
_cell_measurement_theta_max 31.0880
_cell_measurement_theta_min 2.4266
_cell_volume 2481.5(2)
_computing_cell_refinement
;
SAINT V8.40B (Bruker, 2019)
;
_computing_data_reduction
;
SAINT V8.40B (Bruker, 2019)
;
_computing_molecular_graphics
;
ShelXle (H\"ubschle et al., 2011)
;
_computing_structure_refinement
;
SHELXL2018/3 (Sheldrick, 2015b)
;
_computing_structure_solution
;
SHELXT2018/2 (Sheldrick, 2015a)
;
_diffrn_ambient_temperature 173.(2)
_diffrn_detector_area_resol_mean 7.3910
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.892
_diffrn_measurement_device_type 'Bruker D8 QUEST'
_diffrn_measurement_method '\f and \w scans'
_diffrn_radiation_type MoK\a
_diffrn_radiation_wavelength 0.71073
_diffrn_reflns_av_R_equivalents 0.0358
_diffrn_reflns_av_unetI/netI 0.0391
_diffrn_reflns_limit_h_max 7
_diffrn_reflns_limit_h_min -7
_diffrn_reflns_limit_k_max 22
_diffrn_reflns_limit_k_min -22
_diffrn_reflns_limit_l_max 40
_diffrn_reflns_limit_l_min -40
_diffrn_reflns_number 31718
_diffrn_reflns_theta_full 25.00
_diffrn_reflns_theta_max 31.36
_diffrn_reflns_theta_min 2.44
_exptl_absorpt_coefficient_mu 1.771
_exptl_absorpt_correction_T_max 0.72
_exptl_absorpt_correction_T_min 0.46
_exptl_absorpt_correction_type multi-scan
_exptl_absorpt_process_details
;
(SADABS; Krause et al., 2015)
;
_exptl_crystal_colour green
_exptl_crystal_density_diffrn 1.658
_exptl_crystal_density_method 'not measured'
_exptl_crystal_description prism
_exptl_crystal_F_000 1280
_exptl_crystal_size_max 0.300
_exptl_crystal_size_mid 0.300
_exptl_crystal_size_min 0.200
_refine_diff_density_max 0.281
_refine_diff_density_min -0.309
_refine_ls_abs_structure_details
;
Flack x determined using 2499 quotients
[(I^+^)-(I^-^)]/[(I^+^)+(I^-^)]
(Parsons et al., 2013)
;
_refine_ls_abs_structure_Flack 0.011(4)
_refine_ls_extinction_method none
_refine_ls_goodness_of_fit_ref 1.038
_refine_ls_hydrogen_treatment mixed
_refine_ls_matrix_type full
_refine_ls_number_parameters 358
_refine_ls_number_reflns 6889
_refine_ls_number_restraints 6
_refine_ls_restrained_S_all 1.082
_refine_ls_R_factor_all 0.0254
_refine_ls_R_factor_gt 0.0235
_refine_ls_shift/su_max 0.005
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0222P)^2^+0.2409P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.0519
_refine_ls_wR_factor_ref 0.0525
_reflns_number_gt 6586
_reflns_number_total 6889
_reflns_threshold_expression 'I > 2\s(I)'
_cod_data_source_file ex2068sup1.cif
_cod_data_source_block I
_cod_database_code 2022727
_shelx_hkl_file
;
1 0 0 1.80 0.80
1 0 0 0.50 0.80
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2 0 0 25.50 4.70
2 0 0 30.70 4.10
-2 0 0 26.90 3.80
-2 0 0 20.50 4.20
2 0 0 23.70 3.70
-3 0 0 0.20 2.30
3 0 0 -0.60 1.70
3 0 0 -1.30 1.70
3 0 0 0.50 2.30
-3 0 0 0.30 1.90
4 0 0 1943.81 89.89
4 0 0 1869.71 86.09
5 0 0 1.10 3.50
5 0 0 1.00 3.80
-5 0 0 -2.40 2.70
5 0 0 3.10 3.30
6 0 0 195.58 17.60
-6 0 0 202.68 16.80
6 0 0 220.78 17.20
1 -1 0 3.70 0.90
-1 -1 0 2.20 1.00
1 1 0 5.60 1.40
-1 1 0 3.40 1.30
1 -1 0 3.00 1.10
-1 1 0 3.40 0.80
1 -1 0 3.50 1.20
2 1 0 1016.60 47.60
3 -1 0 1.20 2.40
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3 -1 0 0.40 1.90
-3 -1 0 2.00 2.20
-3 1 0 1.60 1.90
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3 1 0 0.00 2.00
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-4 1 0 190.98 12.80
4 -1 0 163.08 15.00
4 -1 0 186.78 14.30
-4 -1 0 196.78 13.90
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2 2 0 10.30 2.90
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4 3 0 286.27 21.70
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2 -5 0 18.70 4.40
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2 5 0 19.10 2.60
2 5 0 25.10 5.00
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3 -5 0 233.68 16.20
3 -5 0 225.18 15.40
3 5 0 228.68 16.30
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3 5 0 237.98 12.40
3 -5 0 229.18 10.40
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4 5 0 49.40 5.60
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4 -5 0 64.29 9.80
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6 5 0 30.90 6.50
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7 5 0 1.10 3.70
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0 -6 0 245.18 12.80
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5 6 0 149.19 17.50
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5 6 0 148.59 10.80
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5 -6 0 138.59 14.30
5 6 0 145.29 11.40
6 6 0 163.18 13.20
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6 6 0 169.98 12.90
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2 7 0 8978.60 458.05
3 7 0 2131.39 97.99
3 -7 0 2160.68 97.59
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4 7 0 631.04 39.70
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4 7 0 600.64 36.80
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4 -7 0 656.43 37.00
4 -7 0 668.53 35.50
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5 7 0 21.70 4.80
-5 7 0 16.90 7.60
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6 7 0 311.87 19.00
6 7 0 291.87 18.20
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2 -8 0 19.70 4.60
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2 -8 0 5.00 3.30
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3 8 0 66.39 5.30
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2 9 0 50.79 4.70
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3 9 0 137.09 8.50
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1 -10 0 174.88 13.30
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-2 10 0 185.08 15.50
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3 -10 0 1175.38 59.39
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3 -10 0 1164.48 56.59
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4 10 0 575.84 26.60
4 -10 0 570.04 36.10
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0 11 0 10.30 3.60
0 -11 0 9.50 3.40
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2 -11 0 1283.97 60.49
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3 11 0 118.49 7.60
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3 11 0 111.69 15.10
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3 -11 0 121.49 11.70
3 -11 0 119.79 17.80
-4 -11 0 13.80 6.30
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4 -11 0 11.30 5.10
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0 -12 0 762.22 37.70
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-1 -12 0 82.59 8.00
1 -12 0 81.09 9.10
1 -12 0 84.19 7.30
1 -12 0 84.69 10.80
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-1 12 0 81.79 7.60
1 12 0 80.89 9.40
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1 12 0 75.89 10.70
-2 12 0 247.88 20.80
-2 -12 0 234.58 14.80
2 -12 0 269.77 17.50
2 12 0 258.27 18.30
2 12 0 235.28 18.80
2 -12 0 225.08 18.00
-2 -12 0 231.48 18.10
2 12 0 247.18 14.30
-2 12 0 236.38 11.90
-2 12 0 276.27 19.70
-3 -12 0 10.90 6.20
3 12 0 16.00 3.10
-3 12 0 17.70 7.70
3 12 0 5.70 5.70
3 -12 0 20.90 7.10
3 -12 0 11.80 4.90
-4 12 0 9.10 6.90
-4 -12 0 5.90 5.60
4 -12 0 8.10 5.00
-5 12 0 7.80 9.70
0 -13 0 7.50 4.00
0 13 0 4.90 3.60
0 13 0 10.00 4.30
0 -13 0 9.60 4.10
0 13 0 4.60 4.30
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1 13 0 1008.40 50.79
1 -13 0 996.60 49.99
-1 13 0 1046.20 52.79
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0 -5 -35 13.50 4.60
0 5 -35 17.20 3.60
0 5 35 12.00 5.80
0 -5 -35 3.50 6.20
1 5 -35 10.90 4.30
-1 -5 -35 0.20 4.40
-1 5 35 2.40 5.20
1 5 35 3.00 3.20
1 -5 -35 -4.20 4.10
1 -5 -35 2.80 3.90
-2 -5 -35 26.60 8.10
2 5 -35 35.40 8.70
-3 -5 -35 37.60 9.30
0 6 35 128.69 14.70
0 6 -35 107.49 8.20
0 -6 -35 112.99 11.40
0 -6 -35 113.49 18.30
-1 -6 -35 210.48 19.40
1 6 -35 223.18 16.90
-1 6 35 225.08 21.20
1 -6 -35 177.68 19.00
1 6 35 184.48 16.30
-2 -6 -35 96.69 15.10
-2 6 35 122.49 19.40
2 6 35 127.49 11.80
-3 -6 -35 21.60 6.30
0 7 35 443.26 30.60
0 -7 -35 403.76 33.70
0 7 -35 412.26 21.70
0 -7 -35 454.35 26.90
-1 7 35 178.48 19.90
1 7 -35 183.78 15.70
-1 -7 -35 187.38 18.20
1 7 35 205.58 18.80
-2 7 35 146.09 21.60
-2 -7 -35 146.29 15.60
2 7 35 166.88 15.50
0 8 35 7.80 6.20
0 -8 -35 14.10 5.10
-1 8 35 52.29 12.80
1 8 -35 57.89 12.00
-1 -8 -35 54.79 11.40
1 -8 -35 48.60 11.50
1 8 35 50.19 10.10
-2 -8 -35 37.90 8.90
-2 8 35 37.70 14.00
2 8 35 47.80 11.80
0 9 35 103.29 16.60
-1 9 35 12.50 7.80
-1 -9 -35 13.50 6.00
1 -9 -35 5.50 5.90
1 9 35 4.90 5.30
-2 -9 -35 48.90 9.30
0 10 35 13.50 8.00
0 -10 -35 9.70 6.50
-1 -10 -35 53.09 10.30
-1 10 35 46.30 11.60
1 10 35 45.30 10.50
0 11 35 39.60 10.40
0 -11 -35 50.29 10.60
-1 -11 -35 93.69 13.40
1 11 35 105.59 15.70
0 -12 -35 2.00 3.50
1 12 35 44.80 11.10
0 -13 -35 170.18 16.60
0 0 -36 514.55 37.10
0 0 -36 621.94 29.80
-1 0 -36 3.00 5.80
1 0 -36 4.80 3.20
-2 0 -36 43.60 11.50
-3 0 -36 4.50 4.70
-4 0 -36 155.28 21.70
0 -1 -36 1.70 4.90
0 1 -36 4.40 2.90
0 1 -36 7.10 7.10
-1 -1 -36 1.40 4.80
1 1 -36 5.70 3.40
1 -1 -36 2.70 6.40
1 -1 -36 6.40 3.50
-1 1 -36 4.20 5.90
-2 -1 -36 282.57 29.50
-2 1 -36 329.87 28.00
-3 -1 -36 25.30 8.70
-3 1 -36 28.60 9.70
-4 -1 -36 33.20 10.20
0 -2 -36 78.19 14.30
0 2 -36 92.49 15.50
0 2 -36 85.39 7.50
0 -2 -36 96.19 9.00
-1 -2 -36 12.10 11.20
1 2 -36 25.00 5.60
-1 2 36 15.90 7.00
1 -2 -36 17.10 5.10
-1 2 -36 29.80 10.50
1 -2 -36 19.80 7.90
-2 -2 -36 50.79 11.90
-2 2 36 80.49 14.60
-2 2 -36 44.90 12.80
-3 2 36 33.40 17.00
-3 -2 -36 15.50 6.70
0 3 -36 14.50 3.30
0 -3 -36 11.70 4.10
0 -3 -36 13.60 7.30
0 3 36 10.50 5.20
-1 -3 -36 109.99 19.90
1 3 -36 130.59 11.60
-1 3 36 132.69 15.40
1 -3 -36 81.29 13.10
1 -3 -36 92.29 15.70
-1 3 -36 97.49 17.00
2 3 -36 632.64 40.90
-2 3 36 558.24 39.30
-2 -3 -36 560.74 38.70
-3 -3 -36 11.40 5.70
0 -4 -36 610.44 31.20
0 -4 -36 596.34 37.80
0 4 -36 480.55 26.30
0 4 36 615.64 35.30
1 4 -36 111.89 10.90
-1 4 36 105.29 16.20
-1 -4 -36 118.59 17.20
1 4 36 96.39 9.80
1 -4 -36 93.39 15.60
1 -4 -36 101.49 11.30
-2 4 36 92.39 24.20
-2 -4 -36 53.59 11.80
-3 -4 -36 59.79 12.50
0 -5 -36 36.70 6.90
0 -5 -36 31.50 9.80
0 5 36 27.70 7.80
-1 5 36 14.90 7.30
1 5 -36 17.40 5.10
-1 -5 -36 8.90 5.80
1 -5 -36 8.00 6.50
1 -5 -36 5.10 4.40
1 5 36 13.50 4.80
-2 -5 -36 113.79 16.60
-2 5 36 118.59 18.60
-3 -5 -36 30.10 8.20
0 -6 -36 276.87 23.80
0 6 36 260.97 22.10
0 -6 -36 296.77 19.90
1 6 -36 14.40 4.80
-1 6 36 14.80 7.50
-1 -6 -36 16.80 6.90
1 -6 -36 12.00 8.90
1 6 36 14.10 5.40
-2 -6 -36 26.00 8.00
-2 6 36 21.40 9.20
0 -7 -36 13.90 5.00
0 7 36 14.30 6.60
0 -7 -36 13.60 6.30
-1 -7 -36 50.59 10.90
-1 7 36 68.59 13.60
1 7 36 79.59 12.00
-2 7 36 352.86 30.90
-2 -7 -36 363.56 26.90
0 -8 -36 70.19 12.90
0 -8 -36 79.19 13.30
0 8 36 79.39 14.00
-1 -8 -36 60.29 11.80
-1 8 36 58.09 13.20
1 8 36 71.39 12.10
-2 -8 -36 72.59 12.10
0 9 36 3.10 4.80
0 -9 -36 -3.00 3.40
-1 -9 -36 74.59 12.80
-1 9 36 68.89 14.50
1 9 36 95.59 14.40
0 10 36 226.68 22.40
0 -10 -36 206.18 19.50
-1 -10 -36 138.59 15.40
-1 10 36 162.08 35.60
1 10 36 220.58 19.90
0 11 36 66.29 13.50
0 -11 -36 64.79 11.60
-1 -11 -36 90.19 17.40
0 -12 -36 31.00 8.00
1 12 36 9.30 5.10
0 0 -37 5.50 2.80
0 0 -37 10.80 6.70
-1 0 -37 78.99 15.20
1 0 -37 57.69 8.90
-2 0 -37 458.05 34.80
-3 0 -37 39.40 11.30
0 -1 -37 174.58 19.60
0 1 -37 198.88 12.50
-1 -1 -37 105.49 17.00
1 1 -37 124.29 11.20
1 -1 -37 95.89 10.40
-1 1 -37 101.79 17.20
-2 -1 -37 65.39 14.30
-2 1 -37 81.29 15.90
-3 -1 -37 33.50 10.60
0 -2 -37 186.08 19.00
0 2 -37 123.59 9.30
-1 2 37 44.00 10.10
-1 -2 -37 56.99 12.50
1 2 -37 52.29 8.20
1 -2 -37 57.89 11.00
-2 2 37 24.00 9.00
-2 -2 -37 16.60 7.50
-3 -2 -37 10.70 6.10
0 -3 -37 326.17 27.00
0 3 37 340.67 23.30
0 -3 -37 335.67 20.50
1 3 -37 98.19 10.20
-1 3 37 90.69 14.70
-1 -3 -37 116.19 18.20
1 -3 -37 106.59 11.20
-2 3 37 30.70 11.40
-3 -3 -37 12.00 6.20
0 -4 -37 13.50 4.40
0 -4 -37 8.80 6.20
1 4 -37 133.39 12.60
-1 4 37 104.29 16.00
-1 -4 -37 131.39 18.80
1 -4 -37 149.99 13.60
1 4 37 151.38 11.90
-2 4 37 238.18 23.40
-2 -4 -37 214.98 21.20
-3 -4 -37 31.40 9.00
0 -5 -37 1.10 3.00
0 -5 -37 3.50 5.20
0 5 37 4.90 4.60
-1 -5 -37 22.70 12.40
-1 5 37 30.70 9.20
1 5 37 28.00 6.30
-2 -5 -37 210.98 20.90
-2 5 37 249.78 24.20
-3 -5 -37 13.70 8.40
0 6 37 36.90 9.20
0 -6 -37 39.70 11.50
0 -6 -37 26.90 9.00
-1 6 37 -0.70 3.50
1 6 37 1.80 3.10
-2 6 37 50.39 12.70
-2 -6 -37 55.79 11.30
0 -7 -37 425.56 30.90
0 7 37 434.26 30.70
-1 -7 -37 105.49 16.50
-1 7 37 91.69 16.50
1 7 37 143.49 14.10
-2 -7 -37 -0.40 2.80
0 8 37 11.40 6.30
0 -8 -37 7.90 5.40
-1 8 37 173.08 20.00
-1 -8 -37 172.98 17.80
1 8 37 182.58 17.20
-2 -8 -37 48.50 11.80
0 9 37 30.50 9.70
0 -9 -37 30.60 9.10
-1 -9 -37 27.30 7.70
-1 9 37 18.20 8.00
1 9 37 35.40 9.10
0 10 37 2.40 3.70
0 -10 -37 9.50 5.70
-1 -10 -37 205.08 18.70
0 -11 -37 115.99 15.70
0 11 37 101.69 17.00
1 0 -38 625.84 34.20
-2 0 -38 86.19 19.00
-1 -1 -38 82.09 15.30
1 1 -38 104.19 12.40
1 -1 -38 82.39 9.60
-2 -1 -38 44.60 11.70
-3 -1 -38 174.88 23.30
-1 -2 -38 84.79 15.90
1 -2 -38 98.99 11.10
-2 2 38 243.48 27.50
-3 -2 -38 35.20 10.60
0 3 38 228.38 18.30
-1 -3 -38 119.99 18.60
-1 3 38 125.09 15.40
1 -3 -38 148.69 13.30
-2 3 38 59.69 13.40
-2 -3 -38 57.19 12.60
-3 -3 -38 130.89 18.70
0 4 38 2.10 6.40
0 -4 -38 5.90 6.00
-1 -4 -38 228.28 22.60
-1 4 38 266.07 22.80
1 -4 -38 259.57 19.40
-2 -4 -38 1.00 3.80
-2 4 38 3.40 5.30
-3 -4 -38 74.89 13.80
0 -5 -38 117.19 17.60
0 5 38 122.99 14.00
-1 5 38 123.49 17.40
-1 -5 -38 111.99 17.10
-2 5 38 2.70 5.20
-2 -5 -38 5.00 5.00
0 -6 -38 130.49 18.90
0 6 38 132.19 15.10
-1 -6 -38 18.40 7.60
-1 6 38 37.30 10.20
-2 6 38 261.87 41.80
-2 -6 -38 203.38 20.10
0 -7 -38 85.79 14.90
0 7 38 72.49 12.50
-1 -7 -38 128.89 17.50
-1 7 38 122.79 19.20
-2 -7 -38 58.19 11.50
0 -8 -38 152.68 23.10
0 8 38 227.38 20.90
-1 8 38 97.19 16.50
-1 -8 -38 93.89 15.30
0 9 38 159.08 23.30
-1 -9 -38 8.20 5.10
-1 9 38 6.10 6.60
0 10 38 14.40 6.60
-2 -2 -39 20.50 8.20
-3 -2 -39 192.68 21.00
-1 -3 -39 36.10 11.40
-1 3 39 54.09 11.30
-2 -3 -39 47.50 11.80
-2 3 39 49.50 12.10
-3 -3 -39 4.50 4.20
0 4 39 39.30 8.90
-1 -4 -39 66.49 13.60
-1 4 39 69.99 13.10
-2 4 39 38.80 11.30
-2 -4 -39 41.70 10.70
0 5 39 215.28 18.80
-1 -5 -39 229.78 22.40
-1 5 39 232.68 22.10
-2 -5 -39 56.09 11.70
-2 5 39 62.59 14.40
0 6 39 20.20 7.20
-1 -6 -39 163.38 18.50
-1 6 39 188.18 20.00
-2 -6 -39 25.70 8.70
0 7 39 1.10 3.80
-1 -7 -39 15.90 7.00
-1 7 39 17.80 8.10
0 8 39 2.60 4.10
-1 -8 -39 66.89 12.50
-1 8 39 71.99 14.90
-1 -9 -39 119.99 16.90
-1 3 40 30.90 8.80
-2 3 40 14.30 7.90
-1 4 40 170.48 18.20
-2 -4 -40 62.59 13.00
-2 4 40 85.89 16.10
-1 5 40 78.49 14.20
-2 -5 -40 62.49 12.80
-1 6 40 56.99 12.80
-1 7 40 9.90 6.30
-1 -7 -40 3.00 4.60
-1 8 40 49.80 13.70
-1 -8 -40 63.19 12.80
0 0 0 0.00 0.00
_computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)'
;
_shelx_hkl_checksum 40259
_shelx_res_file
;
TITL akiyama_val_2_0m_a.res in P2(1)2(1)2(1)
akiyama_val_2_0m_a.res
created by SHELXL-2018/3 at 16:37:17 on 09-Nov-2022
CELL 0.71073 5.2966 15.8698 29.5216 90.000 90.000 90.000
ZERR 4.000 0.0003 0.0010 0.0016 0.000 0.000 0.000
LATT -1
SYMM 1/2-X, -Y, 1/2+Z
SYMM -X, 1/2+Y, 1/2-Z
SYMM 1/2+X, 1/2-Y, -Z
SFAC C H Cu N O
UNIT 96 128 8 8 36
LIST 4 ! automatically inserted. Change 6 to 4 for CHECKCIF!!
L.S. 10
ACTA 50
BOND
DFIX 0.84 O9 H11 O9 H12
DANG 1.33 H11 H12
FMAP 2
HTAB
BUMP
PLAN 20
TEMP -100
EQIV $1 x-1/2, -y+3/2, -z+1
HTAB O2 O9_$1
HTAB O2 O8
EQIV $2 x+3/2, -y+3/2, -z+1
HTAB O6 O3_$2
EQIV $3 x+1/2, -y+3/2, -z+1
HTAB O6 O7_$3
EQIV $4 x-1, y, z
HTAB O9 O5_$4
HTAB O9 O4_$2
WGHT 0.022200 0.240900
FVAR 0.46268
CU1 3 0.112619 0.884253 0.638669 11.00000 0.01555 0.01609 =
0.01265 -0.00101 -0.00113 0.00322
O1 5 0.359493 0.833467 0.676293 11.00000 0.02005 0.02223 =
0.01533 0.00070 -0.00005 0.00474
N1 4 -0.050226 0.943015 0.687461 11.00000 0.01435 0.01377 =
0.01490 -0.00101 -0.00245 0.00186
C1 1 0.360652 0.833471 0.720302 11.00000 0.01513 0.01383 =
0.01940 0.00050 -0.00236 -0.00216
O2 5 0.219635 0.824543 0.584890 11.00000 0.02591 0.01697 =
0.01595 0.00133 0.00244 0.00695
AFIX 148
H2A 2 0.243910 0.858648 0.564114 11.00000 -1.50000
AFIX 0
H2B 2 0.301523 0.788170 0.582794 11.00000 0.03715
CU2 3 1.101297 0.590800 0.526182 11.00000 0.01489 0.01297 =
0.01415 0.00287 0.00415 0.00229
N2 4 0.948786 0.527291 0.574497 11.00000 0.01416 0.01404 =
0.01451 0.00102 0.00198 0.00302
C2 1 0.553079 0.788890 0.743383 11.00000 0.01782 0.01948 =
0.02474 0.00218 -0.00105 0.00159
AFIX 43
H2 2 0.678688 0.760457 0.726235 11.00000 -1.20000
AFIX 0
O3 5 -0.179232 0.925075 0.604064 11.00000 0.01997 0.02378 =
0.01612 -0.00537 -0.00359 0.00589
C3 1 0.563566 0.785526 0.789732 11.00000 0.02351 0.02208 =
0.02574 0.00502 -0.00779 0.00132
AFIX 43
H3 2 0.696009 0.754944 0.803896 11.00000 -1.20000
AFIX 0
C4 1 0.385141 0.825773 0.816374 11.00000 0.03282 0.02705 =
0.01680 0.00248 -0.00614 0.00028
AFIX 43
H4 2 0.393972 0.823083 0.848482 11.00000 -1.20000
AFIX 0
O4 5 -0.542328 0.994727 0.611286 11.00000 0.02163 0.03181 =
0.02457 -0.00864 -0.00959 0.00928
O5 5 1.352415 0.504270 0.514396 11.00000 0.01763 0.01470 =
0.02165 0.00395 0.00510 0.00105
C5 1 0.195627 0.869552 0.795288 11.00000 0.02982 0.02165 =
0.01724 -0.00102 -0.00144 0.00370
AFIX 43
H5 2 0.070134 0.896356 0.813204 11.00000 -1.20000
AFIX 0
C6 1 0.181927 0.875869 0.747775 11.00000 0.02002 0.01644 =
0.01553 -0.00003 -0.00339 -0.00041
O6 5 1.245090 0.658296 0.477795 11.00000 0.03307 0.01282 =
0.01810 0.00037 0.00848 -0.00452
AFIX 148
H6 2 1.254836 0.633329 0.457681 11.00000 -1.50000
AFIX 0
H10 2 1.267714 0.705793 0.475703 11.00000 0.02051
C7 1 -0.018621 0.926200 0.729642 11.00000 0.01943 0.01378 =
0.01745 -0.00220 0.00045 0.00149
AFIX 43
H7 2 -0.137447 0.948897 0.750431 11.00000 -1.20000
AFIX 0
O7 5 0.833113 0.674030 0.542077 11.00000 0.02067 0.01441 =
0.01575 0.00312 0.00341 0.00359
O8 5 0.459215 0.679024 0.577003 11.00000 0.02266 0.02155 =
0.02560 0.00322 0.00660 0.00931
C8 1 -0.264895 0.995140 0.673888 11.00000 0.01387 0.01515 =
0.01522 -0.00127 -0.00075 0.00267
AFIX 13
H8 2 -0.409690 0.983539 0.694712 11.00000 -1.20000
AFIX 0
C9 1 -0.206563 1.091071 0.674672 11.00000 0.01861 0.01356 =
0.02030 -0.00012 -0.00105 0.00178
AFIX 13
H9 2 -0.369691 1.120986 0.668994 11.00000 -1.20000
AFIX 0
O9 5 0.796157 0.546668 0.472659 11.00000 0.01780 0.02575 =
0.01629 0.00107 0.00386 -0.00398
H11 2 0.638816 0.529814 0.484470 11.00000 0.03646
C10 1 -0.112716 1.119702 0.720844 11.00000 0.02972 0.01915 =
0.02825 -0.00543 -0.00396 -0.00094
AFIX 137
H10A 2 0.052137 1.094098 0.726988 11.00000 -1.50000
H10B 2 -0.233321 1.102247 0.744205 11.00000 -1.50000
H10C 2 -0.096470 1.181214 0.721102 11.00000 -1.50000
AFIX 0
C11 1 -0.026411 1.117911 0.637721 11.00000 0.03849 0.02161 =
0.03054 0.00277 0.00702 -0.00262
AFIX 137
H11A 2 -0.095199 1.101598 0.608178 11.00000 -1.50000
H11B 2 0.137196 1.090352 0.642289 11.00000 -1.50000
H11C 2 -0.004356 1.179195 0.638722 11.00000 -1.50000
AFIX 0
C12 1 -0.338722 0.969515 0.626165 11.00000 0.01769 0.01580 =
0.01966 -0.00278 -0.00188 0.00057
H12 2 0.887970 0.521866 0.445785 11.00000 0.08264
C13 1 1.359697 0.428031 0.531822 11.00000 0.01434 0.01464 =
0.01669 -0.00186 -0.00187 0.00046
C14 1 1.549013 0.371000 0.517757 11.00000 0.01822 0.01819 =
0.02889 -0.00140 0.00491 0.00147
AFIX 43
H14 2 1.667897 0.388197 0.495506 11.00000 -1.20000
AFIX 0
C15 1 1.564797 0.290949 0.535645 11.00000 0.01937 0.01845 =
0.02977 -0.00410 0.00013 0.00561
AFIX 43
H15 2 1.694644 0.254278 0.525437 11.00000 -1.20000
AFIX 0
C16 1 1.396089 0.262553 0.568150 11.00000 0.03089 0.01433 =
0.02492 0.00036 -0.00346 0.00443
AFIX 43
H16 2 1.409610 0.207391 0.580411 11.00000 -1.20000
AFIX 0
C17 1 1.209682 0.316266 0.582044 11.00000 0.02702 0.01669 =
0.02031 0.00306 0.00407 0.00259
AFIX 43
H17 2 1.090484 0.297210 0.603799 11.00000 -1.20000
AFIX 0
C18 1 1.188793 0.399029 0.565106 11.00000 0.01780 0.01392 =
0.01463 0.00079 -0.00012 0.00204
C19 1 0.989969 0.449737 0.583564 11.00000 0.02014 0.01678 =
0.01385 0.00301 0.00375 -0.00033
AFIX 43
H19 2 0.878687 0.423325 0.604428 11.00000 -1.20000
AFIX 0
C20 1 0.734961 0.568260 0.596880 11.00000 0.01443 0.01568 =
0.01500 0.00074 0.00400 0.00244
AFIX 13
H20 2 0.587525 0.528907 0.596481 11.00000 -1.20000
AFIX 0
C21 1 0.797491 0.590834 0.646871 11.00000 0.01966 0.02118 =
0.01492 0.00096 0.00248 0.00535
AFIX 13
H21 2 0.913474 0.546104 0.658543 11.00000 -1.20000
AFIX 0
C22 1 0.564323 0.589423 0.676220 11.00000 0.02911 0.03827 =
0.01923 -0.00057 0.00939 -0.00184
AFIX 137
H22A 2 0.446763 0.633181 0.666033 11.00000 -1.50000
H22B 2 0.611852 0.600033 0.707791 11.00000 -1.50000
H22C 2 0.482905 0.534139 0.673900 11.00000 -1.50000
AFIX 0
C23 1 0.936614 0.674461 0.650908 11.00000 0.02474 0.02997 =
0.01978 -0.00285 -0.00025 -0.00326
AFIX 137
H23A 2 1.075345 0.676035 0.628960 11.00000 -1.50000
H23B 2 1.004679 0.680335 0.681614 11.00000 -1.50000
H23C 2 0.819359 0.720835 0.644748 11.00000 -1.50000
AFIX 0
C24 1 0.667741 0.646706 0.569660 11.00000 0.01607 0.01508 =
0.01374 -0.00176 -0.00063 0.00181
HKLF 4
REM akiyama_val_2_0m_a.res in P2(1)2(1)2(1)
REM wR2 = 0.052496, GooF = S = 1.03811, Restrained GooF = 1.08173 for all data
REM R1 = 0.023533 for 6586 Fo > 4sig(Fo) and 0.025407 for all 6889 data
REM 358 parameters refined using 6 restraints
END
WGHT 0.0222 0.2409
REM Instructions for potential hydrogen bonds
HTAB O2 O9_$1
HTAB O2 O8
HTAB O6 O3_$2
HTAB O6 O7_$3
HTAB O9 O5_$4
HTAB O9 O4_$2
REM Highest difference peak 0.281, deepest hole -0.309, 1-sigma level 0.057
Q1 1 0.0995 0.9002 0.7391 11.00000 0.05 0.28
Q2 1 1.1869 0.3567 0.5659 11.00000 0.05 0.28
Q3 1 -0.1198 1.0994 0.6590 11.00000 0.05 0.27
Q4 1 -0.2803 0.9770 0.6486 11.00000 0.05 0.27
Q5 1 0.7024 0.6051 0.5852 11.00000 0.05 0.26
Q6 1 0.8055 0.5839 0.4733 11.00000 0.05 0.25
Q7 1 -0.1808 0.9621 0.6839 11.00000 0.05 0.25
Q8 1 0.4318 0.7989 0.8006 11.00000 0.05 0.25
Q9 1 0.5491 0.7928 0.7671 11.00000 0.05 0.24
Q10 1 -0.2095 1.0531 0.6742 11.00000 0.05 0.24
Q11 1 0.8397 0.6554 0.5247 11.00000 0.05 0.24
Q12 1 1.1202 0.4203 0.5792 11.00000 0.05 0.24
Q13 1 -0.0445 0.9384 0.6073 11.00000 0.05 0.23
Q14 1 0.6049 0.7825 0.7358 11.00000 0.05 0.23
Q15 1 0.3310 0.8543 0.8086 11.00000 0.05 0.23
Q16 1 0.9685 0.6593 0.5552 11.00000 0.05 0.22
Q17 1 0.8081 0.5217 0.4499 11.00000 0.05 0.22
Q18 1 -0.6042 1.0593 0.5855 11.00000 0.05 0.21
Q19 1 1.3448 0.4581 0.5231 11.00000 0.05 0.21
Q20 1 -0.5077 1.0224 0.5947 11.00000 0.05 0.21
;
_shelx_res_checksum 25057
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-x, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Cu Cu1 0.11262(5) 0.88425(2) 0.63867(2) 0.01477(6) Uani d 1 . .
O O1 0.3595(3) 0.83347(9) 0.67629(5) 0.0192(3) Uani d 1 . .
N N1 -0.0502(3) 0.94302(10) 0.68746(6) 0.0143(3) Uani d 1 . .
C C1 0.3607(4) 0.83347(12) 0.72030(7) 0.0161(4) Uani d 1 . .
O O2 0.2196(3) 0.82454(11) 0.58489(5) 0.0196(3) Uani d 1 . .
H H2A 0.244(5) 0.8586(12) 0.5641(8) 0.029 Uiso calc 1 . .
H H2B 0.302(7) 0.788(2) 0.5828(10) 0.037(9) Uiso d 1 . .
Cu Cu2 1.10130(5) 0.59080(2) 0.52618(2) 0.01400(6) Uani d 1 . .
N N2 0.9488(3) 0.52729(10) 0.57450(6) 0.0142(3) Uani d 1 . .
C C2 0.5531(4) 0.78889(14) 0.74338(8) 0.0207(4) Uani d 1 . .
H H2 0.678688 0.760457 0.726235 0.025 Uiso calc 1 . .
O O3 -0.1792(3) 0.92508(10) 0.60406(5) 0.0200(3) Uani d 1 . .
C C3 0.5636(4) 0.78553(14) 0.78973(8) 0.0238(5) Uani d 1 . .
H H3 0.696009 0.754944 0.803896 0.029 Uiso calc 1 . .
C C4 0.3851(5) 0.82577(14) 0.81637(7) 0.0256(5) Uani d 1 . .
H H4 0.393972 0.823083 0.848482 0.031 Uiso calc 1 . .
O O4 -0.5423(3) 0.99473(11) 0.61129(5) 0.0260(4) Uani d 1 . .
O O5 1.3524(3) 0.50427(9) 0.51440(5) 0.0180(3) Uani d 1 . .
C C5 0.1956(5) 0.86955(14) 0.79529(7) 0.0229(5) Uani d 1 . .
H H5 0.070134 0.896356 0.813204 0.027 Uiso calc 1 . .
C C6 0.1819(4) 0.87587(13) 0.74778(7) 0.0173(4) Uani d 1 . .
O O6 1.2451(3) 0.65830(10) 0.47779(5) 0.0213(3) Uani d 1 . .
H H6 1.255(6) 0.6333(13) 0.4577(9) 0.032 Uiso calc 1 . .
H H10 1.268(5) 0.7058(17) 0.4757(9) 0.021(7) Uiso d 1 . .
C C7 -0.0186(4) 0.92620(12) 0.72964(7) 0.0169(4) Uani d 1 . .
H H7 -0.137447 0.948897 0.750431 0.02 Uiso calc 1 . .
O O7 0.8331(3) 0.67403(9) 0.54208(5) 0.0169(3) Uani d 1 . .
O O8 0.4592(3) 0.67902(10) 0.57700(5) 0.0233(4) Uani d 1 . .
C C8 -0.2649(4) 0.99514(13) 0.67389(7) 0.0147(4) Uani d 1 . .
H H8 -0.40969 0.983539 0.694712 0.018 Uiso calc 1 . .
C C9 -0.2066(4) 1.09107(13) 0.67467(7) 0.0175(4) Uani d 1 . .
H H9 -0.369691 1.120986 0.668994 0.021 Uiso calc 1 . .
O O9 0.7962(3) 0.54667(10) 0.47266(5) 0.0199(3) Uani d 1 . .
H H11 0.639(4) 0.5298(17) 0.4845(9) 0.036(8) Uiso d 1 . .
C C10 -0.1127(5) 1.11970(13) 0.72084(7) 0.0257(5) Uani d 1 . .
H H10A 0.052137 1.094098 0.726988 0.039 Uiso calc 1 . .
H H10B -0.233321 1.102247 0.744205 0.039 Uiso calc 1 . .
H H10C -0.09647 1.181214 0.721102 0.039 Uiso calc 1 . .
C C11 -0.0264(5) 1.11791(15) 0.63772(8) 0.0302(5) Uani d 1 . .
H H11A -0.095199 1.101598 0.608178 0.045 Uiso calc 1 . .
H H11B 0.137196 1.090352 0.642289 0.045 Uiso calc 1 . .
H H11C -0.004356 1.179195 0.638722 0.045 Uiso calc 1 . .
C C12 -0.3387(4) 0.96951(13) 0.62616(7) 0.0177(4) Uani d 1 . .
H H12 0.888(6) 0.5219(18) 0.4458(9) 0.083(13) Uiso d 1 . .
C C13 1.3597(4) 0.42803(12) 0.53182(7) 0.0152(4) Uani d 1 . .
C C14 1.5490(4) 0.37100(13) 0.51776(8) 0.0218(5) Uani d 1 . .
H H14 1.667897 0.388197 0.495506 0.026 Uiso calc 1 . .
C C15 1.5648(4) 0.29095(14) 0.53564(8) 0.0225(5) Uani d 1 . .
H H15 1.694644 0.254278 0.525437 0.027 Uiso calc 1 . .
C C16 1.3961(5) 0.26255(13) 0.56815(7) 0.0234(4) Uani d 1 . .
H H16 1.40961 0.207391 0.580411 0.028 Uiso calc 1 . .
C C17 1.2097(5) 0.31627(13) 0.58204(7) 0.0213(5) Uani d 1 . .
H H17 1.090484 0.29721 0.603799 0.026 Uiso calc 1 . .
C C18 1.1888(4) 0.39903(12) 0.56511(7) 0.0154(4) Uani d 1 . .
C C19 0.9900(4) 0.44974(13) 0.58356(7) 0.0169(4) Uani d 1 . .
H H19 0.878687 0.423325 0.604428 0.02 Uiso calc 1 . .
C C20 0.7350(4) 0.56826(13) 0.59688(7) 0.0150(4) Uani d 1 . .
H H20 0.587525 0.528907 0.596481 0.018 Uiso calc 1 . .
C C21 0.7975(4) 0.59083(14) 0.64687(7) 0.0186(4) Uani d 1 . .
H H21 0.913474 0.546104 0.658543 0.022 Uiso calc 1 . .
C C22 0.5643(5) 0.58942(17) 0.67622(8) 0.0289(5) Uani d 1 . .
H H22A 0.446763 0.633181 0.666033 0.043 Uiso calc 1 . .
H H22B 0.611852 0.600033 0.707791 0.043 Uiso calc 1 . .
H H22C 0.482905 0.534139 0.6739 0.043 Uiso calc 1 . .
C C23 0.9366(5) 0.67446(15) 0.65091(8) 0.0248(5) Uani d 1 . .
H H23A 1.075345 0.676035 0.62896 0.037 Uiso calc 1 . .
H H23B 1.004679 0.680335 0.681614 0.037 Uiso calc 1 . .
H H23C 0.819359 0.720835 0.644748 0.037 Uiso calc 1 . .
C C24 0.6677(4) 0.64671(13) 0.56966(7) 0.0150(4) Uani d 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Cu1 0.01555(12) 0.01609(11) 0.01265(11) 0.00322(11) -0.00113(10) -0.00101(8)
O1 0.0201(8) 0.0222(7) 0.0153(7) 0.0047(7) -0.0001(6) 0.0007(5)
N1 0.0144(8) 0.0138(8) 0.0149(8) 0.0019(7) -0.0025(6) -0.0010(6)
C1 0.0151(10) 0.0138(9) 0.0194(9) -0.0022(8) -0.0024(8) 0.0005(7)
O2 0.0259(8) 0.0170(7) 0.0160(7) 0.0069(7) 0.0024(6) 0.0013(6)
Cu2 0.01489(11) 0.01297(11) 0.01415(11) 0.00229(10) 0.00415(10) 0.00287(8)
N2 0.0142(8) 0.0140(8) 0.0145(8) 0.0030(7) 0.0020(6) 0.0010(6)
C2 0.0178(11) 0.0195(10) 0.0247(11) 0.0016(9) -0.0010(8) 0.0022(8)
O3 0.0200(7) 0.0238(8) 0.0161(7) 0.0059(6) -0.0036(6) -0.0054(6)
C3 0.0235(12) 0.0221(10) 0.0257(11) 0.0013(10) -0.0078(9) 0.0050(8)
C4 0.0328(12) 0.0271(11) 0.0168(10) 0.0003(12) -0.0061(10) 0.0025(8)
O4 0.0216(8) 0.0318(9) 0.0246(8) 0.0093(7) -0.0096(6) -0.0086(7)
O5 0.0176(8) 0.0147(6) 0.0217(7) 0.0011(6) 0.0051(6) 0.0040(5)
C5 0.0298(12) 0.0217(11) 0.0172(10) 0.0037(10) -0.0014(9) -0.0010(8)
C6 0.0200(10) 0.0164(9) 0.0155(9) -0.0004(9) -0.0034(8) 0.0000(8)
O6 0.0331(9) 0.0128(7) 0.0181(8) -0.0045(7) 0.0085(7) 0.0004(6)
C7 0.0194(10) 0.0138(9) 0.0174(10) 0.0015(8) 0.0005(8) -0.0022(7)
O7 0.0207(8) 0.0144(6) 0.0157(7) 0.0036(6) 0.0034(6) 0.0031(5)
O8 0.0227(8) 0.0216(8) 0.0256(8) 0.0093(7) 0.0066(6) 0.0032(6)
C8 0.0139(9) 0.0151(9) 0.0152(9) 0.0027(8) -0.0008(7) -0.0013(7)
C9 0.0186(9) 0.0136(9) 0.0203(10) 0.0018(9) -0.0011(8) -0.0001(8)
O9 0.0178(7) 0.0258(8) 0.0163(7) -0.0040(6) 0.0039(6) 0.0011(6)
C10 0.0297(12) 0.0191(10) 0.0282(11) -0.0009(11) -0.0040(11) -0.0054(8)
C11 0.0385(14) 0.0216(11) 0.0305(12) -0.0026(10) 0.0070(11) 0.0028(10)
C12 0.0177(11) 0.0158(9) 0.0197(10) 0.0006(8) -0.0019(8) -0.0028(7)
C13 0.0143(9) 0.0146(8) 0.0167(9) 0.0005(8) -0.0019(8) -0.0019(7)
C14 0.0182(11) 0.0182(10) 0.0289(11) 0.0015(8) 0.0049(8) -0.0014(8)
C15 0.0194(11) 0.0184(10) 0.0298(12) 0.0056(9) 0.0001(9) -0.0041(8)
C16 0.0309(11) 0.0143(9) 0.0249(10) 0.0044(11) -0.0035(11) 0.0004(8)
C17 0.0270(11) 0.0167(10) 0.0203(11) 0.0026(9) 0.0041(9) 0.0031(8)
C18 0.0178(9) 0.0139(9) 0.0146(9) 0.0020(8) -0.0001(7) 0.0008(7)
C19 0.0201(10) 0.0168(10) 0.0139(9) -0.0003(8) 0.0038(8) 0.0030(7)
C20 0.0144(9) 0.0157(9) 0.0150(9) 0.0024(8) 0.0040(7) 0.0007(7)
C21 0.0197(10) 0.0212(10) 0.0149(9) 0.0053(9) 0.0025(8) 0.0010(8)
C22 0.0291(13) 0.0383(13) 0.0192(10) -0.0018(12) 0.0094(9) -0.0006(9)
C23 0.0247(12) 0.0300(11) 0.0198(10) -0.0033(10) -0.0002(9) -0.0029(9)
C24 0.0161(10) 0.0151(9) 0.0137(9) 0.0018(8) -0.0006(7) -0.0018(7)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
O1 Cu1 N1 . . 94.40(7) ?
O1 Cu1 O2 . . 94.04(7) ?
N1 Cu1 O2 . . 170.16(7) ?
O1 Cu1 O3 . . 171.32(7) ?
N1 Cu1 O3 . . 82.90(7) ?
O2 Cu1 O3 . . 88.01(7) ?
C1 O1 Cu1 . . 126.10(14) ?
C7 N1 C8 . . 118.99(17) ?
C7 N1 Cu1 . . 124.59(15) ?
C8 N1 Cu1 . . 114.74(12) ?
O1 C1 C2 . . 119.00(19) ?
O1 C1 C6 . . 124.71(19) ?
C2 C1 C6 . . 116.29(19) ?
N2 Cu2 O6 . . 177.73(7) ?
N2 Cu2 O5 . . 92.86(6) ?
O6 Cu2 O5 . . 89.41(7) ?
N2 Cu2 O7 . . 82.74(6) ?
O6 Cu2 O7 . . 95.00(7) ?
O5 Cu2 O7 . . 175.60(6) ?
N2 Cu2 O9 . . 93.05(7) ?
O6 Cu2 O9 . . 86.56(7) ?
O5 Cu2 O9 . . 97.98(6) ?
O7 Cu2 O9 . . 82.34(6) ?
C19 N2 C20 . . 117.73(17) ?
C19 N2 Cu2 . . 126.01(15) ?
C20 N2 Cu2 . . 115.27(12) ?
C3 C2 C1 . . 122.0(2) ?
C12 O3 Cu1 . . 115.88(13) ?
C2 C3 C4 . . 121.4(2) ?
C5 C4 C3 . . 118.4(2) ?
C13 O5 Cu2 . . 126.88(13) ?
C4 C5 C6 . . 121.8(2) ?
C5 C6 C1 . . 120.1(2) ?
C5 C6 C7 . . 116.7(2) ?
C1 C6 C7 . . 123.11(18) ?
N1 C7 C6 . . 125.1(2) ?
C24 O7 Cu2 . . 114.52(12) ?
N1 C8 C12 . . 107.65(16) ?
N1 C8 C9 . . 113.31(17) ?
C12 C8 C9 . . 109.13(17) ?
C11 C9 C10 . . 110.89(19) ?
C11 C9 C8 . . 113.03(18) ?
C10 C9 C8 . . 111.79(17) ?
O4 C12 O3 . . 125.1(2) ?
O4 C12 C8 . . 118.02(18) ?
O3 C12 C8 . . 116.81(18) ?
O5 C13 C18 . . 123.56(18) ?
O5 C13 C14 . . 119.67(19) ?
C18 C13 C14 . . 116.76(18) ?
C15 C14 C13 . . 121.4(2) ?
C14 C15 C16 . . 121.7(2) ?
C17 C16 C15 . . 118.1(2) ?
C16 C17 C18 . . 122.1(2) ?
C17 C18 C13 . . 119.99(19) ?
C17 C18 C19 . . 116.49(19) ?
C13 C18 C19 . . 123.52(18) ?
N2 C19 C18 . . 125.9(2) ?
N2 C20 C24 . . 107.80(16) ?
N2 C20 C21 . . 111.48(17) ?
C24 C20 C21 . . 111.23(17) ?
C22 C21 C23 . . 111.35(19) ?
C22 C21 C20 . . 111.56(18) ?
C23 C21 C20 . . 112.23(17) ?
O8 C24 O7 . . 125.85(19) ?
O8 C24 C20 . . 117.06(18) ?
O7 C24 C20 . . 117.07(17) ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Cu1 O1 . 1.8955(15) yes
Cu1 N1 . 1.9205(16) yes
Cu1 O2 . 1.9339(16) yes
Cu1 O3 . 1.9629(15) yes
O1 C1 . 1.299(2) ?
N1 C7 . 1.284(3) yes
N1 C8 . 1.462(3) ?
C1 C2 . 1.415(3) ?
C1 C6 . 1.417(3) ?
Cu2 N2 . 1.9243(17) yes
Cu2 O6 . 1.9411(15) yes
Cu2 O5 . 1.9432(14) yes
Cu2 O7 . 1.9956(14) yes
Cu2 O9 . 2.3663(16) yes
N2 C19 . 1.278(3) yes
N2 C20 . 1.464(3) ?
C2 C3 . 1.370(3) ?
O3 C12 . 1.279(3) ?
C3 C4 . 1.386(3) ?
C4 C5 . 1.370(3) ?
O4 C12 . 1.231(3) ?
O5 C13 . 1.315(2) ?
C5 C6 . 1.408(3) ?
C6 C7 . 1.433(3) ?
O7 C24 . 1.272(2) ?
O8 C24 . 1.237(3) ?
C8 C12 . 1.518(3) ?
C8 C9 . 1.554(3) ?
C9 C11 . 1.511(3) ?
C9 C10 . 1.520(3) ?
C13 C18 . 1.413(3) ?
C13 C14 . 1.413(3) ?
C14 C15 . 1.378(3) ?
C15 C16 . 1.387(3) ?
C16 C17 . 1.367(3) ?
C17 C18 . 1.410(3) ?
C18 C19 . 1.433(3) ?
C20 C24 . 1.524(3) ?
C20 C21 . 1.554(3) ?
C21 C22 . 1.509(3) ?
C21 C23 . 1.523(3) ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
O2 H2A O9 4_466 0.83 1.87 2.688(2) 167.4 yes
O2 H2B O8 . 0.72(3) 1.93(3) 2.645(2) 169.(4) yes
O6 H6 O3 4_666 0.72 2.07 2.784(2) 171.3 yes
O6 H10 O7 4_566 0.77(3) 2.01(3) 2.764(2) 169.(3) yes
O9 H11 O5 1_455 0.942(19) 1.802(19) 2.738(2) 172.(3) yes
O9 H12 O4 4_666 1.01(2) 1.74(2) 2.703(2) 157.(3) yes
_cod_database_fobs_code 2022727