#------------------------------------------------------------------------------ #$Date: 2023-04-05 13:19:31 +0200 (Wed, 05 Apr 2023) $ #$Revision: 282403 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/27/2022721.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022721 loop_ _publ_author_name 'Shyshkina, Mariia O.' 'Lega, Dmitry A.' 'Shemchuk, Liudmyla M.' 'Starchikova, Irina L.' 'Shemchuk, Leonid A.' _publ_section_title ; 3,3′-(Phenylmethylene)bis(1-ethyl-3,4-dihydro-1H-2,1-benzothiazine-2,2,4-trione): single-crystal X-ray diffraction study, quantum-chemical calculations and Hirshfeld surface analysis ; _journal_coeditor_code EX2067 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E Crystallographic Communications' _journal_page_first 349 _journal_page_last 355 _journal_paper_doi 10.1107/S2056989023002505 _journal_volume 79 _journal_year 2023 _chemical_formula_iupac 'C27 H26 N2 O6 S2' _chemical_formula_moiety 'C27 H26 N2 O6 S2' _chemical_formula_sum 'C27 H26 N2 O6 S2' _chemical_formula_weight 538.62 _chemical_name_systematic 3,3'-(Phenylmethylene)bis(1-ethyl-3,4-dihydro-1H-2,1-benzothiazine-2,2,4-trione) _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _audit_creation_method ; Olex2 1.5 (compiled 2022.04.07 svn.rca3783a0 for OlexSys, GUI svn.r6498) ; _cell_angle_alpha 90 _cell_angle_beta 108.613(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 11.7125(4) _cell_length_b 18.4040(6) _cell_length_c 12.8601(5) _cell_measurement_reflns_used 3809 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 24.8050 _cell_measurement_theta_min 3.6020 _cell_volume 2627.09(17) _computing_cell_refinement ; CrysAlisPro 1.171.39.46 (Rigaku OD, 2018) ; _computing_data_collection ; CrysAlisPro 1.171.39.46 (Rigaku OD, 2018) ; _computing_data_reduction ; CrysAlisPro 1.171.39.46 (Rigaku OD, 2018) ; _computing_molecular_graphics ; Mercury (Macrae et al., 2020) ; _computing_publication_material ; Olex2 1.5 (Dolomanov et al., 2009) ; _computing_structure_refinement ; SHELXL2016/6 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2014/5 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 293(2) _diffrn_detector_area_resol_mean 16.1827 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Xcalibur, Sapphire3' _diffrn_measurement_method '\w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0720 _diffrn_reflns_av_unetI/netI 0.0529 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 18007 _diffrn_reflns_theta_full 24.999 _diffrn_reflns_theta_max 24.999 _diffrn_reflns_theta_min 3.057 _exptl_absorpt_coefficient_mu 0.247 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.77349 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (CrysAlisPro; Rigaku OD, 2018) ; _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.362 _exptl_crystal_description block _exptl_crystal_F_000 1128 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.1 _refine_diff_density_max 0.209 _refine_diff_density_min -0.354 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.038 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 356 _refine_ls_number_reflns 4617 _refine_ls_number_restraints 4 _refine_ls_restrained_S_all 1.038 _refine_ls_R_factor_all 0.0754 _refine_ls_R_factor_gt 0.0583 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0785P)^2^+0.6422P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1453 _refine_ls_wR_factor_ref 0.1632 _reflns_number_gt 3493 _reflns_number_total 4617 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ex2067sup1.cif _cod_data_source_block I _cod_database_code 2022721 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_hkl_file ; 0 0 2 4672.06 24.81 0 0 2 3512.85 27.45 0 0 3 0.17 0.32 0 0 3 1.07 0.76 0 0 -3 0.49 0.70 0 0 -3 0.27 0.36 0 0 -4 202.47 10.57 0 0 -4 145.24 6.56 0 0 4 268.25 10.68 0 0 4 302.99 9.26 0 0 5 0.62 0.18 0 0 -5 -0.11 0.38 0 0 -6 91.99 6.55 0 0 6 254.04 12.64 0 0 7 2.83 1.72 0 0 -7 -0.14 0.02 0 0 -8 10.95 2.13 0 0 8 14.64 3.72 0 0 -9 -0.05 0.27 0 0 9 0.23 0.80 0 0 10 53.57 8.03 0 0 11 -0.38 0.39 0 0 12 0.21 0.88 0 0 13 1.50 2.57 0 0 14 5.49 3.73 0 0 15 4.25 3.97 0 0 16 -0.71 0.93 0 -1 2 2842.25 23.63 0 1 2 2693.79 24.24 0 -1 -3 249.18 7.27 0 1 -3 275.99 10.18 0 -1 3 258.21 8.83 0 1 3 245.44 8.75 0 -1 3 272.57 7.94 0 -1 4 75.19 5.55 0 1 4 66.35 5.18 0 -1 4 74.67 4.72 0 1 -4 60.22 5.63 0 -1 5 201.18 8.82 0 -1 5 195.39 10.24 0 1 5 165.67 9.21 0 -1 6 4.39 1.56 0 1 6 4.86 1.40 0 -1 -6 0.94 0.58 0 -1 6 5.31 1.62 0 -1 7 3.26 1.87 0 -1 -7 0.65 0.57 0 1 -7 0.14 0.19 0 1 7 1.34 1.65 0 -1 7 0.76 0.94 0 -1 8 82.09 8.66 0 1 8 71.86 7.93 0 -1 9 17.08 4.33 0 1 9 13.18 3.54 0 1 -9 5.61 1.40 0 1 10 5.44 2.12 0 -1 10 2.64 0.86 0 -1 11 16.01 4.91 0 1 11 16.12 4.96 0 -1 12 30.97 7.12 0 1 12 33.12 7.44 0 -1 13 4.74 3.46 0 1 13 6.77 4.33 0 1 14 40.85 9.78 0 -1 14 42.86 9.77 0 1 15 3.45 3.96 0 -1 15 5.50 4.34 0 1 16 5.00 3.78 0 -1 16 2.20 2.77 0 -2 2 1781.79 20.20 0 -2 -2 1961.36 24.95 0 -2 2 2050.07 25.59 0 2 -2 1781.46 21.62 0 2 2 1783.29 22.01 0 2 3 762.68 11.66 0 -2 3 748.97 15.24 0 2 -3 883.85 18.98 0 2 -3 845.98 10.07 0 -2 3 845.16 19.72 0 -2 -3 838.92 19.17 0 2 3 792.38 16.95 0 2 4 1035.31 17.04 0 2 4 979.34 20.93 0 -2 4 1010.08 20.13 0 2 5 30.09 3.47 0 -2 5 34.88 4.33 0 -2 5 34.83 3.79 0 2 5 31.81 4.18 0 2 -6 1.95 0.52 0 2 6 5.59 1.77 0 -2 6 6.11 1.85 0 -2 6 7.00 2.38 0 2 6 5.34 1.95 0 -2 -6 2.34 1.03 0 -2 7 48.21 6.18 0 2 7 48.98 6.16 0 -2 -7 33.53 4.04 0 -2 7 54.34 5.61 0 2 8 1.05 1.69 0 -2 8 0.43 1.22 0 -2 8 0.84 1.39 0 2 -8 0.02 0.11 0 -2 9 5.42 2.48 0 2 9 3.76 1.87 0 2 -9 1.59 0.55 0 2 10 -0.18 0.77 0 -2 10 3.90 2.35 0 -2 11 16.79 4.93 0 2 11 14.78 4.77 0 2 12 6.74 4.58 0 -2 12 8.75 3.89 0 -2 13 3.87 3.32 0 2 13 5.67 3.51 0 -2 14 0.93 2.41 0 2 14 1.94 1.94 0 -2 15 -0.10 2.09 0 2 15 0.49 1.18 0 -2 16 4.15 3.84 0 2 16 9.47 5.93 0 -3 0 1.62 0.74 0 -3 0 0.86 0.63 0 3 -1 416.42 9.84 0 -3 1 469.56 8.93 0 3 1 431.76 9.89 0 -3 1 380.05 8.09 0 -3 -1 488.47 11.56 0 -3 -1 514.66 11.86 0 -3 1 476.71 11.37 0 3 2 1.39 0.94 0 3 -2 1.28 0.43 0 -3 2 0.97 0.48 0 3 -2 1.96 0.94 0 -3 -2 -0.17 0.26 0 -3 2 0.81 0.26 0 -3 2 2.04 0.90 0 -3 -3 822.53 20.39 0 3 -3 968.24 11.04 0 3 3 880.20 18.87 0 -3 3 893.17 18.03 0 -3 3 1019.67 22.85 0 -3 3 920.68 11.39 0 3 3 878.27 10.18 0 3 -4 207.62 5.57 0 3 4 185.55 9.52 0 -3 4 178.59 8.65 0 3 4 181.19 6.35 0 -3 5 84.66 6.41 0 -3 5 78.38 6.41 0 3 -5 99.97 4.58 0 3 5 77.78 5.12 0 3 5 82.58 6.95 0 -3 6 61.74 5.72 0 3 -6 72.17 4.34 0 -3 6 58.65 6.13 0 3 6 63.02 6.85 0 -3 7 39.17 5.55 0 3 7 38.74 5.78 0 -3 7 42.89 5.13 0 -3 -7 28.65 3.78 0 3 -7 43.85 3.68 0 3 7 25.75 3.86 0 3 8 9.39 3.39 0 -3 8 9.42 2.60 0 3 -8 7.05 1.60 0 -3 8 10.62 3.19 0 -3 9 7.65 2.35 0 3 9 4.73 2.29 0 3 -9 2.77 1.08 0 -3 9 7.00 2.98 0 3 10 -0.37 0.19 0 -3 10 3.95 2.33 0 -3 10 2.76 2.10 0 3 -10 1.06 0.86 0 3 11 1.14 0.51 0 -3 11 5.78 3.29 0 -3 12 101.08 12.72 0 3 12 98.59 13.12 0 -3 13 2.27 1.57 0 3 13 3.47 2.77 0 -3 14 22.43 7.04 0 3 14 30.95 8.44 0 -3 15 6.33 3.73 0 3 15 8.46 4.78 0 3 16 1.97 2.27 0 -3 16 -0.33 0.56 0 4 0 1067.61 16.35 0 4 0 1062.26 17.61 0 -4 0 1088.05 19.05 0 -4 1 16.89 2.07 0 4 1 17.46 2.29 0 -4 -1 18.80 2.67 0 4 -1 15.68 1.88 0 -4 1 19.17 2.76 0 -4 1 13.54 1.85 0 4 -1 16.44 2.17 0 -4 -1 18.50 2.57 0 -4 2 283.57 7.72 0 -4 -2 321.26 11.88 0 4 -2 316.79 7.55 0 -4 2 306.09 11.58 0 4 -2 302.17 10.71 0 4 2 283.42 10.14 0 -4 -2 301.89 11.62 0 -4 2 336.39 8.53 0 4 3 181.44 8.72 0 -4 3 215.96 6.35 0 4 -3 214.11 9.89 0 -4 3 181.57 5.32 0 4 -3 190.40 5.56 0 -4 3 187.59 10.84 0 -4 4 20.24 3.21 0 4 4 20.29 3.39 0 4 -4 20.93 1.85 0 -4 5 602.42 18.11 0 4 5 608.35 12.66 0 4 5 639.22 20.33 0 -4 6 58.69 6.12 0 4 6 52.07 4.39 0 4 -6 71.09 3.92 0 -4 6 66.55 6.26 0 4 6 62.94 6.87 0 4 7 1.40 0.82 0 4 -7 3.83 1.09 0 -4 7 2.59 1.41 0 -4 7 5.18 2.28 0 4 7 2.01 1.71 0 -4 8 33.36 5.67 0 -4 8 29.83 4.73 0 4 8 32.25 5.92 0 4 -8 19.18 2.38 0 4 9 37.11 6.71 0 -4 9 42.90 6.75 0 -4 9 41.36 5.97 0 -4 10 0.57 0.27 0 4 10 1.02 2.29 0 -4 10 2.98 2.34 0 -4 11 6.47 2.77 0 4 11 6.05 3.16 0 -4 11 5.86 3.54 0 4 12 39.35 8.41 0 -4 12 23.71 6.62 0 -4 13 14.02 5.60 0 4 13 13.75 5.70 0 4 14 2.12 3.11 0 -4 14 1.21 1.82 0 -4 15 3.68 3.76 0 4 15 2.92 2.50 0 4 16 0.12 1.11 0 -4 16 -0.27 1.22 0 5 0 1.38 1.22 0 5 0 -0.29 0.59 0 -5 0 -0.48 0.34 0 -5 0 -0.81 0.83 0 5 -1 5.84 1.65 0 -5 -1 4.63 1.44 0 5 1 5.93 1.49 0 -5 1 4.79 1.11 0 5 -1 4.78 1.01 0 -5 1 3.22 1.13 0 -5 -1 3.92 1.39 0 -5 1 3.27 0.94 0 -5 2 38.37 3.39 0 -5 2 33.91 3.13 0 -5 -2 24.07 3.70 0 5 -2 35.82 3.78 0 5 -2 35.42 2.86 0 -5 2 36.21 4.43 0 5 2 33.59 3.71 0 -5 -2 35.43 4.34 0 5 -3 830.42 20.03 0 5 3 799.49 19.50 0 5 -3 839.43 13.45 0 -5 3 814.66 14.13 0 -5 3 869.76 14.94 0 -5 4 73.24 6.08 0 5 -4 79.79 3.98 0 -5 4 91.34 4.79 0 5 -4 79.40 6.74 0 5 4 71.56 6.24 0 5 5 -0.23 1.09 0 -5 5 0.92 0.92 0 5 -5 0.23 0.19 0 5 6 83.06 7.96 0 -5 6 80.02 7.27 0 5 -6 80.36 4.11 0 -5 7 7.34 2.23 0 5 7 9.15 3.09 0 5 -7 8.41 1.45 0 -5 7 7.01 2.27 0 5 8 0.65 0.76 0 5 -8 0.63 0.48 0 5 8 1.63 1.95 0 -5 8 1.74 1.47 0 -5 8 1.33 1.27 0 -5 9 62.06 8.46 0 5 9 72.14 9.60 0 -5 9 52.18 6.77 0 -5 10 0.81 1.70 0 5 10 5.57 2.86 0 -5 10 4.79 2.85 0 -5 11 27.35 5.45 0 -5 11 28.55 6.74 0 5 11 30.73 6.96 0 -5 12 35.30 7.84 0 5 12 30.03 7.51 0 -5 12 26.83 5.82 0 -5 13 16.44 6.01 0 5 13 13.26 4.99 0 -5 14 13.60 5.85 0 5 14 13.33 5.41 0 5 15 -0.62 2.39 0 -5 15 4.93 4.43 0 -5 16 0.18 0.88 0 -6 0 1386.26 26.67 0 6 0 1254.75 23.64 0 6 -1 4.56 1.31 0 -6 1 4.17 1.87 0 6 -1 3.76 0.93 0 -6 1 2.70 1.15 0 -6 -1 2.65 1.50 0 -6 1 1.88 0.84 0 6 1 4.22 1.53 0 6 -2 62.67 4.52 0 -6 2 58.33 4.66 0 6 2 56.91 5.29 0 6 -2 57.12 5.23 0 -6 2 66.03 5.21 0 6 3 18.23 3.10 0 6 -3 17.15 2.25 0 -6 3 23.36 2.99 0 6 -3 17.72 3.05 0 -6 3 16.42 2.31 0 6 -4 35.93 4.84 0 6 4 31.51 4.43 0 6 -4 36.44 3.08 0 -6 4 33.66 3.08 0 -6 4 41.31 3.60 0 -6 5 1.05 1.13 0 6 5 0.45 0.05 0 -6 5 0.24 0.21 0 6 -5 1.31 0.63 0 6 -6 32.94 2.71 0 -6 6 39.50 5.38 0 6 6 32.11 4.91 0 6 -7 1.91 0.62 0 6 7 3.54 1.70 0 -6 7 5.13 2.06 0 -6 7 1.28 0.69 0 -6 8 99.52 9.82 0 -6 8 103.66 9.69 0 6 8 98.33 10.27 0 -6 9 359.94 18.54 0 6 9 359.00 20.98 0 -6 9 379.29 20.80 0 6 10 146.96 14.38 0 -6 10 148.47 14.14 0 -6 10 126.15 11.61 0 -6 11 2.99 1.89 0 6 11 5.93 3.11 0 -6 11 7.06 3.95 0 -6 12 1.91 2.45 0 -6 12 -0.01 1.50 0 6 12 -1.37 0.42 0 -6 13 7.00 4.47 0 6 13 7.32 3.93 0 6 14 0.49 0.95 0 -6 14 4.79 3.76 0 -6 15 0.48 0.92 0 6 15 2.06 2.34 0 -6 16 -0.12 1.40 0 7 0 1.57 1.51 0 -7 1 52.58 5.23 0 7 -1 62.40 5.69 0 7 1 62.79 5.68 0 7 -1 65.52 5.15 0 -7 2 105.06 7.38 0 -7 2 97.38 6.82 0 7 -2 145.61 8.79 0 7 -2 154.45 7.62 0 7 2 140.21 8.81 0 7 -3 14.59 3.03 0 7 -3 14.68 2.31 0 7 3 13.00 2.57 0 -7 3 10.13 2.09 0 -7 3 9.08 2.12 0 7 -4 73.66 4.81 0 7 4 66.86 6.45 0 -7 4 63.18 4.80 0 7 -4 65.54 6.75 0 -7 4 73.74 5.43 0 7 5 37.21 5.29 0 -7 5 42.09 3.93 0 7 -5 36.26 5.29 0 -7 5 40.39 5.22 0 7 -5 38.15 3.29 0 7 -6 253.49 8.06 0 7 6 228.55 13.83 0 -7 6 258.71 14.62 0 7 7 159.19 12.35 0 -7 7 164.25 11.84 0 -7 8 2.14 0.24 0 -7 8 3.71 1.97 0 7 8 2.88 3.32 0 7 -8 0.59 0.27 0 -7 9 2.94 2.01 0 7 9 0.94 1.47 0 -7 9 3.81 2.04 0 7 10 78.16 10.71 0 -7 10 84.12 10.95 0 -7 10 77.85 9.46 0 7 11 4.96 3.97 0 -7 11 3.80 2.04 0 -7 11 4.50 3.33 0 -7 12 0.49 1.34 0 -7 12 1.13 1.21 0 7 12 3.33 2.71 0 -7 13 2.01 1.97 0 -7 13 11.75 5.32 0 7 13 10.55 5.41 0 7 14 6.80 4.23 0 -7 14 10.01 5.30 0 7 15 1.95 1.95 0 -7 15 1.76 2.65 0 -7 16 -0.71 1.72 0 8 0 242.64 11.97 0 8 1 92.70 7.13 0 8 -1 95.02 7.53 0 8 -2 256.96 12.45 0 8 -2 262.48 10.76 0 8 2 248.76 12.16 0 -8 3 2.28 1.26 0 8 3 3.16 1.35 0 8 -3 2.95 1.27 0 -8 3 0.76 0.61 0 8 -3 2.42 1.15 0 8 -4 172.95 8.26 0 8 -4 165.56 11.05 0 8 4 155.59 10.40 0 -8 4 112.66 7.59 0 -8 4 124.81 7.65 0 8 -5 124.49 6.68 0 -8 5 135.81 10.04 0 8 -5 145.88 11.21 0 -8 5 142.51 7.97 0 -8 5 116.73 6.82 0 8 5 126.18 10.09 0 8 -6 14.06 2.20 0 -8 6 19.91 4.71 0 8 6 14.89 3.92 0 8 -6 20.13 4.91 0 -8 6 12.97 2.29 0 -8 7 8.09 2.57 0 8 -7 2.70 0.84 0 8 7 10.87 3.58 0 -8 8 668.82 26.49 0 -8 8 590.48 24.77 0 8 8 590.83 25.99 0 -8 9 4.81 1.52 0 8 9 5.38 2.99 0 -8 9 4.43 2.33 0 8 10 36.57 7.53 0 -8 10 21.26 5.19 0 -8 10 36.09 7.12 0 8 11 2.84 2.89 0 -8 11 -0.40 0.78 0 -8 11 0.61 0.78 0 8 12 7.38 4.31 0 -8 12 4.43 2.75 0 -8 12 3.98 2.86 0 8 13 4.65 3.49 0 -8 13 0.37 0.69 0 -8 13 4.91 3.72 0 -8 14 -0.04 0.70 0 8 14 -0.64 1.12 0 -8 15 0.39 1.25 0 8 15 1.01 1.25 0 -8 16 -1.31 3.07 0 9 0 0.46 1.33 0 9 -1 0.74 0.36 0 9 1 1.12 0.36 0 9 2 393.85 16.20 0 9 -2 390.97 16.06 0 9 -3 56.88 6.54 0 9 3 60.99 6.71 0 9 -3 59.98 5.31 0 9 -4 331.94 12.12 0 -9 4 196.06 10.60 0 9 4 352.36 16.80 0 -9 4 220.70 11.94 0 9 -4 377.19 17.58 0 9 4 352.03 16.41 0 -9 5 188.70 9.69 0 9 -5 343.74 11.91 0 9 5 351.73 17.42 0 9 -5 393.55 19.63 0 -9 5 206.23 10.65 0 9 -6 647.72 15.53 0 9 6 915.82 30.07 0 9 -6 967.22 31.16 0 -9 6 932.52 29.10 0 9 7 40.83 6.67 0 -9 7 44.58 7.11 0 -9 8 69.75 8.72 0 9 8 77.26 9.95 0 9 9 7.77 3.62 0 -9 9 2.01 2.25 0 -9 9 3.48 1.89 0 -9 10 38.75 7.49 0 -9 10 40.63 7.31 0 9 10 41.54 8.14 0 9 11 4.03 2.96 0 -9 11 2.78 2.42 0 -9 11 1.68 1.97 0 -9 12 2.92 2.57 0 -9 12 3.29 2.15 0 9 12 2.56 3.04 0 -9 13 0.23 0.20 0 -9 13 2.53 2.89 0 9 13 3.24 3.26 0 9 14 -1.20 1.34 0 -9 14 0.46 1.05 0 -9 15 -0.71 1.52 0 -9 16 0.90 2.76 0 10 0 165.41 11.14 0 10 1 20.20 4.10 0 10 -1 20.23 4.05 0 10 -2 1.58 1.00 0 10 2 1.25 0.61 0 10 2 1.31 1.13 0 -10 2 1.05 0.43 0 10 3 89.58 8.38 0 10 -3 99.85 9.03 0 10 4 92.76 9.19 0 10 -4 103.73 7.25 0 10 -4 111.27 10.15 0 10 5 1.28 0.29 0 10 5 1.03 1.66 0 -10 5 0.15 0.23 0 10 -5 1.47 1.00 0 -10 5 1.07 0.95 0 10 -5 1.90 1.60 0 10 6 33.38 6.13 0 -10 6 23.07 3.67 0 -10 6 37.09 6.32 0 10 -6 36.41 6.43 0 -10 7 255.23 17.29 0 10 7 216.39 15.79 0 -10 8 370.50 21.44 0 10 8 354.99 21.45 0 -10 9 4.30 2.71 0 -10 9 1.84 1.18 0 10 9 4.43 3.16 0 -10 10 4.99 3.02 0 -10 10 7.05 3.13 0 10 10 6.74 3.98 0 -10 11 7.72 3.66 0 -10 11 5.21 3.45 0 10 11 10.66 4.53 0 -10 12 6.63 3.35 0 10 12 5.85 3.27 0 -10 12 3.32 2.22 0 -10 13 0.88 1.70 0 -10 13 2.07 2.22 0 10 13 4.84 3.07 0 10 14 0.87 2.96 0 -10 14 2.56 2.98 0 -10 15 0.07 1.20 0 11 0 -0.24 0.72 0 11 1 14.00 3.76 0 11 -1 12.19 3.33 0 11 -2 44.01 6.07 0 -11 2 40.64 2.21 0 11 2 46.78 6.27 0 11 2 31.65 2.38 0 11 3 79.96 8.30 0 11 -3 80.08 8.44 0 11 4 60.81 7.75 0 11 -4 67.92 8.47 0 11 -5 301.15 18.12 0 11 5 283.79 17.39 0 11 6 241.54 16.32 0 11 -6 259.35 17.86 0 -11 7 45.91 7.43 0 11 7 41.24 7.23 0 11 -7 45.93 7.65 0 11 8 13.66 4.73 0 -11 8 18.05 4.93 0 -11 9 29.19 6.70 0 -11 9 34.96 7.02 0 11 9 33.51 7.14 0 -11 10 4.73 3.60 0 11 10 4.05 2.84 0 -11 10 3.76 2.17 0 11 11 2.26 2.84 0 -11 11 2.85 3.10 0 -11 11 -0.21 0.55 0 11 12 7.95 4.04 0 -11 12 5.75 3.86 0 -11 12 4.71 3.15 0 11 13 1.62 1.30 0 -11 13 1.13 1.95 0 -11 13 1.01 2.02 0 -11 14 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4 -6 5 3.15 1.95 4 6 5 1.52 0.57 4 -6 5 0.63 1.02 4 6 5 2.35 1.65 -4 6 -6 19.09 3.92 4 6 6 29.14 5.49 4 -6 6 27.57 5.57 4 -6 6 29.72 5.93 4 6 6 29.26 5.49 4 -6 6 27.83 4.40 4 -6 6 20.60 2.42 -4 6 -7 3.11 1.94 4 -6 7 3.77 1.57 4 -6 7 4.59 2.45 4 6 7 2.91 1.95 4 6 7 4.05 1.70 4 -6 7 5.55 3.24 4 -6 8 27.13 6.23 -4 6 -8 11.35 3.15 4 6 8 23.82 5.68 4 6 8 25.61 6.03 4 -6 8 26.43 6.07 4 -6 8 20.43 4.42 4 -6 9 2.90 2.51 -4 6 -9 0.78 1.08 4 6 9 0.40 0.96 4 -6 9 1.15 1.63 4 6 9 0.27 0.99 4 6 10 7.33 3.74 4 6 10 11.87 5.04 4 -6 10 9.88 4.39 4 -6 10 6.20 3.10 4 6 11 0.57 1.21 4 -6 11 1.11 1.87 4 6 11 -0.01 1.13 4 -6 11 -0.15 0.52 4 6 12 0.59 1.87 4 -6 12 1.07 2.38 4 6 12 -0.44 2.06 4 -6 13 4.02 3.49 4 6 13 1.25 1.84 4 6 13 6.73 4.47 4 6 14 -0.64 1.69 -4 -7 16 8.65 5.38 -4 -7 15 -0.33 1.27 -4 7 15 3.29 3.35 -4 -7 14 12.10 5.47 -4 7 14 11.47 5.09 -4 -7 13 23.89 6.88 -4 7 13 25.91 7.04 -4 -7 12 15.35 3.98 -4 -7 12 16.52 5.26 -4 7 12 21.43 6.06 -4 -7 11 9.50 4.28 -4 7 11 10.64 4.20 -4 7 10 4.72 3.04 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7 9.92 3.13 -4 -8 7 12.00 3.48 4 8 -7 10.13 2.65 -4 8 7 10.23 3.11 -4 -8 7 4.86 1.06 4 8 -7 14.27 4.21 4 8 -6 40.01 6.47 -4 8 6 37.93 5.57 -4 8 6 36.95 5.63 4 8 -6 36.91 5.02 4 8 -5 197.32 13.49 -4 8 5 183.07 11.42 -4 8 5 186.10 12.11 4 8 -5 213.04 12.02 4 8 -4 1.19 1.28 -4 8 4 2.80 1.54 4 8 -4 3.24 1.89 4 8 -4 1.25 1.14 -4 8 4 2.56 1.40 -4 8 3 28.40 3.89 -4 8 3 29.13 4.73 -4 8 3 30.60 4.35 4 8 -3 33.36 5.00 4 8 -3 29.72 4.50 4 8 -3 28.67 4.48 4 8 -2 252.50 13.35 4 8 -2 298.21 13.86 -4 8 2 278.47 12.41 -4 8 2 249.67 12.91 4 8 -2 254.18 13.11 4 8 -1 46.35 5.23 4 8 -1 39.96 5.49 4 -8 -1 31.58 4.12 4 8 -1 47.92 5.88 -4 8 1 51.98 5.35 -4 8 1 45.67 5.53 4 -8 -1 57.13 6.37 4 -8 0 725.24 17.36 4 8 0 710.16 19.18 4 8 0 710.66 22.85 -4 8 0 695.19 19.16 4 -8 0 731.14 23.26 4 8 0 645.13 21.59 4 8 1 35.18 5.11 -4 8 -1 35.37 4.39 4 8 1 39.35 4.34 -4 8 -1 36.60 4.99 4 8 1 36.31 5.22 4 -8 1 41.23 5.80 -4 8 -2 3.76 1.87 4 -8 2 3.59 2.01 4 -8 2 4.31 1.82 4 8 2 2.61 1.63 4 8 2 4.09 1.62 -4 8 -2 4.11 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17.57 5.05 4 9 7 14.02 4.15 4 -9 8 15.06 4.62 4 -9 8 11.87 3.64 4 -9 8 19.99 5.68 4 9 8 11.22 4.08 4 9 8 14.09 4.75 -4 9 -8 6.45 2.42 4 -9 9 5.09 2.60 4 -9 9 7.87 4.08 4 9 9 4.21 2.59 4 -9 9 6.20 3.87 4 9 9 2.26 2.28 4 9 10 11.78 4.88 4 9 10 6.81 3.66 4 -9 10 12.51 5.55 4 -9 10 15.37 5.67 4 -9 11 5.36 4.16 4 9 11 0.49 1.30 4 9 11 2.60 2.60 4 -9 11 2.73 3.45 4 -9 12 27.76 8.52 4 9 12 8.41 4.33 4 9 12 22.76 8.05 4 9 13 -0.46 1.28 4 9 13 4.33 3.79 4 -9 13 0.61 1.24 -4 -10 15 0.74 2.12 -4 10 15 0.14 2.13 -4 -10 14 2.61 2.14 -4 10 14 0.99 1.49 -4 -10 13 -0.56 1.12 -4 10 13 -0.68 1.24 -4 -10 12 10.59 4.92 -4 10 12 10.81 4.48 -4 -10 11 1.53 2.03 -4 10 11 -0.36 0.86 -4 -10 10 1.58 2.13 -4 10 10 -1.63 2.20 4 10 -9 14.44 3.34 4 -10 -9 16.10 3.07 -4 10 9 23.85 5.30 4 10 -8 -0.19 0.71 4 10 -8 2.63 2.40 -4 -10 8 1.19 1.65 -4 10 8 0.89 1.72 -4 10 7 5.29 2.47 4 10 -7 1.70 0.78 -4 10 7 2.06 2.14 4 10 -7 5.42 2.97 4 10 -6 2.69 1.06 -4 10 6 2.78 1.81 4 10 -6 1.85 2.15 -4 -10 6 0.13 0.34 -4 10 6 -0.06 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151.54 11.27 4 10 4 130.10 10.38 4 10 4 149.37 12.80 4 10 4 119.64 5.93 -4 10 -4 132.72 10.41 4 -10 4 172.63 14.15 -4 10 -4 149.14 11.59 4 10 5 0.06 0.13 4 -10 5 0.26 1.00 4 10 5 -1.41 0.81 4 -10 5 0.75 1.06 4 10 5 1.87 1.81 4 -10 5 2.03 0.51 -4 10 -5 -0.04 0.71 4 -10 6 9.54 2.79 4 -10 6 10.76 3.85 4 -10 6 10.34 3.24 4 10 6 10.98 3.58 4 10 6 10.73 3.59 -4 10 -6 11.79 3.30 4 -10 7 1.82 1.50 4 -10 7 2.19 2.34 4 -10 7 2.96 2.36 4 10 7 3.76 2.07 4 10 7 1.15 0.88 -4 10 -7 1.59 1.24 4 -10 8 7.72 3.61 4 -10 8 16.36 5.42 4 -10 8 10.09 3.41 4 10 8 10.98 4.29 4 10 9 8.78 3.67 4 -10 9 18.91 6.23 4 -10 9 14.80 4.97 4 -10 10 18.72 6.30 4 10 10 4.99 2.96 4 -10 10 19.64 6.80 4 10 10 23.60 7.21 4 10 11 1.87 1.90 4 10 11 7.15 4.23 4 -10 11 5.63 3.59 4 -10 11 5.97 3.55 4 -10 12 0.63 2.28 4 10 12 0.44 1.81 4 10 12 3.20 3.47 4 10 13 0.61 2.40 4 -10 13 0.64 1.71 4 10 13 1.27 2.02 -4 -11 15 1.62 2.60 -4 -11 14 3.62 3.27 -4 11 14 1.38 1.97 -4 -11 13 6.08 4.16 -4 11 13 1.72 2.20 -4 -11 12 1.78 2.82 -4 11 12 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2 326.32 18.99 -4 11 -3 71.88 8.14 4 -11 3 65.73 6.85 4 11 3 63.05 6.82 4 11 3 80.55 9.58 -4 11 -3 64.13 7.67 4 -11 3 77.56 9.86 4 -11 4 21.89 5.63 4 -11 4 13.94 3.46 4 11 4 16.19 3.93 4 -11 4 12.74 3.17 -4 11 -4 13.64 3.83 4 11 4 13.38 4.09 -4 11 -4 14.36 3.51 4 -11 5 3.49 2.48 4 -11 5 -0.93 1.11 4 -11 5 0.61 0.92 4 11 5 1.09 1.01 4 11 5 1.33 0.76 -4 11 -5 1.16 1.47 4 -11 6 9.64 2.90 4 -11 6 13.29 4.73 4 -11 6 9.31 3.14 4 11 6 11.59 3.71 4 11 6 12.73 4.29 -4 11 -6 6.71 2.63 4 -11 7 0.97 1.39 4 11 7 0.93 1.94 4 -11 7 0.18 1.25 4 -11 7 1.06 2.03 4 11 7 -0.72 1.43 -4 11 -7 0.27 0.71 4 -11 8 20.64 6.63 4 11 8 4.85 2.67 4 -11 8 15.93 4.41 4 11 8 12.42 4.98 4 -11 8 9.56 3.80 4 -11 9 2.28 1.96 4 11 9 0.62 1.01 4 11 9 1.02 2.63 4 -11 9 1.13 2.27 4 -11 10 1.06 1.74 4 11 10 0.17 0.77 4 -11 10 0.82 1.97 4 -11 11 2.08 2.29 4 11 11 0.75 0.93 4 -11 11 0.84 3.49 4 -11 12 22.59 7.58 4 11 12 8.11 4.47 4 -11 12 32.18 10.07 4 -11 13 2.38 2.25 4 11 13 3.10 2.92 -4 -12 15 2.57 2.51 -4 12 14 3.40 3.03 -4 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1.95 4 -12 12 4.91 5.29 4 12 12 0.04 1.00 4 12 12 0.95 1.41 4 -12 13 6.79 4.71 -4 -13 14 24.70 8.27 -4 13 14 21.68 7.71 -4 -13 13 2.94 3.07 -4 13 13 -0.19 0.61 -4 -13 12 3.35 3.01 -4 13 12 1.50 1.49 -4 13 11 12.56 4.78 -4 -13 11 8.97 4.81 -4 -13 10 8.78 4.85 -4 13 10 11.30 4.86 4 13 -9 19.66 5.62 -4 13 9 14.56 4.69 -4 -13 9 18.33 6.56 4 13 -8 36.82 7.93 4 13 -8 16.04 4.03 -4 13 8 34.13 7.06 4 13 -7 2.06 1.53 4 13 -7 7.58 3.99 -4 13 7 6.74 2.90 -4 13 7 3.87 2.28 4 13 -6 11.72 3.55 4 13 -6 16.90 5.05 -4 13 6 11.17 3.95 -4 13 6 12.44 4.37 -4 13 6 12.26 3.95 4 13 -5 39.42 7.53 -4 13 5 34.96 6.35 4 13 -5 32.85 5.75 -4 13 5 30.84 6.10 4 13 -4 48.65 7.32 4 13 -4 55.44 8.51 -4 13 4 52.51 7.56 -4 13 4 50.08 7.57 4 13 -3 34.71 6.31 4 13 -3 35.13 6.62 -4 13 3 33.05 5.78 -4 13 3 30.08 5.59 -4 13 2 21.51 4.86 -4 13 2 24.04 5.04 4 13 -2 24.16 4.96 4 13 -2 24.61 5.34 4 13 -1 39.44 6.94 -4 13 1 35.65 6.04 4 13 -1 32.66 5.82 -4 13 1 32.21 5.92 -4 13 0 82.77 9.22 -4 13 0 88.61 9.47 4 13 0 80.54 9.36 4 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2.36 4 13 12 2.01 2.17 -4 -14 14 15.34 6.64 -4 -14 13 7.31 4.90 -4 14 13 2.99 2.85 -4 -14 12 27.99 8.52 -4 14 12 9.65 4.72 -4 -14 11 15.20 5.85 -4 14 11 3.58 2.47 -4 -14 10 20.54 6.80 -4 14 10 13.31 4.97 4 14 -9 0.44 0.53 -4 14 9 0.65 1.43 -4 14 9 3.67 2.84 -4 -14 9 -0.38 1.82 4 14 -8 23.10 6.69 -4 14 8 16.53 5.32 -4 14 8 18.31 5.87 4 14 -7 5.87 3.36 4 14 -7 3.55 2.03 -4 14 7 5.94 3.34 -4 14 7 8.32 3.76 4 14 -6 24.22 5.45 4 14 -6 28.05 6.66 -4 14 6 24.23 6.05 -4 14 5 11.93 3.96 4 14 -5 9.12 3.65 4 14 -5 9.84 4.08 -4 14 5 9.63 3.42 -4 14 4 5.16 2.61 4 14 -4 4.61 2.82 -4 14 4 4.30 2.61 4 14 -4 6.54 3.52 -4 14 3 1.52 1.30 4 14 -3 1.37 1.27 4 14 -3 4.49 3.21 -4 14 3 4.11 2.35 -4 14 2 65.70 8.88 4 14 -2 58.36 8.79 -4 14 2 62.44 8.52 4 14 -2 61.54 8.53 4 14 -1 1.39 1.45 -4 14 1 1.82 1.96 -4 14 1 0.50 1.06 -4 14 0 84.26 9.60 -4 14 0 94.04 10.11 4 14 0 100.66 11.93 4 14 1 87.39 11.48 -4 14 -1 80.05 9.51 -4 14 -1 73.73 8.94 -4 14 -2 9.26 3.41 -4 14 -2 7.45 3.04 4 14 2 17.58 5.68 -4 14 -3 74.44 9.70 4 14 3 88.12 11.67 -4 14 -3 68.86 8.56 4 -14 3 86.10 11.40 4 -14 4 22.95 5.70 4 -14 4 14.90 3.55 4 14 4 10.59 3.02 -4 14 -4 19.16 5.12 4 -14 4 14.48 3.78 4 14 4 22.02 6.07 -4 14 -4 15.53 4.02 4 -14 5 31.03 7.23 4 -14 5 22.26 4.68 4 14 5 15.54 3.96 4 -14 5 29.90 5.76 -4 14 -5 18.56 5.23 4 14 5 32.98 7.62 -4 14 -5 11.99 3.67 4 -14 6 32.82 8.00 4 -14 6 24.24 5.36 4 14 6 12.66 3.95 4 14 6 32.87 7.87 -4 14 -6 11.58 3.57 4 -14 7 5.00 3.98 4 -14 7 0.34 1.00 4 14 7 0.29 0.51 4 14 7 1.98 2.40 4 -14 8 5.67 4.24 4 -14 8 -0.30 0.30 4 14 8 0.59 1.30 4 14 8 6.43 4.34 4 -14 9 3.23 4.46 4 -14 9 1.85 2.12 4 14 9 0.71 1.27 4 14 9 4.12 3.51 4 14 10 -0.13 0.55 4 14 10 -0.04 0.45 4 14 11 -0.12 1.54 4 -14 11 2.12 2.95 -4 15 13 0.39 1.59 -4 -15 13 2.65 3.01 -4 -15 12 1.81 3.49 -4 15 12 0.93 1.38 -4 15 11 4.67 3.01 -4 -15 11 16.03 6.49 -4 -15 10 3.04 3.11 -4 15 10 1.44 2.02 -4 15 10 0.12 1.62 -4 -15 9 17.62 6.39 4 15 -9 16.69 6.48 -4 15 9 12.47 4.50 -4 15 9 13.77 4.66 -4 15 8 20.22 5.84 4 15 -8 21.19 6.82 -4 15 8 19.45 5.89 4 15 -7 2.50 1.70 -4 15 7 5.63 2.86 4 15 -6 76.52 11.71 -4 15 6 79.28 10.78 4 15 -5 61.66 10.16 -4 15 5 65.11 9.47 -4 15 5 60.49 9.31 -4 15 4 3.04 2.19 4 15 -4 0.90 2.39 -4 15 4 1.31 1.97 4 15 -3 54.68 9.00 -4 15 3 54.82 8.62 -4 15 3 38.70 7.15 -4 15 2 2.64 1.57 4 15 -2 0.25 2.41 -4 15 2 2.50 1.82 -4 15 1 4.63 2.83 -4 15 1 5.89 2.92 4 15 -1 6.66 3.39 4 15 0 45.15 8.32 -4 15 0 46.63 7.57 -4 15 0 40.64 6.98 -4 15 -1 148.07 13.39 -4 15 -1 129.21 12.32 4 15 1 157.85 15.68 -4 15 -2 150.48 13.99 -4 15 -2 146.08 12.92 4 15 2 167.49 16.69 4 -15 3 33.81 7.72 4 15 3 31.55 7.21 -4 15 -3 22.59 5.15 -4 15 -3 24.60 5.85 -4 15 -4 38.92 7.63 4 15 4 51.20 9.31 4 -15 4 62.56 10.24 4 15 5 6.52 3.62 -4 15 -5 0.65 1.20 -4 15 -5 0.86 1.21 4 -15 5 5.66 3.98 4 15 6 18.27 5.91 4 -15 6 26.22 7.53 -4 15 -6 7.39 2.95 4 15 7 2.39 3.38 4 -15 7 -0.57 0.42 4 -15 8 3.41 3.52 4 15 8 0.72 2.02 4 15 9 1.51 2.10 4 -15 9 1.28 1.83 4 -15 10 1.96 2.94 4 15 10 0.63 2.54 4 -15 11 5.53 4.58 -4 -16 13 13.18 6.20 -4 -16 12 1.81 2.15 -4 16 12 1.12 2.19 -4 16 12 0.77 1.44 -4 -16 11 13.08 6.35 -4 16 11 4.06 2.85 -4 16 11 3.52 3.05 -4 16 10 3.60 2.32 -4 16 10 3.29 2.89 4 16 -9 -1.03 1.84 -4 -16 9 0.14 1.32 -4 16 9 1.53 1.20 4 16 -8 55.23 10.99 -4 16 8 44.29 9.01 4 16 -7 -1.09 1.45 -4 16 7 -0.02 0.58 -4 16 6 6.62 2.67 4 16 -6 11.39 4.84 4 16 -5 3.70 2.21 -4 16 5 -0.21 1.24 -4 16 4 36.21 7.39 4 16 -4 43.14 8.50 -4 16 4 34.54 7.21 4 16 -3 182.23 17.15 -4 16 3 191.20 16.80 -4 16 3 164.28 15.34 4 16 -2 2.48 3.23 -4 16 2 0.37 0.74 -4 16 2 2.92 2.07 -4 16 1 241.32 18.35 4 16 -1 242.12 19.59 -4 16 1 205.71 16.75 -4 16 0 124.64 12.97 4 16 0 134.32 15.03 -4 16 0 127.53 12.75 -4 16 -1 71.69 9.86 4 16 1 71.72 11.37 -4 16 -1 65.80 9.20 4 16 2 19.47 6.37 -4 16 -2 18.41 5.29 -4 16 -2 14.25 4.33 -4 16 -3 3.42 1.70 4 16 3 6.49 3.76 -4 16 -3 3.62 2.21 4 -16 4 2.61 2.47 -4 16 -4 0.74 0.82 -4 16 -4 1.34 1.20 4 -16 5 2.56 2.97 -4 16 -5 0.29 0.59 4 16 5 2.47 2.78 -4 16 -5 -0.77 0.99 4 -16 6 4.84 3.51 -4 16 -6 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62.94 6.42 -5 4 1 57.83 5.85 5 -4 0 193.99 11.35 5 4 0 203.31 9.80 5 4 0 189.57 11.08 -5 4 0 169.25 10.10 5 -4 1 337.17 15.57 5 4 1 323.75 13.93 5 4 1 337.43 12.62 5 -4 1 277.43 8.00 5 4 1 321.77 14.44 -5 4 -1 315.97 14.27 -5 4 -2 56.83 6.25 5 -4 2 62.26 7.00 5 -4 2 50.00 5.93 5 4 2 62.82 6.56 5 4 2 53.98 6.05 5 4 2 61.81 5.79 5 -4 2 58.93 4.65 -5 4 -3 208.08 12.60 5 -4 3 230.28 14.24 5 -4 3 216.02 12.98 5 4 3 218.98 13.08 5 -4 3 203.06 7.42 5 4 3 241.73 12.26 5 4 3 205.66 12.21 -5 4 -4 208.74 13.11 5 -4 4 202.27 13.30 5 4 4 207.91 13.36 5 4 4 209.51 12.56 5 -4 4 220.19 9.70 5 4 5 60.92 6.94 -5 4 -5 57.57 7.13 5 -4 5 60.10 7.72 5 4 5 61.62 7.82 5 -4 5 59.07 5.57 5 -4 5 63.44 6.03 5 4 5 53.80 6.80 5 4 6 24.28 5.05 5 -4 6 21.23 4.80 -5 4 -6 22.27 4.46 5 4 6 22.92 4.33 5 -4 6 20.24 3.09 5 -4 6 23.95 4.20 5 4 6 23.34 4.62 5 -4 7 1.13 0.78 -5 4 -7 0.81 0.33 5 4 7 2.19 2.86 5 -4 7 1.01 1.56 5 4 7 2.07 1.37 5 -4 7 1.41 1.49 5 4 8 84.24 10.70 5 -4 8 98.26 12.16 5 4 8 93.72 11.69 5 -4 8 79.84 9.12 5 -4 9 47.60 8.94 5 4 9 40.51 8.33 5 -4 9 33.88 6.57 5 4 9 28.17 6.63 5 -4 10 3.19 2.22 -5 4 -10 1.58 1.54 5 -4 10 5.42 3.15 5 4 10 11.11 5.42 5 4 10 5.99 3.36 5 -4 11 3.47 2.67 5 4 11 5.61 4.42 5 4 11 2.23 2.02 5 -4 12 3.59 3.48 5 4 12 4.63 3.70 5 4 12 4.92 3.13 5 -4 13 3.26 4.41 5 4 13 1.90 2.15 5 4 13 -0.02 0.32 5 4 14 1.41 2.38 -5 -5 16 7.29 4.97 -5 5 16 4.88 3.90 -5 -5 15 -0.39 1.78 -5 5 15 1.53 2.65 -5 -5 14 27.81 7.96 -5 5 14 30.74 8.21 -5 -5 13 0.36 1.63 -5 5 13 1.64 1.98 -5 -5 12 12.03 4.17 -5 5 12 11.27 4.66 -5 -5 11 2.70 2.86 5 -5 -11 2.19 1.84 -5 5 11 2.89 2.86 -5 -5 10 18.96 4.74 5 -5 -10 18.28 4.18 -5 5 10 21.72 5.11 5 -5 -9 39.04 5.81 -5 5 9 38.05 6.39 -5 5 9 42.71 6.44 -5 -5 9 38.43 6.54 -5 5 8 6.83 2.48 -5 -5 8 6.36 3.16 -5 5 8 9.44 2.61 5 5 -8 6.60 2.80 -5 -5 8 5.95 1.16 -5 -5 7 56.12 7.43 5 5 -7 62.62 7.86 -5 -5 7 51.85 4.14 -5 5 7 49.82 6.36 -5 5 7 56.52 6.49 -5 -5 6 336.95 11.75 -5 -5 6 327.91 16.75 -5 5 6 317.80 15.09 5 5 -6 344.41 16.57 -5 5 6 301.90 14.32 -5 -5 5 13.37 2.58 -5 5 5 9.67 2.70 5 5 -5 12.86 3.15 -5 5 5 11.39 2.52 5 5 -5 13.11 3.09 5 -5 -4 128.90 7.71 5 5 -4 118.38 8.87 5 5 -4 123.93 9.17 -5 5 4 109.69 7.44 -5 5 4 110.73 8.43 5 -5 -3 273.20 11.85 -5 5 3 263.14 10.29 5 5 -3 289.49 13.42 -5 5 3 238.19 12.45 5 -5 -2 254.24 12.11 5 5 -2 271.27 13.44 5 5 -2 250.44 11.59 -5 5 2 241.61 8.15 -5 5 2 254.46 9.02 -5 5 2 231.61 12.06 5 -5 -2 290.60 9.60 5 5 -1 7.77 1.78 -5 5 1 7.89 2.27 5 -5 -1 6.74 0.95 5 5 -1 8.74 2.29 5 -5 -1 8.06 2.22 -5 5 1 10.67 1.71 5 -5 0 607.56 20.44 5 5 0 672.68 19.28 -5 5 0 698.44 13.17 -5 5 0 574.53 19.11 5 5 0 584.31 19.57 5 -5 1 40.66 5.47 5 -5 1 34.00 3.29 5 5 1 49.50 5.29 5 5 1 45.21 5.75 -5 5 -1 38.60 5.10 5 -5 2 48.11 6.10 5 -5 2 49.21 5.88 5 5 2 49.95 5.98 5 5 2 47.68 5.34 5 -5 2 52.54 4.91 5 5 2 43.78 5.32 -5 5 -2 49.33 5.97 5 -5 3 60.95 7.25 5 -5 3 62.90 7.17 5 5 3 62.26 7.04 5 5 3 61.28 6.47 5 5 3 63.69 7.04 5 -5 3 66.03 4.15 -5 5 -3 58.25 6.58 5 -5 4 37.25 5.81 5 5 4 39.06 6.03 5 -5 4 40.26 6.19 5 -5 4 39.74 4.02 5 5 4 41.52 5.81 -5 5 -4 36.85 5.48 5 -5 5 31.22 5.59 5 5 5 29.60 5.41 5 5 5 31.11 4.90 5 -5 5 32.93 4.28 5 -5 5 36.91 6.60 -5 5 -5 30.51 5.24 5 -5 6 3.15 1.96 -5 5 -6 3.27 1.38 5 5 6 7.27 3.20 5 5 6 0.84 0.80 5 -5 6 3.43 1.28 5 -5 6 3.03 1.52 5 5 6 2.28 1.56 -5 5 -7 1.32 1.88 5 5 7 3.99 2.92 5 -5 7 -0.93 1.71 5 5 7 0.68 0.97 5 -5 7 2.86 1.75 -5 5 -8 2.89 2.00 5 -5 8 3.84 2.79 5 5 8 4.59 2.78 5 5 8 6.48 3.46 5 -5 8 3.34 1.93 -5 5 -9 -0.37 0.92 5 -5 9 2.14 1.62 5 -5 9 1.83 1.66 5 5 9 0.02 0.63 5 5 9 1.68 1.35 5 5 10 15.01 5.34 5 -5 10 16.96 5.74 5 5 10 16.57 5.41 5 -5 10 6.56 3.14 5 5 11 4.81 3.02 5 -5 11 11.21 4.53 5 5 11 8.45 4.53 5 -5 12 3.35 2.38 5 5 12 0.70 1.21 5 5 12 1.62 2.00 5 -5 13 0.53 1.72 5 5 13 1.76 2.46 5 5 14 0.02 0.30 -5 -6 16 4.09 3.05 -5 6 16 3.77 2.98 -5 -6 15 2.66 2.25 -5 6 15 3.03 2.89 -5 -6 14 2.39 2.61 -5 6 14 4.16 3.58 -5 -6 13 2.14 2.82 -5 6 13 1.13 2.19 -5 -6 12 -1.38 0.99 -5 6 12 0.11 1.31 -5 6 11 81.63 11.15 -5 -6 11 82.62 10.93 -5 -6 10 4.48 2.80 5 -6 -10 1.65 1.49 -5 6 10 1.74 2.21 -5 -6 9 40.70 7.09 5 -6 -9 37.84 5.60 -5 6 9 43.18 7.12 -5 6 9 44.41 6.93 -5 -6 8 0.70 1.81 -5 -6 8 0.64 0.44 -5 6 8 0.69 1.51 -5 6 8 1.74 1.87 -5 6 7 165.70 12.00 -5 -6 7 160.58 12.51 5 6 -7 173.96 12.82 -5 6 7 161.73 11.49 -5 -6 7 155.25 7.30 -5 -6 6 0.88 0.82 5 6 -6 -0.21 1.43 5 -6 -6 0.42 0.64 5 6 -6 -0.87 1.03 -5 6 6 0.10 0.71 -5 6 6 0.04 1.27 5 -6 -5 6.61 1.74 5 6 -5 5.22 2.36 5 6 -5 5.67 2.26 -5 -6 5 6.99 1.96 5 6 -5 3.30 1.59 -5 6 5 4.06 1.65 -5 6 5 4.41 1.63 5 -6 -4 843.08 20.66 5 6 -4 764.78 23.65 -5 6 4 781.20 20.77 5 6 -4 741.68 22.91 5 6 -4 850.99 24.92 5 6 -3 307.84 14.72 5 6 -3 305.14 14.29 5 6 -3 266.01 13.22 -5 6 3 277.14 10.80 -5 6 3 245.50 12.73 5 -6 -3 292.53 12.78 -5 6 2 13.32 3.05 5 -6 -2 15.16 2.97 5 6 -2 14.90 3.30 5 -6 -2 16.88 2.60 5 6 -2 14.25 2.77 -5 6 2 14.53 2.13 -5 6 2 16.45 2.45 -5 6 1 6.87 2.57 5 -6 -1 3.35 0.81 5 -6 -1 9.80 2.57 5 6 -1 3.48 1.78 5 6 -1 4.08 1.58 -5 6 1 6.06 1.39 5 -6 0 344.28 15.75 -5 6 0 367.62 11.14 5 6 0 349.52 14.84 5 6 0 307.18 14.84 -5 6 0 304.50 14.34 5 -6 1 17.76 2.71 -5 6 -1 15.27 3.30 5 6 1 14.07 2.80 5 -6 1 14.75 3.52 -5 6 -1 14.29 2.42 5 6 1 17.53 3.32 5 -6 2 189.97 12.93 5 -6 2 186.74 11.36 5 6 2 189.32 11.62 -5 6 -2 180.49 11.46 5 6 2 195.68 11.37 5 6 2 183.88 11.90 5 -6 3 81.88 8.59 5 -6 3 85.92 8.26 5 6 3 87.52 8.44 5 6 3 89.25 8.15 5 -6 3 79.90 4.47 -5 6 -3 85.45 8.11 5 6 3 84.45 8.22 -5 6 -4 0.70 1.00 5 6 4 1.54 1.02 5 -6 4 2.26 1.45 5 6 4 0.67 1.40 5 -6 4 4.81 2.25 5 6 4 1.33 1.15 5 -6 4 2.70 1.12 5 6 5 40.95 6.20 5 -6 5 39.21 6.22 5 6 5 42.97 6.55 5 -6 5 41.29 6.93 5 -6 5 36.05 4.36 -5 6 -5 43.31 6.20 5 -6 6 65.26 9.47 5 6 6 54.95 7.40 5 -6 6 51.90 7.78 5 6 6 59.92 8.35 5 -6 6 52.09 5.80 5 -6 6 47.15 4.56 -5 6 -6 47.17 6.69 5 -6 7 21.58 5.65 5 6 7 19.95 5.00 5 -6 7 25.90 6.29 5 6 7 20.86 5.36 5 -6 7 15.73 3.57 -5 6 -7 15.70 4.08 -5 6 -8 7.57 2.79 5 -6 8 13.32 4.60 5 6 8 18.75 5.18 5 6 8 14.53 4.40 5 -6 8 13.66 3.64 -5 6 -9 5.95 2.73 5 -6 9 15.44 5.51 5 6 9 15.11 5.40 5 6 9 12.84 4.62 5 -6 9 12.00 3.89 5 6 10 0.46 1.82 5 -6 10 1.58 2.31 5 6 10 2.64 2.76 5 -6 11 -0.34 1.75 5 6 11 -1.11 1.06 5 6 11 0.13 0.72 5 6 12 0.56 1.46 5 -6 12 3.74 2.33 5 6 12 2.58 2.67 5 -6 13 1.25 2.13 5 6 13 -0.58 1.52 5 6 14 7.36 4.74 -5 -7 16 4.84 3.59 -5 7 16 3.57 3.95 -5 -7 15 0.23 0.70 -5 7 15 2.97 3.10 -5 -7 14 8.33 4.49 -5 7 14 6.93 4.02 -5 7 13 4.35 3.74 -5 -7 13 0.95 0.88 -5 -7 12 0.75 0.71 -5 7 12 0.93 1.68 5 7 -11 0.55 0.78 -5 -7 11 1.60 2.50 -5 7 11 2.12 1.58 5 -7 -11 1.41 1.30 -5 7 10 4.83 2.65 5 7 -10 3.17 1.85 -5 -7 10 4.29 2.58 5 -7 -10 2.36 1.46 5 7 -9 0.95 1.12 -5 -7 9 -0.88 1.66 5 -7 -9 1.15 1.07 -5 7 9 0.82 1.94 -5 7 9 1.65 1.94 -5 -7 8 34.74 6.27 -5 7 8 43.34 6.62 -5 7 8 39.36 6.42 5 7 -8 39.49 5.76 -5 -7 8 20.54 2.06 -5 -7 7 20.04 2.67 -5 -7 7 21.80 4.78 -5 7 7 24.62 4.75 5 7 -7 23.15 4.47 5 -7 -7 7.49 1.56 -5 7 7 18.84 4.10 5 7 -7 23.70 4.94 5 7 -6 50.78 7.21 -5 -7 6 41.98 4.39 -5 7 6 41.82 5.72 5 7 -6 40.74 6.04 -5 7 6 32.77 5.42 5 7 -6 49.39 6.37 5 -7 -6 33.34 3.81 5 7 -5 29.03 4.68 -5 7 5 25.61 4.17 5 7 -5 27.77 5.02 5 7 -5 25.99 4.71 -5 7 5 22.57 4.39 5 -7 -5 25.54 3.54 -5 7 4 104.36 7.65 5 7 -4 119.24 9.88 5 7 -4 105.87 8.84 5 7 -4 119.53 9.34 -5 7 4 93.21 8.43 5 -7 -4 110.08 7.80 5 7 -3 31.35 4.77 5 7 -3 32.54 4.96 5 7 -3 34.29 4.84 5 -7 -3 20.96 3.74 -5 7 3 31.72 3.85 -5 7 3 25.93 4.36 5 -7 -3 30.35 4.36 -5 7 3 37.07 4.47 5 -7 -2 7.91 2.03 5 7 -2 4.05 1.41 5 7 -2 6.13 1.91 5 -7 -2 5.29 1.87 5 7 -2 4.01 1.53 -5 7 2 5.62 1.63 -5 7 2 4.36 1.87 5 7 -1 75.93 7.26 5 7 -1 79.17 7.64 -5 7 1 89.41 6.35 5 -7 -1 74.74 4.67 -5 7 1 71.25 7.12 5 -7 -1 80.74 7.52 -5 7 0 11.55 3.11 5 -7 0 14.20 3.54 -5 7 0 9.94 1.96 5 7 0 14.13 3.24 5 -7 0 10.02 1.24 5 -7 0 9.36 2.22 5 7 0 12.69 3.22 5 7 1 432.18 17.67 5 7 1 404.33 17.81 -5 7 -1 417.40 17.91 -5 7 -1 478.88 14.81 5 -7 1 434.41 19.18 5 -7 2 80.78 8.53 -5 7 -2 71.14 6.14 5 -7 2 69.93 7.04 5 7 2 74.42 7.39 -5 7 -2 71.65 7.45 5 7 2 79.26 7.67 5 -7 2 72.97 3.46 5 7 2 77.05 7.91 -5 7 -3 1.72 1.18 5 -7 3 1.83 1.66 5 7 3 1.31 0.78 5 -7 3 0.48 0.65 5 7 3 1.75 1.43 5 7 3 0.71 0.78 5 -7 3 1.07 0.68 5 -7 4 86.80 9.60 5 7 4 75.82 8.37 5 -7 4 78.64 8.50 5 7 4 79.60 8.47 5 -7 4 67.66 5.21 5 7 4 81.57 8.68 -5 7 -4 78.25 8.12 -5 7 -5 1.56 1.37 5 -7 5 3.86 2.33 5 7 5 1.64 1.95 5 -7 5 3.92 2.38 5 7 5 1.19 2.03 5 -7 5 1.00 0.84 5 7 5 1.57 1.63 -5 7 -6 7.08 2.67 5 -7 6 7.05 3.11 5 7 6 9.72 3.70 5 -7 6 11.44 4.42 5 -7 6 6.87 2.01 -5 7 -7 -0.18 0.68 5 -7 7 0.56 2.15 5 -7 7 2.10 2.32 5 7 7 3.72 1.90 5 -7 7 -0.11 0.70 -5 7 -8 0.49 0.58 5 -7 8 2.34 1.38 5 7 8 1.47 2.09 5 7 8 1.35 1.06 5 -7 8 1.66 1.02 5 -7 8 0.70 0.99 5 7 9 2.34 2.86 -5 7 -9 0.14 0.84 5 -7 9 4.25 3.23 5 7 9 2.59 2.79 5 7 10 6.83 3.86 5 -7 10 12.42 5.00 5 7 10 12.95 5.15 5 -7 11 6.54 3.87 5 7 11 3.11 2.75 5 7 11 11.37 4.81 5 -7 12 1.60 1.87 5 7 12 1.79 2.25 5 7 12 5.68 4.09 5 -7 13 0.69 1.45 5 7 13 1.87 2.77 -5 -8 15 0.32 1.57 -5 8 15 2.56 3.24 -5 -8 14 2.69 2.29 -5 8 14 0.52 2.23 -5 8 13 1.68 2.70 -5 -8 13 -1.56 1.30 -5 -8 12 8.32 4.03 -5 8 12 15.05 5.28 -5 -8 11 1.79 2.61 5 -8 -11 0.11 0.72 -5 8 11 -0.55 1.51 -5 -8 10 7.15 3.49 -5 8 10 5.06 3.33 5 8 -10 4.17 2.00 5 -8 -10 2.75 1.53 -5 -8 9 32.29 6.81 5 8 -9 31.08 5.13 5 -8 -9 26.86 4.53 -5 8 9 38.74 6.93 -5 8 9 32.79 6.41 -5 -8 8 28.05 5.92 5 -8 -8 8.16 1.49 5 8 -8 33.70 5.31 -5 8 8 31.36 6.05 -5 8 8 29.39 5.73 -5 -8 8 12.63 1.59 -5 -8 7 34.45 3.76 5 8 -7 39.06 6.71 -5 8 7 39.79 6.22 5 8 -7 35.34 5.48 -5 8 7 37.04 5.91 5 8 -6 66.20 8.60 -5 8 6 58.46 6.94 5 8 -6 58.89 6.85 -5 8 6 56.99 7.20 5 8 -6 51.45 6.92 5 -8 -6 54.11 5.04 5 8 -5 64.16 7.76 -5 8 5 61.83 6.45 5 8 -5 65.77 7.81 -5 8 5 49.82 6.45 5 8 -5 60.05 6.86 5 -8 -5 60.24 5.74 -5 8 4 96.00 8.02 5 8 -4 100.43 9.48 -5 8 4 84.88 7.20 5 8 -4 93.19 8.82 -5 8 4 79.30 7.93 5 8 -4 93.78 8.51 5 -8 -4 93.51 7.55 -5 8 3 111.93 7.55 5 8 -3 115.92 9.59 5 8 -3 127.40 9.60 -5 8 3 119.87 8.32 -5 8 3 107.41 9.03 5 8 -3 123.22 9.89 5 -8 -3 128.45 9.28 -5 8 2 153.64 10.70 5 8 -2 169.21 11.33 5 8 -2 171.24 10.78 5 -8 -2 135.48 8.53 -5 8 2 157.88 9.29 5 8 -2 163.41 11.36 5 -8 -2 190.89 11.66 5 8 -1 8.64 2.36 5 8 -1 9.38 2.79 5 -8 -1 10.27 3.07 5 8 -1 11.58 3.01 -5 8 1 13.27 2.73 5 -8 -1 10.18 1.96 -5 8 1 10.17 2.83 -5 8 0 291.55 12.02 5 8 0 297.76 15.54 5 -8 0 270.25 8.72 -5 8 0 267.04 14.63 5 8 0 276.23 14.93 5 -8 0 295.48 15.58 5 -8 1 67.81 3.74 -5 8 -1 66.90 6.12 5 -8 1 56.33 3.54 5 8 1 70.33 7.62 -5 8 -1 56.95 6.79 5 8 1 70.93 7.76 5 -8 1 58.46 7.39 5 -8 2 144.25 11.88 5 -8 2 131.70 9.65 5 8 2 131.42 9.70 5 8 2 142.53 10.86 5 -8 2 144.50 5.72 -5 8 -2 140.18 10.92 5 8 2 131.42 10.86 -5 8 -2 159.67 9.90 -5 8 -3 5.53 2.26 5 -8 3 5.37 1.34 5 8 3 6.67 2.86 5 -8 3 5.99 2.52 5 8 3 6.38 2.48 5 -8 3 4.59 1.08 5 8 3 7.02 2.63 5 8 4 35.40 5.98 5 -8 4 35.71 5.85 5 8 4 34.63 5.80 5 -8 4 35.90 6.70 5 8 4 34.12 5.82 5 -8 4 34.18 3.97 -5 8 -4 34.54 5.51 5 -8 5 9.67 2.35 -5 8 -5 10.30 3.08 5 -8 5 10.20 3.78 5 -8 5 8.02 3.03 5 8 5 7.46 2.96 5 8 5 11.46 3.39 5 8 5 5.74 2.71 5 -8 6 73.92 10.15 5 -8 6 63.31 8.72 5 8 6 64.03 8.71 5 8 6 70.08 9.51 5 -8 6 59.68 6.30 -5 8 -6 53.09 7.20 5 -8 7 88.90 11.80 5 -8 7 75.87 10.41 5 8 7 78.39 10.24 5 -8 7 59.08 6.85 -5 8 -8 10.43 3.48 5 8 8 24.49 6.29 5 -8 8 31.32 7.00 5 -8 8 32.82 7.95 5 -8 9 5.70 3.58 5 8 9 4.54 3.17 5 -8 9 5.25 3.19 5 8 9 6.58 3.84 5 -8 10 3.91 3.10 5 8 10 2.02 2.28 5 8 10 2.53 1.85 5 -8 11 3.74 3.43 5 8 11 0.55 1.59 5 8 11 0.31 1.85 5 8 12 -0.84 1.41 5 8 12 0.26 2.38 5 -8 12 2.16 2.98 5 -8 13 1.81 3.21 5 8 13 2.19 3.36 -5 -9 15 -1.25 1.69 -5 9 15 2.69 2.71 -5 -9 14 13.46 6.18 -5 9 14 11.28 5.24 -5 -9 13 19.62 6.50 -5 9 13 20.88 6.55 -5 -9 12 12.22 4.50 -5 9 12 15.95 5.76 -5 -9 11 1.02 2.03 -5 9 11 -1.58 1.97 -5 -9 10 11.29 3.89 5 -9 -10 5.68 2.17 5 9 -10 5.35 2.06 -5 9 10 13.81 4.53 -5 -9 9 2.61 2.77 5 -9 -9 0.19 0.76 5 9 -9 0.27 0.58 -5 9 9 1.09 1.31 -5 9 9 2.48 2.28 -5 -9 8 92.29 10.92 5 9 -8 84.70 8.59 -5 9 8 97.92 10.53 -5 9 8 93.23 10.51 5 -9 -8 43.07 4.09 5 9 -7 83.92 8.51 -5 -9 7 83.65 6.03 -5 9 7 90.30 9.35 5 9 -7 94.39 10.95 -5 9 7 87.67 9.73 5 9 -6 66.64 8.88 -5 9 6 62.11 7.71 -5 9 6 64.18 7.51 5 9 -6 58.15 6.99 5 -9 -6 56.09 5.76 -5 9 5 3.21 1.88 5 -9 -5 0.69 0.78 5 9 -5 1.15 1.05 5 9 -5 0.11 1.64 5 9 -5 -0.70 1.64 -5 9 5 0.92 1.08 5 9 -4 23.33 4.48 5 -9 -4 24.84 4.11 -5 9 4 24.96 4.06 5 9 -4 28.23 5.26 -5 9 4 25.65 4.23 5 9 -4 29.07 5.17 -5 9 4 20.06 4.20 5 -9 -3 0.74 1.35 -5 9 3 0.86 0.74 5 9 -3 -0.17 1.21 -5 9 3 1.85 1.90 5 9 -3 -0.17 1.18 5 9 -3 -2.41 1.72 5 9 -2 7.12 2.60 5 -9 -2 3.48 1.51 5 9 -2 4.72 2.16 -5 9 2 1.91 1.14 5 9 -2 3.22 1.15 5 -9 -2 1.79 1.03 -5 9 2 2.63 2.02 5 9 -1 180.17 12.66 -5 9 1 190.77 10.96 5 9 -1 170.90 10.70 -5 9 1 163.45 11.47 5 9 -1 154.59 11.65 5 -9 -1 193.81 12.89 5 -9 0 26.01 4.81 -5 9 0 19.66 3.51 5 -9 0 24.35 3.17 5 9 0 23.82 4.61 5 9 0 29.40 5.30 5 9 0 23.67 3.97 -5 9 0 22.22 4.36 -5 9 -1 219.53 11.85 5 -9 1 198.71 8.16 5 9 1 245.21 15.16 -5 9 -1 220.38 13.63 5 -9 1 243.31 15.22 5 9 1 231.21 11.61 5 9 1 225.62 14.32 5 9 2 104.65 9.85 5 -9 2 112.84 6.14 -5 9 -2 85.90 7.86 5 9 2 109.69 9.99 -5 9 -2 103.91 9.52 5 -9 2 120.48 11.03 5 -9 3 3.87 1.32 -5 9 -3 2.50 1.45 5 -9 3 4.44 1.50 5 -9 3 3.11 1.91 5 9 3 3.99 1.96 5 9 3 3.74 2.16 5 9 3 1.78 2.29 -5 9 -3 2.25 1.33 5 9 4 83.05 9.57 5 -9 4 91.85 9.42 5 9 4 90.52 9.32 5 9 4 93.77 10.14 5 -9 4 81.93 6.33 -5 9 -4 86.95 9.09 5 -9 4 94.91 10.49 5 -9 5 5.16 2.77 5 9 5 3.03 1.47 5 -9 5 6.71 3.07 5 -9 5 4.21 1.70 -5 9 -5 2.69 1.71 5 9 5 2.35 1.34 5 -9 6 5.16 1.96 -5 9 -6 3.71 2.28 5 -9 6 4.84 2.48 5 9 6 3.85 2.40 5 -9 6 6.93 4.18 5 9 6 5.95 3.01 -5 9 -7 1.28 1.58 5 -9 7 2.88 2.53 5 9 7 3.64 2.42 5 -9 7 4.48 3.10 5 9 7 4.21 2.90 -5 9 -8 2.88 1.85 5 -9 8 12.13 4.65 5 9 8 4.05 2.44 5 -9 8 10.43 4.81 5 -9 9 9.00 4.52 5 9 9 4.37 2.89 5 -9 9 8.79 5.17 5 -9 10 0.55 2.08 5 9 10 1.81 1.21 5 -9 11 4.94 3.51 5 9 11 1.74 1.90 5 -9 12 9.39 5.44 5 9 12 3.92 3.35 -5 -10 15 3.91 4.25 -5 10 15 4.01 3.14 -5 -10 14 -0.14 1.60 -5 10 14 0.02 0.63 -5 -10 13 -0.43 0.51 -5 10 13 0.19 1.41 -5 10 12 53.87 9.89 -5 -10 12 56.28 10.28 -5 -10 11 11.03 4.62 -5 10 11 8.83 3.65 5 10 -10 0.70 0.86 -5 -10 10 1.45 1.70 -5 10 10 0.90 1.64 -5 -10 9 20.45 5.26 -5 10 9 18.71 4.68 5 -10 -9 10.71 2.95 5 10 -9 9.53 3.03 5 -10 -8 14.76 2.75 5 10 -8 32.30 6.95 -5 10 8 28.59 5.68 -5 -10 8 29.38 6.54 -5 10 8 32.09 6.57 5 10 -8 29.56 5.26 5 -10 -7 11.44 2.61 5 10 -7 26.56 6.20 -5 10 7 21.72 4.88 -5 10 7 22.91 5.32 5 10 -7 22.63 4.55 -5 10 6 86.01 9.06 5 10 -6 91.97 10.74 5 10 -6 91.28 9.31 -5 10 6 92.15 9.83 5 -10 -6 96.79 8.06 5 10 -5 2.50 1.93 5 -10 -5 1.27 1.37 -5 10 5 0.55 0.81 -5 10 5 0.21 1.20 -5 10 5 0.64 1.75 5 10 -5 0.99 1.33 5 10 -4 3.53 2.52 5 -10 -4 1.27 0.92 5 10 -4 0.20 1.03 -5 10 4 2.15 1.47 -5 10 4 1.60 1.21 -5 10 4 1.51 1.15 5 10 -4 -0.51 0.57 5 10 -3 170.27 12.25 5 10 -3 156.58 12.56 -5 10 3 148.13 10.38 -5 10 3 146.17 11.42 5 10 -3 168.78 12.29 5 -10 -3 170.23 11.97 5 10 -2 54.92 7.38 -5 10 2 61.01 6.73 -5 10 2 54.04 6.88 5 -10 -2 63.91 7.57 5 10 -2 61.79 7.42 5 10 -2 60.73 7.06 -5 10 1 171.76 11.10 5 10 -1 181.41 13.29 5 10 -1 181.36 11.53 -5 10 1 159.87 11.73 5 -10 -1 188.11 13.51 5 10 -1 171.80 12.59 -5 10 0 222.18 13.95 5 10 0 245.73 12.48 -5 10 0 208.93 11.82 5 10 0 243.64 15.69 5 -10 0 274.62 16.63 5 10 0 235.76 15.06 5 -10 1 18.56 4.63 5 10 1 11.77 3.17 -5 10 -1 11.27 2.83 -5 10 -1 14.93 3.73 5 -10 1 6.99 1.77 5 10 1 11.56 3.74 5 10 1 15.96 3.08 5 10 2 240.82 15.43 5 -10 2 242.81 9.98 -5 10 -2 238.08 13.44 5 10 2 240.85 11.58 5 10 2 279.87 17.18 5 -10 2 280.55 17.66 -5 10 -2 259.02 15.32 5 -10 3 10.03 3.71 5 -10 3 7.49 1.78 5 -10 3 11.28 3.26 5 10 3 9.75 2.89 -5 10 -3 7.44 2.39 5 10 3 6.95 1.63 5 10 3 14.57 4.16 5 10 3 10.91 3.58 -5 10 -3 7.83 2.42 -5 10 -4 6.58 2.39 5 -10 4 9.72 2.34 5 -10 4 14.68 4.55 5 -10 4 12.54 3.48 5 10 4 11.00 3.27 5 10 4 11.36 3.80 5 10 4 12.49 4.14 5 -10 5 12.70 2.80 5 -10 5 18.43 5.16 5 -10 5 12.92 3.80 5 10 5 15.83 4.36 -5 10 -5 13.82 3.79 5 10 5 17.61 4.73 -5 10 -6 8.83 3.05 5 -10 6 17.01 4.66 5 10 6 25.80 5.70 5 -10 6 20.49 5.82 5 10 6 25.11 6.13 -5 10 -7 0.15 0.57 5 -10 7 1.08 1.62 5 10 7 0.17 0.18 5 -10 7 2.26 2.08 5 10 7 2.66 2.04 5 -10 8 26.62 6.48 5 10 8 23.28 6.01 5 -10 8 43.14 9.42 5 10 8 37.89 8.64 5 -10 9 17.24 5.82 5 10 9 7.30 3.58 5 -10 9 22.53 7.21 5 10 9 16.91 6.07 5 -10 10 0.95 2.58 5 10 10 0.06 0.71 5 -10 10 1.44 1.93 5 -10 11 4.47 3.58 5 10 11 1.05 1.69 5 -10 12 2.88 3.04 5 10 12 2.14 3.05 -5 -11 15 0.59 1.39 -5 11 15 0.57 0.50 -5 -11 14 4.93 3.80 -5 11 14 0.96 1.09 -5 -11 13 2.98 3.81 -5 11 13 0.63 0.37 -5 11 12 45.59 9.36 -5 -11 12 59.03 11.20 -5 -11 11 1.49 2.06 -5 11 11 1.20 2.03 -5 -11 10 34.41 8.07 -5 11 10 26.41 6.41 5 11 -9 -0.13 0.51 -5 -11 9 1.40 2.41 -5 11 9 1.39 2.06 -5 11 8 94.65 10.79 5 11 -8 106.10 12.82 -5 11 8 96.52 11.25 5 11 -8 77.09 8.69 5 -11 -7 2.85 1.57 5 11 -7 4.90 1.96 5 11 -7 7.55 3.38 -5 11 7 5.65 2.51 -5 11 7 6.96 3.41 5 11 -6 60.74 8.94 -5 11 6 58.27 7.51 -5 11 6 64.16 8.33 -5 11 6 61.42 8.43 5 11 -6 57.87 7.58 5 11 -5 19.74 4.77 5 11 -5 18.86 4.99 -5 11 5 18.63 4.34 -5 11 5 14.95 4.24 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72.09 9.82 -5 11 -4 52.07 7.39 5 -11 4 55.36 5.66 5 -11 4 77.84 10.23 5 -11 5 4.21 1.77 5 -11 5 4.21 2.58 5 -11 5 4.47 2.58 5 11 5 3.64 2.36 5 11 5 3.40 2.20 -5 11 -5 2.33 1.82 5 -11 6 -0.42 0.80 5 11 6 0.61 0.55 5 11 6 -0.33 0.56 -5 11 -6 0.01 0.59 5 -11 7 3.21 2.71 5 11 7 1.51 1.58 5 -11 7 7.29 4.21 5 11 7 2.10 2.64 -5 11 -7 0.56 0.76 5 -11 8 0.29 0.84 5 11 8 0.02 0.70 5 -11 8 -0.21 1.68 5 11 8 0.04 1.21 5 -11 9 3.04 2.89 5 11 9 0.74 1.25 5 -11 9 3.95 3.58 5 11 9 1.09 1.46 5 -11 10 5.07 3.42 5 11 10 0.63 1.08 5 -11 10 7.75 5.55 5 11 10 4.91 3.54 5 -11 11 0.90 0.64 5 -11 11 1.70 2.31 5 11 11 -0.13 0.93 5 -11 12 -0.11 1.51 5 11 12 3.03 2.98 5 11 12 0.39 0.62 -5 -12 14 0.13 1.50 -5 12 14 0.34 0.58 -5 -12 13 -1.01 2.07 -5 12 13 2.19 1.43 -5 -12 12 23.80 7.32 -5 12 12 14.11 5.28 -5 -12 11 22.20 6.83 -5 12 11 23.22 6.51 -5 -12 10 58.76 10.90 -5 12 10 50.12 9.23 -5 12 9 12.24 4.44 5 12 -9 3.59 2.22 -5 -12 9 12.60 4.84 5 12 -8 0.88 0.87 -5 12 8 1.16 1.68 5 12 -8 0.93 0.95 -5 12 8 1.18 2.91 5 12 -7 17.40 4.47 5 12 -7 25.96 6.44 -5 12 7 22.34 5.24 -5 12 7 30.09 6.48 -5 12 7 22.59 5.53 5 12 -6 20.18 5.50 -5 12 6 21.30 4.80 5 12 -6 20.52 4.69 -5 12 6 28.56 6.04 -5 12 6 24.45 5.66 5 12 -5 17.66 4.98 -5 12 5 15.28 3.80 5 12 -5 18.24 4.72 -5 12 5 15.97 4.28 -5 12 5 18.93 4.84 -5 12 4 5.25 2.26 5 12 -4 8.07 3.45 5 12 -4 6.16 2.58 -5 12 4 7.36 3.03 5 12 -3 32.23 6.38 -5 12 3 28.77 5.29 -5 12 3 30.06 5.72 5 12 -3 27.67 5.68 5 -12 -2 7.84 2.27 5 12 -2 12.80 3.24 5 12 -2 9.80 3.16 -5 12 2 8.87 2.95 -5 12 2 9.13 2.80 5 12 -1 188.78 15.15 5 12 -1 182.12 13.89 -5 12 1 182.06 12.88 -5 12 1 174.59 13.36 5 -12 -1 207.20 15.35 5 12 0 254.73 16.63 5 12 0 306.28 19.50 -5 12 0 270.20 15.18 5 12 0 257.78 13.77 -5 12 0 258.10 16.04 5 -12 0 304.79 19.24 5 12 1 83.52 9.69 5 12 1 79.64 7.31 -5 12 -1 70.64 7.88 5 12 1 99.78 11.40 -5 12 -1 83.11 9.26 5 -12 1 95.42 11.31 5 12 2 183.20 14.53 5 12 2 194.23 16.02 5 12 2 155.07 9.54 -5 12 -2 174.19 13.04 -5 12 -2 168.79 13.14 5 -12 2 162.00 14.96 5 -12 3 25.86 6.18 5 12 3 18.50 3.11 5 -12 3 18.58 3.47 -5 12 -3 21.33 4.88 5 12 3 24.81 6.14 -5 12 -3 18.18 4.29 5 -12 4 35.59 7.11 5 -12 4 29.71 5.41 5 12 4 18.75 4.33 -5 12 -4 24.93 5.29 -5 12 -4 27.70 5.44 5 -12 4 25.98 4.10 5 12 4 34.12 7.13 5 -12 5 41.11 7.91 5 12 5 36.00 7.40 5 -12 5 29.98 6.03 5 12 5 16.09 4.27 -5 12 -5 17.14 4.29 5 -12 6 24.84 5.93 5 12 6 17.92 4.87 5 12 6 29.62 7.08 -5 12 -6 10.28 3.52 5 -12 7 2.60 2.12 5 12 7 0.37 1.02 5 -12 7 3.11 4.08 5 12 7 3.09 3.04 -5 12 -7 0.80 1.18 5 -12 8 2.85 2.66 5 12 8 0.87 1.24 5 -12 8 6.04 3.96 5 12 8 3.48 2.94 5 -12 9 -1.28 1.30 5 12 9 -0.52 1.11 5 12 9 0.17 0.96 5 12 10 0.42 1.12 5 -12 10 -1.75 2.04 5 12 10 -0.74 1.39 5 -12 10 3.66 5.41 5 -12 11 1.53 1.88 5 12 11 1.88 1.76 5 -12 11 1.41 2.86 5 12 11 3.47 3.17 5 -12 12 3.26 3.22 5 12 12 0.38 0.57 5 12 12 0.65 1.33 -5 -13 14 9.90 5.26 -5 13 14 4.48 3.89 -5 -13 13 1.09 1.68 -5 13 13 0.04 1.02 -5 -13 12 19.89 6.95 -5 13 12 8.27 4.08 -5 -13 11 -2.20 3.13 -5 13 11 3.07 2.65 -5 -13 10 16.01 6.16 -5 13 10 12.64 4.84 5 13 -9 31.17 5.88 5 13 -9 59.22 10.36 -5 -13 9 63.64 10.87 -5 13 9 49.85 8.87 -5 13 8 38.71 7.40 5 13 -8 13.51 3.89 5 13 -8 37.31 8.14 -5 13 8 42.26 7.89 5 13 -7 10.26 3.55 5 13 -7 8.83 4.04 -5 13 7 7.69 3.24 -5 13 7 10.21 3.91 -5 13 7 10.17 3.95 5 13 -6 7.24 3.19 -5 13 6 7.26 2.96 -5 13 6 6.79 2.86 -5 13 6 9.40 3.91 5 13 -6 4.74 2.86 5 13 -5 2.14 2.75 5 13 -5 -0.08 1.58 -5 13 5 1.02 1.47 -5 13 5 2.23 1.58 5 13 -4 14.48 4.16 5 13 -4 11.72 4.15 -5 13 4 11.93 3.43 -5 13 4 12.40 3.73 5 13 -3 0.32 0.17 5 13 -3 3.93 2.83 -5 13 3 1.72 1.35 -5 13 3 2.13 2.14 5 13 -2 97.26 10.47 5 13 -2 101.68 11.36 -5 13 2 93.82 9.86 -5 13 2 92.76 10.28 5 13 -1 67.95 8.79 5 13 -1 69.68 9.48 -5 13 1 68.37 8.33 -5 13 1 57.76 8.07 5 -13 -1 75.57 9.44 5 -13 0 36.82 7.32 5 13 0 31.34 6.20 -5 13 0 21.59 4.60 5 13 0 33.99 6.93 -5 13 0 35.21 6.33 5 13 1 268.21 17.74 -5 13 -1 255.48 16.03 5 13 1 268.02 19.44 -5 13 -1 237.71 16.15 5 -13 1 303.57 20.56 -5 13 -2 269.11 17.37 5 13 2 300.00 20.89 5 -13 2 317.17 21.37 5 -13 3 70.58 7.09 -5 13 -3 78.13 9.26 -5 13 -3 61.94 8.49 5 13 3 92.08 11.82 5 -13 3 99.33 12.29 5 13 4 111.64 13.25 5 -13 4 87.33 9.15 5 13 4 51.21 7.14 -5 13 -4 60.29 8.72 -5 13 -4 88.57 9.95 5 -13 4 123.30 13.86 5 -13 5 2.15 2.01 5 -13 5 0.55 1.07 5 13 5 1.50 1.47 5 13 5 2.08 1.94 -5 13 -5 0.69 0.69 5 -13 6 9.25 4.63 5 -13 6 4.08 2.82 5 13 6 1.95 1.43 5 13 6 5.34 2.83 -5 13 -6 1.21 1.24 5 -13 7 4.39 3.29 5 -13 7 0.24 1.26 5 13 7 -0.26 0.95 5 13 7 3.28 3.15 5 -13 8 1.90 1.85 5 13 8 0.88 1.03 5 -13 8 9.69 4.72 5 13 8 5.18 4.08 5 -13 9 1.59 1.14 5 13 9 0.59 0.78 5 -13 9 6.03 4.23 5 13 9 3.34 3.10 5 -13 10 12.12 6.16 5 -13 10 4.29 2.95 5 13 10 4.94 3.15 5 13 10 11.17 5.69 5 -13 11 3.23 4.01 5 -13 11 2.83 2.91 5 13 11 0.52 1.25 5 13 11 0.70 1.50 5 13 12 0.00 1.11 -5 -14 13 1.11 1.20 -5 14 13 0.34 0.67 -5 -14 12 34.25 9.33 -5 14 12 14.76 5.81 -5 -14 11 22.75 7.59 -5 14 11 11.50 4.90 -5 -14 10 64.21 11.75 -5 14 10 34.77 7.95 5 14 -9 6.66 3.89 -5 -14 9 6.67 3.43 -5 14 9 7.90 3.61 -5 14 9 6.43 3.79 5 14 -8 -0.19 0.44 -5 14 8 2.82 2.02 -5 14 8 1.26 2.85 5 14 -8 0.56 1.69 5 14 -7 30.40 7.21 -5 14 7 26.03 5.82 -5 14 7 30.94 6.82 5 14 -7 20.86 5.32 -5 14 7 28.83 6.58 5 14 -6 1.76 0.87 -5 14 6 2.53 1.77 5 14 -6 2.70 2.31 -5 14 6 3.54 2.90 5 14 -5 51.74 8.22 5 14 -5 50.24 9.13 -5 14 5 46.09 7.67 -5 14 5 47.42 7.93 -5 14 4 16.12 4.58 -5 14 4 13.17 4.29 5 14 -4 15.20 5.04 5 14 -4 14.09 4.46 5 14 -3 19.48 4.99 -5 14 3 19.51 5.00 5 14 -3 17.60 5.26 -5 14 3 14.48 4.46 5 14 -2 7.02 3.47 5 14 -2 5.98 2.75 -5 14 2 9.77 3.65 -5 14 2 6.19 2.84 5 14 -1 22.71 5.03 -5 14 1 23.54 5.19 -5 14 1 21.38 5.23 5 14 -1 24.36 5.36 5 -14 0 51.52 8.53 5 14 0 50.41 8.27 -5 14 0 44.04 7.32 -5 14 0 42.94 6.70 5 14 0 55.31 8.93 5 14 1 137.82 14.51 -5 14 -1 99.76 10.53 -5 14 -1 112.00 11.50 5 -14 1 137.73 14.43 5 -14 2 35.65 7.72 -5 14 -2 13.69 4.17 5 14 2 35.72 7.96 -5 14 -2 24.07 5.42 5 -14 3 3.81 3.90 5 14 3 2.35 3.40 -5 14 -3 2.39 1.95 -5 14 -3 1.02 1.60 -5 14 -4 12.17 4.18 5 -14 4 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10.02 7 7 -5 95.68 9.79 -7 7 5 69.73 6.96 7 7 -5 92.94 9.88 -7 7 5 81.78 8.95 7 -7 -4 105.93 9.28 7 7 -4 100.62 9.54 7 7 -4 106.60 9.96 -7 7 4 66.92 5.99 -7 7 4 77.27 6.73 7 7 -4 112.26 10.64 -7 7 4 84.17 8.78 7 -7 -3 201.49 13.27 7 -7 -3 92.54 7.05 7 7 -3 186.72 12.60 -7 7 3 134.28 7.43 -7 7 3 154.84 8.49 7 7 -3 200.41 14.01 -7 7 3 169.72 12.56 7 -7 -2 66.73 7.97 7 7 -2 56.97 6.74 -7 7 2 33.16 3.65 7 7 -2 52.67 7.34 -7 7 2 45.54 6.87 -7 7 1 18.91 4.62 -7 7 1 7.75 1.59 7 -7 -1 26.31 5.18 7 7 -1 20.04 4.52 7 7 -1 21.56 4.20 7 -7 0 387.91 20.56 7 7 0 363.76 17.34 7 7 0 323.85 18.24 -7 7 0 322.35 17.87 7 -7 1 101.17 11.04 7 7 1 102.11 9.39 7 7 1 101.25 10.35 -7 7 -1 81.34 9.15 7 -7 2 195.69 15.75 7 7 2 162.88 12.06 7 7 2 160.72 13.25 -7 7 -2 152.99 12.84 -7 7 -3 3.46 2.09 7 -7 3 2.42 2.44 7 -7 3 2.94 2.27 7 7 3 2.96 2.41 7 7 3 2.71 2.51 7 7 3 0.44 0.77 -7 7 -4 9.39 3.42 7 -7 4 10.77 3.60 7 7 4 13.23 4.33 7 7 4 12.05 3.72 7 7 4 9.09 3.77 -7 7 -5 6.14 3.07 7 -7 5 7.67 3.68 7 7 5 7.50 3.85 7 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1.30 1.79 7 8 -6 3.61 2.22 -7 8 6 1.13 1.24 -7 8 6 0.59 0.38 7 8 -5 6.85 2.36 7 8 -5 9.32 3.02 7 -8 -5 10.85 3.05 7 8 -5 8.32 3.04 -7 8 5 6.22 2.03 -7 8 5 9.54 2.82 7 8 -4 23.32 4.74 7 8 -4 22.65 4.77 7 -8 -4 23.22 4.36 7 8 -4 26.47 5.12 -7 8 4 16.92 3.04 -7 8 4 17.35 3.34 -7 8 4 20.07 4.65 7 -8 -3 14.18 2.75 -7 8 3 13.87 2.48 7 -8 -3 23.14 4.59 7 8 -3 28.37 5.19 7 8 -3 25.55 4.93 -7 8 3 16.19 3.05 7 8 -3 29.02 5.48 -7 8 3 25.79 5.13 7 -8 -2 601.65 24.22 7 8 -2 607.09 23.09 -7 8 2 340.07 12.98 7 8 -2 550.33 23.70 -7 8 2 500.25 22.19 -7 8 1 29.53 5.50 7 -8 -1 27.48 5.55 7 8 -1 24.76 4.59 7 8 -1 26.26 5.13 -7 8 1 8.53 1.91 7 -8 0 365.21 20.33 7 8 0 342.31 17.97 7 8 0 316.61 18.36 -7 8 0 300.72 17.85 -7 8 -1 26.72 5.67 7 8 1 33.50 6.33 7 -8 1 33.04 6.58 7 8 1 32.38 5.54 7 -8 2 62.94 9.14 7 8 2 56.88 7.45 -7 8 -2 56.51 7.90 7 8 2 59.28 8.35 -7 8 -3 4.84 2.52 7 8 3 6.61 3.14 7 -8 3 2.52 0.48 7 8 3 2.65 2.06 7 8 3 5.85 2.82 -7 8 -4 28.32 5.87 7 8 4 31.42 6.52 7 8 4 30.09 5.93 7 -8 4 33.36 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9 -8 0.51 0.58 -7 -9 7 29.25 4.67 7 9 -7 25.03 5.97 7 9 -7 33.35 6.29 -7 9 7 22.08 4.72 7 9 -7 33.23 6.88 -7 9 7 25.52 5.38 -7 -9 6 1.24 0.77 7 -9 -6 -0.42 0.24 -7 9 6 -0.38 0.53 7 9 -6 -1.01 1.40 -7 9 6 0.34 1.08 7 9 -6 1.27 1.15 7 -9 -5 61.82 7.17 7 9 -5 56.57 7.89 -7 9 5 46.52 5.84 7 9 -5 66.87 8.59 -7 9 5 53.97 6.55 7 9 -5 68.74 8.71 -7 9 5 55.39 7.67 7 -9 -4 143.06 11.36 7 9 -4 138.94 11.99 7 9 -4 147.91 12.86 -7 9 4 100.77 8.32 7 9 -4 145.82 12.59 -7 9 4 117.50 11.16 7 -9 -3 108.75 10.40 7 9 -3 102.60 10.28 7 9 -3 97.90 10.05 7 9 -3 107.65 10.80 -7 9 3 89.58 9.44 7 -9 -2 5.30 2.61 7 9 -2 7.06 3.64 7 9 -2 4.91 2.42 -7 9 2 1.47 1.12 7 9 -2 9.34 3.67 -7 9 2 4.74 3.10 7 -9 -1 45.15 7.23 7 9 -1 42.00 6.64 7 9 -1 41.95 7.34 -7 9 1 38.55 6.43 7 -9 0 627.08 27.92 7 9 0 669.36 26.51 -7 9 0 567.72 24.85 7 9 0 596.00 25.41 7 -9 1 62.49 9.02 -7 9 -1 31.32 4.06 7 9 1 56.37 7.77 -7 9 -1 57.40 8.21 7 9 1 64.21 8.72 7 -9 2 220.23 17.18 -7 9 -2 189.02 14.94 7 9 2 192.22 15.26 -7 9 -3 1.72 1.96 7 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1.05 -8 -6 14 5.72 4.04 -8 6 14 -0.82 1.11 -8 -6 13 0.77 2.19 8 -6 -13 0.23 0.30 -8 6 13 0.44 0.63 -8 -6 12 5.32 2.91 8 -6 -12 1.82 2.01 -8 6 12 3.14 2.14 -8 6 12 1.72 1.30 -8 -6 11 14.78 5.04 8 -6 -11 12.51 4.21 -8 6 11 9.65 4.02 8 6 -11 15.24 5.16 -8 6 11 10.05 3.80 -8 -6 10 48.29 8.62 -8 6 10 45.33 7.59 -8 6 10 39.99 7.19 8 6 -10 69.04 10.46 -8 -6 9 14.34 3.10 -8 -6 9 16.47 4.99 8 6 -9 20.44 5.43 -8 6 9 14.12 4.06 -8 6 9 17.03 4.48 -8 -6 8 69.49 9.56 8 6 -8 73.47 9.76 -8 6 8 55.44 7.49 -8 6 8 53.97 7.83 -8 -6 8 55.68 6.41 -8 -6 7 70.61 7.57 -8 -6 7 77.19 9.42 8 6 -7 77.15 9.69 -8 6 7 67.99 7.68 -8 6 7 71.27 8.74 -8 -6 6 124.36 10.78 8 6 -6 121.45 11.92 -8 6 6 99.91 8.69 -8 6 6 113.79 10.96 -8 -6 5 3.64 2.08 8 6 -5 4.94 2.51 -8 6 5 4.98 1.98 -8 6 5 5.72 3.03 -8 -6 4 41.58 6.52 8 6 -4 45.54 7.12 8 6 -4 45.39 6.19 -8 6 4 14.67 2.75 -8 6 4 14.84 2.63 -8 6 4 43.72 6.98 -8 -6 3 365.93 19.57 8 6 -3 395.43 17.93 8 6 -3 391.35 20.83 -8 6 3 332.92 18.58 8 6 -2 161.66 11.05 -8 6 2 160.18 13.06 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21.18 6.26 8 7 -10 20.88 5.94 -8 7 10 17.71 5.06 -8 7 10 16.40 4.90 -8 -7 9 6.83 2.08 -8 -7 9 7.99 3.28 8 7 -9 9.64 4.43 -8 7 9 8.91 3.68 -8 7 9 8.02 3.22 -8 -7 8 117.77 12.86 8 7 -8 144.35 13.73 -8 7 8 111.17 10.95 -8 7 8 136.78 12.73 -8 -7 8 97.52 8.53 -8 -7 7 2.14 1.75 -8 -7 7 0.14 1.65 8 7 -7 6.32 3.52 -8 7 7 1.00 1.52 -8 7 7 2.22 2.27 8 7 -6 2.78 2.09 -8 -7 6 5.81 2.48 8 7 -6 5.69 2.79 8 7 -6 5.42 3.30 -8 7 6 2.76 1.54 -8 7 6 6.44 2.65 -8 -7 5 122.73 10.92 8 7 -5 118.57 11.49 8 7 -5 136.54 12.30 8 7 -5 123.25 11.96 -8 7 5 117.96 11.29 -8 -7 4 23.26 4.88 8 7 -4 20.69 4.78 8 7 -4 18.74 4.09 -8 7 4 6.55 1.85 -8 7 4 7.80 2.01 -8 7 4 19.59 4.53 8 7 -3 56.39 7.80 8 7 -3 57.96 7.25 -8 7 3 13.75 2.10 -8 7 3 18.33 2.75 -8 7 3 41.90 6.92 8 7 -2 223.00 13.61 8 7 -2 229.52 15.96 -8 7 2 201.04 14.89 -8 7 1 25.85 5.73 8 7 -1 23.34 5.24 8 7 -1 23.38 4.46 8 7 0 130.73 10.70 8 7 0 125.68 12.34 -8 7 0 121.49 11.75 -8 7 -1 -3.23 1.90 8 7 1 0.50 0.76 8 7 1 1.13 1.90 8 7 2 163.28 12.72 8 7 2 169.85 14.49 -8 7 -2 151.85 13.58 -8 7 -3 26.00 5.98 8 7 3 40.13 7.34 8 7 3 27.05 5.40 -8 7 -4 27.95 6.24 8 -7 4 27.35 6.44 8 7 4 27.90 6.29 8 7 4 38.96 7.30 8 7 4 30.26 5.78 -8 7 -5 9.09 4.11 8 7 5 9.65 3.41 8 -7 5 11.68 4.49 8 7 5 14.57 5.09 8 7 5 6.38 3.02 -8 7 -6 2.32 2.07 8 -7 6 7.15 3.81 8 7 6 3.65 2.95 8 7 6 2.82 1.84 8 7 6 5.23 3.22 -8 7 -7 0.48 1.16 8 -7 7 3.38 2.61 8 7 7 2.21 2.48 8 7 7 0.96 1.93 8 7 7 1.33 1.68 -8 7 -8 0.82 1.41 8 -7 8 7.93 4.12 8 7 8 3.80 2.50 8 7 8 2.38 2.04 8 -7 9 0.62 0.34 8 7 9 -1.01 1.97 8 -7 10 3.43 2.63 8 7 10 1.76 2.19 -8 -8 15 10.40 5.44 -8 8 15 3.48 3.36 -8 -8 14 5.41 3.81 -8 8 14 0.69 1.26 -8 -8 13 0.18 0.84 -8 8 13 -0.20 0.90 -8 -8 12 16.91 5.93 8 -8 -12 5.82 3.14 -8 8 12 13.63 4.85 -8 8 12 8.70 3.78 8 8 -11 5.73 2.97 -8 -8 11 15.95 5.56 8 -8 -11 6.18 2.78 -8 8 11 7.94 3.48 -8 8 11 11.27 4.58 8 8 -10 45.93 8.46 -8 -8 10 47.67 9.06 -8 8 10 44.01 7.97 -8 8 10 37.33 7.43 8 8 -10 51.08 8.98 8 8 -9 49.33 8.54 -8 -8 9 34.48 7.20 -8 8 9 33.23 6.50 8 8 -9 47.76 8.63 -8 8 9 36.28 7.07 -8 -8 8 2.57 1.52 8 8 -8 5.04 3.22 -8 -8 8 6.38 3.64 8 8 -8 4.01 3.07 -8 8 8 3.38 2.33 -8 8 8 4.48 2.13 -8 -8 7 4.48 2.16 8 8 -7 4.79 2.82 8 8 -7 6.68 2.99 8 8 -7 9.97 3.84 -8 8 7 3.79 1.57 -8 8 7 7.00 2.94 -8 -8 6 103.49 9.88 8 8 -6 118.76 12.31 8 8 -6 112.78 11.87 -8 8 6 72.84 7.77 8 8 -6 115.52 12.29 -8 8 6 103.92 10.97 -8 -8 5 -0.50 1.09 8 8 -5 0.23 1.70 8 8 -5 2.60 2.04 -8 8 5 -0.14 0.14 -8 8 5 0.25 0.74 8 8 -5 0.20 1.16 -8 8 5 0.65 1.03 8 8 -4 -0.42 1.95 8 8 -4 1.13 1.16 -8 8 4 1.28 1.03 -8 8 4 0.75 0.58 -8 8 4 2.71 2.02 8 8 -3 142.41 11.88 8 8 -3 149.20 13.00 -8 8 3 129.04 11.99 8 -8 -2 62.88 8.56 8 8 -2 55.94 7.25 -8 8 2 31.11 3.35 8 8 -2 60.00 8.13 -8 8 2 60.35 8.19 8 -8 -1 235.51 17.26 8 8 -1 197.16 13.48 8 8 -1 198.30 15.08 -8 8 1 201.51 15.34 8 -8 0 129.99 13.41 8 8 0 104.76 10.22 8 8 0 106.82 11.62 -8 8 0 96.56 11.04 -8 8 -1 26.22 5.79 8 8 1 36.70 6.90 8 8 1 30.26 5.72 8 -8 1 32.31 6.85 -8 8 -2 10.22 3.67 8 8 2 13.20 4.59 8 8 2 14.38 3.97 -8 8 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1.90 1.64 8 9 -7 2.42 2.00 8 9 -7 3.03 2.48 -8 9 7 0.69 1.03 8 9 -7 3.03 2.03 -8 9 7 0.42 0.55 -8 -9 6 13.25 3.68 8 9 -6 12.61 4.24 8 9 -6 12.56 3.83 -8 9 6 9.94 2.79 8 9 -6 14.23 4.61 -8 9 6 8.44 2.85 -8 9 6 11.67 4.15 8 9 -5 5.00 2.33 8 9 -5 8.09 2.99 -8 9 5 2.84 1.45 8 -9 -5 5.35 2.46 8 9 -5 8.19 3.93 -8 9 5 2.44 1.37 -8 9 5 5.80 2.86 8 9 -4 2.76 1.71 8 9 -4 2.96 1.85 -8 9 4 1.38 0.90 8 -9 -4 4.25 2.04 8 9 -4 6.13 2.73 -8 9 4 1.68 1.05 -8 9 4 0.42 1.71 8 9 -3 5.45 2.42 8 -9 -3 5.78 2.19 8 9 -3 5.94 2.22 -8 9 3 2.98 1.43 8 9 -3 8.45 3.86 -8 9 3 3.30 2.10 8 9 -2 2.16 2.70 -8 9 2 -0.06 0.43 8 -9 -2 0.58 1.75 8 9 -2 1.14 1.94 -8 9 2 -0.04 1.03 8 -9 -1 86.82 10.76 8 9 -1 79.04 9.15 8 9 -1 87.41 10.53 -8 9 1 75.82 9.92 -8 9 0 7.63 3.40 8 9 0 9.89 3.67 8 -9 0 7.25 3.09 8 9 0 7.45 3.04 8 -9 1 203.51 17.73 8 9 1 165.35 13.89 -8 9 -1 179.06 15.30 8 9 1 182.72 15.41 8 -9 2 151.04 15.56 8 9 2 108.37 11.55 -8 9 -2 125.57 13.11 8 9 2 142.13 13.95 -8 9 -3 2.28 2.39 8 -9 3 6.11 3.52 8 9 3 3.16 2.59 8 9 3 10.79 4.61 -8 9 -4 33.29 6.93 8 9 4 35.89 7.88 8 9 4 27.57 6.05 -8 9 -5 0.02 0.72 8 -9 5 0.88 1.87 8 9 5 0.32 1.16 8 9 5 -0.59 0.25 8 9 5 1.97 2.63 -8 9 -6 -0.55 1.26 8 9 6 -0.17 0.90 8 -9 6 1.28 2.14 8 9 6 -0.45 0.40 8 9 6 0.39 1.46 -8 9 -7 0.04 0.40 8 -9 7 2.14 2.89 8 9 7 -0.14 1.38 8 9 7 1.53 1.79 8 -9 8 20.68 7.06 8 9 8 9.47 4.34 8 9 8 8.88 4.14 8 -9 9 1.34 1.43 8 9 9 0.71 1.18 8 -9 10 0.29 0.90 -8 10 15 7.08 4.55 -8 -10 14 3.77 3.80 -8 10 14 0.07 0.53 -8 -10 13 3.80 3.24 -8 10 13 0.71 1.46 -8 -10 12 25.12 7.57 -8 10 12 10.30 4.36 -8 10 12 32.02 7.78 -8 -10 11 -1.39 0.46 8 10 -11 0.11 0.59 -8 10 11 0.64 1.31 -8 10 11 1.07 0.58 -8 -10 10 44.04 9.14 8 10 -10 20.55 5.61 -8 10 10 12.15 4.24 -8 10 10 47.99 8.85 -8 -10 9 -0.18 0.87 8 10 -9 2.69 2.48 -8 10 9 0.11 0.56 -8 10 9 2.22 1.69 8 10 -8 31.40 7.23 8 10 -8 26.49 6.32 -8 10 8 11.09 3.52 8 10 -8 28.05 6.60 -8 10 8 24.49 6.06 -8 -10 7 3.62 2.13 8 10 -7 4.48 2.03 8 10 -7 4.80 2.86 -8 10 7 2.73 1.65 8 10 -7 7.91 3.54 -8 10 7 3.01 1.72 -8 -10 6 41.83 6.52 8 10 -6 52.15 8.69 8 10 -6 47.01 8.11 8 -10 -6 25.34 5.10 -8 10 6 21.44 4.39 -8 10 6 22.16 4.66 8 10 -6 48.56 8.25 -8 10 6 43.64 7.48 8 10 -5 8.40 3.28 8 -10 -5 8.12 3.03 -8 10 5 3.23 1.52 8 10 -5 7.82 3.89 -8 10 5 3.11 1.65 8 10 -5 6.79 3.93 -8 10 5 6.20 2.92 8 10 -4 0.36 1.05 8 -10 -4 1.35 1.85 -8 10 4 0.34 0.49 8 10 -4 -0.14 0.71 8 10 -4 1.82 2.01 -8 10 4 -0.39 1.30 8 -10 -3 56.25 8.25 8 10 -3 57.02 8.43 8 10 -3 51.91 7.81 -8 10 3 29.16 4.60 -8 10 3 41.95 7.15 8 10 -3 55.44 8.47 8 -10 -2 23.66 5.86 8 10 -2 21.70 5.09 -8 10 2 11.71 2.67 8 10 -2 29.40 5.80 8 10 -2 23.85 5.44 -8 10 2 20.62 4.99 8 -10 -1 115.37 12.68 8 10 -1 96.80 10.58 8 10 -1 104.80 10.52 -8 10 1 108.54 11.67 8 10 -1 102.61 11.40 -8 10 0 12.89 4.33 8 10 0 18.85 5.30 8 -10 0 15.11 4.74 8 10 0 14.94 4.34 -8 10 -1 3.03 1.72 8 10 1 3.07 2.67 8 -10 1 5.53 3.42 8 10 1 6.01 3.03 -8 10 -2 16.55 4.65 8 -10 2 17.21 5.43 8 10 2 16.64 4.77 8 10 2 15.60 5.24 -8 10 -3 -0.62 1.74 8 10 3 1.66 1.13 8 -10 3 0.33 1.51 8 10 3 0.45 1.11 8 10 4 46.92 8.68 8 -10 4 54.79 10.48 8 10 4 30.44 6.73 -8 10 -4 53.81 9.17 -8 10 -5 1.50 1.65 8 -10 5 2.86 2.45 8 10 5 2.75 2.20 8 10 5 3.03 2.88 8 -10 5 5.54 3.61 8 10 5 2.33 2.09 -8 10 -6 1.22 1.76 8 10 6 7.08 4.08 8 -10 6 6.22 3.73 8 10 6 1.35 1.54 8 10 6 4.20 2.88 -8 10 -7 0.43 0.88 8 -10 7 3.27 2.95 8 10 7 0.27 1.19 8 10 7 0.95 2.10 8 -10 8 1.52 2.86 8 10 8 0.59 1.40 8 10 8 0.82 1.58 8 -10 9 -0.33 1.71 8 10 9 1.21 2.08 8 -10 10 2.39 2.58 -8 -11 14 33.86 9.59 -8 11 14 8.96 4.69 -8 -11 13 4.42 3.30 -8 11 13 1.18 1.66 -8 -11 12 5.49 3.87 -8 11 12 0.34 0.38 -8 -11 11 2.19 1.63 -8 11 11 0.29 0.20 8 11 -11 0.37 0.87 -8 11 11 2.66 2.58 -8 -11 10 21.62 6.67 -8 11 10 4.78 2.67 8 11 -10 9.83 3.98 -8 11 10 21.89 6.27 -8 -11 9 15.20 4.99 -8 11 9 5.06 2.52 8 11 -9 7.76 3.41 -8 11 9 11.25 4.56 8 11 -8 15.73 5.42 -8 11 8 3.84 2.12 8 11 -8 16.88 5.12 -8 11 8 14.99 4.86 8 11 -8 21.87 5.97 -8 -11 7 0.33 0.32 8 11 -7 -1.22 1.41 8 -11 -7 0.52 1.31 -8 11 7 0.33 0.76 -8 11 7 0.99 1.13 8 11 -7 2.22 2.35 8 11 -7 3.02 1.60 -8 11 7 2.75 2.54 8 11 -6 0.58 1.51 8 -11 -6 0.64 1.18 -8 11 6 0.61 0.67 -8 11 6 1.05 1.28 8 11 -6 2.96 3.42 8 11 -6 1.47 2.97 -8 11 6 1.14 0.64 8 11 -5 1.33 2.09 8 -11 -5 0.96 1.21 -8 11 5 0.39 0.80 -8 11 5 0.92 1.15 8 11 -5 2.54 2.14 8 11 -5 2.52 2.47 -8 11 5 2.00 1.53 8 -11 -4 32.38 6.39 8 11 -4 38.15 7.53 -8 11 4 16.38 3.77 8 11 -4 32.19 6.25 8 11 -4 36.40 7.05 -8 11 4 31.89 6.49 8 11 -3 0.57 1.72 8 -11 -3 -0.01 1.00 8 11 -3 2.23 1.85 -8 11 3 0.92 0.56 8 11 -3 2.76 1.53 -8 11 3 0.24 1.62 8 11 -2 -0.96 1.32 8 -11 -2 0.29 1.33 8 11 -2 2.67 2.20 8 11 -2 2.83 2.80 -8 11 2 -0.43 1.49 8 11 -1 22.49 5.25 8 -11 -1 32.52 6.99 8 11 -1 31.56 6.33 8 11 -1 24.80 5.16 -8 11 1 31.15 6.54 8 11 0 26.73 6.04 8 -11 0 32.15 7.24 8 11 0 33.51 6.83 8 11 0 27.76 5.17 -8 11 0 27.88 6.11 8 -11 1 4.66 3.83 8 11 1 2.53 1.19 8 11 1 5.07 2.90 8 11 1 4.35 2.73 -8 11 -1 3.07 2.23 -8 11 -2 15.41 4.41 8 11 2 19.05 5.41 8 -11 2 16.57 5.25 8 11 2 16.54 5.07 -8 11 -3 2.79 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0.74 10 5 -1 1.56 1.41 -10 -5 0 67.16 10.54 10 5 0 79.01 10.76 -10 5 0 61.99 9.57 -10 5 -1 9.70 4.56 -10 -5 -1 7.48 3.54 10 5 1 11.54 4.50 -10 5 -2 41.13 8.18 -10 -5 -2 32.82 7.65 10 5 2 37.04 7.40 -10 5 -3 -1.70 1.85 -10 -5 -3 -4.04 3.78 10 5 3 2.63 2.77 -10 5 -4 14.58 5.35 10 5 4 10.90 4.20 -10 -5 -4 9.34 4.16 -10 5 -5 1.22 1.87 -10 -5 -5 0.44 0.52 10 5 5 1.02 1.47 -10 5 -6 -0.39 1.01 -10 -5 -6 0.12 0.95 10 5 6 0.83 0.62 10 5 6 0.70 1.20 -10 5 -7 0.24 0.96 -10 -5 -7 0.87 2.35 10 -5 7 3.34 3.10 10 5 7 -1.00 1.32 -10 5 -8 -1.06 1.47 -10 -5 -8 2.79 2.95 10 -5 8 0.89 1.40 10 5 8 -0.04 1.77 -10 6 15 -0.81 1.45 -10 -6 14 1.82 2.15 10 -6 -14 3.91 2.98 -10 6 14 0.76 1.54 -10 -6 13 1.03 1.34 10 -6 -13 0.18 1.60 -10 6 13 1.47 2.32 10 6 -13 -2.28 2.06 -10 6 13 0.39 1.30 -10 -6 12 16.96 5.84 10 -6 -12 22.72 6.63 -10 6 12 24.49 6.50 -10 6 12 6.85 3.46 -10 -6 11 0.06 1.50 10 6 -11 3.30 3.62 -10 6 11 0.43 1.65 -10 6 11 0.05 0.48 -10 -6 10 13.17 5.03 10 6 -10 18.62 5.92 -10 6 10 3.81 2.23 -10 6 10 13.14 4.72 -10 -6 9 2.85 1.63 -10 -6 9 4.61 2.85 10 6 -9 5.32 3.42 -10 6 9 1.40 1.46 -10 6 9 7.01 3.89 -10 -6 8 24.53 5.24 -10 -6 8 32.12 7.11 10 6 -8 45.07 8.51 -10 6 8 14.34 3.92 -10 6 8 31.51 6.89 -10 -6 7 38.66 7.05 -10 -6 7 67.29 9.58 10 6 -7 71.15 10.55 -10 6 7 27.10 5.05 -10 6 7 69.06 9.88 -10 -6 6 18.49 5.37 -10 6 6 6.56 2.33 -10 6 6 23.07 6.27 -10 -6 5 224.97 17.70 10 6 -5 192.75 14.11 -10 6 5 218.29 17.72 -10 6 4 0.45 2.64 10 6 -4 -0.24 1.50 -10 -6 4 3.33 3.13 10 6 -4 2.23 1.66 -10 6 3 36.65 7.25 -10 -6 3 38.09 7.65 10 6 -3 39.00 7.44 10 6 -3 33.32 5.47 -10 -6 2 57.08 9.36 10 6 -2 60.23 9.39 10 6 -2 43.33 6.17 -10 6 2 55.94 8.75 -10 6 1 2.04 2.34 -10 -6 1 -0.50 1.93 10 6 -1 3.30 2.35 10 6 -1 2.22 1.45 -10 6 0 2.54 1.62 -10 -6 0 -0.11 2.02 10 6 0 1.77 2.60 10 6 0 2.67 1.69 -10 6 -1 8.37 3.48 -10 -6 -1 10.92 3.23 10 6 1 11.43 4.37 10 6 2 30.35 6.82 -10 6 -2 43.47 8.52 10 6 3 12.40 4.55 -10 6 -3 13.44 5.32 -10 6 -4 9.35 4.21 10 6 4 14.75 5.67 -10 6 -5 0.71 1.25 10 6 5 0.14 1.49 -10 6 -6 7.20 3.89 10 6 6 15.68 5.67 -10 6 -7 1.07 1.91 -10 -6 -7 1.34 1.91 10 -6 7 7.58 4.35 10 6 7 2.45 2.28 -10 6 -8 -0.42 1.25 -10 -6 -8 1.30 2.00 10 -6 8 -0.13 1.06 10 6 8 0.05 1.43 -10 7 15 0.72 0.92 -10 -7 14 9.35 4.85 -10 7 14 4.74 3.21 -10 -7 13 2.23 1.60 10 -7 -13 1.81 1.95 -10 7 13 2.02 2.29 -10 7 13 0.20 0.72 -10 -7 12 0.65 1.46 10 -7 -12 0.65 1.47 -10 7 12 2.41 2.17 -10 7 12 0.48 1.09 10 7 -12 0.44 3.27 -10 -7 11 5.62 3.73 10 7 -11 9.66 5.81 -10 7 11 2.01 1.74 -10 7 11 12.87 4.62 -10 -7 10 60.93 10.64 10 7 -10 60.38 10.57 -10 7 10 42.82 8.19 -10 -7 9 0.02 1.32 10 7 -9 0.24 2.02 -10 7 9 0.62 1.12 -10 7 9 -0.08 1.54 -10 -7 8 3.99 1.98 -10 -7 8 5.75 2.92 10 7 -8 5.51 3.47 -10 7 8 1.75 1.41 -10 7 8 2.96 2.27 -10 -7 7 58.02 8.59 -10 -7 7 69.02 10.01 10 7 -7 79.21 10.93 10 7 -7 86.87 12.55 -10 7 7 62.00 9.47 10 7 -6 18.63 5.57 -10 -7 6 14.87 4.53 10 7 -6 21.25 6.29 -10 7 6 14.34 4.83 -10 7 5 15.70 5.11 -10 -7 5 10.60 3.95 10 7 -5 15.38 5.02 10 7 -5 11.00 3.77 -10 -7 4 57.94 9.07 10 7 -4 54.23 8.98 10 7 -4 49.50 7.42 -10 7 4 54.22 8.77 -10 7 3 24.03 6.04 -10 -7 3 31.20 6.95 10 7 -3 24.45 6.24 10 7 -3 16.67 4.03 -10 7 2 3.59 2.90 -10 -7 2 0.74 0.63 10 7 -2 4.50 3.52 10 7 -2 2.07 1.93 -10 7 1 8.59 3.27 -10 -7 1 6.50 3.11 10 7 -1 5.54 2.42 10 7 -1 8.95 3.83 10 7 0 55.37 7.15 10 7 0 76.00 10.85 -10 7 0 61.44 9.53 -10 7 -1 10.09 3.87 10 7 1 14.93 5.18 10 7 2 7.40 4.14 -10 7 -2 12.10 4.71 -10 7 -3 3.35 2.56 10 7 3 3.79 3.42 -10 7 -4 2.08 2.36 10 7 4 4.39 3.15 -10 7 -5 0.18 1.20 10 7 5 -0.56 1.05 -10 7 -6 0.80 1.53 10 7 6 1.71 2.78 -10 7 -7 0.52 1.41 10 -7 7 0.65 1.59 10 7 7 -0.14 0.92 10 7 7 -0.26 0.95 -10 7 -8 0.53 1.18 10 -7 8 -1.09 1.52 -10 8 15 2.14 2.04 -10 -8 14 10.22 5.24 -10 8 14 2.12 2.42 -10 -8 13 2.00 2.35 -10 8 13 2.47 2.09 -10 8 13 0.01 0.65 10 8 -12 5.59 3.45 -10 -8 12 6.64 3.71 10 -8 -12 7.49 3.68 -10 8 12 3.43 2.39 -10 8 12 17.46 5.81 10 8 -12 17.72 6.93 10 8 -11 12.41 5.18 -10 -8 11 10.26 4.77 -10 8 11 3.09 2.13 10 8 -11 19.74 7.44 -10 8 11 18.99 5.74 10 8 -10 3.95 3.81 -10 -8 10 2.32 2.97 10 8 -10 -0.19 2.42 -10 8 10 -0.38 0.76 -10 8 10 1.46 1.66 10 8 -9 2.91 2.61 -10 -8 9 1.49 1.44 10 8 -9 2.28 3.21 -10 8 9 -0.29 0.61 -10 8 9 2.12 2.38 -10 -8 8 53.04 7.82 -10 -8 8 76.19 11.15 10 8 -8 76.77 11.20 10 8 -8 79.35 12.17 -10 8 8 68.77 10.27 -10 -8 7 3.52 2.44 10 8 -7 7.13 4.20 10 8 -7 9.04 4.18 -10 8 7 7.34 3.76 -10 -8 6 2.73 2.27 10 8 -6 1.72 1.85 10 8 -6 0.89 0.81 10 8 -6 5.79 4.23 -10 8 6 -0.38 1.40 -10 -8 5 10.47 4.12 10 8 -5 16.42 4.73 10 8 -5 12.42 4.12 10 8 -5 15.26 5.40 -10 8 5 12.72 4.52 -10 8 4 6.04 3.59 -10 -8 4 2.99 2.86 10 8 -4 2.25 3.10 10 8 -4 3.49 2.22 -10 8 3 1.83 1.68 -10 -8 3 5.54 3.21 10 8 -3 3.59 2.67 10 8 -3 0.71 0.97 10 8 -2 98.64 10.40 10 8 -2 112.72 12.74 -10 8 2 105.08 12.50 -10 8 1 43.64 8.18 10 8 -1 31.52 5.80 10 8 -1 44.79 8.14 -10 8 0 4.91 3.14 10 8 0 3.52 1.85 10 8 0 6.76 2.78 -10 8 -1 0.43 1.20 10 8 1 3.26 2.08 10 8 1 4.67 3.60 -10 8 -2 18.11 5.62 10 8 2 27.85 6.87 -10 8 -3 4.01 2.61 10 8 3 6.00 2.91 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2.27 10 9 -5 2.31 2.85 -10 9 5 0.24 1.71 -10 -9 4 2.67 2.09 10 9 -4 1.22 1.54 10 9 -4 9.12 4.23 10 9 -4 3.64 3.27 -10 9 4 1.52 1.45 -10 9 3 1.58 1.69 10 9 -3 0.71 1.13 10 9 -3 0.84 1.88 -10 9 2 9.31 4.10 10 9 -2 11.00 3.86 10 9 -2 15.12 5.03 -10 9 1 3.36 3.38 10 9 -1 1.47 2.02 10 9 -1 4.62 3.47 10 9 0 66.04 8.84 10 9 0 84.57 12.04 -10 9 0 83.40 11.72 -10 9 -1 -0.39 1.12 10 9 1 0.65 2.66 10 9 1 0.94 1.66 -10 9 -2 24.97 6.68 10 9 2 45.62 9.07 -10 9 -3 0.36 1.14 10 9 3 2.08 3.10 -10 9 -4 0.86 1.53 10 9 4 -1.83 2.16 -10 9 -5 -0.78 1.82 10 9 5 -0.13 0.94 -10 9 -6 0.32 0.70 10 9 6 0.82 1.33 -10 9 -7 0.48 1.30 10 9 7 -1.52 1.95 10 -9 8 0.23 1.24 -10 10 15 0.50 1.30 -10 10 14 1.41 1.93 -10 -10 13 6.39 4.37 -10 10 13 5.31 3.30 -10 10 13 7.57 3.99 -10 -10 12 4.48 3.39 -10 10 12 1.64 2.02 -10 10 12 9.50 4.63 -10 -10 11 9.32 4.93 10 10 -11 7.38 4.12 -10 10 11 4.11 2.56 -10 10 11 16.79 5.99 -10 -10 10 3.02 3.26 10 10 -10 5.85 3.90 -10 10 10 1.30 1.28 10 10 -10 9.75 5.26 -10 10 10 5.21 2.99 -10 -10 9 0.29 1.22 10 10 -9 2.84 3.64 10 10 -9 -0.63 1.95 -10 10 9 1.20 2.06 10 10 -8 2.26 1.94 -10 -10 8 -0.53 1.75 10 10 -8 0.67 2.29 -10 10 8 1.54 0.68 -10 -10 7 59.99 9.08 10 10 -7 62.81 10.13 10 10 -7 75.32 11.46 10 10 -7 82.24 12.10 -10 10 7 64.94 10.24 -10 -10 6 1.91 1.49 10 10 -6 1.20 1.47 10 10 -6 5.98 3.38 10 10 -6 4.41 3.87 -10 10 6 3.07 2.36 -10 -10 5 10.48 3.90 10 10 -5 3.07 2.02 10 10 -5 7.93 3.77 10 10 -5 8.49 4.05 -10 10 5 4.88 2.46 -10 -10 4 -0.11 0.93 10 10 -4 -1.57 1.82 10 10 -4 -1.16 1.38 10 10 -4 -2.33 1.96 -10 10 4 -0.50 0.51 10 10 -3 28.14 6.30 10 10 -3 36.19 7.19 10 10 -3 37.01 7.87 -10 10 3 33.56 7.02 10 10 -2 110.98 12.13 10 10 -2 129.79 14.80 -10 10 2 129.98 14.32 10 10 -1 8.70 3.97 -10 10 1 4.97 2.67 10 10 -1 5.11 2.63 -10 10 0 10.78 4.25 10 10 0 13.99 4.79 10 10 0 8.83 3.36 -10 10 -1 1.88 2.22 10 10 1 0.77 1.32 -10 10 -2 9.10 4.12 10 10 2 4.96 2.69 -10 10 -3 0.29 0.61 10 10 3 3.80 3.80 -10 10 -4 7.32 3.81 10 10 4 22.83 7.23 10 10 5 0.08 2.14 -10 10 -5 0.30 0.86 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26.75 6.54 10 11 -1 21.44 6.56 10 11 -1 12.82 4.31 10 11 -1 16.78 4.75 -10 11 1 19.68 5.84 -10 11 0 18.18 5.67 10 11 0 27.92 7.18 10 11 0 17.40 5.07 -10 11 -1 2.40 2.40 10 11 1 8.11 4.84 10 11 1 2.02 1.93 -10 11 -2 8.75 3.97 10 11 2 10.64 4.44 10 11 2 19.75 6.63 -10 11 -3 0.10 0.83 10 11 3 3.84 3.83 -10 11 -4 0.36 0.93 10 11 4 4.78 4.40 -10 11 -5 0.40 0.56 10 11 5 -0.40 2.25 -10 11 -6 2.89 2.85 10 11 6 4.03 3.49 -10 12 14 4.79 3.64 -10 12 13 3.15 3.07 -10 -12 12 0.61 1.81 -10 12 12 2.34 2.66 -10 -12 11 1.28 1.32 10 12 -11 0.68 0.43 -10 12 11 3.84 2.97 -10 -12 10 10.97 4.91 10 12 -10 7.90 4.03 -10 12 10 20.30 6.67 -10 -12 9 1.33 1.03 10 12 -9 1.43 2.38 -10 12 9 2.84 2.48 10 12 -9 0.81 0.76 10 12 -8 3.46 2.84 10 12 -8 4.72 3.97 10 12 -8 1.26 1.01 -10 12 8 6.04 3.36 -10 -12 7 0.14 1.06 10 12 -7 2.29 2.48 10 12 -7 3.58 2.06 -10 12 7 1.74 2.16 -10 -12 6 0.20 1.08 10 12 -6 1.41 1.38 10 12 -6 -1.11 1.71 10 12 -6 -0.53 1.65 -10 12 6 -0.40 0.71 10 12 -5 0.34 1.50 10 12 -5 3.28 3.51 10 12 -5 2.82 2.06 -10 12 5 1.97 2.39 10 12 -4 73.79 11.40 10 12 -4 75.92 10.96 -10 12 4 74.68 11.20 10 12 -4 88.51 12.82 10 12 -3 4.79 3.19 10 12 -3 -0.02 0.36 10 12 -3 3.74 3.32 -10 12 3 -2.17 2.47 10 12 -2 45.49 9.22 10 12 -2 24.60 6.42 10 12 -2 43.85 8.00 -10 12 2 35.94 7.86 10 12 -1 5.97 3.57 10 12 -1 3.83 2.69 10 12 -1 2.41 2.21 -10 12 1 4.94 2.66 10 12 0 6.80 4.40 10 12 0 2.90 2.45 10 12 0 1.79 1.66 -10 12 0 8.43 4.35 10 12 1 0.39 1.05 10 12 1 3.01 3.71 -10 12 -1 0.40 0.88 10 12 2 11.86 5.30 10 12 2 5.26 3.28 -10 12 -2 4.73 3.02 -10 12 -3 13.99 5.29 10 12 3 29.24 8.54 -10 12 -4 6.63 3.68 10 12 4 36.00 9.61 -10 12 -5 4.37 3.36 10 12 5 8.96 5.40 -10 12 -6 2.56 2.59 -10 13 13 0.51 1.57 -10 13 12 4.11 3.33 -10 -13 11 9.38 4.83 -10 13 11 8.85 4.66 -10 -13 10 1.53 1.33 -10 13 10 2.22 2.38 10 13 -10 -0.50 1.27 -10 -13 9 -1.65 2.32 -10 13 9 1.33 2.21 10 13 -9 0.01 1.01 10 13 -8 1.26 1.71 -10 13 8 1.31 1.44 10 13 -8 -2.13 2.76 10 13 -8 -0.48 1.52 10 13 -7 11.50 4.93 10 13 -7 6.85 3.22 10 13 -7 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-15 3 4 6.93 4.03 15 3 -4 6.67 4.30 -15 -3 4 8.58 4.84 -15 3 3 -0.90 1.52 -15 -3 3 -0.44 1.85 15 3 -3 1.83 2.63 -15 -3 2 12.63 6.25 15 3 -2 4.34 3.78 15 3 -1 1.53 2.98 15 3 0 2.63 4.09 -15 4 11 -0.20 0.64 -15 4 10 1.16 1.90 -15 -4 9 1.68 1.93 -15 4 9 0.75 0.33 -15 4 8 -1.08 2.25 -15 -4 8 -0.59 1.24 -15 4 7 0.55 0.26 -15 -4 7 0.74 2.06 -15 4 6 6.35 4.31 -15 -4 6 10.32 5.05 -15 4 5 3.53 3.58 -15 -4 5 6.31 4.63 15 4 -5 16.94 8.20 -15 4 4 0.50 1.25 -15 -4 4 6.04 4.25 15 4 -4 6.54 5.18 -15 -4 3 1.34 2.01 15 4 -3 6.63 5.13 15 4 -2 0.20 1.71 -15 5 11 9.48 4.97 -15 5 10 0.81 0.89 -15 5 9 -0.46 1.06 -15 -5 8 0.06 1.88 -15 5 8 -0.97 0.14 -15 5 7 -0.43 0.70 -15 -5 7 0.57 1.30 -15 5 6 0.53 1.30 -15 -5 6 -0.57 1.07 -15 5 5 6.12 4.90 -15 -5 5 7.50 4.87 -15 5 4 2.25 2.82 -15 -5 4 1.70 3.43 -15 -5 3 0.30 2.00 -15 6 11 0.29 1.40 -15 6 10 0.25 1.52 -15 6 9 0.61 1.20 -15 -6 8 0.30 1.34 -15 6 8 -2.42 3.05 -15 -6 7 0.53 0.24 -15 6 7 -0.80 2.09 -15 6 6 12.00 5.70 -15 -6 6 11.71 5.75 -15 -6 5 1.05 2.25 -15 -6 4 6.29 4.40 -15 -6 3 4.06 4.34 -15 -7 7 0.21 0.63 -15 -7 6 0.62 0.83 -15 -7 5 3.33 3.29 -15 -7 4 -0.06 1.12 -15 -7 3 7.21 5.35 -15 -8 7 7.27 4.61 -15 -8 6 1.43 2.06 -15 -8 5 1.31 2.53 -15 -8 4 4.43 3.90 -15 -9 7 0.33 1.51 -15 -9 6 1.76 2.39 -15 -9 5 0.19 1.20 -15 -9 4 1.51 2.82 -15 -10 6 9.25 5.34 -15 -10 5 1.21 2.56 15 10 -3 1.07 2.58 -15 -11 6 2.52 3.09 -16 0 10 -0.77 2.27 -16 0 9 -1.89 2.16 -16 0 8 3.80 3.67 -16 0 7 -0.40 0.65 -16 1 10 1.21 2.04 -16 1 9 -0.08 0.51 -16 -1 9 -0.49 1.38 -16 1 8 -0.63 0.72 -16 -1 8 -0.70 0.39 -16 -1 7 1.26 2.02 -16 -2 9 0.12 1.65 -16 -2 8 -0.32 1.66 -16 -2 7 1.21 0.92 -16 -3 8 6.32 4.17 -16 -3 7 -0.83 1.59 -16 -4 8 3.08 2.85 -16 -4 7 0.86 2.29 -16 -5 8 8.69 4.88 -16 -5 7 5.49 4.04 -16 -6 7 0.93 1.60 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 29502 _shelx_res_file ; TITL farm16_a.res in P2(1)/c farm16.res created by SHELXL-2016/6 at 17:39:20 on 19-Dec-2022 REM Old TITL farm16 in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.204, Rweak 0.018, Alpha 0.050, Orientation as input REM Formula found by SHELXT: C25 N4 O6 S2 CELL 0.71073 11.7125 18.404 12.8601 90 108.613 90 ZERR 4 0.0004 0.0006 0.0005 0 0.003 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H N O S UNIT 108 104 8 24 8 DFIX 1.47 0.002 N2 C26B DFIX 1.54 0.002 C26B C27B DFIX 1.54 0.002 C26A C27A DFIX 1.47 0.002 N2 C26A L.S. 4 0 0 PLAN 14 CONF BOND $H list 4 MORE -1 fmap 2 53 acta OMIT -2 50 REM REM REM WGHT 0.078500 0.642200 FVAR 0.45451 0.82343 S1 5 0.477935 0.257675 0.194342 11.00000 0.04806 0.04141 = 0.05044 0.00423 0.01318 -0.00776 S2 5 0.833420 0.297500 0.128658 11.00000 0.06170 0.06580 = 0.07906 -0.01767 0.03249 0.00135 O1 4 0.487912 0.402594 -0.010800 11.00000 0.06941 0.08200 = 0.05280 0.02162 0.01938 -0.00023 O2 4 0.395689 0.219640 0.105042 11.00000 0.05932 0.05577 = 0.06427 -0.01085 0.01461 -0.02276 O3 4 0.560910 0.216626 0.278209 11.00000 0.05738 0.05250 = 0.07485 0.02703 0.01041 0.00007 O4 4 0.870313 0.483321 0.219543 11.00000 0.07943 0.05437 = 0.11103 0.00331 0.02575 -0.02167 O5 4 0.925532 0.325884 0.089927 11.00000 0.07387 0.11252 = 0.09076 -0.01890 0.05214 -0.00414 O6 4 0.750220 0.246528 0.062504 11.00000 0.08139 0.08192 = 0.11431 -0.05322 0.03916 -0.00922 N1 3 0.406915 0.312045 0.253269 11.00000 0.05414 0.05509 = 0.04401 0.00597 0.01870 -0.00306 N2 3 0.891360 0.260769 0.250035 11.00000 0.06535 0.05513 = 0.10414 0.01044 0.02909 0.01864 C1 1 0.330793 0.365776 0.186199 11.00000 0.04849 0.04601 = 0.06328 0.00339 0.01847 -0.00385 C2 1 0.230983 0.391117 0.211169 11.00000 0.07215 0.06834 = 0.10973 0.00864 0.05223 0.00568 AFIX 43 H2 2 0.213177 0.372912 0.271679 11.00000 -1.20000 AFIX 0 C3 1 0.158370 0.443447 0.145728 11.00000 0.07566 0.07909 = 0.17393 0.02670 0.06570 0.02108 AFIX 43 H3 2 0.093015 0.461227 0.164150 11.00000 -1.20000 AFIX 0 C4 1 0.179997 0.469712 0.054853 11.00000 0.06287 0.10027 = 0.15971 0.05921 0.03865 0.03140 AFIX 43 H4 2 0.128496 0.503913 0.010587 11.00000 -1.20000 AFIX 0 C5 1 0.278301 0.445359 0.029067 11.00000 0.05762 0.07773 = 0.10123 0.03444 0.02329 0.01143 AFIX 43 H5 2 0.293003 0.463059 -0.033195 11.00000 -1.20000 AFIX 0 C6 1 0.356575 0.394299 0.095203 11.00000 0.04114 0.05186 = 0.05973 0.01282 0.01118 -0.00020 C7 1 0.386569 0.285475 0.353691 11.00000 0.06920 0.08587 = 0.04416 0.00935 0.01965 -0.00854 AFIX 23 H7A 2 0.364483 0.326257 0.391083 11.00000 -1.20000 H7B 2 0.461418 0.265607 0.402041 11.00000 -1.20000 AFIX 0 C8 1 0.290217 0.228356 0.333628 11.00000 0.07633 0.08952 = 0.07412 0.02103 0.03680 -0.00871 AFIX 137 H8A 2 0.216782 0.246542 0.282656 11.00000 -1.50000 H8B 2 0.277153 0.216385 0.401607 11.00000 -1.50000 H8C 2 0.315178 0.185659 0.303806 11.00000 -1.50000 AFIX 0 C9 1 0.463606 0.375449 0.065666 11.00000 0.04891 0.04808 = 0.04012 0.00619 0.00925 -0.00838 C10 1 0.553505 0.320257 0.135381 11.00000 0.04311 0.04247 = 0.03864 -0.00321 0.01289 -0.00446 AFIX 13 H10 2 0.582604 0.292278 0.084064 11.00000 -1.20000 AFIX 0 C11 1 0.666828 0.353350 0.220115 11.00000 0.03899 0.03798 = 0.04065 0.00360 0.01107 -0.00216 AFIX 13 H11 2 0.703254 0.314563 0.272388 11.00000 -1.20000 AFIX 0 C12 1 0.641623 0.415696 0.286777 11.00000 0.03676 0.04029 = 0.04913 -0.00300 0.01344 -0.00394 C13 1 0.662218 0.406546 0.397551 11.00000 0.06898 0.06219 = 0.05351 -0.00464 0.02141 -0.00743 AFIX 43 H13 2 0.691505 0.362551 0.431097 11.00000 -1.20000 AFIX 0 C14 1 0.638913 0.463583 0.459004 11.00000 0.10584 0.10704 = 0.06900 -0.03105 0.04507 -0.01901 AFIX 43 H14 2 0.652657 0.457362 0.533779 11.00000 -1.20000 AFIX 0 C15 1 0.596161 0.528503 0.410935 11.00000 0.10243 0.07210 = 0.11884 -0.03911 0.05670 -0.00968 AFIX 43 H15 2 0.580782 0.566206 0.452748 11.00000 -1.20000 AFIX 0 C16 1 0.576278 0.537769 0.302382 11.00000 0.07560 0.04833 = 0.11221 -0.01652 0.03728 -0.00146 AFIX 43 H16 2 0.546752 0.581930 0.269590 11.00000 -1.20000 AFIX 0 C17 1 0.599370 0.482327 0.239729 11.00000 0.05831 0.04011 = 0.06893 -0.00319 0.02129 -0.00045 AFIX 43 H17 2 0.586499 0.489687 0.165310 11.00000 -1.20000 AFIX 0 C18 1 0.760976 0.374137 0.163026 11.00000 0.04417 0.04579 = 0.04697 0.00214 0.01574 -0.00259 AFIX 13 H18 2 0.721111 0.401986 0.096348 11.00000 -1.20000 AFIX 0 C19 1 0.865207 0.418878 0.237827 11.00000 0.04725 0.05169 = 0.06641 -0.00244 0.02505 -0.00852 C20 1 0.951054 0.381408 0.328158 11.00000 0.03843 0.08257 = 0.06280 -0.00232 0.01475 -0.00594 C21 1 1.025256 0.424272 0.413019 11.00000 0.05114 0.14201 = 0.08042 -0.02281 0.01288 -0.02365 AFIX 43 H21 2 1.020907 0.474641 0.407315 11.00000 -1.20000 AFIX 0 C22 1 1.103638 0.392928 0.503720 11.00000 0.05642 0.25675 = 0.07989 -0.01307 -0.00068 -0.02096 AFIX 43 H22 2 1.152568 0.421830 0.559600 11.00000 -1.20000 AFIX 0 C23 1 1.110327 0.319315 0.512540 11.00000 0.05828 0.26060 = 0.08242 0.04017 0.00772 0.03351 AFIX 43 H23 2 1.162666 0.298517 0.575744 11.00000 -1.20000 AFIX 0 C24 1 1.041214 0.274554 0.429834 11.00000 0.06209 0.15477 = 0.10464 0.04879 0.03240 0.04038 AFIX 43 H24 2 1.048072 0.224317 0.436921 11.00000 -1.20000 AFIX 0 C25 1 0.960781 0.305749 0.335292 11.00000 0.03677 0.10223 = 0.07358 0.02073 0.01856 0.01534 PART 1 C26A 1 0.865068 0.185625 0.274276 21.00000 0.09262 0.05824 = 0.17794 0.02569 0.07279 0.01122 AFIX 23 H26A 2 0.782421 0.173685 0.232684 21.00000 -1.20000 H26B 2 0.874295 0.181114 0.351686 21.00000 -1.20000 AFIX 0 C27A 1 0.951014 0.132500 0.244281 21.00000 0.16715 0.06239 = 0.27463 0.02175 0.11972 0.04902 AFIX 137 H27A 2 0.948918 0.141105 0.170067 21.00000 -1.50000 H27B 2 0.926259 0.083490 0.251111 21.00000 -1.50000 H27C 2 1.031506 0.139747 0.292943 21.00000 -1.50000 AFIX 0 PART 2 C26B 1 0.915451 0.186524 0.220236 -21.00000 0.06683 0.15475 = 0.15051 -0.01540 0.05294 0.02194 AFIX 23 H26C 2 1.000208 0.174041 0.249165 -21.00000 -1.20000 H26D 2 0.886487 0.178665 0.141547 -21.00000 -1.20000 AFIX 0 C27B 1 0.839333 0.145737 0.279419 -21.00000 0.11268 0.07864 = 0.19662 0.01299 0.02548 0.00528 AFIX 137 H27D 2 0.764720 0.130614 0.226797 -21.00000 -1.50000 H27E 2 0.823032 0.177321 0.332400 -21.00000 -1.50000 H27F 2 0.882787 0.103844 0.315959 -21.00000 -1.50000 AFIX 0 HKLF 4 REM farm16_a.res in P2(1)/c REM R1 = 0.0583 for 3493 Fo > 4sig(Fo) and 0.0754 for all 4617 data REM 356 parameters refined using 4 restraints END WGHT 0.0785 0.6422 REM Highest difference peak 0.209, deepest hole -0.354, 1-sigma level 0.051 Q1 1 0.7403 0.3000 0.0272 11.00000 0.05 0.21 Q2 1 0.4984 0.2569 0.2786 11.00000 0.05 0.20 Q3 1 0.7826 0.4022 0.1791 11.00000 0.05 0.20 Q4 1 1.0363 0.1976 0.3998 11.00000 0.05 0.20 Q5 1 0.3963 0.2031 0.1655 11.00000 0.05 0.19 Q6 1 0.5751 0.2583 0.2204 11.00000 0.05 0.19 Q7 1 0.9031 0.2781 0.2011 11.00000 0.05 0.19 Q8 1 0.9051 0.3600 0.1591 11.00000 0.05 0.19 Q9 1 0.4620 0.3157 0.2582 11.00000 0.05 0.18 Q10 1 1.0984 0.3067 0.4339 11.00000 0.05 0.18 Q11 1 0.8418 0.3632 0.0397 11.00000 0.05 0.18 Q12 1 0.3819 0.2723 0.1028 11.00000 0.05 0.18 Q13 1 0.2809 0.4803 0.1008 11.00000 0.05 0.18 Q14 1 0.3779 0.2574 0.1637 11.00000 0.05 0.17 ; _shelx_res_checksum 38578 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S S1 0.47793(6) 0.25767(4) 0.19434(5) 0.0472(2) Uani d 1 . . S S2 0.83342(7) 0.29750(5) 0.12866(7) 0.0665(3) Uani d 1 . . O O1 0.48791(18) 0.40259(12) -0.01080(16) 0.0681(6) Uani d 1 . . O O2 0.39569(17) 0.21964(11) 0.10504(16) 0.0610(5) Uani d 1 . . O O3 0.56091(17) 0.21663(11) 0.27821(17) 0.0641(6) Uani d 1 . . O O4 0.8703(2) 0.48332(12) 0.2195(2) 0.0827(7) Uani d 1 . . O O5 0.9255(2) 0.32588(15) 0.0899(2) 0.0863(7) Uani d 1 . . O O6 0.7502(2) 0.24653(13) 0.0625(2) 0.0907(8) Uani d 1 . . N N1 0.40691(19) 0.31205(12) 0.25327(17) 0.0504(6) Uani d 1 . . N N2 0.8914(2) 0.26077(14) 0.2500(3) 0.0744(8) Uani d 1 . . C C1 0.3308(2) 0.36578(15) 0.1862(2) 0.0524(7) Uani d 1 . . C C2 0.2310(3) 0.39112(19) 0.2112(3) 0.0779(10) Uani d 1 . . H H2 0.213177 0.372912 0.271679 0.093 Uiso calc 1 . . C C3 0.1584(4) 0.4434(2) 0.1457(4) 0.1034(15) Uani d 1 . . H H3 0.093015 0.461227 0.164150 0.124 Uiso calc 1 . . C C4 0.1800(3) 0.4697(2) 0.0549(4) 0.1069(15) Uani d 1 . . H H4 0.128496 0.503913 0.010587 0.128 Uiso calc 1 . . C C5 0.2783(3) 0.44536(19) 0.0291(3) 0.0793(10) Uani d 1 . . H H5 0.293003 0.463059 -0.033195 0.095 Uiso calc 1 . . C C6 0.3566(2) 0.39430(15) 0.0952(2) 0.0521(7) Uani d 1 . . C C7 0.3866(3) 0.28547(19) 0.3537(2) 0.0660(8) Uani d 1 . . H H7A 0.364483 0.326257 0.391083 0.079 Uiso calc 1 . . H H7B 0.461418 0.265607 0.402041 0.079 Uiso calc 1 . . C C8 0.2902(3) 0.2284(2) 0.3336(3) 0.0770(10) Uani d 1 . . H H8A 0.216782 0.246542 0.282656 0.115 Uiso calc 1 . . H H8B 0.277153 0.216385 0.401607 0.115 Uiso calc 1 . . H H8C 0.315178 0.185659 0.303806 0.115 Uiso calc 1 . . C C9 0.4636(2) 0.37545(14) 0.0657(2) 0.0469(6) Uani d 1 . . C C10 0.5535(2) 0.32026(13) 0.13538(19) 0.0414(6) Uani d 1 . . H H10 0.582604 0.292278 0.084064 0.050 Uiso calc 1 . . C C11 0.6668(2) 0.35335(13) 0.22011(19) 0.0396(6) Uani d 1 . . H H11 0.703254 0.314563 0.272388 0.048 Uiso calc 1 . . C C12 0.6416(2) 0.41570(13) 0.2868(2) 0.0421(6) Uani d 1 . . C C13 0.6622(3) 0.40655(17) 0.3976(2) 0.0611(8) Uani d 1 . . H H13 0.691505 0.362551 0.431097 0.073 Uiso calc 1 . . C C14 0.6389(4) 0.4636(3) 0.4590(3) 0.0899(12) Uani d 1 . . H H14 0.652657 0.457362 0.533779 0.108 Uiso calc 1 . . C C15 0.5962(4) 0.5285(2) 0.4109(4) 0.0927(12) Uani d 1 . . H H15 0.580782 0.566206 0.452748 0.111 Uiso calc 1 . . C C16 0.5763(3) 0.53777(18) 0.3024(4) 0.0770(10) Uani d 1 . . H H16 0.546752 0.581930 0.269590 0.092 Uiso calc 1 . . C C17 0.5994(2) 0.48233(14) 0.2397(3) 0.0556(7) Uani d 1 . . H H17 0.586499 0.489687 0.165310 0.067 Uiso calc 1 . . C C18 0.7610(2) 0.37414(14) 0.1630(2) 0.0454(6) Uani d 1 . . H H18 0.721111 0.401986 0.096348 0.054 Uiso calc 1 . . C C19 0.8652(2) 0.41888(16) 0.2378(2) 0.0535(7) Uani d 1 . . C C20 0.9511(2) 0.38141(19) 0.3282(2) 0.0616(8) Uani d 1 . . C C21 1.0253(3) 0.4243(3) 0.4130(3) 0.0931(13) Uani d 1 . . H H21 1.020907 0.474641 0.407315 0.112 Uiso calc 1 . . C C22 1.1036(4) 0.3929(5) 0.5037(4) 0.136(2) Uani d 1 . . H H22 1.152568 0.421830 0.559600 0.164 Uiso calc 1 . . C C23 1.1103(4) 0.3193(5) 0.5125(5) 0.137(3) Uani d 1 . . H H23 1.162666 0.298517 0.575744 0.165 Uiso calc 1 . . C C24 1.0412(4) 0.2746(3) 0.4298(4) 0.1058(15) Uani d 1 . . H H24 1.048072 0.224317 0.436921 0.127 Uiso calc 1 . . C C25 0.9608(3) 0.3057(2) 0.3353(3) 0.0706(9) Uani d 1 . . C C26A 0.8651(6) 0.18562(17) 0.2743(7) 0.103(2) Uani d 0.823(10) A 1 H H26A 0.782421 0.173685 0.232684 0.123 Uiso calc 0.823(10) A 1 H H26B 0.874295 0.181114 0.351686 0.123 Uiso calc 0.823(10) A 1 C C27A 0.9510(7) 0.1325(3) 0.2443(7) 0.156(4) Uani d 0.823(10) A 1 H H27A 0.948918 0.141105 0.170067 0.235 Uiso calc 0.823(10) A 1 H H27B 0.926259 0.083490 0.251111 0.235 Uiso calc 0.823(10) A 1 H H27C 1.031506 0.139747 0.292943 0.235 Uiso calc 0.823(10) A 1 C C26B 0.915(2) 0.1865(6) 0.220(2) 0.120(13) Uani d 0.177(10) A 2 H H26C 1.000208 0.174041 0.249165 0.144 Uiso calc 0.177(10) A 2 H H26D 0.886487 0.178665 0.141547 0.144 Uiso calc 0.177(10) A 2 C C27B 0.839(3) 0.1457(17) 0.279(3) 0.135(14) Uani d 0.177(10) A 2 H H27D 0.764720 0.130614 0.226797 0.202 Uiso calc 0.177(10) A 2 H H27E 0.823032 0.177321 0.332400 0.202 Uiso calc 0.177(10) A 2 H H27F 0.882787 0.103844 0.315959 0.202 Uiso calc 0.177(10) A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 S1 0.0481(4) 0.0414(4) 0.0504(4) -0.0078(3) 0.0132(3) 0.0042(3) S2 0.0617(5) 0.0658(6) 0.0791(6) 0.0014(4) 0.0325(4) -0.0177(4) O1 0.0694(13) 0.0820(16) 0.0528(12) -0.0002(11) 0.0194(10) 0.0216(11) O2 0.0593(12) 0.0558(12) 0.0643(13) -0.0228(9) 0.0146(9) -0.0109(10) O3 0.0574(12) 0.0525(12) 0.0748(14) 0.0001(9) 0.0104(10) 0.0270(10) O4 0.0794(16) 0.0544(15) 0.1110(19) -0.0217(11) 0.0258(13) 0.0033(13) O5 0.0739(15) 0.113(2) 0.0908(17) -0.0041(13) 0.0521(13) -0.0189(15) O6 0.0814(16) 0.0819(17) 0.114(2) -0.0092(13) 0.0392(14) -0.0532(15) N1 0.0541(13) 0.0551(14) 0.0440(13) -0.0031(10) 0.0187(10) 0.0060(10) N2 0.0654(17) 0.0551(17) 0.104(2) 0.0186(13) 0.0291(16) 0.0104(15) C1 0.0485(16) 0.0460(16) 0.0633(18) -0.0039(12) 0.0185(13) 0.0034(13) C2 0.072(2) 0.068(2) 0.110(3) 0.0057(17) 0.052(2) 0.009(2) C3 0.076(3) 0.079(3) 0.174(5) 0.021(2) 0.066(3) 0.027(3) C4 0.063(2) 0.100(3) 0.160(4) 0.031(2) 0.039(2) 0.059(3) C5 0.058(2) 0.078(2) 0.101(3) 0.0114(16) 0.0233(17) 0.034(2) C6 0.0411(15) 0.0519(17) 0.0597(17) -0.0002(11) 0.0112(12) 0.0128(13) C7 0.069(2) 0.086(2) 0.0442(17) -0.0085(16) 0.0196(14) 0.0094(15) C8 0.076(2) 0.090(3) 0.074(2) -0.0087(18) 0.0368(17) 0.0210(19) C9 0.0489(15) 0.0481(16) 0.0401(15) -0.0084(11) 0.0092(11) 0.0062(12) C10 0.0431(14) 0.0425(15) 0.0386(14) -0.0045(10) 0.0129(10) -0.0032(11) C11 0.0390(13) 0.0380(14) 0.0407(14) -0.0022(10) 0.0111(10) 0.0036(10) C12 0.0368(13) 0.0403(15) 0.0491(16) -0.0039(10) 0.0134(10) -0.0030(11) C13 0.069(2) 0.062(2) 0.0535(18) -0.0074(14) 0.0214(14) -0.0046(15) C14 0.106(3) 0.107(3) 0.069(2) -0.019(2) 0.045(2) -0.031(2) C15 0.102(3) 0.072(3) 0.119(4) -0.010(2) 0.057(3) -0.039(3) C16 0.076(2) 0.048(2) 0.112(3) -0.0015(15) 0.037(2) -0.0165(19) C17 0.0583(17) 0.0401(16) 0.0689(19) -0.0004(12) 0.0213(14) -0.0032(13) C18 0.0442(14) 0.0458(15) 0.0470(15) -0.0026(11) 0.0157(11) 0.0021(12) C19 0.0473(16) 0.0517(18) 0.0664(19) -0.0085(12) 0.0251(13) -0.0024(14) C20 0.0384(15) 0.083(2) 0.0628(19) -0.0059(14) 0.0147(12) -0.0023(16) C21 0.051(2) 0.142(4) 0.080(3) -0.024(2) 0.0129(18) -0.023(2) C22 0.056(3) 0.257(8) 0.080(3) -0.021(4) -0.001(2) -0.013(4) C23 0.058(3) 0.261(8) 0.082(3) 0.034(4) 0.008(2) 0.040(5) C24 0.062(2) 0.155(4) 0.105(3) 0.040(3) 0.032(2) 0.049(3) C25 0.0368(16) 0.102(3) 0.074(2) 0.0153(16) 0.0186(14) 0.0207(19) C26A 0.093(4) 0.058(4) 0.178(6) 0.011(3) 0.073(4) 0.026(4) C27A 0.167(7) 0.062(4) 0.275(10) 0.049(4) 0.120(7) 0.022(5) C26B 0.067(16) 0.15(3) 0.15(3) 0.022(17) 0.053(17) -0.02(2) C27B 0.11(2) 0.08(2) 0.20(4) 0.005(19) 0.03(2) 0.01(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O2 S1 N1 . . 111.18(12) ? O2 S1 C10 . . 106.09(11) ? O3 S1 O2 . . 118.32(13) ? O3 S1 N1 . . 107.48(13) ? O3 S1 C10 . . 111.02(12) ? N1 S1 C10 . . 101.48(12) ? O5 S2 N2 . . 110.81(15) ? O5 S2 C18 . . 105.76(14) ? O6 S2 O5 . . 118.91(15) ? O6 S2 N2 . . 107.12(17) ? O6 S2 C18 . . 112.50(13) ? N2 S2 C18 . . 100.17(13) ? C1 N1 S1 . . 117.23(18) ? C1 N1 C7 . . 121.2(2) ? C7 N1 S1 . . 116.9(2) ? C25 N2 S2 . . 117.4(2) ? C25 N2 C26A . . 119.7(4) ? C25 N2 C26B . . 129.7(11) ? C26A N2 S2 . . 122.6(4) ? C26B N2 S2 . . 101.0(12) ? C2 C1 N1 . . 120.3(3) ? C2 C1 C6 . . 119.3(3) ? C6 C1 N1 . . 120.4(2) ? C1 C2 H2 . . 120.2 ? C3 C2 C1 . . 119.6(3) ? C3 C2 H2 . . 120.2 ? C2 C3 H3 . . 119.2 ? C4 C3 C2 . . 121.6(4) ? C4 C3 H3 . . 119.2 ? C3 C4 H4 . . 120.3 ? C3 C4 C5 . . 119.5(3) ? C5 C4 H4 . . 120.3 ? C4 C5 H5 . . 119.6 ? C4 C5 C6 . . 120.8(3) ? C6 C5 H5 . . 119.6 ? C1 C6 C9 . . 124.0(2) ? C5 C6 C1 . . 119.1(3) ? C5 C6 C9 . . 116.9(3) ? N1 C7 H7A . . 108.8 ? N1 C7 H7B . . 108.8 ? N1 C7 C8 . . 113.9(3) ? H7A C7 H7B . . 107.7 ? C8 C7 H7A . . 108.8 ? C8 C7 H7B . . 108.8 ? C7 C8 H8A . . 109.5 ? C7 C8 H8B . . 109.5 ? C7 C8 H8C . . 109.5 ? H8A C8 H8B . . 109.5 ? H8A C8 H8C . . 109.5 ? H8B C8 H8C . . 109.5 ? O1 C9 C6 . . 123.7(2) ? O1 C9 C10 . . 116.9(2) ? C6 C9 C10 . . 119.5(2) ? S1 C10 H10 . . 106.0 ? C9 C10 S1 . . 109.84(16) ? C9 C10 H10 . . 106.0 ? C9 C10 C11 . . 115.2(2) ? C11 C10 S1 . . 112.91(16) ? C11 C10 H10 . . 106.0 ? C10 C11 H11 . . 106.5 ? C10 C11 C18 . . 110.02(19) ? C12 C11 C10 . . 114.7(2) ? C12 C11 H11 . . 106.5 ? C12 C11 C18 . . 112.09(19) ? C18 C11 H11 . . 106.5 ? C13 C12 C11 . . 119.4(2) ? C13 C12 C17 . . 118.7(3) ? C17 C12 C11 . . 121.9(2) ? C12 C13 H13 . . 120.2 ? C12 C13 C14 . . 119.6(3) ? C14 C13 H13 . . 120.2 ? C13 C14 H14 . . 119.6 ? C15 C14 C13 . . 120.9(4) ? C15 C14 H14 . . 119.6 ? C14 C15 H15 . . 120.1 ? C16 C15 C14 . . 119.7(4) ? C16 C15 H15 . . 120.1 ? C15 C16 H16 . . 119.7 ? C15 C16 C17 . . 120.6(3) ? C17 C16 H16 . . 119.7 ? C12 C17 H17 . . 119.7 ? C16 C17 C12 . . 120.6(3) ? C16 C17 H17 . . 119.7 ? S2 C18 H18 . . 109.3 ? C11 C18 S2 . . 112.95(17) ? C11 C18 H18 . . 109.3 ? C19 C18 S2 . . 103.61(17) ? C19 C18 C11 . . 112.3(2) ? C19 C18 H18 . . 109.3 ? O4 C19 C18 . . 118.8(3) ? O4 C19 C20 . . 123.8(3) ? C20 C19 C18 . . 117.3(2) ? C21 C20 C19 . . 117.2(3) ? C25 C20 C19 . . 123.3(3) ? C25 C20 C21 . . 119.5(3) ? C20 C21 H21 . . 119.7 ? C22 C21 C20 . . 120.7(5) ? C22 C21 H21 . . 119.7 ? C21 C22 H22 . . 120.0 ? C23 C22 C21 . . 119.9(5) ? C23 C22 H22 . . 120.0 ? C22 C23 H23 . . 119.2 ? C22 C23 C24 . . 121.7(5) ? C24 C23 H23 . . 119.2 ? C23 C24 H24 . . 120.4 ? C23 C24 C25 . . 119.3(5) ? C25 C24 H24 . . 120.4 ? C20 C25 N2 . . 121.4(3) ? C20 C25 C24 . . 118.9(4) ? C24 C25 N2 . . 119.8(4) ? N2 C26A H26A . . 109.6 ? N2 C26A H26B . . 109.6 ? N2 C26A C27A . . 110.3(4) ? H26A C26A H26B . . 108.1 ? C27A C26A H26A . . 109.6 ? C27A C26A H26B . . 109.6 ? C26A C27A H27A . . 109.5 ? C26A C27A H27B . . 109.5 ? C26A C27A H27C . . 109.5 ? H27A C27A H27B . . 109.5 ? H27A C27A H27C . . 109.5 ? H27B C27A H27C . . 109.5 ? N2 C26B H26C . . 112.2 ? N2 C26B H26D . . 112.2 ? N2 C26B C27B . . 97.7(16) ? H26C C26B H26D . . 109.8 ? C27B C26B H26C . . 112.2 ? C27B C26B H26D . . 112.2 ? C26B C27B H27D . . 109.5 ? C26B C27B H27E . . 109.5 ? C26B C27B H27F . . 109.5 ? H27D C27B H27E . . 109.5 ? H27D C27B H27F . . 109.5 ? H27E C27B H27F . . 109.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag S1 O2 . 1.4250(18) ? S1 O3 . 1.4175(19) ? S1 N1 . 1.634(2) ? S1 C10 . 1.764(2) ? S2 O5 . 1.424(2) ? S2 O6 . 1.423(2) ? S2 N2 . 1.636(3) ? S2 C18 . 1.773(3) ? O1 C9 . 1.215(3) ? O4 C19 . 1.214(3) ? N1 C1 . 1.423(3) ? N1 C7 . 1.470(3) ? N2 C25 . 1.407(4) ? N2 C26A . 1.472(2) ? N2 C26B . 1.471(2) ? C1 C2 . 1.388(4) ? C1 C6 . 1.401(4) ? C2 H2 . 0.9300 ? C2 C3 . 1.379(5) ? C3 H3 . 0.9300 ? C3 C4 . 1.361(6) ? C4 H4 . 0.9300 ? C4 C5 . 1.371(5) ? C5 H5 . 0.9300 ? C5 C6 . 1.396(4) ? C6 C9 . 1.463(4) ? C7 H7A . 0.9700 ? C7 H7B . 0.9700 ? C7 C8 . 1.503(4) ? C8 H8A . 0.9600 ? C8 H8B . 0.9600 ? C8 H8C . 0.9600 ? C9 C10 . 1.530(3) ? C10 H10 . 0.9800 ? C10 C11 . 1.548(3) ? C11 H11 . 0.9800 ? C11 C12 . 1.517(3) ? C11 C18 . 1.555(3) ? C12 C13 . 1.377(4) ? C12 C17 . 1.387(4) ? C13 H13 . 0.9300 ? C13 C14 . 1.392(5) ? C14 H14 . 0.9300 ? C14 C15 . 1.365(6) ? C15 H15 . 0.9300 ? C15 C16 . 1.351(6) ? C16 H16 . 0.9300 ? C16 C17 . 1.379(4) ? C17 H17 . 0.9300 ? C18 H18 . 0.9800 ? C18 C19 . 1.531(4) ? C19 C20 . 1.446(4) ? C20 C21 . 1.401(4) ? C20 C25 . 1.398(5) ? C21 H21 . 0.9300 ? C21 C22 . 1.361(7) ? C22 H22 . 0.9300 ? C22 C23 . 1.360(8) ? C23 H23 . 0.9300 ? C23 C24 . 1.384(8) ? C24 H24 . 0.9300 ? C24 C25 . 1.401(5) ? C26A H26A . 0.9700 ? C26A H26B . 0.9700 ? C26A C27A . 1.538(2) ? C27A H27A . 0.9600 ? C27A H27B . 0.9600 ? C27A H27C . 0.9600 ? C26B H26C . 0.9700 ? C26B H26D . 0.9700 ? C26B C27B . 1.540(2) ? C27B H27D . 0.9600 ? C27B H27E . 0.9600 ? C27B H27F . 0.9600 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag S1 N1 C1 C2 . . . . 151.3(2) ? S1 N1 C1 C6 . . . . -29.5(3) ? S1 N1 C7 C8 . . . . -73.9(3) ? S1 C10 C11 C12 . . . . -81.3(2) ? S1 C10 C11 C18 . . . . 151.25(17) ? S2 N2 C25 C20 . . . . 19.5(4) ? S2 N2 C25 C24 . . . . -160.7(3) ? S2 N2 C26A C27A . . . . 85.8(6) ? S2 N2 C26B C27B . . . . -122.2(18) ? S2 C18 C19 O4 . . . . 131.0(3) ? S2 C18 C19 C20 . . . . -50.2(3) ? O1 C9 C10 S1 . . . . -152.2(2) ? O1 C9 C10 C11 . . . . 79.0(3) ? O2 S1 N1 C1 . . . . -57.6(2) ? O2 S1 N1 C7 . . . . 98.5(2) ? O2 S1 C10 C9 . . . . 63.6(2) ? O2 S1 C10 C11 . . . . -166.28(17) ? O3 S1 N1 C1 . . . . 171.43(19) ? O3 S1 N1 C7 . . . . -32.4(2) ? O3 S1 C10 C9 . . . . -166.63(17) ? O3 S1 C10 C11 . . . . -36.5(2) ? O4 C19 C20 C21 . . . . 16.1(4) ? O4 C19 C20 C25 . . . . -165.5(3) ? O5 S2 N2 C25 . . . . 59.5(3) ? O5 S2 N2 C26A . . . . -125.8(3) ? O5 S2 N2 C26B . . . . -87.0(10) ? O5 S2 C18 C11 . . . . -173.21(18) ? O5 S2 C18 C19 . . . . -51.5(2) ? O6 S2 N2 C25 . . . . -169.3(2) ? O6 S2 N2 C26A . . . . 5.4(3) ? O6 S2 N2 C26B . . . . 44.2(10) ? O6 S2 C18 C11 . . . . 55.4(2) ? O6 S2 C18 C19 . . . . 177.18(19) ? N1 S1 C10 C9 . . . . -52.65(19) ? N1 S1 C10 C11 . . . . 77.47(19) ? N1 C1 C2 C3 . . . . 179.7(3) ? N1 C1 C6 C5 . . . . 178.1(3) ? N1 C1 C6 C9 . . . . -3.6(4) ? N2 S2 C18 C11 . . . . -58.0(2) ? N2 S2 C18 C19 . . . . 63.7(2) ? C1 N1 C7 C8 . . . . 81.3(4) ? C1 C2 C3 C4 . . . . 1.9(7) ? C1 C6 C9 O1 . . . . -176.9(3) ? C1 C6 C9 C10 . . . . 1.3(4) ? C2 C1 C6 C5 . . . . -2.7(4) ? C2 C1 C6 C9 . . . . 175.6(3) ? C2 C3 C4 C5 . . . . -2.0(7) ? C3 C4 C5 C6 . . . . -0.3(7) ? C4 C5 C6 C1 . . . . 2.6(5) ? C4 C5 C6 C9 . . . . -175.7(3) ? C5 C6 C9 O1 . . . . 1.4(4) ? C5 C6 C9 C10 . . . . 179.5(3) ? C6 C1 C2 C3 . . . . 0.5(5) ? C6 C9 C10 S1 . . . . 29.5(3) ? C6 C9 C10 C11 . . . . -99.3(3) ? C7 N1 C1 C2 . . . . -3.8(4) ? C7 N1 C1 C6 . . . . 175.4(3) ? C9 C10 C11 C12 . . . . 46.0(3) ? C9 C10 C11 C18 . . . . -81.4(3) ? C10 S1 N1 C1 . . . . 54.8(2) ? C10 S1 N1 C7 . . . . -149.0(2) ? C10 C11 C12 C13 . . . . 112.5(3) ? C10 C11 C12 C17 . . . . -68.2(3) ? C10 C11 C18 S2 . . . . -73.1(2) ? C10 C11 C18 C19 . . . . 170.1(2) ? C11 C12 C13 C14 . . . . -179.8(3) ? C11 C12 C17 C16 . . . . 179.4(3) ? C11 C18 C19 O4 . . . . -106.9(3) ? C11 C18 C19 C20 . . . . 72.0(3) ? C12 C11 C18 S2 . . . . 157.98(17) ? C12 C11 C18 C19 . . . . 41.3(3) ? C12 C13 C14 C15 . . . . -0.1(5) ? C13 C12 C17 C16 . . . . -1.2(4) ? C13 C14 C15 C16 . . . . -0.1(6) ? C14 C15 C16 C17 . . . . -0.3(6) ? C15 C16 C17 C12 . . . . 1.0(5) ? C17 C12 C13 C14 . . . . 0.8(4) ? C18 S2 N2 C25 . . . . -51.8(2) ? C18 S2 N2 C26A . . . . 122.9(3) ? C18 S2 N2 C26B . . . . 161.7(10) ? C18 C11 C12 C13 . . . . -121.1(2) ? C18 C11 C12 C17 . . . . 58.2(3) ? C18 C19 C20 C21 . . . . -162.7(3) ? C18 C19 C20 C25 . . . . 15.8(4) ? C19 C20 C21 C22 . . . . 176.3(4) ? C19 C20 C25 N2 . . . . 4.1(5) ? C19 C20 C25 C24 . . . . -175.7(3) ? C20 C21 C22 C23 . . . . 0.0(7) ? C21 C20 C25 N2 . . . . -177.5(3) ? C21 C20 C25 C24 . . . . 2.8(5) ? C21 C22 C23 C24 . . . . 1.7(9) ? C22 C23 C24 C25 . . . . -1.1(8) ? C23 C24 C25 N2 . . . . 179.1(4) ? C23 C24 C25 C20 . . . . -1.2(5) ? C25 N2 C26A C27A . . . . -99.6(6) ? C25 N2 C26B C27B . . . . 97.3(19) ? C25 C20 C21 C22 . . . . -2.2(5) ? C26A N2 C25 C20 . . . . -155.3(3) ? C26A N2 C25 C24 . . . . 24.4(5) ? C26B N2 C25 C20 . . . . 154.8(14) ? C26B N2 C25 C24 . . . . -25.5(14) ? _cod_database_fobs_code 2022721