#------------------------------------------------------------------------------ #$Date: 2022-10-08 03:46:06 +0200 (Sat, 08 Oct 2022) $ #$Revision: 278498 $ #$URL: svn://www.crystallography.net/cod/cif/2/02/26/2022682.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022682 loop_ _publ_author_name 'An, Yan-Yan' 'Su, Li-Jun' 'Zhao, Xin' 'Yan, Juan-Zhi' _publ_section_title ; Cd^II^-based compound as a multi-responsive fluorescent probe for sensing Fe^III^ cations and Cr^VI^ oxyanions ; _journal_coeditor_code EF3033 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first ; ; _journal_paper_doi 10.1107/S2053229622009445 _journal_volume 78 _journal_year 2022 _chemical_formula_iupac '[Cd (C16 H10 O7) (C12 H10 N4)]' _chemical_formula_moiety 'C28 H20 Cd N4 O7' _chemical_formula_sum 'C28 H20 Cd N4 O7' _chemical_formula_weight 636.88 _chemical_name_systematic Poly[[\m~2~-1,4-bis(1H-imidazol-1-yl)benzene]{\m~2~-5-[(3-carboxyphenoxy)methyl]isophthalato}cadmium(II)] _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 103.0668(12) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 10.1105(6) _cell_length_b 12.0603(6) _cell_length_c 21.2013(12) _cell_measurement_reflns_used 9023 _cell_measurement_temperature 298(2) _cell_measurement_theta_max 28.28 _cell_measurement_theta_min 2.96 _cell_volume 2518.3(2) _computing_cell_refinement ; SAINT (Bruker, 2012) ; _computing_data_collection ; APEX2 (Bruker, 2012) ; _computing_data_reduction ; SAINT (Bruker, 2012) ; _computing_publication_material ; SHELXL2018 (Sheldrick, 2015b) ; _computing_structure_refinement ; SHELXL2018 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2014 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 298(2) _diffrn_measured_fraction_theta_full 0.989 _diffrn_measured_fraction_theta_max 0.991 _diffrn_measurement_device_type 'Bruker APEXII CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0212 _diffrn_reflns_av_unetI/netI 0.0189 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 28 _diffrn_reflns_limit_l_min -28 _diffrn_reflns_number 23463 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.285 _diffrn_reflns_theta_min 3.004 _exptl_absorpt_coefficient_mu 0.925 _exptl_absorpt_correction_T_max 0.7457 _exptl_absorpt_correction_T_min 0.6609 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Bruker, 2001) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.680 _exptl_crystal_description Block _exptl_crystal_F_000 1280 _exptl_crystal_size_max 0.250 _exptl_crystal_size_mid 0.200 _exptl_crystal_size_min 0.200 _refine_diff_density_max 0.459 _refine_diff_density_min -0.373 _refine_ls_extinction_coef 0.0114(5) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method ; SHELXL2018 (Sheldrick, 2015b) ; _refine_ls_goodness_of_fit_ref 1.083 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 363 _refine_ls_number_reflns 6188 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.083 _refine_ls_R_factor_all 0.0263 _refine_ls_R_factor_gt 0.0237 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0239P)^2^+2.0994P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0601 _refine_ls_wR_factor_ref 0.0614 _reflns_number_gt 5751 _reflns_number_total 6188 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ef3033sup1.cif _cod_data_source_block I _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 2022682 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.802 _shelx_estimated_absorpt_t_max 0.837 _shelx_hkl_file ; 3 0 0 0.13 0.14 -3 0 0 0.61 0.15 -3 0 0 0.35 0.08 -3 0 0 0.21 0.15 3 0 0 0.19 0.18 -4 0 0 687.38 16.36 5 0 0 0.38 0.25 -5 0 0 0.06 0.11 -5 0 0 -0.05 0.19 -6 0 0 43.53 1.10 6 0 0 43.27 1.31 -6 0 0 41.57 1.22 -7 0 0 -0.12 0.16 7 0 0 0.08 0.39 -7 0 0 0.06 0.29 -8 0 0 58.93 1.70 8 0 0 57.94 1.81 -9 0 0 0.42 0.32 9 0 0 -0.15 0.43 10 0 0 16.44 1.02 -11 0 0 0.75 0.41 11 0 0 0.59 0.58 -12 0 0 52.18 1.73 12 0 0 49.27 1.89 -13 0 0 0.95 0.54 13 0 0 -0.11 0.68 2 -1 0 48.75 1.26 -2 -1 0 49.94 1.25 -2 -1 0 48.96 1.22 -2 -1 0 49.25 1.19 2 -1 0 50.44 1.24 -2 1 0 51.25 1.32 2 1 0 47.55 1.19 -2 1 0 46.88 1.24 2 1 0 50.63 1.22 -3 -1 0 196.03 4.85 3 -1 0 208.99 4.87 3 -1 0 192.37 4.89 -3 -1 0 213.54 4.88 3 1 0 198.40 4.88 -3 1 0 208.64 4.89 -3 1 0 195.29 4.87 3 1 0 210.18 4.85 3 1 0 193.94 4.80 -4 -1 0 158.75 3.88 4 -1 0 152.61 3.93 -4 -1 0 163.56 3.81 4 1 0 168.52 3.89 -4 1 0 153.94 3.90 4 1 0 160.32 3.93 -5 -1 0 141.03 3.45 5 -1 0 140.31 3.51 5 1 0 138.04 3.50 -5 1 0 138.70 3.47 6 -1 0 177.24 4.52 -6 -1 0 178.97 4.45 6 1 0 187.74 4.54 -6 1 0 178.21 4.47 -7 -1 0 208.15 5.10 7 -1 0 208.47 5.19 -7 1 0 191.96 5.43 -7 1 0 216.79 4.99 7 1 0 206.16 5.18 -8 -1 0 453.79 10.92 8 -1 0 449.17 11.02 -8 1 0 459.07 10.78 -8 1 0 452.67 10.95 8 1 0 442.02 11.00 -9 -1 0 131.41 3.43 9 -1 0 134.00 3.58 9 1 0 134.57 3.57 -9 1 0 130.92 3.47 -10 -1 0 25.57 1.02 10 -1 0 25.97 1.23 10 1 0 26.54 1.35 11 -1 0 99.41 2.97 -11 -1 0 99.09 2.78 11 1 0 101.20 2.97 -11 1 0 103.58 3.11 -12 -1 0 37.50 1.35 12 -1 0 33.24 1.55 12 1 0 32.89 1.54 -12 1 0 32.36 1.36 13 -1 0 12.32 1.22 -13 -1 0 11.36 0.94 13 1 0 11.09 1.20 -13 1 0 13.18 1.19 0 2 0 0.56 0.07 0 2 0 0.49 0.09 0 2 0 0.54 0.08 -4 -2 0 60.77 1.60 -4 -2 0 64.10 1.51 4 -2 0 61.97 1.65 4 2 0 62.21 1.51 4 2 0 60.16 1.63 4 2 0 63.71 1.57 -4 2 0 57.83 1.61 5 -2 0 221.33 5.35 -5 -2 0 215.12 5.26 -5 2 0 218.16 5.31 5 2 0 213.92 5.33 6 -2 0 25.53 0.95 -6 -2 0 24.48 0.79 -6 2 0 24.15 0.85 6 2 0 25.53 0.96 7 -2 0 1.90 0.44 -7 -2 0 2.22 0.34 7 2 0 2.20 0.42 -7 2 0 1.68 0.35 -8 -2 0 14.47 0.80 8 -2 0 13.63 0.89 8 2 0 14.58 0.86 -8 2 0 14.67 0.73 -9 -2 0 12.08 0.64 9 -2 0 11.33 0.86 -9 2 0 12.33 0.50 -9 2 0 11.93 0.71 9 2 0 12.50 0.85 -10 -2 0 17.45 0.79 10 -2 0 16.71 1.02 -10 2 0 16.16 0.84 10 2 0 17.04 1.02 -10 2 0 16.58 0.62 -11 -2 0 6.74 0.67 11 -2 0 6.14 0.93 11 2 0 8.36 0.93 -11 2 0 7.80 0.76 12 -2 0 1.82 0.66 12 2 0 2.42 0.68 -12 2 0 2.48 0.56 -13 -2 0 23.13 1.29 13 -2 0 22.69 1.41 -13 2 0 22.34 1.42 13 2 0 22.45 1.42 0 -3 0 0.39 0.09 0 -3 0 0.61 0.10 0 3 0 0.34 0.10 0 3 0 0.34 0.09 0 3 0 0.31 0.11 1 -3 0 0.28 0.12 -1 -3 0 0.48 0.11 1 -3 0 0.26 0.09 1 3 0 0.11 0.11 -1 3 0 0.42 0.09 -1 3 0 0.17 0.13 1 3 0 0.35 0.11 -1 3 0 0.45 0.18 -2 -3 0 153.03 3.60 2 -3 0 144.25 3.65 2 -3 0 158.29 3.62 2 -3 0 144.55 3.57 2 3 0 146.28 3.59 -2 3 0 148.51 3.65 -2 3 0 146.45 3.62 2 3 0 151.28 3.56 -3 -3 0 18.72 0.50 3 -3 0 17.07 0.51 3 -3 0 17.31 0.62 3 3 0 17.62 0.60 3 3 0 18.15 0.50 -3 3 0 16.57 0.57 3 3 0 17.90 0.51 -5 -3 0 18.01 0.61 -5 -3 0 18.36 0.51 5 3 0 17.90 0.69 -5 3 0 16.86 0.66 5 3 0 18.05 0.53 -6 -3 0 371.92 8.82 6 -3 0 356.06 8.99 6 3 0 373.58 8.93 -6 3 0 364.90 8.89 -7 -3 0 87.10 2.29 7 -3 0 86.97 2.44 -7 3 0 87.73 2.37 7 3 0 88.27 2.41 -8 -3 0 138.94 3.51 8 -3 0 137.13 3.64 8 3 0 136.50 3.62 -8 3 0 135.45 3.56 9 -3 0 18.11 1.11 -9 -3 0 23.72 0.87 -9 3 0 22.45 0.76 9 3 0 23.90 1.07 10 -3 0 31.70 1.34 -10 -3 0 32.16 1.11 -10 3 0 31.47 0.99 10 3 0 31.97 1.33 -10 3 0 32.00 1.22 11 -3 0 35.46 1.51 -11 3 0 36.58 1.39 11 3 0 37.01 1.52 -12 -3 0 20.18 1.50 12 -3 0 19.54 1.29 -12 3 0 21.10 1.11 12 3 0 18.64 1.25 0 4 0 423.60 9.74 0 4 0 396.55 9.79 1 -4 0 22.31 0.62 1 -4 0 21.88 0.57 1 4 0 22.19 0.61 -1 4 0 21.68 0.66 -1 4 0 23.20 0.58 -1 4 0 21.76 0.62 -1 4 0 21.75 0.68 1 4 0 21.48 0.64 2 -4 0 173.92 4.31 -2 -4 0 188.86 4.36 2 -4 0 191.03 4.37 2 -4 0 167.18 4.40 2 4 0 175.89 4.35 2 4 0 185.41 4.36 -2 4 0 178.81 4.36 3 -4 0 91.00 2.21 -3 -4 0 94.52 2.23 3 -4 0 85.71 2.31 -3 4 0 88.04 2.28 3 4 0 93.68 2.19 3 4 0 88.84 2.23 4 -4 0 79.35 1.97 4 -4 0 76.18 2.08 -4 -4 0 82.48 1.96 4 4 0 77.95 2.07 4 4 0 82.28 1.95 -4 4 0 76.24 2.04 4 4 0 77.31 1.97 5 -4 0 90.78 2.48 -5 -4 0 96.15 2.31 5 4 0 95.07 2.33 5 4 0 90.92 2.46 -5 4 0 93.44 2.44 5 4 0 97.22 2.34 -6 -4 0 112.78 2.63 6 -4 0 101.21 2.97 -6 -4 0 109.19 2.69 -6 4 0 103.73 2.92 6 4 0 109.67 2.64 -7 -4 0 3.86 0.39 7 -4 0 4.53 0.69 7 4 0 4.67 0.63 -7 4 0 3.71 0.52 8 -4 0 20.40 1.11 -8 -4 0 23.80 0.83 -8 4 0 23.43 0.80 8 4 0 22.48 1.01 -9 -4 0 1.27 0.33 9 4 0 0.74 0.44 -9 4 0 1.34 0.26 -10 -4 0 28.51 1.02 10 -4 0 29.00 1.32 -10 4 0 29.21 0.97 10 4 0 28.02 1.26 -10 4 0 26.89 1.17 11 -4 0 1.87 0.60 -11 4 0 2.19 0.49 -11 4 0 1.62 0.37 11 4 0 2.81 0.63 12 -4 0 40.01 1.71 12 4 0 39.45 1.71 -12 4 0 40.00 1.58 0 -5 0 0.07 0.10 0 -5 0 0.10 0.11 0 5 0 0.48 0.15 0 5 0 -0.07 0.11 0 5 0 0.37 0.12 1 -5 0 48.26 1.20 1 -5 0 49.88 1.25 -1 5 0 49.66 1.21 -1 5 0 47.47 1.24 1 5 0 47.31 1.19 -1 5 0 45.46 1.30 1 5 0 50.82 1.25 1 5 0 48.90 1.29 2 -5 0 0.00 0.20 2 -5 0 0.14 0.21 2 -5 0 0.38 0.11 -2 5 0 0.20 0.16 -2 5 0 0.37 0.11 -2 5 0 0.04 0.16 2 5 0 0.36 0.14 2 5 0 -0.11 0.16 3 -5 0 153.36 3.97 3 -5 0 159.71 3.85 -3 -5 0 166.75 3.90 3 5 0 161.23 3.90 -3 5 0 157.74 3.93 4 -5 0 37.87 1.20 -4 -5 0 41.41 1.08 4 -5 0 39.80 1.06 4 5 0 41.81 1.03 4 5 0 39.44 1.08 -4 5 0 38.62 1.15 4 5 0 39.40 1.19 -5 -5 0 314.81 7.29 5 -5 0 302.24 7.45 5 -5 0 293.25 7.30 -5 5 0 298.68 7.40 5 5 0 303.26 7.44 5 5 0 318.81 7.28 5 5 0 295.64 7.30 6 -5 0 1.76 0.27 6 -5 0 1.67 0.40 6 5 0 2.39 0.33 6 5 0 2.36 0.42 -6 5 0 1.64 0.36 7 -5 0 134.59 3.60 7 -5 0 134.95 3.42 -7 5 0 139.11 3.46 7 5 0 135.46 3.58 -7 5 0 134.79 3.54 7 5 0 139.36 3.34 8 -5 0 38.33 1.32 -8 5 0 39.79 1.23 8 5 0 42.01 1.41 9 -5 0 99.96 2.60 -9 5 0 93.78 2.69 9 5 0 100.46 2.85 10 -5 0 31.49 1.12 10 -5 0 32.46 1.49 -10 5 0 31.61 1.09 -10 5 0 34.69 1.39 11 -5 0 35.41 1.74 11 -5 0 36.26 1.54 -11 5 0 37.02 1.17 11 5 0 35.24 1.52 -11 5 0 34.84 1.40 12 -5 0 18.40 1.08 12 5 0 14.41 1.25 0 -6 0 585.36 13.56 0 6 0 554.01 13.56 0 6 0 585.25 13.57 0 6 0 558.81 13.66 1 -6 0 824.41 19.15 -1 6 0 774.32 19.23 1 6 0 820.90 19.15 2 -6 0 64.34 1.60 -2 6 0 66.53 1.59 2 6 0 63.48 1.68 -2 6 0 62.57 1.71 -2 6 0 63.01 1.66 3 -6 0 179.01 4.34 3 -6 0 180.07 4.50 3 6 0 183.60 4.43 -3 6 0 178.41 4.43 -3 6 0 181.60 4.47 4 -6 0 11.91 0.43 -4 6 0 11.39 0.55 4 6 0 11.05 0.49 -4 6 0 10.68 0.55 5 -6 0 68.70 1.72 5 -6 0 66.66 1.91 -5 6 0 59.24 2.10 5 6 0 71.63 1.68 5 6 0 67.07 1.74 -5 6 0 66.35 1.82 5 6 0 64.67 2.08 6 -6 0 2.87 0.38 6 -6 0 2.61 0.46 6 6 0 2.65 0.37 -6 6 0 2.87 0.42 -6 6 0 2.35 0.34 6 6 0 2.77 0.45 6 6 0 2.92 0.43 7 -6 0 25.31 0.83 -7 6 0 24.63 0.92 7 6 0 24.46 1.03 7 6 0 25.70 0.79 -7 6 0 24.68 0.97 8 -6 0 14.21 0.67 8 6 0 15.07 0.54 8 6 0 14.58 0.86 -8 6 0 15.34 0.72 9 -6 0 19.49 0.80 9 6 0 19.47 1.04 -9 6 0 19.43 0.81 10 -6 0 0.36 0.50 10 -6 0 0.60 0.34 10 6 0 1.78 0.54 -10 6 0 0.36 0.42 -10 6 0 0.67 0.30 11 -6 0 30.03 1.43 -11 6 0 30.74 1.32 -11 6 0 31.18 1.07 11 6 0 27.92 1.40 12 -6 0 0.99 0.62 -12 6 0 0.99 0.54 12 6 0 -0.31 0.70 0 -7 0 0.36 0.16 0 7 0 0.76 0.17 0 7 0 0.34 0.16 0 7 0 0.49 0.21 1 -7 0 11.57 0.39 1 -7 0 12.32 0.47 1 7 0 10.95 0.53 -1 7 0 11.47 0.54 -1 7 0 11.53 0.40 -1 7 0 10.31 0.45 1 7 0 11.08 0.37 2 -7 0 48.49 1.23 2 7 0 47.85 1.36 -2 7 0 48.94 1.40 -2 7 0 49.77 1.24 -2 7 0 48.30 1.40 3 -7 0 2.28 0.24 3 7 0 1.60 0.25 -3 7 0 1.59 0.28 -3 7 0 1.94 0.28 4 -7 0 1.82 0.39 4 -7 0 1.58 0.20 -4 7 0 1.49 0.35 4 7 0 1.39 0.25 -4 7 0 1.67 0.33 5 -7 0 49.47 1.57 5 -7 0 49.36 1.33 -5 7 0 51.00 1.49 5 7 0 50.32 1.40 -5 7 0 50.36 1.49 5 7 0 49.57 1.55 6 -7 0 122.78 3.10 6 -7 0 117.01 3.30 6 7 0 128.15 3.03 6 7 0 124.32 3.28 -6 7 0 121.78 3.22 -6 7 0 125.99 3.20 6 7 0 122.76 3.10 7 -7 0 17.47 0.67 -7 7 0 17.84 0.78 7 7 0 18.40 0.67 7 7 0 17.51 0.89 -7 7 0 17.46 0.83 8 -7 0 189.54 4.70 -8 7 0 190.89 4.78 -8 7 0 192.63 4.97 8 7 0 191.22 4.63 8 7 0 183.26 4.91 9 -7 0 32.43 1.10 -9 7 0 32.13 1.80 -9 7 0 32.26 1.13 9 7 0 32.13 1.34 10 -7 0 69.64 1.97 10 -7 0 69.10 2.25 10 7 0 69.22 2.25 -10 7 0 70.28 2.00 -10 7 0 70.07 2.16 11 -7 0 14.10 1.18 -11 7 0 15.56 1.06 11 7 0 14.83 1.16 0 -8 0 337.84 8.06 0 8 0 324.74 8.06 0 8 0 346.78 8.08 0 8 0 338.22 8.21 1 -8 0 111.05 2.71 -1 8 0 113.65 2.72 -1 8 0 109.52 2.76 1 8 0 109.17 2.87 -1 8 0 110.30 3.13 2 -8 0 126.68 3.01 -2 8 0 120.70 3.10 -2 8 0 129.36 3.02 -2 8 0 118.64 3.32 2 8 0 124.71 3.17 3 -8 0 49.51 1.24 3 8 0 49.09 1.41 -3 8 0 48.94 1.46 -3 8 0 46.43 1.38 4 -8 0 11.60 0.76 4 -8 0 12.82 0.46 4 8 0 12.84 0.62 -4 8 0 11.44 0.76 -4 8 0 14.34 0.69 5 -8 0 4.89 0.35 5 -8 0 5.15 0.65 -5 8 0 3.90 0.56 -5 8 0 4.44 0.54 5 8 0 3.50 0.46 5 8 0 3.67 0.60 6 -8 0 42.73 1.18 -6 8 0 42.29 1.36 -6 8 0 42.17 1.34 6 8 0 43.47 1.45 6 8 0 43.06 1.26 7 -8 0 0.97 0.26 -7 8 0 0.28 0.36 -7 8 0 1.15 0.30 7 8 0 1.06 0.26 7 8 0 1.44 0.41 8 -8 0 2.97 0.36 -8 8 0 3.46 0.50 -8 8 0 4.34 0.56 8 8 0 2.80 0.53 8 8 0 3.46 0.46 9 -8 0 9.81 0.91 9 -8 0 7.79 0.64 -9 8 0 9.79 0.81 9 8 0 10.75 0.89 10 -8 0 4.47 0.69 10 -8 0 3.68 0.55 10 8 0 3.49 0.65 -10 8 0 3.57 0.59 11 -8 0 10.18 1.10 -11 8 0 9.94 0.76 -11 8 0 8.71 1.27 11 8 0 9.03 1.44 0 -9 0 0.17 0.22 0 9 0 0.04 0.19 0 9 0 0.41 0.30 1 9 0 4.21 0.53 -1 9 0 4.08 0.37 -1 9 0 4.77 0.35 -1 9 0 5.28 0.54 2 -9 0 0.25 0.17 2 9 0 0.09 0.27 -2 9 0 0.42 0.19 -2 9 0 -0.21 0.24 -2 9 0 0.00 0.28 3 -9 0 73.14 1.82 -3 9 0 73.09 2.06 -3 9 0 72.83 1.97 -4 9 0 98.03 2.64 4 9 0 92.77 2.74 -4 9 0 99.93 2.58 5 -9 0 112.80 2.75 5 9 0 111.25 2.91 -5 9 0 111.08 2.99 6 -9 0 23.84 0.75 -6 9 0 24.52 0.97 6 9 0 24.08 1.04 6 9 0 23.18 0.89 -6 9 0 23.45 0.96 7 -9 0 125.99 3.16 7 9 0 126.08 3.47 -7 9 0 127.70 3.40 7 9 0 127.22 3.25 8 -9 0 21.38 0.75 8 -9 0 25.04 1.19 -8 9 0 22.72 1.21 8 9 0 21.82 0.83 9 -9 0 46.70 1.71 9 9 0 44.63 1.66 -9 9 0 44.86 1.50 -9 9 0 44.19 1.59 10 -9 0 16.82 1.21 -10 9 0 14.41 1.04 -10 9 0 15.84 1.03 10 9 0 15.46 1.15 0 10 0 6.59 0.60 0 10 0 6.75 0.40 -1 10 0 114.22 2.75 1 10 0 109.17 2.92 -1 10 0 107.85 2.93 -1 10 0 106.93 2.76 -2 10 0 9.17 0.41 -2 10 0 8.10 0.93 2 10 0 8.84 0.64 -2 10 0 9.54 0.54 -3 10 0 26.90 0.99 3 10 0 29.28 1.04 -3 10 0 28.21 1.26 4 10 0 104.74 2.76 -4 10 0 103.34 2.73 -4 10 0 101.65 2.81 5 10 0 80.60 2.20 -5 10 0 78.78 2.21 6 10 0 5.35 0.71 -6 10 0 4.59 0.60 6 10 0 3.92 0.55 7 -10 0 5.86 0.47 7 -10 0 5.54 0.92 7 10 0 5.31 0.59 7 10 0 4.83 0.68 -7 10 0 5.20 0.64 8 -10 0 1.05 0.50 -8 10 0 0.62 0.36 8 10 0 0.87 0.49 9 -10 0 1.98 0.61 9 10 0 1.71 0.57 -9 10 0 1.36 0.51 10 -10 0 2.73 0.65 -10 10 0 1.59 0.46 -10 10 0 2.03 1.06 0 11 0 0.69 0.32 0 11 0 0.42 0.21 1 11 0 19.77 0.88 -1 11 0 19.56 0.89 -1 11 0 21.20 0.71 -2 11 0 49.34 1.42 2 11 0 50.85 1.57 3 11 0 -0.27 0.29 -3 11 0 0.38 0.33 -4 11 0 125.41 3.31 4 11 0 129.77 3.37 5 11 0 2.23 0.38 -5 11 0 2.44 0.43 -5 11 0 2.83 0.42 -6 11 0 27.54 1.09 6 11 0 25.47 1.00 -6 11 0 26.81 1.12 6 11 0 26.60 1.48 7 11 0 1.73 0.50 7 11 0 0.83 0.33 -7 11 0 1.25 0.51 -7 11 0 1.49 0.47 8 -11 0 75.50 2.37 8 11 0 71.68 2.07 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7.13 0.67 -10 8 3 8.01 0.82 9 -8 -3 1.44 0.30 9 -8 -3 1.30 0.55 -9 8 3 1.27 0.48 9 8 -3 0.87 0.29 8 -8 -3 8.58 0.51 8 -8 -3 9.52 0.83 8 8 -3 8.91 0.62 -8 8 3 10.02 0.76 8 8 -3 10.30 0.83 7 -8 -3 0.89 0.23 7 8 -3 1.89 0.43 7 8 -3 1.54 0.32 -7 8 3 1.09 0.39 6 -8 -3 74.21 2.14 6 8 -3 73.44 2.15 -6 8 3 72.24 2.07 6 8 -3 73.79 2.02 5 -8 -3 282.66 7.16 -5 8 3 291.09 7.11 5 8 -3 292.85 7.08 4 -8 -3 34.72 1.20 -4 8 3 32.65 1.44 4 8 -3 36.02 1.13 3 8 -3 216.40 5.36 -3 8 3 215.35 5.31 -2 8 3 7.64 0.48 2 8 -3 7.18 0.56 -1 -8 3 200.69 4.84 -1 8 3 185.73 5.05 -1 8 3 202.25 4.84 1 8 -3 204.62 4.98 0 -8 3 127.55 3.13 0 -8 3 125.78 3.17 0 8 3 127.06 3.16 0 8 3 128.22 3.28 0 8 -3 127.12 3.13 0 8 3 132.69 3.12 1 -8 3 214.53 5.13 -1 8 -3 200.97 5.37 1 8 3 208.69 5.10 -1 8 -3 215.58 5.14 1 8 3 217.57 5.24 2 -8 3 22.76 0.71 -2 8 -3 23.87 0.89 -2 8 -3 22.48 0.77 2 8 3 23.03 0.82 2 8 3 22.22 0.68 3 -8 3 65.03 1.72 -3 8 -3 67.13 1.87 3 8 3 66.16 1.80 3 8 3 66.20 1.71 -3 8 -3 66.27 1.80 4 -8 3 39.85 1.13 -4 8 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3 -4 77.60 2.23 -8 3 4 78.73 2.17 -7 -3 4 65.97 1.78 7 -3 -4 67.75 1.97 7 3 -4 68.76 1.94 7 3 -4 67.56 1.76 -7 3 4 67.28 1.89 -6 -3 4 0.42 0.19 6 -3 -4 0.66 0.34 6 3 -4 0.35 0.31 -6 3 4 0.58 0.30 6 3 -4 0.26 0.20 5 -3 -4 129.19 3.34 -5 -3 4 128.15 3.22 -5 -3 4 146.06 3.32 5 3 -4 129.26 3.33 5 3 -4 129.11 3.26 -5 3 4 125.90 3.31 5 3 -4 135.11 3.23 4 -3 -4 34.51 1.06 -4 -3 4 35.78 0.94 -4 -3 4 37.29 0.99 4 -3 -4 36.94 0.94 4 3 -4 34.73 1.06 4 3 -4 37.05 0.94 4 3 -4 35.67 1.01 -3 -3 4 16.82 0.56 3 -3 -4 16.15 0.60 -3 -3 4 17.76 0.48 3 -3 -4 17.66 0.47 -3 -3 4 18.14 0.56 3 3 -4 18.25 0.57 3 3 -4 19.09 0.49 -3 3 4 17.82 0.62 -3 3 4 15.89 0.58 -2 -3 4 24.16 0.71 -2 -3 4 24.99 0.71 2 -3 -4 25.92 0.73 -2 -3 4 25.57 0.63 2 -3 -4 24.32 0.72 -2 3 4 25.47 0.73 2 3 -4 25.31 0.72 2 3 -4 23.92 0.72 -2 3 4 23.84 0.75 -1 -3 4 3.31 0.25 1 -3 -4 3.63 0.26 -1 -3 4 3.48 0.25 -1 3 4 3.35 0.25 -1 3 4 3.49 0.26 1 3 -4 3.27 0.25 1 3 -4 3.64 0.27 0 -3 4 0.68 0.14 0 -3 4 0.80 0.12 0 -3 4 0.61 0.15 0 3 -4 0.80 0.15 0 3 -4 0.69 0.15 -1 3 -4 0.98 0.17 2 -3 4 30.17 0.84 2 -3 4 29.82 0.88 2 -3 4 30.06 0.84 2 -3 4 32.02 0.87 -2 3 -4 29.34 0.84 2 3 4 29.20 0.84 -2 3 -4 31.73 0.90 -2 3 -4 31.11 0.84 -2 3 -4 29.27 0.85 3 -3 4 2.00 0.28 3 -3 4 1.89 0.26 3 3 4 2.19 0.28 -3 3 -4 2.08 0.25 3 3 4 1.96 0.24 -3 3 -4 1.75 0.29 3 3 4 1.66 0.16 4 -3 4 95.98 2.49 4 -3 4 95.66 2.43 -4 3 -4 94.74 2.47 4 3 4 95.13 2.45 -4 3 -4 99.31 2.40 5 -3 4 86.56 2.30 5 -3 4 84.28 2.22 -5 3 -4 86.18 2.27 5 3 4 84.44 2.26 -5 3 -4 88.87 2.18 6 -3 4 84.32 2.24 6 -3 4 85.61 2.71 -6 3 -4 82.99 2.28 -6 3 -4 85.88 2.16 6 3 4 86.18 2.30 7 -3 4 77.53 2.24 7 -3 4 78.60 2.14 7 3 4 80.41 2.22 -7 3 -4 77.53 2.18 -7 3 -4 79.55 2.02 8 -3 4 182.45 4.72 8 -3 4 179.39 4.58 -8 3 -4 181.79 4.44 8 3 4 183.09 4.68 9 -3 4 34.30 1.20 9 -3 4 36.25 1.38 9 3 4 35.34 1.35 -9 3 -4 35.85 1.07 10 -3 4 76.74 2.65 10 -3 4 74.21 2.20 10 3 4 74.04 2.30 -10 3 -4 73.15 2.27 11 -3 4 41.52 1.66 11 -3 4 47.91 1.84 11 3 4 39.40 1.96 -11 3 -4 44.29 1.59 12 -3 4 7.86 1.07 12 -3 4 8.68 0.85 12 3 4 6.71 1.07 13 -4 -4 3.75 0.74 13 4 -4 3.22 0.79 -13 4 4 4.08 0.67 12 -4 -4 5.28 0.78 12 4 -4 5.02 0.77 -12 4 4 5.57 0.82 11 -4 -4 9.75 0.97 -11 -4 4 10.16 0.67 -11 4 4 11.89 0.86 11 4 -4 9.62 0.97 -10 -4 4 8.05 0.57 10 -4 -4 7.54 1.13 -10 4 4 9.11 0.73 -9 -4 4 0.67 0.31 -8 -4 4 18.64 0.70 8 -4 -4 20.18 0.97 -8 4 4 19.33 0.85 -7 -4 4 2.53 0.29 7 -4 -4 2.66 0.48 7 4 -4 3.21 0.40 7 4 -4 2.54 0.42 -7 4 4 2.79 0.40 6 -4 -4 156.43 4.20 -6 -4 4 158.35 4.02 6 4 -4 160.69 4.06 6 4 -4 184.44 4.22 -5 -4 4 33.89 0.93 5 -4 -4 34.39 1.10 5 4 -4 35.15 1.01 5 4 -4 35.12 1.10 5 4 -4 35.56 0.94 4 -4 -4 585.35 13.26 4 -4 -4 530.69 13.38 -4 4 4 555.79 13.37 4 4 -4 591.29 13.26 4 4 -4 554.27 13.34 4 4 -4 534.41 13.39 -3 -4 4 12.67 0.51 3 -4 -4 15.20 0.56 3 4 -4 14.32 0.52 2 -4 -4 574.41 14.19 -2 4 4 595.61 14.18 -2 4 4 615.70 14.20 -1 -4 4 110.92 2.80 -1 -4 4 114.54 2.74 1 -4 -4 119.31 2.81 1 4 -4 118.10 2.84 -1 4 4 115.15 2.82 1 4 -4 108.70 2.83 -1 4 4 111.79 2.81 1 -4 4 50.40 1.27 1 -4 4 48.40 1.28 -1 4 -4 50.00 1.28 -1 4 -4 48.54 1.27 -1 4 -4 48.46 1.31 2 -4 4 377.78 9.18 2 -4 4 380.04 9.14 -2 4 -4 380.50 9.15 -2 4 -4 380.56 9.16 -2 4 -4 389.96 9.13 3 -4 4 14.82 0.54 3 -4 4 14.34 0.61 3 4 4 14.71 0.56 3 4 4 14.30 0.45 -3 4 -4 14.79 0.54 3 4 4 14.71 0.50 4 -4 4 111.24 2.86 4 -4 4 109.03 2.83 -4 4 -4 111.00 2.83 4 4 4 109.70 2.82 4 4 4 111.04 2.69 -4 4 -4 113.73 2.79 5 -4 4 44.37 1.29 5 -4 4 46.10 1.40 -5 4 -4 45.97 1.26 5 4 4 45.00 1.34 -5 4 -4 46.29 1.36 6 -4 4 4.51 0.53 6 -4 4 4.19 0.66 -6 4 -4 4.29 0.38 6 4 4 4.22 0.78 -6 4 -4 3.84 0.50 7 -4 4 0.37 0.32 7 -4 4 0.25 0.43 -7 4 -4 0.46 0.21 -7 4 -4 0.22 0.30 7 4 4 0.31 0.39 8 -4 4 3.97 0.51 8 -4 4 3.09 0.54 -8 4 -4 3.87 0.39 8 4 4 2.73 0.47 9 -4 4 1.98 0.51 9 -4 4 1.69 0.38 -9 4 -4 1.24 0.27 9 4 4 1.14 0.49 10 -4 4 27.46 1.09 10 -4 4 28.51 1.31 -10 4 -4 29.07 1.20 10 4 4 27.65 1.37 11 -4 4 1.74 0.61 11 4 4 1.90 0.80 -11 4 -4 1.66 0.52 12 -4 4 40.98 2.08 12 -4 4 46.86 1.64 12 4 4 47.63 2.01 -12 4 -4 48.32 1.76 12 -5 -4 15.09 1.20 12 5 -4 12.82 1.17 -12 5 4 13.35 1.03 11 -5 -4 105.51 3.17 -11 -5 4 110.69 2.88 -11 5 4 111.13 3.10 11 5 -4 109.42 3.18 10 -5 -4 43.22 1.78 -10 -5 4 42.20 1.28 10 5 -4 40.51 1.87 -10 5 4 38.58 1.68 -9 -5 4 133.38 3.40 9 5 -4 136.18 3.38 -8 -5 4 40.81 1.18 8 -5 -4 41.56 1.44 8 5 -4 42.25 1.20 -7 -5 4 159.54 3.92 7 -5 -4 160.11 4.15 7 5 -4 161.11 4.15 7 5 -4 161.88 3.98 -7 5 4 158.70 4.09 -6 -5 4 23.86 0.71 6 -5 -4 24.89 0.99 6 5 -4 24.52 0.96 6 5 -4 24.58 0.73 6 5 -4 24.25 0.83 -6 5 4 24.51 0.91 5 -5 -4 179.55 4.58 -5 -5 4 181.91 4.40 5 5 -4 182.24 4.51 5 5 -4 184.60 4.60 5 5 -4 191.69 4.41 -5 5 4 179.15 4.56 4 -5 -4 55.97 1.60 -4 5 4 57.56 1.57 4 5 -4 58.75 1.55 3 -5 -4 31.18 0.97 -3 -5 4 32.11 0.94 3 5 -4 32.28 0.95 -3 5 4 31.81 0.95 -2 -5 4 50.15 1.34 2 -5 -4 49.39 1.37 2 5 -4 51.24 1.37 -2 5 4 50.83 1.35 -1 -5 4 114.99 2.92 1 -5 -4 125.26 2.93 1 5 -4 116.99 2.96 -1 5 4 116.35 2.92 0 -5 4 80.76 1.95 0 -5 4 78.44 1.99 0 5 -4 79.90 2.00 0 5 -4 79.42 1.96 0 5 4 78.88 1.99 0 5 -4 78.64 2.05 1 -5 4 0.66 0.16 1 -5 4 0.45 0.17 -1 5 -4 0.82 0.18 -1 5 -4 0.46 0.16 -1 5 -4 0.36 0.18 2 -5 4 189.21 4.58 -2 5 -4 186.57 4.62 -2 5 -4 189.39 4.59 3 -5 4 135.29 3.36 3 -5 4 135.52 3.44 -3 5 -4 136.07 3.39 -3 5 -4 136.82 3.40 3 5 4 136.00 3.33 4 -5 4 329.52 7.95 4 -5 4 333.12 8.04 -4 5 -4 332.79 7.98 4 5 4 326.30 7.88 4 5 4 331.47 8.01 -4 5 -4 324.66 8.00 5 -5 4 147.04 3.58 5 -5 4 136.41 3.81 5 5 4 145.84 3.65 -5 5 -4 137.84 3.69 -5 5 -4 147.74 3.59 5 5 4 143.95 3.47 6 -5 4 87.44 2.49 6 -5 4 91.47 2.37 -6 5 -4 90.12 2.35 -6 5 -4 88.77 2.44 6 5 4 92.18 2.46 7 -5 4 128.17 3.21 7 -5 4 122.82 3.34 -7 5 -4 124.75 3.16 7 5 4 123.93 3.29 -7 5 -4 121.87 3.27 8 -5 4 47.35 1.61 8 -5 4 48.25 1.46 8 5 4 50.04 1.59 -8 5 -4 47.72 1.40 9 -5 4 44.81 1.61 9 -5 4 45.17 1.43 -9 5 -4 46.23 1.36 9 5 4 45.87 1.60 10 -5 4 3.93 0.67 10 -5 4 5.69 0.85 -10 5 -4 3.74 0.56 -10 5 -4 3.47 0.40 11 -5 4 30.57 1.45 11 -5 4 33.94 1.26 11 5 4 27.86 1.41 -11 5 -4 31.71 1.36 12 -6 -4 0.88 1.22 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0.93 0.23 2 6 4 0.64 0.19 3 -6 4 181.31 4.52 3 -6 4 193.59 4.80 3 6 4 182.42 4.51 -3 6 -4 185.14 4.59 -3 6 -4 182.37 4.56 4 -6 4 65.08 1.72 4 6 4 64.17 1.68 -4 6 -4 64.78 1.78 4 6 4 66.04 1.82 -4 6 -4 64.54 1.79 5 -6 4 56.70 1.56 5 -6 4 53.33 1.69 -5 6 -4 58.43 1.60 -5 6 -4 57.67 1.64 5 6 4 55.89 1.47 6 -6 4 16.12 0.72 6 -6 4 15.85 0.87 -6 6 -4 16.55 0.77 6 6 4 15.54 0.81 -6 6 -4 16.49 0.72 7 -6 4 0.24 0.31 7 -6 4 0.11 0.45 -7 6 -4 0.06 0.52 -7 6 -4 0.01 0.31 7 6 4 0.37 0.36 8 -6 4 4.78 0.55 8 -6 4 5.44 0.89 -8 6 -4 5.23 0.63 8 6 4 4.77 0.68 -8 6 -4 5.78 0.57 9 -6 4 14.99 0.77 -9 6 -4 14.54 0.96 -9 6 -4 15.67 0.75 10 -6 4 0.45 0.42 10 -6 4 0.63 0.51 -10 6 -4 -0.15 0.30 10 6 4 0.62 0.51 -10 6 -4 0.29 0.43 11 -6 4 36.41 1.35 11 -6 4 32.28 1.54 11 6 4 32.71 1.51 -11 6 -4 30.20 1.70 12 -7 -4 22.58 1.37 12 7 -4 19.30 1.32 -12 7 4 22.46 1.01 -12 7 4 21.30 1.20 11 -7 -4 8.91 0.62 11 -7 -4 10.84 1.06 11 7 -4 8.03 1.02 -11 7 4 10.87 0.96 -11 7 4 9.04 0.98 10 -7 -4 44.11 1.33 10 -7 -4 42.41 1.64 10 7 -4 44.12 1.64 10 7 -4 43.30 1.30 -10 7 4 43.00 1.56 9 -7 -4 24.95 0.87 9 -7 -4 26.00 1.21 9 7 -4 26.16 0.91 -9 7 4 25.34 1.11 9 7 -4 26.92 1.22 8 -7 -4 204.23 4.94 -8 7 4 197.62 5.16 8 7 -4 205.98 5.03 7 -7 -4 25.93 1.08 7 -7 -4 25.69 0.77 7 7 -4 25.61 0.91 -7 7 4 24.93 0.99 6 -7 -4 98.72 2.71 -6 7 4 100.55 2.67 6 7 -4 100.59 2.61 6 7 -4 98.37 2.73 5 -7 -4 17.53 0.85 -5 7 4 17.50 0.79 5 7 -4 18.77 0.75 4 -7 -4 6.60 0.71 -4 7 4 7.07 0.54 4 7 -4 6.88 0.51 3 7 -4 18.32 0.72 -3 7 4 18.22 0.70 -2 -7 4 9.69 0.47 2 7 -4 9.66 0.53 -2 7 4 9.32 0.48 -1 -7 4 62.44 1.67 -1 7 4 63.31 1.66 1 7 -4 65.05 1.80 0 -7 4 265.70 6.62 0 -7 4 284.92 6.58 0 7 -4 275.57 6.72 0 7 -4 270.89 6.58 0 7 4 269.96 6.62 0 7 4 281.02 6.57 1 -7 4 20.37 0.67 1 7 4 20.87 0.64 -1 7 -4 21.31 0.67 1 7 4 20.65 0.65 1 7 4 21.38 0.74 2 -7 4 318.55 7.81 2 7 4 327.23 7.86 -2 7 -4 323.93 7.91 2 7 4 323.45 7.79 -2 7 -4 329.81 7.84 3 -7 4 97.37 2.47 -3 7 -4 98.37 2.60 3 7 4 97.94 2.49 -3 7 -4 96.35 2.52 4 -7 4 140.86 3.43 4 -7 4 136.09 3.57 4 7 4 141.34 3.42 4 7 4 133.85 3.67 -4 7 -4 135.43 3.62 5 -7 4 112.32 2.87 5 -7 4 109.03 3.02 5 7 4 111.98 2.82 5 7 4 113.57 2.99 -5 7 -4 112.01 2.95 -5 7 -4 116.03 2.95 6 -7 4 151.61 4.02 6 -7 4 154.99 3.87 6 7 4 152.39 3.82 -6 7 -4 157.74 3.93 6 7 4 154.79 4.00 -6 7 -4 153.38 3.97 7 -7 4 27.60 1.14 7 -7 4 28.08 0.99 -7 7 -4 26.53 0.99 -7 7 -4 26.74 1.06 7 7 4 27.59 1.09 8 -7 4 30.08 1.26 8 -7 4 29.90 1.04 -8 7 -4 28.47 1.04 -8 7 -4 28.39 1.15 9 -7 4 27.05 1.04 9 -7 4 27.20 1.27 9 7 4 27.60 1.36 -9 7 -4 26.55 1.17 -9 7 -4 25.85 1.00 10 -7 4 36.59 1.53 10 -7 4 35.35 1.50 -10 7 -4 36.15 1.21 -10 7 -4 35.91 1.43 10 7 4 33.56 1.48 11 -7 4 3.72 0.83 -11 7 -4 2.89 0.61 11 7 4 3.02 0.73 11 -8 -4 0.10 0.65 11 8 -4 0.10 0.68 -11 8 4 0.05 0.66 10 -8 -4 0.63 0.53 10 8 -4 0.53 0.51 -10 8 4 0.70 0.36 -10 8 4 0.58 0.45 9 -8 -4 1.13 0.29 9 -8 -4 1.38 0.54 9 8 -4 0.71 0.34 -9 8 4 0.71 0.45 8 -8 -4 60.84 1.59 8 -8 -4 59.99 1.92 -8 8 4 60.39 1.86 8 8 -4 59.48 1.82 -7 8 4 66.72 1.92 7 8 -4 62.99 1.96 6 -8 -4 216.53 5.52 6 8 -4 217.61 5.43 -6 8 4 217.24 5.45 5 -8 -4 80.61 2.29 5 8 -4 79.93 2.25 -5 8 4 84.02 2.24 4 8 -4 36.12 1.19 -3 8 4 8.96 0.55 3 8 -4 7.59 0.59 -2 -8 4 307.71 7.34 2 8 -4 294.06 7.53 -2 8 4 307.16 7.35 -1 -8 4 8.76 0.47 -1 8 4 8.75 0.47 0 -8 4 513.70 12.06 0 -8 4 490.28 12.11 0 8 -4 522.38 12.13 0 8 4 520.97 12.05 0 8 4 506.68 12.21 0 8 4 485.08 12.10 1 -8 4 -0.08 0.20 1 8 4 0.18 0.20 1 8 4 -0.22 0.25 -1 8 -4 0.18 0.30 -1 8 -4 -0.34 0.22 2 -8 4 139.65 3.53 -2 8 -4 144.10 3.67 2 8 4 141.83 3.61 2 8 4 144.30 3.50 -2 8 -4 144.63 3.56 3 -8 4 18.26 0.66 -3 8 -4 18.99 0.81 3 8 4 18.72 0.71 -3 8 -4 17.41 0.72 3 8 4 18.63 0.62 4 -8 4 122.71 3.12 4 8 4 123.22 3.15 -4 8 -4 125.75 3.54 -4 8 -4 126.32 3.26 5 -8 4 0.83 0.30 5 -8 4 0.62 0.38 5 8 4 0.42 0.36 5 8 4 0.70 0.23 -5 8 -4 0.98 0.35 -5 8 -4 1.01 0.30 6 -8 4 0.35 0.30 6 -8 4 0.70 0.40 -6 8 -4 0.26 0.32 -6 8 -4 0.44 0.29 6 8 4 0.42 0.57 6 8 4 0.51 0.31 7 -8 4 1.21 0.38 7 -8 4 1.28 0.48 -7 8 -4 1.22 0.36 -7 8 -4 1.81 0.45 7 8 4 1.77 0.64 7 8 4 1.19 0.23 8 -8 4 28.22 1.03 8 -8 4 28.78 1.59 -8 8 -4 28.29 1.07 -8 8 -4 30.44 1.64 8 8 4 28.42 1.36 9 -8 4 10.66 0.96 9 -8 4 10.52 0.71 9 8 4 12.62 0.92 -9 8 -4 8.62 0.74 -9 8 -4 10.99 0.85 10 -8 4 52.60 1.94 10 -8 4 51.48 1.76 -10 8 -4 51.89 1.83 10 8 4 50.45 1.87 11 -9 -4 58.75 2.13 -11 9 4 58.29 2.03 -11 9 4 58.66 1.88 11 9 -4 58.27 2.14 10 -9 -4 7.16 0.99 10 9 -4 6.34 0.96 -10 9 4 8.36 0.75 -10 9 4 5.20 0.85 9 -9 -4 68.17 2.22 9 9 -4 68.34 2.23 9 9 -4 70.96 1.98 -9 9 4 70.60 2.16 -9 9 4 68.97 2.08 8 -9 -4 11.99 1.41 -8 9 4 9.10 0.77 8 9 -4 10.28 0.74 7 -9 -4 31.30 1.32 7 9 -4 36.64 1.20 -7 9 4 35.88 1.26 6 9 -4 49.19 1.49 -6 9 4 47.86 1.52 5 -9 -4 25.91 1.06 -5 9 4 26.46 0.98 5 9 -4 26.31 0.99 4 9 -4 33.08 1.39 -3 9 4 60.18 1.69 3 9 -4 59.96 1.75 -2 -9 4 1.54 0.30 -2 9 4 1.80 0.32 2 9 -4 1.73 0.34 -1 -9 4 32.93 1.01 -1 9 4 33.41 1.01 -1 9 4 33.21 1.13 1 9 -4 33.70 1.15 0 -9 4 22.51 0.69 0 -9 4 21.94 0.75 0 9 4 21.54 0.88 0 9 4 22.12 0.74 0 9 -4 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9 179.75 4.44 0 3 -9 186.03 4.44 0 3 -9 183.62 4.50 1 -3 9 115.69 2.97 -1 3 -9 127.34 2.95 1 3 9 116.44 2.93 1 3 9 113.94 2.85 -1 3 -9 114.70 2.96 2 -3 9 36.48 1.11 2 -3 9 36.84 1.06 -2 3 -9 37.20 1.08 2 3 9 36.46 1.08 2 3 9 38.95 1.00 2 3 9 37.09 1.02 3 -3 9 387.70 9.55 3 -3 9 390.69 9.58 3 3 9 393.70 9.50 3 3 9 390.46 9.57 -3 3 -9 404.08 9.67 3 3 9 413.83 9.48 4 -3 9 53.11 1.49 4 -3 9 48.63 1.66 4 3 9 50.72 1.42 -4 3 -9 52.27 1.41 5 -3 9 258.27 6.42 5 -3 9 261.84 6.42 -5 3 -9 258.20 6.32 5 3 9 263.19 6.38 6 -3 9 127.60 3.34 6 -3 9 126.53 3.32 6 3 9 127.22 3.30 -6 3 -9 128.67 3.18 7 -3 9 202.55 5.19 7 -3 9 203.05 5.18 7 3 9 206.79 5.17 -7 3 -9 207.35 5.00 8 -3 9 44.06 1.51 8 3 9 43.77 1.47 -8 3 -9 42.82 1.21 9 -3 9 6.51 0.80 9 3 9 5.64 0.66 10 -3 9 0.76 0.52 10 -3 9 -0.10 0.46 10 3 9 0.26 0.88 11 -3 9 2.18 0.63 11 -3 9 1.69 0.60 11 3 9 1.60 0.63 12 -4 -9 0.20 0.61 12 4 -9 1.00 0.62 -12 4 9 0.55 0.49 -11 -4 9 8.83 0.62 11 -4 -9 9.13 0.98 -11 4 9 8.98 0.79 11 4 -9 7.54 0.93 -10 -4 9 1.16 0.39 10 -4 -9 1.07 0.49 -10 4 9 1.14 0.44 10 4 -9 1.34 0.51 9 -4 -9 75.33 2.55 -9 -4 9 86.80 2.25 9 4 -9 88.15 2.30 8 -4 -9 3.14 0.50 -8 -4 9 2.39 0.44 8 4 -9 3.30 0.67 -8 4 9 4.33 0.54 7 -4 -9 115.26 3.01 -7 -4 9 110.06 2.83 7 4 -9 112.78 3.01 -7 4 9 109.69 2.98 7 4 -9 115.92 2.96 6 -4 -9 0.52 0.37 -6 -4 9 -0.03 0.22 6 4 -9 0.63 0.34 6 4 -9 0.60 0.30 -6 4 9 1.07 0.35 5 -4 -9 342.13 7.98 -5 -4 9 333.78 8.00 5 -4 -9 327.07 8.09 5 4 -9 332.52 8.12 5 4 -9 332.39 8.13 4 -4 -9 55.03 1.36 -4 -4 9 51.74 1.39 4 -4 -9 50.98 1.46 -4 4 9 56.69 1.53 -4 4 9 54.47 1.35 4 4 -9 52.65 1.52 4 4 -9 52.42 1.50 3 -4 -9 312.13 7.31 -3 -4 9 304.68 7.33 -3 -4 9 308.58 7.42 3 -4 -9 299.59 7.36 -3 4 9 300.21 7.43 -3 4 9 304.98 7.30 3 4 -9 310.78 7.45 2 -4 -9 8.98 0.33 -2 -4 9 8.60 0.46 -2 4 9 10.10 0.44 2 4 -9 8.79 0.50 -2 4 9 8.85 0.35 -1 -4 9 298.77 7.47 -1 4 9 329.83 7.39 -1 4 9 309.58 7.49 -1 4 9 305.66 7.39 1 4 -9 299.42 7.49 0 -4 9 0.96 0.24 0 4 9 1.37 0.20 0 4 -9 0.84 0.23 0 4 9 0.86 0.18 1 -4 9 40.17 1.17 -1 4 -9 39.80 1.16 1 4 9 39.09 1.10 2 -4 9 7.96 0.50 2 4 9 8.28 0.38 -2 4 -9 8.03 0.47 2 4 9 8.18 0.45 3 -4 9 2.48 0.34 3 -4 9 1.85 0.32 3 4 9 1.56 0.21 3 4 9 2.10 0.34 -3 4 -9 1.75 0.27 4 -4 9 11.62 0.68 4 4 9 12.42 0.46 4 4 9 12.12 0.58 -4 4 -9 12.87 0.59 5 -4 9 11.14 0.68 5 -4 9 9.72 0.95 -5 4 -9 11.12 0.56 5 4 9 10.85 0.62 6 -4 9 2.05 0.73 6 -4 9 1.62 0.37 6 4 9 1.38 0.68 -6 4 -9 1.30 0.26 7 -4 9 35.36 1.23 7 -4 9 35.12 1.36 7 4 9 36.54 1.25 -7 4 -9 36.85 1.09 8 -4 9 12.01 0.86 8 -4 9 11.35 1.15 -8 4 -9 12.79 0.61 8 4 9 12.51 0.83 9 -4 9 38.63 1.49 9 4 9 41.25 1.47 10 -4 9 5.34 0.86 10 -4 9 5.56 0.78 11 -4 9 68.57 2.25 11 -4 9 65.32 2.15 11 4 9 66.29 2.22 12 -5 -9 34.68 1.59 -12 -5 9 33.33 1.15 12 5 -9 32.35 1.59 -12 5 9 35.11 1.48 -11 -5 9 50.07 1.48 11 -5 -9 49.25 1.81 11 5 -9 49.36 1.83 -11 5 9 50.32 1.72 10 -5 -9 47.33 1.70 -10 -5 9 46.34 1.43 -10 5 9 51.76 2.15 10 5 -9 48.42 1.50 -9 -5 9 107.85 2.76 9 5 -9 112.00 2.89 9 5 -9 104.15 3.17 8 -5 -9 87.44 2.51 -8 -5 9 89.31 2.30 8 5 -9 87.51 2.52 8 5 -9 94.83 2.46 7 -5 -9 31.84 1.17 -7 -5 9 31.00 0.92 7 5 -9 29.45 1.21 -7 5 9 31.89 1.27 7 5 -9 32.77 1.17 -6 -5 9 13.44 0.51 6 -5 -9 13.64 0.50 -6 5 9 12.75 0.71 6 5 -9 13.16 0.74 6 5 -9 13.17 0.74 -5 -5 9 0.02 0.28 -5 -5 9 0.11 0.18 5 -5 -9 0.26 0.16 5 -5 -9 -0.15 0.30 -5 5 9 0.25 0.33 5 5 -9 0.31 0.31 5 5 -9 0.68 0.63 -4 -5 9 11.11 0.59 -4 -5 9 11.20 0.42 4 -5 -9 10.34 0.56 4 5 -9 11.55 0.64 -4 5 9 11.51 0.61 -3 -5 9 0.70 0.26 -3 -5 9 0.63 0.18 3 -5 -9 0.86 0.24 3 5 -9 1.20 0.29 -3 5 9 0.56 0.28 -2 -5 9 10.82 0.52 2 5 -9 11.02 0.57 -2 5 9 10.73 0.54 -2 5 9 10.96 0.37 -1 -5 9 1.11 0.25 -1 -5 9 1.30 0.21 -1 5 9 1.40 0.19 -1 5 9 1.10 0.27 1 5 -9 0.85 0.25 0 -5 9 121.61 3.07 0 5 -9 121.38 3.10 0 5 9 121.35 2.99 0 5 9 121.29 2.99 1 -5 9 47.16 1.36 1 5 9 47.75 1.30 -1 5 -9 48.70 1.38 2 -5 9 210.34 5.24 -2 5 -9 210.08 5.24 2 5 9 215.88 5.20 2 5 9 213.96 5.17 3 -5 9 48.51 1.44 3 -5 9 48.85 1.44 -3 5 -9 48.55 1.41 3 5 9 48.22 1.35 4 -5 9 145.70 4.42 4 -5 9 168.47 4.11 4 5 9 161.47 4.04 4 5 9 166.56 3.95 -4 5 -9 166.86 4.07 5 -5 9 14.48 0.80 5 -5 9 15.09 0.75 -5 5 -9 14.31 0.67 5 5 9 13.62 0.70 6 -5 9 164.90 4.67 6 -5 9 162.86 4.20 6 5 9 166.54 4.19 -6 5 -9 164.23 4.13 7 -5 9 3.06 0.56 7 -5 9 2.92 0.44 7 5 9 2.95 0.47 -7 5 -9 2.82 0.37 8 -5 9 64.17 2.00 8 5 9 63.63 1.95 -8 5 -9 63.63 1.78 9 -5 9 1.89 0.53 9 5 9 1.46 0.76 10 -5 9 12.37 0.90 10 -5 9 11.22 0.99 10 5 9 14.71 1.05 12 -6 -9 1.22 0.77 12 6 -9 1.26 1.11 -12 6 9 0.38 0.65 11 -6 -9 1.71 0.61 -11 -6 9 1.91 0.44 -11 6 9 1.57 0.52 11 6 -9 1.34 0.59 -10 -6 9 18.16 0.76 10 6 -9 19.88 0.86 10 6 -9 20.56 1.13 -10 6 9 19.09 1.01 9 -6 -9 1.17 0.57 -9 -6 9 1.80 0.30 9 6 -9 1.94 0.52 9 6 -9 2.04 0.36 -8 -6 9 52.86 1.43 8 -6 -9 53.01 1.70 8 6 -9 55.71 1.63 -7 -6 9 37.06 1.02 7 -6 -9 39.52 1.14 7 -6 -9 37.26 1.28 -7 6 9 32.97 1.32 7 6 -9 36.87 1.30 7 6 -9 37.93 1.25 6 -6 -9 148.75 3.83 -6 -6 9 150.06 3.61 6 6 -9 147.05 3.86 -6 6 9 149.04 3.84 -5 -6 9 37.67 1.21 5 -6 -9 38.50 1.23 -5 6 9 39.19 1.24 5 6 -9 36.83 1.37 5 6 -9 36.79 1.26 4 -6 -9 173.36 4.29 -4 -6 9 177.14 4.14 -4 -6 9 183.23 4.33 -4 6 9 174.95 4.36 4 6 -9 150.57 4.69 -3 -6 9 2.52 0.26 -3 -6 9 2.09 0.32 3 6 -9 3.10 0.50 -2 -6 9 270.25 6.41 -2 -6 9 263.71 6.52 2 6 -9 266.46 6.57 -2 6 9 267.86 6.53 -1 -6 9 35.95 0.97 -1 -6 9 33.53 1.06 1 6 -9 33.85 1.12 -1 6 9 33.78 0.92 -1 6 9 33.95 1.07 0 -6 9 462.08 11.10 0 6 9 468.50 11.01 0 6 9 455.23 11.10 0 6 -9 458.08 11.14 1 -6 9 3.00 0.36 -1 6 -9 2.73 0.35 1 6 9 2.63 0.35 2 -6 9 75.58 2.05 -2 6 -9 75.84 2.09 3 -6 9 7.42 0.70 3 6 9 7.85 0.50 -3 6 -9 7.03 0.68 4 -6 9 6.19 0.59 4 -6 9 5.98 0.63 4 6 9 5.41 0.51 5 -6 9 7.19 0.65 5 -6 9 6.89 0.60 5 6 9 7.24 0.38 5 6 9 6.86 0.73 5 6 9 7.16 0.35 -5 6 -9 6.80 0.59 6 -6 9 10.20 0.67 6 -6 9 10.57 0.81 -6 6 -9 10.29 0.70 -6 6 -9 11.77 0.67 6 6 9 11.14 0.70 7 -6 9 7.11 0.61 -7 6 -9 7.46 0.68 7 6 9 6.04 0.66 -7 6 -9 6.31 0.59 8 -6 9 31.31 1.29 8 -6 9 30.56 1.19 -8 6 -9 31.54 1.27 8 6 9 31.79 1.25 -8 6 -9 32.78 1.10 9 -6 9 2.78 0.81 9 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100.22 2.60 -1 7 -9 99.62 2.65 1 7 9 97.42 2.58 1 7 9 98.96 2.50 2 -7 9 13.52 0.70 -2 7 -9 13.41 0.72 3 -7 9 117.19 3.07 3 7 9 117.70 3.03 -3 7 -9 118.45 3.09 4 -7 9 6.55 0.58 -4 7 -9 5.59 0.58 4 7 9 4.73 0.41 4 7 9 6.67 0.58 5 -7 9 10.91 0.75 5 -7 9 11.95 0.69 5 7 9 12.32 0.71 5 7 9 12.37 0.50 -5 7 -9 13.11 0.70 -5 7 -9 13.27 0.71 6 -7 9 73.42 2.09 6 -7 9 71.97 2.15 6 7 9 73.20 2.08 -6 7 -9 72.12 2.05 -6 7 -9 71.95 2.11 7 -7 9 42.12 1.54 7 -7 9 34.63 1.49 -7 7 -9 42.25 1.33 -7 7 -9 42.23 1.44 7 7 9 41.33 1.41 8 -7 9 26.97 1.56 8 -7 9 23.38 1.04 -8 7 -9 23.68 0.98 -8 7 -9 23.27 1.10 8 7 9 22.90 1.18 9 -7 9 15.36 0.97 9 -7 9 12.36 0.99 -9 7 -9 11.08 0.72 9 7 9 12.83 1.50 10 -7 9 0.03 0.48 10 -7 9 0.12 0.65 10 7 9 -0.58 0.53 11 -8 -9 7.81 1.07 11 8 -9 8.12 0.71 -11 8 9 9.26 1.42 10 -8 -9 0.74 0.53 10 8 -9 0.45 0.36 10 8 -9 -0.04 0.53 -10 8 9 0.75 0.48 9 8 -9 9.61 0.89 -9 8 9 9.07 0.82 9 8 -9 9.57 0.70 8 -8 -9 25.47 1.18 8 8 -9 26.40 1.19 -8 8 9 25.92 1.11 8 8 -9 25.24 1.05 7 -8 -9 36.01 1.28 -7 8 9 35.93 1.31 7 8 -9 36.99 1.27 6 -8 -9 10.33 0.69 6 8 -9 9.35 0.68 -6 8 9 9.10 0.68 6 8 -9 10.10 0.73 -5 -8 9 203.61 5.03 5 -8 -9 197.83 5.02 -5 8 9 198.07 5.03 5 8 -9 198.61 5.06 -4 -8 9 62.10 1.78 -4 8 9 63.55 1.81 4 8 -9 62.51 1.85 -3 -8 9 146.90 3.73 -3 8 9 150.12 3.75 3 8 -9 142.46 3.79 -2 -8 9 24.61 0.90 -2 -8 9 25.39 0.70 2 8 -9 24.69 0.99 -1 -8 9 144.41 3.43 -1 -8 9 135.67 3.55 1 8 -9 137.08 3.61 -1 8 9 139.43 3.54 0 8 9 30.69 0.87 0 8 9 30.09 1.01 0 8 -9 30.04 1.10 1 8 9 45.74 1.36 -1 8 -9 46.55 1.47 1 8 9 47.49 1.30 2 -8 9 6.89 0.58 -2 8 -9 6.00 0.59 3 -8 9 30.04 1.05 -3 8 -9 30.40 1.10 4 -8 9 0.24 0.32 -4 8 -9 0.22 0.30 4 8 9 0.13 0.34 4 8 9 0.09 0.22 5 -8 9 10.09 0.66 -5 8 -9 9.35 0.66 5 8 9 10.23 0.70 -5 8 -9 9.78 0.92 5 8 9 10.19 0.49 6 -8 9 2.83 0.44 6 -8 9 2.11 0.47 6 8 9 2.56 0.43 -6 8 -9 1.76 0.38 -6 8 -9 2.80 0.45 7 -8 9 44.20 2.10 -7 8 -9 46.43 1.75 7 8 9 46.16 1.58 -7 8 -9 45.44 1.47 8 -8 9 7.65 0.74 8 8 9 6.90 0.79 -8 8 -9 7.17 0.79 9 -8 9 62.82 2.13 9 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0.73 5 9 9 9.76 0.55 -5 9 -9 11.38 0.72 6 -9 9 95.41 2.61 6 9 9 92.43 2.44 6 9 9 96.37 2.69 -6 9 -9 98.67 2.70 7 9 9 5.54 0.77 -7 9 -9 5.69 0.81 8 -9 9 45.28 1.83 8 -9 9 45.49 1.51 8 9 9 46.77 1.83 -8 9 -9 42.78 1.50 -8 9 -9 41.44 1.59 9 9 9 0.83 0.54 -9 9 -9 0.99 0.43 10 -10 -9 14.62 1.21 10 10 -9 13.65 1.17 -10 10 9 13.26 1.37 10 10 -9 12.85 0.90 9 -10 -9 10.20 0.98 -9 10 9 7.52 0.89 9 10 -9 10.42 1.03 9 10 -9 7.06 1.03 8 -10 -9 38.70 1.52 8 10 -9 40.16 1.43 -8 10 9 39.16 1.45 8 10 -9 39.88 1.58 7 -10 -9 6.54 0.77 -7 10 9 5.51 0.88 7 10 -9 6.25 0.70 -6 10 9 102.42 2.84 6 10 -9 103.60 2.87 5 10 -9 15.74 0.92 -4 -10 9 90.41 2.47 -4 10 9 89.57 2.50 4 10 -9 91.27 2.56 -3 -10 9 22.58 0.89 -3 10 9 22.24 0.91 3 10 -9 22.58 0.99 -2 -10 9 85.78 2.29 -2 10 9 84.08 2.29 2 10 -9 83.46 2.40 -1 -10 9 2.62 0.37 -1 10 9 2.97 0.50 0 -10 9 130.18 3.24 0 10 9 115.99 3.51 0 10 9 130.18 3.09 1 -10 9 4.92 0.51 1 10 9 4.94 0.51 1 10 9 3.88 0.38 2 -10 9 0.57 0.32 2 10 9 0.33 0.32 2 10 9 0.49 0.29 3 -10 9 2.83 0.40 3 10 9 3.30 0.49 3 10 9 3.19 0.41 4 -10 9 0.16 0.32 4 10 9 0.37 0.35 4 10 9 0.21 0.60 4 10 9 -0.03 0.29 -4 10 -9 0.21 0.37 5 -10 9 0.42 0.35 5 10 9 0.52 0.38 -5 10 -9 0.70 0.38 6 -10 9 7.15 0.62 -6 10 -9 7.57 0.75 6 10 9 6.40 0.84 6 10 9 7.20 0.82 7 -10 9 9.08 0.95 7 10 9 10.64 1.15 -7 10 -9 10.70 0.81 8 -10 9 26.43 1.15 8 10 9 24.48 1.39 -8 10 -9 30.04 1.22 9 -11 -9 32.09 1.49 9 11 -9 30.79 2.17 9 11 -9 34.13 1.55 -9 11 9 32.40 1.45 -8 11 9 8.97 0.81 8 11 -9 8.59 0.97 8 11 -9 8.54 0.81 7 11 -9 2.63 0.56 -7 11 9 4.11 0.79 7 11 -9 2.93 0.48 6 11 -9 2.13 0.44 -6 11 9 1.70 0.47 5 11 -9 5.22 0.75 -5 11 9 5.15 0.66 4 11 -9 9.05 0.87 -4 11 9 8.94 0.68 -3 -11 9 0.18 0.33 3 11 -9 0.25 0.38 -3 11 9 0.15 0.34 -2 -11 9 28.36 1.16 2 11 -9 26.77 1.28 -2 11 9 28.87 1.02 -1 -11 9 38.90 1.24 -1 11 9 38.91 1.24 0 -11 9 14.24 0.69 0 11 9 13.27 0.69 1 -11 9 107.24 2.82 1 11 9 103.73 2.89 1 11 9 109.55 2.71 1 11 9 108.73 2.91 2 -11 9 10.11 0.61 -2 11 -9 9.33 0.77 2 11 9 9.13 0.99 2 11 9 9.30 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5 12 161.78 4.22 -1 5 12 163.13 4.07 0 -5 12 9.88 0.63 0 5 12 9.00 0.42 0 5 12 9.21 0.50 1 -5 12 174.93 4.34 1 5 12 172.73 4.17 1 5 12 167.67 4.25 2 -5 12 29.28 1.05 2 5 12 29.00 0.86 2 5 12 29.02 0.98 3 -5 12 194.50 4.94 3 5 12 201.05 4.80 -3 5 -12 185.69 5.29 3 5 12 202.95 4.90 4 -5 12 43.63 1.35 4 -5 12 41.19 1.36 4 5 12 41.73 1.23 4 5 12 41.53 1.32 5 -5 12 35.19 1.20 5 -5 12 34.71 1.22 5 5 12 32.87 1.11 5 5 12 34.83 1.19 -5 5 -12 33.59 1.28 6 -5 12 11.57 0.74 6 5 12 10.18 0.74 6 5 12 10.70 0.73 -6 5 -12 10.60 0.82 7 -5 12 48.43 1.62 7 -5 12 49.34 1.61 7 5 12 49.57 1.72 7 5 12 48.23 1.54 8 -5 12 21.30 1.04 8 -5 12 18.54 1.00 8 5 12 18.04 0.97 8 5 12 18.03 1.02 9 -5 12 8.46 0.86 9 -5 12 7.48 0.86 9 5 12 8.36 0.90 9 5 12 6.00 0.83 12 -6 -12 1.87 0.79 -12 6 12 0.97 0.56 12 6 -12 1.44 0.67 11 -6 -12 18.30 1.15 -11 6 12 17.83 1.07 11 6 -12 17.97 1.20 11 6 -12 17.72 0.93 -10 -6 12 0.77 0.42 -10 6 12 0.52 0.46 10 6 -12 0.33 0.50 10 6 -12 1.02 0.36 -9 -6 12 45.77 1.28 9 6 -12 47.45 1.49 9 6 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48.32 1.88 -12 1 14 48.83 1.70 -11 -1 14 11.78 0.78 11 -1 -14 11.54 1.16 11 1 -14 13.24 1.02 -11 1 14 12.79 0.87 10 -1 -14 19.07 1.31 10 1 -14 18.07 1.05 -10 1 14 20.25 0.95 9 -1 -14 2.93 0.52 -9 -1 14 4.51 0.61 9 1 -14 3.79 0.54 8 -1 -14 3.42 0.50 -8 -1 14 3.61 0.51 8 1 -14 3.59 0.61 -8 1 14 4.01 0.55 7 -1 -14 4.39 0.85 -7 -1 14 5.21 0.53 -7 -1 14 4.85 0.51 -7 1 14 5.29 0.55 7 1 -14 4.43 0.58 -7 1 14 4.81 0.50 7 1 -14 4.45 0.62 -6 -1 14 27.01 0.99 -6 -1 14 26.91 0.95 6 -1 -14 26.42 0.96 6 1 -14 26.12 1.04 -6 1 14 28.07 0.93 6 1 -14 26.55 1.01 -6 1 14 27.56 1.01 -5 -1 14 17.67 0.86 5 -1 -14 18.83 0.73 -5 -1 14 18.96 0.80 -5 1 14 20.50 0.86 -5 1 14 19.10 0.73 5 1 -14 19.30 0.74 5 1 -14 19.24 0.86 -4 -1 14 112.29 2.88 4 -1 -14 111.68 2.76 -4 -1 14 108.43 2.86 4 1 -14 111.35 2.78 -4 1 14 108.68 2.82 4 1 -14 111.77 2.93 -3 -1 14 12.15 0.62 3 -1 -14 11.91 0.44 -3 1 14 11.17 0.65 3 1 -14 12.47 0.48 -3 1 14 11.20 0.57 2 -1 -14 0.89 0.29 -2 -1 14 0.88 0.33 2 1 -14 0.97 0.17 -2 1 14 0.84 0.28 2 1 -14 0.57 0.28 1 -1 -14 194.69 4.83 -1 -1 14 193.37 4.84 -1 1 14 194.40 4.82 1 1 -14 194.99 4.85 0 -1 -14 59.50 1.65 0 -1 14 55.35 1.77 0 1 14 60.81 1.67 0 1 -14 60.43 1.67 1 -1 14 106.66 2.77 -1 -1 -14 108.36 2.71 1 1 14 99.18 2.87 -1 1 -14 105.58 2.72 2 -1 14 95.70 2.58 -2 -1 -14 94.65 2.47 -2 1 -14 96.51 2.38 2 1 14 97.43 2.63 -2 1 -14 94.50 2.51 3 -1 14 168.26 4.15 -3 -1 -14 171.76 4.11 3 -1 14 168.03 4.32 3 1 14 171.06 4.12 -3 1 -14 166.79 4.20 3 1 14 168.61 4.30 4 -1 14 82.15 2.13 4 1 14 79.22 2.26 -4 1 -14 80.89 2.12 4 1 14 82.19 2.11 5 -1 14 73.09 1.94 -5 1 -14 71.43 1.86 5 1 14 65.42 2.03 5 1 14 72.96 1.92 6 -1 14 13.12 0.76 6 1 14 12.12 0.76 -6 1 -14 12.90 0.58 7 -1 14 23.07 0.94 7 1 14 20.80 1.19 7 1 14 20.08 0.95 8 -1 14 10.10 0.76 8 -1 14 9.09 0.84 8 1 14 10.17 0.84 8 1 14 9.47 0.77 9 -1 14 -0.15 0.52 9 -1 14 0.96 0.48 9 1 14 0.19 0.47 9 1 14 -0.44 0.51 12 -2 -14 -0.08 0.60 12 2 -14 0.94 0.64 -11 -2 14 9.73 0.95 11 -2 -14 12.10 1.08 11 2 -14 14.04 1.06 -11 2 14 10.85 0.85 10 -2 -14 8.65 1.13 -10 -2 14 8.38 0.65 10 2 -14 8.55 0.86 -10 2 14 10.06 0.77 -9 -2 14 103.26 2.74 9 -2 -14 105.79 2.86 9 2 -14 98.44 2.87 8 -2 -14 7.42 0.71 -8 -2 14 7.69 0.60 8 2 -14 7.47 0.73 -8 2 14 9.31 0.67 8 2 -14 8.09 0.70 -7 -2 14 93.27 2.56 -7 -2 14 98.99 2.55 7 2 -14 94.89 2.62 -7 2 14 92.98 2.59 7 2 -14 98.78 2.60 -6 -2 14 31.33 1.10 -6 -2 14 33.10 1.11 6 -2 -14 34.19 1.10 -6 2 14 32.93 1.03 6 2 -14 34.63 1.13 6 2 -14 33.08 1.19 -6 2 14 33.28 1.16 -5 -2 14 322.29 7.78 -5 -2 14 326.06 7.76 5 -2 -14 319.41 7.70 -5 2 14 316.98 7.81 5 2 -14 311.22 7.82 5 2 -14 317.20 7.73 -5 2 14 315.40 7.71 -4 -2 14 1.26 0.31 4 -2 -14 1.20 0.26 -4 -2 14 1.00 0.34 4 2 -14 1.24 0.27 4 2 -14 1.07 0.34 -4 2 14 1.29 0.27 -4 2 14 1.13 0.23 -4 2 14 1.00 0.36 3 -2 -14 152.06 3.67 3 2 -14 154.50 3.81 -3 2 14 146.79 3.99 -3 2 14 151.11 3.78 3 2 -14 153.47 3.90 -2 -2 14 -0.34 0.33 -2 2 14 1.11 0.29 2 2 -14 0.27 0.18 2 2 -14 -0.20 0.33 1 2 -14 315.61 7.67 -1 2 14 303.58 7.61 1 2 -14 321.37 7.51 0 -2 14 7.07 0.68 0 2 -14 8.54 0.42 0 2 -14 7.24 0.58 0 2 14 7.47 0.55 1 -2 14 87.28 2.39 -1 2 -14 90.71 2.22 1 2 14 87.88 2.36 -1 2 -14 86.70 2.34 2 -2 14 33.24 1.15 -2 2 -14 32.73 1.07 2 2 14 34.00 1.14 3 -2 14 0.67 0.37 3 -2 14 0.16 0.37 -3 2 -14 0.68 0.28 3 2 14 1.48 0.37 3 2 14 0.33 0.24 4 -2 14 4.36 0.49 -4 2 -14 3.87 0.46 4 2 14 5.00 0.62 4 2 14 4.64 0.45 5 -2 14 24.97 0.94 -5 2 -14 24.31 0.84 5 2 14 24.53 0.87 5 2 14 24.30 1.00 6 -2 14 0.61 0.37 6 -2 14 0.38 0.40 6 2 14 0.57 0.38 -6 2 -14 0.46 0.25 6 2 14 0.01 0.38 7 -2 14 157.06 4.10 7 -2 14 165.94 4.74 7 2 14 156.54 4.07 7 2 14 156.58 4.23 8 -2 14 6.60 0.70 8 -2 14 6.36 0.79 8 2 14 7.01 0.79 8 2 14 4.71 0.70 9 -2 14 72.52 2.31 9 -2 14 75.19 2.27 9 2 14 72.10 2.35 9 2 14 72.48 2.21 12 -3 -14 15.10 1.18 -12 -3 14 16.67 0.88 12 3 -14 17.51 1.22 -12 3 14 17.08 1.08 11 -3 -14 16.63 1.25 11 3 -14 15.68 1.10 -11 3 14 17.99 1.00 -10 -3 14 16.98 0.80 10 -3 -14 15.99 0.99 10 3 -14 17.83 1.03 -10 3 14 17.90 1.47 9 -3 -14 6.34 0.75 -9 -3 14 7.27 0.58 -9 3 14 7.23 0.70 9 3 -14 7.55 0.69 8 -3 -14 41.34 1.39 -8 -3 14 42.65 1.30 8 3 -14 41.07 1.39 7 -3 -14 0.82 0.47 -7 -3 14 0.81 0.32 -7 -3 14 0.83 0.57 7 3 -14 1.17 0.36 -7 3 14 0.56 0.34 7 3 -14 1.17 0.38 -6 -3 14 3.49 0.47 6 -3 -14 3.23 0.40 -6 -3 14 3.09 0.40 -6 3 14 2.94 0.43 6 3 -14 3.24 0.44 -6 3 14 3.02 0.38 -5 -3 14 1.01 0.30 5 -3 -14 1.01 0.31 -5 -3 14 1.10 0.34 5 3 -14 0.79 0.36 -5 3 14 1.25 0.36 5 3 -14 1.06 0.32 -5 3 14 1.12 0.25 4 -3 -14 62.20 1.62 -4 -3 14 61.37 1.75 -4 -3 14 61.36 1.70 4 3 -14 62.00 1.81 -4 3 14 61.60 1.65 -4 3 14 66.75 1.70 -4 3 14 60.59 1.79 4 3 -14 59.29 1.68 -3 -3 14 76.95 2.10 3 -3 -14 77.99 1.92 -3 3 14 76.67 2.13 -3 3 14 75.28 2.00 -3 3 14 78.79 1.92 3 3 -14 76.27 2.00 3 3 -14 75.84 2.14 -2 -3 14 25.24 0.93 -2 3 14 24.94 0.97 -2 3 14 24.93 0.85 2 3 -14 25.88 0.99 -1 -3 14 108.28 2.80 -1 3 14 103.80 2.71 0 -3 14 129.76 3.31 0 3 -14 123.83 3.32 0 3 14 128.13 3.24 1 -3 14 69.76 1.97 1 3 14 70.50 1.93 -1 3 -14 69.12 1.94 2 -3 14 381.47 9.56 -2 3 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1.30 7 -4 -14 1.64 0.40 -7 -4 14 1.41 0.33 -7 -4 14 1.31 0.36 7 4 -14 1.53 0.38 7 4 -14 1.57 0.37 -6 -4 14 174.92 4.56 6 -4 -14 179.06 4.50 -6 -4 14 182.43 4.47 6 4 -14 183.22 4.56 -6 4 14 183.01 4.42 6 4 -14 177.41 4.60 5 -4 -14 0.77 0.29 -5 -4 14 0.38 0.32 -5 -4 14 0.75 0.29 -5 4 14 0.23 0.36 5 4 -14 0.69 0.33 5 4 -14 0.75 0.35 -5 4 14 0.34 0.25 4 -4 -14 92.91 2.33 -4 -4 14 91.73 2.39 -4 -4 14 91.71 2.46 4 4 -14 90.29 2.41 -4 4 14 92.99 2.50 4 4 -14 91.20 2.52 -4 4 14 91.72 2.33 -3 -4 14 2.38 0.36 -3 4 14 2.65 0.43 3 4 -14 2.94 0.42 -3 4 14 2.87 0.38 -3 4 14 2.03 0.34 -2 -4 14 72.23 2.00 -2 4 14 70.90 1.89 -2 4 14 72.24 2.03 2 4 -14 71.86 2.04 -1 -4 14 26.28 0.96 -1 4 14 23.69 0.84 0 -4 14 140.79 3.69 0 4 14 140.68 3.60 0 4 -14 147.80 3.69 1 -4 14 69.64 2.00 -1 4 -14 70.61 1.99 1 4 14 69.82 1.93 2 -4 14 3.59 0.58 -2 4 -14 4.12 0.51 3 -4 14 12.11 0.73 3 4 14 11.31 0.68 -3 4 -14 11.82 1.05 3 4 14 10.72 0.51 4 -4 14 1.43 0.38 4 4 14 1.22 0.29 4 4 14 0.82 0.35 5 -4 14 1.73 0.39 5 4 14 1.29 0.39 5 4 14 1.12 0.35 6 -4 14 42.36 1.38 6 -4 14 41.70 1.46 6 4 14 41.06 1.44 -6 4 -14 42.48 1.33 7 -4 14 3.72 0.63 7 4 14 3.67 0.50 -7 4 -14 3.29 0.42 8 -4 14 104.44 3.03 8 -4 14 108.62 2.98 8 4 14 109.62 2.94 8 4 14 105.09 3.04 9 -4 14 1.91 0.52 9 -4 14 2.31 0.62 9 4 14 1.38 0.56 9 4 14 -0.76 0.94 12 -5 -14 15.99 1.22 -12 5 14 14.84 1.09 11 -5 -14 22.24 1.20 -11 -5 14 22.16 0.87 -11 5 14 21.45 1.14 11 5 -14 21.89 1.25 -10 -5 14 4.68 0.54 10 -5 -14 5.83 0.82 10 5 -14 4.92 0.84 -10 5 14 5.43 0.75 -9 -5 14 10.98 0.63 9 5 -14 8.69 0.75 -9 5 14 9.58 1.32 9 5 -14 9.71 0.84 -8 -5 14 4.27 0.50 8 -5 -14 5.10 0.64 8 5 -14 3.81 0.63 -7 -5 14 2.35 0.32 -7 -5 14 1.77 0.37 7 -5 -14 2.17 0.41 7 5 -14 1.75 0.42 7 5 -14 1.59 0.38 -6 -5 14 1.81 0.29 6 -5 -14 1.44 0.37 6 5 -14 1.73 0.41 6 5 -14 1.48 0.38 -5 -5 14 5.16 0.44 5 -5 -14 5.36 0.48 -5 5 14 5.59 0.36 5 5 -14 5.57 0.60 5 5 -14 5.09 0.64 -5 5 14 5.40 0.58 -4 -5 14 18.85 0.71 -4 -5 14 18.90 0.82 4 -5 -14 18.85 0.69 -4 5 14 19.97 0.65 4 5 -14 19.20 0.91 -4 5 14 19.66 0.87 -3 -5 14 27.77 1.03 -3 5 14 28.37 1.07 -3 5 14 31.54 0.94 3 5 -14 28.60 1.10 -3 5 14 29.56 0.88 -2 -5 14 13.93 0.74 -2 5 14 15.23 0.78 2 5 -14 16.19 0.82 -2 5 14 15.09 0.61 -2 5 14 15.16 0.56 -1 -5 14 187.15 4.82 -1 5 14 192.10 4.86 1 5 -14 194.87 4.86 -1 5 14 192.17 4.71 0 -5 14 107.72 2.88 0 5 -14 109.63 2.90 0 5 14 107.60 2.78 1 -5 14 78.53 2.20 1 5 14 78.62 2.13 -1 5 -14 79.10 2.20 2 -5 14 260.43 6.60 -2 5 -14 267.42 6.58 2 5 14 271.78 6.54 2 5 14 262.89 6.38 3 -5 14 139.15 3.76 3 5 14 146.17 3.63 -3 5 -14 145.95 3.71 4 -5 14 5.36 0.67 4 5 14 4.12 0.46 -4 5 -14 4.03 0.58 4 5 14 4.07 0.63 5 -5 14 44.50 1.42 5 5 14 42.64 1.35 -5 5 -14 43.83 1.39 5 5 14 45.81 1.46 6 -5 14 18.37 0.89 6 -5 14 17.82 0.97 -6 5 -14 17.62 0.84 6 5 14 18.17 0.93 6 5 14 18.14 0.88 7 -5 14 34.68 1.34 7 -5 14 32.85 1.25 7 5 14 31.87 1.28 -7 5 -14 32.81 1.14 7 5 14 30.69 1.18 8 -5 14 10.20 0.93 8 5 14 10.03 0.83 8 5 14 10.52 0.92 9 -5 14 0.35 0.47 9 -5 14 0.13 0.61 9 5 14 0.01 0.53 9 5 14 -0.23 0.53 11 -6 -14 24.63 1.28 11 6 -14 25.54 1.14 11 6 -14 23.28 1.35 -11 6 14 24.07 1.25 -10 -6 14 0.51 0.38 -10 6 14 0.68 0.48 10 6 -14 0.87 0.54 10 6 -14 1.37 0.41 -9 -6 14 114.38 2.96 9 6 -14 114.08 3.18 9 6 -14 117.46 3.37 -9 6 14 118.34 3.24 8 -6 -14 2.12 0.43 -8 -6 14 1.40 0.31 8 6 -14 1.50 0.42 -7 -6 14 151.91 3.75 7 -6 -14 151.27 3.89 7 6 -14 149.81 3.96 7 6 -14 151.06 3.98 -6 -6 14 1.80 0.28 6 -6 -14 2.31 0.46 6 6 -14 1.83 0.40 6 6 -14 1.84 0.39 5 -6 -14 232.46 5.80 -5 -6 14 237.17 5.74 5 6 -14 236.44 5.90 5 6 -14 237.66 5.97 -5 6 14 236.28 5.93 -4 -6 14 48.90 1.36 -4 -6 14 48.37 1.70 4 -6 -14 47.74 1.28 4 6 -14 48.96 1.57 -4 6 14 50.36 1.28 -3 -6 14 135.97 3.51 3 6 -14 133.76 3.58 -3 6 14 134.97 3.54 -3 6 14 137.06 3.33 -2 -6 14 26.42 1.02 -2 6 14 27.12 1.05 -2 6 14 30.61 0.99 -2 6 14 27.34 0.87 2 6 -14 27.88 1.08 -1 -6 14 10.81 0.68 -1 6 14 11.06 0.55 -1 6 14 11.47 0.70 1 6 -14 11.25 0.74 -1 6 14 12.11 0.52 0 -6 14 5.28 0.58 0 6 -14 4.85 0.61 0 6 14 5.18 0.48 0 6 14 5.79 0.41 1 -6 14 18.64 0.87 1 6 14 20.14 0.81 1 6 14 20.51 0.66 -1 6 -14 19.10 0.89 1 6 14 20.14 0.65 2 -6 14 0.36 0.34 -2 6 -14 0.48 0.31 2 6 14 0.77 0.33 2 6 14 0.62 0.26 3 -6 14 29.76 1.11 3 6 14 28.38 1.17 3 6 14 28.83 1.05 -3 6 -14 29.87 1.09 -4 6 -14 7.04 0.63 4 6 14 6.65 0.61 4 6 14 5.34 0.50 5 -6 14 35.62 1.32 -5 6 -14 36.48 1.24 5 6 14 36.61 1.39 5 6 14 35.94 1.19 6 -6 14 9.90 0.76 6 -6 14 9.82 0.88 6 6 14 10.54 0.86 6 6 14 9.16 0.72 -6 6 -14 9.78 0.70 7 -6 14 58.24 1.84 7 -6 14 57.64 1.90 7 6 14 55.25 1.85 -7 6 -14 59.28 1.73 7 6 14 58.79 1.78 8 -6 14 1.56 0.51 8 -6 14 0.23 0.52 8 6 14 1.00 0.49 11 -7 -14 9.71 1.01 11 7 -14 11.22 0.97 -11 7 14 8.33 0.93 11 7 -14 9.52 1.45 10 -7 -14 14.33 1.02 -10 7 14 13.61 0.96 10 7 -14 12.01 0.87 10 7 -14 11.27 1.03 9 -7 -14 1.01 0.46 9 7 -14 1.89 0.52 -9 7 14 0.74 0.44 9 7 -14 0.47 0.38 -8 -7 14 14.91 0.60 8 -7 -14 13.55 0.92 8 7 -14 15.19 0.94 -8 7 14 17.19 0.95 8 7 -14 15.42 0.92 -7 -7 14 1.57 0.28 7 -7 -14 1.22 0.39 -7 7 14 0.93 0.44 -6 -7 14 4.46 0.39 6 -7 -14 4.56 0.57 6 7 -14 3.65 0.49 -6 7 14 3.84 0.56 6 7 -14 4.50 0.63 -5 -7 14 35.62 1.02 5 7 -14 35.29 1.23 -5 7 14 34.63 1.25 5 7 -14 34.37 1.29 -4 -7 14 5.59 0.56 -4 -7 14 6.82 0.43 4 7 -14 6.08 0.67 -4 7 14 6.15 0.61 -3 -7 14 46.46 1.47 -3 7 14 49.10 1.25 -3 7 14 47.43 1.51 -2 -7 14 66.25 1.91 -2 7 14 66.45 1.72 -2 7 14 66.03 1.93 -1 -7 14 70.81 2.03 -1 7 14 71.24 1.88 -1 7 14 72.13 2.06 1 7 -14 73.25 2.10 0 -7 14 89.01 2.46 0 7 14 90.07 2.32 0 7 14 88.73 2.47 0 7 -14 89.72 2.51 1 -7 14 44.63 1.43 -1 7 -14 43.69 1.46 1 7 14 45.01 1.33 1 7 14 45.50 1.25 2 -7 14 158.34 4.19 -2 7 -14 163.73 4.25 2 7 14 162.07 4.10 2 7 14 165.47 4.14 3 -7 14 29.51 1.23 3 7 14 27.86 1.03 3 7 14 29.54 0.94 -3 7 -14 29.45 1.12 4 7 14 188.53 4.67 4 7 14 180.84 4.70 -4 7 -14 185.77 4.74 5 -7 14 2.17 0.47 5 7 14 1.96 0.42 5 7 14 2.42 0.36 -5 7 -14 1.33 0.39 5 7 14 1.63 0.50 6 7 14 43.24 1.43 -6 7 -14 44.89 1.46 7 -7 14 3.69 0.58 -7 7 -14 2.85 0.41 7 7 14 3.66 0.54 7 7 14 3.25 0.52 8 -7 14 32.72 1.33 8 -7 14 28.78 1.33 8 7 14 27.92 1.31 10 -8 -14 26.60 1.28 10 8 -14 30.66 1.26 -10 8 14 27.22 1.44 10 8 -14 26.56 1.40 9 -8 -14 10.45 1.04 9 8 -14 9.58 0.95 -9 8 14 8.76 0.85 9 8 -14 8.79 0.95 8 8 -14 38.19 1.42 -8 8 14 36.62 1.42 8 8 -14 39.63 1.57 7 -8 -14 18.51 0.89 7 8 -14 18.57 1.00 7 8 -14 18.41 1.05 -6 -8 14 111.60 3.03 6 -8 -14 109.75 2.95 6 8 -14 113.40 3.14 -6 8 14 110.27 3.06 5 8 -14 29.98 1.20 -5 8 14 27.33 1.12 -4 -8 14 153.60 3.69 -4 8 14 149.52 3.92 4 8 -14 146.66 3.97 -3 -8 14 27.37 1.06 -3 8 14 27.37 1.06 -2 -8 14 49.13 1.53 -2 8 14 49.88 1.31 -2 8 14 49.88 1.56 -1 -8 14 12.57 0.73 -1 8 14 13.91 0.78 -1 8 14 13.42 0.56 0 -8 14 71.33 2.04 0 8 14 70.30 1.88 0 8 14 70.12 2.03 1 -8 14 1.13 0.38 1 8 14 1.01 0.39 1 8 14 1.23 0.33 2 -8 14 6.77 0.70 2 8 14 7.95 0.52 2 8 14 7.41 0.58 3 8 14 14.57 0.73 3 8 14 13.28 0.71 4 -8 14 19.64 1.05 4 8 14 19.60 0.88 5 -8 14 13.77 0.87 5 8 14 13.80 0.79 5 8 14 12.55 0.77 5 8 14 14.45 0.63 6 -8 14 70.61 2.11 6 8 14 67.36 2.05 -6 8 -14 66.99 2.08 6 8 14 67.25 1.99 7 -8 14 8.37 0.95 7 8 14 6.62 0.83 7 8 14 8.44 0.80 -7 8 -14 6.99 0.78 10 -9 -14 4.83 0.68 10 9 -14 4.76 0.81 -10 9 14 4.45 0.68 9 -9 -14 11.61 0.96 -9 9 14 8.39 0.95 9 9 -14 9.99 1.02 9 9 -14 13.40 0.93 8 -9 -14 0.17 0.43 -8 9 14 0.69 0.47 8 9 -14 0.73 0.89 8 9 -14 0.10 0.45 7 9 -14 0.20 0.43 -7 9 14 0.69 0.44 7 9 -14 0.68 0.53 -6 9 14 32.24 1.34 6 9 -14 30.57 1.28 6 9 -14 31.01 1.30 -5 -9 14 27.68 1.12 -5 9 14 28.28 1.15 5 9 -14 27.76 1.20 -4 -9 14 6.34 0.64 -4 9 14 7.80 0.70 4 9 -14 7.74 0.77 -2 9 14 16.17 0.83 -1 9 14 114.43 2.86 -1 9 14 115.56 3.08 0 9 14 3.14 0.42 0 9 -14 3.04 0.60 0 9 14 3.64 0.58 1 9 14 139.04 3.64 -1 9 -14 136.85 3.72 1 9 14 140.33 3.52 2 9 14 7.89 0.60 2 9 14 7.53 0.58 2 9 14 8.07 0.67 -2 9 -14 7.68 0.74 3 9 14 111.23 2.97 -3 9 -14 114.67 3.13 4 -9 14 12.67 0.84 4 9 14 13.35 0.75 -4 9 -14 13.11 0.86 4 9 14 13.53 0.72 4 9 14 13.17 0.74 5 9 14 54.10 1.68 -5 9 -14 54.60 1.79 5 9 14 55.50 1.72 6 -9 14 0.08 0.45 6 9 14 -0.20 0.39 7 -9 14 28.56 1.27 7 9 14 26.96 1.20 7 9 14 24.82 1.61 -7 9 -14 29.46 1.31 9 -10 -14 38.07 1.49 -9 10 14 33.04 2.04 9 10 -14 36.75 1.48 9 10 -14 38.65 2.06 8 10 -14 28.82 1.30 -8 10 14 27.01 1.27 8 10 -14 27.25 1.37 -7 10 14 45.04 1.66 7 10 -14 50.63 2.01 7 10 -14 51.50 1.75 -6 -10 14 5.36 0.73 6 10 -14 8.21 0.82 -6 10 14 7.43 0.78 6 10 -14 7.75 0.83 -5 -10 14 55.79 1.99 -5 10 14 55.10 1.78 -4 -10 14 0.47 0.38 -4 10 14 0.71 0.43 4 10 -14 0.64 0.70 -3 -10 14 81.50 2.32 -3 10 14 81.20 2.34 3 10 -14 82.18 2.54 -2 -10 14 1.01 0.40 -2 10 14 0.90 0.40 2 10 -14 -0.06 0.43 1 10 -14 8.81 0.83 -1 10 14 10.46 0.71 0 10 14 5.03 0.45 0 10 -14 6.34 0.75 0 10 14 5.92 0.62 1 10 14 1.16 0.34 -1 10 -14 0.99 0.51 1 10 14 1.35 0.40 2 -10 14 7.27 0.69 2 10 14 6.98 0.59 2 10 14 8.31 0.65 2 10 14 7.97 0.67 3 -10 14 0.63 0.43 -3 10 -14 0.92 0.51 3 10 14 0.78 0.35 3 10 14 1.19 0.39 3 10 14 1.23 0.41 4 -10 14 7.93 1.00 4 10 14 7.88 0.59 -4 10 -14 10.28 1.06 4 10 14 7.19 0.65 4 10 14 7.66 0.67 5 -10 14 28.29 1.17 5 10 14 23.65 1.05 5 10 14 25.16 1.23 -5 10 -14 25.42 1.22 6 -10 14 5.47 0.80 6 10 14 5.14 0.71 -6 10 -14 5.01 0.62 6 10 14 5.36 0.65 -8 11 14 4.52 0.79 8 11 -14 4.88 0.63 8 11 -14 5.06 0.93 7 11 -14 0.56 0.48 -7 11 14 0.32 0.48 7 11 -14 0.62 0.54 -6 -11 14 0.83 0.45 -6 11 14 0.37 0.47 6 11 -14 0.43 0.69 -5 -11 14 0.73 0.47 5 11 -14 0.84 0.46 -5 11 14 1.43 0.47 -4 -11 14 50.93 1.65 -4 11 14 47.07 1.61 4 11 -14 48.26 1.74 -3 -11 14 0.45 0.45 -3 11 14 -0.03 0.40 3 11 -14 0.98 0.43 -2 -11 14 58.25 1.77 2 11 -14 57.30 1.93 -2 11 14 56.64 1.78 -1 -11 14 -0.33 0.35 1 11 -14 0.36 0.43 -1 11 14 0.32 0.36 0 -11 14 93.51 2.62 0 11 -14 95.47 2.78 0 11 14 94.03 2.63 1 -11 14 3.80 0.50 -1 11 -14 5.03 0.77 1 11 14 3.43 0.51 1 11 14 3.78 0.59 2 -11 14 72.89 2.12 2 11 14 72.89 2.00 -2 11 -14 69.42 2.24 2 11 14 72.59 2.10 3 -11 14 0.56 0.49 3 11 14 0.48 0.39 3 11 14 0.32 0.34 3 11 14 0.26 0.36 -3 11 -14 -0.11 0.43 3 11 14 -0.10 0.33 4 -11 14 30.28 1.23 4 11 14 27.78 1.05 -4 11 -14 27.61 1.28 4 11 14 27.26 1.16 4 11 14 27.08 1.15 4 11 14 27.45 1.10 5 -11 14 0.77 0.48 5 11 14 -0.43 0.47 5 11 14 0.67 0.48 -5 11 -14 -0.07 0.46 -7 12 14 11.13 0.99 7 12 -14 10.07 1.05 -6 12 14 57.45 1.92 6 12 -14 59.27 2.05 -5 -12 14 25.42 1.17 5 12 -14 25.88 1.29 -5 12 14 24.73 1.15 -4 -12 14 29.64 1.21 -4 12 14 30.64 1.22 4 12 -14 28.68 1.35 -3 -12 14 12.48 0.81 3 12 -14 9.54 0.93 -3 12 14 9.87 0.82 2 12 -14 2.28 0.52 -2 12 14 3.39 0.51 1 12 -14 8.86 0.88 -1 12 14 6.83 0.68 0 12 -14 8.51 0.89 0 12 14 8.83 0.71 -1 12 -14 -0.06 0.45 1 12 14 -0.32 0.37 2 -12 14 11.49 1.26 -2 12 -14 9.12 0.95 2 12 14 8.82 0.73 2 12 14 10.19 0.74 3 12 14 8.25 0.74 3 12 14 8.33 0.72 3 12 14 8.39 0.66 3 12 14 7.93 0.71 -3 12 -14 7.63 0.97 4 -12 14 5.76 0.75 4 12 14 6.10 0.79 -4 12 -14 5.96 0.74 4 12 14 6.18 1.12 4 12 14 5.79 0.66 4 12 14 5.67 0.65 -5 -13 14 4.64 0.63 5 13 -14 2.44 1.00 -5 13 14 3.91 0.62 -4 -13 14 2.14 0.53 4 13 -14 2.66 0.67 -4 13 14 2.86 0.54 -3 -13 14 15.22 1.00 -3 13 14 20.72 0.98 3 13 -14 15.70 1.19 -2 -13 14 0.32 0.42 -2 13 14 0.09 0.78 2 13 -14 0.53 0.53 -1 -13 14 40.30 1.42 -1 13 14 38.33 1.38 1 13 -14 38.36 1.64 0 -13 14 0.26 0.40 0 13 -14 -0.09 0.51 0 13 14 -0.17 0.40 1 -13 14 70.87 2.09 1 13 14 65.77 2.41 -1 13 -14 69.69 3.17 1 13 14 70.63 2.15 2 -13 14 2.57 0.48 -2 13 -14 1.24 0.63 2 13 14 2.23 0.83 -12 0 15 0.97 0.47 12 0 -15 1.14 0.63 11 0 -15 52.39 1.99 10 0 -15 0.02 0.49 -10 0 15 -0.08 0.41 9 0 -15 155.73 4.09 -8 0 15 0.73 0.35 8 0 -15 0.54 0.39 -7 0 15 188.78 4.67 -7 0 15 186.81 4.71 7 0 -15 182.90 5.10 -6 0 15 0.49 0.36 -6 0 15 0.00 0.34 6 0 -15 0.37 0.33 5 0 -15 136.32 3.43 5 0 -15 135.94 3.58 -5 0 15 139.01 3.54 -4 0 15 0.17 0.35 -4 0 15 0.18 0.29 4 0 -15 0.57 0.25 4 0 -15 0.79 0.34 -3 0 15 134.26 3.45 3 0 -15 133.86 3.49 3 0 -15 137.90 3.30 -2 0 15 0.26 0.30 -1 0 15 171.46 4.35 1 0 -15 172.77 4.34 0 0 -15 -0.17 0.28 0 0 15 -0.29 0.36 -1 0 -15 0.29 0.26 1 0 15 0.64 0.36 -2 0 -15 -0.20 0.24 2 0 15 -0.52 0.34 3 0 15 22.89 0.96 -3 0 -15 23.50 0.82 3 0 15 23.84 0.74 -3 0 -15 23.09 0.73 4 0 15 -0.29 0.25 -4 0 -15 0.07 0.22 4 0 15 0.11 0.38 5 0 15 3.10 0.37 7 0 15 132.17 3.40 7 0 15 126.52 3.52 8 0 15 -0.13 0.45 8 0 15 0.29 0.43 9 0 15 68.66 2.10 -12 -1 15 31.48 1.25 12 -1 -15 28.72 1.46 -12 1 15 29.62 1.28 12 1 -15 28.86 1.48 -11 -1 15 6.42 0.70 11 1 -15 9.69 0.95 -11 1 15 9.53 0.81 10 -1 -15 9.49 0.90 -10 1 15 11.92 0.79 10 1 -15 10.45 1.02 9 -1 -15 75.04 2.24 -9 -1 15 77.92 2.18 9 1 -15 77.35 2.25 8 -1 -15 2.23 0.47 -8 -1 15 2.26 0.39 -8 1 15 2.55 0.43 8 1 -15 2.71 0.47 7 -1 -15 6.72 1.12 -7 -1 15 7.28 0.58 -7 -1 15 7.78 0.56 7 1 -15 7.81 0.65 7 1 -15 8.32 0.66 -7 1 15 7.92 0.54 -7 1 15 7.18 0.60 -6 -1 15 2.14 0.36 6 -1 -15 2.21 0.38 -6 -1 15 2.39 0.40 6 1 -15 2.28 0.41 -6 1 15 2.33 0.59 -6 1 15 2.56 0.41 6 1 -15 2.74 0.39 -5 -1 15 11.07 0.67 5 -1 -15 11.31 0.58 -5 -1 15 11.28 0.64 -5 1 15 10.87 0.68 -5 1 15 11.16 0.61 5 1 -15 10.61 0.71 5 1 -15 11.19 0.59 4 -1 -15 58.69 1.55 -4 -1 15 58.28 1.69 4 1 -15 56.97 1.74 -4 1 15 60.27 1.73 -4 1 15 58.80 1.64 4 1 -15 60.40 1.58 3 1 -15 21.78 0.68 -3 1 15 21.57 0.81 -3 1 15 22.19 0.90 3 1 -15 21.98 0.91 2 1 -15 77.02 1.86 -2 1 15 74.97 2.03 2 1 -15 72.95 2.09 1 -1 -15 200.61 4.77 -1 -1 15 181.15 4.86 -1 1 15 193.43 4.75 1 1 -15 186.14 4.89 0 -1 -15 130.58 3.35 0 -1 15 133.07 3.39 0 1 -15 134.53 3.38 0 1 15 126.22 3.55 1 -1 15 99.52 2.68 -1 -1 -15 100.15 2.61 -1 1 -15 100.43 2.64 1 1 15 101.39 2.67 2 -1 15 204.19 5.15 -2 1 -15 208.30 4.94 -2 1 -15 202.70 5.19 2 1 15 203.44 5.14 3 -1 15 151.25 3.71 3 -1 15 145.40 3.91 3 1 15 154.17 3.67 -3 1 -15 151.11 3.78 3 1 15 149.72 3.89 4 -1 15 186.67 4.57 -4 1 -15 178.19 4.57 4 1 15 189.31 4.54 4 1 15 186.60 4.73 5 -1 15 50.55 1.45 -5 1 -15 49.12 1.39 5 1 15 50.84 1.43 5 1 15 48.49 1.59 6 -1 15 40.02 1.27 6 1 15 35.42 1.34 -6 1 -15 36.82 1.08 6 1 15 37.04 1.25 7 -1 15 10.89 0.84 7 -1 15 9.96 0.71 7 1 15 10.12 0.83 7 1 15 9.25 0.73 8 -1 15 1.33 0.44 8 -1 15 0.65 0.48 8 1 15 0.49 0.48 8 1 15 0.50 0.44 9 -1 15 0.84 0.49 9 1 15 0.55 0.83 9 1 15 0.91 0.50 -12 -2 15 36.99 1.34 12 -2 -15 32.28 1.52 12 2 -15 32.97 1.53 -12 2 15 33.87 1.41 11 -2 -15 1.62 0.59 -11 -2 15 1.03 0.41 -11 2 15 1.19 0.48 11 2 -15 1.94 0.60 10 -2 -15 57.83 1.92 -10 2 15 57.91 2.11 10 2 -15 58.02 1.89 9 -2 -15 8.99 0.81 -9 -2 15 9.81 0.66 9 2 -15 9.46 0.83 -9 2 15 9.14 0.80 8 -2 -15 185.78 4.68 -8 -2 15 182.90 4.63 8 2 -15 181.26 4.72 8 2 -15 184.33 4.69 -7 -2 15 4.54 0.52 7 -2 -15 5.19 0.86 -7 -2 15 4.33 0.52 7 2 -15 5.33 0.60 -7 2 15 4.58 0.58 7 2 -15 5.39 0.76 -7 2 15 5.12 0.59 -6 -2 15 152.17 3.81 -6 -2 15 149.66 3.83 6 -2 -15 149.92 3.77 6 2 -15 146.36 3.89 -6 2 15 147.07 3.86 6 2 -15 151.44 3.81 -6 2 15 150.90 3.76 -5 -2 15 23.94 1.04 5 -2 -15 24.99 0.85 -5 -2 15 24.76 0.94 5 2 -15 24.45 1.01 -5 2 15 25.07 0.86 5 2 -15 25.73 0.88 -5 2 15 25.54 0.99 -4 -2 15 180.38 4.48 4 -2 -15 175.84 4.31 -4 -2 15 176.71 4.45 -4 2 15 174.69 4.39 4 2 -15 177.69 4.36 -4 2 15 179.45 4.31 -4 2 15 177.51 4.50 4 2 -15 174.63 4.50 -3 -2 15 1.46 0.36 3 2 -15 1.86 0.38 -3 2 15 1.74 0.38 3 2 -15 2.16 0.35 -3 2 15 1.53 0.31 -2 -2 15 137.97 3.55 -2 2 15 135.95 3.49 2 2 -15 139.16 3.57 2 2 -15 140.12 3.39 -1 -2 15 0.00 0.33 -1 2 15 0.42 0.31 1 2 -15 -0.34 0.35 0 -2 15 0.71 0.36 0 2 15 1.00 0.34 0 2 -15 0.91 0.44 1 -2 15 0.81 0.37 -1 2 -15 -0.38 0.30 -1 2 -15 0.29 0.24 1 2 15 0.21 0.36 2 -2 15 1.35 0.40 -2 2 -15 1.32 0.34 -3 2 -15 0.45 0.28 3 2 15 0.42 0.35 4 -2 15 69.95 1.90 -4 2 -15 69.33 1.91 4 2 15 72.15 1.85 4 2 15 70.58 2.04 5 -2 15 8.56 0.62 -5 2 -15 7.41 0.52 5 2 15 6.95 0.68 5 2 15 7.37 0.54 6 -2 15 73.63 2.25 6 -2 15 80.04 2.15 6 2 15 77.12 2.10 6 2 15 74.81 2.25 -6 2 -15 75.90 2.01 7 -2 15 0.63 0.45 7 -2 15 0.62 0.40 7 2 15 0.32 0.45 7 2 15 -0.14 0.40 8 -2 15 34.37 1.43 8 -2 15 36.61 1.32 8 2 15 35.49 1.29 8 2 15 35.57 1.44 9 2 15 -0.35 0.54 9 2 15 0.02 0.48 -12 -3 15 17.69 0.94 12 -3 -15 17.90 1.22 12 3 -15 17.76 1.27 -12 3 15 18.43 1.13 11 -3 -15 35.69 1.47 11 3 -15 31.43 1.42 -11 3 15 32.36 1.34 10 -3 -15 6.51 0.82 -10 -3 15 6.05 0.61 -10 3 15 8.02 0.76 10 3 -15 6.40 0.82 -9 -3 15 0.17 0.33 9 -3 -15 0.82 0.46 -9 3 15 -0.11 0.39 9 3 -15 0.00 0.36 8 -3 -15 0.99 0.43 -8 -3 15 1.25 0.36 8 3 -15 0.94 0.40 8 3 -15 1.60 0.37 -7 -3 15 17.30 0.79 -7 -3 15 16.41 0.75 7 3 -15 17.32 0.82 -7 3 15 16.81 0.82 7 3 -15 17.35 0.87 -6 -3 15 4.84 0.61 -6 -3 15 5.43 0.54 6 -3 -15 4.98 0.52 6 3 -15 5.05 0.61 -6 3 15 5.52 0.58 6 3 -15 5.55 0.82 -6 3 15 4.72 0.42 -5 -3 15 33.85 1.09 5 -3 -15 32.87 1.02 -5 -3 15 32.39 1.12 5 3 -15 32.97 1.07 -5 3 15 32.96 1.15 5 3 -15 32.85 1.20 -5 3 15 33.65 1.02 4 -3 -15 58.08 1.51 -4 -3 15 58.39 1.64 -4 -3 15 57.78 1.67 -4 3 15 57.58 1.51 4 3 -15 57.55 1.58 -4 3 15 58.06 1.57 -4 3 15 56.36 1.71 4 3 -15 55.19 1.71 -3 -3 15 58.37 1.69 3 3 -15 58.00 1.73 -3 3 15 58.38 1.72 -3 3 15 58.02 1.59 3 3 -15 58.12 1.57 -2 -3 15 43.24 1.36 -2 3 15 43.06 1.39 -2 3 15 42.94 1.27 2 3 -15 44.13 1.40 -1 -3 15 182.32 4.58 -1 3 15 178.17 4.50 1 3 -15 183.15 4.66 0 -3 15 69.66 2.00 0 3 15 70.60 1.95 0 3 -15 71.55 2.00 1 -3 15 85.59 2.37 1 3 15 88.56 2.35 -1 3 -15 84.08 2.47 2 -3 15 4.78 0.59 2 3 15 2.95 0.42 -3 3 -15 115.45 3.17 3 3 15 119.53 3.10 4 -3 15 48.16 1.41 -4 3 -15 47.30 1.43 4 3 15 48.31 1.33 4 3 15 47.42 1.51 5 -3 15 58.04 1.65 5 -3 15 46.79 1.81 5 3 15 56.05 1.54 -5 3 -15 55.47 1.58 5 3 15 55.59 1.72 6 -3 15 28.33 1.05 6 -3 15 27.48 1.20 6 3 15 28.57 1.05 -6 3 -15 27.75 0.97 6 3 15 27.40 1.15 7 -3 15 44.74 1.46 7 -3 15 42.84 1.57 7 3 15 43.67 1.56 7 3 15 45.82 1.46 8 -3 15 4.23 0.64 8 -3 15 4.29 0.94 8 3 15 4.31 0.61 8 3 15 3.78 0.54 9 -3 15 3.51 1.05 9 3 15 3.26 0.63 9 3 15 3.63 0.59 -12 -4 15 1.29 0.42 12 -4 -15 1.01 0.62 12 4 -15 1.41 0.68 11 -4 -15 18.72 1.15 11 4 -15 16.85 1.22 -11 4 15 17.85 1.07 10 -4 -15 5.55 0.80 -10 -4 15 4.40 0.56 10 4 -15 4.52 0.66 -10 4 15 5.84 0.74 9 -4 -15 89.24 2.63 -9 -4 15 97.05 2.54 -9 4 15 95.66 2.91 9 4 -15 98.06 2.69 -8 -4 15 0.44 0.34 8 -4 -15 0.59 0.39 -8 4 15 0.39 0.45 8 4 -15 0.38 0.39 7 -4 -15 78.87 2.15 -7 -4 15 76.59 2.18 7 4 -15 75.75 2.22 7 4 -15 78.17 2.19 6 -4 -15 0.44 0.31 -6 -4 15 0.44 0.32 -6 -4 15 0.08 0.32 -6 4 15 0.27 0.23 6 4 -15 0.70 0.34 6 4 -15 0.64 0.35 -5 -4 15 215.38 5.21 5 -4 -15 207.04 5.16 -5 -4 15 207.04 5.28 -5 4 15 215.10 5.15 5 4 -15 206.81 5.34 5 4 -15 211.48 5.24 -5 4 15 212.20 5.56 -4 -4 15 27.17 0.92 4 -4 -15 26.84 0.83 -4 -4 15 26.40 0.99 4 4 -15 27.46 0.92 4 4 -15 26.24 1.06 -4 4 15 25.98 1.02 -4 4 15 27.13 0.85 -3 -4 15 119.93 3.13 3 4 -15 120.78 3.18 -3 4 15 116.94 3.01 -3 4 15 117.98 3.17 -3 4 15 122.55 2.93 -2 -4 15 3.23 0.42 -2 4 15 3.44 0.57 -2 4 15 2.83 0.45 2 4 -15 2.69 0.41 -1 -4 15 68.61 1.96 1 4 -15 69.74 1.98 -1 4 15 67.74 1.86 0 -4 15 9.96 0.69 0 4 15 9.75 0.62 0 4 -15 9.61 0.69 1 -4 15 46.36 1.46 -1 4 -15 47.07 1.45 1 4 15 44.46 1.50 2 -4 15 16.41 0.82 2 4 15 16.09 0.81 -2 4 -15 16.41 0.80 3 -4 15 25.69 1.02 -3 4 -15 25.75 0.98 3 4 15 25.79 0.99 -4 4 -15 2.97 0.40 4 4 15 2.75 0.36 4 4 15 3.03 0.43 5 -4 15 32.54 1.25 5 -4 15 32.32 1.14 5 4 15 32.29 1.32 5 4 15 33.16 1.06 -5 4 -15 33.20 1.14 6 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4.18 0.68 8 -6 -15 94.66 2.61 -8 -6 15 94.27 2.44 8 6 -15 92.34 2.76 8 6 -15 94.87 2.70 7 -6 -15 8.80 0.67 -7 -6 15 7.55 0.52 7 6 -15 8.35 0.75 7 6 -15 8.68 0.69 -6 -6 15 158.87 3.91 6 6 -15 159.26 4.09 6 6 -15 154.58 4.13 -5 -6 15 0.19 0.27 5 -6 -15 1.41 0.30 5 6 -15 0.75 0.56 -5 6 15 0.32 0.18 -5 6 15 0.50 0.39 5 6 -15 0.82 0.35 -4 -6 15 178.65 4.37 -4 6 15 174.53 4.53 -4 6 15 178.59 4.33 4 6 -15 173.80 4.56 -3 -6 15 1.71 0.42 -3 6 15 2.42 0.34 -3 6 15 1.98 0.40 -2 -6 15 24.00 0.96 -2 6 15 24.41 0.78 2 6 -15 22.87 1.06 -2 6 15 23.41 0.98 -2 6 15 24.53 0.80 -1 -6 15 -0.46 0.32 -1 6 15 0.30 0.35 1 6 -15 0.01 0.33 -1 6 15 0.26 0.27 -1 6 15 0.00 0.24 0 -6 15 98.62 2.69 0 6 15 98.90 2.57 0 6 -15 98.97 2.72 1 -6 15 19.83 0.96 1 6 15 18.87 1.20 -1 6 -15 21.17 0.91 2 -6 15 4.85 0.60 -2 6 -15 4.62 0.60 2 6 15 4.18 0.37 2 6 15 5.55 0.56 3 6 15 -0.27 0.24 -3 6 -15 -0.49 0.30 3 6 15 -0.28 0.32 4 -6 15 12.80 1.22 4 6 15 12.35 0.64 4 6 15 14.81 0.80 -4 6 -15 14.32 0.78 5 -6 15 1.71 0.46 5 6 15 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27.59 1.31 1 -2 25 0.05 0.50 1 2 25 -0.27 0.42 -1 2 -25 0.54 0.44 2 -2 25 34.25 1.85 -2 2 -25 33.52 1.50 2 2 25 33.89 1.45 3 -2 25 1.45 0.60 -8 -3 25 8.23 0.86 -8 -3 25 8.24 1.06 -8 3 25 8.77 0.82 -8 3 25 8.06 1.06 8 3 -25 8.89 1.04 -7 -3 25 5.09 0.77 -7 3 25 4.82 0.67 7 3 -25 5.04 1.12 -7 3 25 4.52 0.76 -6 -3 25 28.73 1.29 -6 -3 25 30.77 1.28 6 3 -25 29.58 1.42 -6 3 25 27.87 1.12 -6 3 25 27.99 1.41 -5 -3 25 81.05 2.46 -5 -3 25 83.81 2.46 5 3 -25 81.27 2.53 -5 3 25 79.15 2.53 -5 3 25 80.20 2.32 -4 -3 25 12.38 0.91 -4 -3 25 15.06 0.97 -4 3 25 11.25 0.77 4 3 -25 11.93 0.99 -4 3 25 11.12 1.00 -3 -3 25 25.16 1.22 -3 3 25 25.85 1.29 3 3 -25 24.60 1.23 -3 3 25 26.21 1.09 -2 -3 25 24.19 1.19 -2 3 25 22.78 1.23 -2 3 25 23.29 1.08 2 3 -25 22.00 1.19 -1 -3 25 69.26 2.22 -1 3 25 68.64 2.27 1 3 -25 69.27 2.25 0 -3 25 9.15 0.95 0 3 25 10.58 0.89 0 3 -25 10.52 0.90 1 -3 25 29.12 1.42 -1 3 -25 29.11 1.29 1 3 25 29.54 1.30 2 -3 25 11.26 1.41 2 3 25 11.13 0.98 -2 3 -25 14.40 0.94 -7 -4 25 16.04 1.23 -7 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25 14.75 0.87 3 5 -25 16.69 1.12 -3 5 25 15.65 1.13 -2 -5 25 45.95 1.71 -2 5 25 42.20 1.49 2 5 -25 45.09 1.72 -2 5 25 42.35 1.74 -1 -5 25 24.08 1.26 -1 5 25 21.90 1.29 1 5 -25 22.06 1.23 -1 5 25 21.66 1.17 0 -5 25 28.31 1.96 0 5 -25 26.14 1.33 0 5 25 32.13 1.26 1 -5 25 14.98 1.14 -1 5 -25 14.69 1.05 1 5 25 14.36 0.98 -6 -6 25 2.39 0.71 -6 -6 25 3.11 0.61 6 6 -25 3.15 0.63 -6 6 25 3.36 0.66 -5 -6 25 13.24 1.11 5 6 -25 13.27 1.14 -5 6 25 10.79 1.08 -4 6 25 4.62 0.58 -3 6 25 0.25 0.36 3 6 -25 -0.16 0.54 -3 6 25 -0.01 0.64 -2 6 25 18.00 1.39 -2 6 25 17.29 0.98 2 6 -25 19.65 1.25 -1 -6 25 13.97 1.69 1 6 -25 11.27 1.11 -1 6 25 13.15 0.85 0 -6 25 10.09 1.03 0 6 25 8.30 1.12 0 6 -25 9.46 1.04 -4 -7 25 9.59 0.96 -4 7 25 7.75 0.99 4 7 -25 8.09 1.05 -3 -7 25 29.20 1.39 -3 7 25 28.28 1.42 3 7 -25 29.70 1.49 -2 -7 25 11.47 1.05 -2 7 25 11.14 0.89 2 7 -25 10.34 1.44 -2 7 25 10.69 1.10 -1 -7 25 26.65 1.34 -1 7 25 25.46 1.39 1 7 -25 26.16 2.07 -1 7 25 25.30 1.09 -7 0 26 0.35 0.54 -7 0 26 0.54 0.42 -6 0 26 17.72 1.11 -6 0 26 17.74 0.99 -5 0 26 -0.08 0.43 -5 0 26 0.01 0.52 -4 0 26 3.44 0.54 -4 0 26 3.55 0.67 -3 0 26 -0.55 0.53 -3 0 26 -0.01 0.43 -2 0 26 2.90 0.54 0 0 26 19.10 1.11 1 0 26 1.06 0.60 2 0 26 32.44 1.65 -7 -1 26 8.33 0.83 -7 -1 26 9.41 0.94 -7 1 26 8.55 0.99 -7 1 26 9.54 1.01 -6 -1 26 7.67 0.90 -6 -1 26 8.54 0.84 -6 1 26 8.17 0.96 -6 1 26 10.21 1.03 -5 -1 26 24.28 1.24 -5 -1 26 24.22 1.16 -5 1 26 27.86 1.15 -5 1 26 25.87 1.29 -4 -1 26 15.08 1.08 -4 -1 26 15.01 0.96 -4 1 26 14.79 1.09 -4 1 26 17.65 0.95 -3 -1 26 37.85 1.56 -3 1 26 38.70 1.58 -3 1 26 37.42 1.45 -2 -1 26 48.64 1.70 -2 1 26 46.91 1.66 2 1 -26 46.89 1.72 -1 -1 26 25.08 1.25 1 1 -26 25.92 1.20 -1 1 26 23.49 1.17 0 -1 26 5.37 0.67 0 1 26 6.31 0.88 1 -1 26 22.23 1.36 1 1 26 23.21 1.67 2 -1 26 10.94 1.03 -7 -2 26 19.99 1.12 -7 -2 26 17.57 1.10 -7 2 26 23.59 1.02 -6 -2 26 0.12 0.50 -6 -2 26 0.58 0.47 6 2 -26 0.22 0.70 -6 2 26 0.55 0.60 -5 -2 26 6.66 0.86 -5 -2 26 6.45 1.06 -5 2 26 7.64 0.97 5 2 -26 7.02 0.98 -4 -2 26 3.15 0.62 -4 -2 26 2.05 0.51 -4 2 26 2.85 0.67 4 2 -26 2.05 0.57 -3 -2 26 1.16 0.51 3 2 -26 -0.12 0.47 -3 2 26 0.46 0.53 -2 -2 26 1.17 0.51 -2 2 26 0.50 0.60 2 2 -26 -0.48 0.46 -2 2 26 -0.09 0.43 -1 -2 26 14.10 1.03 -1 2 26 12.64 0.93 1 2 -26 13.81 1.01 0 -2 26 5.56 0.72 0 2 -26 5.64 0.81 0 2 26 5.86 0.85 -1 2 -26 18.94 1.06 1 2 26 19.16 1.11 2 -2 26 2.60 0.63 2 2 26 2.41 1.01 -2 2 -26 1.93 0.49 -7 -3 26 15.60 1.03 -7 -3 26 17.82 1.65 -7 3 26 18.14 1.19 7 3 -26 17.55 1.20 -6 -3 26 34.92 1.46 -6 -3 26 32.41 1.38 -6 3 26 30.19 2.13 -6 3 26 33.71 1.75 6 3 -26 32.50 2.18 -5 -3 26 23.17 1.19 -5 -3 26 24.84 1.26 -5 3 26 25.45 1.23 -5 3 26 23.27 1.33 5 3 -26 24.78 1.39 -4 -3 26 31.17 1.37 -4 -3 26 31.80 1.36 4 3 -26 30.90 1.44 -4 3 26 29.60 1.47 -3 -3 26 26.24 1.30 -3 3 26 24.74 1.36 -3 3 26 27.37 1.63 3 3 -26 27.64 1.34 -2 -3 26 23.84 1.28 -2 3 26 27.71 1.16 2 3 -26 24.52 1.27 -2 3 26 22.59 1.30 -1 -3 26 4.12 0.67 1 3 -26 4.28 0.60 -1 3 26 6.11 0.77 0 -3 26 9.48 1.17 0 3 26 8.93 0.89 0 3 -26 8.25 0.91 1 -3 26 7.43 1.01 1 3 26 8.83 0.89 -1 3 -26 8.21 0.92 -6 -4 26 7.18 0.86 6 4 -26 7.56 0.99 -6 4 26 8.24 0.70 -6 4 26 6.97 0.98 -5 -4 26 1.20 0.55 -5 -4 26 0.30 0.55 -5 4 26 1.18 0.43 -4 -4 26 5.63 0.84 -4 -4 26 6.19 0.74 -4 4 26 4.75 0.67 4 4 -26 4.88 0.70 -4 4 26 5.52 0.89 -3 -4 26 -0.48 0.52 -3 4 26 -0.04 0.47 3 4 -26 -0.20 0.54 -3 4 26 -0.22 0.54 -2 -4 26 3.67 0.67 -2 4 26 3.89 0.79 2 4 -26 2.68 0.60 -1 -4 26 0.91 0.86 1 4 -26 0.05 0.48 -1 4 26 0.21 0.42 0 -4 26 42.09 1.73 0 4 -26 43.22 1.64 0 4 26 40.53 1.56 1 -4 26 3.27 0.67 -1 4 -26 2.85 0.56 1 4 26 3.25 0.59 -5 -5 26 25.79 1.21 -5 -5 26 25.65 1.30 -5 5 26 25.48 1.14 5 5 -26 25.28 1.40 -5 5 26 24.83 1.35 -4 -5 26 12.81 1.00 -4 -5 26 11.68 1.34 -4 5 26 12.63 1.19 4 5 -26 11.91 1.73 -4 5 26 12.47 0.79 -3 5 26 22.52 1.04 -3 5 26 21.28 1.93 3 5 -26 26.22 1.73 -2 -5 26 16.64 1.33 -2 5 26 17.33 1.39 2 5 -26 17.45 1.19 -1 -5 26 14.47 1.13 1 5 -26 14.31 1.13 -1 5 26 13.46 1.16 -1 5 26 17.60 0.95 0 -5 26 15.98 1.15 0 5 -26 16.89 1.16 0 5 26 17.01 1.04 -4 -6 26 2.63 0.61 -4 -6 26 2.51 0.58 4 6 -26 2.83 0.64 -4 6 26 2.51 0.69 -4 6 26 2.70 0.61 -3 -6 26 3.44 0.62 -3 6 26 2.27 0.45 -3 6 26 2.71 0.68 3 6 -26 2.09 0.61 -2 -6 26 2.82 0.64 -2 6 26 2.58 0.49 2 6 -26 2.04 0.70 -2 6 26 2.19 0.69 -6 0 27 0.49 0.58 -6 0 27 0.79 0.47 -5 0 27 2.67 0.51 -5 0 27 3.00 0.67 -4 0 27 -0.22 0.42 -4 0 27 -0.55 0.54 -3 0 27 5.99 0.98 -3 0 27 7.51 0.86 -2 0 27 -0.43 0.46 -1 0 27 29.89 1.38 -6 -1 27 16.03 1.03 -6 -1 27 14.43 1.09 -6 1 27 16.43 0.96 -5 -1 27 18.21 1.15 -5 -1 27 17.36 1.04 -5 1 27 17.23 1.23 -5 1 27 17.85 0.99 -4 -1 27 12.94 1.09 -4 -1 27 13.07 0.97 -4 1 27 12.57 1.11 -4 1 27 13.03 0.89 -3 -1 27 38.21 1.52 -3 -1 27 38.43 1.62 -3 1 27 37.25 1.64 -3 1 27 38.16 1.47 -2 -1 27 26.12 1.57 -2 1 27 25.57 1.21 -1 -1 27 5.74 0.73 -1 1 27 5.75 0.85 0 1 27 21.78 1.24 -6 -2 27 9.61 0.98 -6 -2 27 10.37 0.98 -6 2 27 10.53 0.82 -6 2 27 9.18 1.05 -5 -2 27 2.03 0.59 -5 -2 27 1.95 0.62 -5 2 27 2.39 0.54 5 2 -27 1.66 0.68 -4 -2 27 0.66 0.57 -4 2 27 1.18 0.44 4 2 -27 -0.02 0.59 -4 2 27 -0.02 1.06 -3 -2 27 0.53 0.57 -3 -2 27 0.48 0.53 -3 2 27 0.00 1.03 -3 2 27 0.70 0.44 3 2 -27 -0.15 0.54 -2 -2 27 7.50 0.99 -2 2 27 7.80 0.83 2 2 -27 7.73 1.00 -1 -2 27 0.35 0.67 -1 2 27 0.64 0.50 1 2 -27 -0.56 0.46 0 -2 27 16.64 1.18 0 2 -27 18.13 1.10 0 2 27 18.22 1.15 -5 -3 27 31.01 1.44 -5 3 27 37.41 1.31 5 3 -27 32.97 1.56 -5 3 27 32.08 1.54 -4 -3 27 8.48 1.22 -4 -3 27 9.35 0.99 -4 3 27 7.88 1.21 4 3 -27 6.10 1.15 -3 -3 27 26.30 1.65 3 3 -27 25.42 1.51 -3 3 27 19.92 1.50 -3 3 27 23.60 1.14 2 3 -27 22.14 1.30 -2 3 27 21.36 1.31 -2 3 27 22.76 1.12 -1 -3 27 28.26 1.49 1 3 -27 31.40 1.43 -1 3 27 30.22 1.30 0 -3 27 12.02 1.07 0 3 27 11.29 0.99 0 3 -27 12.71 1.04 -5 -4 27 1.43 0.58 5 4 -27 2.10 0.58 -5 4 27 2.31 0.62 -4 -4 27 -0.34 0.52 -4 -4 27 0.38 0.55 4 4 -27 0.02 0.65 -4 4 27 -0.69 0.53 -3 -4 27 1.53 0.57 -3 4 27 1.01 0.58 3 4 -27 0.59 0.74 -2 -4 27 1.21 0.55 -2 4 27 0.17 0.56 -2 4 27 0.52 0.46 2 4 -27 -0.08 0.95 -1 -4 27 20.65 1.22 -1 4 27 16.49 1.25 -1 4 27 18.03 1.02 1 4 -27 17.65 1.29 -4 0 28 0.38 0.50 -4 0 28 0.96 1.06 -3 0 28 -0.07 0.51 -3 0 28 -0.47 0.65 -2 0 28 22.43 1.27 -4 -1 28 15.55 1.11 -4 -1 28 11.89 1.70 -4 1 28 14.22 1.15 -4 1 28 16.14 0.99 -3 -1 28 39.18 1.94 -3 1 28 36.90 1.65 -3 1 28 35.77 1.48 -2 1 28 7.99 0.96 -3 -2 28 0.41 0.55 3 2 -28 0.82 0.61 -3 2 28 0.20 0.59 -3 2 28 0.23 0.47 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 65046 _shelx_res_file ; TITL AYY323-Cd in P2(1)/n compound.res created by SHELXL-2018/3 at 14:28:25 on 19-Sep-2022 CELL 0.71073 10.11050 12.06030 21.20130 90.0000 103.0668 90.0000 ZERR 4.00 0.00060 0.00060 0.00120 0.0000 0.0012 0.0000 LATT 1 SYMM 0.5-X, 0.5+Y, 0.5-Z SFAC C H N O Cd UNIT 112 80 16 28 4 L.S. 8 ACTA BOND $H FMAP 2 PLAN 1 SIZE 0.25 0.20 0.20 CONF EQIV $1 x+1, y-1, z HTAB O7 O4_$1 EQIV $2 -x+1/2, y-1/2, -z+1/2 HTAB C9 O4_$2 EQIV $3 -x+1, -y, -z HTAB C15 O5_$3 EQIV $4 -x+1/2, y+1/2, -z+1/2 HTAB C17 O3_$4 HTAB C23 O3_$4 EQIV $5 x-1/2, -y+1/2, z+1/2 HTAB C28 O7_$5 BIND Cd1 O4 FREE C1 Cd1 TEMP 25 WGHT 0.023900 2.099400 EXTI 0.011443 FVAR 0.18541 MOLE 1 CD1 5 0.220220 0.382757 0.236169 11.00000 0.01754 0.02276 = 0.02298 -0.00162 0.00386 0.00044 N1 3 0.240270 0.448337 0.336129 11.00000 0.02142 0.03004 = 0.02637 -0.00332 0.00450 -0.00070 N2 3 0.313390 0.551276 0.422786 11.00000 0.02810 0.02893 = 0.02434 -0.00410 0.00632 -0.00276 N3 3 0.636714 0.863030 0.585217 11.00000 0.04462 0.04200 = 0.03839 -0.01673 0.01544 -0.01471 N4 3 0.712183 0.983646 0.662459 11.00000 0.03636 0.04459 = 0.04155 -0.01731 0.01638 -0.01164 O1 4 0.473554 0.378639 0.255054 11.00000 0.02722 0.04887 = 0.05567 -0.02317 0.00926 0.00687 O2 4 0.344463 0.251021 0.198738 11.00000 0.01994 0.04488 = 0.09200 -0.02355 0.01816 -0.00308 O3 4 0.057646 0.250575 0.219277 11.00000 0.01784 0.03114 = 0.05621 -0.00676 0.01017 -0.00023 O4 4 -0.045864 0.410812 0.218776 11.00000 0.02267 0.02503 = 0.04324 -0.00123 0.00164 -0.00306 O5 4 0.625763 -0.053044 0.085210 11.00000 0.03723 0.01900 = 0.02459 0.00098 0.00222 0.00412 O6 4 0.731502 -0.543074 0.077078 11.00000 0.11144 0.02819 = 0.04955 -0.00853 -0.00809 0.02034 O7 4 0.789703 -0.433244 0.162454 11.00000 0.05228 0.02598 = 0.03593 0.00042 -0.00360 0.01148 AFIX 147 H7 2 0.832251 -0.488287 0.178216 11.00000 -1.50000 AFIX 0 C1 1 0.458524 0.293529 0.221114 11.00000 0.01915 0.02840 = 0.03026 0.00333 0.00951 0.00553 C2 1 0.580877 0.238913 0.204956 11.00000 0.01611 0.02492 = 0.02112 0.00136 0.00405 0.00301 C3 1 0.574766 0.129697 0.183916 11.00000 0.01788 0.02421 = 0.02647 0.00100 0.00360 -0.00187 AFIX 43 H3 2 0.493198 0.091071 0.177501 11.00000 -1.20000 AFIX 0 C4 1 0.689926 0.077419 0.172321 11.00000 0.02046 0.01958 = 0.02443 -0.00081 0.00408 -0.00002 C5 1 0.811386 0.135891 0.182814 11.00000 0.01851 0.02449 = 0.03132 -0.00345 0.00681 0.00165 AFIX 43 H5 2 0.889475 0.100569 0.176930 11.00000 -1.20000 AFIX 0 C6 1 0.817958 0.246486 0.201993 11.00000 0.01586 0.02517 = 0.02487 -0.00211 0.00474 -0.00142 C7 1 0.701494 0.298026 0.212428 11.00000 0.01864 0.02153 = 0.02176 -0.00275 0.00304 0.00087 AFIX 43 H7A 2 0.704414 0.372305 0.224447 11.00000 -1.20000 AFIX 0 C8 1 -0.049207 0.307073 0.213675 11.00000 0.01731 0.02843 = 0.02250 -0.00335 0.00468 -0.00250 C9 1 0.686727 -0.042341 0.153115 11.00000 0.02598 0.02009 = 0.02460 -0.00026 0.00252 0.00165 AFIX 23 H9A 2 0.778391 -0.071717 0.162082 11.00000 -1.20000 H9B 2 0.634812 -0.084499 0.178121 11.00000 -1.20000 AFIX 0 C10 1 0.611507 -0.159802 0.062173 11.00000 0.02561 0.02001 = 0.02621 -0.00099 0.00726 0.00092 C11 1 0.669899 -0.251484 0.097163 11.00000 0.02732 0.02251 = 0.02384 -0.00064 0.00316 0.00161 AFIX 43 H11 2 0.716571 -0.243958 0.140087 11.00000 -1.20000 AFIX 0 C12 1 0.657791 -0.354990 0.067233 11.00000 0.03689 0.02172 = 0.02913 -0.00008 0.00528 0.00204 C13 1 0.584641 -0.367007 0.004057 11.00000 0.07118 0.02650 = 0.03134 -0.00711 -0.00029 0.00172 AFIX 43 H13 2 0.577335 -0.436160 -0.015842 11.00000 -1.20000 AFIX 0 C14 1 0.522388 -0.275394 -0.029342 11.00000 0.07008 0.03618 = 0.02399 -0.00220 -0.00675 0.00062 AFIX 43 H14 2 0.470604 -0.283855 -0.071289 11.00000 -1.20000 AFIX 0 C15 1 0.536246 -0.171825 -0.001170 11.00000 0.04207 0.02808 = 0.02517 0.00443 0.00089 0.00383 AFIX 43 H15 2 0.495691 -0.110440 -0.024249 11.00000 -1.20000 AFIX 0 C16 1 0.728330 -0.453760 0.101938 11.00000 0.04108 0.02301 = 0.03587 0.00005 0.00557 0.00314 C17 1 0.315347 0.534680 0.359797 11.00000 0.02564 0.03171 = 0.02417 -0.00251 0.00616 -0.00283 AFIX 43 H17 2 0.363176 0.578285 0.336400 11.00000 -1.20000 AFIX 0 C18 1 0.186280 0.408216 0.385858 11.00000 0.02569 0.03173 = 0.03309 -0.00311 0.00950 -0.00405 AFIX 43 H18 2 0.128264 0.347660 0.382955 11.00000 -1.20000 AFIX 0 C19 1 0.230763 0.470547 0.439444 11.00000 0.03281 0.03642 = 0.03070 -0.00297 0.01325 -0.00565 AFIX 43 H19 2 0.209816 0.460923 0.479606 11.00000 -1.20000 AFIX 0 C20 1 0.390153 0.632873 0.464458 11.00000 0.03481 0.02882 = 0.02638 -0.00577 0.00538 -0.00336 C21 1 0.414378 0.621126 0.531083 11.00000 0.02819 0.03434 = 0.02666 -0.00225 0.00820 -0.00387 AFIX 43 H21 2 0.377766 0.561282 0.548953 11.00000 -1.20000 AFIX 0 C22 1 0.493198 0.698570 0.571130 11.00000 0.02907 0.03967 = 0.02575 -0.00707 0.00680 -0.00128 AFIX 43 H22 2 0.508012 0.691674 0.615872 11.00000 -1.20000 AFIX 0 C23 1 0.443708 0.722293 0.437943 11.00000 0.10634 0.04855 = 0.02497 -0.00253 0.00892 -0.03407 AFIX 43 H23 2 0.425369 0.731428 0.393250 11.00000 -1.20000 AFIX 0 C24 1 0.524555 0.798124 0.477934 11.00000 0.11154 0.04656 = 0.03826 -0.00421 0.01524 -0.04272 AFIX 43 H24 2 0.562256 0.857517 0.460181 11.00000 -1.20000 AFIX 0 C25 1 0.549289 0.785486 0.544457 11.00000 0.04292 0.03551 = 0.03397 -0.01196 0.00940 -0.00920 C26 1 0.762487 0.896611 0.578268 11.00000 0.07743 0.09530 = 0.07825 -0.05617 0.05556 -0.05055 AFIX 43 H26 2 0.807336 0.873294 0.546852 11.00000 -1.20000 AFIX 0 C27 1 0.807877 0.970288 0.626235 11.00000 0.06728 0.09052 = 0.07887 -0.05270 0.04895 -0.04789 AFIX 43 H27 2 0.891196 1.006468 0.633625 11.00000 -1.20000 AFIX 0 C28 1 0.612822 0.916379 0.637009 11.00000 0.03281 0.04254 = 0.04022 -0.01510 0.01113 -0.00611 AFIX 43 H28 2 0.535083 0.906755 0.652919 11.00000 -1.20000 AFIX 0 HKLF 4 REM AYY323-Cd in P2(1)/n REM wR2 = 0.0614, GooF = S = 1.083, Restrained GooF = 1.083 for all data REM R1 = 0.0237 for 5751 Fo > 4sig(Fo) and 0.0263 for all 6188 data REM 363 parameters refined using 0 restraints END WGHT 0.0251 1.7740 REM Highest difference peak 0.459, deepest hole -0.373, 1-sigma level 0.062 Q1 1 0.7442 1.0188 0.6052 11.00000 0.05 0.46 ; _shelx_res_checksum 32959 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cd Cd1 0.22022(2) 0.38276(2) 0.23617(2) 0.02121(6) Uani d 1 . . N N1 0.24027(15) 0.44834(13) 0.33613(7) 0.0261(3) Uani d 1 . . N N2 0.31339(16) 0.55128(13) 0.42279(7) 0.0271(3) Uani d 1 . . N N3 0.6367(2) 0.86303(16) 0.58522(9) 0.0407(4) Uani d 1 . . N N4 0.71218(19) 0.98365(16) 0.66246(9) 0.0396(4) Uani d 1 . . O O1 0.47355(15) 0.37864(13) 0.25505(9) 0.0439(4) Uani d 1 . . O O2 0.34446(15) 0.25102(14) 0.19874(10) 0.0514(5) Uani d 1 . . O O3 0.05765(13) 0.25058(12) 0.21928(8) 0.0348(3) Uani d 1 . . O O4 -0.04586(13) 0.41081(11) 0.21878(7) 0.0312(3) Uani d 1 . . O O5 0.62576(14) -0.05304(10) 0.08521(6) 0.0277(3) Uani d 1 . . O O6 0.7315(3) -0.54307(14) 0.07708(9) 0.0672(6) Uani d 1 . . O O7 0.78970(17) -0.43324(12) 0.16245(7) 0.0402(4) Uani d 1 . . H H7 0.832251 -0.488287 0.178216 0.060 Uiso calc 1 . . C C1 0.45852(17) 0.29353(15) 0.22111(9) 0.0253(4) Uani d 1 . . C C2 0.58088(16) 0.23891(14) 0.20496(8) 0.0207(3) Uani d 1 . . C C3 0.57477(17) 0.12970(14) 0.18392(8) 0.0231(3) Uani d 1 . . H H3 0.493198 0.091071 0.177501 0.028 Uiso calc 1 . . C C4 0.68993(17) 0.07742(14) 0.17232(8) 0.0216(3) Uani d 1 . . C C5 0.81139(17) 0.13589(15) 0.18281(9) 0.0246(3) Uani d 1 . . H H5 0.889475 0.100569 0.176930 0.030 Uiso calc 1 . . C C6 0.81796(16) 0.24649(15) 0.20199(8) 0.0219(3) Uani d 1 . . C C7 0.70149(16) 0.29803(14) 0.21243(8) 0.0209(3) Uani d 1 . . H H7A 0.704414 0.372305 0.224447 0.025 Uiso calc 1 . . C C8 -0.04921(17) 0.30707(15) 0.21368(8) 0.0227(3) Uani d 1 . . C C9 0.68673(18) -0.04234(14) 0.15311(8) 0.0241(3) Uani d 1 . . H H9A 0.778391 -0.071717 0.162082 0.029 Uiso calc 1 . . H H9B 0.634812 -0.084499 0.178121 0.029 Uiso calc 1 . . C C10 0.61151(18) -0.15980(15) 0.06217(9) 0.0237(3) Uani d 1 . . C C11 0.66990(18) -0.25148(15) 0.09716(9) 0.0250(3) Uani d 1 . . H H11 0.716571 -0.243958 0.140087 0.030 Uiso calc 1 . . C C12 0.6578(2) -0.35499(16) 0.06723(9) 0.0296(4) Uani d 1 . . C C13 0.5846(3) -0.36701(18) 0.00406(11) 0.0449(6) Uani d 1 . . H H13 0.577335 -0.436160 -0.015842 0.054 Uiso calc 1 . . C C14 0.5224(3) -0.27539(19) -0.02934(10) 0.0462(6) Uani d 1 . . H H14 0.470604 -0.283855 -0.071289 0.055 Uiso calc 1 . . C C15 0.5362(2) -0.17182(17) -0.00117(9) 0.0328(4) Uani d 1 . . H H15 0.495691 -0.110440 -0.024249 0.039 Uiso calc 1 . . C C16 0.7283(2) -0.45376(16) 0.10194(10) 0.0338(4) Uani d 1 . . C C17 0.31535(19) 0.53468(16) 0.35980(9) 0.0271(4) Uani d 1 . . H H17 0.363176 0.578285 0.336400 0.033 Uiso calc 1 . . C C18 0.18628(19) 0.40822(17) 0.38586(10) 0.0297(4) Uani d 1 . . H H18 0.128264 0.347660 0.382955 0.036 Uiso calc 1 . . C C19 0.2308(2) 0.47055(17) 0.43944(10) 0.0323(4) Uani d 1 . . H H19 0.209816 0.460923 0.479606 0.039 Uiso calc 1 . . C C20 0.3902(2) 0.63287(16) 0.46446(9) 0.0302(4) Uani d 1 . . C C21 0.4144(2) 0.62113(16) 0.53108(9) 0.0294(4) Uani d 1 . . H H21 0.377766 0.561282 0.548953 0.035 Uiso calc 1 . . C C22 0.4932(2) 0.69857(18) 0.57113(9) 0.0314(4) Uani d 1 . . H H22 0.508012 0.691674 0.615872 0.038 Uiso calc 1 . . C C23 0.4437(4) 0.7223(2) 0.43794(12) 0.0609(8) Uani d 1 . . H H23 0.425369 0.731428 0.393250 0.073 Uiso calc 1 . . C C24 0.5246(4) 0.7981(2) 0.47793(13) 0.0657(9) Uani d 1 . . H H24 0.562256 0.857517 0.460181 0.079 Uiso calc 1 . . C C25 0.5493(2) 0.78549(19) 0.54446(10) 0.0374(5) Uani d 1 . . C C26 0.7625(4) 0.8966(3) 0.57827(17) 0.0776(12) Uani d 1 . . H H26 0.807336 0.873294 0.546852 0.093 Uiso calc 1 . . C C27 0.8079(3) 0.9703(3) 0.62623(16) 0.0737(11) Uani d 1 . . H H27 0.891196 1.006468 0.633625 0.088 Uiso calc 1 . . C C28 0.6128(2) 0.91638(19) 0.63701(11) 0.0381(5) Uani d 1 . . H H28 0.535083 0.906755 0.652919 0.046 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Cd1 0.01754(7) 0.02276(8) 0.02298(8) 0.00044(4) 0.00386(5) -0.00162(4) N1 0.0214(7) 0.0300(8) 0.0264(7) -0.0007(6) 0.0045(6) -0.0033(6) N2 0.0281(8) 0.0289(8) 0.0243(7) -0.0028(6) 0.0063(6) -0.0041(6) N3 0.0446(10) 0.0420(11) 0.0384(10) -0.0147(8) 0.0154(8) -0.0167(8) N4 0.0364(9) 0.0446(11) 0.0415(10) -0.0116(8) 0.0164(8) -0.0173(8) O1 0.0272(7) 0.0489(10) 0.0557(10) 0.0069(6) 0.0093(7) -0.0232(8) O2 0.0199(7) 0.0449(9) 0.0920(14) -0.0031(6) 0.0182(8) -0.0236(9) O3 0.0178(6) 0.0311(7) 0.0562(9) -0.0002(5) 0.0102(6) -0.0068(6) O4 0.0227(6) 0.0250(6) 0.0432(8) -0.0031(5) 0.0016(6) -0.0012(6) O5 0.0372(7) 0.0190(6) 0.0246(6) 0.0041(5) 0.0022(5) 0.0010(5) O6 0.1114(18) 0.0282(8) 0.0496(11) 0.0203(10) -0.0081(11) -0.0085(8) O7 0.0523(9) 0.0260(7) 0.0359(8) 0.0115(7) -0.0036(7) 0.0004(6) C1 0.0192(8) 0.0284(9) 0.0303(9) 0.0055(6) 0.0095(7) 0.0033(7) C2 0.0161(7) 0.0249(8) 0.0211(7) 0.0030(6) 0.0041(6) 0.0014(6) C3 0.0179(7) 0.0242(8) 0.0265(8) -0.0019(6) 0.0036(6) 0.0010(6) C4 0.0205(8) 0.0196(8) 0.0244(8) 0.0000(6) 0.0041(6) -0.0008(6) C5 0.0185(7) 0.0245(9) 0.0313(9) 0.0016(6) 0.0068(6) -0.0034(7) C6 0.0159(7) 0.0252(8) 0.0249(8) -0.0014(6) 0.0047(6) -0.0021(6) C7 0.0186(7) 0.0215(8) 0.0218(8) 0.0009(6) 0.0030(6) -0.0027(6) C8 0.0173(7) 0.0284(9) 0.0225(8) -0.0025(6) 0.0047(6) -0.0034(6) C9 0.0260(8) 0.0201(8) 0.0246(8) 0.0017(6) 0.0025(6) -0.0003(6) C10 0.0256(8) 0.0200(8) 0.0262(8) 0.0009(6) 0.0073(7) -0.0010(6) C11 0.0273(8) 0.0225(8) 0.0238(8) 0.0016(7) 0.0032(7) -0.0006(7) C12 0.0369(10) 0.0217(8) 0.0291(9) 0.0020(7) 0.0053(8) -0.0001(7) C13 0.0712(16) 0.0265(10) 0.0313(11) 0.0017(10) -0.0003(10) -0.0071(8) C14 0.0701(16) 0.0362(12) 0.0240(10) 0.0006(11) -0.0068(10) -0.0022(8) C15 0.0421(11) 0.0281(10) 0.0252(9) 0.0038(8) 0.0009(8) 0.0044(7) C16 0.0411(11) 0.0230(9) 0.0359(10) 0.0031(8) 0.0056(8) 0.0001(8) C17 0.0256(8) 0.0317(9) 0.0242(8) -0.0028(7) 0.0062(7) -0.0025(7) C18 0.0257(9) 0.0317(10) 0.0331(10) -0.0041(7) 0.0095(7) -0.0031(8) C19 0.0328(10) 0.0364(10) 0.0307(10) -0.0056(8) 0.0133(8) -0.0030(8) C20 0.0348(10) 0.0288(10) 0.0264(9) -0.0034(8) 0.0054(7) -0.0058(7) C21 0.0282(9) 0.0343(10) 0.0267(9) -0.0039(7) 0.0082(7) -0.0023(7) C22 0.0291(9) 0.0397(11) 0.0258(9) -0.0013(8) 0.0068(7) -0.0071(8) C23 0.106(2) 0.0486(15) 0.0250(11) -0.0341(15) 0.0089(12) -0.0025(10) C24 0.112(3) 0.0466(15) 0.0383(13) -0.0427(16) 0.0152(14) -0.0042(11) C25 0.0429(12) 0.0355(11) 0.0340(11) -0.0092(9) 0.0094(9) -0.0120(8) C26 0.077(2) 0.095(2) 0.078(2) -0.0506(18) 0.0556(18) -0.0562(19) C27 0.0673(18) 0.091(2) 0.079(2) -0.0479(17) 0.0489(17) -0.0527(18) C28 0.0328(10) 0.0425(12) 0.0402(11) -0.0061(9) 0.0111(9) -0.0151(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cd Cd -0.8075 1.2024 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag N1 Cd1 N4 . 4_575 112.99(7) yes N1 Cd1 O3 . . 107.92(6) yes N4 Cd1 O3 4_575 . 119.21(7) yes N1 Cd1 O2 . . 129.84(7) yes N4 Cd1 O2 4_575 . 101.26(7) yes O3 Cd1 O2 . . 83.76(5) yes N1 Cd1 O1 . . 89.15(5) yes N4 Cd1 O1 4_575 . 90.02(6) yes O3 Cd1 O1 . . 133.88(5) yes O2 Cd1 O1 . . 54.29(5) yes N1 Cd1 O4 . . 87.61(5) yes N4 Cd1 O4 4_575 . 86.30(6) yes O3 Cd1 O4 . . 52.37(4) yes O2 Cd1 O4 . . 131.50(5) yes O1 Cd1 O4 . . 173.71(5) yes C17 N1 C18 . . 106.21(16) ? C17 N1 Cd1 . . 124.25(13) ? C18 N1 Cd1 . . 129.47(13) ? C17 N2 C19 . . 107.02(16) ? C17 N2 C20 . . 125.75(16) ? C19 N2 C20 . . 127.11(16) ? C28 N3 C26 . . 106.79(19) ? C28 N3 C25 . . 127.28(19) ? C26 N3 C25 . . 125.93(19) ? C28 N4 C27 . . 105.59(19) ? C28 N4 Cd1 . 4_676 129.70(15) ? C27 N4 Cd1 . 4_676 123.84(16) ? C1 O1 Cd1 . . 86.39(11) ? C1 O2 Cd1 . . 96.64(12) ? C8 O3 Cd1 . . 102.18(11) ? C8 O4 Cd1 . . 83.78(10) ? C10 O5 C9 . . 115.28(13) ? C16 O7 H7 . . 109.5 ? O1 C1 O2 . . 122.59(17) ? O1 C1 C2 . . 119.54(16) ? O2 C1 C2 . . 117.86(17) ? C3 C2 C7 . . 119.84(15) ? C3 C2 C1 . . 120.57(15) ? C7 C2 C1 . . 119.58(15) ? C2 C3 C4 . . 120.52(15) ? C2 C3 H3 . . 119.7 ? C4 C3 H3 . . 119.7 ? C5 C4 C3 . . 119.04(16) ? C5 C4 C9 . . 119.76(15) ? C3 C4 C9 . . 121.07(15) ? C6 C5 C4 . . 121.01(16) ? C6 C5 H5 . . 119.5 ? C4 C5 H5 . . 119.5 ? C5 C6 C7 . . 119.21(15) ? C5 C6 C8 . 1_655 119.81(15) ? C7 C6 C8 . 1_655 120.94(15) ? C2 C7 C6 . . 120.29(16) ? C2 C7 H7A . . 119.9 ? C6 C7 H7A . . 119.9 ? O4 C8 O3 . . 121.66(16) ? O4 C8 C6 . 1_455 120.36(15) ? O3 C8 C6 . 1_455 117.96(16) ? O5 C9 C4 . . 109.66(14) ? O5 C9 H9A . . 109.7 ? C4 C9 H9A . . 109.7 ? O5 C9 H9B . . 109.7 ? C4 C9 H9B . . 109.7 ? H9A C9 H9B . . 108.2 ? O5 C10 C11 . . 124.03(16) ? O5 C10 C15 . . 115.53(16) ? C11 C10 C15 . . 120.41(17) ? C12 C11 C10 . . 119.20(17) ? C12 C11 H11 . . 120.4 ? C10 C11 H11 . . 120.4 ? C13 C12 C11 . . 120.50(18) ? C13 C12 C16 . . 118.98(18) ? C11 C12 C16 . . 120.47(17) ? C12 C13 C14 . . 119.55(19) ? C12 C13 H13 . . 120.2 ? C14 C13 H13 . . 120.2 ? C15 C14 C13 . . 120.78(19) ? C15 C14 H14 . . 119.6 ? C13 C14 H14 . . 119.6 ? C14 C15 C10 . . 119.47(18) ? C14 C15 H15 . . 120.3 ? C10 C15 H15 . . 120.3 ? O6 C16 O7 . . 122.8(2) ? O6 C16 C12 . . 123.7(2) ? O7 C16 C12 . . 113.43(17) ? N1 C17 N2 . . 110.86(16) ? N1 C17 H17 . . 124.6 ? N2 C17 H17 . . 124.6 ? C19 C18 N1 . . 109.47(17) ? C19 C18 H18 . . 125.3 ? N1 C18 H18 . . 125.3 ? C18 C19 N2 . . 106.44(17) ? C18 C19 H19 . . 126.8 ? N2 C19 H19 . . 126.8 ? C23 C20 C21 . . 119.96(19) ? C23 C20 N2 . . 119.60(18) ? C21 C20 N2 . . 120.41(18) ? C22 C21 C20 . . 120.01(18) ? C22 C21 H21 . . 120.0 ? C20 C21 H21 . . 120.0 ? C25 C22 C21 . . 119.72(18) ? C25 C22 H22 . . 120.1 ? C21 C22 H22 . . 120.1 ? C20 C23 C24 . . 119.9(2) ? C20 C23 H23 . . 120.0 ? C24 C23 H23 . . 120.0 ? C23 C24 C25 . . 119.9(2) ? C23 C24 H24 . . 120.1 ? C25 C24 H24 . . 120.1 ? C22 C25 C24 . . 120.5(2) ? C22 C25 N3 . . 120.35(19) ? C24 C25 N3 . . 119.1(2) ? C27 C26 N3 . . 106.2(2) ? C27 C26 H26 . . 126.9 ? N3 C26 H26 . . 126.9 ? C26 C27 N4 . . 109.6(2) ? C26 C27 H27 . . 125.2 ? N4 C27 H27 . . 125.2 ? N4 C28 N3 . . 111.80(19) ? N4 C28 H28 . . 124.1 ? N3 C28 H28 . . 124.1 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Cd1 N1 . 2.2280(15) yes Cd1 N4 4_575 2.2332(17) yes Cd1 O3 . 2.2595(14) yes Cd1 O2 . 2.2765(15) yes Cd1 O1 . 2.5019(15) yes Cd1 O4 . 2.6532(13) yes N1 C17 . 1.319(2) ? N1 C18 . 1.380(2) ? N2 C17 . 1.355(2) ? N2 C19 . 1.380(2) ? N2 C20 . 1.429(2) ? N3 C28 . 1.341(3) ? N3 C26 . 1.374(3) ? N3 C25 . 1.434(3) ? N4 C28 . 1.309(3) ? N4 C27 . 1.374(3) ? O1 C1 . 1.243(2) ? O2 C1 . 1.253(2) ? O3 C8 . 1.260(2) ? O4 C8 . 1.256(2) ? O5 C10 . 1.373(2) ? O5 C9 . 1.438(2) ? O6 C16 . 1.203(3) ? O7 C16 . 1.316(3) ? O7 H7 . 0.8200 ? C1 C2 . 1.508(2) ? C2 C3 . 1.388(2) ? C2 C7 . 1.390(2) ? C3 C4 . 1.394(2) ? C3 H3 . 0.9300 ? C4 C5 . 1.390(2) ? C4 C9 . 1.499(2) ? C5 C6 . 1.392(2) ? C5 H5 . 0.9300 ? C6 C7 . 1.393(2) ? C6 C8 1_655 1.500(2) ? C7 H7A . 0.9300 ? C9 H9A . 0.9700 ? C9 H9B . 0.9700 ? C10 C11 . 1.387(2) ? C10 C15 . 1.393(3) ? C11 C12 . 1.393(3) ? C11 H11 . 0.9300 ? C12 C13 . 1.384(3) ? C12 C16 . 1.494(3) ? C13 C14 . 1.384(3) ? C13 H13 . 0.9300 ? C14 C15 . 1.378(3) ? C14 H14 . 0.9300 ? C15 H15 . 0.9300 ? C17 H17 . 0.9300 ? C18 C19 . 1.352(3) ? C18 H18 . 0.9300 ? C19 H19 . 0.9300 ? C20 C23 . 1.382(3) ? C20 C21 . 1.385(3) ? C21 C22 . 1.386(3) ? C21 H21 . 0.9300 ? C22 C25 . 1.373(3) ? C22 H22 . 0.9300 ? C23 C24 . 1.382(3) ? C23 H23 . 0.9300 ? C24 C25 . 1.384(3) ? C24 H24 . 0.9300 ? C26 C27 . 1.350(4) ? C26 H26 . 0.9300 ? C27 H27 . 0.9300 ? C28 H28 . 0.9300 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag O7 H7 O4 1_645 0.82 1.81 2.613(2) 168.1 yes C9 H9B O4 2_545 0.97 2.55 3.387(2) 145.2 yes C15 H15 O5 3_655 0.93 2.52 3.449(2) 177.0 yes C17 H17 O3 2 0.93 2.60 3.495(2) 160.6 yes C23 H23 O3 2 0.93 2.44 3.348(3) 164.8 yes C28 H28 O7 4_566 0.93 2.55 3.435(3) 158.2 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag Cd1 O1 C1 O2 . . . . -3.0(2) ? Cd1 O1 C1 C2 . . . . 176.13(15) ? Cd1 O2 C1 O1 . . . . 3.3(2) ? Cd1 O2 C1 C2 . . . . -175.83(13) ? O1 C1 C2 C3 . . . . 161.41(18) ? O2 C1 C2 C3 . . . . -19.4(3) ? O1 C1 C2 C7 . . . . -17.4(3) ? O2 C1 C2 C7 . . . . 161.84(18) ? C7 C2 C3 C4 . . . . 2.2(3) ? C1 C2 C3 C4 . . . . -176.54(16) ? C2 C3 C4 C5 . . . . 0.7(3) ? C2 C3 C4 C9 . . . . 176.60(16) ? C3 C4 C5 C6 . . . . -2.7(3) ? C9 C4 C5 C6 . . . . -178.65(16) ? C4 C5 C6 C7 . . . . 1.7(3) ? C4 C5 C6 C8 . . . 1_655 179.31(16) ? C3 C2 C7 C6 . . . . -3.2(3) ? C1 C2 C7 C6 . . . . 175.58(16) ? C5 C6 C7 C2 . . . . 1.2(3) ? C8 C6 C7 C2 1_655 . . . -176.32(15) ? Cd1 O4 C8 O3 . . . . 0.83(17) ? Cd1 O4 C8 C6 . . . 1_455 179.54(15) ? Cd1 O3 C8 O4 . . . . -1.0(2) ? Cd1 O3 C8 C6 . . . 1_455 -179.73(12) ? C10 O5 C9 C4 . . . . -177.29(14) ? C5 C4 C9 O5 . . . . -104.31(19) ? C3 C4 C9 O5 . . . . 79.8(2) ? C9 O5 C10 C11 . . . . -10.4(2) ? C9 O5 C10 C15 . . . . 171.63(16) ? O5 C10 C11 C12 . . . . -174.93(17) ? C15 C10 C11 C12 . . . . 3.0(3) ? C10 C11 C12 C13 . . . . -2.1(3) ? C10 C11 C12 C16 . . . . 175.35(18) ? C11 C12 C13 C14 . . . . -0.4(4) ? C16 C12 C13 C14 . . . . -178.0(2) ? C12 C13 C14 C15 . . . . 2.2(4) ? C13 C14 C15 C10 . . . . -1.4(4) ? O5 C10 C15 C14 . . . . 176.8(2) ? C11 C10 C15 C14 . . . . -1.3(3) ? C13 C12 C16 O6 . . . . 4.0(4) ? C11 C12 C16 O6 . . . . -173.5(2) ? C13 C12 C16 O7 . . . . -177.3(2) ? C11 C12 C16 O7 . . . . 5.2(3) ? C18 N1 C17 N2 . . . . 0.7(2) ? Cd1 N1 C17 N2 . . . . -176.69(12) ? C19 N2 C17 N1 . . . . -0.5(2) ? C20 N2 C17 N1 . . . . 175.78(17) ? C17 N1 C18 C19 . . . . -0.6(2) ? Cd1 N1 C18 C19 . . . . 176.58(14) ? N1 C18 C19 N2 . . . . 0.3(2) ? C17 N2 C19 C18 . . . . 0.1(2) ? C20 N2 C19 C18 . . . . -176.10(18) ? C17 N2 C20 C23 . . . . 18.6(3) ? C19 N2 C20 C23 . . . . -165.8(2) ? C17 N2 C20 C21 . . . . -159.50(19) ? C19 N2 C20 C21 . . . . 16.1(3) ? C23 C20 C21 C22 . . . . -0.5(3) ? N2 C20 C21 C22 . . . . 177.61(18) ? C20 C21 C22 C25 . . . . -1.3(3) ? C21 C20 C23 C24 . . . . 1.8(5) ? N2 C20 C23 C24 . . . . -176.3(3) ? C20 C23 C24 C25 . . . . -1.3(5) ? C21 C22 C25 C24 . . . . 1.9(4) ? C21 C22 C25 N3 . . . . -176.79(19) ? C23 C24 C25 C22 . . . . -0.5(5) ? C23 C24 C25 N3 . . . . 178.1(3) ? C28 N3 C25 C22 . . . . -49.6(4) ? C26 N3 C25 C22 . . . . 130.2(3) ? C28 N3 C25 C24 . . . . 131.7(3) ? C26 N3 C25 C24 . . . . -48.4(4) ? C28 N3 C26 C27 . . . . -0.7(4) ? C25 N3 C26 C27 . . . . 179.4(3) ? N3 C26 C27 N4 . . . . -0.5(5) ? C28 N4 C27 C26 . . . . 1.5(4) ? Cd1 N4 C27 C26 4_676 . . . -168.7(3) ? C27 N4 C28 N3 . . . . -2.0(3) ? Cd1 N4 C28 N3 4_676 . . . 167.41(17) ? C26 N3 C28 N4 . . . . 1.8(3) ? C25 N3 C28 N4 . . . . -178.4(2) ? _cod_database_fobs_code 2022682