#------------------------------------------------------------------------------
#$Date: 2022-10-07 03:48:09 +0200 (Fri, 07 Oct 2022) $
#$Revision: 278481 $
#$URL: svn://www.crystallography.net/cod/cif/2/02/26/2022680.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2022680
loop_
_publ_author_name
'Yoshiasa, Akira'
'Kitahara, Ginga'
'Tokuda, Makoto'
'Ishimaru, Satoko'
'Ono, Shin-ichiro'
'Terai, Kunihisa'
'Nakatsuka, Akihiko'
'Sugiyama, Kazumasa'
_publ_section_title
;
 Single-crystal structure refinements and Debye temperatures of Ir2S3
 kashinite and Rh2S3 bowieite
;
_journal_coeditor_code           EP3024
_journal_issue                   11
_journal_name_full
'Acta Crystallographica Section C Structural Chemistry'
_journal_paper_doi               10.1107/S2053229622009603
_journal_volume                  78
_journal_year                    2022
_chemical_formula_iupac          'Rh2 S3'
_chemical_formula_moiety         'Rh2 S3'
_chemical_formula_sum            'Rh2 S3'
_chemical_formula_weight         302.00
_chemical_name_systematic
;
Dirhodium trisulfide
;
_space_group_IT_number           60
_space_group_name_Hall           '-P 2n 2ab'
_space_group_name_H-M_alt        'P b c n'
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2n 2ab'
_symmetry_space_group_name_H-M   'P b c n'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   8.4672(3)
_cell_length_b                   5.98537(18)
_cell_length_c                   6.13921(19)
_cell_measurement_reflns_used    6842
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      45.0370
_cell_measurement_theta_min      4.8040
_cell_volume                     311.131(17)
_computing_cell_refinement
;
CrysAlis PRO (Rigaku OD, 2019)
;
_computing_data_collection
;
CrysAlis PRO (Rigaku OD, 2019)
;
_computing_data_reduction
;
CrysAlis PRO (Rigaku OD, 2019)
;
_computing_molecular_graphics
;
OLEX2 (Dolomanov <i>et al.</i>,  2009) and
<i>VESTA</i> (Momma & Izumi, 2011).
;
_computing_publication_material
;
WinGX (Farrugia, 2012)
;
_computing_structure_refinement
;
SHELXL2018 (Sheldrick, 2015)
;
_computing_structure_solution
;
SHELXS (Sheldrick, 2008)
;
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean 10.0000
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type
;
XtaLAB Synergy, single source at offset/far, HyPix6000
;
_diffrn_measurement_method       '\w scans'
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0460
_diffrn_reflns_av_sigmaI/netI    0.0174
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       11
_diffrn_reflns_limit_l_min       -11
_diffrn_reflns_number            14229
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         40.990
_diffrn_reflns_theta_min         4.170
_exptl_absorpt_coefficient_mu    12.343
_exptl_absorpt_correction_T_max  0.822
_exptl_absorpt_correction_T_min  0.777
_exptl_absorpt_correction_type   gaussian
_exptl_absorpt_process_details
;
(CrysAlis PRO; Rigaku OD, 2019)
;
_exptl_crystal_colour            silver
_exptl_crystal_density_diffrn    6.447
_exptl_crystal_description       block
_exptl_crystal_F_000             552
_exptl_crystal_size_max          0.029
_exptl_crystal_size_mid          0.024
_exptl_crystal_size_min          0.022
_refine_diff_density_max         1.109
_refine_diff_density_min         -2.751
_refine_ls_extinction_coef       0.0400(10)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_extinction_method
;
SHELXL2018 (Sheldrick, 2015)
;
_refine_ls_goodness_of_fit_ref   1.140
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     25
_refine_ls_number_reflns         1025
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.140
_refine_ls_R_factor_all          0.0210
_refine_ls_R_factor_gt           0.0176
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0278P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0440
_refine_ls_wR_factor_ref         0.0451
_reflns_number_gt                893
_reflns_number_total             1025
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            ep3024sup1.cif
_cod_data_source_block           II
_cod_original_cell_volume        311.131(16)
_cod_database_code               2022680
_shelx_hkl_file
;
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   5   0   2 132.019 6.79984   7
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   2  -1   4 22.6827 1.59113   9
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   4  -1   4 10.7138 1.61066   9
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   4   1   4 10.4943 2.15290  12
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   5  -1   4 49.7585 4.59713   7
   5   1   4 49.8852 3.85296   9
   5  -1   4 45.0869 3.16027  11
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   6  -1   4 4.63952 1.83027  12
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   6   1   4 5.44482 1.56212   9
   6  -1   4 2.35388 1.23614   9
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   6   1  -4 3.96253 1.40100   4
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   7   1  -4 166.011 8.69127   4
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   7  -1   4 174.481 10.0189   9
   7   1   4 176.901 9.88987   9
   7   1  -4 172.406 10.0129   9
   7  -1   4 177.654 8.85278   2
  -7  -1   4 183.784 9.04831   2
  -7  -1  -4 178.431 10.7294   5
   7  -1   4 156.048 7.84873  11
  -7   1  -4 180.295 10.8558  26
  -7   1   4 156.736 10.8984  18
   7   1   4 172.772 10.2413   7
  -7  -1  -4 170.232 10.4429  26
  -7  -1   4 157.321 10.5676  24
  -7  -1  -4 157.510 9.84133  17
   7  -1   4 180.840 10.4332   7
  -7  -1   4 183.557 9.85844  21
  -7  -1  -4 162.542 10.2389   6
  -8  -1  -4 18.6425 3.20627  26
  -8   1   4 12.2676 1.61126  26
  -8  -1   4 13.7649 1.90831   2
  -8   1  -4 16.4053 3.22421  17
  -8   1  -4 15.2039 3.05162  26
  -8  -1   4 12.9624 2.48093  21
  -8  -1  -4 13.3482 2.77468  17
  -8   1  -4 10.2126 2.24163   5
  -8  -1  -4 8.17899 2.45235   5
   8  -1   4 18.5568 2.25616   2
   8  -1   4 11.9275 1.68367  11
   8   1   4 9.74797 2.49177   9
   8   1  -4 7.52768 2.26372   9
  -8   1  -4 10.9292 1.83671   4
   8  -1  -4 19.1725 3.33468   9
  -8  -1   4 11.5422 2.14664  20
  -8   1   4 16.5309 3.26814  21
   8   1   4 12.3403 2.69191   7
   8   1  -4 17.4204 2.19333   4
   8  -1   4 10.0591 2.45806   9
  -8  -1   4 11.4133 2.90242  24
  -9  -1   4 0.93618 1.64701  18
  -9  -1   4 1.10018 1.29842  21
   9   1   4-0.75431 1.57018   9
   9  -1   4 0.77545 1.49446   9
  -9   1  -4 0.90170 1.73773  26
   9   1  -4-1.58681 1.52905   9
  -9  -1   4 0.48383 1.14205  20
  -9  -1   4-0.52054 1.22867  22
  -9  -1  -4 0.66934 1.39332  17
  -9  -1  -4 0.80801 1.79808   5
   9   1   4 0.67673 1.59729   7
  -9   1  -4-0.58398 1.02744   5
  -9   1  -4-0.83878 1.86654  17
  -9  -1   4-1.83284 1.76611  14
  -9   1   4 1.58897 1.65380  21
   9  -1  -4-2.46298 1.82696   9
  -9   1   4-0.29296 0.89279  26
  -9  -1  -4-0.87910 1.54660  26
  10   1   4-0.86038 1.65807   9
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  10   1   4 0.69081 1.33131   7
  10  -1  -4 7.46544 3.59669   9
 -10   1   4-0.86452 1.79953  14
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 -10  -1  -4 2.08609 1.89513  17
 -10  -1   4-0.51706 1.28644  22
 -10  -1   4 1.07311 1.57949  20
 -10   1   4-1.09814 2.11625  18
  10  -1   4 0.88129 1.96111   9
 -10  -1   4-0.99039 1.74233  14
 -10   1   4 0.34055 1.07173  26
 -10   1  -4 0.88749 1.97490  17
 -10   1  -4 2.00854 1.93536  26
  11   1  -4 1.01125 1.94893   9
 -11  -1   4 1.09674 1.72585  18
 -11   1   4 7.27824 2.77222  14
  11   1   4 1.37956 1.62820   7
 -11   1  -4 3.96220 1.94407   5
 -11  -1   4 0.58372 1.52328  20
  11   1   4-0.96510 1.86000   9
  11  -1  -4-1.04498 2.17526   9
 -11   1  -4 0.92339 1.77963  17
 -11  -1  -4 1.08073 1.70067  26
 -11  -1   4-1.06391 1.87177  14
  11  -1   4 0.98728 1.90273   9
 -11  -1  -4 0.92431 1.78140   5
 -11  -1  -4 0.70657 1.47093  17
 -11   1  -4 3.30970 2.29651  26
 -11   1   4-1.19397 1.87883  18
 -12   1  -4 7.48485 2.40085   5
 -12   1   4 3.83047 2.25343  18
 -12  -1  -4 3.50626 1.91965  17
  12   1  -4 8.90239 3.03812   9
 -12  -1  -4 7.73571 2.95188   5
 -12  -1  -4 5.86522 2.77451  26
 -12  -1   4 7.91153 2.81764  14
  12  -1  -4 3.43372 2.38927   9
 -12   1  -4 4.76242 2.48482  26
 -12   1  -4 9.40286 3.05544  17
  12  -1   4 2.16689 2.26241   9
 -12  -1   4 9.27170 3.41641  18
  12   1   4 2.12813 2.51790   9
 -12   1   4 3.79146 2.79606  14
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  13   1   4 67.7082 7.83433   9
  13  -1   4 59.1785 7.42649   9
  13  -1  -4 52.7528 7.13404   9
  13   1  -4 51.5079 7.04345   9
 -13   1   4 58.7440 7.78350  18
 -13   1   4 63.0865 6.97337  14
 -13  -1  -4 63.1964 6.95502   5
 -13   1  -4 69.2148 8.12842  26
 -13  -1  -4 54.9358 7.57519  26
 -13  -1   4 53.8151 7.07541  14
 -13  -1   4 63.5916 7.54246  18
 -14   1  -4 6.18916 2.60324  17
  14  -1   4 4.53925 3.14993  12
 -14  -1   4 2.34913 2.26411  14
 -14   1   4 2.87737 2.61445  14
 -14  -1  -4 2.93533 2.66709   5
 -14   1   4 1.24481 3.09737   8
  14   1  -4 2.50831 3.12062   9
 -14   1   4 4.06841 3.84720  18
  14   1   4 3.60908 3.13950   9
 -14  -1   4-1.18317 2.28068   5
  14  -1  -4 3.83093 2.84204   9
 -14  -1   4-1.20091 2.31485  18
  14  -1   4-1.20857 3.29417   9
 -15   1   4 0.96064 2.26970   5
 -15  -1   4-1.16560 2.59581   5
 -15  -1   4 4.57547 2.98652  14
 -15   1   4 8.34404 3.51045   8
  15   1  -4 1.26884 3.86759   9
 -15  -1  -4 4.65664 2.64388   5
 -15  -1   4 4.62237 2.72943  18
  15  -1   4 1.21570 3.17386   9
  15  -1  -4 3.85352 3.91531   9
  15   1   4 4.86962 3.17829   9
  15  -1   4 4.51764 3.74790  12
   0  -1   5-1.72424 1.42991  12
   0  -1   5 1.88295 1.17114   7
   0  -1   5 0.57569 1.35874  24
   0   1   5 0.44679 1.11155  12
   0  -1  -5 1.86706 1.10167  10
   0  -1  -5 0.56721 0.99784   4
   0   1   5 0.51507 1.14616  24
   0   1  -5-0.48652 1.08261  17
   0   1  -5 0.33080 0.48689  26
   0   1  -5-0.32679 0.81303  10
   1   1   5 650.353 27.4383  24
   1   1   5 704.430 27.6979  12
  -1  -1   5 672.500 28.2659  24
  -1   1  -5 707.386 28.0262  17
   1   1  -5 659.622 27.3318  17
  -1  -1   5 682.102 27.1224   7
  -1   1   5 690.034 28.2242  24
   1  -1  -5 679.183 27.4717  10
  -1  -1  -5 670.763 27.5164  10
   1   1  -5 660.640 26.3154  10
   1  -1  -5 648.126 27.9948   4
   1  -1   5 672.211 27.7261   7
   1   1  -5 662.469 24.1462  26
   1  -1   5 718.927 28.5170  24
   1  -1   5 720.191 28.7120  12
  -1   1  -5 656.492 25.5128  26
  -2   1   5 742.187 29.8822  25
   2  -1   5 772.018 30.8259  12
   2   1   5 724.387 29.2175  24
   2   1  -5 758.094 28.4664  10
  -2  -1  -5 735.730 30.1309   4
   2   1   5 738.365 25.8486   9
  -2   1   5 744.472 30.3974  24
   2   1  -5 689.161 25.9497   9
  -2   1  -5 723.181 30.0221  17
   2  -1  -5 755.817 30.2238   4
  -2   1   5 715.391 28.8655  13
  -2  -1   5 756.566 30.2732  13
  -2   1  -5 732.822 28.0368  26
  -2  -1  -5 712.421 27.7663  26
   2  -1  -5 718.020 29.3712  10
  -2   1  -5 699.492 27.1047   6
  -2  -1   5 739.800 28.6801   7
   2   1   5 735.378 29.7944  12
  -2  -1   5 732.660 30.4051  24
   3   1   5 246.076 11.7683  24
  -3   1  -5 219.789 11.1005  26
   3   1   5 242.178 9.63877   9
  -3   1   5 243.154 12.4597  25
   3  -1  -5 235.977 12.0370  10
  -3  -1  -5 254.985 12.6946   4
   3   1  -5 232.083 9.72325   9
  -3   1  -5 234.052 12.5640  17
  -3  -1   5 222.811 11.0415  25
  -3   1   5 237.653 13.0718  24
  -3   1  -5 240.422 10.3620   6
   3  -1  -5 219.947 12.1618   4
   3  -1   5 247.905 12.7870   7
  -3  -1  -5 227.240 11.0260  26
   3  -1  -5 228.193 9.77495   9
  -3   1   5 228.986 11.6143  13
  -3  -1   5 263.203 13.0316  13
   3  -1   5 248.882 13.3146  12
   3   1   5 232.515 12.4665  12
   3  -1   5 236.200 9.50472   9
   4   1   5 16.4296 3.03728  12
  -4   1  -5 22.5234 2.86731  26
  -4   1   5 16.4257 2.87832  25
   4  -1   5 21.3769 2.10696   9
  -4   1   5 21.1495 3.35666  24
  -4   1  -5 18.4599 3.09039  17
   4   1  -5 16.8689 2.05097   9
  -4  -1  -5 16.4576 2.78909   4
   4  -1   5 22.8567 3.22237   7
  -4   1  -5 14.5416 1.98221   6
  -4  -1   5 17.3881 3.02183  13
  -4  -1   5 13.9971 2.19116  25
   4  -1  -5 18.2691 2.07049   9
   4   1   5 19.3917 2.01892   9
   4  -1   5 24.9632 3.61697  12
  -4  -1  -5 18.7345 2.66766   6
  -4   1   5 20.4446 2.85947  13
  -4  -1  -5 17.1385 2.87886  17
  -4  -1  -5 16.2892 2.44524  26
   4   1   5 21.0447 2.70262  24
   4  -1  -5 17.0246 2.77198   4
  -4   1   5 18.2885 3.03427  21
   5   1  -5 1021.36 41.1350   4
   5   1  -5 997.947 39.5738   9
   5  -1   5 1073.23 39.5563   9
   5   1   5 1050.86 42.8404  12
  -5   1   5 1071.80 42.7433  21
   5  -1   5 1043.24 42.2212   7
   5   1   5 1019.17 39.3831   9
  -5  -1  -5 1057.32 42.0578  17
  -5   1  -5 1093.26 41.6166  26
  -5  -1   5 1106.10 43.2782  24
   5  -1   5 1069.54 43.4702  12
  -5  -1  -5 1054.06 41.2790   6
   5  -1  -5 1035.24 39.8226   9
  -5  -1   5 1024.75 41.6756  21
  -5   1   5 1050.46 41.1818  13
  -5  -1   5 1059.15 42.6930  13
  -5  -1  -5 1071.34 41.3692  26
  -5   1   5 1118.40 43.7776  24
  -5   1  -5 979.448 41.0468   4
   5   1   5 1057.40 40.3192  24
   6   1  -5 304.393 14.6676   4
   6   1   5 294.445 15.6903   7
   6   1   5 308.302 13.9083   9
  -6  -1   5 304.479 16.4933  24
  -6  -1   5 293.591 15.0806  21
   6   1  -5 297.549 14.0468   9
   6  -1   5 295.434 13.8932   9
  -6  -1  -5 305.447 15.3388  26
   6  -1   5 308.873 16.9223  12
  -6   1   5 303.675 16.1545  21
   6  -1  -5 269.370 13.8725   9
   6  -1   5 299.782 15.7425   7
  -6   1   5 316.522 11.9096   7
  -6   1  -5 294.787 14.5552   4
  -6  -1   5 303.379 12.1689  19
   6   1   5 304.872 16.5477  12
  -6  -1   5 295.327 16.0203  13
  -6  -1  -5 296.326 15.5908  17
  -6   1  -5 310.740 15.5906  26
  -6  -1  -5 281.468 14.9165   6
  -6   1  -5 307.465 16.2587  17
  -7  -1   5 14.2405 2.83764  21
   7  -1   5 20.4014 2.81689   2
  -7  -1   5 15.2279 2.63212   2
   7  -1   5 13.6770 3.03412   7
  -7   1  -5 19.6015 3.39553  26
  -7   1  -5 16.7002 3.32584  17
  -7   1   5 19.5948 3.55666  21
   7   1  -5 19.4998 3.01826   9
  -7  -1   5 13.3511 3.09659  24
  -7  -1  -5 17.0441 3.07868   6
   7   1  -5 10.4321 2.20328   4
   7   1   5 13.5251 3.05909   7
   7   1   5 13.5232 2.44239   9
   7  -1   5 14.4591 2.64902   9
  -7  -1  -5 16.6834 3.27009  17
  -7  -1  -5 20.4065 3.38379  26
   7  -1  -5 13.9327 2.71375   9
  -7   1  -5 15.4331 2.54886   4
   7   1   5 10.1914 2.87083  12
  -7  -1   5 13.3767 1.94997  20
   7  -1   5 13.8111 3.33388  12
  -8  -1  -5 37.2780 4.75604  17
   8  -1   5 54.0724 5.10917   9
  -8   1   5 48.3353 5.66305  21
   8  -1   5 38.0017 5.63432  12
  -8  -1   5 41.2680 4.08270   2
  -8  -1  -5 33.9807 4.79233  26
   8   1  -5 46.8487 4.21859   4
   8   1   5 47.9584 5.41661   7
   8  -1  -5 52.1400 5.30990   9
   8   1  -5 39.5181 4.53302   9
  -8   1  -5 55.4505 6.05970  17
   8   1   5 40.1032 4.49769   9
  -8  -1   5 42.1866 5.86702  24
   8  -1   5 51.8839 4.37006   2
  -8  -1   5 47.8194 4.99466  21
  -8   1  -5 64.9227 6.43448  26
  -8   1  -5 53.8802 4.51603   4
  -8   1   5 51.4358 6.14939  18
  -8  -1   5 42.9800 3.71454  20
  -9   1  -5 607.888 28.1264  26
  -9  -1   5 569.228 23.6157   2
  -9  -1   5 591.915 25.2009  22
   9   1  -5 566.684 26.2157   9
  -9  -1   5 565.107 25.5781  21
  -9   1   5 552.437 27.0162  21
   9   1   5 533.376 26.2360   7
  -9  -1  -5 616.156 26.9614  17
   9  -1  -5 627.236 26.9964   9
  -9  -1   5 587.512 28.4040  14
   9   1   5 566.166 25.8914   9
  -9   1  -5 605.972 27.8823  17
   9  -1   5 551.425 25.8988   9
   9  -1   5 651.095 30.1211  12
  -9  -1  -5 612.897 27.4349   5
  -9  -1   5 562.212 27.8820  24
  -9  -1  -5 566.972 27.4871  26
 -10  -1  -5 26.8387 4.40802   5
  10   1   5 28.1559 4.27538   7
  10  -1   5 40.9258 5.09109   9
 -10  -1   5 23.1438 4.76208  14
 -10  -1   5 19.4286 4.31988  18
 -10   1  -5 31.7595 4.96525  17
 -10  -1  -5 28.8706 4.82176  26
 -10   1   5 22.2085 4.22325  21
  10  -1   5 32.3270 5.65012  12
  10  -1  -5 26.0279 4.39586   9
 -10   1  -5 16.8505 3.91057  26
  10   1  -5 25.0951 4.29983   9
 -10  -1  -5 28.5317 4.30843  17
  10   1   5 28.4941 4.25509   9
 -10  -1   5 26.9200 3.52846  22
 -10  -1   5 32.8391 4.11042  21
 -11  -1  -5 111.777 8.75521  17
 -11   1  -5 83.7346 8.36056  17
 -11   1  -5 108.772 9.87373  26
  11   1   5 113.639 9.14864   9
  11   1   5 102.550 8.43202   7
  11   1  -5 102.323 9.04079   9
 -11  -1   5 95.7665 9.65110  18
 -11  -1  -5 101.311 8.90889   5
 -11  -1   5 120.941 10.4174  14
 -11   1   5 116.811 9.71259  14
  11  -1  -5 110.438 9.34020   9
 -11  -1  -5 99.1646 9.41039  26
 -11   1   5 104.124 10.2045  18
  11  -1   5 93.6376 8.61876   9
 -12   1   5 66.8377 7.51663  14
 -12  -1  -5 74.8997 6.93920  17
 -12  -1   5 57.9268 7.46161  14
  12  -1   5 79.3554 7.79608   9
  12   1   5 70.3548 7.54020   9
 -12  -1  -5 49.5732 6.97344  26
 -12  -1   5 75.7848 8.62076  18
  12  -1  -5 63.6207 7.40638   9
 -12   1  -5 56.2010 7.29648  26
  12   1  -5 69.3456 7.64803   9
 -12   1   5 69.1926 8.50964  18
 -12   1  -5 58.5014 7.12983  17
 -13   1   5 251.998 18.0299  18
  13   1  -5 242.050 16.5365   9
 -13   1  -5 267.228 16.3409  17
  13  -1   5 270.456 16.9084   9
 -13  -1   5 292.366 18.3953  18
  13  -1  -5 275.529 17.3539   9
 -13  -1   5 276.782 17.8519  14
 -13   1   5 298.737 17.3154  14
 -13  -1  -5 268.184 17.7742  26
 -13   1  -5 308.502 18.7474  26
  13   1   5 269.416 16.7785   9
 -14   1  -5 9.06407 3.82240  26
  14  -1   5 8.68178 3.92296   9
  14   1   5 7.58636 3.42251   9
 -14  -1   5 9.78064 3.73617  14
 -14   1   5 9.79910 3.66387  18
 -14  -1   5 3.81666 2.46830  18
 -14   1   5 11.3064 3.97188  14
  14  -1  -5 8.16656 3.44614   9
  14   1   5 9.29349 4.05169  12
  14   1  -5 9.18567 3.62464   9
 -14   1  -5 9.36089 3.22284  17
  15  -1   5 202.087 16.2795  12
  15   1   5 211.780 16.6822  12
 -15   1   5 225.046 14.4436   5
  15  -1  -5 222.060 15.3308   9
 -15   1   5 194.662 14.7630   8
 -15  -1   5 233.360 15.4370  14
  15   1  -5 207.093 14.8012   9
 -15   1  -5 205.931 15.2190  26
 -15  -1   5 243.909 15.7732   5
 -15  -1   5 215.365 15.2054  18
 -15   1   5 191.450 15.2760  18
   0   1  -6-0.41538 0.86469  10
   0  -1  -6-0.57370 1.19422  10
   0  -1   6 0.58822 1.03486   7
   0   1  -6-1.24035 1.29095  17
   0   1  -6-0.15357 0.52676  26
   0  -1   6 0.72306 1.50509  24
   0  -1  -6 0.71903 1.13143   4
   0   1   6-0.65721 1.63510  24
   0   1   6 1.13579 1.73042  12
   0  -1   6-1.43014 1.25800  12
  -1  -1   6 3.24562 1.28573   7
   1   1  -6 4.24120 1.46235  10
  -1   1  -6 6.54203 1.99915  17
  -1  -1   6 2.22093 1.54843  24
   1  -1  -6 4.04918 1.64787  10
   1   1   6 5.39071 1.76972  12
   1  -1   6 6.98459 2.06529   7
   1   1   6 3.73682 1.70413  24
   1  -1   6 7.32236 2.30932  12
  -1   1   6 2.80653 1.56867  24
  -1   1  -6 3.46873 1.04259  26
   1  -1   6 7.09570 2.16741  24
   1  -1  -6 8.59386 2.32803   4
   2   1  -6 50.9785 4.24576  10
  -2   1  -6 44.3395 4.82925  17
  -2   1   6 47.8797 4.93866  25
   2  -1   6 52.1150 5.29111  24
   2  -1  -6 46.9777 5.00873   4
   2   1   6 61.1667 5.40849  12
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   7   1  -9 10.0523 3.36501   4
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   8   1   9 6.47852 3.22471  12
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   2   1  10 9.08919 3.34616  24
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   7   1  10 39.6466 6.35018  12
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   7  -1  10 58.3739 7.90852  12
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   8   1  10 1.25528 2.42120  12
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   1  -2   6 372.223 19.6775  12
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   2   2   6 49.8010 4.65471  24
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   3   2   6 894.893 34.3041  24
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   3   2   6 862.696 35.0845  12
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   4  -2   6 35.1136 4.44191   2
   4   2   6 36.4165 4.41602  12
   4  -2   6 31.9783 4.70964  12
   4   2  -6 36.3371 2.89705   9
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   5  -2  -6 23.1412 2.70016   9
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   5   2  -6 20.9227 2.51595   9
   5   2   6 21.0669 2.41067   9
   5   2   6 16.6976 2.60512  24
   5  -2  -6 22.8722 3.80401  10
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   5  -2   6 22.9515 3.65324   2
   5  -2   6 20.5642 3.93042  12
   5   2   6 25.4665 4.08440  12
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   6   2   6-0.88522 1.39319  12
   6   2  -6 0.43957 1.14736   9
   6   2   6 0.81820 1.06788   9
   6   2  -6 2.10336 1.65506   4
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   6  -2   6 1.39080 1.44779   2
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   7   2  -6 805.797 33.1200   9
   7  -2   6 819.254 37.9371  12
   7   2   6 883.763 33.2098   9
  -7  -2   6 819.686 34.6273  21
  -7   2   6 822.539 37.0235  21
   7   2   6 832.728 36.8268  12
   7   2   6 829.561 36.4212   7
   7  -2   6 839.957 32.9778   9
   7  -2  -6 787.531 33.2435   9
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  11  -2  -8 387.987 21.5728  10
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  11   2   8 356.683 21.6566  12
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  11   2  -8 354.699 18.6532  10
  11  -2   8 343.200 22.3986  12
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  11   2   8 316.873 19.8775   7
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   0   2   9 1.01329 1.95273   7
   0   2   9-0.77414 1.92599  13
   0   2   9 1.09757 2.28463  24
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   1   2   9 39.2896 5.95382  25
   1  -2   9 43.5033 6.42756   2
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   2   2  -9 11.2431 3.55485   4
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   2   2   9 4.83221 2.29843  24
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   3   2   9 4.60917 2.29975  12
   3   2   9 1.80151 2.24746  24
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  -3   2   9 7.72975 2.28179   7
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   4  -2  -9 11.6256 3.34083  10
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   4   2  -9 13.1453 3.65488   4
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   5  -2   9 44.9921 6.31380   2
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   5  -2   9 41.3800 6.77104  12
   5   2   9 44.2229 5.97188  12
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   6  -2   9 1.15327 2.40056  24
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   6   2  -9 3.93643 2.36534  10
   6  -2  -9 1.12325 2.16463  10
   6   2   9 1.08372 2.08845  12
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   6  -2   9 9.64928 3.95635   2
   6   2  -9-1.09629 2.72745   4
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   6   2   9 1.29555 2.03853   7
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  -6   2   9 1.48209 2.60729  24
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   7  -2  -9 9.23304 3.74763  10
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   7   2  -9 6.13265 2.90432   4
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   7   2   9 5.68985 3.69527  12
   7  -2   9 7.01133 2.73504   2
   7   2   9 1.31253 2.53509   7
   7  -2   9 1.12919 2.35656  24
   7   2  -9 6.20837 2.55119  10
   7  -2   9 1.45919 3.25148  12
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   8  -2   9 1.48858 3.31288  12
   8  -2  -9 2.36060 2.45741  10
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   8   2   9-1.31096 2.52694   7
  -8  -2   9 3.84880 2.72994   2
   8   2   9 2.37233 2.80013  12
   8  -2   9 3.28033 2.43377  24
  -8   2   9 5.55977 3.28101  18
  -8  -2   9 2.08534 2.32082  21
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   9   2   9 15.4697 4.34130   7
  -9   2   9 17.8113 5.20143  21
   9  -2  -9 19.0780 4.43753  10
  -9   2   9 9.95584 3.91867  18
  -9   2  -9 19.3044 4.76354  17
   9   2   9 18.3327 4.54661  12
   9  -2   9 12.0221 4.30149  12
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  10  -2  -9 11.8825 4.08671  10
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  10   2   9 6.20027 3.39382  12
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  10   2   9 12.4312 4.16096   7
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  11   2   9 11.1093 4.16481  12
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   0   2 -10 103.926 10.8058   4
   0   2  10 111.742 10.3513  24
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   0   2  10 112.354 10.0560   7
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   1   2 -10 207.783 15.2855   4
   1   2  10 179.816 13.3563  24
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   2   2  10 2.44749 2.54725   7
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   2   2 -10 1.37488 2.41869   4
   2  -2  10 1.31885 2.54156  24
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   2  -2  10-1.35196 2.37838   2
   2   2  10 1.31726 2.74190  25
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   3   2 -10 333.257 20.7431   4
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   3   2  10 348.211 20.5693   7
  -3   2  10 283.340 19.0355  25
  -3   2  10 341.701 21.2961  24
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   4  -2 -10 193.554 13.8380  10
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   4  -2  10 178.040 14.2669   2
   4   2 -10 230.145 15.8225   4
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   4  -2  10 206.756 15.6431  12
   4   2  10 168.482 14.0897   7
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   4   2  10 197.226 13.5281  12
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   5  -2  10 23.2554 5.23739  24
   5   2  10 12.4835 3.54922  12
   5   2 -10 28.5945 5.40744   4
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   5  -2  10 17.3512 4.74753  12
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   6  -2  10 81.0308 8.59241   2
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   6   2 -10 89.7692 9.09003   4
   6  -2  10 76.1103 9.37018  12
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   6   2  10 59.1896 7.21638  12
   7  -2  10 289.377 18.5393  24
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  -7  -2  10 275.500 18.3366  21
   7  -2 -10 298.335 18.6316  10
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  -7  -2  10 346.185 19.4206   2
   7  -2  10 327.873 18.5894   2
   7   2 -10 327.159 18.8760   4
  -7   2 -10 317.792 18.6240   4
   7   2  10 322.203 18.9036  12
   7   2  10 305.479 19.9269   7
  -7   2 -10 330.895 20.6768  17
   7  -2  10 355.203 21.5945  12
  -7  -2  10 350.308 21.8866  24
   8   2  10 11.2574 3.58020  12
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   8   2  10 10.6743 4.09837   7
   8  -2 -10 14.9404 3.97496  10
  -8   2  10 10.9347 4.33236  18
  -8  -2  10 21.4469 4.57257  21
  -8  -2  10 18.6216 4.25487   2
   8  -2  10 10.3052 4.20790  12
   9   2  10 19.1968 4.56105  12
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   9  -2 -10 11.3067 3.81123  10
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   9   2  10 14.1706 4.78339   7
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   9  -2  10 17.3808 4.99537  12
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   0   2  11 10.4907 3.74936  21
   0   2  11 16.5008 3.98558   7
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   1   2 -11 8.77366 3.64185   4
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   1   2  11 1.33421 2.78224  25
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   2   2  11 8.10999 3.69856  25
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   2   2  11 7.17189 3.40155  21
   2  -2  11 14.1470 4.32329   2
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   3   2  11 3.87818 3.05117   7
   3   2  11-1.38896 2.67674  21
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   3  -2  11 2.73629 2.40691   2
   3  -2  11 1.31758 2.53918  24
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   3   2  11-1.36305 3.21714  25
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   4   2  11 26.6274 5.41739  21
   4   2  11 29.1329 5.77789   7
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   4   2 -11 17.3250 4.77585   4
  -4   2 -11 13.4946 4.59470   4
   4  -2  11 30.4649 5.54458  24
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   4  -2  11 20.9471 4.80637   2
   4   2  11 17.8182 4.90698  25
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   5  -2  11 6.04947 3.01460  24
   5   2  11 3.77742 2.97643  21
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   5  -2 -11 2.17258 2.42288  10
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   5   2 -11 10.0507 3.83166   4
  -5   2 -11 3.80883 2.64786   4
  -5  -2  11 7.75860 3.81008  13
   5   2  11 2.68302 2.59050   7
  -5   2  11 6.04257 2.85713  18
  -5  -2  11 7.71529 3.35933   2
   5  -2  11 3.69778 3.22046   2
  -5   2  11 8.98832 3.73064  24
   6   2  11 7.01865 3.05787  21
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  -6   2  11 4.41277 3.27833  21
  -6   2  11 11.1772 3.52766  18
   6  -2  11 6.86527 2.99129  24
   6  -2  11 2.27278 2.53544   2
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   6  -2 -11 8.63179 3.29282  10
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   0   2  12 298.378 19.8472  21
   0   2  12 297.961 18.9196  25
   0  -2  12 277.564 19.5335   2
   0   2 -12 303.131 19.8192   4
   0  -2  12 287.919 18.8847  13
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  -1   2  12 48.6750 7.48134  21
   1   2 -12 55.4618 7.81237   4
   1  -2  12 48.9911 7.34089  24
   1   2  12 52.7961 7.67488  21
  -1  -2  12 49.9283 7.56423  13
   1  -2  12 55.6623 7.77793  13
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   0   3   0 1.03544 1.01601   3
   0  -3   0-0.15436 0.54310   5
   0   3   0-0.98060 1.02864  16
   0  -3   0 0.12361 0.44567  13
   0   3   0-0.21703 0.63889   8
   0  -3   0 0.13244 0.48874  10
   1   3   0 129.740 7.16436   3
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   1  -3   0 140.909 6.26093  22
  -1  -3   0 131.883 6.81192  19
   1  -3   0 126.093 5.46519   5
   1   3   0 133.759 5.99960  25
   1   3   0 133.318 7.11199  16
  -1   3   0 148.278 6.95700   8
  -1  -3   0 143.899 6.13687  13
   1  -3   0 134.829 5.85829  10
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  -2  -3   0-0.27035 0.79584   5
   2   3   0-0.34852 0.77554   3
   2  -3   0 0.14845 0.48156  22
  -2   3   0-0.10427 0.27518   5
  -2   3   0-0.68289 1.07452   3
   2  -3   0 0.84377 0.57490  12
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   2  -3   0 0.36407 0.94998   9
  -2   3   0-0.33771 0.88119  16
   2   3   0-0.97694 0.92375  16
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   1  -3  -1 108.793 5.50674  10
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   3   3  -4 77.3843 6.21234   3
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  11   3  -4 32.1448 5.23322   9
  11   3   4 25.0338 4.61076   9
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  11   3   4 21.3096 3.47563   7
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   0   3   5 0.67543 1.30171  25
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   1   3   5 1011.22 37.6465  12
   1  -3  -5 1039.60 40.0248  10
   1   3  -5 947.462 40.6621   3
  -1   3   5 980.455 36.8448  13
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  -1   3   5 1026.59 39.7982  24
   1   3   5 999.700 38.6027  24
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   2   3   5 83.5874 6.33408  21
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   2   3  -5 73.4824 4.14984  10
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   2  -3   5 81.9389 6.62539   2
   2   3  -5 67.7382 5.07323  17
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   2   3  -5 92.8743 7.21154   3
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   2   3   5 110.890 6.08540  12
   2  -3  -5 78.4444 6.20052  10
   2   3   5 74.0889 5.23109  24
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   3   3  -5 126.821 6.34974  10
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   3  -3   5 118.715 8.52064   2
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   3   3  -5 128.175 9.03916   3
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   3   3   5 132.956 7.86890  12
   3  -3  -5 123.736 8.54200  10
   3   3   5 125.298 6.99894  24
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   4   3   5 185.448 11.0724  12
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   4   3  -5 219.213 12.5395   3
   4   3   5 215.740 9.75926  24
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   5  -3   5 609.968 24.7849   9
  -5   3   5 586.013 22.2174  26
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   5  -3   5 570.441 25.9710   2
  -5   3  -5 629.020 27.6941  17
   5  -3  -5 622.333 25.1900   9
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   5   3  -5 622.561 26.8887   3
  -5  -3   5 615.033 27.9071  13
  -5   3  -5 618.952 26.4471  26
   5  -3   5 586.064 27.5464  12
   5   3   5 602.953 26.2026  12
  -6  -3   5 83.8666 7.08455  24
   6  -3   5 57.0867 5.04578  11
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  -6  -3   5 49.8044 4.82697  21
   6  -3  -5 65.4768 5.56996   9
  -6   3   5 68.4382 6.89879  18
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   6  -3   5 61.2079 5.60167   2
   6  -3   5 59.3888 5.19046   9
  -6   3   5 68.2241 6.89714  21
  -6   3  -5 62.9742 5.88035   3
   6   3  -5 62.3519 5.83585   3
  -6  -3   5 53.0489 6.28933  13
  -6   3  -5 65.2828 6.21216  26
  -6  -3   5 61.8203 4.81385  19
   6  -3   5 72.2025 7.10752  12
  -6  -3  -5 55.9233 5.99304   6
  -7  -3   5 22.0279 3.83870  24
   7  -3   5 20.6676 4.12829  12
   7  -3   5 24.4459 3.31768  11
  -7   3   5 21.6065 4.26727  21
  -7  -3   5 18.4048 2.59438  19
  -7   3   5 22.4330 4.26416  18
   7  -3   5 16.5573 2.92420   9
   7  -3  -5 18.6213 3.37812   9
  -7  -3  -5 30.4796 4.44566  23
  -7   3   5 18.9464 2.51091  16
  -7  -3  -5 19.1481 3.63022   6
  -7  -3   5 22.2624 3.03867  21
  -7   3  -5 22.9579 3.90977  26
   8  -3   5 344.169 16.8827  11
   8  -3   5 406.490 18.9624   9
  -8  -3   5 377.068 16.8288  21
   8  -3  -5 361.535 18.7620   9
  -8   3   5 377.442 20.8827  18
  -8   3  -5 379.359 19.9798  26
  -8  -3  -5 368.195 20.1974   5
  -8  -3   5 343.678 20.2103  14
  -8   3   5 362.173 20.5917  21
   8  -3   5 393.621 21.2557  12
  -8  -3  -5 387.491 20.1653   6
  -8  -3   5 372.929 19.5043  24
  -9  -3   5 643.645 29.9693  24
  -9   3   5 691.047 31.9733  21
  -9  -3  -5 619.604 30.8060   5
  -9  -3   5 651.613 28.1538  20
   9  -3   5 671.555 29.5623   9
   9  -3  -5 690.080 30.1531   9
  -9   3   5 660.616 32.0932  18
   9   3  -5 626.619 29.2680   9
  -9   3  -5 636.488 31.2455  17
  -9  -3   5 669.724 29.7169  22
  -9   3  -5 646.474 26.8921   4
   9  -3   5 662.553 32.0893  12
  -9  -3   5 621.837 31.2424  14
   9   3   5 623.338 29.6430   7
   9   3   5 653.940 29.2404   9
  -9   3  -5 683.122 31.3013  26
  -9  -3  -5 642.052 30.7912   6
  10  -3   5 42.6731 6.31307  12
 -10   3   5 44.6360 6.54476  18
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  10  -3   5 29.1803 4.81420   9
  10  -3  -5 30.4299 5.04142   9
 -10  -3  -5 25.2599 5.02226   5
 -10   3  -5 29.5311 5.56094  17
  10   3  -5 37.8759 5.48488   9
  10   3   5 38.2324 5.14925   9
 -10  -3   5 46.5964 6.66114  14
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  10   3   5 39.0248 5.32345   7
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  11  -3   5 149.397 11.4871   9
  11  -3  -5 158.834 12.1671   9
  11  -3   5 169.267 13.6154  12
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  11   3  -5 162.053 11.7989   9
  11   3   5 145.127 11.3209   9
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  11   3   5 157.822 11.1417   7
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  12  -3   5 254.652 16.4669   9
  12  -3  -5 288.550 17.6388   9
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  12   3  -5 266.833 16.8647   9
  12   3   5 257.112 16.4491   9
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  12  -3   5 278.561 18.8019  12
  13  -3   5 120.950 10.3042   9
  13  -3  -5 106.314 10.1531   9
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  13   3   5 109.287 9.77337   9
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  13  -3   5 108.811 11.4870  12
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  14  -3   5 12.6728 4.43771  12
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   1   3   6 35.7394 4.47311  21
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   1   3   6 24.2827 3.04606  12
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   2   3  -6 15.9963 3.34905   3
   2   3  -6 21.8710 2.17343  10
   2   3   6 14.5200 2.52158  12
   2   3   6 28.1017 3.35419  24
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   6   3  -6 1.99847 1.58444   9
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   7  -3   6 28.4992 3.68369   9
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   7   3   6 22.1849 4.16202  12
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   7  -3   6 21.6466 3.58477   2
  -7   3   6 27.5561 5.04046  21
  -7   3   6 35.3117 5.47580  18
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   7   3  -6 25.7291 3.48487   9
   7   3   6 31.1952 3.81631   9
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   7  -3  -6 37.2781 4.20144   9
   8  -3   6 12.4464 4.15994  12
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   8   3   6 7.17063 3.02305  12
   8  -3   6 6.98173 2.24337   9
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   8   3  -6 4.69525 2.24907   9
   8   3   6 7.65596 2.19834   9
   8   3  -6 3.34794 1.83737   4
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   8   3   6 5.03299 2.75166   7
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   9   3   6 1.12665 2.17128  12
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   9  -3   6 3.96869 2.54946  12
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   9   3  -6-0.75455 1.67920   9
   9   3   6 0.71666 1.69162   9
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   9   3   6 4.08118 2.53847   7
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  11   3   6 0.98918 1.90627   7
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  12  -3   6 7.33223 3.82709  12
  12   3   6 1.37420 2.86132  12
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  13   3   6 12.6250 4.56624  12
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  14   3   6 5.53251 3.07947  12
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  14  -3   6 1.39718 2.91003  12
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 -14   3   6 2.78647 2.90183   8
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  -1   3  -7 630.809 25.6476  26
  -1   3   7 639.471 30.4027  21
   1   3   7 701.913 30.5765  21
   1  -3   7 667.717 30.3455   2
   1   3  -7 621.960 28.1122  17
   1   3   7 603.987 29.7608  25
   1  -3   7 655.374 30.6083  24
  -1   3   7 600.422 26.0306  13
  -1  -3   7 652.350 30.4264  13
   1   3   7 677.107 27.1467  12
  -1   3   7 658.024 29.4766  24
   1   3   7 671.562 28.5356  24
   2   3   7 8.54638 2.21174  24
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   2   3   7 11.0063 2.98805  21
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   2  -3   7 6.27701 2.61743  12
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   2  -3   7 12.5196 3.13619   2
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   2   3   7 3.53716 1.87576  12
  -2   3   7 8.86084 2.69745  25
  -3   3   7 621.210 29.7414  21
   3   3  -7 580.394 23.7968  10
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  -3  -3   7 585.238 28.9415  24
  -3  -3   7 626.137 28.8603   2
   3  -3   7 656.427 29.1268   2
   3   3   7 606.831 26.3110  12
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   3  -3   7 621.301 29.5662  12
  -3   3   7 558.211 24.3635  13
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  -3   3  -7 634.028 25.7224  26
  -3   3   7 625.388 28.9824  25
  -3   3   7 620.332 29.0576  24
   3   3   7 606.430 25.8665  24
  -4   3   7-1.08643 2.09402  24
   4   3   7 1.57378 1.43021  24
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   4   3  -7 2.73127 1.18952  10
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   4   3   7 0.72645 1.40048  12
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   4  -3   7 2.80403 2.08023   2
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   4  -3   7 2.23255 1.96413  12
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  -5   3   7 933.738 41.2717  18
  -5  -3   7 941.845 41.0906   2
   5  -3   7 902.399 40.5640   2
  -5   3  -7 936.503 41.9487  17
   5   3  -7 976.733 37.2275  10
  -5  -3   7 1021.58 43.1846  13
   5   3   7 959.215 40.0285  12
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   6  -3   7 6.16445 2.30135   2
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   6   3   7 8.01155 2.89033  12
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  -6   3   7-1.22342 1.92919  21
  -6  -3   7 2.47100 2.05311  21
  -6   3   7 2.15354 1.69900  18
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  -6  -3   7 3.54515 2.08274  13
  -6   3  -7 4.09220 2.13933  26
   6   3  -7 3.98293 1.61995  10
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  -7   3   7 8.90651 3.32504  21
   7   3   7 2.93352 2.67124  12
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   7  -3   7 3.34931 2.19252   2
  -7  -3   7 3.93584 2.24040  21
   7   3  -7 4.46900 1.71198  10
  -7   3  -7 12.0854 3.56230  17
  -7   3   7 6.99910 3.04932  18
  -7  -3   7 3.53660 2.46066  24
   7   3  -7 17.8178 3.53695   4
  -7   3  -7 9.42091 2.70142   4
  -7  -3   7 5.98910 2.67172  14
   7   3   7 2.23808 2.16428   7
  -7  -3   7 2.47500 2.58238  13
  -7   3  -7 8.17395 2.77342  26
  -8  -3   7 1.20368 2.11925  24
   8   3   7 2.13368 2.22230  12
  -8  -3  -7 4.15379 2.58496   6
  -8   3   7-1.31565 2.53685  21
  -8  -3   7 5.16758 2.01375  21
  -8   3  -7 4.97402 2.71254  26
  -8   3   7 1.25363 2.79094  18
   8   3   7 5.69842 3.10721   7
   8   3  -7 3.90856 2.21909   4
  -8   3  -7 0.78934 1.64527   4
   9   3   7 277.621 17.4548  12
  -9   3   7 316.294 19.1808  21
  -9  -3   7 308.523 18.4684  24
  -9   3   7 265.074 18.2104  18
  -9   3  -7 284.404 14.9576   4
   9   3   7 230.374 16.4820   7
  -9   3  -7 284.290 17.2460  26
  10  -3   7 5.87192 3.05569  12
  10   3   7 2.45532 2.55547  12
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 -10   3   7-1.39936 2.46183  18
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  10   3   7 3.39014 2.51469   7
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  11   3   7 39.8983 6.49337  12
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  11   3   7 20.6482 4.57049   7
 -11  -3   7 32.5319 5.98535  14
  12   3   7 2.63808 3.11323  12
 -12   3   7-1.45758 3.44022  18
 -12  -3   7 3.88603 2.88245  18
 -12   3  -7-1.29356 3.05308  17
  12   3   7 8.04481 3.53811   7
 -12  -3   7 2.84817 3.54296  14
 -12   3   7 4.07028 2.40169  14
 -12   3  -7 1.20381 2.31989  26
  12  -3   7 4.44768 3.29905  12
  13   3   7 120.822 11.7131  12
 -13   3   7 132.739 12.4063  18
 -13  -3   7 147.867 12.2749  18
 -13   3  -7 134.518 11.7331  17
 -13  -3   7 151.460 13.0324  14
 -13   3  -7 166.037 12.6088  26
  13  -3   7 136.157 12.5515  12
   0   3   8-1.14762 1.80614  21
   0   3  -8-1.79782 2.00062  17
   0  -3   8 1.17370 2.06510  24
   0  -3   8-1.13986 2.00558   2
   0   3   8-0.55987 1.52630  13
   0   3   8-0.92829 1.78930  24
  -1   3   8 13.0346 3.65910  24
  -1  -3   8 17.7546 4.30488  24
   1  -3   8 16.3340 4.14395  24
  -1   3   8 14.1537 3.63836  21
   1   3   8 17.8798 4.06858  21
  -1   3  -8 10.5100 3.15076  17
   1  -3   8 19.2044 4.20703   2
   1  -3  -8 18.7036 4.06399  10
  -1   3   8 18.0315 2.82513  13
  -1  -3   8 19.6564 4.30425  13
  -1   3   8 22.3236 4.33920  25
   1   3   8 13.6972 3.27942  24
  -2   3   8 8.64045 3.21398  24
   2   3   8 17.9891 3.34692  24
   2  -3   8 17.4296 4.31356  24
  -2   3   8 13.3252 3.72096  21
   2   3   8 14.1225 3.45089  21
   2  -3  -8 7.97699 2.75793  10
  -2   3  -8 13.1438 3.49901  17
  -2  -3   8 18.3031 4.15100   2
   2  -3   8 15.6102 3.64735   2
  -2  -3   8 10.5286 3.35161  13
   2  -3   8 10.8624 3.58388  12
   2   3   8 17.4363 3.11222  12
  -2   3   8 20.2456 4.26977  25
  -2  -3   8 12.3223 2.62889  25
  -3   3   8 1.15394 1.81596  24
   3   3   8-0.70704 1.66906  24
   3  -3   8 1.16318 1.58534  24
  -3   3   8 1.25125 2.60469  21
   3   3   8 1.05418 1.85477  21
  -3   3  -8-2.13815 1.88098  17
   3  -3  -8 1.02283 1.97135  10
  -3  -3   8-2.27167 2.36446   2
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   3  -3   8-1.23205 2.37451  12
   3   3   8-0.72902 1.72093  12
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  -4   3   8 5.99180 2.83386  18
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   4  -3   8 2.33542 2.25170  24
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   5   3   8 12.0872 3.19771  12
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   5   3  -8 8.54079 2.92246   4
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   5   3   8 2.37538 2.48734   7
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   5  -3   8 9.37676 3.29013   2
   5  -3   8 11.8068 3.87145  12
   6  -3   8-1.35935 2.83143  12
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   6  -3   9 8.75916 3.45220   2
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   2  -3  11 136.830 12.3337   2
   2   3 -11 111.678 11.5439   4
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   2   3  11 142.524 11.9262   7
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   2  -3  11 121.154 11.8766  13
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   3  -3  11 20.5034 4.96912  24
   3   3  11 23.9657 5.06386  21
   3   3 -11 16.6521 4.67551   4
  -3   3 -11 15.4695 4.47130   4
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   3   3  11 18.1391 4.37143   7
  -3   3  11 19.8199 4.91737  25
  -3   3  11 15.4479 4.90302  21
   3  -3  11 16.3476 4.46479   2
   3   3  11 18.2478 4.97968  25
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   4  -3  11 54.4970 7.73204   2
   4  -3  11 50.3155 7.30952  24
   4   3  11 62.2532 8.02006   7
   4   3  11 59.0510 7.69437  21
  -4  -3  11 43.9313 6.92428  21
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   9  -4   5 6.18279 2.31149   9
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   1   4  -6 159.626 12.1534   3
   1   4   6 184.302 9.10027  12
   1   4   6 174.693 12.0517  25
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   3   4   6 640.552 26.4291  12
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   3  -4   6 690.581 30.0059   2
   3  -4   6 612.220 29.8559  12
  -3   4  -6 634.961 27.5121  26
  -3   4  -6 667.675 30.4583   3
   3   4  -6 596.102 29.7110   3
   3   4   6 676.443 26.0725  24
   4  -4   6 219.125 14.3660  12
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   4   4   6 232.191 12.9424  21
   4  -4  -6 240.904 14.2621  10
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   4  -4   6 235.252 14.0037   2
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   4   4  -6 214.286 14.0283   3
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   4   4   6 250.094 12.4137  12
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   5   4   6-0.66127 1.56083  12
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   5   4  -6 3.75596 2.45019   3
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   5  -4   6-0.86508 1.52196   2
   5   4   6-0.64984 1.25244  21
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   6   4  -6 10.8899 2.95793   3
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  -7   4   6 825.055 32.8827  16
  -7  -4   6 838.012 37.1651  14
   7  -4   6 760.982 36.9238  12
   7   4   6 810.900 35.0276  12
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   8   4   6 18.0902 3.80630  12
  -8   4   6 21.0150 4.67076  21
  -8   4   6 27.3927 5.00432  18
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   8   4  -6 22.7287 3.75528   9
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   9  -4  -6 98.4380 8.54187   9
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   9   4  -6 110.774 8.75956   9
   9   4   6 101.032 8.25916   9
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  -9   4  -6 119.966 10.2489  26
   9  -4   6 107.536 10.6802  12
   9   4   6 107.223 9.55482  12
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  11   4   6 541.641 25.9641   7
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   0   4   7 76.5891 7.92074  21
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   1  -4   7-1.05468 1.65953   2
   1   4   7 1.05738 1.86016  25
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   2   4   7 9.71111 2.46614  24
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   2   4   7 8.52031 3.04642  25
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   5  -4   7 0.98373 2.04771   2
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   5  -4   7-1.20871 1.64715  12
   6  -4   7 26.4096 5.28045  12
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   6   4   7 38.7338 4.88721  12
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   6   4   7 32.0219 4.33906  21
   6  -4  -7 31.0798 5.51647  10
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   7  -4   7 1.31138 2.52722  12
   7   4   7 1.75688 1.82856  12
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   7  -4  -7-1.16271 2.04550  10
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   8  -4   7 20.4408 4.84165  12
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   8   4   7 21.2184 4.14131  12
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  -8   4   7 18.3176 4.75115  21
   8  -4  -7 15.8001 4.32894  10
  -8   4   7 17.5575 4.35311  18
  -8   4  -7 27.7563 5.54345  17
   8   4  -7 18.4009 3.72513   4
  -8   4  -7 20.8488 3.88451   4
  -8  -4   7 15.3139 4.19403  14
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   9   4   7-1.04544 1.83934  12
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   9  -4  -7 2.51604 2.61873  10
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   9  -4   7 1.40501 2.47185  12
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  10   4   7 1.14902 2.39170   7
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  11  -4   7-1.43248 2.98184  12
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  11   4   7-1.08798 2.42114   7
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  12   4   7 7.12747 3.97596  12
  12   4   7 9.90138 3.12976   7
  12  -4  -7 14.0250 4.02312  10
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  12  -4   7 7.00265 3.49674  12
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   0   4   8 39.2259 5.39410  24
   0  -4   8 31.7968 5.49962  13
   0  -4   8 31.3701 5.72143  24
   0   4   8 34.3045 5.64463  21
   0   4   8 38.6450 6.13652  25
   0   4  -8 33.9588 4.92814  17
   0  -4   8 42.2766 6.13771   2
   1  -4   8 175.421 12.9609  24
   1   4   8 148.994 11.8905  25
  -1   4   8 125.259 11.2640  21
   1   4   8 167.584 12.2401  21
  -1   4   8 141.007 9.37880  18
   1  -4   8 147.311 12.0042   2
  -1   4  -8 144.361 10.8367  17
  -1  -4   8 124.778 11.3600  13
  -1   4   8 138.030 10.8747  24
   1   4   8 141.733 10.0072  24
   2  -4   8 4.72763 2.63365   2
  -2  -4   8 2.51704 2.62326  24
   2  -4   8 5.03026 2.97134  24
  -2   4   8 6.35882 3.16702  21
   2   4   8 2.18438 2.10930  21
  -2   4   8 3.86054 1.82757  18
  -2   4  -8 7.19137 2.80326  17
  -2  -4   8 1.25491 2.42229  13
   2   4   8 4.88126 3.03915  25
  -2  -4   8 4.84061 2.69641   2
  -3  -4   8 462.157 25.8613  24
   3  -4   8 525.881 26.8684  24
  -3   4   8 472.017 26.4041  21
   3   4   8 505.664 25.1949  21
  -3   4   8 475.975 23.5480  18
  -3  -4   8 505.744 26.1147   2
   3  -4   8 472.509 25.4696   2
  -3   4  -8 498.320 25.3817  17
   3   4   8 483.534 26.0900  25
  -3  -4   8 500.040 26.6238  13
  -3   4   8 493.291 26.2017  25
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  -4  -4   8 52.0286 6.92019   2
   4  -4   8 64.5837 7.49640   2
  -4   4   8 46.1610 7.02765  21
   4   4   8 56.2555 6.55282  21
  -4   4   8 51.8925 6.48442  18
  -4   4  -8 67.4097 7.78492  17
  -4   4  -8 56.5790 5.60023  26
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  -4   4   8 62.5295 7.62762  25
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   5  -4   8-1.09663 2.11335   2
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   5   4   8 1.84567 2.05355  21
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  -5   4  -8 3.84448 2.18110  26
  -5   4   8-1.05239 2.19060  18
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   6  -4   8 1.04781 2.33170   2
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   6  -4   8-1.38541 2.66991  12
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  -7  -4   8 639.236 28.7836  21
   7  -4   8 612.391 32.4527  12
  -7  -4  -8 633.221 30.9128   6
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  -7   4  -8 617.401 32.1193  17
   7   4  -8 628.344 30.0011   4
  -7   4  -8 637.891 30.1566   4
   7   4   8 655.208 29.4143  12
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   7   4   8 634.063 32.0027   7
  -7   4  -8 638.923 29.6480  26
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   8   4   8 1.89317 2.10657  12
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  -8   4  -8 2.73035 2.02542   4
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   8   4   8 1.28175 2.47023   7
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  -9   4   8 72.3793 9.31995  21
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   9  -4   8 76.1817 9.24997  12
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   9   4   8 70.5187 8.54063   7
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   9   4   8 92.3692 8.81398  12
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  11   4   8 373.382 21.8491   7
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   0  -4   9 4.15965 3.08857  24
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   0   4   9 3.93461 2.32585  24
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   1  -4   9 4.14719 3.07694  24
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   1   4   9 3.85099 3.49911  21
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   2  -4   9 10.4386 3.71660   2
   2  -4   9 6.88663 3.44315  24
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   2   4   9 4.93112 2.76383  21
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  -2  -4   9 20.7459 4.62873  13
  -2   4   9 9.44353 3.37321  25
   2   4   9 6.76755 3.21229  25
   3  -4   9-1.37109 2.41207  24
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   3  -4   9 1.27596 2.45895   2
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   3   4   9 1.17131 2.60649  21
   3  -4  -9 2.40323 2.50123  10
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  -3   4   9 1.35666 2.61447  25
   3   4   9 1.36374 2.62813  25
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   4  -4   9 17.7632 4.60680  24
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   4  -4   9 12.3645 3.82299   2
   4  -4  -9 23.2460 5.04352  10
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   4   4   9 20.9813 4.47721  21
  -4   4   9 17.0911 4.00768  18
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   4   4  -9 19.0266 4.93175   4
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  -4   4   9 16.3700 3.47575   7
  -4  -4   9 24.1545 5.62677  13
   4   4   9 26.1448 5.55815  25
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   5   4   9 4.00418 3.15660   7
   5  -4   9 8.16334 4.01008  24
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   5  -4   9 4.74138 2.64526   2
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   5   4   9 5.12656 2.68284  21
   5  -4  -9 11.2445 3.81219  10
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   5   4  -9 4.88677 2.89040   4
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   6  -4   9 2.69791 2.61165  24
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   6  -4  -9 10.1940 3.75939  10
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   6   4  -9 5.78034 3.16065   4
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   6   4   9 9.45150 3.53205   7
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   7  -4   9-2.65581 2.76408  24
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   7  -4  -9-1.28949 2.48502  10
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   7   4  -9 1.06838 1.87953   4
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   7   4   9 1.35007 2.81022   7
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   8  -4   9 7.75737 3.21925  24
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   8  -4  -9 6.47371 3.53105  10
  -8   4   9 3.83898 3.34162  18
  -8   4  -9 6.96648 3.29110  17
  -8   4  -9 1.88665 2.35055   4
  -8  -4   9 5.32624 2.96593  14
   8   4   9 1.32886 2.76915   7
   8  -4   9 10.3943 4.21413  12
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   9  -4   9-1.23879 2.75762  24
  -9  -4   9 3.32867 2.47016  22
  -9   4   9 1.47008 3.06091  21
   9  -4  -9 1.28434 2.67443  10
  -9   4   9 6.53828 3.71009  18
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   9   4   9 7.70203 3.49925   7
   9  -4   9 1.46727 3.05506  12
   0  -4  10 330.945 21.0142  24
   0   4  10 285.471 19.7484  21
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   0   4 -10 338.842 21.0242   4
   0   4  10 304.178 18.7631   7
   0  -4  10 318.458 20.4837  13
   0   4  10 315.289 20.3917  25
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   1   4 -10 203.577 15.7851   4
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   1   4  10 210.774 14.8346   7
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   2  -4  10 1.38795 2.44364   2
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   2   4  10 2.64238 2.54795  21
   2   4 -10 1.41985 2.49971   4
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   2   4  10 3.82327 3.32681   7
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   3   4  10 305.570 19.3080  21
   3  -4 -10 355.713 20.1921  10
  -3   4  10 336.207 21.4547  21
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   3  -4  10 309.830 19.7877   2
   3   4 -10 327.958 20.6027   4
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   3   4  10 332.058 20.1641   7
  -3   4  10 315.095 17.3672   7
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   3   4  10 284.593 19.7450  25
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   4  -4  10 135.164 12.5548  24
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   4   4  10 169.947 12.9887  21
   4  -4 -10 161.044 12.7582  10
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   4  -4  10 169.541 13.3763   2
   4   4 -10 139.882 12.6248   4
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   4   4  10 155.226 13.1114   7
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   4   4  10 142.406 12.9784  25
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   5  -4  10 37.2170 6.42261  24
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   5  -4  10 24.5379 5.22999   2
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   5  -4 -10 40.4981 6.39683  10
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   5   4 -10 39.2419 6.32033   4
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   5   4  10 28.6950 6.28403  25
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   6   4 -10 2.35715 2.93407   4
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   6   4  10 1.36779 2.63802   7
   6   4  10 5.67773 3.35184  25
   7  -4  10 258.004 17.6620  24
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   7  -4 -10 277.357 17.7608  10
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   7   4 -10 278.119 16.9901   4
  -7   4 -10 280.051 16.7656   4
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   7   4  10 238.552 17.4575   7
   7   4  10 252.628 17.9449  25
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   0   4 -11 2.92701 3.25665   4
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   2   4  11 7.46921 3.26502   7
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   3  -4  11-1.34334 2.79619   2
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   3   4  11 1.28484 2.47604   7
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   4   4 -11 17.0117 4.95100   4
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   4   4  11 11.2461 4.15436  25
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   4   4  11 7.84660 3.43203   7
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   2  -5   0 0.94419 1.33918  19
   2   5   0 0.61428 1.27866  16
  -2   5   0 1.03948 1.15657   8
   2  -5   0 0.15012 0.51486  13
   3   5   0 111.836 8.08972   3
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   3  -5   0 129.590 6.18379  22
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   3  -5   0 112.010 7.17855  19
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   3   5   0 116.700 8.02463  16
  -3   5   0 136.263 8.39830   8
   3  -5   0 116.027 5.51115  12
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   4  -5   0 0.67147 0.78751  12
   4   5   0 0.65467 1.36272   3
   4   5   0-0.61292 1.36389  16
   4   5   0 0.17694 0.59061  25
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   5  -5   0 8.02407 1.49542  12
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   5   5   0 6.38164 1.00510  25
   5  -5   0 2.36860 1.40702   9
   5   5   0 10.3484 2.40508  16
  -5   5   0 13.1447 2.72977   8
   5   5   0 5.16500 1.98003   3
  -5   5   0 7.39508 2.01161   3
   6  -5   0-0.35787 1.01517  12
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   6  -5   0-0.86585 1.92675   9
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   6   5   0 1.79395 1.41140  16
  -6   5   0-0.86549 1.66792   8
   6   5   0-0.62821 1.48274   3
  -6   5   0 0.59713 1.32877   3
   7   5   0 109.164 7.54965   3
  -7   5   0 94.5364 7.12395   3
  -7  -5   0 109.493 8.75925   5
   7  -5   0 126.992 7.85286   1
   7  -5   0 109.390 9.12039   9
   7   5   0 115.339 7.61161  16
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   8   6   5 17.3958 3.81291   3
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  -9   6   5 21.1953 3.82420   3
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   9  -6  -5 19.4130 4.45904  10
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   1   6   8 316.335 18.9106  21
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   1   6  -8 318.320 20.4907   3
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   3   6   8 486.108 24.6153  21
   3  -6  -8 460.930 25.7578  10
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   3   6  -8 518.364 27.8625   3
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   3   6   8 526.017 27.4138  25
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   5   6   8 52.7039 7.46235  25
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  -6  -6   8 13.5103 3.90102  24
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   6  -6  -8 19.3146 4.88695  10
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   7  -6  -8 396.806 22.9344  10
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   9   6   8 13.5704 4.24188   7
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   9  -6   8 12.9588 3.82714  12
   9   6   8 9.26269 3.65669  25
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   1   6   9 13.6739 4.16805  21
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   0 -10  -2 255.587 19.2098   1
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  -3 -11   0 1.50014 2.89365   1
   3 -11   0 7.38228 3.28786   1
   3  11   0 9.35888 4.25288   3
  -3  11   0 1.51478 2.92184   3
   4 -11   0 1.39477 2.90344  11
   4 -11   0-0.93533 2.54935  19
   4  11   0-1.49485 3.71918   3
  -4  11   0-1.44131 4.08860   3
  -4 -11   0-1.43345 3.18996   1
   4 -11   0-1.40786 3.67371   1
   5 -11   0 15.6122 4.90806  11
   5  11   0 21.1193 5.57440   3
  -5  11   0 17.5758 4.67925   3
  -5 -11   0 17.2639 4.59775  15
  -5 -11   0 14.7900 4.65398   1
   5 -11   0 25.1038 5.53660   1
  -6 -11   0-4.92853 4.44327   1
   6 -11   0-1.21412 4.27287   1
   6 -11   0-1.42363 2.96493  11
   6  11   0-5.17365 4.88111   3
  -6  11   0-3.71702 4.36042   3
  -6 -11   0-1.30146 2.05016  15
   0 -11   1 1.25059 2.41011  19
   0  11  -1 1.62754 3.13650   3
   0  11   1-1.63008 3.14141   3
   0 -11  -1-1.56230 2.74847   1
   0 -11   1 6.26855 3.69883   1
   1 -11  -1 3.57075 2.96140  11
  -1 -11   1-1.27816 2.84440  19
   1 -11   1 1.20896 2.33004  19
   1  11  -1 1.62687 3.13534   3
  -1 -11  -1-1.25069 2.20048  15
   1  11   1 1.62765 3.62207   3
   1 -11  -1 1.54875 2.98480   1
   1 -11   1 1.55361 3.23405   1
   2  11   1 566.634 31.0865   3
  -2  11   1 573.006 30.6873   3
   2 -11  -1 571.265 28.7258  11
  -2 -11   1 520.441 29.7134   1
   2 -11   1 526.791 29.8786   1
  -2 -11   1 582.730 29.2403  19
   2 -11   1 561.225 27.9438  19
  -2 -11  -1 536.282 30.0445   1
   2 -11  -1 594.874 30.7150   1
  -2 -11  -1 460.762 27.4570  15
   2  11  -1 578.314 31.2046   3
  -2  11  -1 482.816 29.2115   3
   3 -11  -1 1.46767 3.05531   1
  -3 -11   1 2.99287 3.33022   1
   3 -11   1 4.42554 3.07094   1
   3 -11   1 4.20458 3.11905  11
   3 -11  -1-1.30300 2.29268  11
   3 -11   1 3.28713 3.10844  19
   3  11  -1 4.68372 3.68513   3
  -3  11  -1-1.51339 2.91681   3
  -3 -11  -1-1.31594 2.31544  15
   3  11   1-1.55750 3.24226   3
  -3  11   1 4.54340 3.37034   3
  -3 -11  -1 1.49063 2.62269   1
   4 -11   1 48.4864 7.73371  11
   4 -11  -1 43.1405 6.68246  11
  -4 -11  -1 34.2325 6.59264   1
  -4 -11   1 34.3954 6.22690   1
   4 -11  -1 29.4383 6.29392   1
   4 -11   1 39.4400 6.88081   1
   4 -11   1 50.8775 6.30229  19
   4  11  -1 41.7973 7.37012   3
  -4  11  -1 33.0461 6.54181   3
   4  11   1 43.1502 7.25329   3
  -4  11   1 45.9799 7.54036   3
  -4 -11  -1 37.1547 6.49865  15
   5 -11   1 15.8289 4.57762  11
   5 -11  -1 31.7195 5.88110  11
   5 -11   1 20.3017 4.03244  19
  -5 -11   1 17.5110 4.78632   1
   5 -11   1 14.5399 4.33962   1
  -5 -11  -1 29.3755 5.79259   1
   5 -11  -1 31.5632 5.89110   1
   5  11  -1 15.4580 5.22866   3
  -5  11  -1 6.73333 3.87818   3
   5  11   1 22.3965 5.76132   3
  -5  11   1 28.2780 5.74417   3
   6 -11  -1 315.916 19.5981  11
  -6 -11   1 288.750 18.2700   1
   6 -11   1 289.654 18.3091   1
  -6 -11  -1 314.927 19.2236  15
  -6 -11   1 261.315 17.8394  15
  -6 -11  -1 256.581 17.5703   1
   6 -11  -1 243.072 17.0504   1
   6  11  -1 272.571 18.1934   3
  -6  11  -1 270.016 17.8156   3
   6  11   1 228.877 17.0925   3
  -6  11   1 309.704 18.5505   3
   0 -11   2 2.55669 2.66094  19
   0 -11  -2 1.55356 2.44454   1
   0  11  -2 1.61539 3.36249   3
   0 -11  -2-2.29300 2.85240  15
   0  11   2 1.62867 3.13866   3
   1 -11  -2 12.0776 3.79851  11
  -1 -11   2 22.0645 4.81565  19
   1 -11   2 17.4436 4.82837  19
   1  11  -2 8.07594 4.94701   3
   1 -11  -2 10.7756 4.39533   1
  -1 -11  -2 10.8663 3.58936  15
   1 -11  -2 22.5639 4.80814  15
   1  11   2 16.2605 5.45064   3
  -2 -11  -2 6.23724 2.71883   6
   2 -11  -2 3.50462 2.60353  11
   2 -11   2 4.80769 3.13951  19
   2  11  -2 3.19191 3.55430   3
  -2  11  -2 3.11895 3.24928   3
  -2 -11  -2 1.52538 3.79771   1
   2 -11  -2 3.01479 3.56070   1
  -2 -11  -2 3.76846 3.12850  15
   2 -11  -2 5.93701 3.11726  15
   2  11   2 6.40974 4.18375   3
  -2  11   2 3.14570 3.71507   3
  -3 -11  -2 1.79613 2.12381   6
   3 -11  -2 6.15398 3.21430  11
  -3 -11   2 7.84947 3.56791  19
   3 -11   2 8.02207 3.12611  19
   3  11  -2 6.21818 3.67148   3
  -3  11  -2 1.50422 2.64958   3
  -3 -11  -2 3.87414 3.52197  15
   3 -11  -2 8.90205 2.89073  15
   3  11   2 3.11256 3.24216   3
  -3  11   2-1.51417 2.38624   3
  -3 -11  -2 5.92534 3.86757   1
   3 -11  -2 2.91609 2.81297   1
  -4 -11  -2 1.80605 2.00990   6
   4 -11  -2 5.12652 3.49314  11
  -4 -11   2 2.58294 2.87415  19
   4 -11   2-1.07573 2.67665  19
  -4 -11  -2 1.41430 2.94419   1
   4  11  -2 1.48594 3.09329   3
  -4  11  -2 4.27852 4.04575   3
   4 -11  -2 1.39182 2.89742   1
  -4 -11  -2 3.93205 3.26111  15
   4  11   2-1.48330 2.60977   3
  -4  11   2 1.43354 2.98424   3
  -5 -11   2-1.33757 2.57765   1
   5 -11   2-1.31069 2.91660   1
  -5 -11  -2 1.32116 3.28691   1
   5 -11  -2 3.95136 3.10870  11
   5 -11  -2-1.30551 2.51588   1
  -5 -11  -2-1.06459 2.64860  20
   5 -11   2 2.97504 2.34060  19
   5  11  -2 1.39282 2.89918   3
  -5  11  -2-1.33030 2.56365   3
  -5 -11  -2 1.31642 2.92935  15
   5  11   2-1.38656 3.27259   3
  -5  11   2-1.33502 3.32139   3
   0 -11  -3-1.54063 3.20736   1
   0 -11   3-1.29256 2.69110  19
   0  11  -3-1.60165 2.81822   3
   0 -11  -3-1.08368 2.25643  15
   0  11   3-3.24473 3.12700   3
   1 -11  -3 60.0147 6.77173  11
   1 -11   3 48.1425 6.92996  19
   1  11  -3 54.4872 8.27602   3
   1  11   3 43.1751 7.60069  16
   1 -11  -3 53.4354 7.99455   1
  -1 -11  -3 48.5898 6.75041  15
   1 -11  -3 46.0209 6.31429  15
   1  11   3 77.7252 9.78907   3
   2  11   3 180.175 15.4317   3
  -2  11   3 206.395 16.1511   3
   2 -11  -3 208.704 13.9438  11
  -2 -11   3 145.683 13.2982  19
   2 -11   3 212.694 14.7737  19
   2  11   3 200.066 15.7988  16
  -2 -11  -3 180.808 13.9484  15
   2 -11  -3 175.448 12.2381  15
  -2 -11  -3 184.278 15.1878   1
   2 -11  -3 174.769 14.7721   1
   2  11  -3 188.235 15.6801   3
  -2  11  -3 185.235 15.4140   3
  -2 -11  -3 179.663 13.0171   6
  -3 -11  -3 1.01074 2.51462   6
   3 -11  -3 2.27131 2.52710  11
  -3 -11   3 1.30209 2.50927  19
   3 -11   3-3.53996 2.78502  19
   3 -11  -3-1.44381 2.78237   1
   3  11  -3 1.53594 2.95993   3
  -3  11  -3-1.48375 3.08845   3
   3  11   3 3.02935 2.91894  16
  -3 -11  -3 2.92637 3.25593   1
  -3 -11  -3 1.25510 2.41871  15
   3  11   3-1.54519 3.64699   3
  -3  11   3-1.50399 3.34673   3
  -4 -11  -3 55.6538 6.93943   6
   4 -11  -3 72.7585 8.25923  11
  -4 -11   3 58.8182 7.63651  19
   4 -11   3 70.3369 8.02055  19
   4  11  -3 67.6233 8.97783   3
  -4  11  -3 71.8271 9.04500   3
   4  11   3 85.1263 10.0179  16
  -4 -11  -3 69.2368 8.41520  15
   4  11   3 63.3488 9.07009   3
  -4  11   3 89.6833 10.0509   3
   0  11  -4-4.73798 2.77886   3
   0 -11  -4-1.00957 2.51225  15
   0  11   4 1.59850 3.32773   3
  -1 -11   4-1.29984 2.28668  19
   1 -11   4-2.54297 2.82935  19
   1  11  -4 1.57873 3.51305   3
  -1  11   4 1.46311 2.57390  16
   1  11   4-1.51808 2.92551  16
   1 -11  -4 7.32947 2.79164  15
  -1 -11  -4 1.08800 2.83895  15
   1  11   4 1.59473 3.31946   3
  -2 -11   4 1.29687 2.70134  19
   2 -11   4 3.71731 2.75914  19
   2  11  -4 3.10552 3.45673   3
  -2  11  -4 6.05803 3.15409   3
   2  11   4 1.51619 2.92360  16
  -2 -11  -4 3.45569 2.39981  15
   2  11   4 1.56652 2.75767   3
  -2  11   4 3.07481 3.42258   3
  -3 -11  -4 17.4886 4.07663   6
   3 -11  -4 23.3418 4.48469  11
  -3 -11   4 15.3522 4.31109  19
   3 -11   4 15.5194 4.02844  19
   3  11  -4 10.5479 4.14908   3
  -3  11  -4 11.6370 4.61574   3
   3  11   4 23.9007 5.54398  16
  -3 -11  -4 16.8029 4.46828  15
   3  11   4 33.3180 6.33242   3
  -3  11   4 13.2682 4.67699   3
   0   0   0    0.00    0.00   0
TITL Rh2S3_001 in Pbcn
REM Pbcn (#60, found as Pbna in cab setting)
CELL 0.71073   8.467198   5.985370   6.139212  90.0000  90.0000  90.0000
ZERR    4.00   0.000264   0.000177   0.000188   0.0000   0.0000   0.0000
LATT  1
SYMM -x+1/2,-y+1/2, z+1/2
SYMM -x, y,-z+1/2
SYMM  x+1/2,-y+1/2,-z
SFAC S Rh
UNIT 12.00 8.00
TREF
HKLF 4
END
;
_shelx_hkl_checksum              80869
_shelx_res_file
;
TITL Rh2S3_001_synergy in Pbcn #60
    rh2s3_001_synergy.res
    created by SHELXL-2018/3 at 13:27:58 on 07-Jun-2022
REM reset to Pbcn #60
CELL 0.71073 8.467198 5.98537 6.139212 90 90 90
ZERR 4 0.000264 0.000177 0.000188 0 0 0
LATT 1
SYMM 0.5-X,0.5-Y,0.5+Z
SYMM 0.5+X,0.5-Y,-Z
SYMM -X,+Y,0.5-Z
SFAC S Rh
UNIT 12 8
L.S. 4
PLAN  5
SIZE 0.029 0.024 0.022
TEMP 21
CONF
MORE -1
fmap 2
acta
OMIT -2 82
REM <olex2.extras>
REM <HklSrc "%.\\Rh2S3_001_synergy.hkl">
REM </olex2.extras>
WGHT    0.020800    0.198300
EXTI    0.040000
FVAR       0.23890
RH1   2    0.106396    0.251300    0.033459    11.00000    0.00369    0.00356 =
         0.00372    0.00005   -0.00013   -0.00002
S1    1    0.151659    0.390985    0.393068    11.00000    0.00448    0.00453 =
         0.00502   -0.00032   -0.00027    0.00015
S2    1    0.000000    0.952139    0.250000    10.50000    0.00530    0.00429 =
         0.00460    0.00000   -0.00040    0.00000
HKLF 4
REM  Rh2S3_001_synergy in Pbcn #60
REM wR2 = 0.0451, GooF = S = 1.140, Restrained GooF = 1.140 for all data
REM R1 = 0.0176 for 893 Fo > 4sig(Fo) and 0.0210 for all 1025 data
REM 25 parameters refined using 0 restraints
END
WGHT      0.0208      0.1981
REM Highest difference peak  1.109,  deepest hole -2.751,  1-sigma level  0.405
Q1    1   0.0919  0.3679  0.0565  11.00000  0.05    1.11
Q2    1   0.1264  0.1214  0.0220  11.00000  0.05    1.08
Q3    1   0.1056  0.5135  0.5391  11.00000  0.05    0.98
Q4    1   0.1320  0.0373  0.0016  11.00000  0.05    0.95
Q5    1   0.0261  1.0263  0.4802  11.00000  0.05    0.94
;
_shelx_res_checksum              45932
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, -y+1/2, z+1/2'
'x+1/2, -y+1/2, -z'
'-x, y, -z+1/2'
'-x, -y, -z'
'x-1/2, y-1/2, -z-1/2'
'-x-1/2, y-1/2, z'
'x, -y, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Rh Rh1 0.10640(2) 0.25130(2) 0.03346(2) 0.00365(5) Uani d 1 . .
S S1 0.15166(5) 0.39098(6) 0.39307(6) 0.00468(7) Uani d 1 . .
S S2 0.000000 0.95214(9) 0.250000 0.00473(9) Uani d 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Rh1 0.00369(7) 0.00356(7) 0.00372(7) -0.00002(3) -0.00013(3) 0.00005(3)
S1 0.00448(14) 0.00453(14) 0.00502(14) 0.00015(11) -0.00027(11) -0.00032(11)
S2 0.00530(19) 0.00429(19) 0.00460(19) 0.000 -0.00040(15) 0.000
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rh Rh -1.1178 0.9187 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
S1 Rh1 S1 8_565 2_554 93.041(12) ?
S1 Rh1 S1 2_554 . 108.750(11) ?
S1 Rh1 S1 8_565 4 84.194(14) ?
S1 Rh1 S1 4 . 81.345(16) ?
S1 Rh1 S1 8_565 . 89.651(9) ?
S1 Rh1 S1 2_554 4 169.564(8) ?
S1 Rh1 S2 . 1_545 79.051(12) ?
S1 Rh1 S2 4 1_545 79.228(12) ?
S1 Rh1 S2 2_554 1_545 104.843(13) ?
S1 Rh1 S2 8_565 1_545 161.128(14) ?
S2 Rh1 S1 5_565 . 160.625(13) ?
S2 Rh1 S1 5_565 4 88.276(12) ?
S2 Rh1 S1 5_565 8_565 105.609(15) ?
S2 Rh1 S1 5_565 2_554 82.767(11) ?
S2 Rh1 S2 5_565 1_545 82.977(6) ?
Rh1 S1 Rh1 4 . 84.556(13) ?
Rh1 S1 Rh1 8_566 4 95.806(14) ?
Rh1 S1 Rh1 2 4 126.529(17) ?
Rh1 S1 Rh1 8_566 2 109.574(16) ?
Rh1 S1 Rh1 2 . 110.312(15) ?
Rh1 S1 Rh1 8_566 . 129.325(18) ?
Rh1 S2 Rh1 5_565 8_566 116.29(2) ?
Rh1 S2 Rh1 4_565 1_565 83.775(18) ?
Rh1 S2 Rh1 5_565 4_565 131.573(9) ?
Rh1 S2 Rh1 8_566 1_565 131.573(9) ?
Rh1 S2 Rh1 8_566 4_565 97.023(5) ?
Rh1 S2 Rh1 5_565 1_565 97.023(6) ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Rh1 S1 8_565 2.3396(4) ?
Rh1 S1 2_554 2.3801(4) ?
Rh1 S1 . 2.3916(4) ?
Rh1 S1 4 2.3826(4) ?
Rh1 S2 1_545 2.4052(4) ?
Rh1 S2 5_565 2.3071(3) ?

_cod_database_fobs_code 2022680